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NC0038377_Waste load Allocation_19901015
NPDES WASTE LOAD ALLOCATION PERMIT NO.: NCO038377 PERMITTEE NAME. CP & L / Mayo Steam Electric Plant Facility Status: Existing Permit Status: Modification Major Minor Pipe No.: 002 Design Capacity: 20.0125 MGD Domestic (% of Flow): Industrial (% of Flow): 0.07 % 99.93 Comments: CP & L wants to reroute sewage from 003 to 002 (the ash pond). Sewage flow is 0.0125 MGD. RECEIVING STREAM: Mayo Creek Class: C Sub -Basin: 03-02-05 Reference USGS Quad: A 23 SW (please attach) County: Person Regional Office: Raleigh Regional Office Previous Exp. Date: 00/00/00 Treatment Plant Class: Class 2 Classification changes within three miles: none Requested by Rosanne Barona Date: 10/14/90 Prepared by: Date: 1 Reviewed by: Date: Boo,. uJQ Modeler Date Rec. # SCM W12*10 sgos Drainage Area (mil ) L&k%,lt_ Avg. Streamflow (cfs): 7Q10 (cfs) Winter 7Q10 (cfs) 30Q2 (cfs) Toxicity Limits: IWC Q Ok % Acute hronic Instream Monitoring: Parameters N A Upstream Location Downstream Location Effluent Characteristics BODS (mg/1) M (CA NB3-N(mg/1) M ( CA D.O. (mg/l) S TSS (mg/1) -30 F. Col. (/100 ml) -40c) pH (SU) 6- a I S^ You �i lroO'OI L eke%) P V0 iments: � V' W -� H IV "Aom 4 1 ce-J o c_o cvlt� c �; o w� G,-unuA-^ coo A F4:w Request No. �f-(; "5 ------------------- WASTELOAD ALLOCATION APPROVAL FORM ------------------- Facility Name: CP & L/ Mayo Steam Electric Plant NPDES No.: NC0038377 Type of Waste: 0.07 % Dom/99.93 % Ind Status: Existing/Mod Receiving Stream: Mayo Reservoir Classification: C Subbasin: 030205 Drainage County: Person Summer Regional Office: Raleigh Winter Requestor: Barona Average Date of Request: 101590 Quad: A 23 SW -------------------- RECOMMENDED EFFLUENT LIMITS --- EXISTING EXISTING 002 003 Wasteflow (mgd) : n/a 0.0125 area: 7Q10: LAKE 7Q10: flow: 30Q2: sq mi cfs cfs cfs cfs PROPOSED 002 (combined) 20.0125 a BODS (mg/1) : n/a 30 eon ___-n 30 NH3N (mg/1) : n/a n/a Mon n/a DO (mg/1) : n/a n/a (#/day) : 3.8 TSS (mg/1) : n/a 30 Fecal coliform (#/100ml): n/a 1000 pH (su) : 6-9 6-9 Oil & Grease (mg/1) : 15 n/a Toxicity Testing Req.: Copper (ug/1): 1000 Iron (ug/1) : 1000 Arsenic (ug/1): Mon Vanadium (ug/1) : Mon Selenium (#/day) : 3.8 Zinc (ug/1) : n/a Mercury (ug/1); n/a TRC (ug/1) : n/a ----------------------------- COMMENTS n/a n/a n/a n/a n/a n/a n/a n/a 500 (min) 213 U 00 6-9 15 Chr Crd 995 qrt 1000 1000 Mon Mon 3.8 Mon Mon 28 (max) This facility is combining outfalls 002 & 003 into 003. At no time shall the discharge from the reservoir to Mayo Creek exceed 0.01 mg/1 of Selenium The permit should contain the same conditions currently contained in the permit being modified. /,/�/1 , � �+ /J A/ /'yam/f ----------------------- 1 - - - - - - - - - - - - - - - - - - - L--------------------------- Prepared ------------Prepared by: Date: 1Z 10 l r o Juan C. Mangles i Reviewed by Instream Assessment: Date: Regional Supervisor: Date: la� T Permits & Engineering: Date: RETURN TO d� TECHNICAL SUPPORT BY: n0 �, n, TL J A N 18 1991 �l 10/89 Facility Nannie L t 0 0 3 Permit #�3 C 0U 3 0 r CHRONIC TOXICITY TESTING REQUIREMENT (QRTRLY) The effluent discharge shall at no time exhibit chronic toxicity in any two consecutive toxicity tests, using test procedures outlined in: 1.) The North Carolina Ceriodaphnia chronic effluent bioassay procedure (North Carolina Chronic Bioassay Procedure - Revised *September 1989) or subsequent versions. The effluent concentrati n at which there may be no observable inhibition of reproduction or significant mortality is % (defined as treatment two in the North Carolina procedure document). The permit holder shall perform quarte-rly quarte-rmonitoring using this procedure to establish compliance with the permit condition. The first gest w(W be performed fte thirty days from issuance of this permit during the months of Maty , JV -1 _Q C Effluent sampling for this testing shall be performed at the NPDES permitted final effluent discharge below all treatment processes. All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge Monitoring Form (MR -1) for the month in which it was performed, using the parameter code TGP3B. Additionally, DEM Form AT -1 (original) is to be sent to the following address: Attention: Environmental Sciences Branch North Carolina Division of Environmental Management P.O. Box 27687 Raleigh, N.C. 27611 Test data shall be complete and accurate and include all supporting clietnical/physical measurements performed in -association with the toxicity tests, as well as all dose/response data. Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for disinfection of the waste stream. Should any single quarterly monitoring indicate a failure to meet specified limits, then monthly monitoring will begin immediately until such time that a single test is passed. Upon passing, this monthly test requirement will revert to quarterly in the months specified above. Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Environmental Management indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include alternate monitoring requirements or limits. NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism survival and appropriate environmental controls, shall constitute an invalid test and will require immediate retesting(within 30 days of initial monitoring event). Failure to submit suitable test results will constitute noncompliance with monitoring requirements. 7Q10 0'0 cfs Permited Flo RD •01ZJ MGD Recommended by: IWC% l Basin & Sub -basin Receiving tream k v et- CountyQ-..-. Date **Chronic Toxicity (Ceriodaphnia) P/Fat%, ,See Part , Condition — ��< MEMO. TO -ma , � DATE tl" ( 9 0 SUBJECT: C P � q A � 3-, %� 0" uki � c Irl d c STATE n " North Carolina Department of Natural Resources &Community Development JCM 11-4-90 CP & L Electric Steam Station Mayo Reservoir - This is a modification of an expired permit. Tech. Support did a WLA in 11-87. The NPDES permit was never issued because EPA objected to the permit. Permits & Engineering is still waiting for additional calculations from CP & L to reactivate the NPDES permit reneal. In addition, P & E is waiting on the results of a court decision on a similar facility and NPDES permit objected by EPA in Ohio. - This modification is to combine the