NC0038377_J15090208report_20171101

13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number:J15090208
Project Name:MAYO STEAM - AB GW ASSESSMENT WATER
Lab Contact:Mary Ann Ogle
Date:9/18/2015
Customer Address:
Customer Name(s):Tim Hunsucker, Jerry Wylie,Brandon Russo, Kathy Webb, John Toepfer
Phone: [phone]
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.
Mary Ann Ogle
Page 1 of 103
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection
Date and Time Collected By Sample Description
2015029903 MAYO STEAM 09-Sep-15 11:15 AM Erin Black MW-16S
2015029904 MAYO STEAM 09-Sep-15 10:04 AM Erin Black MW-16D
2015029905 MAYO STEAM 09-Sep-15 10:04 AM Erin Black MW-16D Dup
2015029906 MAYO STEAM 09-Sep-15 11:55 AM Erin Black MW-16BR
2015029907 MAYO STEAM 09-Sep-15 10:30 AM Erin Black MW-05BR
2015029908 MAYO STEAM 09-Sep-15 Erin Black CW-4
2015029909 MAYO STEAM 09-Sep-15 5:00 PM Erin Black CW-6
2015029910 MAYO STEAM 09-Sep-15 2:15 PM Erin Black CW-5
2015029911 MAYO STEAM 09-Sep-15 9:25 AM Erin Black MW-14BR
2015029912 MAYO STEAM 09-Sep-15 10:13 AM Erin Black MW-4
2015029913 MAYO STEAM 09-Sep-15 2:37 PM Erin Black ABMW-04
2015029914 MAYO STEAM 09-Sep-15 1:07 PM Erin Black ABMW-04D
2015029915 MAYO STEAM 09-Sep-15 11:16 AM Erin Black ABMW-04BR
2015029916 MAYO STEAM 09-Sep-15 11:45 AM Erin Black Filter Blank
2015029917 MAYO STEAM 09-Sep-15 11:45 AM Erin Black Equipment Blank
15 Total Samples
Page 2 of 103
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:DBA Account Date:9/18/2015
Electronic Data Deliverable (EDD) Sent Separately
Page 3 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029903
Collection Date:09-Sep-15 11:15 AM
Site:MW-16S
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.037 mg-N/L EPA 353.2 09/14/2015 13:32 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 12 mg/L EPA 300.0 09/10/2015 16:55 BGN9034110
Sulfate 2.6 mg/L EPA 300.0 09/10/2015 16:55 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 11:34 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 13:04 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 14:08 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.020 mg/L EPA 200.7 09/11/2015 10:43 FCJORDA0.005 1
Barium (Ba)0.046 mg/L EPA 200.7 09/11/2015 10:43 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 10:43 FCJORDA0.05 1
Iron (Fe)4.00 mg/L EPA 200.7 09/11/2015 10:43 FCJORDA0.01 1
Manganese (Mn)0.686 mg/L EPA 200.7 09/11/2015 10:43 FCJORDA0.005 1
Strontium (Sr)0.130 mg/L EPA 200.7 09/11/2015 10:43 FCJORDA0.005 1
Zinc (Zn)0.012 mg/L EPA 200.7 09/11/2015 10:43 FCJORDA0.005 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)0.009 mg/L EPA 200.7 09/11/2015 13:07 FCJORDA0.005 1
Barium (Ba)0.048 mg/L EPA 200.7 09/11/2015 13:07 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 13:07 FCJORDA0.05 1
Iron (Fe)4.19 mg/L EPA 200.7 09/11/2015 13:07 FCJORDA0.01 1
Manganese (Mn)0.696 mg/L EPA 200.7 09/11/2015 13:07 FCJORDA0.005 1
Strontium (Sr)0.134 mg/L EPA 200.7 09/11/2015 13:07 FCJORDA0.005 1
Zinc (Zn)0.013 mg/L EPA 200.7 09/11/2015 13:07 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)11.1 mg/L EPA 200.7 09/15/2015 09:29 FCJORDA0.01 1
Magnesium (Mg)4.18 mg/L EPA 200.7 09/15/2015 09:29 FCJORDA0.005 1
Potassium (K)1.99 mg/L EPA 200.7 09/15/2015 09:29 FCJORDA0.1 1
Sodium (Na)9.54 mg/L EPA 200.7 09/15/2015 09:29 FCJORDA0.05 1
Page 4 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029903
Collection Date:09-Sep-15 11:15 AM
Site:MW-16S
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.018 mg/L EPA 200.7 09/15/2015 09:24 MHH71310.005 1
Barium (Ba)0.050 mg/L EPA 200.7 09/15/2015 09:24 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 09:24 MHH71310.05 1
Iron (Fe)3.86 mg/L EPA 200.7 09/15/2015 09:24 MHH71310.01 1
Manganese (Mn)0.768 mg/L EPA 200.7 09/15/2015 09:24 MHH71310.005 1
Strontium (Sr)0.131 mg/L EPA 200.7 09/15/2015 09:24 MHH71310.005 1
Zinc (Zn)0.010 mg/L EPA 200.7 09/15/2015 09:24 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 15:23 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 15:23 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 15:23 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 15:23 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 15:23 JAHERMA11
Cobalt (Co)9.73 ug/L EPA 200.8 09/15/2015 15:23 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 15:23 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 15:23 JAHERMA11
Molybdenum (Mo)1.31 ug/L EPA 200.8 09/15/2015 15:23 JAHERMA11
Nickel (Ni)1.65 ug/L EPA 200.8 09/15/2015 15:23 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 15:23 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 15:23 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 15:23 JAHERMA0.3 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 12:31 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 12:31 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 12:31 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 12:31 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 12:31 MHALL311
Cobalt (Co)9.59 ug/L EPA 200.8 09/15/2015 12:31 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 12:31 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 12:31 MHALL311
Molybdenum (Mo)1.10 ug/L EPA 200.8 09/15/2015 12:31 MHALL311
Nickel (Ni)1.32 ug/L EPA 200.8 09/15/2015 12:31 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 12:31 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 12:31 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 12:31 MHALL30.3 1
Page 5 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029903
Collection Date:09-Sep-15 11:15 AM
Site:MW-16S
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 21:06 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 21:06 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 21:06 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 21:06 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 21:06 JAHERMA11
Cobalt (Co)10.3 ug/L EPA 200.8 09/15/2015 21:06 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 21:06 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 21:06 JAHERMA11
Molybdenum (Mo)1.24 ug/L EPA 200.8 09/15/2015 21:06 JAHERMA11
Nickel (Ni)1.31 ug/L EPA 200.8 09/15/2015 21:06 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 21:06 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 21:06 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 21:06 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 110 mg/L SM2540C 09/10/2015 15:23 CJELLIO251
Total Carbon
TOC 0.479 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 09/10/2015 11:27 GHUTCHI51
Page 6 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029904
Collection Date:09-Sep-15 10:04 AM
Site:MW-16D
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)3.1 mg-N/L EPA 353.2 09/14/2015 13:41 LSTARL10.05 5
INORGANIC IONS BY IC
Chloride 8.8 mg/L EPA 300.0 09/10/2015 16:02 BGN90340.1 1
Sulfate 7.0 mg/L EPA 300.0 09/10/2015 16:02 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 11:37 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 13:06 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 14:10 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 09/11/2015 10:55 FCJORDA0.005 1
Barium (Ba)0.011 mg/L EPA 200.7 09/11/2015 10:55 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 10:55 FCJORDA0.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 09/11/2015 10:55 FCJORDA0.01 1
Manganese (Mn)0.161 mg/L EPA 200.7 09/11/2015 10:55 FCJORDA0.005 1
Strontium (Sr)0.169 mg/L EPA 200.7 09/11/2015 10:55 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/11/2015 10:55 FCJORDA0.005 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)< 0.005 mg/L EPA 200.7 09/11/2015 13:18 FCJORDA0.005 1
Barium (Ba)0.011 mg/L EPA 200.7 09/11/2015 13:18 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 13:18 FCJORDA0.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 09/11/2015 13:18 FCJORDA0.01 1
Manganese (Mn)0.139 mg/L EPA 200.7 09/11/2015 13:18 FCJORDA0.005 1
Strontium (Sr)0.166 mg/L EPA 200.7 09/11/2015 13:18 FCJORDA0.005 1
Zinc (Zn)0.022 mg/L EPA 200.7 09/11/2015 13:18 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)25.2 mg/L EPA 200.7 09/15/2015 09:40 FCJORDA0.01 1
Magnesium (Mg)5.07 mg/L EPA 200.7 09/15/2015 09:40 FCJORDA0.005 1
Potassium (K)2.15 mg/L EPA 200.7 09/15/2015 09:40 FCJORDA0.1 1
Sodium (Na)9.69 mg/L EPA 200.7 09/15/2015 09:40 FCJORDA0.05 1
Page 7 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029904
Collection Date:09-Sep-15 10:04 AM
Site:MW-16D
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.074 mg/L EPA 200.7 09/15/2015 09:36 MHH71310.005 1
Barium (Ba)0.010 mg/L EPA 200.7 09/15/2015 09:36 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 09:36 MHH71310.05 1
Iron (Fe)0.079 mg/L EPA 200.7 09/15/2015 09:36 MHH71310.01 1
Manganese (Mn)0.141 mg/L EPA 200.7 09/15/2015 09:36 MHH71310.005 1
Strontium (Sr)0.166 mg/L EPA 200.7 09/15/2015 09:36 MHH71310.005 1
