Loading...
HomeMy WebLinkAboutNC0022217_Renewal Application_20171023Waxer Resources ENVIRONMENTAL QUALITY October 24, 2017 Scott Dilling, Complex Manager Motiva Enterprises LLC 410 Tom Sadler Rd Charlotte, NC 28214 Subject: Permit Renewal Application No. NCO022217 Apex Terminal Wake County Dear Applicant: ROY COOPER Gowemar MICHAEL S. REGAN secretary S. JAY ZIMMERMAN lfmor The Water Quality Permitting Section acknowledges the October 23, 2017 receipt of your permit renewal application and supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW permitting branch. Per G.S. 1506-3 your current permit does not expire until permit decision on the application is made. Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit. The permit writer will contact you if additional information is required to complete your permit renewal. Please respond in a timely manner to requests for additional information necessary to allow a complete review of the application and renewal of the permit. Information regarding the status of your renewal application can be found online using the Department of Environmental Quality's Environmental Application Tracker at: https://deq. nc.gov/permits-reg ulations/permit-guidance/environmental-application-tracker If you have any additional questions about the permit, please contact the primary reviewer of the application using the links available within the Application Tracker. .J�SincereYdfk Wren Td Administrative Assistant Water Quality Permitting Section cc: Central Files w/application(RRO) ec: WQPS Laserfiche File w/application State of North Carolina I Environmental Quality I Water Resources 1617 Mail Service Center I Raleigh, North Carolina 27699-1617 919-807-6300 MOTIVA ENTERPRISES LLC October 23, 2017 John Hennessy 512 N. Salisbury Street (9th Floor -Archdale Bldg) Raleigh, NC 27604 Phone: 919-807-6397 RE: NPDES Minor Industrial Permit Renewal Application Motiva Enterprises, LLC Apex Terminal Permit No. NCO022217 Dear Mr. Hennessy, Please find included with this cover letter, Motiva's NPDES minor industrial permit renewal application for our bulk terminal in Apex, North Carolina. Our current permit expires on April 30, 2018. This application is being submitted more than 180 days prior to expiration of the permit as required. This application is not requesting any modification to the current design of our NPDES storm water and wastewater system and includes the following: • Application Form —Short Form C • Attachment I —Topographical Map and Process Flow Diagram • Attachment II — Detailed Sampling Results August 2014 - August 2017 If you have any questions, please contact Kristine Pelt at (919) 616-5476 or kristine.pelt@motiva.com. Very UNyo , D. Scott Dilling Complex Manager Enclosures cc: Kristine Pelt (electronic) file 550-03 RECEIVEMCDEQ/M OCT 2 3 2017 Water Quality Permitting Section NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial Minor industrial, manufacturing and commercial facilities. Mail the complete application to: N. C. Department of Environment and Natural Resources Division of Water Quality / NPDES Unit 1617 Mail Service