NC0038377_J15020119report_20171101

13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number:J15020119
Project Name:
Lab Contact:Mary Ann Ogle
Date:2/19/2015
Customer Address:
Customer Name(s):Tim Hunsucker, Jerry Wylie, Kathy Webb, John Toepfer
Phone: [phone]
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.
Mary Ann Ogle
Page 1 of 40
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection
Date and Time Collected By Sample Description
2015002836 MAYO STEAM 03-Feb-15 3:19 PM Water Source
2015002837 MAYO STEAM 03-Feb-15 3:33 PM illegible Water Source
2015002838 MAYO STEAM 03-Feb-15 3:25 PM illegible Water Source
2015002840 MAYO STEAM 03-Feb-15 3:26 PM illegible Water Source
2015002841 MAYO STEAM 03-Feb-15 3:27 PM illegible Water Source
2015002843 MAYO STEAM 03-Feb-15 3:31 PM illegible Water Source
2015002844 MAYO STEAM 03-Feb-15 3:40 PM illegible Water Source
2015002845 MAYO STEAM 03-Feb-15 3:21 PM illegible Water Source
2015002846 MAYO STEAM 03-Feb-15 3:24 PM illegible Water Source
2015002851 MAYO STEAM 03-Feb-15 3:33 PM illegible Field Blank
2015002852 MAYO STEAM 03-Feb-15 3:38 PM illegible Trip Blank
11 Total Samples
Page 2 of 40
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:DBA Account Date:2/19/2015
Electronic Data Deliverable (EDD) Sent Separately
Page 3 of 40
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020119
2015002836
Collection Date:03-Feb-15 3:19 PM
Site: Water Source
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L SM2540C 02/10/2015 15:53 GHUTCHI251
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 02/05/2015 09:41 GHUTCHI51
Page 4 of 40
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020119
2015002837
Collection Date:03-Feb-15 3:33 PM
Site: Water Source
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
Page 5 of 40
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020119
2015002838
Collection Date:03-Feb-15 3:25 PM
Site: Water Source
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
INORGANIC IONS BY IC
Chloride < 0.1 mg/L EPA 300.0 02/05/2015 22:26 BGN90340.1 1
Nitrate < 0.1 mg/L EPA 300.0 02/05/2015 22:26 BGN90340.1 1
Nitrate as N < 0.023 mg-N/L EPA 300.0 02/05/2015 22:26 BGN90340.023 1
Sulfate < 0.1 mg/L EPA 300.0 02/05/2015 22:26 BGN90340.1 1
Page 6 of 40
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020119
2015002840
Collection Date:03-Feb-15 3:26 PM
Site: Water Source
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 02/14/2015 11:24 TLINN0.01 1
Total Carbon
TOC < 0.1 mg/L SM5310C/EPA9060A 02/12/2015 15:45 TJA70670.1 1
Page 7 of 40
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020119
2015002841
Collection Date:03-Feb-15 3:27 PM
Site: Water Source
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
Page 8 of 40
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020119
2015002843
Collection Date:03-Feb-15 3:31 PM
Site: Water Source
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
Page 9 of 40
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020119
2015002844
Collection Date:03-Feb-15 3:40 PM
Site: Water Source
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
Page 10 of 40
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020119
2015002845
Collection Date:03-Feb-15 3:21 PM
Site: Water Source
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/06/2015 09:28 TLINN0.05 1
UNDIGESTED METALS BY ICP
Calcium (Ca)< 0.01 mg/L EPA 200.7 02/11/2015 15:14 MHALL30.01 1
Magnesium (Mg)< 0.005 mg/L EPA 200.7 02/11/2015 15:14 MHALL30.005 1
Potassium (K)< 0.1 mg/L EPA 200.7 02/11/2015 15:14 MHALL30.1 1
Sodium (Na)< 0.05 mg/L EPA 200.7 02/11/2015 15:14 MHALL30.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 02/05/2015 15:21 MHH71310.005 1
Barium (Ba)< 0.005 mg/L EPA 200.7 02/05/2015 15:21 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 02/05/2015 15:21 MHH71310.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 02/05/2015 15:21 MHH71310.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 02/05/2015 15:21 MHH71310.005 1
Strontium (Sr)< 0.005 mg/L EPA 200.7 02/05/2015 15:21 MHH71310.005 1