Zinc (Zn)0.044 mg/L EPA 200.7 09/15/2015 09:36 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 15:43 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 15:43 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 15:43 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 15:43 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 15:43 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 15:43 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 15:43 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 15:43 JAHERMA11
Molybdenum (Mo)8.56 ug/L EPA 200.8 09/15/2015 15:43 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 15:43 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 15:43 JAHERMA11
Thallium (Tl) Low Level 0.256 ug/L EPA 200.8 09/15/2015 15:43 JAHERMA0.2 1
Vanadium (V) Low Level 0.489 ug/L EPA 200.8 09/15/2015 15:43 JAHERMA0.3 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 12:46 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 12:46 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 12:46 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 12:46 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 12:46 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 12:46 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 12:46 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 12:46 MHALL311
Molybdenum (Mo)7.64 ug/L EPA 200.8 09/15/2015 12:46 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 12:46 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 12:46 MHALL311
Thallium (Tl) Low Level 0.221 ug/L EPA 200.8 09/15/2015 12:46 MHALL30.2 1
Vanadium (V) Low Level 0.523 ug/L EPA 200.8 09/15/2015 12:46 MHALL30.3 1
Page 8 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029904
Collection Date:09-Sep-15 10:04 AM
Site:MW-16D
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 20:46 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 20:46 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 20:46 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 20:46 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 20:46 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 20:46 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 20:46 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 20:46 JAHERMA11
Molybdenum (Mo)8.23 ug/L EPA 200.8 09/15/2015 20:46 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 20:46 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 20:46 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 20:46 JAHERMA0.2 1
Vanadium (V) Low Level 0.676 ug/L EPA 200.8 09/15/2015 20:46 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 150 mg/L SM2540C 09/10/2015 15:23 CJELLIO251
Total Carbon
TOC 1.1 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 09/10/2015 11:27 GHUTCHI51
Page 9 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029905
Collection Date:09-Sep-15 10:04 AM
Site:MW-16D Dup
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)3.0 mg-N/L EPA 353.2 09/14/2015 13:43 LSTARL10.05 5
INORGANIC IONS BY IC
Chloride 8.8 mg/L EPA 300.0 09/10/2015 16:20 BGN90340.1 1
Sulfate 7.0 mg/L EPA 300.0 09/10/2015 16:20 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 11:39 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 13:09 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 14:13 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 09/11/2015 10:59 FCJORDA0.005 1
Barium (Ba)0.009 mg/L EPA 200.7 09/11/2015 10:59 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 10:59 FCJORDA0.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 09/11/2015 10:59 FCJORDA0.01 1
Manganese (Mn)0.157 mg/L EPA 200.7 09/11/2015 10:59 FCJORDA0.005 1
Strontium (Sr)0.166 mg/L EPA 200.7 09/11/2015 10:59 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/11/2015 10:59 FCJORDA0.005 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)< 0.005 mg/L EPA 200.7 09/11/2015 13:22 FCJORDA0.005 1
Barium (Ba)0.010 mg/L EPA 200.7 09/11/2015 13:22 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 13:22 FCJORDA0.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 09/11/2015 13:22 FCJORDA0.01 1
Manganese (Mn)0.159 mg/L EPA 200.7 09/11/2015 13:22 FCJORDA0.005 1
Strontium (Sr)0.166 mg/L EPA 200.7 09/11/2015 13:22 FCJORDA0.005 1
Zinc (Zn)0.006 mg/L EPA 200.7 09/11/2015 13:22 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)25.2 mg/L EPA 200.7 09/15/2015 09:44 FCJORDA0.01 1
Magnesium (Mg)5.07 mg/L EPA 200.7 09/15/2015 09:44 FCJORDA0.005 1
Potassium (K)2.13 mg/L EPA 200.7 09/15/2015 09:44 FCJORDA0.1 1
Sodium (Na)9.66 mg/L EPA 200.7 09/15/2015 09:44 FCJORDA0.05 1
Page 10 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029905
Collection Date:09-Sep-15 10:04 AM
Site:MW-16D Dup
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.089 mg/L EPA 200.7 09/15/2015 09:40 MHH71310.005 1
Barium (Ba)0.010 mg/L EPA 200.7 09/15/2015 09:40 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 09:40 MHH71310.05 1
Iron (Fe)0.090 mg/L EPA 200.7 09/15/2015 09:40 MHH71310.01 1
Manganese (Mn)0.143 mg/L EPA 200.7 09/15/2015 09:40 MHH71310.005 1
Strontium (Sr)0.166 mg/L EPA 200.7 09/15/2015 09:40 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 09:40 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 15:50 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 15:50 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 15:50 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 15:50 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 15:50 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 15:50 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 15:50 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 15:50 JAHERMA11
Molybdenum (Mo)8.57 ug/L EPA 200.8 09/15/2015 15:50 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 15:50 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 15:50 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 15:50 JAHERMA0.2 1
Vanadium (V) Low Level 0.531 ug/L EPA 200.8 09/15/2015 15:50 JAHERMA0.3 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 12:51 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 12:51 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 12:51 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 12:51 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 12:51 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 12:51 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 12:51 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 12:51 MHALL311
Molybdenum (Mo)8.39 ug/L EPA 200.8 09/15/2015 12:51 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 12:51 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 12:51 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 12:51 MHALL30.2 1
Vanadium (V) Low Level 0.538 ug/L EPA 200.8 09/15/2015 12:51 MHALL30.3 1
Page 11 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029905
Collection Date:09-Sep-15 10:04 AM
Site:MW-16D Dup
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 21:12 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 21:12 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 21:12 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 21:12 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 21:12 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 21:12 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 21:12 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 21:12 JAHERMA11
Molybdenum (Mo)8.06 ug/L EPA 200.8 09/15/2015 21:12 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 21:12 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 21:12 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 21:12 JAHERMA0.2 1
Vanadium (V) Low Level 0.772 ug/L EPA 200.8 09/15/2015 21:12 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 150 mg/L SM2540C 09/10/2015 15:23 CJELLIO251
Total Carbon
TOC 0.269 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 09/10/2015 11:27 GHUTCHI51
Page 12 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029906
Collection Date:09-Sep-15 11:55 AM
Site:MW-16BR
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.014 mg-N/L EPA 353.2 09/14/2015 13:35 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 6.9 mg/L EPA 300.0 09/10/2015 17:13 BGN90340.1 1
Sulfate 7.3 mg/L EPA 300.0 09/10/2015 17:13 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 11:42 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 13:21 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 14:15 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.021 mg/L EPA 200.7 09/11/2015 11:03 FCJORDA0.005 1
Barium (Ba)0.007 mg/L EPA 200.7 09/11/2015 11:03 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 11:03 FCJORDA0.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 09/11/2015 11:03 FCJORDA0.01 1
Manganese (Mn)0.016 mg/L EPA 200.7 09/11/2015 11:03 FCJORDA0.005 1
Strontium (Sr)0.084 mg/L EPA 200.7 09/11/2015 11:03 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/11/2015 11:03 FCJORDA0.005 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)0.022 mg/L EPA 200.7 09/11/2015 13:26 FCJORDA0.005 1
Barium (Ba)0.007 mg/L EPA 200.7 09/11/2015 13:26 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 13:26 FCJORDA0.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 09/11/2015 13:26 FCJORDA0.01 1