Center, Raleigh, NC 27699-1617 1. Contact Information: Owner Name Facility Name Mailing Address City State / Zip Code Telephone Number Fax Number e-mail Address NPDES Permit Number INCO022217 Please print or type. Motiva Enterprises LLC Motiva Enterprises LLC - Raleigh Terminal 2232 Ten Ten Road Apex NC 27539-8115 (919) 362-8341 Kristine. Pelt@Motiva. Com 2. Location of facility producing discharge: Check here if same as above Street Address or State Road City State / Zip Code County Wake 3. Operator Information: Name of the firm, consultant or other entity that operates the facility (Note that this is not referring to the Operator in Responsible Charge or ORC) Name Motiva Enterprises LLC Mailing Address City State / Zip Code Telephone Number Fax Number 2232 Ten Ten Road Apex NC 27539-8115 (919) 362-8341 Page 1 of 4 C -MI 10/08 NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial Minor industrial, manufacturing and commercial facilities. 4. Ownership Status: Federal ❑ State ❑ Private S. Standard Industrial Classification (SIC) code(s): 5171 6. Number of employees_ Public ❑ 7. Describe the treatment system List all installed waste treatment components with capacities, describe the processes that generate wastewaters If the space proinded is not sufficient attach a separate sheet of paper with the system description An oil -water separator (OWS) receives water from the truck loading rack. Water from the OWS is routed to a 10,000 -gallon tank in the tank dike area. The tank is equipped with a hydrocarbon sensor and level control. A figure is included in Attachment I. 8. Is facility covered under federal effluent limitation guidelines? No ® Yes ❑ If yes, specify the category? 9. Principal product(s) produced: No products are produced. The facility is a bulk terminal for gasoline, petroleum distillates and ethanol. Principal raw material(s) consumed: No raw materials are consumed. The facility is a bulk terminal for gasoline, petroleum distillates and ethanol. Briefly describe the manufacturing process(es): The facility is a bulk distribution terminal for gasoline, petroleum distillates and ethanol. It does not produce, manufacture or consume products or raw materials. Gasoline and distillates are received via pipeline which are then stored in above ground tanks. Ethanol is received via tank truck. All products are loaded out via tanker truck through the terminal's loading rack. 10. Amount of principal product produced or raw material consumed /List specific amounts consumed and/or units of production over the last three /ears) 11. Frequency of discharge: Continuous ❑ Intermittent If intermittent: Days per week discharge occurs: 7* Duration: 24* * Discharge is intermittent and is determined by local rainfall amounts Page 2 of 4 C -MI 10108 Product Produced or Raw Material Consumed (AVERAGE) Product Produced or Raw Material Consumed (PEAK) per Day 500,000 gallons product distributed 607,500 gallons product distributed per Month 15,000,000 gallons product distributed 18,220,000 gallons product distributed per Year 183,000,000 gallons product distributed 194,200,000 gallons product distributed 11. Frequency of discharge: Continuous ❑ Intermittent If intermittent: Days per week discharge occurs: 7* Duration: 24* * Discharge is intermittent and is determined by local rainfall amounts Page 2 of 4 C -MI 10108 NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial Minor industrial, manufacturing and commercial facilities. 