domestic discharge (003) with the ash pond discharge (002). - I will assign existing limits of 002 and 003 to the combined outfall. However, P & E has established that a flow limitation of 20.0125 MGD should be contained in the combined outfall 003. In addition fecal coliform limitation is revised to current WQ standard, and a TRC limitation of 28 ug/l is required, since I am treating this outfall 003 as a combination of effluent combination and expansion. Data from the domestic WWTP shows superchlorination of the effluent. However, a mass balance is not appropriate to calculate the instream concentration of TRC because the discharge is into a lake. There is no - PPA in file. However, I was able to locate an old PPA (1983) through searching the P & E files. The PPA indicates levels of Hg and Zn above the WQ standard and action level specifically. Therefeore, I will require monitoring of these two parameters. - It is not possible to evaluate ammonia toxicity since the discharge is into a lake. - I will assign a whole effluent toxicity requirement in this modification. The toxicity requirement reflects the recommenmdation contained in the 11-87 WLA. R G. a,9 i SlT p .. n 1 ml 1 km i i i LOCATION MAP CAROLINA POWER & LIGHT COMPANY MAYO ELECTRIC GENERATING PLANT PERSON COUNTY, N. C. i DIVISION OF ENVIRONMENTAL MANAGEMENT December 4, 1990 MEMORANDUM TO: File FROM: Juan C. Mangles SUBJECT: CP & L Mayo Steam Electric Plant WLA NPDES Permit No. NC0038377 Person County A WLA was prepared for renewal of the subject NPDES Permit on September 10, 1987; however, a permit has not yet been issued because EPA objected to the permit limitations and requirements. Therefore, the subject facility has been operating without a valid permit since 1988. Conversations with Dale Overcash of Permits & Engineering indicated that his office is still waiting for additional information from CP & L in order to reacti- vate the permitting process. Also, Dale informed me that DEM is waiting for a court ruling involving a similar steam electric plant in Ohio. EPA objected to the NPDES permit issued to a similar steam electric plant by the State of Ohio. The objections are based on the same concerns EPA had regarding the CP & L NPDES permit. The Ohio facility contested EPA requirements and a decision is expected in a future date. Therefore, this WLA is for a permit modification of the expired NPDES permit for the subject facility. The NPDES permit will be renewed when all the necessary information is received by Permits & Engineering, and a court ruling is made on the Ohio's steam electric facility. k- Sheet No. _ of . � "•"'...�a.ri�^� SECTION, ENVIRONMENTAL TECHNOLOGY APPLICATION. SPECIAL ANALYSIS REMARKS. Q Z Q S 3 5` 9 8 qyo 83-5300 Sample flm Ellectlr, Data 6/16/77 Revision Deb. 8/9/82 Sample No. o,u R«,wod ,� �.� /' L3 oats s,mpl,d ,,,_ „ 19 93 l anWlatlon ro&I S�lf�dL Y - AX Surefufa /� Tlfa/ �e r.�L /V,ef � n 5 col�n,��;,, �tla! CeI,EoR.n, Bob slay T1" p,��q,�.c c'V,e�N Tovi, S,�v.deti sol.ds 4 Co/of chlacoplat1- IaUlf- rtnlTS /11><ICa+�- Nifty% to/r plosp�.