Manganese (Mn)0.015 mg/L EPA 200.7 09/11/2015 13:26 FCJORDA0.005 1
Strontium (Sr)0.084 mg/L EPA 200.7 09/11/2015 13:26 FCJORDA0.005 1
Zinc (Zn)0.007 mg/L EPA 200.7 09/11/2015 13:26 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)17.6 mg/L EPA 200.7 09/15/2015 09:48 FCJORDA0.01 1
Magnesium (Mg)2.56 mg/L EPA 200.7 09/15/2015 09:48 FCJORDA0.005 1
Potassium (K)1.93 mg/L EPA 200.7 09/15/2015 09:48 FCJORDA0.1 1
Sodium (Na)28.5 mg/L EPA 200.7 09/15/2015 09:48 FCJORDA0.05 1
Page 13 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029906
Collection Date:09-Sep-15 11:55 AM
Site:MW-16BR
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.033 mg/L EPA 200.7 09/15/2015 09:44 MHH71310.005 1
Barium (Ba)0.007 mg/L EPA 200.7 09/15/2015 09:44 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 09:44 MHH71310.05 1
Iron (Fe)0.022 mg/L EPA 200.7 09/15/2015 09:44 MHH71310.01 1
Manganese (Mn)0.016 mg/L EPA 200.7 09/15/2015 09:44 MHH71310.005 1
Strontium (Sr)0.080 mg/L EPA 200.7 09/15/2015 09:44 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 09:44 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)1.18 ug/L EPA 200.8 09/15/2015 15:56 JAHERMA11
Arsenic (As)1.38 ug/L EPA 200.8 09/15/2015 15:56 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 15:56 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 15:56 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 15:56 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 15:56 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 15:56 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 15:56 JAHERMA11
Molybdenum (Mo)34.6 ug/L EPA 200.8 09/15/2015 15:56 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 15:56 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 15:56 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 15:56 JAHERMA0.2 1
Vanadium (V) Low Level 1.51 ug/L EPA 200.8 09/15/2015 15:56 JAHERMA0.3 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)1.36 ug/L EPA 200.8 09/15/2015 12:56 MHALL311
Arsenic (As)1.41 ug/L EPA 200.8 09/15/2015 12:56 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 12:56 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 12:56 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 12:56 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 12:56 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 12:56 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 12:56 MHALL311
Molybdenum (Mo)33.7 ug/L EPA 200.8 09/15/2015 12:56 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 12:56 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 12:56 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 12:56 MHALL30.2 1
Vanadium (V) Low Level 1.50 ug/L EPA 200.8 09/15/2015 12:56 MHALL30.3 1
Page 14 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029906
Collection Date:09-Sep-15 11:55 AM
Site:MW-16BR
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)1.39 ug/L EPA 200.8 09/15/2015 21:19 JAHERMA11
Arsenic (As)1.45 ug/L EPA 200.8 09/15/2015 21:19 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 21:19 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 21:19 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 21:19 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 21:19 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 21:19 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 21:19 JAHERMA11
Molybdenum (Mo)34.9 ug/L EPA 200.8 09/15/2015 21:19 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 21:19 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 21:19 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 21:19 JAHERMA0.2 1
Vanadium (V) Low Level 2.00 ug/L EPA 200.8 09/15/2015 21:19 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 170 mg/L SM2540C 09/10/2015 15:23 CJELLIO251
Total Carbon
TOC 7.3 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.5 5
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 09/10/2015 11:27 GHUTCHI51
Page 15 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029907
Collection Date:09-Sep-15 10:30 AM
Site:MW-05BR
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 09/14/2015 13:37 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 63 mg/L EPA 300.0 09/10/2015 17:32 BGN9034110
Sulfate 0.51 mg/L EPA 300.0 09/10/2015 17:32 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 11:44 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 13:28 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.015 mg/L EPA 200.7 09/11/2015 11:06 FCJORDA0.005 1
Barium (Ba)0.038 mg/L EPA 200.7 09/11/2015 11:06 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 11:06 FCJORDA0.05 1
Iron (Fe)6.92 mg/L EPA 200.7 09/11/2015 11:06 FCJORDA0.01 1
Manganese (Mn)1.84 mg/L EPA 200.7 09/11/2015 11:06 FCJORDA0.005 1
Strontium (Sr)0.215 mg/L EPA 200.7 09/11/2015 11:06 FCJORDA0.005 1
Zinc (Zn)0.005 mg/L EPA 200.7 09/11/2015 11:06 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)85.4 mg/L EPA 200.7 09/15/2015 09:51 FCJORDA0.01 1
Magnesium (Mg)6.77 mg/L EPA 200.7 09/15/2015 09:51 FCJORDA0.005 1
Potassium (K)6.83 mg/L EPA 200.7 09/15/2015 09:51 FCJORDA0.1 1
Sodium (Na)16.5 mg/L EPA 200.7 09/15/2015 09:51 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.039 mg/L EPA 200.7 09/15/2015 09:53 MHH71310.005 1
Barium (Ba)0.034 mg/L EPA 200.7 09/15/2015 09:53 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 09:53 MHH71310.05 1
Iron (Fe)4.11 mg/L EPA 200.7 09/15/2015 09:53 MHH71310.01 1
Manganese (Mn)1.80 mg/L EPA 200.7 09/15/2015 09:53 MHH71310.005 1
Strontium (Sr)0.214 mg/L EPA 200.7 09/15/2015 09:53 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 09:53 MHH71310.005 1
Page 16 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029907
Collection Date:09-Sep-15 10:30 AM
Site:MW-05BR
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 16:03 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 16:03 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 16:03 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 16:03 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 16:03 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 16:03 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 16:03 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 16:03 JAHERMA11
Molybdenum (Mo)1.21 ug/L EPA 200.8 09/15/2015 16:03 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 16:03 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 16:03 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 16:03 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 16:03 JAHERMA0.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 21:26 JAHERMA11
Arsenic (As)1.20 ug/L EPA 200.8 09/15/2015 21:26 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 21:26 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 21:26 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 21:26 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 21:26 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 21:26 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 21:26 JAHERMA11
Molybdenum (Mo)2.48 ug/L EPA 200.8 09/15/2015 21:26 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 21:26 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 21:26 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 21:26 JAHERMA0.2 1
Vanadium (V) Low Level 0.367 ug/L EPA 200.8 09/15/2015 21:26 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 410 mg/L SM2540C 09/10/2015 15:23 CJELLIO251
Total Carbon
TOC 4.3 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 18 mg/L SM2540D 09/10/2015 11:27 GHUTCHI51
Page 17 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029908
Collection Date:09-Sep-15
Site:CW-4
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.126 mg-N/L EPA 353.2 09/14/2015 13:38 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 7.3 mg/L EPA 300.0 09/11/2015 09:20 BGN90340.1 1
Sulfate 23 mg/L EPA 300.0 09/11/2015 09:20 BGN9034110
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 11:46 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/14/2015 13:49 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 09/11/2015 11:10 FCJORDA0.005 1
Barium (Ba)0.027 mg/L EPA 200.7 09/11/2015 11:10 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 11:10 FCJORDA0.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 09/11/2015 11:10 FCJORDA0.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 09/11/2015 11:10 FCJORDA0.005 1
Strontium (Sr)0.138 mg/L EPA 200.7 09/11/2015 11:10 FCJORDA0.005 1
Zinc (Zn)0.008 mg/L EPA 200.7 09/11/2015 11:10 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)11.8 mg/L EPA 200.7 09/15/2015 09:55 FCJORDA0.01 1
Magnesium (Mg)3.38 mg/L EPA 200.7 09/15/2015 09:55 FCJORDA0.005 1
Potassium (K)1.16 mg/L EPA 200.7 09/15/2015 09:55 FCJORDA0.1 1
Sodium (Na)15.7 mg/L EPA 200.7 09/15/2015 09:55 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.048 mg/L EPA 200.7 09/15/2015 09:57 MHH71310.005 1
Barium (Ba)0.026 mg/L EPA 200.7 09/15/2015 09:57 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 09:57 MHH71310.05 1
Iron (Fe)0.030 mg/L EPA 200.7 09/15/2015 09:57 MHH71310.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 09/15/2015 09:57 MHH71310.005 1
