WQ0018087_Monitoring Report_20170127

GW -59A COMPLIANCE REPORT FORINT Permit # W00018087
(Submit one each monitoring period with GW -59 forms.)
1
Enter date monitoring results were due. ( 0113112017) Will this monitoring report (GW -59 and GW-
YES
NO
59A) be submitted after the established due date?
X
2
Was any required information missing on the GW -59 report forms?
YES
NO
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes'; contact the Regional Officefor guidance.
X
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below: See Summary of Groundwater Monitoring Results for more detail.
MW -28 Ammonia -nitrogen 12/02/2016 82.5 mg/L Resample 01/04/2017 83.5 mg/L Permit Limit 1.5 mg/L
Total Dissolved Solids 12/02/2015 827 mg/L Resample 12/21/2016 509 mg/L Permit Limit 500 mg/L
MW -21D Ammonia -nitrogen 12/02/2016 157 mg/L Resample 01/04/2017 12.8 mg/L Permit Limit 1.5 mg/L
Total Dissolved Solids 12/02/2015 678 mg/L Resample 12/21/2016 846 mg/L Permit Limit 500 mg/L
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
X
If the answer to question 5 is "NO" skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentratiori(s) reported, and sample collection date for each occurrence (for the last two years).
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES". a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO'; monitoring wells may be improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES" describe those actions in the space provided below.
If the answer to question 7 is "NO'; contact the Regional Office within 90 days: an evaluation may be
reguired to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do s@0ay subject the permittee to a Notice of Violation.
Fines, and/or penalties.
z AN 7 20O
-0m 1P
o n -a
� �
N
8
The person completing this portion (GW -59A) of the _M?Wtorft rely t should sign below and submit this
form with GW -59 forms for required wells to the addras provided a , he top of the current GW -59 form.
I hereby acknowledge that the above information wasvaluated and the information submitted in this
report (C liance Report WYA"tru and complete to the best of my knowledge.
tZ )3 cV
Signatur ermittee (or Authorized �a Date
GW -59A 12/8/2003

SUtiMI I
R QUALITY MONITORING:
Name: ' DAK Americas LLC, Cape Fear Site
Name (if -different)
Address: 1205 C_ulbreth Drive, Suite 100
ngton is"`E'' NC 28405 County, Brunswick
PAPER
act Person: Larry Young Telephone#. [phone] _
Location/Site Name: Down gradient/Monitoring Well # 2A No. of wells to be sampled: 6
LID NUMBER (from Permit): MW. # 2A
Depth 13.0 ft.
i to Water Level: 6.60 ft. below measuring point
wring Point is 1.92 ft. above land surface_
ne of water pumped/bailed before sampling: 7
sample
GOD
mg/I
Coliform; MF Fecal /100ml
Coliform: MF Total /100ml
(Note: Use MPN method for lighly turbid samples)
Dissolved Solids: Total
252_mg/l.
pH (when analyzed)
7.45 Units -
TOC
mg/I
Chloride _
9 mgll
Arsenic
<0.1 mg/I
Grease and Oils
mg/I
Phenol -
mg/1
Sulfate-
mg/l
Specific Conductance
µMhos
TotahAmmonia
0..3_mg/I
(Ammonia Nitrogen; NH, as N Ammonia Nitrogen; Total)
TKN as'N mg/I
ror memewailon �yslems umy tArmcn LaD
tuNIT
WQ0018087 Expiration'Date:
r=Discharge, _- UIC
IDES NC0000663 Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ WaterSource Heat Pump 1 Other: Surface Disposal Re:
Date sample collected: 12/02/16 FIELD ANALYSES:
Well Diameter: 2.0 in. pH 6.4 units Temp. 16.6 °C'
Screened Interval: 3.0 ft. to 13.0ft. Spec. Cond. µMhos
Relative M.P. Elevation: 20.39 ft, ' Odor
Appearance
Laboratory Name: Enyirochem _ Certification No. 37729
colloidal concentrations. -
Nitrite (NO2) as N <0.02 mg/I Pb -Lead _ <Q:016 mg/I
Nitrate (NO3:)' as N. <14.3 mg/I Zn - Zinc 0.011 'mg%I
Phosphorus: Total as P
<0.04 mg/l
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Al - Aluminum
- -__ mg/I
Cobalt - <0.01 mg/1 _
B'a - Barium
mg /I
Selenium - <0.01 mg/1 -
Ca - Calcium
_mg/I
-
Cd - Cadmium
<0.005 mg/I
Chromium: Total
<0.010 mg/I
Cu -Copper<0.010
