NC0000353_Renewal (Application)_20150713

•
• THE QUARTZ"
CORP
•
•
•
• July 10, 2015
• Mrs. Diana Sprinkle RECEIVED/DENR/DWR
• NCDENR/DWQ/Point Source Branch
• 1617 Mail Service Center JUL 1 3 2015
• Raleigh, NC 27699-1617
Via FedEx Water Quality
• Permitting Section
• RE: The Quartz Corp USA
• Renewal Application: NPDES Permit NC0000353
• Dear Mrs. Sprinkle,
• The Quartz Corp USA (Quartz) hereby respectfully requests renewal of our NPDES Permit No.
• NC0000353 for our "TFC Plant" located at 787 Altapass Road, PO Box 309, Spruce Pine, NC
• 28777.
•
• The only change since issuance of the last permit is that Plant 2 has been dismantled and
replaced with Plant 4 with similar operating parameters.
•
• Enclosed you will find three (3) signed copies of the NPDES renewal application which includes:
• • The EPA Form 2C Renewal Forms;
• • Wastewater Treatment Flow;
• • A narrative description of the sludge management plan; and
• • Laboratory Sample Results
• Should you have any questions, please contact me at 828-765-8977 or at
• [e-mail]
•
•
• Sincerely,
•
• � ,.--
•
• Jerry Prosser
• Plant Manager
•
•
•
•
•
•
•
•

•
•
•
• THE QUARTZ'
CORP The Quartz Corp USA
• APPENDIX 1
•
• EPA Form 2C Renewal Form
•
•
•
• RECEIVED/DENR/DWR
• JUL 1 3 2015
•
• Water Quality
Section
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•

•
•
• EPA I.D.NUMBER(copy from Item I of Form I) Form Approved.
NCO 000353 OMB No.2040-0086.
• Please print or type in the unshaded areas only. Approval expires 3-31-98.
FORM U.S.ENVIRONMENTAL PROTECTION AGENCY
• 2C ".EPAEXISTING MANUFAAPPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
CTURING,COMMERCIAL,MINING AND SILVICULTURE OPERATIONS
• NPDES Consolidated Permits Program
• I.OUTFALL LOCATION
For each outfall,list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
• A.OUTFALL NUMBER B.LATITUDE C.LONGITUDE
(list) 1.DEC 2 MIN. 3.SEC. 1.DEG. 2 MIN 3.SEC. D.RECEIVING WATER(name)
• 001 35 54 16 82 03 47 North Toe River
•
• .
-
• II.FLOWS,SOURCES OF POLLUTION,AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility.Indicate sources of intake water.operations contributing wastewater to the effluent,and treatment units
• labeled to correspond to the more detailed descriptions in Item B.Construct a water balance on the line drawing by showing average flows between intakes,operations,
treatment units,and outfalls. If a water balance cannot be determined(e.g.,for certain mining activities),provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
•
B. For each outfall, provide a description of: (1)All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water,
and storm water runoff; (2)The average flow contributed by each operation; and (3)The treatment received by the wastewater. Continue on additional sheets if
•
necessary.
• 1.OUT- 2.OPERATION(S)CONTRIBUTING FLOW 3.TREATMENT
FALL b.AVERAGE FLOW b.LIST CODES FROM
• NO.(fist) a.OPERATION(list) (include units) a.DESCRIPTION TABLE 2C-1
ORE PROCESSING PLANT #1 Wastewater streatms from processing are
• 00 1 2200-3060 GPM separated into fluoride and non-fluoride 1-0 2-K
ORE PROCESSING PLANT 63 streams. They are equalized and neutralized
• 250-1400 GPM 1-G 5-L
before adding polymers and then pumped to the
ORE PROCESSING PLANT 44 clarifiers. Underflows are pumped to vaccuum
800-1800 GPM filters for moisture removal. The resultant 5-0 5-Q
• tailings are used as fill or landfilled.
Clarifier effluent is recylced or discharged. 4"C 4-A
•
•
•
•
••
A
• ___
II
•
•
•
•
•
•
•
• OFFICIAL USE ONLY(effluent guidelines sub-categories)
• EPA Form 3510-2C(8-90) PAGE 1 of 4 CONTINUE ON REVERSE
•
•

•
• CONTINUED FROM THE FRONT
• C.Except for storm runoff,leaks,or spills,are any of the discharges described in Items II-A or B intermittent or seasonal?
❑YES(complete the following table) WI NO(go to Section III)
• 3.FREQUENCY 4 FLOW
• a.DAYS PER B.TOTAL VOLUME
2.OPERATION(s) WEEK b.MONTHS a.FLOW RATE(m rnk(l) (.cp'i/.r with units)
• 1 OUTFALL CONTRIBUTING FLOW (speritt PER YEAR 1.LONG TERM 2.MAXIMUM 1.LONG TERM 2.MAXIMUM C.DURATION
NUMBER(list) (list) nrrruge) AVERAGE DAILY AVERAGE DAILY (f°days)
•
•
•
•
•
•
•
• lll.PRODUCTION
A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
• ❑ YES(complete Item Ill-B) NO(go to Section IV)
• B.Are the limitations in the applicable effluent guideline expressed in terms of production(or other measure of operation)?
❑YES(complete Rem Ill-C) ❑NO(go to Section IV)
• C. If you answered"yes"to Item III-B,list the quantity which represents an actual measurement of your level of production,expressed in the terms and units used in the
applicable effluent guideline,and indicate the affected outfalls.
• 1.AVERAGE DAILY PRODUCTION
2.AFFECTED OUTFALLS
cOPERATION,PRODUCT,MATERIAL,ETC.
C.
• a.QUANTITY PER DAY b.UNITS OF MEASURE (list outfa!!numbers)
(specifi')
•
•
•
•
•
•
•
• i
• IV.IMPROVEMENTS
• A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application'?This includes,but is not limited to,
permit conditions,administrative or enforcement orders,enforcement compliance schedule letters,stipulations,court orders,and grant or loan conditions.
• ❑YES(complete thefollowing table) 17:1NO(go to Item IV-B)
• 1.IDENTIFICATION OF CONDITION, 2.AFFECTED OUTFALLS 3.BRIEF DESCRIPTION OF PROJECT 4.FINAL COMPLIANCE DATE
AGREEMENT.ETC.
•
a.NO. b SOURCE OF DISCHARGE a.REQUIRED b.PROJECTED
•
•
•
•
•
•
• B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges)you now have underway or which you plan. Indicate whether each program is now underway or planned,and indicate your actual or planned schedules for
•
construction.
• ❑MARK"X"IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C(8-90) PAGE 2 of 4 CONTINUE ON PAGE 3
•
•

•
• EPA I.D.NUMBER(copy Jronr Item I of Form I)
• CONTINUED FROM PAGE 2 NC0000353
• V.INTAKE AND EFFLUENT CHARACTERISTICS
A,B,&C: See instructions before proceeding—Complete one set of tables for each outfall—Annotate the outfall number in the space provided
• NOTE:Tables V-A,V-B.and V-C are included on separate sheets numbered V-1 through V-9.
• D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions,which you know or have reason to believe is discharged or may be discharged
from any outfall.For every pollutant you list,briefly describe the reasons you believe it to be present and report any analytical data in your possession.
• 1.POLLUTANT 2.SOURCE 1.POLLUTANT 2.SOURCE
•
•
•
•
•
•
•
•
•
•
•
•
• VI.POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS
Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct?
• YES(list all such pollutants below) IZ NO(go to Item V/-B)
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
• EPA Form 3510-2C(8-90) PAGE 3 of 4 CONTINUE ON REVERSE
•
•

•
• CONTINUED FROM THE FRONT
• VII.BIOLOGICAL TOXICITY TESTING DATA
• Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
• YES(identify the test(s)and describe their purposes below) ElNO(go to Section VIII)
• CURRENT PERMIT REQUIRES QUARTERLY TOXICITY TESTING
•
• RECEIVED/DENR/DWR
® JUL 1 3 2015
•
• Water Quality
Permitting Section
•
•
•
•
•
•
•
• VIII.CONTRACT ANALYSIS INFORMATION
• Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
• YES(list the name,address,and telephone number of and pollutants analyzed by, El NO(go to Section IX)
each such laboratory or firm below)
• A.NAME B.ADDRESS C.TELEPHONE D.POLLUTANTS ANALYZED
(area code&no.) (list)
• ENVIRONMENTAL TESTING SOLUTIONS, PO, BOX 7565 Asheville, NC 28802-7565 828-350-9364 ALL EXCEPT TSS, PH, TEMP,
INC. FLUORIDE
•
•
•
•
•
•
•
•
•
•
•
• IX.CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
• qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there
. are significant penalties for submitting false information,including the possibility of fine and imprisonment for knowing violations.
A.NAME 8,OFFICIAL TITLE(type or print) B.PHONE NO.(area code&no.)
• JERRY PROSSER, PLANT MANAGER (828) 765-8977
• C.SIGNATURE D DATE SIGNED
S _ _ /le/a°(5
• EPA •140;-90)
PAGE 4of4
•
•