�ea�s Q.I awd �RehSL U 83 SaM S -As 845 jA4, _ c,Lgkc Z .0 -41,0 4l1 410.05 "0.05 < 0.0.5 0-1�;L 0,41 A 3c L 5 4,9 <5 .0/ 3,0 5.7 #13 ao 17 io © 120 10,03 &IN 0.03 19,vim 0,03 D. All .4.1'o < .0 Date Analyzed g_ -fly 9-26-83 9.1143 g-;2583 8-30-83 -/6-83 -a5-83 _ 643 9-/9-13 q-7-83 -) -93 Reference y2 8re J7.2 t8 13M-54RL ISH .W la%'9C-C JJ-�.K 3 -�ILR /3 -sI RL 15 7!� w 15/C s0r7ILJ ///��� Analysis Requ,eted By: Ua c k4 eq, 0f !/, ant $drJ Chap. Na Analysis P,rformed BY: -CB k L SWC .L R /•n VJ pn,lYAS Rwlewed BY: Thl RL. 04J ! a la �-� noportln7 Data L-11 Z_;6 Supervisor-An,lylle WLaboralory v�3 1 { Dab Data Sampo Recelvrd SamPld NO Identification _L 19X3 X 7074 -// /(/ N, Ivn a A &3 v75 -/ 1 // CvoGn e as c Ii 83 706 /- r 1/ sc 4r. SECTION APPLICATION1 REMARKS __ ENVIRONMENTAL SPECIAL �/ TECHNOLOGY ANALYSISAYO 4 Ellaethe Dela. Rwblon Dab;6/19177 019/82 r� p _ J (� rot'L/ AprAoKlo. IW -WrItedy RaXkc vi/ �(1C/y11 C0./ 7'7 r 1 / / NQtN d�.. PiAca IO Q.. 1V,'4tA�C.. Sitif,p I q �X- m�x rC tlt� loco �B yI mJ ANJd /� �� f- N dledc Z2. 0 /�. L . S 4 . SFS <o tea• D -- o.0 -D O1 /-a. 0 9.03 4f. 79 <6. �• 41 0 46-0/ O, d Z tea. 0 0.03 D /Z0.3 --o' y,aY•,•lw(, rp �Ol/ ScL�4e- , 9 EE Sampl. Cloy I 1 1 Date Analyzed lo83 10L818 Reference (13- 6 DB 119//f,:? 717Gd 19.6 6 /acm o 1121,42.[MAA Ix4 (.MR Analysb Requested By: Charge No. RA,Q*gA I i IWIMAI-10/y -I Anslyslo Perfa and By: M p p ),n 1� Analysis Reviewed By L / Superq.nr•Analytical aDoratory RuDortln) Dab EXHIBIT II - COMPOUND LIST SAMPLE IDENTIFIER: Lake COMPUCHEM SAMPLE NUMBER: 15033 INORGANICS PRIORITY POLLUTANTS 1. CYANIDE, TOTAL 2. PHENOLS, TOTAL BDL=BELOW DETECTION LIMIi CONCENTRATION (MG/L) DETECTION LIMIT (MG/L) 0.01 0.01 EXHIBIT II - COMPOUND LIST SAMPLE IDENTIFIER: Ash Pond COMPUCHEM SAMPLE NUMBER: 15034 INORGANICS PRIORITY POLLUTANTS 1. CYANIDE, TOTAL 2. PHENOLS, TOTAL BDL=BELOW DETECTION LIM-li CONCENTRATION (MG/L) mm 0 © rN. DETECTION LIMIT (MG/L) BDL 0.01 BDL 0.01 EXHIBIT II - COMPOUND LIST BDL=BELOW DETECTION LIMIT A4* SAMPLE IDENTIFIER: 83-5299 Discharge COMPUCHEM SAMPLE NUMBER: 11378 DETECTION VOLATILE ORGANICS CONCENTRATION LIMIT SCAN (UG/L) (UG/L) NUMBER 1V. ACROLEIN BDL 100 2V. ACRYLONITRILE BDL 100 3V. BENZENE BDL 10 4V. BIS (CHLOROMETHYL) ETHER BDL 10 5V. BROMOFORM BDL 10 6V. CARBON TETRACHLORIDE BDL 10 7V. CHLOROBENZENE• BDL 10 8V. CHLORODIBROMOMETHANE BDL 10 9V. CHLOROETHANE BDL 10 1OV. 2-CHLOROETHYLVINYL ETHER BDL 10 11V. CHLOROFORM BDL 10 12V. DICHLOROBROMOMETHANE BDL 10 13V. DICHLORODIFLUOROMETHANE BDL 10 14V. 1,1-DICHLOROETHANE BDL 10 15V. 1,2-DICHLOROETHANE BDL 10 16V. 1,1-DICHLOROETHYLENE BDL 10 17V. 1,2-DICHLOROPROPANE BDL 10 18V. CIS-1,3-DICHLOROPROPENE BDL 10 19V. TRANS-I,3-DICHLOROPROPENE BDL 10 20V. ETHYLBENZENE BDL 10 21V. BROMOMETHANE BDL 10 22V. CHLOROMETHANE BDL 10 23V. METHYLENE CHLORIDE BDL 10 24V. 1,1,2,2 -TETRACHLOROETHANE BDL 10 25V. TETRACHLOROETHYLENE BDL 10 26V. TOLUENE BDL 10 27V. 1,2-TRANS-DICHLOROETHYLENE BDL 10 28V. 1,1,3 -TRICHLOROETHANE BDL 10 29". ' 1,'-TRTrHLO OETHANE BDL 10 30V i RICHL')KOETH'!'