mg/l
ORGANICSc (by GC, GC/MS, HPLC;)
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Hg - Mercury
<0.0002 mg/I
Report Attached? IR Yes (1)' ❑ No (0)
K.- Potassium
- rngll
VOC, - method # SM 620013
Mg - Magnesium
2.58 mg/i
method # -
Mn --Manganese-
mg/1
method #
Ni - Nickel -_
<0.01 mg/I
, method #
1 otal VOGs:
Effluent Total VOCs: mg/L VOC ,Removal%o
Penny C. Mahoney - Director of Sustainability and Operations Supp
Permittee (or Authorized Agent) Name and Title - Please print or type Signet ur rmittee (or
GW -59 Rev.. 1/2007
at
of

IT FORM
EPARTME NT or ENVIRQNtEifENT & NATURAL RESOURCES'
GROUNDWATER QUALITY MONITORING: � � � � SIONOFWATER ®uAUTY4NFORMAII NPROCESSINGUNIT
COMPLIANCE REPORT FORM 517MAILSERVICECENTER,Rl1lEiGH,k�27$i)9-7617 Pfionec($9$1.735-3221,+
-- —
Please Pdnt Clearly or Type
FACILITI( INFORMATION PERMIT Number: wQ0018087 Expiration Date: Jan. 31, 2021'
Facility Name: DAK Americas LLC, C_ ape 'Fear Site _ _ Non -Discharge UIC -
Permit Name (if different): _ _ NPDES NC0000663 Other
Facility Address: 1205 Culbreth Drive, Suite 100 _ - - _ _ TYPE OF PERMITTED OPERATION BEING MONITORED
Wilmington rs""`' NC 28405_ _ County Brunswick _ El Lagoon ❑ Remediation: infiltration Gallery
(ciy, - (Stale) - VIP) El Spray Field ❑ Remediation:
Contact Person: 'Larry Young _- Telephone#: {•910)264-2564 ❑ Rotary Distributor El Land Application of Sludge
Well Location/Site Name! Down gradient(Monitoring Well # 2BNo. of wells to be sampled: 6 ❑ Water Source Heat Pump X Other. SurfaceDisposal Res .Sol
L ID NUMBER (from Permit): MW #'2B _ Date sample collected: 12/02/16 FIELD ANALYSES: AS
Depth: 13 ft.
Well Diameter: 2.0 in.
pH 6.5. units Temp., 19.g oC
DRY at.
i to Water Level: 7.50 ft. below measuring point
Screened Interval: 3 ft. to 133 ft.
Spec. Cond. - µMhos
time li
sampling,,
wring Point is 2.9 ft. above land surface
Relative M.P. Elevation: 24 ft..
Odor
check
ne of water pumped/bailed before sampling:
12 gallons
Appearance _
here: ❑
)les for metals were collected unfiltered: ®YES
ElNO and field acidified: W YES 11NO
Grease and Oils
mg/I
sample analyzed: 12/02/16-01/08/17 _ LaboratoryName: Envirochem___ _- Certification No. .37729
4METERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/I
Coliform: MF Fecal
/100ml:
Coliform: MF Total
/tooml
(Note: Use MPN method for highly turbidsamples)
mg/I
Dissolved Solids: Total
827 mg/I
pH (when analyzed)
7.02 units
TOC -
mg/I
Chloride
31 mg/I
- Arsenic
<0.1 mg/l
Grease and Oils
mg/I
Phenol _
mg/I
Sulfate
mg/I
Specific Conductance
µMhos
Total Ammonia
82.5 mg/I
(Ammonia Nitrogen; NH3 as, N Ammonia Nitrogen, Total)
TKN. as N mg/I
For Remediation Systems Only (Attach Lab
Nitrite (NO2) as N _ <0.12 mg/I Pb - Lead <0.010 mg/I
Nitrate (NOa) as N <0.2 mg/I Zn - Zinc, 0.026 mgA
Phosphorus: Total as P
<0.04 mg/I
Orthophosphate:
mgll
Other (Specify Compounds and Concentration Units):
Al -Aluminum
mg/I
Cobalt - <0.011 mg/I
Ba - Barium
mg/I
Selenium - <0.01 mg/1
Ca -Calcium
mg/I
Cd - Cadmium
<0.005 _mg/I
Chromium: Total
<0.014 mg/I
Cu - Copper _ ._
-- <0.010 mg/I
ORGANICS:. (by GC, GC/MS, HPLC)
Fe - iron __ .
mg/I
(Specify test and method #. ATTACH'' LAB, REPORT.)
Hg - Mercury
<0.0002 mg/I
Report,Attached? ® Yes (1) D No (0)•
K - Potassium
mg/I
VOC method !# SM 6200C
Mg -Magnesium
12.4 mg/I
method #
"Mn -'Manganese
mg/I
method#
Ni =Nickel
<0.015 mg/I
- _ _ _ _ -_ method #
Influent Total VOCs:' mg/L Effluent Total VOCs: mca/L - VOC
Penny C. Mahoney - Director of Sustainability and Operations Supp Z
Y
Permittee (or Authorized Agent) Name and TitlePlease print or type Signature of` iftee (or Authorized Agent)
GW -59 Rev.. 112007

SUBMIT FORM ON YELLOW PAPER ONLY
For Remediation Systems Only. (Attach. Lab Reports): Influent Total VOCs: mg/L Effluent, Total VOCs: - mg/L VOC Removal%o
Penny C. Mahoney - Director of Sustainability and Operations Supp //J?✓
Permittee (or Authorized Agent) Name and Title- Please print or type 'Signature of Pe ' ee (or
GW -59 Rev. 112007 /
Morr.
