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Home My WebLink AboutNC0038377_J15050018 Report_2017110113339 Hagers Ferry Road Huntersville, NC 28078-7929 McGuire Nuclear Complex - MG03A2 Phone: 980-875-5245 Fax: 980-875-4349 Order Summary Report Analytical Laboratory Order Number: J15050018 Project Name:MAYO STEAM - AB GW ASSESSMENT SOIL Lab Contact:Margaret Galvin-Karr Date:5/28/2015 Customer Address: Customer Name(s):Tim Hunsucker, Jerry Wylie, Kathy Webb, John Toepfer Phone: 980-875-5219 Report Authorized By: (Signature) Program Comments: Please contact the Program Manager (Margaret Galvin-Karr) with any questions regarding this report. Data Flags & Calculations: Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results) under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have been qualified by Duke Energy to perform these analyses except where noted. Data Package: This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The order of individual sections within this report is as follows: Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis, Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports & Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC) Certification: The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina (DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of specific methods. Margaret Galvin-Karr 1 of 36 Sample ID's & Descriptions: Sample ID Plant/Station Collection Date and Time Collected By Sample Description 2015012958 MAYO STEAM 28-Apr-15 1:00 PM illegible MW-12D(88.5-90.0) 1 Total Samples 2 of 36 COC and .pdf report are in agreement with sample totals and analyses (compliance programs and procedures). All Results are less than the laboratory reporting limits. All laboratory QA/QC requirements are acceptable. Yes No Technical Validation Review Checklist: Yes No Yes No Report Sections Included: Job Summary Report Sub-contracted Laboratory Results Sample Identification Customer Specific Data Sheets, Reports, & Documentation Technical Validation of Data Package Customer Database Entries Analytical Laboratory Certificate of Analysis Analytical Laboratory QC Report Chain of Custody Reviewed By: Date: Electronic Data Deliverable (EDD) Sent Separately 3 of 36 Certificate of Laboratory Analysis This report shall not be reproduced, except in full. Order # J15050018 2015012958 Collection Date: 28-Apr-15 1:00 PM Site:MW-12D(88.5-90.0) Matrix: SOIL Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult Sample #: AnalystDF PERCENT SOLIDS - (Analysis Performed by Pace Laboratories) Vendor Parameter Complete Vendor Method V_PACE DIONEX ANIONS BY VENDOR - (Analysis Performed by Pace Laboratories) Vendor Parameter Complete Vendor Method V_PACE METALS ANALYSIS BY VENDOR LAB - (Analysis Performed by Pace Laboratories) Vendor Parameter Complete Vendor Method V_PACE PH IN SOIL - (Analysis Performed by Pace Laboratories) Vendor Parameter Complete Vendor Method V_PACE TOTAL ORGANIC CARBON IN SOILS - (Analysis Performed by Pace Laboratories) Vendor Parameter Complete Vendor Method V_PACE 4 of 36 #=CL# May 27, 2015 LIMS USE: FR - PROGRAM MANAGER LIMS OBJECT ID: 92247909 92247909 Project: Pace Project No.: RE: Program Manager Duke Energy 13339 Hagers Ferry Road Bldg. 7405 MG30A2 Huntersville, NC 28078 J15050018 Dear Program Manager: Enclosed are the analytical results for sample(s) received by the laboratory on May 01, 2015. The results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. If you have any questions concerning this report, please feel free to contact me. Sincerely, Kevin Herring kevin.herring@pacelabs.com HORIZON Database Administrator Enclosures cc:Marge Galvin-Karr, Duke Energy Program Manager, Duke Energy Rodney