•
M m^ ,m a p 70Q n�01 7" m - :m 7.• m (J)a o pv pd < rn0 1 •
D i !i
m o w7' mW �n '0 ! iii
iliH
ZtNp � •
o c o �3 Dy� f m m a ° a` (nZ�' m D D (n m
3 z mm o m �m ZOC 1 m m 0 (n O ^5. O �0 v
w a m m p -I m d m vN m ^,m �3 < m �� •
o, it F7Po Z a c v = C O V C o D Z
C C
0 v —1 y@ a) m m . a. C� O D 3 oo -0 O •
0 '9 --- x CD 0 0 -Z
•I Tml 0 U, .TJ
\J�/ \X/ X m ro v• X O .o m Cn 0 --I
X X ZF
N o 5.
O a5 D m9 - 3 < < < n Z 03 •
Dm x ES o 0- C C C i ?' 7 o Z
X XXN
�mQ X j�N �� m m m w u A (' z, X m D -6m •
z< m ° ot N w w m • _1..., c A C
p v N O N D C • (? Z
x 67 W N F' - N 2
n a d u� (0 w O o m .�2
•
O m m S- o z O m x 0, O
'
O 01 N m j o O N { N H w 0 •
z- o- — D ni n aD
W N U' -�— 5 C rnx m <
(0 N y " 5-y % • 3 t-, 3 D n CO o m •
O -1 C �,o mC �l 00 C N 0 o D
o -c, CD 3 N m 0 3 (n
'Z- D N �x z j O •
CD -0 •
' C C C m 3 0 3 c o
H 71 D 9 m m m m m 3 ( c
m C o d m • g w - co 1;:,
8.0 3 •
n m o w v
C m d
n n(0 N (1'i l0 l,J Z w O o y V
O U Sap N a-0 C 9,
z K g a l K o N IDa O
a) m y 5'p > N - 3 Cr) .
to X" nK m JK •3 D< m N co
`C 3c < F,C J cn r -n N n a •
v m 3 cn C m m m
i 1w m 3 N. m C o - •
o w �a m o
D -mn » m D D D -, o y •
1-' 3co > D C 0-a- (1 (� -,
' i; m m m
cn C Z o o d '[ie O
z r m 3 •
m a j F n O o m
M z
n n n N X (i'rt•, H G1 m •
O c A m N
73 cT
L) .P (On Z o O ` +'' O 1'DJ ' O °N K o z •
m z; O m c a) z D o m
o
--z,'..•m N fD N 4�. n C) o o •
—
21 Z c' 3 �N Q r` '. < o o p
_ w •N Lo C
F-' — -0 .° N N >, .P D m 0 •
4--' C ] ? ♦ O Co CD m
N D < g o m 70
m ° •
m m 2
p O ^ D a 2
Z• o o •
a n w Z
> N C U� N N In r N
U1 r Z N a- a) N Ul N iJ F--' F-� O p 7
F' N N 0 p C N-n a •
�m am(D a �:. •
N•
Ft) -(5--or'rn (71 3 �(7 w' •
A
m?3 3 3 n QON Z
O cC �z 0 r r r r r Om " °N � o Z Z
•\ \ :j,C v
C r C O,,9 :I- x n nZ? c- „ C _
Z N `2't
3ca zv c(n •
Q (0 3i - 0 to D
M3 n m (n 0 (n cn •
m .°:cn 8 (n
o
3 D D D p •
O P, N '.•-.�'. - C C C •
r o ° >uti m m m zC D
m O c $ ,,.. <d
-I- o 3 m .�.- 11 Or-
-I •
2• <-I ( x� ''-...' O �Z
o r A o z m 0
O z m; , c c Dm -as O •
O < x > ? ti a Z -
•
'�' 7m;(�7 m F Y. m 3 0 D -Ti
2 3m
Z •
C
• m a O
Oc .�'�
•
Z D ,. 3 - D
Z Q N Z Q
< <. o m <
U m (D N m •
m
•

•
M 1x vE vl< v1c v- � rw r� �� ":74 1:' X61° ? ^n 3 T.
r A 1�o v ".-..111; .97 y1m •
D pVO A° A° A T� A— () A° y A" E, (A .7.,•.--N 0... 0... .� T 0 JO z m
ly; p� ��' m r�g it'; m sw�pp pp� q�O P� ��� c rnpc 3 �pc S-' s-' z w E. wy m Q ° 0O E •
T w 3 11 m `< 3 bow m Na Z2. 3 a ° 3 a go2u n k a 3 5 v S g O2 4 DDI- <
1m `$ 5. it„"$ a' 1V m E c' d m o- n Is 9.Nzr
N C.
Ind°» $ r° . A' c -6 -0 w0 --I 3 c, w co 3 ° ��-' a •a�' A PAZ O •
co
o E 1 z
z •
N
n
co
XXXX XX X Xzgm • o •
o 7J 0
> •
XX XX XXXXXXXX X zo� 9 •
•o d
z •
0 O •
O O
A
N p O m
awor /
•r C
O $
z •D
; < •
D
Ca C •
• m
n• Q •
z
m •
'C •
O2 g
.o W •
E.,
CI
`D T
• < r •5 < C
w •com
v o 5, •
r
i m
mO •
< 1-
N =Ic m •
z
° •
g
O •
co <
0 C •m
>0. •
r r N r r r r r _<O •
Pi
co T •
to
•
n •
' L] 4J L-. S. G] ,n G.. •
O
C C C C L\-' tt r r Zm C
Z Z •
v
D •
- - y •
co
n
z •
z
o
1. m, •r
• 0 •
Z
z m0 —
•
n - >m >
Om2 •
1
mz CA I •
0 '° ,�
O
z y c •
�-
D z
m •
NO
< in
mm •
w
•

•
m 0 N 0 1 11 1 _ 1 m m .i rn 1u A w N •
Er W ^01 O A vW O N rJ O O v V V v V V V �1J . -0 0
13 _ A• A; O 3 m _(� D
m X o• _ o• y• oz TE pr- Qo �0 �e Qa Q� D �;(n ° -I -
o ��� Z �m rn� yam nNi� "ZiT I') v� M0 p� �o S 3 �� X7,0 '`r ° ZDm 0 Z •
> > �� cyto A �� N� 01° b,c .z..,...4 ao3• ,13 E. �c ��' ooCZC • m
w �N o_ Na ---1 4c' - 4.c' 1 v`-Z 0 J.� 3 :::1
3 _. o &01 m Q am; -*4.- a •
co 69 ) �m o m3 0 cp3 fiNJ' t o 6-' ° J3 1 o 1 D m CO D ex O 0 m°c T
mzmm
m _ 9. N m
4° D mm aq g.c.m 3 d m y •
c X X
z c0m ---.9 m m 0 0
1 5Cz m.•}8rn3 W
01 mvp Nnac � ox�� O •
r M O C ID I'.m. O 7 m •
-0 mr D2en 'o � $oc O
cnm? Xlc.o E o m-o ft XI
O F.io rm09005 -
x3 -. oo ' a0 h •
X XX XXX XXXXXXXX � z � m� �� o
i o comma
s
•' - iom
m o ° mcc
O N 9,'RDDZ0 3 - F •A 0 CMI mr
O z j O m 7' .m.. 0 •
w O N �... C a.m.'<.`c 0.N
.M 1--' 01 -I C 1;1
c c
m p �t
Cl) z a �oa3i �'�+ 7. m •
CO1 -< c`ciran'8002a C. D •
< 7goc m m ° a
> (°�1m33oao W Z •
w C a.( NR-g q m C
c a w
o - Zoo ?- m •
o K m N 0333 .•a m
y n •Z j X m5.R O N o g 0 0
-i... c D
;17 ti C 5335: 7 m1 '''4, •
O G W ft m N' m m O
NI
Z o-0 m m -'O-�p m m _O 3 •
0 -n 3 -'3-2 0 m -.N
< r r27ccbO5 �,
v r Z co$N? 6/'
m •
D cn C 1 trail 0 < 5 3 •
m o a o 3: m
G1 o c m o 2 .�
< o ?3 ac a.
c,., z P mm33 � •X$ o o O •
c) <r ace�o _.cen o 1
m D0 m ' al o o2 ' D
�v cv �a° o 1-
m° •
m m O m c o N r-
-1 `+m N3.NS73m C •
z M m m Nm c. m
1,2 Xa o 3- 71o-C N E •
f = '.) *$ m
3
�o co
cn n a m g N O •
Z•n Sim4.m o •
>z g„§,"-0
I-
I-. r r‹0 c 2'2
on
W0 -Tg-2 m, m E •
P 3 0°•, 0 m •
1 o c c Ha_a
3 30 m 3 3 < ^ g
G) o DiZ mm ^:VD ,.9 •
ow -oon
C' C ZZ C mOOR.moc •
Z cLg2
v3co»
N
> a
0, V< _•0O •
CP oo
c � 3 � .
m3mcmcn $
Ca
o R5.. a. ., *
16 - •'� mm p� CoX
•Z� <" m m w o 3 0 0
Z 0-c 7 m N m C •
c) o rnn0 -Zi 03d °ya
0 <m D =m m m m N •
v �� m • mm �_� nm
z
m mC 'o c2 Ro o1 . •
E_
m o. oo m ad2 _
Z y ...O m A • m •
X z• 2m 7, c 7
< DZ o <°•roc G)G) •
m _<I-0 = m
XI
m ECM
CPO ooc ' m»cncn •
•

•
f ^G. -I 0) y,N A -W ^N0
5
0 j a No ofo ti ac 3 4 g� gA ":=1;LI VY'g N 'Z'
_ 45 tr< no < o < Y'< Wm < < o< CCO
•
2�< < < N� < � K < W < 0 < Yc < o < q< O`C < 0Aonvn n N- � Vb �y ZD .$' 3dw ' "5-:' � _„ 3 -- 3 ., j C NCi .iS.N = 4- z Q? m YoOoja •- S ��m ' mid m � iv : °3 ? � �= Y' 7 wo4'mo Y.ovoa v °°mn vYo 4, WDO
08- m 7 i m � a _ �8- gmO -n Zr Z
�S �g i v ":-.1.9. ---4 0. -:-s
q Y'9 1 o 5 3 ` moR —aa „ CD= c ' ', 2 =

