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NC0088692_Renewal (Application)_20161209
1 PAT MCCRORY IVO Governor DONALD R. VAN DER VAART Secretary Water Resources S. JAY ZIMMERMAN Director ENVIRONMENTAL QUALITY December 09,2016 Mr. Jerry Sparks, President Sparks Oil Company 412 N. Scales Street Reidsville,NC 27320-2909 Subject: Permit Renewal Application No. NC0088692 J.W. Smith/Camp Spring 76 Caswell County Dear Mr. Sparks: The Water Quality Permitting Section acknowledges receipt of your permit application and supporting documentation received on November 22, 2016. The primary reviewer for this renewal application is Derek Denard. The primary reviewer will review your application, and he will contact you if additional information is required to complete your permit renewal. Per G.S. 150B-3 your current permit does not expire until permit decision on the application is made. Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit. Please respond in a timely manner to requests for additional information necessary to complete the permit application. If you have any additional questions concerning renewal of the subject permit,please contact.Mr. Denard at 919-807-6307 or Derek.Denard@ncdenr.gov. • Sincerely, ?area 7 ed,'�o'd Wren Thedford Wastewater Branch cc: Central Files NPDES Winston-Salem Office State of North Carolina I Environmental Quality I Water Resources 1617 Mail Service Center I Raleigh,North Carolina 27699-1617 919-807-6300 Air „ PYRAMID ENVIRONMENTAL&ENGINEERING, P.C. November 14, 2016 Mrs. Dina Sprinkle NCDEQ/DWQ/Point Source Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Re: NPDES Permit Renewal Request for JW Smith/Camp Springs 76 Groundwater Remediation System 8920 Cherry Grove Road Reidsville, Caswell County,NC NPDES Permit# NC0088692 Incident#21685 RECEIVEDINCDEQ/DINR NOV 22 2016 Dear Mrs. Sprinkle: Water Quality As requested by Sparks Oil Company, Pyramid Environmental & Engineeriri ;nP@e1it rl completed a renewal request package for the NPDES Permit # NC0088692. Enclosed please find the NPDES Permit renewal request package containing all required documentation. The Camp Springs 761.1W Smith remediation system has not been changed since the issuance of the current NPDES permit that expires on May 31, 2017. Please note that there is an incorrect number of carbon vessels listed in the current permit. The new permit should list four (4) carbon vessels. Please see the documents in the enclosed Residuals Management Plan regarding the carbon vessel number. If you have any questions or need any additional information regarding this permit renewal request,please call me at 336-335-3174. Sincerely, kfAvowel; Mika Trifunovic Project Manager Enclosures:NPDES Permit Renewal Package P.O.Box 16265•Greensboro,.NC 27416 503 Industrial Ave•Greensboro,NC 27406 Phone(336)335-3174•Fax(336)691-0648•Toll Free(866)545-9507 Email:Info@pyramidenvironmental.com www.pyramidenvironmental.com ' ` NC DENR/DWQ/NPDES Renewal Application Checklist , The following items are REQUIRED for all renewal packages: xi A cover letter requesting renewal of the permit and documenting any changes at the facility since issuance of the last permit. Submit one signed original and two copies. The completed application form (copy attached), signed by the permittee or an Authorized /Representative. Submit one signed original and two copies. N..0 If an Authorized Representative (such as a consulting engineer or environmental consultant) prepares the renewal package,written documentation must be provided showing the authority delegated to the Authorized Representative (see Part II.B.11.b of the existing NPDES permit). A narrative description of the sludge management plan for the facility. Describe how sludge (or other solids) generated during wastewater treatment are handled and disposed. If your facility has no such plan (or the permitted facility does not generate any solids), explain this in writing. Submit one signed original and two copies. The following items must be submitted by any Municipal or Industrial facilities discharging process wastewater: O Industrial facilities classified as Primary Industries (see Appendices A-D to Title 40 of the Code of Federal Regulations,Part 122) and ALL Municipal facilities with a permitted flow >_ 1.0 MGD must submit a Priority Pollutant Analysis (PPA) in accordance with 40 CFR Part 122.21. The above requirement does NOT apply to non-industrial facilities. Send the completed renewal package to: Mrs. Dina Sprinkle NC DENR/DWQ/Point Source Branch 1617 Mail Service Center Raleigh,NC 27699-1617 (919) 807-6304 Jr __ PYRAMID ENVIRONMENTAL&ENGINEERING, P.C. Authorization for NPDES Renewal Package Preparation I, Jerry Sparks, the president of Sparks Oil Company, authorize Pyramid Environmental & Engineering, P.C. to prepare the NPDES Renewal Package for the JW Smith/ Camp Springs 76 groundwater remediation system. (-----'" 'Olt lait iir.2'i 6 e/ par , Pres, ent of Sparks Oil Company . Date P.O.Box 16265•Greensboro,NC 27416 503 Industrial Ave•Greensboro,NC 27406 Phone(336)335-3174•Fax(336)691-0648•Toll Free(866)545-9507 Email:Info@pyrarnidenvironmental.com www.pyramidenvironmental.com NPDES PERMIT APPLICATION - SHORT FORM C - GW For discharges associated with groundwater treatment facilities. Mail the complete application to: N. C. Department of Environment and Natural Resources Division of Water Quality / NPDES Unit 1617 Mail Service Center, Raleigh, NC 27699-1617 NPDES Permit Number NC0088692 If you are completing this form in computer use the TAB key or the up - down arrows to move from one field to the next. To check the boxes, click your mouse on top of the box. Otherwise,please print or type. 1. Contact Information: Owner Name Sparks Oil Company Facility Name JW Smith / Camp Springs 76 remediation system Mailing Address 412 N Scales Street City Reidsville State / Zip Code NC / 27320-2909 Telephone Number (336)349-8231 Fax Number (336)349-9959 e-mail Address jerry@sparksoil.com 2. Location of facility producing discharge: Check here if same as above ❑ Street Address or State Road 8920 Cherry Grove Road City Reidsville State / Zip Code NC / 27320/0227 County Caswell 3. Operator Information: Name of the firm, consultant or other entity that operates the facility. (Note that this is not referring to the Operator in Responsible Charge or ORC) Name Pyramid Environmental & Engineering, P.C. Mailing Address PO Box 16265 City Greensboro State / Zip Code NC / 27416-0265 Telephone Number (336)335-3174 Fax Number (336)691-0648 4. Ownership Status: Federal ❑ State ❑ Private ® Public ❑ Page 1 of 3 C-GW 03/05 NPDES PERMIT APPLICATION - SHORT FORM C - GW For discharges associated with groundwater treatment facilities. 