Wike, Duke Energy REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 1 of 30 5 of 36 #=CP# CERTIFICATIONS Pace Project No.: Project: 92247909 J15050018 Ormond Beach Certification IDs 8 East Tower Circle, Ormond Beach, FL 32174 Alabama Certification #: 41320 Connecticut Certification #: PH-0216 Delaware Certification: FL NELAC Reciprocity Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Illinois Certification #: 200068 Indiana Certification: FL NELAC Reciprocity Kansas Certification #: E-10383 Kentucky Certification #: 90050 Louisiana Certification #: FL NELAC Reciprocity Louisiana Environmental Certificate #: 05007 Maryland Certification: #346 Massachusetts Certification #: M-FL1264 Michigan Certification #: 9911 Mississippi Certification: FL NELAC Reciprocity Missouri Certification #: 236 Montana Certification #: Cert 0074 Nebraska Certification: NE-OS-28-14 Nevada Certification: FL NELAC Reciprocity New Hampshire Certification #: 2958 New Jersey Certification #: FL765 New York Certification #: 11608 North Carolina Environmental Certificate #: 667 Pennsylvania Certification #: 68-00547 Puerto Rico Certification #: FL01264 South Carolina Certification: #96042001 Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity US Virgin Islands Certification: FL NELAC Reciprocity Virginia Environmental Certification #: 460165 Washington Certification #: C955 West Virginia Certification #: 9962C Wisconsin Certification #: 399079670 Wyoming (EPA Region 8): FL NELAC Reciprocity Green Bay Certification IDs 1241 Bellevue Street, Green Bay, WI 54302 Florida/NELAP Certification #: E87948 Illinois Certification #: 200050 Kentucky Certification #: 82 Louisiana Certification #: 04168 Minnesota Certification #: 055-999-334 North Dakota Certification #: R-150 South Carolina Certification #: 83006001 Texas Certification #: T104704529-14-1 US Dept of Agriculture #: S-76505 Wisconsin Certification #: 405132750 Asheville Certification IDs 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Certification #: 99030001 West Virginia Certification #: 356 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 2 of 30 6 of 36 #=SS# SAMPLE SUMMARY Pace Project No.: Project: 92247909 J15050018 Lab ID Sample ID Matrix Date Collected Date Received 92247909001 2015012958 Solid 04/28/15 13:00 05/01/15 12:57 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 30 7 of 36 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92247909 J15050018 Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92247909001 2015012958 EPA 6010 16 PASI-OTAP EPA 6020 8 PASI-ODRS EPA 7471 1 PASI-OCKJ ASTM D2974-87 1 PASI-OMLO EPA 9045 1 PASI-AMLS EPA 9056 2 PASI-OKHC EPA 9056 1 PASI-OKHC EPA 9060 6 PASI-GTJJ REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 4 of 30 8 of 36 #=HO# SUMMARY OF DETECTION Pace Project No.: Project: 92247909 J15050018 Parameters AnalyzedResult Lab Sample ID Report Limit QualifiersUnitsMethod Client Sample ID 92247909001 2015012958 Aluminum 17400 mg/kg 05/10/15 17:4628.1EPA 6010 Barium 179 mg/kg 05/10/15 17:462.8EPA 6010 Beryllium 1.5 mg/kg 05/10/15 17:460.28EPA 6010 Calcium 2870 mg/kg 05/10/15 17:46140EPA 6010 Chromium 141 mg/kg 05/10/15 17:461.4EPA 6010 Copper 11.2 mg/kg 05/10/15 17:461.4EPA 6010 Iron 31500 mg/kg 05/10/15 17:4611.2EPA 6010 Magnesium 15200 mg/kg 05/10/15 17:46140EPA 6010 Manganese 2820 mg/kg 05/11/15 12:51 D42.8EPA 6010 Molybdenum 3.3 mg/kg 05/10/15 17:462.8EPA 6010 Nickel 75.3 mg/kg 05/10/15 17:461.4EPA 6010 Potassium 7650 mg/kg 05/10/15 17:46281EPA 6010 Strontium 24.4 mg/kg 05/10/15 17:462.8EPA 6010 Zinc 195 mg/kg 05/10/15 17:465.6EPA 6010 Cadmium 0.49J mg/kg 05/13/15 11:540.67EPA 6020 Cobalt 19.9 mg/kg 05/13/15 11:545.6EPA 6020 Lead 8.0 mg/kg 05/13/15 11:545.6EPA 