•
V {O n V Qf �J, nA y7 a W m N m N m N ^0 N ^N m N (7N () •
m D D D D D D f0 D G) V V C O t° ao Cl N A -,71['' ?N
mD cg •f�1 -. gyp • m • w• 5^ n < °'° < 5< d< d� < Q� < g< < ° < n _n O
> O N 8 Y 1� O t. V N N O A O y N O N .I N C tc°° 1 m 1 3 -• 3 -L O OD F j 7. D T -41
Z •
T A N S 7 l J N Z Yn'Z ,..7? in 1 i` Oo 0 w 4,7 4,g .. 3 m - m - O N m m 0, m U co p2~
Zoo' v g m g (n S 2'1
04 4 m'Q U1 g -� _� � T 5- ++5 • V IJ 1 al v° v IJ 5 T O Z D r •Z
qo V° 7 7 O N • ° •--t .< 1 m ^ V c Z r c •
tat ° ion �� $ $ N- � y.3 Q� 3 � A m ° m 01 ink � � ° n�}_ $N �'�• � p�pC m
W m 4' cn m s a. a. m .1
Lns NJ ao �3 > > N� 1. °. .< Y'° s -, o m Q oQ cQn�r �' ° nom+ O� n (O".°3 Z O
C _4 4 4 .� , co— AlQ c - m 40 "Q "°� m �4 m N O '-'� zm
•_n ZI Y Z
D ` °� 13
D •
_ D zz� m
c0 -.4 o G) < •
. . O 1- N .b
m
-13 o O mmc D •
C M max
ZM
o �v X •
W c
XXXXXXXXXXX XXXXX XXXXXoz w-n •
N
•
3 0 m
CZa •
ri •
1• 3 •2
•
g D
yc •
cn c
m
1
. O Q •
mx •_,� ^E•
c •
Z▪ a'0 ..nn •
o-
`D T
N < T
<
C
co co m -I •
m •
< <)
in Zl- •
m Dr
O •
—,— CO
m
Z• A •
•
✓ O •
f v p
co
•
Da •
>z
umO •m0
y T
P •
1 n
?
O :I,
•
z? z •
c N •
E
D •
N
o •
O
2
m D •
-I� m"
= O - •
c) 0 mGZ) z
Z Z _Dm > •
z 5• m o^
m ••
codO
Z Cl,' •
xi ZD 0
m p •
m cn w-^ •
•

•
m g N N D1:38D 7 ;15,—a.yr. ,a" mr) ^N - aRTao
Tco SOC V A. N A ^W N 00 •
3O N9 in v7 7. O7 7'A A W �N �S -.3.O N W m . N S W O� N� � n _n
7 m 7 m k'gw m $m COm CO gm m ao ao m o ao �e oo �o 00 �� o g N. N.
> N _ v 7 w 7 7 Y�p W E 0� Q T
m 3 - m 9ao 20 v`s 5Ni pc. �S ��m. s �, � baS° m � 7 � �' � � �$' N tiD _
C 7 7 N W S :T.;`s•
-h C �T W413.7 H'(A T W N �.7..7 cog � m 7 Eli,
�n7 N'^J m y < ZDOr •
m w m 8 g f, 0"m 7' m'1 .W. .. O O AAA g 6?N N ,,,:w N N N -N. v D)7 Z
gio0 37 v -0.
aa ��:, ��ti �mti ._.a , mo ,-.oo - o o. ._.m c m o.C2� C
W 'r N v a i o 0.i 3 0/ c n j-r,) m� 8 6 N wa ° 3 1 1 7 3 c FpC rig •
'hi
o 's 4 7 $ a4 4� 7 a '' q N� 3 n n pp Z
o Qn m m ' 7 o m o r�- do "m •
N w Q •''i?' W l 70 'O N m m 0 XI -I
C) Z $
$W D Dy = •
y c,m m
- T
z vo 7, •
m iv O
m Mm � •
co c XI
00 0 X
XXX XX X XX X X X X X X X XX XXXXz •rl
O an-n
0a •
o01
o S
m
v a •
O c) •
z D
• • < •• <
C •w m
n Q •
m •
- C •-I n M
� •D T
$ D m •
m
m •
< C)
o •
b, m C
<r
Z, rz
'- _
o `;m
m •
Z 1i
• a< •
"G0i
y •
1,0. •
{
o
m0 0
m •
-1n
On A.
z
Z •
c N •
E
cn
o •O
z
o
-I- and •
Z `�
= 0 •
0 0 z
z o Z <m D •
z
c - m a
m co
O y 2
v D
D �z •
m O
< y0
V C T •
•

•
m -a zit A mA aW vW W W N(�1 -:31.2 W SW[� W ^Ou W I SI 2K O 3N sN ° N -N ^3N 3N fNt pN 0 •N O f0 OD "`V WU A gW Nm 7 t0 OD �l 7 U "'�7 U 7 A O GI
y ' m ''-.Fp 4°m m °'m (eNm mm m m 4'm m , nW gm ° o° ,Da° gm -gm gm ° m ° m c _n O
,j0 ip '°• N• U• u 3 2 ,,rept, 0-z m ce 2 '6' d > > m d m tl. N D Z
m a ? Yi ro ? Sn Z 4 Z w g m ° .i'� 2 �p 2 2 w T T tl.J y 0 ° N ° N LIP m 0 a w -' lA Q •
° mZ '°5Z 6' Wv ,..� �8ma rnd .A, k R `° 0x �o 00 �°'3N mz �Q' ^+ mZ „3 m:: iw c°-i' m IZDr Z
] v3 1.Z 7 0 ...-ao v7 vn� ra w v o hoc w ° ^7 p --p �+ c^';or c
7 037 ° �mv $� .-' m ' g s m- c •
o n 3' ? m �°� m Q �Q �Q ° m N$�ye c4 >q �3 �p oR (Djcr D 0
N ° m m ° w i' z CD V? o - - N Y' in-. vQ v� 1 •
o ..7..•
z c
m 00 mm > •
o > ctim o
Z �z m •
mo <
m N b,
i mm c •
mQ
r zm x •
n 1 0 X
K FPI
X X XXXX XX XXXXX XXIXXX XXX ° 'PP •
o -pm
. •
N C) m
O Z DC •
mr
e ZJ •
S C
•Z• D
< •
5 D
m r •
N m
m
, 1 •0• v
0• cy
m X •
,3 c
• C C •
z w w
z c m •
o-
:°D T
< C
D y r Z
m c -1
mm I m •
V ZCc •
m Dr
O •
cc
m
zz 2 i •
o_�
v q 2.
•
P
y
• v •
D
a
0 •
j
rncn o •
-in
•
O n :I'O •
Z? z •
Q y •
m
� •
o •
z
-1.7.• " and •
= ° _ •
0 z R'� 1
1 Dm x •
• ri m
c 5 m; s •
m °
Zo •2 DQ
< J-Z •
m {O
m
m y o •
0

•
m zaw ,4cn
"7-1NA --,4
cw an $o vv „� O-11 T41 9E1 1-3 513 iv 11;3� 1:'
� "'7 n -,,-;at
tzt mt tit
n 0
8
•
m 0 OO C0 (0 W -
D2r ;Cu O Y YV O .A in.4. NA V0. so?, :- T mQ , c _ WOfi2 _Dm Z
m +m pm m 'PNP v v0 A YA Tit ?7 W Tm prt 8a / NPNQdlxZ z(1) O •O -OoSO-> m= O a am �_m . 5 .O0D.m06 .W.� DDvc27mn �n n NT -,9i .1
—.s. tc ZEC
m gc 0 n 0 0 = _> g.E0_, m
•
m 1 6• am @ rZT
N = 0
m 00 0 •
C) z c
co m�m 0 cc •,m m
—1_ SZ� xi
T •
C) Z ° 0
CC mw Z
m x zm •
r_
Q
r mm77
zm
00 ,. X •
g CO
XX XX XXXXXXXXXXXX X XXX Z O WD
. ••
r
o d
•
cn
n DD •
. o
m_
g •
0 0 •= D
1 •
fD
. C •
W
m
f) Q •
-ie. •
C •
2 2,O- W W
o C m •
`D T
< C •m
Z
0 m •m ,
< C)
clo z P •
m Dr
O
- m •
Z aA° •
� °o < •
; G)
y - 5
D 0. •
r-0
m0 •
cn T
N •
50. •
Z 'Z z •
O' c •
N •
oo
•
O
m2
D •
�� m9'
AO z m� -I
<m •
C v m2
m •
•
0 0 2
Z •
D Zo
r •
m mo
CD y0 •
•

•
2 k� kk k mk j\ ---.1
� cl� )70 �7.0 2 7' 0
leg®� 4n §§ kA 2O §) )O en -»I CO
....
7»P § •
( -•co rp7 §e $Y' 2T, TT @� / 7 2 .c7' c
m 0 CO1. IQ 17 �\ o- n a CO n ° .
§ ® ` z $
R k
o .
co m0`
— q XIZ m
§ �° 7 •
m 7r- > •
CT rcg fl %
. -l0` R
•�
X X X X X X X XX \ mim\,
moo. •
j •
-
§� "t•
m .
§ 0 2 •
( § •
} i F
§■
•
CO m co
2
A 7 2 f
\5 =§ 0
\ ' C ° ƒ •
z «2 �
kf � \ •
2 \ n � .
•
m kw
f S o) o q •/
_ k
\- § \ •
° �M c •
1'4 XI
§ §
ƒk •
0 �®
•
>z •
0o •
�� •
n
§\ •
�( ( 0
[ cn
•
k •
o •
-I2 i .
§ §2K •
k m° 5
i93 # •
13 rn
\ m § •
m { .
1- .
\�
��
•
•

•
•
•
• THE QU ARTZ'" The Quartz Corp USA
• APPENDIX 2
•
• Wastewater Treatment Flow
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•