•NMPARTMENTDF
ENVIRONMENT 11 NATURAL kESOURCES-
GROUNDWATER QUALITY MONITORING-
.
sIONQFWATER'QUALITY4NFORMATiON,Pii®CESSit4OpNIT
COMPLIANCE REPORT FORM
- -Please
617 MAIL i§ VlcaMTEkRat h,Nc27699-1617 P6 6—(919)73342211_
Print Clearly or Type
FACILITY INFORMATION
PERMIT Number: WQ00180137 Expiration Date: Jan. 31, 2021
DAK Americas LLC, Cape Fear Site
Facility Name: p
_
_
Non -Discharge' - _ _ UIC
Permit Name (if different):
NPDES NC0000663_ _ Other
Facility Address: 1205 Culbreth Drive,, Suite 1,00 -
-_
-
TYPE OF PERMITTED OPERATION` BEING MONITORED
(street) NC 28405 County Brunswick
Wilmington
❑ Lagoon EIRemediationAnf ltration Gallery
(city) (State) (zip)
El Spray Field ❑ Remediation:
Contact Person: , Larry Youngw_
Telephone#: [phone] _
❑ Rotary Distributor ❑ Land Application of Sludge.
Well Location/Site Name: Down gradierit/Monitofing Well # 2C_ No. of wells to be sampled:
-
6
El Water Source Heat Pump 91 other: Surface Disposal Res.8ol
-
_
fromPermit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW # 2C
_ _ Date sample collected: 12/02/16
FIELD ANALYSES':.
WAS
Well Depth: 13 ft.
Well Diameter: 2.0 in.
pH 6.0 units Temp. 18.8 °C
DRY at.
Depth to Water Level: 6.95 ft. below measuring point
Screened Interval: 3 ft. to 13 ft; Spec. Cond, µMhos
time li
sampling:,
Measuring Point is 3.05 ft. above land surface
Relative M.P. Elevation:
25 ft.
Odor
check
Volume of Water pumped/bailed before sampling:
6 gallons
Appearance - -
here' ❑
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: RIYES
❑ NO
LABORATORY
Date sample analyzed: 12/02/16 - 01/18/17_
Laboratory Name: Envirochem
Certification No. 37729
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD Ing/I
Nitrite (NO,) as N
<0.51 mg/I'
Pb - Lead <0.010mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
<0.02, mg/I
Zn - Zinc 0,069_ mg/I
Coliform; MF Total /100ml
Phosphorus: Total as P
<0.8 mg/I.
(Nate: use MPN method for nighty turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids; Total 753 mg/I
AI - Aluminum
mg/I
Cobalt - <0.03.7 mg/1
pH (when analyzed) 6.81 units
13a - Barium
mg/I'
Selenium - <0.01 mg/1
TOC _ mg/I
Ca - Calcium - -_
- mg/l
Chloride. - 12 mg/I
Cd' - Cadmium
<0.005 mg11
_
Arsenic 0.01 mg/I
Chromium: Total
<0.046 mg/i
Grease. and Oils _ - mg/I
Cu —Copper _
<0.015 mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/l
Fe - iron
_. mg/I
(Specify test and method #. ATTACH'LAB REPORT.)
Sulfate - mg/I
Hg - Mercury _
<0,.0002 mull'
Report Attached? 19 Yes (1) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/I
VOC method # SM 6200C
Total Ammonia 0.9 mg/i
Mg - Magnesium
26.1 .mg/l
-_ - method #
(Ammonia Nitrogen; NH,,as:N; Ammonia Nitrogen, Total
Mn - Manganese
mg/I
method '#
TKN as N mg/I'.
Ni - Nickel
<0.056 ;mg/I
method '# -
For Remediation Systems Only. (Attach. Lab Reports): Influent Total VOCs: mg/L Effluent, Total VOCs: - mg/L VOC Removal%o
Penny C. Mahoney - Director of Sustainability and Operations Supp //J?✓
Permittee (or Authorized Agent) Name and Title- Please print or type 'Signature of Pe ' ee (or
GW -59 Rev. 112007 /

FORM ON
TER QUALITY MONITORING:
Y
UNIT
one. (919) 7334221 -
EACIL)rYIN OR� MATION rteaset-nnrueanyorType PERMIT Number:WQ0018087 Expiration 'Date: _Jan. 31,2021
Facility Name. DAK Americas- LLC, Cape Fear Site Non -Discharge _ UIC _
Permit Name (if different): NPDES NC0000663_ Other
Facility Address: 1205 C._ulbreth Drive, Suite 100 TYPE OF PERMITTED OPERATION BEING MONITORED
WilmincIton (stfe'' NC 28405 County Brunswick ❑ Lagoon El Remediation: Infiltration`Gallery
(City, (state) (zip) ❑ Spray Field ❑ Remediation:
Contact Person: Larry_Young Telephone#:: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
ell Location/Site. Name: Down,gradient/Monitoring Well # 2D No. of wells to be sampled: 6 ❑Water Source Heat Pump ®Other: Surface Disposal Res.Sol
L ID NUMBER (from Permit): MW # 2D Date sample collected: 12/02/16
Depth: 13 ft; Well Diameter: 2.0 in.
h to Water,Level: 7.0 ft. below•measuring point Screened Interval: _ 3,'ft. to 13 ft.