12. Types of wastewater discharged to surface waters only Discharge Flow GALLONS PER DAY) Sanitary - monthly average Not Applicable Utility water, etc - monthly average Not Applicable Process water - monthly average Not Applicable Stormwater - monthly average 181,000 (dependent upon rainfall; last 3 -year average) Other - monthly average mg/l Explain- Not Applicable Monthly Average 181,000 total discharge (all types) Fecal Coliform (If sanitary waste is present) 13. Number of separate discharge points: 1 Outfall Identification number(s) 001 14. Name of receiving stream(s) (Provide a map showing the exact location of each outfall, including latitude and longitude): Unnamed tributary to Middle Creek within the Neuse River Basin. Latitude 35 42'57"N, Longitude 78 48'56"W Refer to Attachment I 15. Effluent Data [for new or proposed discharges] Provide data for the parameters listed Temperature and pH shall be grab samples, for all other parameters 24-hour composite sampling shall be used If more than one analysis is reported, report daily maxzmum and monthly average If only one analysis is reported, report as daily maximum NOTE: Permittees requesting renewal should complete the table ONLY for the parameters currently monitored. Summarize the past 3 years of effluent data. Parameter Daily Maximum Monthly Average Units of Measurement Biochemical Oxygen Demand (BOD5) Not required to be monitored under current permit. See Attachment II for last 3 years of monitoring data. Chemical Oxygen Demand (COD) Total Organic Carbon Total Suspended Solids 27.4 8.2 mg/l Ammonia as N Not required to be monitored under current permit See Attachment II for last 3 years of monitoring data. Temperature (Summer) Temperature (Winter) pH Fecal Coliform (If sanitary waste is present) Total Residual Chlorine (if chlorine is used) Page 3 of 4 C -MI 10108 NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial Minor industrial, manufacturing and commercial facilities. 16. List all permits, construction approvals and/or applications (check all that apply and provide permit numbers or check none if not applicable): Type Permit Number Type Permit Number Hazardous Waste (RCRA) UIC (SDWA) NPDES PSD (CAA) 1►�! WI0500057 NCO022217 None Non -attainment program (CAA) None NESHAPS (CAA) None Ocean Dumping (MPRSA) None Dredge or fill (Section 404 or CWA) None Other - Air Quality Permit 0451ORIS 17. List any chemicals that may be discharged (Please list and explain source and potential amounts ) None in addition to the compounds being sampled and analyzed. 18. Is this facility located on Indian country? (check one) Yes ❑ No 19. Applicant Certification I certify that I am familiar with the information contained in the application and that to the best of my knowledge and belief such information is true, complete, and accurate. L' 60r1rL_" M'0 _M 6.