-ENE-- BDL 10 31V. TRICHLOROFLUOROMETHANE BDL 10 32V. VINYL CHLORIDE BDL 10 BDL=BELOW DETECTION LIMIT A4* EXHIBIT II - COMPOUND LIST SAMPLE IDENTIFIER: 83-5299 Discharge COMPUCHEM SAMPLE NUMBER: 11378 BDL= BELOW DETECTION LIMIT DETECTION ACID EXTRACTABLE ORGANICS CONCENTRATION LIMIT SCAN (UG/L) (UG/L) NUMBER 1A. 2 -CHLOROPHENOL BDL 25 2A. 2,4-DICHLOROPHENOL BDL 25 3A. 2,4 -DIMETHYLPHENOL BDL 25 4A. 4,6-DINITRO-O-CRESOL BDL 250 5A. 2,4-DINITROPHENOL BDL 250 6A. 2-NITROPHENOL BDL 25 7A. 4-NITROPHENOL BDL 25 8A. P -CHLORO -M -CRESOL BDL 25 9A. PENTACHLOROPHENOL BDL 25 10A. PHENOL BDL 25 11A. 2,4,6 -TRICHLOROPHENOL -" BDL 25 BDL= BELOW DETECTION LIMIT EXHIBIT II - COMPOUND LIST BDL=BELOW DETECTION LIMIT fR i SAMPLE IDENTIFIER: 83-5299 Discharge COMPUCHEM SAMPLE NUMBER: 11378 DETECTION BASE -NEUTRAL CONCENTRATION LIMIT SCAN EXTRACTABLE ORGANICS (UG/L) (UG/L) NUMBER 1B. ACENAPHTHENE BDL 10 2B. ACENAPHTHYLENE BDL 10 3B. ANTHRACENE BDL 10 4B. BENZIDINE BDL 10 5B. BENZO (A) ANTHRACENE BDL 10 6B. BENZO (A) PYRENE BDL 10 7B. 3,4-BENZOFLUORANTHENE BDL 10 8B. BENZO (GHI) PERYLENE BBL 25 9B. BENZO (K) FLUORANTHENE BDL 10 10B. BIS (2-CHLOROETHOXY) METHANE BDL 10 11B. BIS (2-CHLOROETHYL) ETHER BDL 10 12B. BIS (2-CHLOROISOPROPYL) ETHER BDL 10 13B. BIS (2-ETHYLHEXYL) PHTHALATE BDL 10 14B. a-BROMOPHENYL PHENYL ETHER BDL 10 15B. BUTYL BENZYL PHTHALATE BDL 10 16B. 2-CHLORONAPHTHALENE BDL 10 17B. 4-CHLOROPHENYL PHENYL ETHER BDL 10 18B. CHRYSENE BDL 10 19B. DIBENZO (A,H) ANTHRACENE BDL 25 20B. 1,2 -DICHLOROBENZENE BDL 10 21B. 1,3 -DICHLOROBENZENE BDL 10 22B. 1,4 -DICHLOROBENZENE BDL 10 23B. 3,3'-DICHLOROBENZIDINE BDL 10 24B. DIETHYL PHTHALATE BDL 10 25B. DIMETHYL PHTHALATE BDL 10 26B. DI -N -BUTYL PHTHALATE BDL 10 27". ',4-DidTTnOTO�.UENE BDL 10 28B. 2,6-DI,JITROTCLUENE BDL 10 29B. DI-N-OCTYL PHTHALATE BDL 10 BDL=BELOW DETECTION LIMIT fR i EXHIBIT II - COMPOUND LIST BDL= BELOW DETECTION LIMIT SAMPLE IDENTIFIER: 83-5299 Discharge COMPUCHEM SAMPLE NUMBER: 11378 BASE -NEUTRAL DETECTION EXTRACTABLE ORGANICS (continued) CONCENTRATION LIMIT SCAN (UG/L) (UG/L) NUMBER 30B. 1,2-DIPHENYLHYDRAZINE BDL 10 31B. FLUORANTHENE BDL 10 32B. FLUORENE BDL 10 33B. HEXACHLOROBENZENE BDL 10 34B. HEXACHLOROBUTADIENE BDL 10 35B. HEXACHLOROCYCLOPENTADIENE BDL 10 36B. HEXACHLOROETHANE BDL 10 37B. INDENO (1,2,3 -CD) PYRENE BDL 25 38B. ISOPHORONE BDL 10 39B. NAPHTHALENE BDL 10 40B. NITROBENZENE BDL 10 41B. N-NITROSODIMETHYLAMINE BDL 10 42B. N-NITROSODI-N-PROPYLAMINE BDL 10 43B. N-NITROSODIPHENYLAMINE BDL 10 44B. PHENANTHRENE BDL 10 45B. PYRENE BDL 10 46B. 1,2,4-TRICHLOROBENZENE BDL 10 BDL= BELOW DETECTION LIMIT EXHIBIT II - COMPOUND LIST SAMPLE IDENTIFIER: 83-5299 Discharge COMPUCHEM SAMPLE NUMBER: 11378 DETECTION PESTICIDES/PCB'S CONCENTRATION LIMIT (UG/L) (UG/L) 1P. ALDRIN BDL 10 2P. ALPHA -BHC BDL 10 3P. BETA -BHC BDL 10 4P. GAMMA -BHC BDL 10 5P. DELTA -BHC BDL 10 6P. CHLORDANE BDL 10 7P. 4,4' -DDT BDL 10 8P. 4,4' -DDE BDL 10 9P. 4,4' -DDD BDL 10 10P. DIELDRIN BDL 10 11P. ALPHA-ENDOSULFAN BDL 10 12P. BETA-ENDOSULFAN BDL 10 13P. ENDOSULFAN SULFATE BDL 10 14P. ENDRIN BDL 10 15P. ENDRIN ALDEHYDE BDL 10 16P. HEPTACHLOR BDL 10 17P. HEPTACHLOR EPDXIDE BDL 10 18P. PCB -1242 BDL 10 19P. PCB -1254 BDL 10 20P. PCB -1221 BDL 10 21P. PCB -1232 BDL 10 22P. PCB -1248 BDL 10 23P. PCB -1260 BDL 10 24P. PCB -1016 BDL 10 25P. TOXAPHENE