Zinc (Zn)0.006 mg/L EPA 200.7 02/05/2015 15:21 MHH71310.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/06/2015 12:07 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 02/06/2015 12:07 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 02/06/2015 12:07 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 02/06/2015 12:07 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 02/06/2015 12:07 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 02/06/2015 12:07 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 02/06/2015 12:07 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 02/06/2015 12:07 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 02/06/2015 12:07 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 02/06/2015 12:07 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 02/06/2015 12:07 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/06/2015 12:07 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/06/2015 12:07 JAHERMA0.3 1
Page 11 of 40
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020119
2015002846
Collection Date:03-Feb-15 3:24 PM
Site: Water Source
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/18/2015 19:47 TLINN0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 02/09/2015 15:46 MHH71310.005 1
Barium (Ba)< 0.005 mg/L EPA 200.7 02/09/2015 15:46 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 02/09/2015 15:46 MHH71310.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 02/09/2015 15:46 MHH71310.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 02/09/2015 15:46 MHH71310.005 1
Strontium (Sr)< 0.005 mg/L EPA 200.7 02/09/2015 15:46 MHH71310.005 1
Zinc (Zn)0.005 mg/L EPA 200.7 02/09/2015 15:46 MHH71310.005 1
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/11/2015 12:32 DJSULL111
Arsenic (As)< 1 ug/L EPA 200.8 02/11/2015 12:32 DJSULL111
Beryllium (Be)< 1 ug/L EPA 200.8 02/11/2015 12:32 DJSULL111
Cadmium (Cd)< 1 ug/L EPA 200.8 02/11/2015 12:32 DJSULL111
Chromium (Cr)< 1 ug/L EPA 200.8 02/11/2015 12:32 DJSULL111
Cobalt (Co)< 1 ug/L EPA 200.8 02/11/2015 12:32 DJSULL111
Copper (Cu)< 1 ug/L EPA 200.8 02/11/2015 12:32 DJSULL111
Lead (Pb)< 1 ug/L EPA 200.8 02/11/2015 12:32 DJSULL111
Molybdenum (Mo)< 1 ug/L EPA 200.8 02/11/2015 12:32 DJSULL111
Nickel (Ni)< 1 ug/L EPA 200.8 02/11/2015 12:32 DJSULL111
Selenium (Se)< 1 ug/L EPA 200.8 02/11/2015 12:32 DJSULL111
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/11/2015 12:32 DJSULL10.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/11/2015 12:32 DJSULL10.3 1
Page 12 of 40
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020119
2015002851
Collection Date:03-Feb-15 3:33 PM
Site: Field Blank
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
Page 13 of 40
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020119
2015002852
Collection Date:03-Feb-15 3:38 PM
Site: Trip Blank
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
Page 14 of 40
Page 15 of 40
Page 16 of 40
Page 17 of 40
Page 18 of 40
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
QB05069Lot Number:
J15020119Project Number:
AB GW Assessment WaterProject Name:
02/12/2015Date Completed:
Grant Wilton
Project Manager
*QB05069*

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Duke Energy
Lot Number: QB05069
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
Project Name: AB GW Assessment Water
Project Number: J15020119
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Page: 2 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QB05069

Project Name: AB GW Assessment Water
Project Number: J15020119
Sample Number Sample ID Matrix Date Sampled Date Received
001 02/03/2015 15332015002837 Water Source (drilling)Aqueous 02/05/2015
002 02/03/2015 15272015002841 Water Source (drilling)Aqueous 02/05/2015
003 02/03/2015 15402015002844 Water Source (drilling)Aqueous 02/05/2015
004 02/03/2015 15352015002851 Field Blank Aqueous 02/05/2015
005 02/03/2015 15302015002852 Trip Blank Aqueous 02/05/2015
(5 samples)
Page: 3 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QB05069

Project Name: AB GW Assessment Water
Project Number: J15020119
Sample Sample ID Matrix Parameter Method Result Q Units Page
(0 detections)
Page: 4 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015002837 Water Source (drilling)
QB05069-001
02/03/2015 1533
02/05/2015
Aqueous
Project Name: AB GW Assessment Water
Project Number: J15020119
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 02/06/2015 2307 JJG 67181
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 5 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015002841 Water Source (drilling)
QB05069-002
02/03/2015 1527
02/05/2015
Aqueous
Project Name: AB GW Assessment Water
Project Number: J15020119
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 02/06/2015 2251 BWS 67140