['1L__ Printed name of Person Signing Title of Applicant / 0 /-Z-5/ 2.z� { 7 Date North Carolina General Statute 1143---21&6�b)(2) provides that Any person who knowingly makes any false statement representation, or certification in any application, record, report, plan, or other document files or required to be maintained under Article 21 or regulations of the Environmental Management Commission implementing that Article, or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under Article 21 or regulations of the Environmental Management Commission implementing that Article, shall be guilty of a misdemeanor punishable by a fine not to exceed $25,000, or by imprisonment not to exceed six months, or by both (18 U S C Section 1001 provides a punishment by a fine of not more than $25,000 or imprisonment not more than 5 years, or both, for a similar offense) Page 4 of 4 C -MI 10/08 Attachment I Figures Topographical Map Oil Water Separator Process Flow Diagram G 0 0.2 04 06 06 1 M WLFL-TV (Raleigh), USGS Apex (NC) Quadrangle Projection is UTM Zone 17 NAD83 Datum M 8.715 G=1.276 Motiva Enterprises Raleigh Terminal Outfall 001 Loading Rack Stormwater Motiva Enterprises LLC Apex Terminal NPDES Permit NCO022217 Recovered Product Sent Offsite SPCC Tank 1 10,000 gal Water , Tank Containment Pond Outfall 001 Unnamed Tributary to Middle Creek Tank Farm Stormwater (Diked Area) Attachment II Detailed Sampling Results August 2014 - August 2017 Detailed Sampling Results August 2014 - August 2017 Motiva Enterprises, LLC Apex, NC Permit No. NC0022217 Month Day Year Parameter Value Units 8 11 2017 00070 - Turbidity 5.2 ntu 6 22 2017 00070 - Turbidity 6.4 ntu 5 30 2017 00070 - Turbidity 6 ntu 4 3 2017 00070 - Turbidity 4.5 ntu 1 10 2017 00070 - Turbidity 2.7 ntu 10 12 2016 00070 - Turbidity 4.8 ntu 9 28 2016 00070 - Turbidity 5.6 ntu 8 23 2016 00070 - Turbidity 5.4 ntu 7 6 2016 00070 - Turbidity 1.31 ntu 5 2 2016 00070 - Turbidity 4.4 ntu 2 9 2016 00070 - Turbidity 7.8 ntu 1 6 2016 00070 - Turbidity 4.2 ntu 11 4 2015 00070 - Turbidity 6.7 ntu 10 5 2015 00070 - Turbidity 8.4 ntu 8 12 2015 00070 - Turbidity 7.4 ntu 7 17 2015 00070 - Turbidity 17 ntu 6 29 2015 00070 - Turbidity 6.6 ntu 4 6 2015 00070 - Turbidity 11 ntu 3 13 2015 00070 - Turbidity 15 ntu 1 6 2015 00070 - Turbidity 9.9 ntu 12 4 2014 00070 - Turbidity 7.1 ntu 10 21 2014 00070 - Turbidity 7.8 ntu 9 15 2014 00070 - Turbidity 5 ntu 8 17 2014 00070 - Turbidity 8.2 8 11 2017 00556 - Oil & Grease <5 f 6 22 2017 00556 - Oil & Grease <5 5 30 2017 00556 - Oil & Grease <5 m /1 4 3 2017 00556 - Oil & Grease <5 m /I 1 10 2017 00556 - Oil & Grease <5 m /I 10 12 2016 00556 - Oil & Grease <5 m /I 9 28 2016 00556 - Oil & Grease <5 m /1 8 23 2016 00556 - Oil & Grease <5 m /1 7 6 2016 00556 - Oil & Grease <5 m /I 5 2 2016 00556 - Oil & Grease 5.9 m /I 2 9 2016 00556 - Oil & Grease <5 m /I 1 6 2016 00556 - Oil & Grease <5 m /1 11 4 2015 00556 - Oil & Grease <5 m /I 10 5 2015 00556 - Oil & Grease <5 m /I 8 12 2015 00556 - Oil & Grease <5 m /I 7 17 2015 00556 - Oil & Grease <5 m /I 6 29 2015 00556 - Oil & Grease <5 4 6 2015 00556 - Oil & Grease 5.3 Er/111 3 13 2015 00556 - Oil & Grease <5 1 6 2015 00556 - Oil & Grease <5 m /I 12 4 2014 00556 - Oil & Grease <5 m /I 10 21 2014 00556 - Oil & Grease <5 m /l Page 1 of 6 Detailed Sampling Results August 2014 - August 2017 Motiva Enterprises, LLC Apex, NC Permit No. NC0022217 Month Day Year Parameter Value Units 9 15 2014 00556 - Oil & Grease <5 m /I 8 17 2014 00556 - Oil & Grease <5 m /I 8 11 2017 22417 - Methyl Tert-But I Ether MTBE <0.5 u /I 6 22 2017 22417 - Methyl Tert-But I Ether MTBE <0.5 u /1 5 30 2017 22417 - Methyl Tert-But I Ether MTBE <0.5 u /I 4 3 2017 22417 - Methyl Tert-But I Ether MTBE <2 u /I 1 10 2017 22417 - Methyl Tert-But I Ether MTBE <0.5 u /I 10 12 2016 22417 - Methyl Tert-But I Ether MTBE <0.5 u /I 7 6 2016 22417 - Methyl Tert-But I Ether MTBE <0.5 u /I 5 2 2016 22417 - Methyl Tert-But I Ether MTBE <0.5 u /I 2 9 2016 22417 - Methyl Tert-But I Ether MTBE <0.5 u /I 1 6 2016 22417 - Methyl Tert-But I Ether MTBE <0.5 u /I 11 4 2015 22417 - Methyl Tert-But I Ether MTBE <2 u /I 10 5 2015 22417 - Methyl Tert-But I Ether MTBE <0.5 u /I 8 12 2015 22417 - Methyl Tert-But 1 Ether MTBE <2 u /I 7 17 2015 22417 - Methyl Tert-But I Ether MTBE <2 UO 6 29 2015 22417 - Methyl Tert-But I Ether MTBE <2 u /I 4 6 2015 22417 - Methyl Tert-But I Ether MTBE <2 u /I 1 6 2015 22417 - Methyl Tert-But I Ether MTBE <2 u /I 10 21 2014 22417 - Methyl Tert-But I Ether MTBE <2 u /1 8 11 2017 34010 - Toluene <0.25 u /I 6 22 2017 34010 - Toluene <0.25 u /I 5 30 2017 34010 - Toluene <0.25 u /I 4 3 2017 34010 - Toluene <1 Ug/1 1 10 2017 34010 - Toluene <0.25 u /I 10 12 2016 34010 - Toluene <0.25 u /1 9 28 2016 34010 - Toluene <0.25 u /1 8 23 2016 34010 - Toluene <0.25 u /I 7 6 2016 34010 - Toluene <0.25 u /I 5 2 2016 34010 - Toluene <0.25 u /I 2 9 2016 34010 - Toluene <0.25 u /I 1 6 2016 34010 - Toluene <0.25 u /I 11 4 2015 34010 - Toluene <1 u /l 10 5 2015 34010 - Toluene <0.25 u /I 8 12 2015 34010 - Toluene <1 u /I 7 17 2015 34010- Toluene <1 u /l 6 29 2015 34010 - Toluene <1 u /1 4 6 2015 34010 - Toluene <1 u /I 3 13 2015 34010 - Toluene <1 u /I 1 6 2015 34010 - Toluene <1 u /I 12 4 2014 34010 - Toluene <1 u /I 10 21 2014 34010 - Toluene <1 u /I 9 15 2014 34010 - Toluene <1 u /I 8 17 2014 34010 - Toluene <1 u /1 8 11 2017 134030- Benzene <0.125 u /I 6 22 2017 134030- Benzene <0.125 u /I Page 2 of 6 Detailed Sampling Results August 2014 - August 2017 Motiva Enterprises, LLC Apex, NC Permit No. NCO022217 Month Day Year Parameter Value Units 5 30 2017 34030- Benzene <0.125 u /I 4 3 2017 34030- Benzene <1 u /I 1 10 2017 34030- Benzene <0.125 u /I 10 12 2016 34030- Benzene <0.125 u /I 9 28 2016 34030- Benzene <0.125 u /1 8 23 2016 34030- Benzene <0.125 u /I 7 6 2016 34030- Benzene <0.125 u /I 5 2 2016 34030- Benzene <0.125 u /I 2 9 2016 34030- Benzene <0.125 u /1 1 6 2016 34030- Benzene <0.125 u /I 11 4 2015 34030- Benzene <1 u /I 10 5 2015 34030- Benzene <0.125 u /I 8 12 2015 34030- Benzene <1 u /1 7 17 2015 34030- Benzene <1 u /I 6 29 2015 34030 -Benzene <1 u /I 4 6 2015 34030 -Benzene <1 u /I 3 