6020 Vanadium 50.1 mg/kg 05/13/15 11:545.6EPA 6020 Percent Moisture 11.6 %05/11/15 10:330.10ASTM D2974-87 pH at 25 Degrees C 7.3 Std. Units 05/06/15 13:000.10EPA 9045 Total Organic Carbon 377J mg/kg 05/26/15 13:05677EPA 9060 Total Organic Carbon 383J mg/kg 05/26/15 13:17685EPA 9060 Total Organic Carbon 346J mg/kg 05/26/15 13:22672EPA 9060 Mean Total Organic Carbon 356J mg/kg 05/26/15 13:05679EPA 9060 RSD%8.3 %05/26/15 13:05EPA 9060 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 5 of 30 9 of 36 #=NA# PROJECT NARRATIVE Pace Project No.: Project: 92247909 J15050018 Method: Client:Duke Energy EPA 6010 Date:May 27, 2015 Description:6010 MET ICP General Information: 1 sample was analyzed for EPA 6010. All samples were received in acceptable condition with any exceptions noted below. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 3050 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. QC Batch: MPRP/24040 A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92247834001 M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. • MS (Lab ID: 1208607) • Aluminum • Iron • MSD (Lab ID: 1208608) • Aluminum • Iron • Manganese Additional Comments: Batch Comments: Samples in this batch were diluted due to the presence of high levels of non-target analytes or other matrix interference. • QC Batch: ICP / 14693 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 6 of 30 10 of 36 #=NA# PROJECT NARRATIVE Pace Project No.: Project: 92247909 J15050018 Method: Client:Duke Energy EPA 6010 Date:May 27, 2015 Description:6010 MET ICP Analyte Comments: QC Batch: MPRP/24040 D4: Sample was diluted due to the presence of high levels of target analytes. • 2015012958 (Lab ID: 92247909001) • Manganese REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 7 of 30 11 of 36 #=NA# PROJECT NARRATIVE Pace Project No.: Project: 92247909 J15050018 Method: Client:Duke Energy EPA 6020 Date:May 27, 2015 Description:6020 MET ICPMS General Information: 1 sample was analyzed for EPA 6020. All samples were received in acceptable condition with any exceptions noted below. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 3050 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Internal Standards: All internal standards were within QC limits with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. QC Batch: MPRP/24041 A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92247834001 M6: Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. • MS (Lab ID: 1208613) • Antimony • Cadmium • Cobalt • Vanadium • MSD (Lab ID: 1208614) • Antimony • Cobalt • Lead • Selenium Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 8 of 30 12 of 36 #=NA# PROJECT NARRATIVE Pace Project No.: Project: 92247909 J15050018 Method: Client:Duke Energy EPA 6020 Date:May 27, 2015 Description:6020 MET ICPMS Batch Comments: Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference. • QC Batch: ICPM / 9756 Analyte Comments: QC Batch: MPRP/24041 N2: The lab does not hold TNI accreditation for this parameter. • 2015012958 (Lab ID: 92247909001) • Antimony • BLANK (Lab ID: 1208611) • Antimony • LCS (Lab ID: 1208612) • Antimony • MS (Lab ID: 1208613) • Antimony • MSD (Lab ID: 1208614) • Antimony REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 9 of 30 13 of 36 #=NA# PROJECT NARRATIVE Pace Project No.: Project: 92247909 J15050018 Method: Client:Duke Energy EPA 7471 Date:May 27, 2015 Description:7471 Mercury General Information: 1 sample was analyzed for EPA 7471. All samples were received in acceptable condition with any exceptions noted below. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Sample Preparation: The samples were prepared in accordance with EPA 7471 with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 10 of 30 14 of 36 #=NA# PROJECT NARRATIVE Pace Project No.: Project: 92247909 J15050018 Method: Client:Duke Energy EPA 9045 Date:May 27, 2015 Description:9045 pH Soil General Information: 1 sample was analyzed for EPA 9045. All samples were received in acceptable condition with any exceptions noted below. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Duplicate Sample: All duplicate sample results were within method acceptance criteria with any exceptions noted below. QC Batch: WET/37238 D6: The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. • DUP (Lab ID: 1450002) • pH at 25 Degrees C Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 11 of 30 15 of 36 #=NA# PROJECT NARRATIVE Pace Project No.: Project: 92247909 J15050018 Method: Client:Duke Energy EPA 9056 Date:May 27, 2015 Description:9056 IC Anions General Information: 1 sample was analyzed for EPA 9056. All samples were received in acceptable condition with any exceptions noted below. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: Analyte Comments: QC Batch: WETA/46118 D3: Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference. • 2015012958 (Lab ID: 92247909001) • Chloride • Sulfate REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 12 of 30 16 of 36 #=NA# PROJECT NARRATIVE Pace Project No.: Project: 92247909 J15050018 Method: Client:Duke Energy EPA 9056 Date:May 27, 2015 Description:9056 IC Anions 48hr General Information: 1 sample was analyzed for EPA 9056. All samples were received in acceptable condition with any exceptions noted below. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. H3: Sample was received or analysis requested beyond the recognized method holding time. • 2015012958 (Lab ID: 92247909001) Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 13 of 30 17 of 36 #=NA# PROJECT NARRATIVE Pace Project No.: Project: 92247909 J15050018 Method: Client:Duke Energy EPA 9060 Date:May 27, 2015 Description:Total Organic Carbon Quad General Information: 1 sample was analyzed for EPA 9060. All samples were received in acceptable condition with any exceptions noted below. Hold Time: The samples were analyzed within the method required hold times with any exceptions noted below. Initial Calibrations (including MS Tune as applicable): All criteria were within method requirements with any exceptions noted below. Continuing Calibration: All criteria were within method requirements with any exceptions noted below. Method Blank: All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below. Laboratory Control Spike: All laboratory control spike compounds were within QC limits with any exceptions noted below. Matrix Spikes: All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below. Additional Comments: This data package has been reviewed for quality and completeness and is approved for release. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 14 of 30 18 of 36 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92247909 J15050018 Sample:2015012958 Lab ID:92247909001 Collected:04/28/15 13:00 Received:05/01/15 12:57 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 6010 Preparation Method: EPA 30506010 MET ICP Aluminum 17400 mg/kg 05/10/15 17:46 7429-90-505/09/15 09:3428.1 14.0 5 Barium 179 mg/kg 05/10/15 17:46 7440-39-305/09/15 09:342.8 1.4 5 Beryllium 1.5 mg/kg 05/10/15 17:46 7440-41-705/09/15 09:340.28 0.14 5 Boron ND mg/kg 05/10/15 17:46 7440-42-805/09/15 09:3414.0 7.0 5 Calcium 2870 mg/kg 05/10/15 17:46 7440-70-205/09/15 09:3414070.2 5 Chromium 141 mg/kg 05/10/15 17:46 7440-47-305/09/15 09:341.4 0.70 5 Copper 11.2 mg/kg 05/10/15 17:46 7440-50-805/09/15 09:341.4 0.70 5 Iron 31500 mg/kg 05/10/15 17:46 7439-89-605/09/15 09:3411.2 5.6 5 