Filter Plant - Fluoride o 0 A O 1
Date—1/02/2015 co 0
w e CD
18
`o o. `0 0 S'
t O 5(Add Add co
Cationic Cationic
Polymer Polymer
Plant 1 / Fluoride Plant 3 Add Liquid
Fluorideli'lTanks N Fluoride Lime
Pump Pump
Sample Point Water sample tak
testing.
Adjust Lime
Lime Feeder
` Feeder /
\ * Controller adjust:
A feeder for proper
pH.
No- - Is pH
correct?
Yes
Pump
I
Splitter
Box}
* Operator adjusts flc
dd
Adjust A�onic 1 Adjust N— proper water c
Flocculant Polymer Flocculant
55'Clarifier 40'Clarifier Water•-
Water
w w
Spillway
ateria ateria
-4--N• Settling Settling Nom
roperly roperly •
Yes Yes
Sample Point Water sample tak
testing.
Pump Disc Filter Pump
T
Sand
Water Room To River
Conveyor Recycle
Pump
(ToSritterBox)I. •- •I Treated Water
Co Pant i Sam) I
Room J
* Control Point
Fluoride
Tailings

Filter Plant - Non-Fluoride 0 0 A O ) O
Date–1/02/2015 w o c o_ r >,
a 1 5"
D .
tct 0 8
Add Add 05
Cationic Cationic
Polymer Polymer
Plant 1 Plant
Tailings Tailings
Pump Pump
Sample Point Splitter
litttr Sample Point Water sample taken for
Box
testing.
Add
Adjust An onic Adjust
Flocculant Poymer Flocculant
Old New Water
Clarifier Clarifier
I
ateria ateria * Operator adjusts
—No Settling Settling No--10- flocculant for proper water
•roperly -ropery quality.
Water
Yes Yes
i
(To Fluoride SysterrtJ
Pump \ ��
Spillway
Disc Filter Water••••<ToSifter Box)
Ir
Sample Point
Conveyor
•
Water sample taken for
•
testing.
Conveyor Plant 1 Plant 3
Recycle Recycle
Pump Pump To River
•
I
Fluoride
To Plant 1 To Plant 3 Treated Water
Tailings
* Control Point

•
•
•
THE 0 QU ARTZ The Quartz Corp USA
• APPENDIX 3
•
• Sludge Management Plan
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•

•
• THE QUARTZ"
CORP
•
•
•
• RE: The Quartz Corp USA
• Sludge Management Plan: NC0000353
•
• The Quartz Corp USA produces mineral tailings (sludge) at its wastewater facility located at the "TFC
Plant" 787 Altapass Road, PO Box 309, Spruce Pine, NC 28777.These mineral tailings are disposed of as
•
follows:
•
• Tailings from the wastewater facility are conveyed outside the building to a staging and storage area
• Tailings are moved to disposal sites by dump bed trucks on Federal, state, municipal and private roads.
Trucks are covered during the transport of this material to prevent the materials from blowing off the
• trucks.
• Sites are chosen for tailings disposal that will enhance the value of real property by filling and not
• present problems through the loss of materials to surface waters by erosion. Steam buffers are
• observed (25' min.) and wetlands and seeps are avoided. Sites are planned and approved by submittal of
• a soil and erosion control plan through the NCDENR Land Quality, which explains the land disturbance
• activities and also gives details on how stormwater runoff will be handled, how sediment loss will be
controlled and how final reclamation of the site will be performed. Landowner agreements must be
• signed to assure future preservation of the sites. Going forward Quartz will apply for mine permits for
• the disposal of mine refuse (tailing) rather than a simple storm and erosion plan.
• The tailings are also used in reclamation of mine sites. Ceramic companies who make floor tile and other
ceramic products have bought the tailings for use as a raw material.
•
• Should you have any questions on this policy, please contact me at 828-765-8977 or at
[e-mail]
•
•
• Sincerely,
•
•
• erry Prosser
• Plant Manager
•
•
•
•
•
•
•
•
•
•
•

•
•
•
• THE 0 QUARTZ'° The Quartz Corp USA
• • APPENDIX 4
•
• Laboratory Sample Results
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•

•
•
o c •
o d
'C 0%) c` c ro 0 0 f d ( y -0 Obi •
3 7 _ 00 v - < n 7 cr 7
X). I, ILILI, IL � I� 1� IL � IL � •
x A A A A A A A UI N V1 N V'I
c0000 0000 0 � Daily1111, •
Mo o 0NwNOwww Flow Rate n, CO m N, Uo •w w w
0o w co in 0 Orn 01 I- o in I. Effluent
Dr 4 CO W 00 w 00 N V A V W 0 4.0
fD 0 V l0 V W I- 01 V VI l0 N 01 A Z •
� 0
0
3 at m V v V V S.U. P H 0 •
N N 00 N N A N A A N A N .p •
to NJ UI NJ VI VI NJ U1 N in U7 00 U9 V 0
7' 0
i Total •
in in NJ N o N N ,- ,~+ o MG/L Suspende •
C O V tD :I v O CO~ l0 A Imo-. 31 N N d Solids
C A in in to oo in l0 0) 0 V N V1 V1 I—
toL.....
�
, Total •
G NJ
inW i-CD. 0 N N N N N #/DAY Suspende
fD N N A N w V N 10 I-1 U7 N A d Solids In •
7. I- in 00 to A in in N A Oo 0 i U7
7' •
N
,74 Total
m cNo I-. w ) to. .J w to V 0 MG2 Fluoride •
3Oo w N co F+
ID 0 ,-. C1 0 31 In v1 O1 UI In in in In •
K
N
0 Total •
in A w w in Ut w v1 #/DAY
in N A o .I 31 w V al Fluoride
G V D1 O N cn N N N A W t0 N V 0
o •
3 w o 0o U, in u, A in W :to. U,
z to
to
•
z Io
m m
3 D •
7
o NI
c 00 •
tri
m N
C d o K > K •
v d
7 E a v ,^. < n 7 IT -
•I--+ 12+ 4 4 N I-+ IL 4. N I-+ IILF+ •
p A A A A A A A V1 V7 vI In U1 �=1,
I
0 Daily •
N o Flow Rate •
Q1 it, N N N N N N N N N N) N Effluent
0) N) O O in in A in VI 0) in 00 V V •
00 01 O l0 Ut I- t0 V A CO0 0 In
WZ
NJ A
U~I S.U. P H 0 •
V m 0) V V V V V V .I of 01 m 0 •
fit
I--) t0 l0 N N N A A A 400 io 0o W
3 N O O W UI O w In VI 0 0 0 03 W
"' W •
A Total
7 I-. W N 1-+ r+ 1--. F+ 1--. N h+ N N MG/L. Suspende •
ID co O t0 V N NJ N A Dl 0 Ln d Solids
d 0)iv 0 o to w o o Ln VVI UNi UVi 0 0 •
..
M Total •
5 w to a m to o 03 NJ c torn 4 v w #IDAY Suspende
00 Lo w 0 '.0 w U+ VI I-. A I•-+ 00 t.0 A
N d Solids •
V O A N i, A O U7 V in in bo in
y, wO 0 VI Ln 0 0 0 U1 0 0 0 0
C •
N
d MG/L Total A w w v1 •
— A VI A A m u, Ln Ln A Fluoride
d 0o A N A ,--. 1-+ W 01 U1 A N F-. bo
d1-4 O O l0 1.0 00 W W V F-' CO V l0 •
n
7'
✓ I-% r I-+ ,--‘ ,-+ F+ r i--‘ F+1--, 1--� I 1--. Total •
r O 01 0 I-` I- 0 0 In N N 1-. N #/DAY
N w V n, }o o w VI to A Vi Un - Fluoride
00 •
N A W N ? 01 W O ...iN 01 in
N O O VI 1--1 00 O U7 o v1 U7 O O
•
•
•

WATER TEMPERATURES •
•
•
NC0000353 0
WINTER SUMMER •
•
Oct 19.2 1.0 April 14.7 1.0 •
18.4 1.0 13.4 1.0 •
16.6 1.0 16.6 1.0
18.9 1.0 15.8 1.0 41
Nov 17.3 1.0 15.8 1.0 •
13.1 1.0 May 15.6 1.0 •
13 1.0 21.3 1.0 •
6.4 1.0 17.7 1.0
11.7 1.021.1 1.0 •
Dec 13.5 1.0 June 21.5 1.0 •
11.1 1.0 22.7 1.0 •
11.4 1.0 25 1.0 •
11.7 1.0 23.7 1.0 •
9.2 1.0 Jul 19.2 1.0
Jan 7.8 1.0 23.1 1.0 •
9.3 1.0 22.6 1.0
11.1 1.0 22.8 1.0 •
5.6 1.0 20.5 1.0 •
Feb 6.9 1.0 Aug 22.3 1.0
8.6 1.0 21.9 1.0 41
4.9 1.0 21.4 1.0 •
4.8 1.0 23.6 1.0 •
March 9.8 1.0 Sept 23.7 1.0 •
14.7 1.0 21.8 1.0
9.9 1.0 19.2 1.0 •
15.7 1.0 20.6 1.0 •
•
MAX 19.2 # MAX 25.0 # •
AVG 11.6 26_ AVG 20.3 26 •
0
•
•
•
•
•
•
•
•
•
•
•
•