BDL 10 BDL=BELOW DETECTION LIMIT -ts EXHIBIT II - COMPOUND LIST SAMPLE IDENTIFIER: 83-5299 Discharge COMPUCHEM SAMPLE NUMBER: 11378 INORGANICS CONCENTRATION DETECTION LIMIT* PRIORITY POLLUTANTS (MG/L) (MG/L) 1. ANTIMONY, TOTAL 2. ARSENIC, TOTAL 3. BERYLLIUM, TOTAL 4. CADMIUM, TOTAL 5. CHROMIUM, TOTAL 6. COPPER, TOTAL 7. LEAD, TOTAL 8. MERCURY, TOTAL 9. NICKEL, TOTAL 10. SELENIUM, TOTAL 11. SILVER, TOTAL 12. THALLIUM, TOTAL 13. ZINC, TOTAL INORGANICS/ CONVENTIONALS (None Requested) BDL=BELOW DETECTION LIMIT m 0.20✓ 0.05 0.09 0.05 BDL 0.02 0.02 0.02 BDL 0.1 BDL 0.1 BDL 0.2 0.0005 't 0.0002 0.10 11, 0.1 BDL 0.05 BDL 0.06 BDL 0.05 BDL 0.02 EXHIBIT II - COMPOUND LIST SAMPLE IDENTIFIER: 83-528 Intake COMPUCHEM SAMPLE NUMBER: 11376 VOLATILE ORGANICS DETECTION CONCENTRATION LIMIT (UG/L) (UG/L) 1V. ACROLEIN BDL 100 2V. ACRYLONITRILE BDL 100 3V. BENZENE BDL 10 4V. BIS (CHLOROMETHYL) ETHER BDL 10 5V. BROMOFORM BDL 10 6V. CARBON TETRACHLORIDE BDL 10 7V. CHLOROBENZENE BDL 10 8V. CHLORODIBROMOMETHANE BDL 10 9V. CHLOROETHANE BDL 10 1OV. 2-CHLOROETHYLVINYL ETHER BDL 10 11V. CHLOROFORM - BDL 10 12V. DICHLOROBROMOMETHANE BDL 10 13V. DICHLORODIFLUOROMETHANE BDL 10 14V. 1,1-DICHLOROETHANE BDL 10 15V. 1,2-DICHLOROETHANE BDL 10 16V. 1,1-DICHLOROETHYLENE BDL 10 17V. 1,2-DICHLOROPROPANE BDL 10 18V. CIS-1,3-DICHLOROPROPENE BDL 10 19V. TRANS-I,3-DICHLOROPROPENE BDL 10 20V. ETHYLBENZENE BDL 10 21V. BROMOMETHANE BDL 10 22V. CHLOROMETHANE BDL 10 23V. METHYLENE CHLORIDE BDL 10 24V. 1,1,2,2 -TETRACHLOROETHANE BDL 10 25V. TETRACHLOROETHYLENE BDL 10 26V. TOLUENE BDL 10 27V. 1,2-TRANS-DICHLOROETHYLENE BDL 10 28V. 1,1,1 -TRICHLOROETHANE BDL 10 2n� , 1,1>21 --TR T CHL O OETHANE BDL 10 30V tRICHLJROETH`.'LENE BDL 10 31V. TRICHLOROFLUOROMETHANE BDL 10 32V. VINYL CHLORIDE BDL 10 BDL=BELOW DETECTION LIMIT SCAN NUMBER "40 EXHIBIT II - COMPOUND LIST SAMPLE IDENTIFIER: COMPUCHEM SAMPLE NUMBER: BASE -NEUTRAL EXTRACTABLE ORGANICS 83-528 Intake 11376 DETECTION CONCENTRATION LIMIT SCAN (UG/L) (UG/L) NUMBER 1B. ACENAPHTHENE BDL 10 2B. ACENAPHTHYLENE BDL 10 3B. ANTHRACENE BDL 10 4B. BENZIDINE BDL 10 5B. BENZO (A) ANTHRACENE BDL 10 6B. BENZO (A) PYRENE BDL 10 7B. 3,4-BENZOFLUORANTHENE BDL 10 8B. BENZO (GHI) PERYLENE BBL 25 9B. BENZO (K) FLUORANTHENE BDL 10 10B. BIS (2-CHLOROETHOXY) METHANE BDL 10 11B. BIS (2-CHLOROETHYL) ETHER BDL 10 12B. BIS (2-CHLOROISOPROPYL) ETHER BDL 10 13B. BIS (2-ETHYLHEXYL) PHTHALATE BDL 10 14B. 4-BROMOPHENYL PHENYL ETHER BDL 10 15B. BUTYL BENZYL PHTHALATE BDL 10 16B. 2-CHLORONAPHTHALENE BDL 10 17B. 4-CHLOROPHENYL PHENYL ETHER BDL 10 18B. CHRYSENE BDL 10 19B. DIBENZO (A,H) ANTHRACENE BDL 25 20B. 1,2 -DICHLOROBENZENE BDL 10 21B. 1,3 -DICHLOROBENZENE BDL 10 22B. 1,4 -DICHLOROBENZENE BDL 10 23B. 3,3'-DICHLOROBENZIDINE BDL 10 24B. DIETHYL PHTHALATE BDL 10 25B. DIMETHYL PHTHALATE BDL 10 26B. DI -N -BUTYL PHTHALATE BDL 10 27D , n ,4--_,L1TTunT0L "ENE BDL 10 28B. z,6-DIM"iROTC:.UENE BDL 10 29B. DI-N-OCTYL PHTHALATE BDL 10 BDL=BELOW DETECTION LIMIT Rm EXHIBIT II - COMPOUND LIST SAMPLE IDENTIFIER: 83-528 Intake COMPUCHEM SAMPLE NUMBER: 11376 ACID EXTRACTABLE ORGANICS DETECTION CONCENTRATION LIMIT SCAN (UG/L) (UG/L) NUMBER 