Magnesium 15200 mg/kg 05/10/15 17:46 7439-95-405/09/15 09:3414070.2 5 Manganese 2820 mg/kg 05/11/15 12:51 7439-96-5 D405/09/15 09:342.8 1.4 10 Molybdenum 3.3 mg/kg 05/10/15 17:46 7439-98-705/09/15 09:342.8 1.4 5 Nickel 75.3 mg/kg 05/10/15 17:46 7440-02-005/09/15 09:341.4 0.70 5 Potassium 7650 mg/kg 05/10/15 17:46 7440-09-705/09/15 09:342811405 Sodium ND mg/kg 05/10/15 17:46 7440-23-505/09/15 09:342811405 Strontium 24.4 mg/kg 05/10/15 17:46 7440-24-605/09/15 09:342.8 1.4 5 Zinc 195 mg/kg 05/10/15 17:46 7440-66-605/09/15 09:345.6 2.8 5 Analytical Method: EPA 6020 Preparation Method: EPA 30506020 MET ICPMS Antimony ND mg/kg 05/13/15 11:54 7440-36-0 N205/09/15 09:345.6 2.8 100 Arsenic ND mg/kg 05/13/15 11:54 7440-38-205/09/15 09:345.6 2.8 100 Cadmium 0.49J mg/kg 05/13/15 11:54 7440-43-905/09/15 09:340.67 0.34 100 Cobalt 19.9 mg/kg 05/13/15 11:54 7440-48-405/09/15 09:345.6 2.8 100 Lead 8.0 mg/kg 05/13/15 11:54 7439-92-105/09/15 09:345.6 2.8 100 Selenium ND mg/kg 05/13/15 11:54 7782-49-205/09/15 09:345.6 2.8 100 Thallium ND mg/kg 05/13/15 11:54 7440-28-005/09/15 09:345.6 2.8 100 Vanadium 50.1 mg/kg 05/13/15 11:54 7440-62-205/09/15 09:345.6 2.8 100 Analytical Method: EPA 7471 Preparation Method: EPA 74717471 Mercury Mercury ND mg/kg 05/09/15 18:03 7439-97-605/09/15 09:410.0092 0.0046 1 Analytical Method: ASTM D2974-87Percent Moisture Percent Moisture 11.6 %05/11/15 10:330.10 0.10 1 Analytical Method: EPA 90459045 pH Soil pH at 25 Degrees C 7.3 Std. Units 05/06/15 13:000.10 0.10 1 Analytical Method: EPA 90569056 IC Anions Chloride ND mg/kg 05/06/15 11:27 16887-00-6 D32781395 Sulfate ND mg/kg 05/06/15 11:27 14808-79-8 D32781395 Analytical Method: EPA 90569056 IC Anions 48hr Nitrate as N ND mg/kg 05/06/15 11:27 14797-55-8 H327.8 13.9 5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 02:42 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 15 of 30 19 of 36 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92247909 J15050018 Sample:2015012958 Lab ID:92247909001 Collected:04/28/15 13:00 Received:05/01/15 12:57 Matrix:Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units DF Prepared Analyzed CAS No.QualMDLLimit Report Analytical Method: EPA 9060Total Organic Carbon Quad Total Organic Carbon 377J mg/kg 05/26/15 13:05 7440-44-06773381 Total Organic Carbon ND mg/kg 05/26/15 13:10 7440-44-06823411 Total Organic Carbon 383J mg/kg 05/26/15 13:17 7440-44-06853431 Total Organic Carbon 346J mg/kg 05/26/15 13:22 7440-44-06723361 Mean Total Organic Carbon 356J mg/kg 05/26/15 13:05 7440-44-06793391 Surrogates RSD%8.3 %05/26/15 13:051 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 02:42 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 16 of 30 20 of 36 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92247909 J15050018 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MERP/5697 EPA 7471 EPA 7471 7471 Mercury Associated Lab Samples:92247909001 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1208617 Associated Lab Samples:92247909001 Matrix:Solid Analyzed Mercury mg/kg ND 0.0082 05/09/15 17:09 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1208618LABORATORY CONTROL SAMPLE: LCSSpike Mercury mg/kg 0.083.083 100 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1208619MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92247834001 1208620 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mercury mg/kg .079 101 80-120102 2 20.0770.018 0.098 0.097 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 02:42 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 17 of 30 21 of 36 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92247909 J15050018 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/24040 EPA 3050 EPA 6010 6010 MET Solid