wring point is 3.0 ft. above land surface Relative M.P. Elevation: 22 ft.
ne of water, pumped/bailed'before sampling: 10 gallons
sample analyzed
COD
mg/1
Coliform[ MF Fecal
/loom[
Coliform: MF Total,_
/loom[
(Note: Use MPN method for highly turbld samples)
Dissolved Solids: Total _
678 mg/I
pH (when analyzed)
7.53 units
TOC _
mg/I
Chloride
42 mg%I
Arsenic
<0.010 mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
_ _ _ mg/I
Specific Conductance
µMhos
Total Ammonia _
157 mg/I
(Ammonia Nitrogen; N1­13as N; Ammonia Nitrogen, Total)
TKN as N mg/l
For Remediation Systems Only (Attach Lab Reports):
FIELD -ANALYSES: WAS
pH 6.6 units Temp, 19.9 °C DRY at
Spec, Cond., µMhos time of
samplin
Odor check
Appearance here: r-
_ Laboratory Name: Envirochem Certification No. 37729
and colloidal concentrations.
Nitrite (NO2) as N
0.09 mg/1
Pb - Lead <0.010 mg/l
Nitrate (NO3) as N
<0,02. mg/I
Zn - Zinc <0.010 mg/ l
Phosphorus: Total as P _
<0.04 mg/1
Mn - Manganese,
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Al = Aluminum _
mg/l
Cobalt - <0.01 mull
Ba - Barium
mg/1
Selenium,- <0.01 mg/1
Ca - Calcium
mg/l
Cd - Cadmium _
<0.005. mg/I
Chromium: Total
<0.010 mg/1
Cu - Copper
<0.01 a mg/I
ORGANICS: (by GC, GC/MS, HPLC),
Influent
Fe -iron _ _
_.. mgA
Hg - Mercury
<00002 rng/I
K_ Potassium
mg/1
Mg - Magnesium
-7.76 mg/I.
Mn - Manganese,
_ _ mg/I
Ni - Nickel
_ <0.010 mg/I.
Penny C Mahoney Director of Sustainability and Operations Supp
Permittee (or Authorized Agent) Name and Title - Please print or type
GWa59 Rev. 1/2007
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? R Yes (1) ❑ No (0)
VOC method ## SM 62-00C
- _
method#
method #
method #•
Effluent Total VOCs:
VOC Removal%

SUBMIT FORM ON YELLOW PAPER ONLY
For Remediation Systems Only (Attach Lab Reports) Influent Total VOCs:
Penny C. Mahoney - Director of Sustainability and Operations Supp
Permittee (or Authorized Agent) Name and Title - Please print or type
GW -59 Rev. 1/2007
Effluent Total VOCs
VOC Removal%
.
e�a�ttMsetr. e�svl�vrstxe�rr° a ru►ir1.IRat. a�l3purtcEs ; •, ,
-
GROUNDWATER QU
QUALITY MONITORING:
s[arI ca�vw°�
ATEazctuAU Y4NFOR A-R.ONPRoc slNGUNI'r
COMPLIANCE REPORT FORM
..
irNlalt se NICEce"K PALEicH,' K *107 I Nbnp (fl19)1;34221
FACILITY INFORMATION
PERMIT PERMIT Number: WQ0018087 Expiration Date: Jar
Facility Name: DAK Americas LLC, Cape Fear Site
-1-.31,3021
Non -Discharge UIC
Permit Name (if different):
- -
NPDES NC0000663 Other
Facility Address: 1205 C- ulbreth 'Drive, Suite 100
_
TYPE OF PERMITTED OPERATION' BEING MONITORED
Wlr6in ton _ NC 28405 County Brunswick
- —.
❑ Lagoon. ❑ Remediation: Infiltration Gallery
(Cuv1 (State) _ 17'p)
_ _ -.
Spray Field ❑ Remediation:
Contact Person: Larry Young
Telephone#: [phone]
l] Rotary Distributor ❑ Land Application of Sludge
ell Location/Site Name; .Down _gradient/Monitoring Well # 2E No. of wells to be sampled: 6
❑ Water Source Heat Pump ® Other: Surface 'Disposal Res.Sol
fromPermk
SAMPLING INFORMATION,
-
--
If WELL
WELL ID NUMBER (from Permit): MW # 2E_-
Date sample collected: 12/07/16
FIELD ANALYSES:
WAS'
Well Depth:. - 13 ft.
Well Diameter: 2.0 in.
pH 6:0 units Temp.. 17.3 °C
DRY at
Depth to Water Level: 6.55 ft; below measuring point
Screened Interval: 3 ft. to 3
ft. Spec. Gond.µMhos
time of
Measuring Point is 3.0 'ft. above land surface
Relative M.P. Elevation: 23 ft.