1 (Bicarbonate ) SM 2320B-2011 1 02/06/2015 2251 BWS 02/06/2015 2251
1 (Carbonate Al) SM 2320B-2011 1 02/06/2015 2251 BWS 02/06/2015 2251
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 ND 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 ND 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015002844 Water Source (drilling)
QB05069-003
02/03/2015 1540
02/05/2015
Aqueous
Project Name: AB GW Assessment Water
Project Number: J15020119
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 02/11/2015 1112 COH 02/09/2015 1616 67306
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E ND 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015002851 Field Blank
QB05069-004
02/03/2015 1535
02/05/2015
Aqueous
Project Name: AB GW Assessment Water
Project Number: J15020119
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 02/11/2015 1126 COH 02/09/2015 1616 67306
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E ND 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 9
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Mercury (CVAFS)
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015002852 Trip Blank
QB05069-005
02/03/2015 1530
02/05/2015
Aqueous
Project Name: AB GW Assessment Water
Project Number: J15020119
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631E 1 02/11/2015 1130 COH 02/09/2015 1616 67306
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS)7439-97-6 1631E ND 1ng/L0.500
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 9
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Shealy Environmental Services, Inc.
Level 1 Report v2.1
QC Summary
QC Data for Lot Number: QB05069
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - MB
Batch:
Sample ID:QQ67140-001
67140
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Alkalinity ND 02/06/2015 204110mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QB05069
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - LCS
Batch:
Sample ID:QQ67140-002
67140
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Alkalinity 100 02/06/2015 204710210090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QB05069
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane - MB
Batch:
Sample ID:QQ67181-001
67181
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Methane ND 02/06/2015 201410ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QB05069
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane - LCS
Batch:
Sample ID:QQ67181-002
67181
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Methane 120 02/06/2015 19317715070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QB05069
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane - LCSD
Batch:
Sample ID:QQ67181-003
67181
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Methane 120 02/06/2015 19577815070-1301.1 301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QB05069
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Mercury (CVAFS) - MB
Batch:Prep Method:
Prep Date:
Sample ID:QQ67306-001
67306 1631E
02/09/2015 1616Analytical Method:1631E
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Mercury (CVAFS)ND 02/11/2015 11020.500 ng/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QB05069
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Mercury (CVAFS) - LCS
Batch:Prep Method:
Prep Date:
Sample ID:QQ67306-002
67306 1631E
02/09/2015 1616Analytical Method:1631E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ng/L)(ng/L)
Mercury (CVAFS)5.06 02/11/2015 11071015.00 75-1251
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QB05069
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Mercury (CVAFS) - MS
Batch:Prep Method:
Prep Date:
Sample ID:QB05069-003MS
67306 1631E
02/09/2015 1616Analytical Method:1631E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
Limit
Sample
Amount
Dil(ng/L)(ng/L)(ng/L)
Mercury (CVAFS)4.72 02/11/2015 1116945.00 71-125ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QB05069
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Mercury (CVAFS) - MSD
Batch:Prep Method:
Prep Date:
Sample ID:QB05069-003MD
67306 1631E
02/09/2015 1616Analytical Method:1631E
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
Limit
Sample
Amount
Dil(ng/L)(ng/L)(ng/L)
Mercury (CVAFS)4.69 02/11/2015 1121945.00 71-1250.64 24ND1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QB05069
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
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