Strontium (Sr)0.138 mg/L EPA 200.7 09/15/2015 09:57 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 09:57 MHH71310.005 1
Page 18 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029908
Collection Date:09-Sep-15
Site:CW-4
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 16:09 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 16:09 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 16:09 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 16:09 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 16:09 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 16:09 JAHERMA11
Copper (Cu)5.19 ug/L EPA 200.8 09/15/2015 16:09 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 16:09 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 16:09 JAHERMA11
Nickel (Ni)1.01 ug/L EPA 200.8 09/15/2015 16:09 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 16:09 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 16:09 JAHERMA0.2 1
Vanadium (V) Low Level 0.900 ug/L EPA 200.8 09/15/2015 16:09 JAHERMA0.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 21:32 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 21:32 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 21:32 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 21:32 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 21:32 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 21:32 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 21:32 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 21:32 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 21:32 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 21:32 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 21:32 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 21:32 JAHERMA0.2 1
Vanadium (V) Low Level 1.07 ug/L EPA 200.8 09/15/2015 21:32 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 140 mg/L SM2540C 09/10/2015 15:23 CJELLIO251
Total Carbon
TOC 0.518 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 09/10/2015 11:27 GHUTCHI51
Page 19 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029909
Collection Date:09-Sep-15 5:00 PM
Site:CW-6
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.019 mg-N/L EPA 353.2 09/14/2015 13:39 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 89 mg/L EPA 300.0 09/10/2015 14:45 BGN9034110
Sulfate 40 mg/L EPA 300.0 09/10/2015 14:45 BGN9034110
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 11:49 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 13:30 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.006 mg/L EPA 200.7 09/11/2015 11:14 FCJORDA0.005 1
Barium (Ba)0.046 mg/L EPA 200.7 09/11/2015 11:14 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 11:14 FCJORDA0.05 1
Iron (Fe)1.94 mg/L EPA 200.7 09/11/2015 11:14 FCJORDA0.01 1
Manganese (Mn)1.43 mg/L EPA 200.7 09/11/2015 11:14 FCJORDA0.005 1
Strontium (Sr)0.336 mg/L EPA 200.7 09/11/2015 11:14 FCJORDA0.005 1
Zinc (Zn)0.007 mg/L EPA 200.7 09/11/2015 11:14 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)96.3 mg/L EPA 200.7 09/15/2015 09:59 FCJORDA0.1 10
Magnesium (Mg)19.9 mg/L EPA 200.7 09/15/2015 09:59 FCJORDA0.05 10
Potassium (K)10.4 mg/L EPA 200.7 09/15/2015 09:59 FCJORDA110
Sodium (Na)35.9 mg/L EPA 200.7 09/15/2015 09:59 FCJORDA0.5 10
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.038 mg/L EPA 200.7 09/15/2015 10:01 MHH71310.005 1
Barium (Ba)0.045 mg/L EPA 200.7 09/15/2015 10:01 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 10:01 MHH71310.05 1
Iron (Fe)1.89 mg/L EPA 200.7 09/15/2015 10:01 MHH71310.01 1
Manganese (Mn)1.46 mg/L EPA 200.7 09/15/2015 10:01 MHH71310.005 1
Strontium (Sr)0.328 mg/L EPA 200.7 09/15/2015 10:01 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 10:01 MHH71310.005 1
Page 20 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029909
Collection Date:09-Sep-15 5:00 PM
Site:CW-6
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 16:16 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 16:16 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 16:16 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 16:16 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 16:16 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 16:16 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 16:16 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 16:16 JAHERMA11
Molybdenum (Mo)4.18 ug/L EPA 200.8 09/15/2015 16:16 JAHERMA11
Nickel (Ni)4.11 ug/L EPA 200.8 09/15/2015 16:16 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 16:16 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 16:16 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 16:16 JAHERMA0.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 21:39 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 21:39 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 21:39 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 21:39 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 21:39 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 21:39 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 21:39 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 21:39 JAHERMA11
Molybdenum (Mo)4.25 ug/L EPA 200.8 09/15/2015 21:39 JAHERMA11
Nickel (Ni)4.39 ug/L EPA 200.8 09/15/2015 21:39 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 21:39 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 21:39 JAHERMA0.2 1
Vanadium (V) Low Level 0.341 ug/L EPA 200.8 09/15/2015 21:39 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 530 mg/L SM2540C 09/10/2015 15:23 CJELLIO251
Total Carbon
TOC 1.9 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 09/10/2015 11:27 GHUTCHI51
Page 21 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029910
Collection Date:09-Sep-15 2:15 PM
Site:CW-5
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 09/14/2015 13:40 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 36 mg/L EPA 300.0 09/10/2015 18:10 BGN9034110
Sulfate 6.6 mg/L EPA 300.0 09/10/2015 18:10 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 11:56 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/14/2015 13:56 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 09/11/2015 11:18 FCJORDA0.005 1
Barium (Ba)0.050 mg/L EPA 200.7 09/11/2015 11:18 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 11:18 FCJORDA0.05 1
Iron (Fe)0.454 mg/L EPA 200.7 09/11/2015 11:18 FCJORDA0.01 1
Manganese (Mn)0.770 mg/L EPA 200.7 09/11/2015 11:18 FCJORDA0.005 1
Strontium (Sr)0.152 mg/L EPA 200.7 09/11/2015 11:18 FCJORDA0.005 1
Zinc (Zn)0.011 mg/L EPA 200.7 09/11/2015 11:18 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)51.5 mg/L EPA 200.7 09/15/2015 10:03 FCJORDA0.01 1
Magnesium (Mg)7.42 mg/L EPA 200.7 09/15/2015 10:03 FCJORDA0.005 1
Potassium (K)5.77 mg/L EPA 200.7 09/15/2015 10:03 FCJORDA0.1 1
Sodium (Na)17.3 mg/L EPA 200.7 09/15/2015 10:03 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.056 mg/L EPA 200.7 09/15/2015 10:05 MHH71310.005 1
Barium (Ba)0.054 mg/L EPA 200.7 09/15/2015 10:05 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 10:05 MHH71310.05 1
Iron (Fe)0.780 mg/L EPA 200.7 09/15/2015 10:05 MHH71310.01 1
Manganese (Mn)0.868 mg/L EPA 200.7 09/15/2015 10:05 MHH71310.005 1
Strontium (Sr)0.161 mg/L EPA 200.7 09/15/2015 10:05 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 10:05 MHH71310.005 1
Page 22 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029910
Collection Date:09-Sep-15 2:15 PM
Site:CW-5
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 16:23 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 16:23 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 16:23 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 16:23 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 16:23 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 16:23 JAHERMA11
Copper (Cu)5.73 ug/L EPA 200.8 09/15/2015 16:23 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 16:23 JAHERMA11
Molybdenum (Mo)1.02 ug/L EPA 200.8 09/15/2015 16:23 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 16:23 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 16:23 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 16:23 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 16:23 JAHERMA0.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 21:45 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 21:45 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 21:45 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 21:45 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 21:45 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 21:45 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 21:45 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 21:45 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 21:45 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 21:45 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 21:45 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 21:45 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 21:45 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 280 mg/L SM2540C 09/10/2015 15:23 CJELLIO251