Associated Lab Samples:92247909001 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1208605 Associated Lab Samples:92247909001 Matrix:Solid Analyzed Aluminum mg/kg ND 5.1 05/10/15 15:56 Barium mg/kg ND 0.51 05/10/15 15:56 Beryllium mg/kg ND 0.051 05/10/15 15:56 Boron mg/kg ND 2.6 05/10/15 15:56 Calcium mg/kg ND 25.6 05/10/15 15:56 Chromium mg/kg ND 0.26 05/10/15 15:56 Copper mg/kg ND 0.26 05/10/15 15:56 Iron mg/kg ND 2.0 05/10/15 15:56 Magnesium mg/kg ND 25.6 05/10/15 15:56 Manganese mg/kg ND 0.26 05/10/15 15:56 Molybdenum mg/kg ND 0.51 05/10/15 15:56 Nickel mg/kg ND 0.26 05/10/15 15:56 Potassium mg/kg ND 51.1 05/10/15 15:56 Sodium mg/kg ND 51.1 05/10/15 15:56 Strontium mg/kg ND 0.51 05/10/15 15:56 Zinc mg/kg ND 1.0 05/10/15 15:56 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1208606LABORATORY CONTROL SAMPLE: LCSSpike Aluminum mg/kg 139130 107 80-120 Barium mg/kg 13.913 106 80-120 Beryllium mg/kg 1.41.3 105 80-120 Boron mg/kg 133130 102 80-120 Calcium mg/kg 699651 107 80-120 Chromium mg/kg 13.113 101 80-120 Copper mg/kg 13.013 100 80-120 Iron mg/kg 138130 106 80-120 Magnesium mg/kg 682651 105 80-120 Manganese mg/kg 13.513 103 80-120 Molybdenum mg/kg 13.313 102 80-120 Nickel mg/kg 13.713 105 80-120 Potassium mg/kg 675651 104 80-120 Sodium mg/kg 708651 109 80-120 Strontium mg/kg 13.713 105 80-120 Zinc mg/kg 68.965.1 106 80-120 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 02:42 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 18 of 30 22 of 36 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92247909 J15050018 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 1208607MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92247834001 1208608 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Aluminum mg/kg M111996975-1251150 9 20130253036904030 Barium mg/kg 11.9 112 75-125120 5 201327.2 40.6 42.9 Beryllium mg/kg 1.2 99 75-12592 1 201.30.18J 1.4 1.4 Boron mg/kg 119 90 75-12583 0 20130ND110109 Calcium mg/kg 595 106 75-125104 4 2064947011001140 Chromium mg/kg 11.9 100 75-12594 2 20134.3 16.2 16.5 Copper mg/kg 11.9 98 75-12593 3 20133.4 15.0 15.5 Iron mg/kg M111916175-125527 9 20130475049505440 Magnesium mg/kg 595 105 75-125101 3 206493499751010 Manganese mg/kg M111.9 122 75-125195 5 2013180195206 Molybdenum mg/kg 11.9 88 75-12581 1 2013ND10.9 11.0 Nickel mg/kg 11.9 102 75-12595 2 20131.7 13.8 14.0 Potassium mg/kg 595 96 75-12590 2 20649135J706717 Sodium mg/kg 595 99 75-12595 4 20649ND644672 Strontium mg/kg 11.9 102 75-12597 3 20134.2 16.4 16.9 Zinc mg/kg 59.5 109 75-125100 0 2064.922.0 87.1 87.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 02:42 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 19 of 30 23 of 36 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92247909 J15050018 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: MPRP/24041 EPA 3050 EPA 6020 6020 MET SOLID Associated Lab Samples:92247909001 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1208611 Associated Lab Samples:92247909001 Matrix:Solid Analyzed Antimony mg/kg ND 0.053 N205/11/15 12:09 Arsenic mg/kg ND 0.053 05/11/15 12:09 Cadmium mg/kg ND 0.0063 05/11/15 12:09 Cobalt mg/kg ND 0.053 05/11/15 12:09 Lead mg/kg ND 0.053 05/11/15 12:09 Selenium mg/kg ND 0.053 05/11/15 12:09 Thallium mg/kg ND 0.053 05/11/15 12:09 Vanadium mg/kg ND 0.053 CU05/12/15 17:01 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1208612LABORATORY CONTROL SAMPLE: LCSSpike Antimony mg/kg 2.7 N22.6 101 80-120 Arsenic mg/kg 2.72.6 102 80-120 Cadmium mg/kg 0.27.26 101 80-120 Cobalt mg/kg 2.72.6 104 80-120 Lead mg/kg 2.72.6 104 80-120 Selenium mg/kg 2.72.6 101 80-120 Thallium mg/kg 2.72.6 104 80-120 Vanadium mg/kg 2.62.6 100 