13 2015 34030- Benzene <1 u /I 1 6 2015 34030- Benzene <1 u /I 12 4 2014 34030- Benzene <1 u /I 10 21 2014 34030- Benzene <1 u /I 9 15 2014 34030- Benzene <1 u /I 8 17 2014 34030- Benzene <1 u /I 8 11 2017 34371 - Eth (benzene <0.25 u /I 6 22 2017 34371 - Eth (benzene <0.25 u /1 5 30 2017 34371 - Eth (benzene <0.25 u /I 4 3 2017 34371 - Eth (benzene <1 u /I 1 10 2017 34371 - Eth (benzene <0.25 u /I 10 12 2016 34371 - Eth (benzene <0.25 u /I 9 28 2016 34371 - Eth (benzene <0.25 u /1 8 23 2016 34371 - Eth (benzene <0.25 u /1 7 6 2016 34371 - Eth (benzene <0.25 u /I 5 2 2016 34371 - Eth (benzene <0.25 u /I 2 9 2016 34371 - Eth (benzene <0.25 u /I 1 6 2016 34371 - Eth (benzene <0.25 u /I 11 4 2015 34371 - Eth (benzene <1 u /I 10 5 2015 34371 - Eth (benzene <0.25 u /I 8 12 2015 34371 - Eth (benzene <1 u /I 7 17 2015 34371 - Eth (benzene <1 u /I 6 29 2015 34371 - Eth (benzene <1 u /I 4 6 2015 34371 - Eth (benzene <1 u /I 3 13 2015 34371 - Eth (benzene <1 u /I 1 6 2015 34371 - Eth (benzene <1 u /I 12 4 2014 34371 - Eth (benzene <1 u /I 10 21 2014 34371 - Eth (benzene <1 u /I 9 15 2014 34371 - Eth (benzene <1 u /I 8 17 1 2014 34371 - Eth (benzene <1 u /I Page 3 of 6 Detailed Sampling Results August 2014 - August 2017 Motiva Enterprises, LLC Apex, NC Permit No. NCO022217 Month Day Year Parameter Value Units 8 11 2017 34696 - Naphthalene <0.2 u /I 6 22 2017 34696 - Naphthalene <0.2 u /I 5 30 2017 34696 - Naphthalene <0.2 u /I 4 1 3 2017 34696 - Naphthalene <1 u /I 1 10 2017 34696 - Naphthalene <0.2 u /I 10 12 2016 34696 - Naphthalene <0.2 u /I 9 28 2016 34696 - Naphthalene <0.2 u /I 8 23 2016 34696 - Naphthalene <0.2 u /I 7 6 2016 34696 - Naphthalene <0.2 u /I 5 2 2016 34696 - Naphthalene <0.2 uqjl 2 9 2016 34696 - Naphthalene <0.2 u /I 1 6 2016 34696 - Naphthalene <0.2 UQ/1 11 4 2015 34696 - Naphthalene <1 u /I 10 5 2015 34696 - Naphthalene <0.2 u /1 8 12 2015 34696 - Naphthalene <1 u /I 7 17 2015 34696 - Naphthalene <1Mug 6 29 2015 34696 - Naphthalene <1 4 6 2015 34696 - Naphthalene <1 3 13 2015 34696 - Naphthalene <1 1 6 2015 34696 - Naphthalene <1 12 4 2014 34696 - Naphthalene <1 u /I 10 21 2014 34696 - Naphthalene <1 u /I 9 15 2014 34696 - Naphthalene <1 u /I 8 17 2014 34696 - Naphthalene <1 u /I 8 11 2017 50050 - Flow, in conduit or thru treatment plant 0.168 mad 6 19 2017 50050 - Flow, in conduit or thru treatment plant 0.126 m d 6 22 2017 50050 - Flow, in conduit or thru treatment plant 0.126 m d 5 26 2017 50050 - Flow, in conduit or thru treatment plant 0.21 m d 5 30 2017 50050 - Flow, in conduit or thru treatment plant 0.021 m d 4 3 2017 50050 -Flow, in conduit or thru treatment plant 0.189 mad 4 25 2017 50050 - Flow, in conduit or thru treatment plant 0.378 m d 4 26 2017 50050 - Flow, in conduit or thru treatment plant 0.147 m d 1 10 2017 50050 - Flow, in conduit or thru treatment plant 0.294 m d 1 31 2017 50050 - Flow, in conduit or thru treatment plant 0.126 m d 10 8 2016 50050 - Flow, in conduit or thru treatment plant 0.42 mad 10 9 2016 50050 - Flow, in conduit or thru treatment plant 0.189 m d 10 12 j 2016 50050 - Flow, in conduit or thru treatment plant 0.042 