5. Products recovered: Gasoline ❑ Diesel fuel ❑ Solvents ❑ Other Petroleum contaminated groundwater 6. Number of separate discharge points: 1 Outfall Identification number(s) 1 7. Frequency of discharge: Continuous ® Intermittent ❑ If intermittent: Days per week discharge occurs: Duration: 8. Treatment System Design flow 0.009 MGD 9. Name of receiving stream(s) (Provide a map showing the exact location of each outfall, including latitude and longitude): Unnamed tributary of County Line Creek 10. Please list all additives to the treatment system, including chemicals or nutrients, that have the potential to be discharged. none 11. Is this facility located on Indian country? (check one) Yes ❑ No IE 12. Additional Information All applicants (including renewals): • A USGS topographical map (or copy of the relevant portion) which shows all outfalls • A summary of the most recent analytical results (effluent data, if available) containing the maximum values for each chemical detected NEW Applicants only: ✓ Engineering Alternative Analysis • Description of remediation treatment system components, capacities, and removal efficiency for detected compounds. • If the treatment system will discharge to a storm sewer, written approval from the municipality responsible for the sewer. • A list of any chemicals found in detectable amounts at the site, with the maximum observed concentration reported for each chemical (the most recent sample must be collected less than one year prior to the date of this application) • For petroleum-contaminated sites—Analyses for Volatile Organic Compounds (VOC) should be performed. Analyses for any fuel additives likely to be present at the site and for phenol and lead should also be performed. • For sites contaminated with solvents or other contaminants - EPA Method 624/625 analysis should be performed. Page 2 of 3 C-GW 03/05 • NPDES PERMIT APPLICATION - SHORT FORM C - GW For discharges associated with groundwater treatment facilities. 13. Applicant Certification I certify that I am familiar with the information contained in the application and that to the best of my knowledge and belief such information is true, complete, and accurate. Jerry Sparks President Printed -me of Person Signing Title � ii / SiOiar - o A 'licant � Date 'o h Carolina General Statute 143-215.6 (b)(2) provides that: Any person who knowingly makes any false atement representation, or certification in any application, record, report, plan, or other document files or required to be maintained under Article 21 or regulations of the Environmental Management Commission implementing that Article, or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under Article 21 or regulations of the Environmental Management Commission implementing that Article, shall be guilty of a misdemeanor punishable by a fine not to exceed $25,000, or by imprisonment not to exceed six months, or by both. (18 U.S.C. Section 1001 provides a punishment by a fine of not more than$25,000 or imprisonment not more than 5 years, or both, fora similar offense.) Page 3 of 3 C-GW 03105 uw ew LULL u7.40 0304.4 arr•}r[na U.I.L. riaut CciI J..1. fes.^' "-: ,t •1 'i.. ., "•''1' • I ri.. y`•1. • :'f ' .%.'1.\.;- ••'�4t'1 •`x••'7,1, 11:,..,/,:?.?•".:),;1•• r. �r • t / ..^,... � \Cs 777 f.';. • •• •• .yam �'• i •. :ter, ,%. ip` .• y ,:▪ ' f• +..1 ! , :. i '.y,L....4.,�,ti', yf:1„;n!se•,;•.j+'4'et.,':r'}4er"lr�+r:l • •r •l�; �•. ..,••••••Yi„;-..ii • •s I '•J� �... 1�``• -•'• ..1;:t... • r: i,."-t•x,{,"'i,•4;••1-'-'1". ..ro 'f''' '/4 �t r•'''{ 'ef ^%'Y°• '. Yr• .Y at, 'i .,,''•ti. 'Ir.. .:t- 1 ^ e r,:•'7 i ••1' •'y}.,;,,.1.'4.--::'..',3•Z,�, • _ ' ~I r fI''T \•::::Cr -_„r. Nt1• -'t,:" f. ;•11_ 'y 6.• rylq L y,. '•I :� • •L.,..j...;:.�'�,�, .tip • ✓m, Ml �y I )!r ; •f�. 1. .J •t��� •. „ ''' ') r ,J,;'i.„,,,,,,:, »I•e•!' ''' K.f':.:� �'4, J��'yyIS' 1.•. Y. • �!, . •v a' 1 'i-•• F {! �..•'ly' r �..,1•.:rl, •:,t't 0,,,„.,--..!--,..,.....1.t. .r:.t.,,,, •::.11,...„„!.,....E..../. '••.y..^!,p'iw� y•' .'` ,; / -•i:.j�.,,,,:•'•'•",l,-•f.:Y.c, ii:, r •1". :,'..? 5:• •••'I l' �'.•- 1.l'.{' �•._ .,.. 1 L .d 1 `L'y'•..•.C..L';r;r.�l,"rl %::-;,',, +�y1•'x,^rV 1."•`,...'i • t 1 "y: j'�•� y �,�.L i +:.• • • •• _ � • '+;.'+! ���' •y t,'.,Mem, ','� �•'.I'•.(�t"� 's.'t� ;!\7s • ':{`1l. '3 .i'.i •• •:�l'; EFFLUENT NPDES PERMIT NO. NC 0088692 DISCHARGE NO. 1 MONTH October YEAR 2016 FACILITY NAME J. W. Smith / Camp Springs 76 CLASS NA COUNTY Caswell CERTIFIED LABORATORY(1) Pace Analytical CERTIFICATION NO. 402 (list additional laboratories on the backside/page 2 of this form) OPERATOR IN RESPONSIBLE CHARGE(ORC)Danny Oldham GRADEP C-10ERTIFICATION NO. 991232 PERSON(S)COLLECTING SAMPLES Danny Oldham ORC PHONE 336-312-4283 CHECK BOX IF ORC HAS CHANGED ® NO FLOW/DISCHARGE FROM SITE* O Mail ORIGINAL and ONE COPY to: Ralit �� ATTN:CENTRAL FILES 2 x < r 6 DIVISION OF WATER QUALITY �r (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE 1617 MAIL SERVICE CENTER BY THIS SIGNATURE,I CERTIFY THAT THIS REPORT IS RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE. _ 50050 C0530 122417 I 34030 34371 81551 34010 77117 34531 77222 77226 34696 34694 77651 77224 01051 F E FLOW ENTER PARAMETER CODE ` I- EFF ]rt( ABOVE NAME AND UNITS 1, -Dichlo o- 1,3 5-Trim_thyl IS, BELOW 0 . c s Lead dg e i O a Toluene Pheno A `a N O. 0 G-a enzene Pro PY ` O U 6: 4I- MTBE Total Isopropyl 1,•,4-Tri -thyl benzen' O O A �i TSS Benzene Xylenes Ether benzene N•phthal=, e HRS HRS Y/B/N MGD mg/L Pg/L u9/L 119/L u9/L pg/L mg/L ug/L 119/L pg/L pg/L u9/L pg/L 119/L mg/L 1 N 0 2 N 0 3 N 0 4 N 0 5 N 0 6 N 0 7 N 0 8 N 0 9 N 0 '10 N 0 11 N 0 12°83° 1630 Y 0.0001 <2.5 <0.50 <0.50 <0.50 <1.0 <0.50 <0.50 <0.50 <0.50 <0.50 <2.0 17 <0.50 <0.50 <5.0 13 N 0 14 N 0 15 N 0 16 N 0 17 N 0 18 N 0 19 N 0 20 N 0 21 N 0 22 N 0 23 N 0 24 N 0 25 N 0 _ 26 N 0 27 N 0 28 N 0 29 N 0 30 N 0 31 N 0 AVERAGE 0.0001 MAXIMUM ' MINIMUM Comp.(C)/Grab(G) G G G G G G G ' G G G G G G G G Monthly Limit 20.0 9.5 0.60 48.5 335 5.5 6.5 0.19 195 315 165 150 None None one Single point totalizing flow meter is used at this remediation system DWQ Fonn MR-1.1 (11/04) • • • Facility Status:(Please check one of the following) All monitoring data and sampling frequencies meet permit requirements (including weekly averages,if applicable) Compliant All monitoring data and sampling frequencies do NOT meet permit requirements Noncompliant The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the permittee becomes aware of the circumstances. If the facility is noncompliant,please attach a list of corrective actions being taken and a time-table for improvements to be made as required by Part II.E.6 of the NPDES permit. "I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the system,or those persons directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete. I am aware that there are significant penalties for submitting false information,including the possibility of fines and imprisonment for knowing violations." • Sparks Oil Company 'ermi tee (Please print oris 1 e) /./kar/ A,/ f.Lr 1. gnatur- if P,/ / * Date Required unl ss s emitted electronically) 412 N Scales St., Reidsville, NC 27320336 49-8231 www.sparksoil.com May 31,2017 Permittee Address Phone Number e-mail address Permit Expiration Date ADDITIONAL