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1208613MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92247834001 1208614 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Antimony mg/kg M6,N22.6 60 75-12561 202.6ND ND ND Arsenic mg/kg 2.6 88 75-12587 202.6ND 3.5J 3.3J Cadmium mg/kg M6.26 60 75-12583 20.26ND ND ND Cobalt mg/kg M62.6 130 75-125129 2 202.63.3J 6.7 6.6 Lead mg/kg M62.6 125 75-125128 1 202.63.6J 6.9 6.9 Selenium mg/kg M62.6 92 75-12555 202.6ND 3.2J ND Thallium mg/kg 2.6 91 75-12593 202.6ND ND ND Vanadium mg/kg M62.6 136 75-125119 5 202.68.5 12.1 11.5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 02:42 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 20 of 30 24 of 36 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92247909 J15050018 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: PMST/3544 ASTM D2974-87 ASTM D2974-87 Dry Weight/Percent Moisture Associated Lab Samples:92247909001 Parameter Units Dup Result Max RPD QualifiersRPDResult 35185070001 1209474SAMPLE DUPLICATE: Percent Moisture %99.2 0 1099.5 Parameter Units Dup Result Max RPD QualifiersRPDResult 92247911001 1209476SAMPLE DUPLICATE: Percent Moisture %26.6 2 1025.9 Parameter Units Dup Result Max RPD QualifiersRPDResult 92247911010 1209477SAMPLE DUPLICATE: Percent Moisture %29.0 1 1028.8 Parameter Units Dup Result Max RPD QualifiersRPDResult 35186853004 1209478SAMPLE DUPLICATE: Percent Moisture %19.0 5 1018.1 Parameter Units Dup Result Max RPD QualifiersRPDResult 35187478002 1209479SAMPLE DUPLICATE: Percent Moisture %8.5 5 108.1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 02:42 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 21 of 30 25 of 36 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92247909 J15050018 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: WET/37238 EPA 9045 EPA 9045 9045 pH Associated Lab Samples:92247909001 Parameter Units Dup Result Max RPD QualifiersRPDResult 92248135013 1450001SAMPLE DUPLICATE: pH at 25 Degrees C Std. Units 7.2 0 107.1 Parameter Units Dup Result Max RPD QualifiersRPDResult 92247913005 1450002SAMPLE DUPLICATE: pH at 25 Degrees C Std. Units 5.0 D62105.0 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 02:42 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 22 of 30 26 of 36 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92247909 J15050018 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/46118 EPA 9056 EPA 9056 9056 IC Anions Associated Lab Samples:92247909001 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1204695 Associated Lab Samples: Matrix:Solid Analyzed Chloride mg/kg ND 50.0 05/06/15 10:44 Sulfate mg/kg ND 50.0 05/06/15 10:44 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1204696LABORATORY CONTROL SAMPLE: LCSSpike Chloride mg/kg 453491 92 80-120 Sulfate mg/kg 450491 92 80-120 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1204698MATRIX SPIKE SAMPLE: MSSpike Result 92247909001 Chloride mg/kg 492561 88 80-120ND Sulfate mg/kg 513561 92 80-120ND Parameter Units Dup Result Max RPD QualifiersRPDResult 92247909001 1204697SAMPLE DUPLICATE: Chloride mg/kg ND D320ND Sulfate mg/kg ND D320ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 02:42 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 23 of 30 27 of 36 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92247909 J15050018 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/46117 EPA 9056 EPA 9056 9056 IC Anions Associated Lab Samples:92247909001 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1204691 Associated Lab Samples: Matrix:Solid Analyzed Nitrate as N mg/kg ND 5.0 05/06/15 10:44 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1204692LABORATORY CONTROL SAMPLE: LCSSpike Nitrate as N mg/kg 46.249.1 94 80-120 Parameter Units MS Result % Rec Limits Qualifiers% RecConc. 