Total Carbon
TOC 0.995 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 09/10/2015 11:27 GHUTCHI51
Page 23 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029911
Collection Date:09-Sep-15 9:25 AM
Site:MW-14BR
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.011 mg-N/L EPA 353.2 09/14/2015 13:49M2 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 11 mg/L EPA 300.0 09/10/2015 15:26 BGN9034110
Sulfate 27 mg/L EPA 300.0 09/10/2015 15:26 BGN9034110
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 12:03 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 13:32 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.007 mg/L EPA 200.7 09/11/2015 11:22 FCJORDA0.005 1
Barium (Ba)0.035 mg/L EPA 200.7 09/11/2015 11:22 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 11:22 FCJORDA0.05 1
Iron (Fe)1.68 mg/L EPA 200.7 09/11/2015 11:22 FCJORDA0.01 1
Manganese (Mn)0.547 mg/L EPA 200.7 09/11/2015 11:22 FCJORDA0.005 1
Strontium (Sr)0.157 mg/L EPA 200.7 09/11/2015 11:22 FCJORDA0.005 1
Zinc (Zn)0.005 mg/L EPA 200.7 09/11/2015 11:22 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)20.2 mg/L EPA 200.7 09/15/2015 10:07 FCJORDA0.01 1
Magnesium (Mg)3.07 mg/L EPA 200.7 09/15/2015 10:07 FCJORDA0.005 1
Potassium (K)6.56 mg/L EPA 200.7 09/15/2015 10:07 FCJORDA0.1 1
Sodium (Na)60.2 mg/L EPA 200.7 09/15/2015 10:07 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.061 mg/L EPA 200.7 09/15/2015 10:09 MHH71310.005 1
Barium (Ba)0.042 mg/L EPA 200.7 09/15/2015 10:09 MHH71310.005 1
Boron (B)0.065 mg/L EPA 200.7 09/15/2015 10:09 MHH71310.05 1
Iron (Fe)2.73 mg/L EPA 200.7 09/15/2015 10:09 MHH71310.01 1
Manganese (Mn)0.648 mg/L EPA 200.7 09/15/2015 10:09 MHH71310.005 1
Strontium (Sr)0.167 mg/L EPA 200.7 09/15/2015 10:09 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/15/2015 10:09 MHH71310.005 1
Page 24 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029911
Collection Date:09-Sep-15 9:25 AM
Site:MW-14BR
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 16:29 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 16:29 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 16:29 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 16:29 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 16:29 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 16:29 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 16:29 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 16:29 JAHERMA11
Molybdenum (Mo)17.0 ug/L EPA 200.8 09/15/2015 16:29 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 16:29 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 16:29 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 16:29 JAHERMA0.2 1
Vanadium (V) Low Level 0.498 ug/L EPA 200.8 09/15/2015 16:29 JAHERMA0.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 21:52 JAHERMA11
Arsenic (As)1.80 ug/L EPA 200.8 09/15/2015 21:52 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 21:52 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 21:52 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 21:52 JAHERMA11
Cobalt (Co)1.09 ug/L EPA 200.8 09/15/2015 21:52 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 21:52 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 21:52 JAHERMA11
Molybdenum (Mo)27.3 ug/L EPA 200.8 09/15/2015 21:52 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 21:52 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 21:52 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 21:52 JAHERMA0.2 1
Vanadium (V) Low Level 0.469 ug/L EPA 200.8 09/15/2015 21:52 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 260 mg/L SM2540C 09/10/2015 15:23 CJELLIO251
Total Carbon
TOC 1.3 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 6.0 mg/L SM2540D 09/10/2015 11:27 GHUTCHI51
Page 25 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029912
Collection Date:09-Sep-15 10:13 AM
Site:MW-4
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.294 mg-N/L EPA 353.2 09/14/2015 13:52 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 7.0 mg/L EPA 300.0 09/10/2015 18:46 BGN90340.1 1
Sulfate 37 mg/L EPA 300.0 09/10/2015 18:46 BGN9034110
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 12:05 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 13:35 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 09/11/2015 11:26 FCJORDA0.005 1
Barium (Ba)0.011 mg/L EPA 200.7 09/11/2015 11:26 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 11:26 FCJORDA0.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 09/11/2015 11:26 FCJORDA0.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 09/11/2015 11:26 FCJORDA0.005 1
Strontium (Sr)0.108 mg/L EPA 200.7 09/11/2015 11:26 FCJORDA0.005 1
Zinc (Zn)0.020 mg/L EPA 200.7 09/11/2015 11:26 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)27.6 mg/L EPA 200.7 09/15/2015 10:11 FCJORDA0.01 1
Magnesium (Mg)8.55 mg/L EPA 200.7 09/15/2015 10:11 FCJORDA0.005 1
Potassium (K)6.48 mg/L EPA 200.7 09/15/2015 10:11 FCJORDA0.1 1
Sodium (Na)17.3 mg/L EPA 200.7 09/15/2015 10:11 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.019 mg/L EPA 200.7 09/15/2015 10:13 MHH71310.005 1
Barium (Ba)0.011 mg/L EPA 200.7 09/15/2015 10:13 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/15/2015 10:13 MHH71310.05 1
Iron (Fe)0.019 mg/L EPA 200.7 09/15/2015 10:13 MHH71310.01 1
Manganese (Mn)0.007 mg/L EPA 200.7 09/15/2015 10:13 MHH71310.005 1
Strontium (Sr)0.102 mg/L EPA 200.7 09/15/2015 10:13 MHH71310.005 1
Zinc (Zn)0.013 mg/L EPA 200.7 09/15/2015 10:13 MHH71310.005 1
Page 26 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029912
Collection Date:09-Sep-15 10:13 AM
Site:MW-4
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 16:36 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 16:36 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 16:36 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 16:36 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 16:36 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 16:36 JAHERMA11
Copper (Cu)7.03 ug/L EPA 200.8 09/15/2015 16:36 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 16:36 JAHERMA11
Molybdenum (Mo)2.46 ug/L EPA 200.8 09/15/2015 16:36 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 16:36 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 16:36 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 16:36 JAHERMA0.2 1
Vanadium (V) Low Level 0.882 ug/L EPA 200.8 09/15/2015 16:36 JAHERMA0.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 21:58 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 21:58 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 21:58 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 21:58 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 21:58 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 21:58 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 21:58 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 21:58 JAHERMA11
Molybdenum (Mo)2.67 ug/L EPA 200.8 09/15/2015 21:58 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 21:58 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 21:58 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 21:58 JAHERMA0.2 1
Vanadium (V) Low Level 0.997 ug/L EPA 200.8 09/15/2015 21:58 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 210 mg/L SM2540C 09/10/2015 15:23 CJELLIO251
Total Carbon
TOC 0.748 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 09/10/2015 11:27 GHUTCHI51
Page 27 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029913
Collection Date:09-Sep-15 2:37 PM
Site:ABMW-04
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.076 mg-N/L EPA 353.2 09/14/2015 13:53 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 11 mg/L EPA 300.0 09/10/2015 20:20 BGN9034110
Sulfate 37 mg/L EPA 300.0 09/10/2015 20:20 BGN9034110
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 12:08 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 13:37 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 14:17 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.022 mg/L EPA 200.7 09/11/2015 11:37 FCJORDA0.005 1
Barium (Ba)0.425 mg/L EPA 200.7 09/11/2015 11:37 FCJORDA0.005 1
Boron (B)5.11 mg/L EPA 200.7 09/11/2015 11:37 FCJORDA0.05 1
Iron (Fe)1.48 mg/L EPA 200.7 09/11/2015 11:37 FCJORDA0.01 1
Manganese (Mn)0.804 mg/L EPA 200.7 09/11/2015 11:37 FCJORDA0.005 1
Strontium (Sr)2.32 mg/L EPA 200.7 09/11/2015 11:37 FCJORDA0.005 1
Zinc (Zn)0.005 mg/L EPA 200.7 09/11/2015 11:37 FCJORDA0.005 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)0.023 mg/L EPA 200.7 09/11/2015 13:30 FCJORDA0.005 1
Barium (Ba)0.422 mg/L EPA 200.7 09/11/2015 13:30 FCJORDA0.005 1
Boron (B)5.24 mg/L EPA 200.7 09/11/2015 13:30 FCJORDA0.05 1
Iron (Fe)0.666 mg/L EPA 200.7 09/11/2015 13:30 FCJORDA0.01 1
Manganese (Mn)0.725 mg/L EPA 200.7 09/11/2015 13:30 FCJORDA0.005 1
Strontium (Sr)2.37 mg/L EPA 200.7 09/11/2015 13:30 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/11/2015 13:30 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)120 mg/L EPA 200.7 09/15/2015 10:22 FCJORDA0.1 10
Magnesium (Mg)33.2 mg/L EPA 200.7 09/15/2015 10:22 FCJORDA0.05 10