Odor - _ - - -.-
sampling;
check
Volume of water pumped/bailed before sampling-
10 gallons
Appearance _
here:
El
Sam les for metals were collected unfiltered: ®YES
❑ NO _ and field acidified: R1 YES . ❑ NO__
LABORATORY INFORMATION
Date sample analyzed: 12/08/16 - 01/18/17
-
Laboratory Name: Enyirochem,
Certification No., 3772.9
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N 0.13 mg/I
Pb - Lead _ <0.030_mg%t
Coliform: MF Fecal /100ml
Nitrate (NOs) as N <o,o2 mg/I
Zn - Zinc <0,03.0 mg/1
Coliform: ,MF Total - _- /Iflon'll
Phosphorus: Total as P 1.42 mg/i
(Note: use•MPN method for highly turbid samples) "
Orthophosphate mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids- Total _ _ _ 138 mg/l
Al -Aluminum_ mg/I
Cobalt - <0:03 mg/i_ _
pH (when analyzed) 5.89 units
Ba.- Barium mg/l
Selenium - <0.03 rng/I
TOC mg/I
Ca - Calcium mgll
<5.0
Chloride mg/I
Cd - Cadmium <0.03 nig/I
Arsenic <0.030 mg/I
Chromium: Total' <0.051_ mg/I
Grease and Oils ,mg/l.
Cu - Copper _ <0.030 ;mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol_ mg/l
Fe -,Iron mgJl
(Specify test and method #. ATTACH LAB REPORT.)_
Sulfate _ ___ - mg/I
Hg - Mercury _ <0.0002 rno
Report Attached? Yes (1') ❑ No (0).
Specific Conductance gMhas
K - Potassium mg/1
VOC _ method # SM 6200C
Total Ammonia 9.5 mg/I
Mg - Magnesium 13.1 mg/l,
method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn -Manganese: mgLl
method
TKN as N _ - -_ mgfl
Ni'- Nickel <0.030 mg/I
method #
For Remediation Systems Only (Attach Lab Reports) Influent Total VOCs:
Penny C. Mahoney - Director of Sustainability and Operations Supp
Permittee (or Authorized Agent) Name and Title - Please print or type
GW -59 Rev. 1/2007
Effluent Total VOCs
VOC Removal%

SUBMIT FORM ONYELLOW PAPER ONLY
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: _ _ - - mg/L Effluent Total VOCs - - __ _ mg/L VOC Removal%
Penny C. Mahoney - Director of Sustainability -and Operations Supp
Permittee (of Authorized Agent) Name and Title - Please print or type
GW -59' Rev. 1/2007
-
EP, IM)FN'1 OFEI ViRONMkNT,ii,NAiURAL'RES,OURCES
GROUNDWATER QUALITY MONITORING.
im"IVISIO
OPWATER QUALIiY4NF6IkMA-if0N-P'RQCESS1NG UNIT
COMPLIANCEREPORT FORM
61TMAIL-SERVICE CENSER,RALEIm4;MC37eg8-1617 Phony (9181,7334221
FACILITY INFORMATION Please Print Clearly or Type
PERMITNumber�wQoo18o87 Expiration Date:Jan. 31, 2021,
Facility Name: DAK Americas LLC, Cape Fear Site
Non -Discharge , _ UIC _
Permit Name (if different):-
NPDES NC0000663 Other -
Facility Address: 1205 Culbreth Drive, Suite 1.00
_ - - - _
TYPE OF PERMITTED OPERATION BEING MONITORED
irecii
Wilmington (SNC 28405 County Brunswick
❑ Lagoon ❑'Remediation:• Infiltration Gallery
(City, ist@tej (z;p)
Spray Field ❑,Remediation: -
Contact Person; Larry Young
Tele hone#: [phone]
P - -
Rotary
❑ Rota Distributor ❑ Land Application of Sludge
ell'Location/Site Name: Background/Monitoring Well #_3A No. of wells to be sampled: 6
❑ Water Source Heat Pump R Other: Surface Disposal Res.Sol
-- ---
.
from Permit _
SAMPLING INFORMATION
_
If WELL
WELL ID NUMBER (from Permit) -i MW # 3A
Date sample collected: 12/07/1.6
FIELD ANALYSES:
WAS.
ell Depth: 3.85 ft,
WeII :Diameter: _ 2.0 in.
pH 6.0 units Temp_ . 17.3 oC.
DRY at
Depth to Water Level:' 1.85 ft. below measuring point
Screened Interval '3.25 ft. to 13.3
ft. Spec: Cond. µMhos
time of
Measurin Point is 1.76ampling„
g ft: above land surface
Relative M.P.MPElevation:',_ 24.78_ft.
Odor
check.
Volume of water pumped/bailed before sampling:
10 gallons
Appearance
here: El
Samples for metals were collected unfiltered: ®YES
❑ NO and field acidified: RYES ❑ NO
LABORATORY_ INEORMATION
Date sample analyzed: 12/08/16-01/1'8/17
Laboratory Name: Envirochem
Certification No. 37729
PARAMETERS NOTE; Values should reflect dissolves'and
colloidal concentrations.