CERTIFIED LABORATORIES Certified Laboratory(2) Certification No. Certified Laboratory(3) Certification No. Certified Laboratory(4) Certification No. Certified Laboratory(5) Certification No. PARAMETER CODES Parameter Code assistance may be obtained by calling the NPDES Unit at(919)733-5083 or by visiting the Surface Water Protection Section's web site at h2o.enr.state.nc.us/wqs and linking to the unit's information pages. Use only units of measurement designated in the reporting facility's NPDES permit for reporting data. * No Flow/Discharge From Site: Check this box if no discharge occurs and,as a result,there are no data to be entered for all of the parameters on the DMR for the entire monitoring period. ** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G.0204. ***Signature of Permittee: If signed by other than the permittee,then the delegation of the signatory authority must be on file with the state per 15A NCAC 2B .0506(b)(2)(D). Page 2 Pace Analytical Services,LLC • • 9800 Kincey Ave. Suite 100 aceAnalytical Huntersville,NC 28078 www.pacelabs.com (704)875-9092 • October 24, 2016 Mr. Mika Trifunovic Pyramid Environmental P.O. Box 16265 Greensboro, NC 27416 RE: Project: JW Smith Pace Project No.: 92315946 Dear Mr. Trifunovic: Enclosed are the analytical results for sample(s) received by the laboratory on October 13, 2016. The results relate only to the samples included in this report. Results reported herein conform to the most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. If you have any questions concerning this report, please feel free to contact me. Sincerely, Nicole Gasiorowski nicole.gasiorowski@pacelabs.com Project Manager Enclosures cz@q -FOj fe-s ': REPORT OF LABORATORY ANALYSIS 1'y This report shall not be reproduced,except in full, `(ilat . without the written consent of Pace Analytical Services,LLC. Page 1 of 20 \!o�2To� Pace Analytical Services,LLC ® 9800 uite�100 aceArialytical KinceyAve. S Huntersville,NC 28078 ( www..pacetabscom (704)875-9092 } CERTIFICATIONS Project: JW Smith Pace Project No.: 92315946 - Charlotte Certification IDs 9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Certification#:99006001 North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#:E87627 North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84 North Carolina Wastewater Certification#: 12 VirginiaNELAP Certification#:460221 Asheville Certification IDs 2225 Riverside Drive,Asheville,NC 28804 North Carolina Wastewater Certification#:40 Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001 Massachusetts Certification#:M-NC030 VirginiaNELAP Certification#:460222 North Carolina Drinking Water Certification#:37712 • REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 20 Pace Analytical Services,LLC • • g/�� /+al q ® 9800 Kincey Ave. Suite 100 aceA IalyticHuntersville,NC 28078 www.pacelabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: JW Smith Pace Project No.: 92315946 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92315946001 INF EPA6010 SH1 1 PASI-A SM 6200B CAH 63 PASI-C SM 2540D MLS 1 PASI-A EPA420.4 DMN 1 PASI-A 92315946002 EFF EPA6010 SH1 1 PASI-A SM 6200B CAH 63 PASI-C SM 2540D ALC 1 PASI-A EPA 420.4 DMN 1 PASI-A REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 20 i ;/ ; Pace Analytical Services,LLC 9800 Kincey Ave. Suite 'aceArralytical Huntersv Ile,NC 28078 wwwpacelabs.com (704)875-9092 . ANALYTICAL RESULTS Project: JW Smith Pace Project No.: 92315946 Sample: INF Lab ID: 92315946001 Collected: 10/12/16 18:00 Received: 10/13/16 10:21 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP,Lab Filtered Analytical Method:EPA 6010 Preparation Method:EPA 3010 Lead,Dissolved ND ug/L _ 5.0 1 10/15/16 01:59 10/21/16 12:26 7439-92-1 6200B MSV Analytical Method:SM 6200B Benzene 29.9 ug/L 1.0 2 10/20/16 05:15 71-43-2 Bromobenzene ND ug/L 1.0 2 10/20/16 05:15 108-86-1 Bromochloromethane ND ug/L 1.0 2 10/20/16 05:15 74-97-5 Bromodichloromethane ND ug/L 1.0 2 10/20/16 05:15 75-27-4 Bromoform ND ug/L 1.0 2 10/20/16 05:15 75-25-2 Bromomethane ND ug/L 10.0 2 10/20/16 05:15 74-83-9 n-Butylbenzene ND ug/L 1.0 2 10/20/16 05:15 104-51-8 sec-Butylbenzene ND ug/L 1.0 2 10/20/16 05:15 135-98-8 tert-Butylbenzene ND ug/L 1.0 2 10/20/16 05:15 98-06-6 Carbon tetrachloride ND ug/L 1.0 2 10/20/16 05:15 56-23-5 Chlorobenzene ND ug/L 1.0 2 10/20/16 05:15 108-90-7 Chloroethane ND ug/L 2.0 2 10/20/16 05:15 75-00-3 Chloroform ND ug/L 1.0 2 10/20/16 05:15 67-66-3 Chloromethane ND ug/L 2.0 2 10/20/16 05:15 74-87-3 2-Chlorotoluene ND ug/L 1.0 2 10/20/16 05:15 95-49-8 4-Chlorotoluene ND ug/L 1.0 2 10/20/16 05:15 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 2 10/20/16 05:15 96-12-8 Dibromochloromethane ND ug/L 1.0 2 10/20/16 05:15 124-48-1 1,2-Dibromoethane(EDB) 2.5 ug/L 1.0 2 10/20/16 05:15 106-93-4 Dibromomethane ND ug/L 1.0 2 10/20/16 05:15 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 2 10/20/16 05:15 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 2 10/20/16 05:15 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 2 10/20/16 05:15 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 2 10/20/16 05:15 75-71-8 1,1-Dichloroethane ND ug/L 1.0 2 10/20/16 05:15 75-34-3 1,2-Dichloroethane 1.8 ug/L 1.0 2 10/20/16 05:15 107-06-2 1,1-Dichloroethene ND ug/L 1.0 2 10/20/16 05:15 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 2 10/20/16 05:15 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 2 10/20/16 05:15 156-60-5 1,2-Dichloropropane ND ug/L 1.0 2 10/20/16 05:15 78-87-5 1,3-Dichloropropane ND ug/L 1.0 2 10/20/16 05:15 142-28-9 2,2-Dichloropropane ND ug/L 1.0 2 10/20/16 05:15 594-20-7 1,1-Dichloropropene ND ug/L 1.0 2 10/20/16 05:15 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 2 10/20/16 05:15 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 2 10/20/16 05:15 10061-02-6 Diisopropyl ether 1.0 ug/L 1.0 2 10/20/16 05:15 108-20-3 Ethylbenzene 16.4 ug/L 1.0 2 10/20/16 05:15 100-41-4 Hexachloro-1,3-butadiene ND ug/L 4.0 2 10/20/16 05:15 87-68-3 Isopropylbenzene(Cumene) ND ' ug/L 1.0 2 10/20/16 05:15 98-82-8 Methylene Chloride 4.0 ug/L 4.0 2 10/20/16 05:15 75-09-2 C9 Methyl-tert-butyl ether 119 ug/L 1.0 2 10/20/16 05:15 1634-04-4 Naphthalene 44.2 ug/L 4.0 2 10/20/16 05:15 91-20-3 . n-Propylbenzene ND ug/L 1.0 2 10/20/16 05:15 103-65-1 . Styrene - ND ug/L 1.0 2 10/20/16 05:15 100-42-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 20 Pace Analytical Services,LLC / 'aceAnalytical 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 / www.pacelabs.com (704)875-9092 1 ANALYTICAL RESULTS Project: JW Smith Pace Project No.: 92315946 Sample: INF Lab ID: 92315946001 Collected: 10/12/16 18:00 Received: 10/13/16 10:21 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method:SM 62006 1,1,1,2-Tetrachloroethane ND ug/L 1.0 2 10/20/16 05:15 630-20-6 1,1,2,2-TetrachloroethaneND ug/L 1.0 2 10/20/16 05:15 79-34-5 Tetrachloroethene ND ug/L 1.0 2 10/20/16 05:15 127-18-4 Toluene 223 ug/L 1.0 2 10/20/16 05:15 108-88-3 1,2,3-Trichlorobenzene ND