m d 9 20 2016 50050 - Flow, in conduit or thru treatment plant 0.21 m d 9 21 2016 50050 - Flow, in conduit or thru treatment plant 0.021 m d 9 28 2016 50050 - Flow, in conduit or thru treatment plant 0.168 m d 8 10 2016 50050: Flow, in conduit or thru treatment plant 0.126 m d 8 23 2016 50050 - Flow, in conduit or thru treatment plant 0.042 m d 7 6 2016 50050 - Flow, in conduit or thru treatment plant 0.252 mad 7 18 2016 50050 - Flow, in conduit or thru treatment plant 0.42 mad 5 2 2016 50050 - Flow, in conduit or thru treatment plant 0.294 m d 5 10 2016 50050 - Flow, in conduit or thru treatment plant 0.105 m d Page 4 of 6 Detailed Sampling Results August 2014 - August 2017 Motiva Enterprises, LLC Apex, NC Permit No. NCO022217 Month Day Year Parameter Value Units 5 11 2016 50050 - Flow, in conduit or thru treatment plant 0.0945 m d 5 31 2016 50050 - Flow, in conduit or thru treatment plant 0.21 m d 2 9 2016 50050 - Flow, in conduit or thru treatment plant 0.278 m d 2 29 2016 50050 - Flow, in conduit or thru treatment plant 0.084 m d 1 6 2016 50050 - Flow, in conduit or thru treatment plant 0.294 m d 11 2 2015 50050 - Flow, in conduit or thru treatment plant 0.126 m d 11 4 2015 50050 - Flow, in conduit or thru treatment plant 0.315 m d 11 20 2015 50050 - Flow, in conduit or thru treatment plant 0.336 m d 10 1 2015 50050 - Flow, in conduit or thru treatment plant 0.126 m d 10 5 2015 50050 - Flow, in conduit or thru treatment plant 0.105 m d 8 12 2015 50050 - Flow, in conduit or thru treatment plant 0.147 m d 8 24 2015 50050 - Flow, in conduit or thru treatment plant 0.042 mad 8 25 2015 50050 - Flow, in conduit or thru treatment plant 0.126 mad 7 15 2015 50050 - Flow, in conduit or thru treatment plant 0.126 m d 7 17 2015 50050 - Flow, in conduit or thru treatment plant 0.126 m d 6 26 2015 50050 - Flow, in conduit or thru treatment plant 0.42 m d 6 29 2015 50050 - Flow, in conduit or thru treatment plant 0.441 m d 4 6 2015 50050 - Flow, in conduit or thru treatment plant 0.126 m d 4 10 2015 50050 - Flow, in conduit or thru treatment plant 0.357 m d 3 9 2015 50050 - Flow, in conduit or thru treatment plant 0.147 m d 3 13 2015 50050 - Flow, in conduit or thru treatment plant 0.001 m d 3 17 2015 50050 - Flow, in conduit or thru treatment plant 0.063 m d 1 6 2015 50050 - Flow, in conduit or thru treatment plant 0.12 m d 1 20 2015 50050 - Flow, in conduit or thru treatment plant 0.21 m d 1 21 2015 50050 - Flow, in conduit or thru treatment plant 0.168 m d 12 4 2014 50050 - Flow, in conduit or thru treatment plant 0.126 m d 12 26 2014 50050 - Flow, in conduit or thru treatment plant 0.21 m d 10 21 2014 50050 - Flow, in conduit or thru treatment plant 0.105 m d 9 11 2014 50050 - Flow, in conduit or thru treatment plant 0.231 m d 9 15 2014 50050 - Flow, in conduit or thru treatment plant 0.105 m d 9 29 2014 50050 - Flow, in conduit or thru treatment plant 0.084 m d 8 17 2014 50050 - Flow, in conduit or thru treatment plant 0.042 m d 8 18 2014 50050 - Flow, in conduit or thru treatment plant 0.105 m d 8 26 2014 50050 - Flow, in conduit or thru treatment plant 0.105 m d 8 11 2017 