1A. 2 -CHLOROPHENOL BDL 25 2A. 2,4-DICHLOROPHENOL BDL 25 3A. 2,4 -DIMETHYLPHENOL BDL 25 4A. 4,6-DINITRO-O-CRESOL BDL 250 5A. 2,4-DINITROPHENOL BDL 250 6A. 2-NITROPHENOL BDL 25 7A. 4-NITROPHENOL BDL 25 8A. P -CHLORO -M -CRESOL BDL 25 9A. PENTACHLOROP14ENOL BDL 25 10A. PHENOL BDL 25 11A. 2,4,6 -TRICHLOROPHENOL BDL 25 BDL= BELOW DETECTION LIMIT 0x EXHIBIT II - COMPOUND LIST SAMPLE IDENTIFIER: 83-528 Intake COMPUCHEM SAMPLE NUMBER: 11376 BASE -NEUTRAL DETECTION EXTRACTABLE ORGANICS (continued) CONCENTRATION LIMIT (UG/L) (UG/L) 30B. 1,2-DIPHENYLHYDRAZINE BDL 10 31B. FLUORANTHENE BDL 10 32B. FLUORENE BDL 10 33B. HEXACHLOROBENZENE BDL 10 34B. HEXACHLOROBUTADIENE BDL 10 35B. HEXACHLOROCYCLOPENTADIENE BDL 10 36B. HEXACHLOROETHANE BDL 10 37B. INDENO (1,2,3 -CD) PYRENE BDL 25 38B. ISOPHORONE BDL 10 39B. NAPHTHALENE BDL 10 40B. NITROBENZENE BDL 10 41B. N-NITROSODIMETHYLAMINE BDL 10 42B. N-NITROSODI-N-PROPYLAMINE BDL 10 43B. N-NITROSODIPHENYLAMINE BDL 10 44B. PHENANTHRENE BDL 10 45B. PYRENE BDL 10 46B. 1,2,4-TRICHLOROBENZENE BDL 10 BDL= BELOW DETECTION LIMIT Rm SCAN NUMBER PESTICIDES/PCB'S EXHIBIT II - COMPOUND LIST SAMPLE IDENTIFIER: 83-528 Intake COMPUCHEM SAMPLE NUMBER: 11376 CONCENTRATION (UG/L) DETECTION LIMIT (UG/L) 1P. ALDRIN BDL 10 2P. ALPHA -BHC BDL 10 3P. BETA -BHC BDL 10 4P. GAMMA -BHC BDL 10 5P. DELTA -BHC BDL 10 6P. CHLORDANE BDL 10 7P. 4,4' -DDT BDL 10 8P. 4,4' -DDE BDL 10 9P. 4,4' -DDD BDL 10 IOP. DIELDRIN BDL 10 11P. ALPHA-ENDOSULFAN BDL 10 12P. BETA-ENDOSULFAN BDL 10 13P. ENDOSULFAN SULFATE BDL 10 14P. ENDRIN BDL 10 15P. ENDRIN ALDEHYDE BDL 10 16P. HEPTACHLOR BDL 10 17P. HEPTACHLOR EPDXIDE BDL 10 18P. PCB -1242 BDL 10 19P. PCB -1254 BDL 10 20P. PCB -1221 BDL 10 21P. PCB -1232 BDL 10 22P. PCB -1248 BDL 10 23P. PCB -1260 BDL 10 24P. PCB -1016 BDL 10 25P. TOXAPHENE BDL 10 BDL=BELOW DETECTION LIMIT RM EXHIBIT II - COMPOUND LIST SAMPLE IDENTIFIER: 83-528 Intake COMPUCHEM SAMPLE NUMBER: 11376 INORGANICS PRIORITY POLLUTANTS 1. ANTIMONY, TOTAL 2. ARSENIC, TOTAL 3. BERYLLIUM, TOTAL 4. CADMIUM, TOTAL 5. CHROMIUM, TOTAL 6. COPPER, TOTAL 7. LEAD, TOTAL 8. MERCURY, TOTAL 9. NICKEL, TOTAL 10. SELENIUM, TOTAL 11. SILVER, TOTAL 12. THALLIUM, TOTAL 13. ZINC, TOTAL INORGANICS/ CONVENTIONALS BDL=BELOW DETECTION LIMIT CONCENTRATION DETECTION LIMIT* (MG/L) (MG/L) (None Requested) 0.13 0.05 0.05 0.05 BDL 0.02 0.02 0.02 BDL 0.1 BDL 0.1 BDL 0.2 0.0004 0.0002 BDL 0.1 BDL 0.05 BDL 0.06 BDL 0.05 BDL 0.02 �t EXHIBIT II - COMPOUND LIST BDL=BELOW DETECTION LIMIT 60 SAMPLE IDENTIFIER: 83-5300 Cooling Lake 00"-" COMPUCHEM SAMPLE NUMBER: 11375 DETECTION VOLATILE ORGANICS CONCENTRATION LIMIT SCAN (UG/L) (UG/L) NUMBER 1V. ACROLEIN BDL 100 2V. ACRYLONITRILE BDL 100 3V. BENZENE BDL 10 4V. BIS (CHLOROMETHYL) ETHER BDL 10 5V. BROMOFORM BDL 10 6V. CARBON TETRACHLORIDE BDL 10 7V. CHLOROBENZENE BDL 10 8V. CHLORODIBROMOMETHANE BDL 10 9V. CHLOROETHANE BDL 10 1OV. -2-CHLOROETHYLVINYL ETHER BDL 10 11V. CHLOROFORM BDL 10 12V. DICHLOROBROMOMETHANE BDL 10 13V. DICHLORODIFLUOROMETHANE BDL 10 14V. 1,1-DICHLOROETHANE BDL 10 15V. 1,2-DICHLOROETHANE BDL 10 16V. 1,1-DICHLOROETHYLENE BDL 10 17V. 1,2-DICHLOROPROPANE BDL 10 18V. CIS-1,3-DICHLOROPROPENE