ug/L 4.0 2 10/20/16 05:15 87-61-6 1,2,4-Trichlorobenzene ND ug/L 4.0 2 10/20/16 05:15 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 2 10/20/16 05:15 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 2 10/20/16 05:15 79-00-5 Trichloroethene ND ug/L 1.0 2 10/20/16 05:15 79-01-6 Trichlorofluoromethane ND ug/L 2.0 2 10/20/16 05:15 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 2 10/20/16 05:15 96-18-4 1,2,4-Trimethylbenzene 73.1 ug/L 1.0 2 10/20/16 05:15 95-63-6 1,3,5-Trimethylbenzene 31.5 ug/L 1.0 2 10/20/16 05:15 108-67-8 Vinyl chloride ND ug/L 2.0 2 10/20/16 05:15 75-01-4 m&p-Xylene 193 ug/L 2.0 2 10/20/16 05:15 179601-23-1 o-Xylene 160 ug/L 1.0 2 10/20/16 05:15 95-47-6 Surrogates 1,2-Dichloroethane-d4(S) 93 % 70-130 2 10/20/16 05:15 17060-07-0 4-Bromofluorobenzene(S) 96 % 70-130 2 10/20/16 05:15 460-00-4 Toluene-d8(S) 105 % 70-130 2 10/20/16 05:15 2037-26-5 • 2540D Total Suspended Solids Analytical Method:SM 2540D Total Suspended Solids ND mg/L 12.5 1 10/17/16 11:51 420.4 Phenolics,Total Analytical Method:EPA 420.4 Phenol 0.047 mg/L 0.010 1 10/21/16 13:50 • REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 20 Pace Analytical Services,LLC 7 aceAnalytical a 9800Hunte sKinceyville,NCve. tte 28078 www.pacelabs.com I (704)875-9Q92 I ANALYTICAL RESULTS Project: JW Smith Pace Project No.: 92315946 Sample: EFF Lab ID: 92315946002 Collected: 10/12/16 18:30 Received: 10/13/16 10:21 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP,Lab Filtered Analytical Method:EPA 6010 Preparation Method:EPA 3010 Lead,Dissolved ND ug/L 5.0 1 10/15/16 01:59 10/21/16 12:29 7439-92-1 • 6200B MSV Analytical Method:SM 6200B Benzene ND ug/L 0.50 1 10/20/16 04:07 71-43-2 Bromobenzene ND ug/L 0.50 1 10/20/16 04:07 108-86-1 ' Bromochloromethane ND ug/L 0.50 1 10/20/16 04:07 74-97-5 Bromodichloromethane ND ug/L 0.50 1 10/20/16 04:07 75-27-4 Bromoform ND ug/L 0.50 1 10/20/16 04:07 75-25-2 Bromomethane ND ug/L 5.0 1 10/20/16 04:07 74-83-9 n-Butylbenzene ND ug/L 0.50 1 10/20/16 04:07 104-51-8 sec-Butylbenzene ND ug/L 0.50 1 10/20/16 04:07 135-98-8 tert-Butylbenzene ND ug/L 0.50 1 10/20/16 04:07 98-06-6 Carbon tetrachloride ND ug/L 0.50 1 10/20/16 04:07 56-23-5 Chlorobenzene ND ug/L 0.50 1 10/20/16 04:07 108-90-7 Chloroethane ND ug/L 1.0 1 10/20/16 04:07 75-00-3 Chloroform ND ug/L 0.50 1 10/20/16 04:07 67-66-3 r- Chloromethane ND ug/L 1.0 1 10/20/16 04:07 74-87-3 2-Chiorotoluene ND ug/L 0.50 1 10/20/16 04:07 95-49-8 4-Chlorotoluene ND ug/L 0.50 1 10/20/16 04:07 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 1.0 1 10/20/16 04:07 96-12-8 Dibromochloromethane ND ug/L 0.50 1 10/20/16 04:07 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 0.50 1 10/20/16 04:07 106-93-4 Dibromomethane ND ug/L 0.50 1 10/20/16 04:07 74-95-3 1,2-Dichlorobenzene ND ug/L 0.50 1 10/20/16 04:07 95-50-1 1,3-Dichlorobenzene ND ug/L 0.50 1 10/20/16 04:07 541-73-1 1,4-Dichlorobenzene ND ug/L 0.50 1 10/20/16 04:07 106-46-7 Dichlorodifluoromethane ND ug/L 0.50 1 10/20/16 04:07 75-71-8 1,1-Dichloroethane ND ug/L 0.50 1 10/20/16 04:07 75-34-3 1,2-Dichloroethane ND ug/L 0.50 1 10/20/16 04:07 107-06-2 1,1-Dichioroethene ND ug/L 0.50 1 10/20/16 04:07 75-35-4 cis-1,2-Dichloroethene ND ug/L 0.50 1 10/20/16 04:07 156-59-2 trans-1,2-Dichloroethene ND ug/L 0.50 1 10/20/16 04:07 156-60-5 1,2-Dichloropropane ND ug/L 0.50 1 10/20/16 04:07 78-87-5 1,3-Dichloropropane ND ug/L 0.50 1 10/20/16 04:07 142-28-9 2,2-Dichloropropane ND ug/L 0.50 1 10/20/16 04:07 594-20-7 1,1-Dichloropropene ND ug/L 0.50 1 10/20/16 04:07 563-58-6 cis-1,3-Dichloropropene ND ug/L 0.50 1 10/20/16 04:07 10061-01-5 trans-1,3-Dichloropropene ND ug/L 0.50 1 10/20/16 04:07 10061-02-6 Diisopropyl ether ND ug/L 0.50 1 10/20/16 04:07 108-20-3 Ethylbenzene ND ug/L 0.50 1 10/20/16 04:07 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 10/20/16 04:07 87-68-3 lsopropylbenzene(Cumene) ND ug/L 0.50 1 10/20/16 04:07 98-82-8 Methylene Chloride ND ug/L 2.0 1 10/20/16 04:07 75-09-2 Methyl-tert-butyl ether ND ug/L 0.50 1 10/20/16 04:07 1634-04-4 Naphthalene ND ug/L 2.0 1 10/20/16 04:07 91-20-3 n-Propylbenzene ND ug/L 0.50 1 10/20/16 04:07 103-65-1 Styrene ND ug/L 0.50 1 10/20/16 04:07 100-42-5 • REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 20 • Y aceAnalytical® Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 ( wwvcpacelabs.com (704)875-9092 71 ANALYTICAL RESULTS Project: JW Smith Pace Project No.: 92315946 Sample: EFF Lab ID: 92315946002 Collected: 10/12/16 18:30 Received: 10/13/16 10:21 Matrix:Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6200B MSV Analytical Method:SM 6200B 1,1,1,2-Tetrachloroethane ND ug/L 0.50 1 10/20/16 04:07 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 0.50 1 10/20/16 04:07 79-34-5 Tetrachloroethene ND ug/L 0.50 1 10/20/16 04:07 127-18-4 Toluene ND ug/L 0.50 1 10/20/16 04:07 108-88-3 1,2,3-Trichlorobenzene ND ug/L 2.0 1 10/20/16 04:07 87-61-6 1,2,4-Trichlorobenzene ND ug/L 2.0 1 10/20/16 04:07 120-82-1 1,1,1-Trichloroethane ND ug/L 0.50 1 10/20/16 04:07 71-55-6 1,1,2-Trichloroethane ND ug/L 0.50 1 10/20/16 04:07 79-00-5 Trichloroethene ND ug/L 0.50 1 10/20/16 04:07 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 10/20/16 04:07 75-69-4 1,2,3-Trichloropropane ND ug/L 0.50 1 10/20/16 04:07 96-18-4 1,2,4-Trimethylbenzene ND ug/L 0.50 1 10/20/16 04:07 95-63-6 1,3,5-Trimethylbenzene ND ug/L 0.50 1 10/20/16 04:07 108-67-8 Vinyl chloride ND ug/L 1.0 1 10/20/16 04:07 75-01-4 m&p-Xylene ND ug/L 1.0 1 10/20/16 04:07 179601-23-1 o-Xylene ND ug/L 0.50 1 10/20/16 04:07 95-47-6 Surrogates 1,2-Dichloroethane-d4(S) 93 % 70-130 1 10/20/16 04:07 17060-07-0 4-Bromofluorobenzene(S) 95 % 70-130 1 10/20/16 04:07 460-00-4 Toluene-d8(S) 101 % 70-130 1 10/20/16 04:07 2037-26-5 2540D Total Suspended Solids Analytical Method:SM 2540D Total Suspended Solids ND mg/L 5.0 1 10/17/16 14:39 420.4 Phenolics,Total Analytical Method:EPA 420.4 Phenol 0.017 mg/L 0.010 1 10/21/16 13:50 • • • REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 20 Pace Analytical Services,LLC ;ace Analytical® 9800 Kincey Ave. Suite?00 • Huntersville,NC 28078 www.pacelabs.com (704)875-9092 • QUALITY CONTROL DATA Project:- JW Smith Pace Project No.: 92315946 QC Batch: 333151 Analysis Method: EPA 6010 QC Batch Method: EPA 3010 Analysis Description: 6010 MET Filtered Diss. Associated Lab Samples: 92315946001,92315946002 METHOD BLANK: 1846102 Matrix: Water Associated Lab Samples: 92315946001,92315946002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Lead,Dissolved ug/L ND 5.0 10/21/16 11:20 LABORATORY CONTROL SAMPLE: 1846103 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Lead,Dissolved ug/L 500 482 96 80-120 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 1846104 1846105 MS MSD • 92315870003 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Lead,Dissolved ug/L ND 500 500 450 453 90 91 75-125 1 • Results presented on this page are In the units indicated by the"Units"column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 20 / ` Pace Analytical