Potassium (K)23.7 mg/L EPA 200.7 09/15/2015 10:22 FCJORDA110
Sodium (Na)11.9 mg/L EPA 200.7 09/15/2015 10:22 FCJORDA0.5 10
Page 28 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029913
Collection Date:09-Sep-15 2:37 PM
Site:ABMW-04
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.135 mg/L EPA 200.7 09/17/2015 09:57 FCJORDA0.005 1
Barium (Ba)0.441 mg/L EPA 200.7 09/17/2015 09:57 FCJORDA0.005 1
Boron (B)5.12 mg/L EPA 200.7 09/17/2015 09:57 FCJORDA0.05 1
Iron (Fe)1.73 mg/L EPA 200.7 09/17/2015 09:57 FCJORDA0.01 1
Manganese (Mn)0.797 mg/L EPA 200.7 09/17/2015 09:57 FCJORDA0.005 1
Strontium (Sr)2.38 mg/L EPA 200.7 09/17/2015 09:57 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/17/2015 09:57 FCJORDA0.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 17:22 JAHERMA11
Arsenic (As)728 ug/L EPA 200.8 09/15/2015 17:22 JAHERMA1010
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 17:22 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 17:22 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 17:22 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 17:22 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 17:22 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 17:22 JAHERMA11
Molybdenum (Mo)408 ug/L EPA 200.8 09/15/2015 17:22 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 17:22 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 17:22 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 17:22 JAHERMA0.2 1
Vanadium (V) Low Level 1.54 ug/L EPA 200.8 09/15/2015 17:22 JAHERMA0.3 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 13:02 MHALL311
Arsenic (As)695 ug/L EPA 200.8 09/15/2015 13:02 MHALL31010
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 13:02 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 13:02 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 13:02 MHALL311
Cobalt (Co)1.02 ug/L EPA 200.8 09/15/2015 13:02 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 13:02 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 13:02 MHALL311
Molybdenum (Mo)402 ug/L EPA 200.8 09/15/2015 13:02 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 13:02 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 13:02 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 13:02 MHALL30.2 1
Vanadium (V) Low Level 1.38 ug/L EPA 200.8 09/15/2015 13:02 MHALL30.3 1
Page 29 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029913
Collection Date:09-Sep-15 2:37 PM
Site:ABMW-04
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 17:32 MHALL311
Arsenic (As)751 ug/L EPA 200.8 09/15/2015 17:32 MHALL31010
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 17:32 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 17:32 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 17:32 MHALL311
Cobalt (Co)1.07 ug/L EPA 200.8 09/15/2015 17:32 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 17:32 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 17:32 MHALL311
Molybdenum (Mo)397 ug/L EPA 200.8 09/15/2015 17:32 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 17:32 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 17:32 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 17:32 MHALL30.2 1
Vanadium (V) Low Level 1.92 ug/L EPA 200.8 09/15/2015 17:32 MHALL30.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 500 mg/L SM2540C 09/10/2015 15:23 CJELLIO251
Total Carbon
TOC 3.1 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 09/10/2015 11:27 GHUTCHI51
Page 30 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029914
Collection Date:09-Sep-15 1:07 PM
Site:ABMW-04D
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.016 mg-N/L EPA 353.2 09/14/2015 13:55 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 12 mg/L EPA 300.0 09/11/2015 09:38 BGN9034110
Sulfate 7.2 mg/L EPA 300.0 09/11/2015 09:38 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 12:10 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/14/2015 13:58 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 14:19 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.076 mg/L EPA 200.7 09/11/2015 11:48 FCJORDA0.005 1
Barium (Ba)0.917 mg/L EPA 200.7 09/11/2015 11:48 FCJORDA0.005 1
Boron (B)4.06 mg/L EPA 200.7 09/11/2015 11:48 FCJORDA0.05 1
Iron (Fe)38.8 mg/L EPA 200.7 09/11/2015 11:48 FCJORDA0.01 1
Manganese (Mn)5.63 mg/L EPA 200.7 09/11/2015 11:48 FCJORDA0.005 1
Strontium (Sr)2.25 mg/L EPA 200.7 09/11/2015 11:48 FCJORDA0.005 1
Zinc (Zn)0.008 mg/L EPA 200.7 09/11/2015 11:48 FCJORDA0.005 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)0.071 mg/L EPA 200.7 09/11/2015 13:33 FCJORDA0.005 1
Barium (Ba)0.902 mg/L EPA 200.7 09/11/2015 13:33 FCJORDA0.005 1
Boron (B)3.97 mg/L EPA 200.7 09/11/2015 13:33 FCJORDA0.05 1
Iron (Fe)38.3 mg/L EPA 200.7 09/11/2015 13:33 FCJORDA0.01 1
Manganese (Mn)5.54 mg/L EPA 200.7 09/11/2015 13:33 FCJORDA0.005 1
Strontium (Sr)2.23 mg/L EPA 200.7 09/11/2015 13:33 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/11/2015 13:33 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)159 mg/L EPA 200.7 09/15/2015 10:26M4 FCJORDA0.1 10
Magnesium (Mg)43.5 mg/L EPA 200.7 09/15/2015 10:26M4 FCJORDA0.05 10
Potassium (K)28.6 mg/L EPA 200.7 09/15/2015 10:26 FCJORDA110
Sodium (Na)20.5 mg/L EPA 200.7 09/15/2015 10:26 FCJORDA0.5 10
Page 31 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029914
Collection Date:09-Sep-15 1:07 PM
Site:ABMW-04D
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.216 mg/L EPA 200.7 09/17/2015 10:01 FCJORDA0.005 1
Barium (Ba)0.953 mg/L EPA 200.7 09/17/2015 10:01 FCJORDA0.005 1
Boron (B)4.61 mg/L EPA 200.7 09/17/2015 10:01 FCJORDA0.05 1
Iron (Fe)44.4 mg/L EPA 200.7 09/17/2015 10:01 FCJORDA0.01 1
Manganese (Mn)4.55 mg/L EPA 200.7 09/17/2015 10:01 FCJORDA0.005 1
Strontium (Sr)2.66 mg/L EPA 200.7 09/17/2015 10:01 FCJORDA0.005 1
Zinc (Zn)0.094 mg/L EPA 200.7 09/17/2015 10:01 FCJORDA0.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 17:42 JAHERMA11
Arsenic (As)138 ug/L EPA 200.8 09/15/2015 17:42 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 17:42 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 17:42 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 17:42 JAHERMA11
Cobalt (Co)3.32 ug/L EPA 200.8 09/15/2015 17:42 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 17:42 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 17:42 JAHERMA11
Molybdenum (Mo)40.7 ug/L EPA 200.8 09/15/2015 17:42 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 17:42 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 17:42 JAHERMA11
Thallium (Tl) Low Level 0.585 ug/L EPA 200.8 09/15/2015 17:42 JAHERMA0.2 1
Vanadium (V) Low Level 9.33 ug/L EPA 200.8 09/15/2015 17:42 JAHERMA0.3 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 13:07 MHALL311
Arsenic (As)94.1 ug/L EPA 200.8 09/15/2015 13:07 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 13:07 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 13:07 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 13:07 MHALL311
Cobalt (Co)3.09 ug/L EPA 200.8 09/15/2015 13:07 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 13:07 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 13:07 MHALL311
Molybdenum (Mo)38.0 ug/L EPA 200.8 09/15/2015 13:07 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 13:07 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 13:07 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 13:07 MHALL30.2 1
Vanadium (V) Low Level 0.585 ug/L EPA 200.8 09/15/2015 13:07 MHALL30.3 1
Page 32 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029914
Collection Date:09-Sep-15 1:07 PM
Site:ABMW-04D
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 16:51 MHALL311
Arsenic (As)143 ug/L EPA 200.8 09/15/2015 16:51 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 16:51 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 16:51 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 16:51 MHALL311
Cobalt (Co)3.38 ug/L EPA 200.8 09/15/2015 16:51 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 16:51 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 16:51 MHALL311
Molybdenum (Mo)92.1 ug/L EPA 200.8 09/15/2015 16:51 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 16:51 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 16:51 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 16:51 MHALL30.2 1
Vanadium (V) Low Level 11.7 ug/L EPA 200.8 09/15/2015 16:51 MHALL30.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 700 mg/L SM2540C 09/10/2015 15:23 CJELLIO251
Total Carbon
TOC 8.0 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.5 5
TOTAL SUSPENDED SOLIDS
TSS 81 mg/L SM2540D 09/10/2015 11:27 GHUTCHI51
Page 33 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029915
Collection Date:09-Sep-15 11:16 AM
Site:ABMW-04BR
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 09/14/2015 13:56 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 4.8 mg/L EPA 300.0 09/10/2015 21:50 BGN90340.1 1
Sulfate 42 mg/L EPA 300.0 09/10/2015 21:50 BGN9034110
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 12:12 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/14/2015 14:00 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/14/2015 14:39 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.017 mg/L EPA 200.7 09/11/2015 11:52 FCJORDA0.005 1