COD _ mg/I'
Nitrite (NO2) as N <0.02 mg/I
Pb - Lead <0.010 mg/1'
Coliform: MF Fecal /loom[
Nitrate ('NO3) as N <0,02 mg/I
Zn - Zinc 0.013 m9/l
Coliform: MF Total /1OOml
Phosphorus: Total as P 0.51 mg/I
-
(Note: use MPN method for highly turbid samples)
Orthophosphate _ - mg/I
Other (Specify Compounds and Concentration Units_):
Dissolved Solids: Total - 47
Al -Aluminum mgll
Cobalt - <0.010 mg/1 _
pH (when analyzed) _ 6.69 units
Be - Barium mgA
Selenium - <0.01 mg)/I
TOC mg/I
Ca - Calcium _ _ _ - mgll
Chloride <5.0 mg/I
Cd - Cadmium <0.005 mg/1
Arsenic <0.01 mg/l
Chromium: Total <0.010 mg/I
Grease and Oils ing/I
Cu - Copper <0.010 mg/I
ORGANICS: (by GC, GC/MS, 'HPLC)
Phenol mg/I
Fe- Iron mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate -_ mg/I
Hg - Mercury _ tO.0002 mg/I
Report Attached? ® Yes (1) ❑ No .(0)
Specific Conductance µMhos
K -,Potassium mg/l
VOC_ _ _ _ _ _ method # 6200C
Total Ammonia _ _ <0.20 mg/l'
Mg = Magnesium 1.26 mg/I
method #
(Ammonia Nitrogen; N%sls N Ammonia Nitrogen, Total)'
Mn - Manganese mgh
method #1
TKN as N mg/I
Ni - Nickel <0.010 mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: _ _ - - mg/L Effluent Total VOCs - - __ _ mg/L VOC Removal%
Penny C. Mahoney - Director of Sustainability -and Operations Supp
Permittee (of Authorized Agent) Name and Title - Please print or type
GW -59' Rev. 1/2007

Summary of Groundwater Monitoring Results'
TEST
PERMIT
LIMIT
UNITS
SAMPLE
DATE
MW-
2A
MW-
2B
MW-
2C
MW-
2D
MW-
2E
RESAMPLE
DATE
MW-
2A
MW-
2B
MW-
2C
MW-
2D
MW -
2E
Ammonia Nitrogen
1.5
mg/L
12/02/16
82.5
157
9.5
01/04/17
83.5
12.8
1.2
Nitrate Nitrogen
10
mg/L
12/02/16
14.3
01/04/16
0.02
Total Dissolved Solids
500
mg/L
12/02/16
827
1 753
1 678
12/31/16
509
1 461
846
See Notes Z, 3, and 4.
' Analytical results not shown in the table above were below the permit limit.
2 Arsenic — Permit Limit 0.01 mg/L. For Well 2C on December 2, 2015, the aresenic level was 0.012 mg/L. Resample on January 4, 2017 was less than 0.01 mg/L.
3 Cadmium — Permit Limit 0.005 mg/L. Initial testing for cadmium conducted for samples collected on December 2 and 7, 2016 showed values less than 0.01 mg/L. This was a
result of the laboratory not performing the test to the proper level. Upon retesting all wells were below the level of 0.005 mg/L.
4 Metals - On December 7, 2016 for MW -2E all metals showed analytical reporting limits that were elevated due to a matix interference. Resample on January 4, 2017 and
subsequent analysis showed test results less than the permit limit for all metals.

DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertovrn Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ° 910.347.5843 Lab/Fax
infonenvironmentalchemists.com
Date of Report: Jan 18, 2017
Customer PO #:
Customer ID: 08100044
Report #: 2016-17309
Project ID: Monitoring Well
Lab ID Sample ID:
16-41717 Site: 2a
Test
Collect Date/Time
12/2/2016 11:15 AM
Method
Matrix Sampled by
Water Larry Young
Results Date Analyzed
Arsenic
EPA 200.7
<0.01 mg/L
12/05/2016
Cadmium
EPA 200.7
<0.005mg/L
01/04/2017
Chromium
EPA 200.7
<0.01 mg/L
12/05/2016
Cobalt
EPA 200.7
<0.01 mg/L
12/05/2016
Copper
EPA 200.7
<0.01 mg/L
12/05/2016
Lead
EPA 200.7
<0.01 mg/L
12/05/2016
Magnesium
EPA 200.7
2.58 mg/L
12/08/2016
Nickel
EPA 200.7
<0.01 mg/L
12/05/2016
Selenium
EPA 200.7
<0.01 mg/L
12/05/2016
Zinc
EPA 200.7
0.011 mg/L
12/05/2016
Mercury
EPA 245.1
<0.0002 mg/L
12/04/2016
Ammonia Nitrogen
EPA 350.1
0.3 mg/L
12/03/2016
Total Dissolved Solids (TDS)
SM 2540 C
252 mg/L
12/05/2016
Chloride
SM 4500 CI E
9 mg/L
12/06/2016
pH
SM 4500 H B
7.45 units
01/18/2017
Total Phosphorus
SM 4500 P F
< 0.04 mg/L
12/06/2016
1,1,1,2 -Tetrachloroethane
SM 6200C
<0.50pg/L
12/9/2016
1,1,1 -Trichloroethane
SM 62000
< 0.50 pg/L
12/9/2016
1,1,2,2 -Tetrachloroethane
SM 62000
< 0.50 pg/L
12/9/2016
1,1,2 -Trichloroethane
SM 62000
< 0.50 pg/L
12/9/2016
1,1-Dichloroethane
SM 62000
< 0.50 pg/L
12/9/2016
1, 1 -Dichloroethene
SM 62000
< 0.50 pg/L
12/9/2016
1,1-Dichloropropene
SM 6200C
< 0.50 pg/L
12/9/2016
1,2;3-Trichlorobenzene
SM 6200C.