Services,LLC 'aceAnaiyticai® 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 wvw.pacelabs.com (704)875-9092 • QUALITY CONTROL DATA Project: JW Smith Pace Project No.: 92315946 QC Batch: 333782 Analysis Method: SM 62008 QC Batch Method: SM 6200B Analysis Description: 6200B MSV Associated Lab Samples: 92315946001,92315946002 METHOD BLANK: 1849729 Matrix: Water Associated Lab Samples: 92315946001,92315946002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers • 1,1,1,2-Tetrachloroethane ug/L ND 0.50 10/20/16 01:01 1,1,1-Trichloroethane ug/L ND 0.50 10/20/16 01:01 1,1,2,2-Tetrachloroethane ug/L ND 0.50 10/20/16 01:01 1,1,2-Trichloroethane ug/L ND 0.50 10/20/16 01:01 1,1-Dichloroethane ug/L ND 0.50 10/20/16 01:01 1,1-Dichloroethene ug/L ND 0.50 10/20/16 01:01 1,1-Dichloropropene ug/L ND 0.50 10/20/16 01:01 1,2,3-Trichlorobenzene ug/L ND 2.0 10/20/16 01:01 1,2,3-Trichloropropane ug/L ND 0.50 10/20/16 01:01 1,2,4-Trichlorobenzene ug/L ND 2.0 10/20/16 01:01 1,2,4-Trimethylbenzene ug/L ND 0.50 10/20/16 01:01 1,2-Dibromo-3-chloropropane ug/L ND 1.0 10/20/16 01:01 1,2-Dibromoethane(EDB) ug/L • ND 0.50 10/20/16 01:01 1,2-Dichlorobenzene ug/L ND 0.50 10/20/16 01:01 1,2-Dichloroethane ug/L ND 0.50 10/20/16 01:01 1,2-Dichloropropane ug/L ND 0.50 10/20/16 01:01 1,3,5-Trimethylbenzene ug/L ND 0.50 10/20/16 01:01 1,3-Dichlorobenzene ug/L ND 0.50 10/20/16 01:01 1,3-Dichioropropane ug/L ND 0.50 10/20/16 01:01 1,4-Dichlorobenzene ug/L ND 0.50 10/20/16 01:01 2,2-Dichloropropane ug/L ND 0.50 10/20/16 01:01 2-Chlorotoluene ug/L ND 0.50 10/20/16 01:01 4-Chlorotoluene ug/L ND 0.50 10/20/16 01:01 Benzene ug/L ND 0.50 10/20/16 01:01 Bromobenzene ug/L ND 0.50 10/20/16 01:01 Bromochloromethane ug/L ND 0.50 10/20/16 01:01 Bromodichloromethane ug/L ND 0.50 10/20/16 01:01 Bromoform ug/L ND 0.50 10/20/16 01:01 Bromomethane ug/L ND 5.0 10/20/16 01:01 Carbon tetrachloride ug/L ND 0.50 10/20/16 01:01 Chlorobenzene ug/L ND 0.50 10/20/16 01:01 Chloroethane ug/L ND 1.0 10/20/16 01:01 Chloroform ug/L ND 0.50 10/20/16 01:01 Chloromethane ug/L ND 1.0 10/20/16 01:01 • cis-1,2-Dichloroethene ug/L ND 0.50 10/20/16 01:01 cis-1,3-Dichloropropene ug/L ND 0.50 10/20/16 01:01 Dibromochloromethane ug/L ND 0.50 10/20/16 01:01 Dibromomethane ug/L ND 0.50 10/20/16 01:01 Dichlorodifluoromethane ug/L ND 0.50 10/20/16 01:01 Diisopropyl ether ug/L ND 0.50 10/20/16 01:01 Ethylbenzene ug/L ND 0.50 10/20/16 01:01 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 20 dif' Pace Analytical Services,LLC 9800 Kincey Ave. Suite 100 • r} aceAnalytical Huntersville,NC 28078 ( www.pacelabs.com (704)875-9892 QUALITY CONTROL DATA Project: JW Smith Pace Project No.: 92315946 METHOD BLANK: 1849729 Matrix: Water Associated Lab Samples: 92315946001,92315946002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Hexachloro-1,3-butadiene ug/L ND 2.0 10/20/16 01:01 Isopropylbenzene(Cumene) ug/L ND 0.50 10/20/16 01:01 m&p-Xylene ug/L ND 1.0 10/20/16 01:01 Methyl-tert-butyl ether ug/L ND 0.50 10/20/16 01:01 Methylene Chloride ug/L ND 2.0 10/20/16 01:01 n-Butylbenzene ug/L ND 0.50 10/20/16 01:01 • n-Propylbenzene ug/L ND 0.50 10/20/16 01:01 Naphthalene ug/L ND 2.0 10/20/16 01:01 o-Xylene ug/L ND 0.50 10/20/16 01:01 sec-Butylbenzene ug/L ND 0.50 10/20/16 01:01 Styrene ug/L ND 0.50 10/20/16 01:01 tert-Butylbenzene ug/L ND 0.50 10/20/16 01:01 Tetrachloroethene ug/L ND 0.50 10/20/16 01:01 Toluene ug/L ND 0.50 10/20/16 01:01 trans-1,2-Dichloroethene ug/L ND 0.50 10/20/16 01:01 trans-1,3-Dichloropropene ug/L ND 0.50 10/20/16 01:01 Trichloroethene ug/L ND 0.50 10/20/16 01:01 Trichlorofluoromethane ug/L ND 1.0 10/20/16 01:01 Vinyl chloride ug/L ND 1.0 10/20/16 01:01 1,2-Dichloroethane-d4(S) % 117 70-130 10/20/16 01:01 4-Bromofluorobenzene(S) % 93 70-130 10/20/16 01:01 Toluene-d8(S) % 102 70-130 10/20/16 01:01 LABORATORY CONTROL SAMPLE: 1849730 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 50 48.6 97 60-140 1,1,1-Trichloroethane ug/L 50 53.8 108 60-140 1,1,2,2-Tetrachloroethane ug/L 50 45.4 91 60-140 1,1,2-Trichloroethane ug/L 50 49.3 99 60-140 1,1-Dichloroethane ug/L 50 51.9 104 60-140 1,1-Dichloroethene ug/L 50 59.3 119 60-140 1,1-Dichloropropene ug/L 50 49.7 99 60-140 1,2,3-Trichlorobenzene ug/L 50 45.7 91 60-140 1,2,3-Trichloropropane ug/L 50 47.5 95 60-140 1,2,4-Trichlorobenzene ug/L 50 47.0 94 60-140 1,2,4-Trimethylbenzene ug/L 50 50.6 101 60-140 1,2-Dibromo-3-chloropropane ug/L 50 53.0 106 60-140 1,2-Dibromoethane(EDB) ug/L 50 51.2 102 60-140 1,2-Dichlorobenzene ug/L 50 49.6 99 60-140 1,2-Dichloroethane ug/L 50 47.7 95 60-140 1,2-Dichloropropane ug/L 50 48.7 97 60-140 1,3,5-Trimethylbenzene ug/L 50 49.5 99 60-140 1,3-Dichlorobenzene ug/L 50 47.3 95 60-140 • Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result. • REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 20 Pace Ariaiytical Services,LLC aceAnalytical® 9800100 HuntersKinceyville,NC'28078 xn»vpacalabs.com (704)875-9092 QUALITY CONTROL DATA Project: JW Smith Pace Project No.: 92315946 LABORATORY CONTROL SAMPLE: 1849730 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers 1,3-Dichloropropane ug/L 50 45.7 91 60-140 1,4-Dichlorobenzene ug/L 50 46.7 93 - 60-140 2,2-Dichloropropane ug/L 50 48.7 97 60-140 2-Chlorotoluene ug/L 50 50.5 101 60-140 4-Chlorotoluene ug/L 50 49.7 99 60-140 Benzene ug/L 50 49.2 98 60-140 Bromobenzene ug/L 50 50.8 102 60-140 Bromochloromethane ug/L 50 49.7 99 60-140 Bromodichloromethane ug/L 50 51.2 102 60-140 Bromoform ug/L 50 47.7 95 60-140 Bromomethane ug/L 50 44.3 89 60-140 Carbon tetrachloride ug/L 50 54.9 110 60-140 Chlorobenzene ug/L 50 48.0 96 60-140 Chloroethane ug/L 50 35.4 71 60-140 Chloroform ug/L 50 49.5 99 60-140 Chloromethane ug/L 50 62.7 125 60-140 cis-1,2-Dichloroethene ug/L 50 55.1 • 110 60-140 cis-1,3-Dichloropropene ug/L 50 48.7 97 60-140 Dibromochloromethane ug/L 50 50.0 100 60-140 Dibromomethane ug/L 50 43.8 88 60-140 Dichlorodifluoromethane ug/L 50 60.5 121 60-140 Diisopropyl ether ug/L 50 65.7 131 60-140 Ethylbenzene ug/L 50 48.9 98 60-140 Hexachloro-1,3-butadiene ug/L 50 46.5 93 60-140 lsopropylbenzene(Cumene) ug/L 50 48.7 97 60-140 • m&p-Xylene ug/L 100 97.0 97 60-140 Methyl-tert-butyl ether ug/L 50 56.4 113 60-140 Methylene Chloride ug/L 50 56.0 112 60-140 n-Butylbenzene ug/L 50 49.5 99 60-140 n-Propylbenzene ug/L 50 47.7 95 60-140 Naphthalene ug/L 50 49.7 99 60-140 o-Xylene ug/L 50 48.5 97 60-140 sec-Butylbenzene ug/L 50 49.0 98 60-140 Styrene ug/L 50 51.1 102 60-140 tert-Butylbenzene ug/L 50 40.7 81 60-140 Tetrachloroethene ug/L 50 44.2 88 60-140 CU Toluene ug/L 50 48.4 97 60-140 • trans-1,2-Dichloroethene ug/L 50 55.9 112 60-140 trans-1,3-Dichloropropene ug/L 50 47.1 94 60-140 Trichloroethene ug/L 50 47.2 94 60-140 Trichlorofluoromethane ug/L 50 39.8 80 60-140 Vinyl chloride ug/L 50 42.9 86 60-140 1,2-Dichloroethane-d4(S) % 106 70-130 4-Bromofluorobenzene(S) % 98 70-130 Toluene-d8(S) % 102 70-130 Results presented on this page are In the units indicated by the"Units"column except where an alternate unit is presented to the right of