Barium (Ba)0.103 mg/L EPA 200.7 09/11/2015 11:52 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 11:52 FCJORDA0.05 1
Iron (Fe)0.123 mg/L EPA 200.7 09/11/2015 11:52 FCJORDA0.01 1
Manganese (Mn)0.335 mg/L EPA 200.7 09/11/2015 11:52 FCJORDA0.005 1
Strontium (Sr)1.78 mg/L EPA 200.7 09/11/2015 11:52 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/11/2015 11:52 FCJORDA0.005 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)0.017 mg/L EPA 200.7 09/11/2015 13:37 FCJORDA0.005 1
Barium (Ba)0.104 mg/L EPA 200.7 09/11/2015 13:37 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 13:37 FCJORDA0.05 1
Iron (Fe)0.055 mg/L EPA 200.7 09/11/2015 13:37 FCJORDA0.01 1
Manganese (Mn)0.343 mg/L EPA 200.7 09/11/2015 13:37 FCJORDA0.005 1
Strontium (Sr)1.79 mg/L EPA 200.7 09/11/2015 13:37 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/11/2015 13:37 FCJORDA0.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)72.9 mg/L EPA 200.7 09/15/2015 10:37 FCJORDA0.01 1
Magnesium (Mg)5.39 mg/L EPA 200.7 09/15/2015 10:37 FCJORDA0.005 1
Potassium (K)8.97 mg/L EPA 200.7 09/15/2015 10:37 FCJORDA0.1 1
Sodium (Na)20.9 mg/L EPA 200.7 09/15/2015 10:37 FCJORDA0.05 1
Page 34 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029915
Collection Date:09-Sep-15 11:16 AM
Site:ABMW-04BR
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.063 mg/L EPA 200.7 09/17/2015 10:12 FCJORDA0.005 1
Barium (Ba)0.106 mg/L EPA 200.7 09/17/2015 10:12 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/17/2015 10:12 FCJORDA0.05 1
Iron (Fe)0.360 mg/L EPA 200.7 09/17/2015 10:12 FCJORDA0.01 1
Manganese (Mn)0.350 mg/L EPA 200.7 09/17/2015 10:12 FCJORDA0.005 1
Strontium (Sr)1.82 mg/L EPA 200.7 09/17/2015 10:12 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/17/2015 10:12 FCJORDA0.005 1
TOTAL RECOVERABLE METALS BY ICP-MS (DISSOLVED)
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 17:48 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 17:48 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 17:48 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 17:48 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 17:48 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 17:48 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 17:48 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 17:48 JAHERMA11
Molybdenum (Mo)2.78 ug/L EPA 200.8 09/15/2015 17:48 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 17:48 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 17:48 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 17:48 JAHERMA0.2 1
Vanadium (V) Low Level 0.476 ug/L EPA 200.8 09/15/2015 17:48 JAHERMA0.3 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 13:12 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 13:12 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 13:12 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 13:12 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 13:12 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 13:12 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 13:12 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 13:12 MHALL311
Molybdenum (Mo)2.10 ug/L EPA 200.8 09/15/2015 13:12 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 13:12 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 13:12 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 13:12 MHALL30.2 1
Vanadium (V) Low Level 0.469 ug/L EPA 200.8 09/15/2015 13:12 MHALL30.3 1
Page 35 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029915
Collection Date:09-Sep-15 11:16 AM
Site:ABMW-04BR
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 17:37 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 17:37 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 17:37 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 17:37 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 17:37 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 17:37 MHALL311
Copper (Cu)2.16 ug/L EPA 200.8 09/15/2015 17:37 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 17:37 MHALL311
Molybdenum (Mo)4.01 ug/L EPA 200.8 09/15/2015 17:37 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 17:37 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 17:37 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 17:37 MHALL30.2 1
Vanadium (V) Low Level 0.458 ug/L EPA 200.8 09/15/2015 17:37 MHALL30.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 320 mg/L SM2540C 09/10/2015 15:23 CJELLIO251
Total Carbon
TOC 4.6 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 09/10/2015 11:27 GHUTCHI51
Page 36 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029916
Collection Date:09-Sep-15 11:45 AM
Site:Filter Blank
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
Mercury Dissolved (cold vapor) in Water (0.1mm FILTER)
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/14/2015 14:46 ACPAYNE0.05 1
DISSOLVED METALS BY ICP (0.1mm FILTER)
Aluminum (Al)< 0.005 mg/L EPA 200.7 09/11/2015 13:41 FCJORDA0.005 1
Barium (Ba)< 0.005 mg/L EPA 200.7 09/11/2015 13:41 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/11/2015 13:41 FCJORDA0.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 09/11/2015 13:41 FCJORDA0.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 09/11/2015 13:41 FCJORDA0.005 1
Strontium (Sr)< 0.005 mg/L EPA 200.7 09/11/2015 13:41 FCJORDA0.005 1
Zinc (Zn)0.013 mg/L EPA 200.7 09/11/2015 13:41 FCJORDA0.005 1
Total Recoverable Metals Dissolved 0.1mm Filter
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 13:17 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 13:17 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 13:17 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 13:17 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 13:17 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 13:17 MHALL311
Copper (Cu)2.82 ug/L EPA 200.8 09/15/2015 13:17 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 13:17 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 13:17 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 13:17 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 13:17 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 13:17 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 13:17 MHALL30.3 1
Page 37 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029917
Collection Date:09-Sep-15 11:45 AM
Site:Equipment Blank
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 09/14/2015 13:57 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride < 0.1 mg/L EPA 300.0 09/10/2015 19:59 BGN90340.1 1
Sulfate < 0.1 mg/L EPA 300.0 09/10/2015 19:59 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 09/11/2015 12:15 ACPAYNE0.05 1
UNDIGESTED METALS BY ICP
Calcium (Ca)0.013 mg/L EPA 200.7 09/15/2015 10:41 FCJORDA0.01 1
Magnesium (Mg)< 0.005 mg/L EPA 200.7 09/15/2015 10:41 FCJORDA0.005 1
Potassium (K)< 0.1 mg/L EPA 200.7 09/15/2015 10:41 FCJORDA0.1 1
Sodium (Na)< 0.05 mg/L EPA 200.7 09/15/2015 10:41 FCJORDA0.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 09/17/2015 10:16 FCJORDA0.005 1
Barium (Ba)< 0.005 mg/L EPA 200.7 09/17/2015 10:16 FCJORDA0.005 1
Boron (B)< 0.05 mg/L EPA 200.7 09/17/2015 10:16 FCJORDA0.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 09/17/2015 10:16 FCJORDA0.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 09/17/2015 10:16 FCJORDA0.005 1
Strontium (Sr)< 0.005 mg/L EPA 200.7 09/17/2015 10:16 FCJORDA0.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 09/17/2015 10:16 FCJORDA0.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 09/15/2015 17:42 MHALL311
Arsenic (As)< 1 ug/L EPA 200.8 09/15/2015 17:42 MHALL311
Beryllium (Be)< 1 ug/L EPA 200.8 09/15/2015 17:42 MHALL311
Cadmium (Cd)< 1 ug/L EPA 200.8 09/15/2015 17:42 MHALL311
Chromium (Cr)< 1 ug/L EPA 200.8 09/15/2015 17:42 MHALL311
Cobalt (Co)< 1 ug/L EPA 200.8 09/15/2015 17:42 MHALL311
Copper (Cu)< 1 ug/L EPA 200.8 09/15/2015 17:42 MHALL311
Lead (Pb)< 1 ug/L EPA 200.8 09/15/2015 17:42 MHALL311
Molybdenum (Mo)< 1 ug/L EPA 200.8 09/15/2015 17:42 MHALL311
Nickel (Ni)< 1 ug/L EPA 200.8 09/15/2015 17:42 MHALL311
Selenium (Se)< 1 ug/L EPA 200.8 09/15/2015 17:42 MHALL311
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 09/15/2015 17:42 MHALL30.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 09/15/2015 17:42 MHALL30.3 1
Page 38 of 103
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15090208
2015029917
Collection Date:09-Sep-15 11:45 AM
Site:Equipment Blank
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L SM2540C 09/10/2015 15:23 CJELLIO251
Total Carbon
TOC 0.181 mg/L SM5310C/EPA9060A 09/14/2015 12:44 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 09/10/2015 11:27 GHUTCHI51
Qualifiers:
M2 Matrix spike recovery was Low: the associated Laboratory Control Spike (LCS) was acceptable.
M4 The spike recovery value was unusable since the analyte concentration in the sample was disproportionate
to the spike level. The associated Laboratory Control Spike recovery was acceptable.