< 0.50 pg/L
12/9/2016
1,2,3-Trichloropropane
SM 62000
< 0.50 pg/L
12/9/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/9/2016
Report #.: 2016-17309 Page 1 of 12

�enviro�,chtem
ANALYTICAL & CONSULTING CHEMISTS
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab ® 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ° 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Jan 18, 2017
Customer PO #:
Customer ID: 08100044
Report #: 2016-17309
Project ID: Monitoring Well
1,2,4-Trimethylbenzene
SM 62000
< 0.50 pg/L
12/9/2016
1,2-Dibromo-3-Chloropropane
SM 6200c
< 0.50 pg/L
12/9/2016
1,2-Dibromoethane
SM 62000
< 0.50 pg/L
12/9/2016
1,2 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/9/2016
1,2-Dichloroethane
SM 6200c
< 0.50 pg/L
12/9/2016
1,2-Dichloropropane
SM 6200c
< 0.50 pg/L
12/912016
1,3,5-Trimethylbenzene
SM 6200c
< 0.50 pg/L
12/9/2016
1,3 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/9/2016
1, 3-Dichloropropane
SM 6200c
< 0.50 pg/L
12/9/2016
1,4 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/9/2016
2,2-Dichloropropane
SM 62000
< 0.50 pg/L
12/9/2016
,2-Chlorotoluene
SM 6200c
< 0.50 pg/L
12/9/2016
4-Chlorotoluene
SM 6200c
< 0.50 pg/L
12/9/2016
Benzene
SM 6200c
< 0.50 pg/L
12/9/2016
Bromobenzene
SM 6200c
< 0.50 pg/L
12/9/2016
Bromochloromethane
SM 6200c
< 0.50 pg/L
12/9/2016
Bromodichloromethane
SM 6200C
< 0.50 pg/L
12/9/2016
Bromoform
SM 6200c
< 0.50 pg/L
12/9/2016
Bromomethane
SM 6200c
<'0.50 pg/L
12/9/2016
Carbon tetrachloride
SM 6200c
< 0.50 pg/L
12/9/2016
Chlorobenzene
SM 6200c
< 0.50 pg/L
12/9/2016
Chloroethane
SM 6200c
< 0.50 pg/L
12/9/2016
Chloroform
SM 6200c
< 0.50 pg/L
12/9/2016
Chloromethane
SM 6200c
< 0.50 pg/L
12/9/2016
cis-1,2-Di6hloroethene
SM 6200c
< 0.50 pg/L
12/9/2016
cis-1,3-Dichloropropene
SM 6200c
< 0.50 pg/L
12/9/2016
Dibromochloromethane
SM 62000
< 0.50 pg/L
12/9/2016
Dibromomethane
SM 6200c
< 0.50 pg/L
12/9/2016
Dichlorodifluoromethane
SM 6200c
< 0.50 pg/L
12/9/2016
Ethylbenzene
SM 62000
< 0.50 pg/L
12/9/2016
Report #:: 2016-17309
m
Page 2 of 12

Environmental Chemists, Inc.
® 6602 Windmill Way, Wilmington, NC 28405 0 910.392.0223 Lab ® 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
DAK Americas
Date of Report: Jan 18, 2017
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention: Larry Young
Report #: 2016-17309
Project ID: Monitoring Well
Hexachlorobutadiene
SM 6200C
< 0.50 pg/L
12/9/2016
I sopropyl benzene
SM 62000
< 0.50 pg/L
12/9/2016
M+P Xylene
SM 62000
< 1.00 pg/L
12/9/2016
Methylene chloride
SM 62000
< 0.50 pg/L
12/9/2016
Naphthalene
SM 62000
< 0.50 pg/L
12/9/2016
n-Butylbenzene
SM 62000
< 0.50 pg/L
12/9/2016
n-Propylbenzene
SM 62000
< 0.50 pg/L ,
12/9/2016
ortho-Xylene
SM 6200C
< 0.50 pg/L
12/9/2016
p-isopropyltoluene
SM 62000
< 0.50 pg/L ,
12/9/2016
sec-Butylbenzene
SM 6200C
< 0.50 pg/L
12/9/2016
Styrene
SM 62000
< 0.50 pg/L
12/9/2016
tert-Butylbenzene
SM 6200C
< 0.50 pg/L
12/9/2016
Tetrachloroethene
SM 62000
< 0.50 pg/L
12/9/2016
Toluene
SM 62000
< 0.50 pg/L
12/9/2016
Trans-1,2-Dichloroethene
SM 6200C
< 0.50 pg/L.