•
• Effluent
• NPDES Permit#:0000353 Discharge#001 Month: lune Year: 2015
• Facility Name The Feldspar Corporation Class: P/C 2 County: Mitchell
Operator In Responsible Charge: Joseph L Pittman Grade: P/C 1 Phone:[phone]
• Certified Laboratory(1)The Feldspar Corp.Water Quality Lab (2)Eli'Environmental
• Check Box If ORC Has Changed: ( X [Persons Collecting Samples: Joseph L Pittman Jeremiah Hoilman
Nail original and one copy to: R binson Joey Fairchild
• 4tt: Central Files, Division of Water QualityZ
• 1617 Mail Service Center (Signator f erator Responsible Charge) Date
Raleigh,NC 27699-1617 By this Signature,I certify That This Report Is
•
Accurate And Complete To The Best Of My Knowledge
• *50050 *00400 *00530 '00530 '00951 *00951 *00076 *00545 TGP-3B '00940
• f0 N co
• Q $ H in 3 0. 0. ICI
A t c 3 a> > v a) a) l'' -0 co co
• W ANY m p u m tn � v_1 -0 v c v m c
H a) o a) 0 >' .N. N m 6 0 0 f2 a7 o
Q E O c = o m o m > > m
• o g 1= 0 &o 0 o w a ►- � 1- cc ti LL co n U
pa
• HRS. HRS. YIN MGD UNIT MG/L #/DAY MGIL #/DAY NTU MUL /Fail
, MG/L
• 1 0700 24 Y 3.00
2 0700 24 Y 3.00
• 3 0700 24 Y 3.00 6.80 33.00 817.00 4.72 118.00 9.90 <0.1
• 4 0700 24 Y 3.00
5 0700 24 Y 3.00
• 6 0700 24 Y 2.70
• 7 0700 24 Y 2.70
• 8 0700 24 Y 2.80
9 0700 24 Y 2.90
• 10 0700 24 Y 2.90 6.60 30.00 734.00 4.97 120.00 9.70 <0.1
• 11 0700 24 Y 2.80
12 0700 24 Y 2.80
• 13 0700 24 Y 2.90 ,
• 14 0700 24 Y 2.80
15 0700 24 Y 2.80
• 16 0700 24 Y 2.80
0
17 0700 24 N 2.80 6.80 20.00 459.00 5.06 118.00 8.90 <0.1
18 0700 24 Y 3.00
• 19 0700 24 Y 3.00
• 20 0700 24 Y 3.00
21 0700 24 Y 3.00
•
22 0700 24 Y 3.00
• 23 0700 24 Y 3.10
• 24 0700 24 Y _ 3.10 6.70 20.00 526.00 4.96 128.00 8.60 <0.1
25 0700 24 Y 3.10
• 26 0700 24 Y _ 3.20
• 27 0700 24 N _ 3.00
28 0700 24 N 1.70
• 29 0700 24 Y _ 1.50
• 30. 0700 _ 24 Y 0.06
AVERAGE 2.75 6.73 25.75 634.00 4.93 121.00 9.28 <0.1
• MAXIMUM 3.20 6.80 33.00 817.00 5.06 128.00 9.90 <0.1
• MINIMUM 0.06 6.60 20.00 459.00 4.72 118.00 8.60 <0.1
Comp.(C)/Grab(G) w • t� G C C C C G G
• MONTHLY LIMIT _j6.0 to101k N/A 1568/3137 N/A 174/348 N/A <0.1 N/A
•
•
•
•

•
Effluent S
NPDES Permit#:0000353 Discharge#001 Month: May Year: 2015 •
Facility Name The Feldspar Corporation Class: P/C 2 County-: Mitchell •
Operator In Responsible Charge: Joseph L Pittman Grade: P/C1 Phone:[phone]
Certified Laboratory(1)The Feldspar Corp.Water Quality Lab (2)ETP Environmental •
Check Box If ORC Has Changed: f X Persons Collecting Samples: seph L Pittman Jeremiah Hoilman •
Wail original and one copy to: RobinsonJoey Fairchild •
Ott: Central Files, Division of Water Quality
tel.
‘/0/4/5---- •
1617 Mail Service Center (Signa a Operator In Responsible Charge)
Raleigh,NC 27699-1617 By t 's Signature,I certify That This Report Is •
Accurate And Complete To The Best Of My Knowledge
*50050 `00400 *00530 '00530 •00951 '00951 *00076 *00545 TGP-3B *00940 •
m -0 0 41 •
> E d C c is
Q $ H Cl) 3 a a 2 •
O N 60 C 0 7 a m >,
w Y C) N -0 'O -c C c0 0 'C •
o- OI= O 00 O Ow a I- r[ i-° ce U. u. F co m 0 •
•ass
HRS. HRS. Y/N MGD UNIT MG/L #/DAY MG/L #/DAY NTU MUL /Fail MG/L •
1 0700 24 Y 3.10 -_- •
2 0700 24 N 3.00 -__-
3 0700 24 N 2.80 -__- •
4 0700 24 Y 3.10 -__- •
5 0700 24 Y 3.20 -------_- •
6 0700 24 Y 2.90 6.70 24.00 589.00 5.18 125.00 6.30 <0.1
7 0700 24 Y 3.20 •
8 0700 24 Y 3.00 •
9 0700 24 Y 3.10
10 0700 24 Y 1.40 •
11 0700 24 Y 2.00 •
12 0700 24 N 2.50
13 0700 24 Y 2.90 7.10 22.00 524.00 4.27 103.00 9.90 <0.1 •
14 0700 24 Y 3.00 •
15 0700 24 Y 2.90 ._-.---_- •
16 0700 24 Y 2.90 -__-
17 0700 24 Y 2.90 -__- •
18 0700 24 Y 2.80 -=== •
19 0700 24 Y 1.30
20 0700 24 Y 3.00 7.00 27.00 667.00 5.26 132.00 10.10 <0.1 ■- •
21 0700 24 Y 3.00 •
22 0700 24 Y 2.90 -_- •
1
23 0700 24 N 2.80 --■-
24 0700 24 N 1.70 •
25 0700 24 N 1.70 --_- •
26 0700 24 Y 2.90 -------_-
27 0700 24 Y 3.10 6.70 29.00 758.00 4.86 126.001- <0.1 •
28 0700 24El 3.10 -�-----_-
29 0700 24 3.10
•
30 0700 24 Y 3.00 __--_--_- •
31 0700 24 N 2-80 -------_- •
AVERAGE 2.75 6.88 25.50 634.50 4.89 121.50 11.35 <0.1
MAXIMUM 3.20 7.10 29.00 758.00 5.26 132.00 19.10 <0.1 _- •
MINIMUM 1.30 6.70 22.00 524.00 4.27 103.00 6.30 <0.1 •
Imp.(C)/Grab(G) G C C C C G G •
�,iiONTHLY LIMIT 6.0 to10.e N/A 1568/313 N/A 174/348 N/A <0.1 N/A
•
•
•

•
•
(Si
AshevillP
• * ,„x2.78,8„
Nx278586
• ETS
8)350-9364
8)
350-9368
•
• Environmental Testing Solutions,Inc.
• Certificate of Analysis
• Project name: Feldspar Project number: 150603.504
•
Collection date: 3-Jun-15
• Date received: 3-Jun-15
• Sample identification: Effluent-Composite Sample number: 126574
•
• Parameter Method Result RL Units Date
Analyzed Analyst Footnotes
• BOD,5 day SM 5210 B 4.2 2.0 mg/L 4-Jun-15 Al
• Solids,Total Suspended SM 2540 D <17 17 mg/L 4-Jun-15 Al
Ammonia Nitrogen SM 4500 NH3 D 0.24 0.10 mg/L 4-Jun-15 KEK
• Chemical Oxygen Demand HACH 8000 <50 50 mg/L 10-Jun-15 KEK
• Fluoride,Total 300.0 6.12 2.0 mg/L 9-Jun-15 LJW 1
Total Kjeldahl Nitrogen 351.2 0.58 0.10 mg/L 12-Jun-15 LDP 1
• Nitrate+Nitrite as N SM 4500-NO3 H 0.39 0.10 mg/L 8-Jun-15 REH 1
• Total Nitrogen Calculation 0.97 0.10 mg/L 12-Jun-15 LDP 1
Total Phosphorus 200.7 <0.050 0.050 mg/L 16-Jun-I5 MLR 1
• Total Organic Carbon SM 5310 B 5.37 2.00 mg/L 9-Jun-15 LJW 1
• Aluminum 200.7 0.41 0.500 mg/L 16-Jun-15 MLR 1
Barium 200.7 0.025 0.010 mg/L 16-Jun-15 MLR 1
• Boron 200.7 <0.10 0.10 mg/L 16-Jun-15 MLR 1
• Iron 200.7 0.93 0.050 mg/L 16-Jun-IS MLR 1
Magnesium 200.7 2.5 0.050 mg/L 16-Jun-15 MLR 1
• Molybdenum 200.8 0.218 0.005 mg/L 16-Jun-15 DER 1
• Manganese 200.7 <0.010 0.010 mg/L 16-Jun-15 MLR 1
Nickel 200.7 0.026 0.010 mg/L 16-Jun-15 DER 1
• Zinc 200.8 <0.010 0.010 mg/L 16-Jun-15 DER 1
•
•
•
•
•
•
•
• Footnotes:
ID RL=Reporting Limit. Values are reported down to the Reporting Limit only.
• 1. Sample analzyed by Rogers&Callcott Environmental.
•
0
• Date reviewed: CAP•lq•ks NC Certification Number: 600
Data reviewed by: Kelley E.Keenan SC Certification Number: 99053
• NC Drinking Water Certification Number: 37786
• Signature:
• This report should not be reproduced,exept in its entirety,without the written consent of Environmental Testing Solutions,Inc.
The results in this report relate only to the samples submitted for analysis.
•
•

•
•
•
• Rogers &Callcott •
ENVIRONMENTAL Laboratory Services •
•
Laboratory Report •
•
Client Environmental Testing Solutions Project: Feldspar •
Kelley E.Keenan Work Order: 5060282 •
351 Depot St. Received: 06/05/2015 09:40 •
Asheville,NC 28801-4310
•
•
Dear Client: •
Rogers and Callcott appreciates the opportunity to be of service to you. The attached laboratory services report includes analytical results and chain of •
custody for samples that were received on June 05,2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted,all analyses
performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval •
for each test method unless otherwise qualified. Estimated uncertainty is available upon request. •
Privileged/Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee,or •
the person responsible for delivering to the person addressed,you may not copy or deliver this message to anyone else. If you receive this message by
mistake,please notify Rogers and Callcott immediately. •
We strive to provide excellent service to our clients. Please contact Amy Ashley,your Project Manager,at [e-mail] or •
(864)-335-4962 if you have any questions about this report. •
•
•
•
•
•
•
•
•
Report Approved By: •
0/Thir J •
•
•
Amy Ashley •
Project Manager
•
•
This report may not he reproduced,except in full,without written permission front Rogers&Callcott,Inc. •
PO Box 5655 1 Greenville,SC 29606 1426 Fairforest Way I Greenville,SC 29607 I main 864.232.1556 I fax [phone] rogersandcallcott.com •
an employee-owned company
•
•
age o 10 • •
•