81551 - Xylene mix of m+o+ <0.5 u /I 6 22 2017 81551 - Xylene mix of m+o+ <0.5 u /I 5 30 2017 81551 - Xylene mix of m+o+ <0.5 u /I 4 3 2017 81551 - Xylene mix of m+o+ <1 u /I 1 10 2017 81551 - Xylene mix of m+o+ <0.5 u /I 10 12 2016 81551 - Xylene mix of m+o+ <0.5 UQ/1 9 28 2016 81551 - Xylene mix of m+o+ <0.5 u /I 8 23 2016 81551 - Xylene mix of m+o+ <0.5 u /I 7 6 2016 81551 - Xylene mix of m+o+ <0.5 u /I 5 2 2016 81551 - Xylene mix of m+o+ <0.5 UQ/1 2 9 2016 81551 - Xylene mix of m+o+ <0.5 U /1 1 6 2016 81551 - Xylene mix of m+o+ <0.5 u /I Page 5 of 6 Detailed Sampling Results August 2014 - August 2017 Motiva Enterprises, LLC Apex, NC Permit No. NC0022217 Month Day Year Parameter Value Units 11 4 2015 81551 - Xylene mix of m+o+ <1 u /I 10 5 2015 81551 - Xylene mix of m+o+ <0.5 u /I 8 12 2015 81551 - Xylene mix of m+o+ <1 u /I 7 17 2015 81551 - Xylene mix of m+o+ <1.1 u /l 6 29 2015 81551 - Xylene mix of m+o+ <1 u /l 4 6 2015 81551 - Xylene mix of m+o+ <1 u /l 3 13 2015 81551 - Xylene mix of m+o+ <1 u /l 1 6 2015 81551 - Xylene mix of m+o+ <1 u /1 12 4 2014 81551 - Xylene mix of m+o+ <1 u /I 10 21 2014 81551 - Xylene mix of m+o+ <1 u /I 9 15 2014 81551 - Xylene mix of m+o+ <1 u /I 8 17 2014 81551 - Xylene mix of m+o+ <1 u /I 8 11 2017 CO530 - Solids, Total Suspended - Concentration 27.4 m /I 6 22 2017 CO530 - Solids, Total Suspended - Concentration 5.4 m /l 5 30 2017 CO530 - Solids, Total Suspended - Concentration 8.2 m /l 4 3 2017 CO530 - Solids, Total Suspended - Concentration 4.8 m /l 1 10 2017 CO530 - Solids, Total Suspended - Concentration 2 m /I 10 12 2016 CO530 - Solids, Total Suspended - Concentration 3.8 m /I 9 28 2016 CO530 - Solids, Total Suspended - Concentration 14.8 m /l 8 23 2016 CO530 - Solids, Total Suspended - Concentration 8.6 m /l 7 6 2016 CO530 - Solids, Total Suspended - Concentration 5.78 m /l 5 2 2016 CO530 - Solids, Total Suspended - Concentration 6.2 mg/1 2 9 2016 CO530 - Solids, Total Suspended - Concentration 5.67 m /l 1 6 2016 CO530 - Solids, Total Suspended - Concentration 3 m /I 11 4 2015 CO530 - Solids, Total Suspended - Concentration 4.75 m /l 10 5 2015 CO530 - Solids, Total Suspended - Concentration 4 m /l 8 12 2015 CO530 - Solids, Total Suspended - Concentration 9.6 m /I 7 17 2015 CO530 - Solids, Total Suspended - Concentration 11.7 m /I 6 29 2015 CO530 - Solids, Total Suspended - Concentration 7.3 mall 4 6 2015 CO530 - Solids, Total Suspended - Concentration 6 m /l 3 13 2015 CO530 - Solids, Total Suspended - Concentration 10 m /I 1 6 2015 CO530 - Solids, Total Suspended - Concentration 5.6 m /I 12 4 2014 CO530 - Solids, Total Suspended - Concentration 4 m /l 10 21 2014 CO530 - Solids, Total Suspended - Concentration 24 m /I 9 15 2014 CO530 - Solids, Total Suspended - Concentration 8 m /I 8 17 2014 CO530 - Solids, Total Suspended - Concentration 7.3 m /l 1 10 2017 TAE6C - LC50 Static 24hr Acute Pime hales >100% percent 2 9 2016 ITAE6C - LC50 Static 24hr Acute Pime hales >100% percent 4 6 2015 1 TAE6C - LC50 Static 24hr Acute Pime hales >100% percent Data is shown for all months with recorded flows sufficient for smapling. Page 6 of 6