the result REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 20 Pace Analytical Services,LLC e 9800 Kincey Ave. Suite 100 79 Pace Huntersville,NC 28078 I www.pacelabs.com (704)875-9092 • I QUALITY CONTROL DATA Project: JW Smith Pace Project No.: 92315946 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 1849731 1849732 MS MSD 92316212007 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual 1,1,1,2-Tetrachloroethane ug/L ND 20 20 20.3 20.1 102 101 60-140 1 1,1,1-Trichloroethane ug/L ND 20 20 23.9 24.0 119 120 60-140 1 1,1,2,2-Tetrachloroethane ug/L ND 20 20 19.9 19.1 100 95 60-140 4 1,1,2-Trichloroethane ug/L ND 20 20 20.8 19.8 104 99 60-140 5 1,1-Dichloroethane ug/L ND 20 20 23.0 22.6 115 113 60-140 2 1,1-Dichloroethene ug/L ND 20 20 27.0 26.9 135 135 60-140 0 1,1-Dichloropropene ug/L ND 20 20 22.5 22.1 112 110 60-140 2 1,2,3-Trichlorobenzene ug/L ND 20 20 21.1 20.1 106 100 60-140 5 1,2,3-Trichloropropane ug/L ND 20 20 20.0 19.2 100 96 60-140 4 1,2,4-Trichlorobenzene ug/L ND 20 20 20.9 19.9 104 99 60-140 5 1,2,4-Trimethylbenzene ug/L ND 20 20 22.7 21.4 113 107 60-140 6 1,2-Dibromo-3-chloropropane ug/L ND 20 20 23.7 22.0 119 110 60-140 8 1,2-Dibromoethane(EDB) ug/L ND 20 20 21.8 21.0 109 105 60-140 4 1,2-Dichlorobenzene ug/L ND 20 20 22.2 20.9 111 104 60-140 6 1,2-Dichloroethane ug/L ND 20 20 21.2 21.8 105 108 60-140 3 1,2-Dichloropropane ug/L ND 20 20 20.8 20.5 104 102 60-140 2 1,3,5-Trimethylbenzene ug/L ND 20 20 22.3 21.0 112 105 60-140 6 1,3-Dichlorobenzene ug/L ND 20 20 21.1 19.8 106 99 60-140 6 1,3-Dichloropropane ug/L ND 20 20 19.7 18.8 98 94 60-140 5 1,4-Dichlorobenzene ug/L ND 20 20 21.1 19.7 105 98 60-140 7 2,2-Dichloropropane ug/L ND 20 20 21.7 21.2 108 106 60-140 2 2-Chlorotoluene ug/L ND 20 20 23.0 21.6 115 108 60-140 6 4-Chlorotoluene ug/L ND 20 20 22.4 21.2 112 106 60-140 6 Benzene ug/L ND 20 20 21.4 20.7 107 103 60-140 4 Bromobenzene ug/L ND 20 20 22.7 21.1 113 105 60-140 7 Bromochloromethane ug/L ND 20 20 21.3 20.6 106 103 60-140 3 Bromodichloromethane ug/L ND 20 20 22.0 21.2 110 106 60-140 4 Bromoform ug/L ND 20 20 18.8 18.3 94 92 60-140 3 Bromomethane ug/L ND 20 20 21.1 21.9 106 109 60-140 4 Carbon tetrachloride ug/L ND 20 20 25.5 24.5 127 123 60-140 4 Chlorobenzene ug/L ND 20 20 21.2 20.5 106 103 60-140 3 Chloroethane ug/L ND 20 20 15.9 17.7 80 88 60-140 10 Chloroform ug/L ND 20 20 21.9 21.6 109 108 60-140 1 Chloromethane ug/L ND 20 20 27.5 29.2 136 145 60-140 6 M1 cis-1,2-Dichloroethene ug/L ND 20 20 24.1 23.9 120 120 60-140 1 cis-1,3-Dichloropropene ug/L ND 20 • 20 20.3 19.7 102 98 60-140 3 Dibromochloromethane ug/L ND 20 20 21.1 20.3 105 101 60-140 4 Dibromomethane ug/L ND 20 20 18.7 18.0 93 90 60-140 4 Dichlorodifluoromethane ug/L ND 20 20 28.2 28.8 141 144 60-140 2 M1 Diisopropyl ether ug/L ND 20 20 27.5 27.0 137 135 60-140 2 Ethylbenzene ug/L ND 20 • 20 22.0 20.9 110 105 60-140 5 Hexachloro-1,3-butadiene ug/L ND 20 20 23.0 21.1 114 105 60-140 9 lsopropylbenzene(Cumene) ug/L ND 20 20 21.5 20.9 108 104 60-140 3 m&p-Xylene ug/L ND 40 40 43.6 42.0 109 105 60-140 4 • Methyl-tert-butyl ether ug/L ND 20 20 24.2 23.6 120 117 60-140 3 Methylene Chloride ug/L ND 20 20 23.9 23.5 119 118 60-140 1 Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 20 rn" M.-T / Pace Analytical Services,LLC ® 9800 Kincey Ave. Suite 100 °aceAnalyticai Huntersville,NC 28078 www.paceiabs.com (704)875-9092 I QUALITY CONTROL DATA Project: JW Smith Pace Project No.: 92315946 . MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 1849731 1849732 MS MSD 92316212007 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual n-Butylbenzene ug/L ND 20 20 23.1 21.5 116 108 60-140 7 n-Propylbenzene ug/L ND 20 20 22.0 20.7 110 104 60-140 6 Naphthalene ug/L ND 20 20 22.7 21.1 113 105 60-140 7 o-Xylene ug/L ND 20 20 21.1 20.4 106 102 60-140 4 sec-Butylbenzene ug/L ND 20 20 22.8 21.5 114 107 60-140 6 Styrene ug/L ND 20 20 21.5 21.1 107 105 60-140 2 tert-Butylbenzene ug/L ND 20 20 18.8 17.6 94 88 60-140 6 Tetrachloroethene ug/L ND 20 20 20.0 19.3 100 96 60-140 4 Toluene ug/L ND 20 20 21.5 20.9 108 105 60-140 3 trans-1,2-Dichloroethene ug/L ND 20 20 25.2 24.4 126 122 60-140 3 trans-1,3-Dichloropropene ug/L ND 20 20 19.3 19.0 97 95 60-140 2 Trichloroethene ug/L ND 20 20 20.6 20.0 103 100 60-140 3 Trichlorofluoromethane ug/L ND 20 20 19.3 20.3 96 102 60-140 5 Vinyl chloride ug/L ND 20 20 21.6 21.8 108 109 60-140 1 1,2-Dichloroethane-d4(S) % 104 112 70-130 4-Bromofluorobenzene(S) % 94 95 70-130 Toluene-d8(S) % 102 101 70-130 • Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. • • REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 20 Pace Analytical Services,LLC aceAnalytical® 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacelabs.com • (704)875-9092 QUALITY CONTROL DATA Project: JW Smith Pace Project No.: 92315946 QC Batch: 333350 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92315946001 METHOD BLANK: 1847344 Matrix: Water Associated Lab Samples: 92315946001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 10/17/16 11:43 LABORATORY CONTROL SAMPLE: 1847345 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Suspended Solids mg/L 250 240 96 90-110 SAMPLE DUPLICATE: 1847346 92315796001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 1847347 92315824001 Dup Parameter Units Result Result RPD Qualifiers " Total Suspended Solids mg/L 18.7 19.0 2 Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result. • REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 20 } Pace Analytical Services,LLC aceAnalytical e 9800 KinceyAve. Suite 100 Huntersville,NC 28078 www..pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: JW Smith Pace Project No.: 92315946 QC Batch: 333411 Analysis Method: SM 2540D QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids Associated Lab Samples: 92315946002 METHOD BLANK: 1847742 Matrix: Water Associated Lab Samples: 92315946002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 10/17/16 14:39 LABORATORY CONTROL SAMPLE: 1847743 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Suspended Solids mg/L 250 230 92 90-110 SAMPLE DUPLICATE: 1847744 92315946002 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND SAMPLE DUPLICATE: 1847745 92315996001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L ND ND Results presented on this page are In the units indicated by the"Units"column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 20 Pace Analytical Services,LLC aceAnalytical 9800 KinceyAveSuite 100 Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: JW Smith Pace Project No.: 92315946 QC Batch: 333927 Analysis Method: EPA 420.4 QC Batch Method: EPA 420.4 Analysis Description: 420.4 Phenolics Associated Lab Samples: 92315946001,92315946002 METHOD BLANK: 1850808 Matrix: Water Associated Lab Samples: 92315946001,92315946002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phenol mg/L ND 0.010 10/21/16 13:26 LABORATORY CONTROL SAMPLE: 1850809 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Phenol mg/L .05 0.050 101 