•
•
• (0---1. Rogers &Callcott
• ENVIRONMENTAL
• South Carolina Greenville Laboratory Identification 23105
• South Carolina Columbia laboratory Identification 40572
Certificate of Analysis North Carolina Laboratory Certification Number 27
• North Carolina Drinking Water Lab Number 45710
NELAP Utah Certificate Number SC000042014-1
• Georgia Drinking Water Lab ID 880
• Client Environmental Testing Solutions Project: Feldspar
• Kelley E.Keenan Work Order: 5060282
351 Depot St. Received: 06/05/2015 09:40
• Asheville,NC 28801-4310
•
• Sample Number Sample Description Matrix Sampled Type
• 5060282-01 Feldspar Effluent Composite Wastewater 06/03/15 07:11 Composite
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
• PO Box 5655 I Greenville,SC 29606 1426 Fairforest Way I Greenville,SC 29607 I main 864.232.1556 I fax [phone] rogersandcallcott.com
• an employee-owned company
06.?8/2015 09:52 This report may not he reproduced,except in MI,without written permission from Rogers R C'allcon,Inc.
• `age o 1
•

•
•
Mji
Rogers &Callcott •
::t+ -moi ! ENVIRONMENTAL •
•
Environmental Testing Solutions Project: Feldspar •
351 Depot St. Work Order: 5060282
Asheville,NC 28801-4310 Reported: 06/18/15 09:52 •
•
Sample Data •
Sample Number 5060282-01 •
Sample Description Feldspar Effluent Composite collected on 06/03/15 07:11 •
Reporting •
Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch
General Chemistry Parameters •
Fluoride 6.12 2.00 mg/L 20.0 06/09/15 16:46 EPA 300.0 LJW B5F0369 •
Nitrate-Nitrite as N 0.39 0.10 mg/L 1.00 06/08/15 15:13 SM4500NO3H-2011 REF] B5F0296 •
Total Kjeldahl Nitrogen 0.58 0.10 mg/L 1.00 06/12/15 19:31 EPA 351.2 LDP B5F0212 •
Total Nitrogen(TKN+Nitrate+Nitrite) 0.97 0.10 mg/L 1.00 06/12/15 19:38 Calculation LDP B5F0279
Total Organic Carbon 5.37 2.00 mg/L 2.00 06/09/15 13:55 SM 53100-201I LJW B5F0312 •
Total Metals •
Aluminum 0.41 0.050 mg/L 1.00 06/16/15 16:59 EPA 200.7 MLR B5F0427 •
Barium 0.025 0.010 mg/L 1.00 06/16/15 16:59 EPA 200.7 MLR B5F0427 •
Boron ND 0.10 mg/L 1.00 06/16/15 16:59 EPA200.7 MLR B5F0427 •
Iron 0.93 0.050 mg/L 1.00 06/16/15 16:59 EPA 200.7 MLR B5F0427
Magnesium 2.5 0.050 mg/L 1.00 06/16/15 16:59 EPA200.7 MLR B5F0427 •
Manganese 0.218 0.005 mg/L 1.00 06/16/15 18:36 EPA 200.8 DER B5F0554 •
Molybdenum ND 0.010 mg/L 1.00 06/16/15 18:36 EPA 200.8 DER B5F0554
Nickel 0.026 0.010 mg/L 1.00 06/16/15 18:36 EPA200.8 DER B5F0554 •
Total Phosphorus as P ND 0.050 mg/L 1.00 06/16/15 16:59 EPA 200.7 MLR B5F0427 •
Zinc ND 0.010 mg/L 1.00 06/16/15 18:36 EPA200.8 DER B5F0554 •
•
•
•
•
•
•
•
•
•
•
•
•
•
PO Box 5655 I Greenville,SC 29606 1426 Fairforest Way I Greenville,SC 29607 I main 864.232.1556 I fax [phone] rogersandcallcott.com •
an employee-owned company •
06/182015 09:52 This report may not he reproduced,except in.Mdl,without written permission front Rogers it('allcoit,Inc. •
Page 3 of 10
0

•
••
ii'i.�. a Rogers &Callcott
• :'a . d.._, ENVIRONMENTAL
•
• Environmental Testing Solutions Project: Feldspar
351 Depot St. Work Order: 5060282
• Asheville,NC 28801-4310 Reported: 06/18/15 09:52
•
• General Chemistry Parameters
• Quality Control Summary
• Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
• Batch B5F0212-EPA 351.2-TKN
•
• Blank(B5F0212-BLKI)
• Total Kjeldahl Nitrogen ND 0.10 mg/L
• Blank(B5F0212-BLK2)
• Total Kjeldahl Nitrogen ND 0.10 mg/L
• LCS(B5F0212-BS1)
Total Kjeldahl Nitrogen 4.89 0.10 mg/L 5.00 98 90-110
• LCS(B5F0212-BS2)
• Total Kjeldahl Nitrogen 4.70 0.10 mg/L 5.00 94 90-110
• Batch B5F0296-General Prep-Wet Chem KL
•
• Blank(B5F0296-BLKI)
• Nitrate-Nitrite as N ND 0.10 mg/L
• Blank(B5F0296-BLK2)
• Nitrate-Nitrite as N ND 0.10 mg/L
• LCS(B5F0296-BS1)
Nitrate-Nitrite as N 2.13 0.10 mg/L 2.00 106 85-115
•
• Batch B5F0312-General Prep-TOC
• Blank(B5F0312-BLKI)
• Total Organic Carbon ND 1.00 mg/L
• LCS(B5F0312-BSI)
• Total Organic Carbon 5.27 1.00 mg/L 5.00 105 85-115
• Batch B5F0369-General Prep-IC
• Blank(B5F0369-BLKI)
• Fluoride ND 0.10 mg/L
•
•
•
• PO Box 5655 I Greenville,SC 29606 1426 Fairforest Way I Greenville,SC 29607 I main 864.232.1556 I fax [phone] rogersandcallcott.com
• an employee-owned company
• 0648,2015 09:52 This report may not he reproduced,except in fill,without written permission from Rogers it C'crllcon,Inc.
Page 4-of 10
•

•
•
(0.-- = Rogers &Callcott •
ENVIRONMENTAL •
•
Environmental Testing Solutions Project: Feldspar •
351 Depot St. Work Order: 5060282
Asheville,NC 28801-4310 Reported: 06/18/15 09:52 •
•
General Chemistry Parameters •
Quality Control Summary •
Reporting Spike Source %REC RPD •
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
Batch B5F0369-General Prep-IC •
•
LCS(B5F0369-BS1) •
Fluoride 0.48 0.10 mg/L 0.500 97 90-110 •
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
PO Box 5655 I Greenville,SC 29606 1426 Fairforest Way I Greenville,SC 29607 I main 864.232.1556 I fax [phone] rogersandcallcott.com •
an employee-owned company •
06'182015 09:52 This report may not he reproduced,except in,Ml,without written permission from Rogers it("oilcan,Inc. •
Page 5 of 10
•

•
•
• �-- 1 Rogers &Callcott
• %.`411- .i ENVIRONMENTAL
•
Environmental Testing Solutions Project: Feldspar
• 351 Depot St. Work Order: 5060282
• Asheville,NC 28801-4310 Reported: 06/18/15 09:52
•
• Total Metals
• Quality Control Summary
• Reporting Spike Source %REC RPD
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
• Batch B5F0427-EPA 200.7
•
•
Blank(B5F0427-BLKI)
Aluminum ND 0.050 mg/L
•
Barium ND 0.010 mg/L
• Boron ND 0.10 mg/L
• lron ND 0.050 mg/L
Magnesium ND 0.050 mg/L
• Total Phosphorus as P ND 0.050 mg/L
• LCS(B5F0427-BSI)
• Aluminum 1.06 0.050 mg/L 1.00 106 85-115
• Barium 1.01 0.010 mg/L 1.00 101 85-115
Boron 1.00 0.10 mg/L 1.00 100 85-115
• Iron 1.08 0.050 mg/L 1,00 108 85-115
• Magnesium 1.05 0.050 mg/L 1.00 105 85-115
• Total Phosphorus as P 0.994 0.050 mg/L 1.00 99 85-115
• Batch B5F0554-EPA 200.8
• Blank(B5F0554-BLKI)
• Manganese ND 0.005 mg/L
Molybdenum ND 0.010 mg/L
•
Nickel ND 0.010 mg/L
• Zinc ND 0.010 mg/L
• LCS(B5F0554-BSI)
• Manganese 0.200 0.005 • mg/L 0.200 100 85-115
Molybdenum 0.198 0.010 mg/L 0.200 99 85-115
•
Nickel 0.203 0.010 mg/L 0.200 102 85-115
• Zinc 0.210 0.010 mg/L 0.200 105 85-115
•
•
•
•
•
•
• PO Box 5655 I Greenville,SC 29606 1426 Fairforest Way I Greenville,SC 29607 I main 864.232.1556 I fax [phone] rogersandcallcott.com
• an employee-owned company
• 06/18,2015 09:52 This report may not he reproduced,except infill,without written permission front Rogers&edictal,Inc.
-..age.p 1
•