BDL 10 19V. TRANS-I,3-DICHLOROPROPENE BDL 10 20V. ETHYLBENZENE BDL 10 21V. BROMOMETHANE BDL 10 22V. CHLOROMETHANE BDL 10 23V. METHYLENE CHLORIDE BDL 10 24V. 1,1,2,2 -TETRACHLOROETHANE BDL 10 25V. TETRACHLOROETHYLENE BDL 10 26V. TOLUENE BDL 10 27V. 1,2-TRANS-DICHLOROETHYLENE BDL 10 28V. 1,1,1 -TRICHLOROETHANE BDL 10 2Qv. 1 1,2-TRICHLD"OETHANE BDL 10 3uV RICHL-jk3ETHYLENE BDL 10 31V. TRICHLOROFLUOROMETHANE BDL 10 32V. VINYL CHLORIDE BDL 10 BDL=BELOW DETECTION LIMIT 60 EXHIBIT II - COMPOUND LIST BDL= BELOW DETECTION LIf.17 SAMPLE IDENTIFIER: 83-5300 Cooling Lake COMPUCHEM SAMPLE NUMBER: 11375 DETECTION ACID EXTRACTABLE ORGANICS CONCENTRATION LIMIT SCAN (UG/L) (UG/L) NUMBER 1A. 2 -CHLOROPHENOL BDL 25 2A. 2,4-DICHLOROPHENOL BDL 25 3A. 2,4 -DIMETHYLPHENOL BDL 25 4A. 4,6-DINITRO-O-CRESOL BDL 250 5A. 2,4-DINITROPHENOL BDL 250 6A. 2-NITROPHENOL BDL 25 7A. 4-NITROPHENOL BDL 25 8A. P -CHLORO -M -CRESOL BDL 25 9A. PENTACHLOROPHENOL BDL 25 10A. PHENOL BDL 25 11A. 2,4,6 -TRICHLOROPHENOL BDL 25 BDL= BELOW DETECTION LIf.17 EXHIBIT II - COMPOUND LIST SAMPLE IDENTIFIER: 83-5300 Cooling Lake COMPUCHEM SAMPLE NUMBER: 11375 BASE -NEUTRAL DETECTION EXTRACTABLE ORGANICS (continued) CONCENTRATION LIMIT (UG/L) (UG/L) 30B. 1,2-DIPHENYLHYDRAZINE BDL 10 31B. FLUORANTHENE BDL 10 32B. FLUORENE BDL 10 33B. HEXACHLOROBENZENE BDL 10 34B. HEXACHLOROBUTADIENE BDL 10 35B. HEXACHLOROCYCLOPENTADIENE BDL 10 36B. HEXACHLOROETHANE BDL 10 37B. INDENO (1,2,3 -CD) PYRENE BDL 25 38B. ISOPHORONE BDL 10 39B. NAPHTHALENE BDL 10 40B. NITROBENZENE BDL 10 41B. N-NITROSODIMETHYLAMINE BDL 10 42B. N-NITROSODI-N-PROPYLAMINE BDL 10 43B. N-NITROSODIPHENYLAMINE BDL 10 44B. PHENANTHRENE BDL 10 45B. PYRENE BDL 10 46B. 1,2,4-TRICHLOROBENZENE BDL 10 BDL= BELOW DETECTION LIMIT ,44 SCAN NUMBER EXHIBIT II - COMPOUND LIST SAMPLE IDENTIFIER: 83-5300 Cooling Lake COMPUCHEM SAMPLE NUMBER: 11375 INORGANICS PRIORITY POLLUTANTS 1. ANTIMONY, TOTAL 2. ARSENIC, TOTAL 3. BERYLLIUM, TOTAL 4. CADMIUM, TOTAL 5. CHROMIUM, TOTAL 6. COPPER, TOTAL 7. LE , TOTAL 8 . Y , TOTAL 9. N , OTAL 10. SELENIUM, TOTAL 11. SILVER, TOTAL 12. T LL 111 M, --TOTAL 13 ZINC, TOTAL INORGANICS/ CONVENTIONALS BDL=BELOW DETECTION LIMIT E] CONCENTRATION DETECTION LIMIT* (MG/L) (MG/L) (None Requested) 0.21 0.05 BDL 0.05 BDL 0.02 BDL 0.02 BDL 0.1 BDL 0.1 BDL 0.2 0.0004 (0 - `� 0.0002 BDL 0.1 BDL 0.05 BDL 0.06 BDL 0.05 0.28ZB c7 0.02 EXHIBIT II - COMPOUND LIST SAMPLE IDENTIFIER: 83-5300 Cooling Lake COMPUCHEM SAMPLE NUMBER: 11375 BDL=BELOW DETECTION LIMIT DETECTION PESTICIDES/PCB'S CONCENTRATION LIMIT (UG/L) (UG/L) 1P. ALDRIN BDL 10 2P. ALPHA -BHC BDL 10 3P. BETA -BHC BDL 10 4P. GAMMA -BHC BDL 10 5P. DELTA -BHC BDL 10 6P. CHLORDANE BDL 10 7P. 4,4' -DDT BDL 10 8P.- 4,4' -DDE BDL 10 9P. 4,4' -DDD BDL 10 10P. DIELDRIN BDL 10 11P. ALPHA-ENDOSULFAN BDL 10 12P. BETA-ENDOSULFAN BDL 10 13P. ENDOSULFAN SULFATE BDL 10 14P. ENDRIN BDL 10 15P. ENDRIN ALDEHYDE BDL 10 16P. HEPTACHLOR BDL 10 17P. HEPTACHLOR EPDXIDE BDL 10 18P. PCB -1242 BDL 10 19P. PCB -1254 BDL 10 20P. PCB -1221 BDL 10 21P. PCB -1232 BDL 10 22P. PCB -1248 BDL 10 23P. PCB -1260 BDL 10 24P. PCB -1016 BDL 10 25P. TOXAPHENE BDL 10 BDL=BELOW DETECTION LIMIT