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 1850810 1850811 MS MSD 92315167005 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Phenol mg/L 175 .05 .05 0.16 0.16 -31 -37 90-110 2 M1 ug/L MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 1850812 1850813 MS MSD 92315180001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Phenol mg/L 0.017 .05 .05 0.064 0.064 94 93 90-110 0 • • Results presented on this page are in the units Indicated by the"Units"column except where an alternate unit is presented to the right of the result. • • REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 16 of 20 Pace Analytical Services,LLC • i © 9800 Kincey Ave. Suite 100 aceAnaiytcai Huntersville,NC 28078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: JW Smith Pace Project No.: 92315946 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services-Asheville PASI-C Pace Analytical Services-Charlotte ANALYTE QUALIFIERS C9 Common Laboratory Contaminant. CU The continuing calibration for this compound is outside of Pace Analytical acceptance limits.Analyte presence below reporting limits in associated samples.Results unaffected by high bias. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery. • REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 17 of 20 Pace Analytical Services,LLC 79 Pace 5 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 www.pacelabs.com (704)875-9092 ., I QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: JW Smith Pace Project No.: 92315946 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92315946001 INF EPA 3010 333151 EPA 6010 333298 92315946002 EFF EPA 3010 333151 EPA 6010 333298 92315946001 INF SM 6200B 333782 92315946002 EFF SM 6200B 333782 92315946001 INF SM 2540D 333350 92315946002 EFF SM 2540D 333411 92315946001 INF EPA 420.4 333927 92315946002 EFF EPA 420.4 333927 • REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:10/24/2016 12:50 PM without the written consent of Pace Analytical Services,LLC. Page 18 of 20 Document Name: Document Revised:Sept.21,2016 • a Sample Condition Upon Recelpt(SCUR) Page 1 of 2 aceAnalytical Document No.: Issuing Authority: F-CAR-CS-033-Rev.08 Pace Quality Office ,,_ Page 2 of 2 for i nternal Use ONLY 5ppeConUoQ Client Name: 61-1/61/1/1A-4.‘c.4 �/� • �, :_".Receip ��s� °^. Project#. O 923159 . 6 Courier: ❑Fed Ex ❑UPS ❑USPS ❑Client 111111 [ll II 1111 I1III III ' 0 Commercial cziPace 0Other: 313946 Custody Seal.Present? Dyes pNo Seals Intact? Dyes ONO 9 m` 2/¢/ Date/Initials Person Examining Contents: fl t 41c, Packing Material: DBubble Wrap (Bubble Bags ❑None ❑Other: Thermometer: ❑IR Gun ID: t E`� Wet ❑Blue :None ❑Samples on ice,cooling process has begun � Type of Ice:� � Correction Factor: Cooler Temp Corrected(°C): . ,xBiological Tissue Frozen? DYes No ❑NJA Temp should be above freezing to 6°C USDA Regulated Soil(❑N/A,water sample) Did samples originate in a quarantine zone within the United States:CA,NY,or SC(check maps)? Did samples originate from a foreign source(internationally, DYes ®No including Hawaii and Puerto Rico)?Oyes INo Comments/Discrepancy: Chain of Custody Present? lIlYes ONo ON/A 1. Samples Arrived within Hold Time? l4Yes DNo ON/A 2. Short Hold Time Analysis(<72 hr.)? OYes (lido ON/A 3. Rush Turn Around Time Requested? Oyes (,3No ON/A 4. Sufficient Volume? VI Yes ONo ON/A S. Correct Containers Used? Lyes ONo ON/A 6. -Pace Containers Used? ®Yes DNo ON/A Containers Intact? [' Yes ONo ON/A 7. Samples Field Filtered? Dyes MNo ON/A 8. Note If sediment is visible in the dissolved container - Sample Labels Match CCC? ,i t.,.�---'pYes ONo ON/A 9. -Includes Date/Time/ID/Analysis Matrix: J\Ca All containers needing acid/base preservation have been 10 checked and documented on page two of SCURF? )ves ONo ON/A Exceptions:VOA,Coliform,TOC,Oil and Grease,DRO/8015 (water)DOC,LLHg Samples checked for dechlorination? Oyes Ei No ON/A 11. Headspace in VOA Vials(>5-6mm)? DYes ($1No ON/A 12. Trip Blank Present? Dyes iNo ON/A 13. Trip Blank Custody Seals Present? DYes ( No ON/A Pace Trip Blank Lot fi(if purchased): CLIENT NOTIFICATION/RESOLUTION Field Data Required? ayes ❑Na Person Contacted: Date/Time: Comments/Sample Discrepancy: Project Manager SCURF Review: \ tJ s Date: 1D,[idt6 ' Project Manager SRF Review: I V V°_(1 Date: (')\, t kk..,2 Note: Whenever there is a discrepancy affecting North Carolina compliance samples,a copy of this form will be sent to the North Caro ina DEHNR Certification Office(i.e. Out of hold,incorrect preservative,out of temp,incorrect containers) Laboratory receiving samples: Asheville❑ Eden[] Greenwood❑ HuntersvillefC Raleigh❑ Mechanicsville❑ Page 19 of 20 .a �-=-; CHAIN-OF-CUSTODY/Analyticalfl Request Document f. The Chain-of-Custody is a LEGAL DOCUMENT.All relevant fields must be completed accurately. N • PaceAnalytical' o - www.paceials.com Section A Section B Section C Page' of N� Required Client information: Required Project Information: Invoice Information: AEl a ,Company: yyy3r.;...-, ReportTo: ..��°' Attention: :-r ,,.} q.. 5 I I t A t p Address 1 I Copy To: Company Name: REGULATORY AGENCY .- Address: 5, NPDES ''33 i r f GROUND WATER DRINKING WATER (,�1 51,,,dt l '�.�' [1 Pace EmailTo: g Purchase Order No.: t- ''j p p UST I RCRA OTHER Pone 4,1 t ry a V a Project Name 71.1 r Paco Protect p Site Location �-..•'5 4i-> t(� (".� it f' %iJ .'T SL$ " Mana7er .- t�C Requested Due Date7TAT + f, .P1,, Project Number: ,, Pace Profile#: ...-ctr:'tet".4/L �a .. re)g STATE: R Requested Analysis Filtered(YIN) so r Section 0 Matrix Codes i Required Client Information MATRIX i CODE o g InformationCOLLECTED Preservative& 5-- r a Drinking Water OW o Oz Water WT o Waste Water WW1.5 m COMPOSITE- consroslre 0 Product P &TART ENO/GRAB d n. SoiUSoiid SL is (9 o to rt). ''��..1{ >U SAMPLE 6D Oil OL Ls t.9 U cc w C 4 ".r.. N I- Lu N G ID (A-Z,0-9!,-) Air pe lil R w °- Z 'p:. Na ' o Sample IDs MUST BE UNIQUE Tissue TS 0 °- t2r1i H d' rn i 0 Other or U ZZ o E a a LL. �' p ra tqi 4 q r;n. �4 w ¢ a rn O O. L C ` t t in' 4ev � C- a I- a c M Z U m e m » Q O 2 u0 DATE TIME DATE TIME 0 D _ = 2 Z Z 2u , N .W Pace Project.No./Lab I.D. 1 ...1-.1% 3'" ID. i °� ,` 1 2s---.-..........-.i" !1,'-,I)" �1 E'- \t ens 3 0 $ 4 S 6 • i7 i i L 9 j 11 1 12 ADDITIONAL COMMENTS RELINQUISHED BY!AFFILIATION DATE TIME ACCEPTED SY!AFFILIATION DATE TIME SAMPLE CONDITIONS 1 U l�tf -' -dll„ %_ i'"413.- lOg-2 _:...r- " -9 , ,Z..�' Ai '1(2i --- �! '„s�ii 3 Pe- „ L'u -- 'Q !t°'(5�;t tv 7g SAMPLER NAME AND SIGNATURE c a`i 15 PRINT Name of SAMPLER: e t <ila c w> r 7- s {• SIGNATURE of SAMPLER: �2j s {, DATE Signod r;^.r /"........?