•
•
el Rogers &Callcott •
�� • ■ ENVIRONMENTAL •
•
Environmental Testing Solutions Project: Feldspar
351 Depot St. Work Order: 5060282 •
Asheville,NC 28801-4310 Reported: 06/18/15 09:52 •
•
Sample Preparation Data •
•
Parameter Batch Sample ID Prepared Analyst •
EPA 200.7 Metal Digestion •
EPA 200.7 B5F0427 5060282-01 06/I 1/2015 16:45 MLR
EPA 200.8 Metal Digestion •
EPA 200.8 B5F0554 5060282-01 06/16/2015 09:11 DER •
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
PO Box 5655 I Greenville,SC 29606 1426 Fairforest Way I Greenville,SC 29607 I main 864.232.1556 i fax [phone] rogersandcallcott.com •
-- an employee-owned company •
06/18/2015 09:52 This report inoy not he reproduced,escepi in lull,without written permission from Rogers it Callum,Inc.
Page 7 Of 10 •
•

•
• a:r
• ` �� �`�� Rogers &Callcott
• , -, ENVIRONMENTAL
•
Environmental Testing Solutions Project: Feldspar
• 351 Depot St. Work Order: 5060282
• Asheville,NC 28801-4310 Reported: 06/18/15 09:52
•
• Data Qualifiers and Definitions
•
• ND Analyte NOT DETECTED at or above the reporting limit
• NR Not reported
• RPD Relative Percent Difference
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
• PO Box 5655 I Greenville,SC 29606 1 426 Fairforest Way I Greenville,SC 29607 I main 864.232.1556 1 fax [phone] rogersandcallcott.com
• — an employee-owned company
• 0648/2015 09:52 This report may not he reproduced,ercepr in 0idf,without written permission front Rogers 8 Callcon Inc.
Page 8 of 10
•

•
s O610 6 abed .
s N - 7J viz W 77 r-• v, 0 N 3 (7J >DD Q n n 3
g I- I- • 1- • D 0rfi CU 1:3
d fD a �' ' r
• = Z Z \ p ? D A. H rt LF
ru Ai C p p m Q 7c O 0. —I IA Z I
°' mDJ
m7o m ;t rD :�- -- --
• �^ O O O , A vi
p 0' ,., nvi
II w nJ
• qm V ml
0 (D
_CL ?
s Elm 85
a vIA
nom.
°° rt1 x//1/1
2 it0 c) 4' Z k n VI
a 0 O 0 6 0 ,,, p w �°
— n
O Qj
tinw
• 1-1 D D -DI 3:21
D N n,
3 N m ' rn di g
• z 0m P N v c ,
• ❑ m m ? 70 N Q N r-
s m m 'O o
p m n mm V n r'
o
III ,3 m m 4n O "'
O O [� Z rSo No
•
• o z
s ' 4 Total Number of Containers 0
fic' -I,
• , Parameter(s) 4. n
• = ?‹ Floorucut v)• C
• Cil A+ned, mI m� rd
• a 'TOL-(4 0 0.*C 0 N;i7R-1n
• 0
• 4 T�Tp c o
• 00 00
• 0
Li D D 3 O O o
m m O
N N N m Ln xi
�+ p O C a d 7C
s o + + 1^--,^ Cl n m D to V, n n 0 -9
" 0 co:), 1 ! 1 I 3 3 0 0 O O
•
' O (� 3 � v H Z o • d bi rD `�° m
m n 6 n m 0 0 0 m ro > > a o m
n + m rD 2 " m rD rD
• `D 7 O N �, --? 2 G7 T m V o .3 C_ - IN I0;
• rl 1 1 I let IGl C O IZ V''''4\
• .'W
�' 3 ur , 3 n. �1
r
- o n . as v Im
• O N Q. c Z tri I' N
y,\ ` r 7c 1 itG
•
• m el-
•
•

•
•
• It Rogers &Callcott
• ENVIR NMENTAL
• Sample Receipt Verification
• , V• Date (..,'
Work
Client: Received: C t 1 ) Order: D
()U-2,../
•
• Carrier Name: Client Fed i _ �(U S 1///7;;; r Courier Field Services Other:
• Tracking Number: V U I Z�n I ��C1
•
Y
• Receipt Criteria e N
o Comments
•
• Shipping container/cooler intact? Damaged Leaking Other:
• Custody seals intact?
• COC included with samples?
• COC signed when relinquished and received?
• Sample bottles intact? Damaged Leaking Other:
• Sample ID on COC agree with label on bottle(s)? r
•
• Date/time on COC agree with label on bottle(s)?
Number of bottles on COC agrees with number of bottles received? '
•
• Samples received within holding time?
• Sample volume sufficient for analysis?
• Y VOA vials free of headspace(<6mm bubble)?
• Samples cooled? Temp at receipt recorded on COC
• Temp measured with IR thermometer-SN:97050067 Cold Packs Dry Ice None
Samples requiring pH preservation at proper pH? 0oi4e- ea_ Mid Note: Samples for metals analysis may be preserved upon receipt in the lab.
• Samples dechlorinated for parameters requiring chlorine removal at
the time of sample collection?
•• If in-house preservation used — r ,L1)0 t,e01
HCL H3PO4
• H,SO4 NaOH
• HNO3 Other
• Co ents: '
• �k 11 i
2 14 1A.17 4� 6� n W '7,
• Were non-conformance issues noted at sample receipt? Yes or No
• Non-Conformance issue other than noted above: -
•
•
• Revised July 2014 Completed by:
•
• Page 10 of 10
•

•
•
•
• a 9 c 5 o. th A. w M =Item Number me ne
• m 5 o° o E to oEa� z Z m <7
• "•
717
• 2r. 0 ,,_
~ 00 Flo
• ,-< -0.,-„,... .. ;' •"
'� r7 i:.'
• z 0 z c' qa• ,,,
c N
• ry 0 G=Grab,C=Composite N n -,
• aI'l .r
.� W 3 rya
�- Sample Number Ay C `cm n T ?
• • ETS Use Onlye ,.
N 3 \ v^ Y
• rioe
• 1 Water,Solid,
Matrix: t,iquid '
c o-
• 0 S Date Collected L
•
N (MM/DD/YY)
• Q O — Time Collected
• 0 6 —
(HH:MM)
• W W g (p #Containers
Cll. 7
_ Unpreserved ,o .d ,y '
O,• Q H,SO4 O c o
CA
O0 HN0 ? o '
• ( HCl C •n i 1c A /�1G NaOH+Ascorbic < •n d• b Na2S203•
cr
ft g a „I Q j 42, LAs, % 11
• picx by 2 O
• y �C
7 EE 3
o,
• s d 1—.
o .Vg.
_
v -411 c 9 R w PD
• •
w o o
22 i
•
•
•
•

•
•
lETS PO Box 7565
•
Asheville,NC 28802
Phone: [phone]
• Fax: [phone]
•
• Environmental Testing Solutions,Inc. Certificate of Analysis
• Project name: Feldspar Project number: 150604.501
•
• Collection date: 4-Jun-15
Date received: 4-Jun-15
•
• Sample identification: Effluent-Grab _ Sample number: 126584
• Parameter Method Result RL Units Date
Analyzed Analyst Footnotes
•
ADMI Color at Original pH SM 2120 E <25.0 25.0 mg/L 5-Jun-15 LJW 1
• ADMI Color at pH=7.6 SM 2540 D <25.0 5.0 mg/L 5-Jun-15 LJW 1
•
•
•
•
•
•
•
•
•
•
•
S
•
•
•
•
•
•
• Footnotes:
RL=Reporting Limit. Values are reported down to the Reporting Limit only.
• 1. Sample analzyed by Rogers&Callcott Environmental.
•
•
• Date reviewed: 0(•t i-K NC Certification Number: 600
• Data reviewed by: Kelley E.Keenan SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
• Signature:
• This report should not be reproduced,exept in its entirety,without the written consent of Environmental Testing Solutions,Inc.
• The results in this report relate only to the samples submitted for analysis.
•

•
•
•
Rogers &Callcott • °''- d. •
-G ENVIRONMENTAL r? .., Laboratory Services •
•
Laboratory Report •
•
Client Environmental Testing Solutions Project: Feldspar •
Kelley E.Keenan Work Order: 5060280 •
351 Depot St. Received: 06/05/2015 09:40
Asheville,NC 28801-4310 •
•
•
Dear Client: •
Rogers and Callcott appreciates the opportunity to be of service to you, The attached laboratory services report includes analytical results and chain of •
custody for samples that were received on June 05,2015. Rogers and Callcott maintains a formal QA/QC program. Unless otherwise noted,all analyses
performed under NELAP certification have complied with all the requirements for the TNI standard. The analyses met the QA/QC confidence interval •
for each test method unless otherwise qualified. Estimated uncertainty is available upon request. •
Privileged/Confidential information may be contained in this report and is intended only for the use of the addressee. If you are not the addressee,or •
the person responsible for delivering to the person addressed,you may not copy or deliver this message to anyone else. If you receive this message by
mistake,please notify Rogers and Callcott immediately. •
We strive to provide excellent service to our clients. Please contact Amy Ashley,your Project Manager,at [e-mail] or •
(864)-335-4962 if you have any questions about this report. •
•
•
•
•
•
•
•
•
Report Approved By: •
•
•
•
Amy Ashley •
Project Manager
•
•
This report may nor he reproduced,except in frill,without written permission from Rogers&Callcott,Inc. •
PO Box 5655 I Greenville,SC 29606 1426 Fairforest Way I Greenville,SC 29607 1 main 864.232.1556 I fax [phone] rogersandcallcott.com •
an employee-owned company
•
•
Page 1 of 7 •
410