Page 39 of 103
Page 40 of 103
Page 41 of 103
Page 42 of 103
Page 43 of 103
Page 44 of 103
Page 45 of 103
Page 46 of 103
Page 47 of 103
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
QI10090Lot Number:
J15090208Project Number:
AB GW Assessment Water - MayoProject Name:
09/15/2015Date Completed:
Grant Wilton
Project Manager

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Duke Energy
Lot Number: QI10090
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
Project Name: AB GW Assessment Water - Mayo
Project Number: J15090208
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Page: 2 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QI10090

Project Name: AB GW Assessment Water - Mayo
Project Number: J15090208
Sample Number Sample ID Matrix Date Sampled Date Received
001 09/09/2015 11152015029903Aqueous 09/10/2015
002 09/09/2015 10042015029904Aqueous 09/10/2015
003 09/09/2015 10042015029905Aqueous 09/10/2015
004 09/09/2015 11552015029906Aqueous 09/10/2015
005 09/09/2015 10302015029907Aqueous 09/10/2015
006 09/09/20152015029908Aqueous 09/10/2015
007 09/09/2015 17002015029909Aqueous 09/10/2015
008 09/09/2015 14152015029910Aqueous 09/10/2015
009 09/09/2015 09252015029911Aqueous 09/10/2015
010 09/09/2015 16132015029912Aqueous 09/10/2015
011 09/09/2015 14372015029913Aqueous 09/10/2015
012 09/09/2015 13072015029914Aqueous 09/10/2015
013 09/09/2015 11162015029915Aqueous 09/10/2015
014 09/09/2015 11452015029917Aqueous 09/10/2015
(14 samples)
Page: 3 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QI10090

Project Name: AB GW Assessment Water - Mayo
Project Number: J15090208
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 2015029903 Aqueous Alkalinity SM 2320B-55 mg/L 5
001 2015029903 Aqueous Bicarbonate Alkalinity SM 2320B-55 mg/L 5
001 2015029903 Aqueous Methane RSK - 175 33 ug/L 6
002 2015029904 Aqueous Alkalinity SM 2320B-81 mg/L 7
002 2015029904 Aqueous Bicarbonate Alkalinity SM 2320B-81 mg/L 7
003 2015029905 Aqueous Alkalinity SM 2320B-80 mg/L 9
003 2015029905 Aqueous Bicarbonate Alkalinity SM 2320B-80 mg/L 9
004 2015029906 Aqueous Alkalinity SM 2320B-99 mg/L 11
004 2015029906 Aqueous Bicarbonate Alkalinity SM 2320B-95 mg/L 11
005 2015029907 Aqueous Alkalinity SM 2320B-200 mg/L 13
005 2015029907 Aqueous Bicarbonate Alkalinity SM 2320B-200 mg/L 13
005 2015029907 Aqueous Methane RSK - 175 670 ug/L 14
006 2015029908 Aqueous Alkalinity SM 2320B-48 mg/L 15
006 2015029908 Aqueous Bicarbonate Alkalinity SM 2320B-48 mg/L 15
007 2015029909 Aqueous Alkalinity SM 2320B-270 mg/L 17
007 2015029909 Aqueous Bicarbonate Alkalinity SM 2320B-270 mg/L 17
007 2015029909 Aqueous Methane RSK - 175 120 ug/L 18
008 2015029910 Aqueous Alkalinity SM 2320B-160 mg/L 19
008 2015029910 Aqueous Bicarbonate Alkalinity SM 2320B-160 mg/L 19
009 2015029911 Aqueous Alkalinity SM 2320B-160 mg/L 21
009 2015029911 Aqueous Bicarbonate Alkalinity SM 2320B-160 mg/L 21
009 2015029911 Aqueous Methane RSK - 175 13 ug/L 22
010 2015029912 Aqueous Alkalinity SM 2320B-110 mg/L 23
010 2015029912 Aqueous Bicarbonate Alkalinity SM 2320B-110 mg/L 23
011 2015029913 Aqueous Alkalinity SM 2320B-410 mg/L 25
011 2015029913 Aqueous Bicarbonate Alkalinity SM 2320B-400 mg/L 25
011 2015029913 Aqueous Methane RSK - 175 5800 ug/L 26
012 2015029914 Aqueous Alkalinity SM 2320B-650 mg/L 27
012 2015029914 Aqueous Bicarbonate Alkalinity SM 2320B-650 mg/L 27
012 2015029914 Aqueous Methane RSK - 175 16000 ug/L 28
013 2015029915 Aqueous Alkalinity SM 2320B-210 mg/L 29
013 2015029915 Aqueous Bicarbonate Alkalinity SM 2320B-210 mg/L 29
013 2015029915 Aqueous Methane RSK - 175 62 ug/L 30
(33 detections)
Page: 4 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029903
QI10090-001
09/09/2015 1115
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/12/2015 2005 HMA 84760
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 2005 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 2005 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 55 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 55 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 5 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029903
QI10090-001
09/09/2015 1115
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/11/2015 1931 DCS 84693
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 33 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029904
QI10090-002
09/09/2015 1004
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/12/2015 2024 HMA 84760
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 2024 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 2024 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 81 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 81 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029904
QI10090-002
09/09/2015 1004
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/11/2015 1944 DCS 84693
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029905
QI10090-003
09/09/2015 1004
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/12/2015 2030 HMA 84760
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 2030 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 2030 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 80 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 80 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029905
QI10090-003
09/09/2015 1004
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/11/2015 1959 DCS 84693
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029906
QI10090-004
09/09/2015 1155
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/12/2015 2037 HMA 84760
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 2037 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 2037 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 99 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 95 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029906
QI10090-004
09/09/2015 1155
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/11/2015 2016 DCS 84693
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029907
QI10090-005
09/09/2015 1030
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/12/2015 2043 HMA 84760
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 2043 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 2043 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 200 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 200 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029907
QI10090-005
09/09/2015 1030
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/11/2015 2106 DCS 84693
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 670 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 14 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029908
QI10090-006
09/09/2015
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/12/2015 2048 HMA 84760
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 2048 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 2048 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 48 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 48 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 15 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029908
QI10090-006
09/09/2015
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/11/2015 2142 DCS 84693
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 16 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029909
QI10090-007
09/09/2015 1700
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/12/2015 2055 HMA 84760
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 2055 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 2055 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 270 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 270 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 17 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029909
QI10090-007
09/09/2015 1700
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/13/2015 1521 JJG 84775
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 120 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 18 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029910
QI10090-008
09/09/2015 1415
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/12/2015 2103 HMA 84760
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 2103 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 2103 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 160 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 160 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 19 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029910
QI10090-008
09/09/2015 1415
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/13/2015 1601 JJG 84775
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 20 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029911
QI10090-009
09/09/2015 0925
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/12/2015 2122 HMA 84760
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 2122 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 2122 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 160 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 160 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 21 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029911
QI10090-009
09/09/2015 0925
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/13/2015 1621 JJG 84775
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 13 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 22 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029912
QI10090-010
09/09/2015 1613
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/12/2015 2128 HMA 84760
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 2128 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 2128 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 110 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 110 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 23 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029912
QI10090-010
09/09/2015 1613
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/13/2015 1632 JJG 84775
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 24 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029913
QI10090-011
09/09/2015 1437
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/12/2015 2137 HMA 84760
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 2137 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 2137 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 410 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 400 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 25 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029913
QI10090-011
09/09/2015 1437
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 RSK - 175 20 09/14/2015 2047 JJG 84867
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 5800 2ug/L200
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 26 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029914
QI10090-012
09/09/2015 1307
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/12/2015 2225 HMA 84762
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 2225 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 2225 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 650 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 650 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 27 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029914
QI10090-012
09/09/2015 1307
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 RSK - 175 100 09/14/2015 2105 JJG 84867
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 16000 2ug/L1000
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 28 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029915
QI10090-013
09/09/2015 1116
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/12/2015 2255 HMA 84762
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 2255 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 2255 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 210 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 210 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 29 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029915
QI10090-013
09/09/2015 1116
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/13/2015 1722 JJG 84775
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 62 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 30 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029917
QI10090-014
09/09/2015 1145
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 09/12/2015 2300 HMA 84762
1 (Bicarbonate ) SM 2320B-2011 1 09/12/2015 2300 HMA
1 (Carbonate Al) SM 2320B-2011 1 09/12/2015 2300 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 ND 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 ND 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 31 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015029917
QI10090-014
09/09/2015 1145
09/10/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15090208
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 09/13/2015 1733 JJG 84775
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 32 of 32
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

QC Summary
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - MB
Batch:
Sample ID:QQ84760-001
84760
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Alkalinity ND 09/12/2015 182510mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - LCS
Batch:
Sample ID:QQ84760-002
84760
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Alkalinity 110 09/12/2015 183110610090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - MS
Batch:
Sample ID:QI10090-001MS
84760
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Alkalinity 150 09/12/2015 20129110070-130551
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - MSD
Batch:
Sample ID:QI10090-001MD
84760
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Alkalinity 150 09/12/2015 20189110070-1300.19 20551
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - MS
Batch:
Sample ID:QI10090-011MS
84760
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Alkalinity 470 09/12/2015 2145N6810070-1304101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - MSD
Batch:
Sample ID:QI10090-011MD
84760
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Alkalinity 470 09/12/2015 2155N6610070-1300.46 204101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - MB
Batch:
Sample ID:QQ84762-001
84762
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Alkalinity ND 09/12/2015 220810mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - LCS
Batch:
Sample ID:QQ84762-002
84762
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Alkalinity 110 09/12/2015 221410610090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - MS
Batch:
Sample ID:QI10090-012MS
84762
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Alkalinity 720 09/12/2015 2237N6710070-1306501
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Inorganic non-metals - MSD
Batch:
Sample ID:QI10090-012MD
84762
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(mg/L)(mg/L)(mg/L)
Alkalinity 720 09/12/2015 2249N6810070-1300.25 206501
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - MB
Batch:
Sample ID:QQ84693-001
84693
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Methane ND 09/11/2015 133510ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - LCS
Batch:
Sample ID:QQ84693-002
84693
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Methane 140 09/11/2015 13109415070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - LCSD
Batch:
Sample ID:QQ84693-003
84693
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Methane 140 09/11/2015 13229415070-1300.078 301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - MB
Batch:
Sample ID:QQ84775-001
84775
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Methane ND 09/13/2015 132610ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - LCS
Batch:
Sample ID:QQ84775-002
84775
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Methane 150 09/13/2015 12369815070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - LCSD
Batch:
Sample ID:QQ84775-003
84775
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Methane 150 09/13/2015 12509615070-1301.8 301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - MB
Batch:
Sample ID:QQ84867-001
84867
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Methane ND 09/14/2015 195110ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - LCS
Batch:
Sample ID:QQ84867-002
84867
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Methane 140 09/14/2015 17209215070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Methane - LCSD
Batch:
Sample ID:QQ84867-003
84867
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Methane 140 09/14/2015 17349515070-1303.4 301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QI10090
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Chain of Custody
and
Miscellaneous Documents
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.

Page 103 of 103