_//z. td _ O V •Impaaarrr Note,By sinning this form you are accepting Pace::NET 30 day payment terms and a3reeinp to late charges of 1.5%per marsh tar any invoices rrotjraid wahin.i0 days. F-ALL-O-O20rev.O7,15-May-2007 Residuals Management Plan J.W. Smith/ Camp Springs 76 Groundwater Remediation System 8920 Cherry Grove Road Reidsville, Caswell County, NC NPDES Permit# NC0088692 NCDEQ Incident#21685 Prepared for: Sparks Oil Company 412 N. Scales Street Reidsville, NC 27320 Plan Prepared by: Plan Reviewed by: ))/fri Mika Trifunovic Michael G.Jones . Project Engineer Operations Man er Pyramid Environmental & Engineering, P.C. P.O. Box 16265 503 Industrial Ave. Greensboro, NC 27416-0265 Residuals Collection, Handling, Processing, Storage & Disposal As requested by the Construction Grants and Loans Section of Division of Water Quality of North Carolina Department of Environmental Quality (NCDEQ), collection, handling, processing, storage and disposal of residuals generated in the product storage drum, oil water separator (OWS),bag filter, aggregate filter, carbon vessels, ion exchange vessels, and backwash filter are addressed in this plan. Oil Water Separator and Product Storage Drum Free product from the OWS discharges by gravity to a 65 gallon polyethylene product storage,. drum installed outside of the system building. The product storage drum is equipped with a high- level switch to shut down operation of the remediation system. Residuals from the OWS and product storage drum are collected and handled by a contractor in accordance with all applicable regulations on an as needed basis. After the collection of the residuals, the contractor immediately hauls the residuals off the site. The contractor is also responsible for the proper disposal or storage/processing of residuals. Bag Filter The bag filter is changed every month during scheduled monthly maintenance events. The used bag filters are removed from the bag filter housing using disposable gloves and placed in a sealed plastic container. The used bags are immediately shipped as a non-hazardous waste for proper disposal. Pyramid is responsible for the collection, handling, and disposal of used bag filters. Aggregate Filter and Carbon Vessels The aggregate filter and carbon vessels are exchanged every six months by a contractor in accordance with all applicable regulation. Used aggregate filter and carbon vessels are immediately hauled off the site. The contractor is responsible for the residuals handling and proper disposal or storage/processing. Ion Exchange Vessels Two ion exchange vessels were replaced with carbon vessels in May 2012. The NCDEQ approved this change, however the number of carbon vessels has never been changed in the current NPDES permit that expires on May 31, 2017. Please see the enclosed correspondence between Pyramid and NCDEQ. Backwash Filter The used backwash filter media is collected and handled by a contractor in accordance with all applicable regulations on an as needed basis. After the collection of the used media, the contractor immediately removes the filter media from the site for processing and/or disposal. The contractor is also responsible for proper disposal or storage/processing of the used media. Camp Springs 76/JW Smith—Residuals Management Plan 1 - Mika Trifunovic From: Mika Trifunovic <mika@pyramidenvironmental.com> Sent: Wednesday,June 20,2012 11:38 AM To: 'Bob Guerra (bob.guerra@ncdenr.gov)' Cc: Mike Jones (Mike@pyramidenvironmental.com) Subject: JW Smith/Camp Springs 76 NPDES Permit#NC0088692 Good morning Bob, I have just received the referenced NPDES permit form our client and I've noticed that the Supplement to Permit Cover Sheet(attached as a PDF file) contains an incorrect number of carbon vessels. There should be four(4)carbon vessels listed on the sheet because two(2) ion exchange vessels have been converted to carbon vessels. Please see the forwarded emails. Could you please email me the NPDES permit with the correct number of carbon vessels. Thank you. Mika From: Guerra, Bob [mailto:bob.guerra(ancdenr.gov] Sent: Wednesday, March 14, 2012 1:26 PM To: Mika Trifunovic Subject: RE: Modification of JW Smith/Camp Springs 76 Remediation System I will be including this request and incorporate the changes into your permit when I issue it. From: Mika Trifunovic fmailto:mikaPpyramidenvironmental.coml Sent: Wednesday, March 14, 2012 12:12 PM To: Corporon,Joe; Guerra, Bob Subject: Modification of JW Smith/Camp Springs 76 Remediation System Good afternoon Joe and Bob, As I mentioned during our conversation,we have intent to modify the JW Smith/Camp Springs 76 petroleum contaminated groundwater remediation system which holds the NPDES Individual Permit#NC0088692. The modification will include conversion of two existing ion exchange vessels into carbon filter vessels. Detailed information about the modification is provided in the attached PDF file. Please let me know if you need any additional information or clarification. Since the permit is currently being renewed, I would like to ask you to include this proposed modification into the permit. Thank you. Mika Trifunovic Project Manager Pyramid Environmental &Engineering 1 'kti AtR01 JW Smith/CampSprings 76 Petroleum Contaminated Groundwater r - �.�a�N. ..-4 • Remediation System NPDES Permit# NC0088692 i SE Al. r 5000 . •.i. '�. �r SQ. 0�j � NEEP SYSTEMS ¢Lo N + � 1 E • Model 2651 ,z n !N. C 6 GPM "WO tt .."%\\ VENT TO Shallow Tray • Z it o i i `HUH ttATMOSPHERE 5-Tray Low Profile O w- •-Z I Ct: co Flow Rate: 2-115 GPM g f5g O E M Wr Flow: Min. 600 CFM Z ra m O NOTE This sump may be O CO co Integrated in the © —� I` All Z M v AIR r cc())a:IT.;■ INLET y_ or v FILTER a 0 ---� American Stainless _ ' Centrifugal Pump - 1HP v . BLOWERr- '- " - O --1 'V NEEP SYSTEMS BLOWER - I `, _ .l 7.5HP/3 Phase a N SUMP #� I r-- I 600 SCFM El M II --,a- J I 9 LEVEL FLOAT SWITCH I I _,--1 : PUMP ON & OFF el ) .__1_1 J ' — I _ 1 L r -W-, !f Q 3 Dischar d zump _ 1 11 L RELAY OPENS • • American.Stainless Il to J O f Centrifugal Pump BACKWASH 1 `; 0 Li- J • 0.5 HP/30/I'EFC TRICKLE II ji( CC VEL RELAY CLOSES ( r ......____ FLIER I# I U In 1 ri I Z_ W L RELAY OPENS li L—_-- Both ion exchange units will be converted , a = ° . into carbon filter vessels. N O CI- Conversion process: 41 r tZ Z (2) Berkely BVM SS Multi Stage -vacuum ion exchange media from the vessels I I .< ` Lu 1 HP Centrifugal Pumps � o!r o_ 1— tEcx -rinse empty vessels ii o tLvE • •• u — -haul the ion exchange media and rinse water :11 O INrr_ _____ off site for proper disposalrU I LEVEL FLO/ -fill the vessels with virgin carbon II __•I Z PUMP ON. There will be no backwash of the carbon ',� O J O a....._i filter vessels. g -' < • The existing ion exchange backwash line �1 Q > 0 =_____ and 320-gallon tank will be removed. !'1 Q ca .'1.'4;5.k., A 6 . " 0 ''') CK Ce ~-- ...,.r:, r •• j• i I ION II i3va 3:ty•..+V.w•r II } I EXCHANGE d 4 ^• / I ! J vEssa f fl. AGGREGATE CARBON CARBON L ,.._ t Ii Q fie" FILTER ©`O© FILTER �© FILTER O O 11 - Z OL _ BACKWASH I 1 uj �� • CHEC 4�©.© I1 Z (1) Multi-Media I _ VALVES Aggregate Filter i BACKWASH ; '''J I FLOW O /TOTALIZING f • 1 r I r FLOW MEIER ;.I:I gos!<' (2) High-Pressure GAC Vessels } >, i . Each with 90 lbs. (3 cu.ft.) carbon ExcyANGE I i " • VESSEL JE "P • •0 Z ION — NOT RELEASED FOR CONSTRUCTION t 9 GROU NDWATER DW ATER TEDI : . _ DISCHARGE I OS • - ,6 . - . . .. •