•
• Rogers &Callcott• •y
• • - ENVIRONMENTAL
• South Carolina Greenville Laboratory Identification 23105
South Carolina Columbia Laboratory/dentif cation 40572
•
Certificate of Analysis North Carolina Laboratory Certification Number 27
• North Carolina Drinking Water Lab Number 45710
NELAP Utah Certificate Number SC000042014-1
Georgia Drinking Water Lab ID 880
• Client Environmental Testing Solutions Project: Feldspar
• Kelley E.Keenan Work Order: 5060280
351 Depot St. Received: 06/05/2015 09:40
• Asheville,NC 28801-4310
•
• Sampte Number Sample Description Matrix Sampled Type
• 5060280-01 Feldspar Effluent Grab Wastewater 06/04/15 07:15 Grab
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
• PO Box 5655 1 Greenville,SC 29606 1 426 Fairforest Way I Greenville,SC 29607 I main 864.232.1556 I fax [phone] rogersandcallcott.com
• an employee-owned company
0tf'!Z7Q/5 13:31 This report in ay not he reproduced,except in ill,without written permission f+•om Xogerr R C'a!!c»a,Inc.
• Page 2 of 7
•

•
•
Rogers &Callcott •
ENVIRONMENTAL •
•
Environmental Testing Solutions Project: Feldspar •
351 Depot St. • Work Order: 5060280
Asheville,NC 28801-4310 Reported: 06/17/15 13:31 •
•
Sample Data •
Sample Number 5060280-01 •
Sample Description Feldspar Effluent Grab collected on 06/04/15 07:15
•
Reporting •
Parameter Result Limit Units DF Analyzed Method Flag Analyst Batch
General Chemistry Parameters •
ADMI Color at original pH ND 25.0 Color Units 1.00 06/05/15 09:55 SM 2120E-1993 LJW B5F0219 •
ADMI Color at pH=7.6 ND 25.0 Color Units 1.00 06/05/15 09:55 SM 2120E-1993 LJW B5F0219 •
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
PO Box 5655 I Greenville,SC 29606 1426 Fairforest Way I Greenville,SC 29607 I main 864.232.1556 I fax [phone] rogersandcallcott.com •
-- an employee-owned company •
06471015 13:31 This report may not he reproduced,except infill,without written permission,front Rogers&C'allcot.Inc. •
Page 3 of 7
•

•
• =
• fri Rogers &Callcott
• '�- j ENVIRONMENTAL
• Environmental Testing Solutions Project: Feldspar
• 351 Depot St. Work Order: 5060280
• Asheville,NC 28801-4310 Reported: 06/17/15 13:31
•
• General Chemistry Parameters
• Quality Control Summary
Reporting Spike Source %REC RPD
•
Parameter Result Limit Units Level Result %REC Limits RPD Limit Flags
• Batch B5F0219-General Prep-Wet Chem
•
• Blank(B5F0219-BLKI)
ADMI Color at original p1-1 ND 25.0 Color Units
• ADMI Color at pH=7.6 ND 25.0 Color Units
• LCS(B5F0219-BSI)
• ADMI Color at original pH 103 25.0 Color Units 100 103 85-115
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
• PO Box 5655 1 Greenville,SC 29606 1426 Fairforest Way I Greenville,SC 29607 I main 864.232.1556 I fax [phone] rogersandcallcott.com
• — an employee-owned company
06,17/2015 13:31 This report may not he reproduced,except Infill,without written permission from Rogers ct•C'allcon Inc.
• Page 4 of 7
•

•
•
Rogers &Callcott
1 ENVIRONMENTAL
•
Environmental Testing Solutions Project: Feldspar •
351 Depot St. Work Order: 5060280
Asheville,NC 28801-4310 Reported: 06/17/15 13:31 •
•
Data Qualifiers and Definitions •
•
ND Analyte NOT DE t ECTED at or above the reporting limit •
NR Not reported •
RPD Relative Percent Difference •
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
•
PO Box 5655 1 Greenville,SC 29606 1 426 Fairforest Way I Greenville,SC 29607 1 main 864.232.1556 I fax [phone] rogersandcallcott.com •
-- — --- an employee-owned company •
06.1172015 13:31 This report may not he reproduced,except in jedl,without written permission from Rogers K-C'alkon,Inc. 1 •
Page 5 of
•

L Jo g abed 1 •
v - O --1 3 CD C. — n 3 r •
vm �^ m Wm ~ D 3
•v Cl. �
g r r r TIC �• ro oo •
ea A p p > -i '^ aii
y c c 1 c � vn (.9 a O 3 � O �;
d m m m aVI
<• aY T •
ti 0 C rn r^ c'43.
m N
R r A
e: � 010 � qz 9 N n v' (� •
`g C •
g I $ U'1
3 0 ( )
m �1 a s LA w�w •
N 3 av Vl
A •
El ti, TZ 91 •
Z _ d 'n �Aj /�/ /
ox•' ` r�
•
R. 33
H 0 N•
N •
❑ D -D-1 r6+C D 3 — A � Z
m m m •
m . , m LA- 31 0 L v r..i z0 •
'° _0 n r � 3 � Dim •
x, vK, T- f ,
El 00 m 91 m A m N m Pt17' °'
n n n n Z 3 n •
m rn m_
•
d 0 0 0 1 `$ a •
Z
AD' CO `a `c •
❑ � `' — _ Z •
o ` Total Number of Containers
•
s 1• n •
c
Parameter
(s)
c
f C
`I CO l of - •
O •
c ' - . . ' ' _ •
-.1-1
•
C D _ - m •
rn�T (J
m ) m Xi
—t:- 0 •
c-7-, •
a • n n
3 3 3 3
'° •
a v
D D 3 g •
0 0 p •
Q. .+ 3 m N r(9
3 T v � 7K
M m ': O ni n"i O n m D in in n n ?+ Q ••
0 0 F 1111 3 3 > > 0 o v
a D n V 0 Z2SZ 6i b'i (D '' m •
Qa o n 3 °t co t,,, m ro > > fl 1Da �o
`o P 07 n - •• 2 . g' < 2i 1 1
v ry 5 o m m 5 `G H , ` •
'u O tp 2 11 iii Jo, C t0 2 Z V \ •
fD
ro 3 � Da o o •
_: 1 n a r 3
•
°1• n N
rD r 7t � I v •
7 •O1 D
r; ria . @0 IQ
M •
•
•

•
•
Pr Rogers &Callcott •
ENVIR NMENTAL •
•
Sample Receipt Verification/. V
.
Date / Worka.; •
Client: Received: (..,' c t i Order: •
ot/rNo
Carrier Name: Client Fed (..0
S C 1 9.51 a' Courier Field Services Other: •
Tracking Number: vzq
•
•
Y
•
Receipt Criteria e a A Comments
Shipping container/cooler intact? Damaged Leaking Other: •
Custody seals intact?
•
COC included with samples? •
COC signed when relinquished and received? • •
Sample bottles intact? Damaged Leaking Other: •
•
Sample ID on COC agree with label on bottle(s)? •
Date/time on COC agree with label on bottle(s)? •
Number of bottles on COC agrees with number of bottles received? 4 •
Samples received within holding time?
3(.1 •
Sample volume sufficient for analysis? •
VOA vials free of headspace(<6mm bubble)? J� •
Temp at receipt recorded on COC •I .
Samples cooled? Temp measured with IR thermometer-SN.97050067 Cold Packs Dry Ice None •
Samples requiring pH preservation at proper pH? •
Note Samples for metals analysis may be preserved upon receipt in the lab.
Samples dechlorinated for parameters requiring chlorine removal at •
the time of sample collection?
•
If in-house preservation used — record Lot# •
HCL HaPO4
H2SO4 NaOH •
HNO3 Other •
Comments: ID
•
I •
Were non-conformance issues noted at sample receipt? Yes or •
Non-Conformance issue other than noted above:
•
Revised July 2014 Completed by: •
••
Page 7 of 7 •
0

•
•
•
•
w d , m c, Q Item Number .ti r.rj, «
It: $ o E o •
z z- m ,rs
n m = co 3 e w, 1? .y •
0 o ."• o 'I 3 3 O < t'. f' ' •' •
o
3 ° rrb N `"� .
O
'� 0r W ,../. •
z O z "' m w
ta y '° •
.\ 7y \ C tQ •
\\\. G=Grab,C=Composite N ��}-
^ 0r. a.
` � tN 00 r r
lc- Sample Number .17p ; rz
(GnD o h, 7's ••
ETS Use Only p 00 7 r } p
0, n •
4
�'
Matrix: Water,Solid,
X
•Liquid
n ..--
0 A1/4
•
R ,1 Date Collected
(MM/DD/YY) n •
, .
\ J— $ Time Collected
C (HH:MM) •
k at 1- #Containers
m •
— Unpreserved
,b b br>1 �
( 1 •
0 H2SO4 M O o b a �' O
-n gi HNO3t.t,
z R
N HCl ta 00Q�,,,���� o :

NCDENR
North Carolina Department of Environment and Natural Resources
Pat McCrory Donald R. van der Vaart
Governor Secretary
July 14, 2015
Jerry Prosser
The Quartz Corp USA
530 Altapass Road
Sprue Pine,NC 28777
Subject: Acknowledgement of Permit Renewal
Permit NC0000353
Mitchell County
Dear Permittee:
The NPDES Unit received your permit renewal application on July 13, 2015. A member of the
NPDES Unit will review your application. They will contact you if additional information is required to
complete your permit renewal. You should expect to receive a draft permit approximately 30-45 days
before your existing permit expires.
If you have any additional questions concerning renewal of the subject permit, please contact Tom
Belnick at(919)807-6390.
Sincerely,
WrewTkeolfaroir
Wren Thedford
Wastewater Branch
cc: Central Files
Asheville Regional Office
NPDES Unit
1617 Mail Service Center,Raleigh,North Carolina 27699-1617
Location:512 N.Salisbury St.Raleigh,North Carolina 27604
Phone:[phone] Fax:[phone]/Customer Service:1-877-623-6748
Internet::www.ncwater.orq
An Equal Opportunity Affirmative Action Employer