1204694MATRIX SPIKE SAMPLE: MSSpike Result 92247909001 Nitrate as N mg/kg 49.9 H356.1 89 80-120ND Parameter Units Dup Result Max RPD QualifiersRPDResult 92247909001 1204693SAMPLE DUPLICATE: Nitrate as N mg/kg ND H320ND REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 02:42 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 24 of 30 28 of 36 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92247909 J15050018 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: WETA/28613 EPA 9060 EPA 9060 9060 TOC Average Associated Lab Samples:92247909001 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:1161513 Associated Lab Samples: Matrix:Solid Analyzed Mean Total Organic Carbon mg/kg ND 600 05/26/15 08:34 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 1161514LABORATORY CONTROL SAMPLE: LCSSpike Mean Total Organic Carbon mg/kg 130000120000 108 80-120 Parameter Units MS Result % Rec Limits Qual% RecConc. 1161515MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92247835016 1161516 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mean Total Organic Carbon mg/kg 7410 101 50-150110 6 30741027501030010900 Parameter Units MS Result % Rec Limits Qual% RecConc. 1161527MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92248424001 1161528 MSD Result MSD % Rec RPD RPD Max MSDMS Spike Conc. Mean Total Organic Carbon mg/kg 60900 102 50-15091 6 306090050700113000106000 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 02:42 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 25 of 30 29 of 36 #=QL# QUALIFIERS Pace Project No.: Project: 92247909 J15050018 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES Pace Analytical Services - AshevillePASI-A Pace Analytical Services - Green BayPASI-G Pace Analytical Services - Ormond BeachPASI-O BATCH QUALIFIERS Batch: ICP/14693 Samples in this batch were diluted due to the presence of high levels of non-target analytes or other matrix interference.[1] Batch: ICPM/9756 Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.[1] ANALYTE QUALIFIERS The continuing calibration for this compound is outside of Pace Analytical acceptance limits. Analyte presence below reporting limits in associated samples. Results unaffected by high bias.CU Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3 Sample was diluted due to the presence of high levels of target analytes.D4 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.D6 Sample was received or analysis requested beyond the recognized method holding time.H3 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 02:42 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 26 of 30 30 of 36 #=QL# QUALIFIERS Pace Project No.: Project: 92247909 J15050018 ANALYTE QUALIFIERS The lab does not hold TNI accreditation for this parameter.N2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 02:42 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 27 of 30 31 of 36 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92247909 J15050018 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92247909001 MPRP/24040 ICP/146932015012958EPA 3050 EPA 6010 92247909001 MPRP/24041 ICPM/97562015012958EPA 3050 EPA 6020 92247909001 MERP/5697 MERC/56842015012958EPA 7471 EPA 7471 92247909001 PMST/35442015012958ASTM D2974-87 92247909001 WET/372382015012958EPA 9045 92247909001 WETA/461182015012958EPA 9056 92247909001 WETA/461172015012958EPA 9056 92247909001 WETA/286132015012958EPA 9060 92247909001 WETA/286142015012958EPA 9060 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc..Date: 05/27/2015 02:42 PM Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 28 of 30 32 of 36 Page 29 of 30 33 of 36 Page 30 of 30 34 of 36 35 of 36 36 of 36