12/9/2016
Trans-1,3-dichloropropene
SM 6200C
< 0.50 pg/L
12/9/2016
Trichloroethene
SM 62000
< 0.50 pg/L
12/9/2016
Trichlorofluoromethane
SM 6200C
< 0.50 pg/L
12/9/2016
Vinyl chloride
SM 6200C
< 0.50 pg/L
12/9/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/02/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 14.3 mg/L 12/07/2016
Nitrate Nitrogen Subtraction Method 14.3 mg/L 12/15/2016
Report #:: 2016-17309 Page 3 of 12

en��
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 o 910.392.0223 Lab ® 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 o 910.347.5843 Lab/Fax
[e-mail]
enviromnentalchemists.com
DAK Americas Date of Report: Jan 18, 2017
1205 Culbreth Drive Suite 200 Customer PO #:
Wilmington NC 28405 Customer ID: 08100044
Attention: Larry Young Report #: 2016-17309
Project ID: Monitoring Well
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-41718 Site: 2b 12/2/2016 11:45 AM Water Larry Young
Test I Method Results Date Analyzed
Arsenic
EPA 200.7
<0.01 mg/L
12/05/2016
Cadmium
EPA 200.7
<0.005 mg/L
01/134/2017
Chromium
EPA 200.7
0.014mg/L
12/05/2016
Cobalt
EPA 200.7
0.011 mg/L
12/05/2016
Copper
EPA 200.7
<0.01 mg/L
12/05/2016
Lead
EPA 200.7
<0.01 mg/L
12/05/2016
Magnesium
EPA 200.7
12.4 mg/L
12/07/2016
Nickel
EPA 200.7
0.015 mg/L
12/05/2016
Selenium
EPA 200.7
<0.01 mg/L
12/05/2016
Zinc
EPA 200.7
0.026 mg/L
12/05/2016
Mercury
EPA 245.1
<0.0002 mg/L
12/04/2016
Ammonia Nitrogen
EPA 350.1
82.5 mg/L
12/05/2016
Total Dissolved Solids (TDS)
SM 2540 C
827 mg/L
12/05/2016
Chloride
SM 4500 C1 E
31 mg/L
12/06/2016
pH
SM 4500 H B
7.02 units
01/18/2017
Total Phosphorus
SM 4500 P F
< 0.04 mg/L
12/10/2016
1,1,1,2 -Tetrachloroethane
SM 6200C
< 0.50 lag/L
12/9/2016
1,1,1 -Trichloroethane
SM 6200C
< 0.50 lag/L
12/9/2016
1,1,2,2 -Tetrachloroethane
SM 6200c
< 0.50 lag/L
12/9/2016
1,1,2 -Trichloroethane
SM 6200c
< 0.50 lag/L
12/9/2016
1,1-Dichloroethane .
SM 6200c
< 0.50 lag/L
12/9/2016
1,1-Dichloroethene
SM 6200c
< 0.50 lag/L
12/9/2016
1, 1 -Dichloropropene
SM 62000
< 0.50 pg/L
12/9/2016
1,2,3-Trichlorobenzene
SM 6200c
< 0.50 lag/L
12/9/2016
1,2,3-Trichloropropane
SM 62000
< 0.50 lag/L
12/9/2016
1,2,4-Trichlorobenzene
SM 6200c
< 0.50 lag/L
12/9/2016
Report #.: 2016-17309 Page 4 of 12

ANALYTICAL & CONSULTING CHEMISTS
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Environmental 'Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 o 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 o 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Jan 18; 2017
Customer PO #:
Customer ID: 08100044
Report #: 2016-17309
Project ID: Monitoring Well
1,2,4-Trimethylbenzene
SM 6200c
< 0.50 pg/L
12/9/2016
1,2-Dibromo-3-Chloropropane
SM 6200c
< 0.50 pg/L
12/9/2016
1,2-Dibromoethane
sM 62ooc
< 0.50 pg1L
12/9/2016
1,2 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/9/2016
1,2-Dichloroethane
SM 6200c
< 0.50 pg/L
12/9/2016
1,2-Dichloropropane
SM 6200c
< 0.50 pg/L
12/9/2016
1,3,5-Trimethylbenzene
SM 6200c
< 0.50 pg/L
12/9/2016
1,3 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/9/2016
1,3-Dichloropropane
SM 6200c
< 0.50 pg/L
12/9/2016
1,4 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/9/2016
2,2-Dichloropropane
SM 6200c
< 0.50 pg/L
12/9/2016
2-Chlorotoluene
SM 6200C
< 0.50.pg/L
12/9/2016
4-Chlorotoluene
SM 6200C
< 0.50 pg/L
12/9/2016
Benzene
SM 62000
< 0.50 pg/L
12/9/2016
Bromobenzene
SM 6200C
< 0.50 pg/L
12/9/2016
Bromochloromethane
SM 6200c
< 0.50 pg/L
12/9/2016
Bromodichloromethane
SM 62000
< 0.50 pg/l-
12/9/2016
Bromoform
SM 6200c
< 0.50 pg/L
12/9/2016
Bromomethane
SM 6200c
< 0.50 pg/L
12/9/2016
Carbon tetrachloride
SM 62000
< 0.50 pg/L
12/9/2016
Chlorobenzene
SM 6200c
< 0.50 pg/L
12/9/2016
Chloroethane
SM 6200C
< 0.50 pg/L
12/9/2016
Chloroform
SM 6200C
< 0.50 pg/L
12/9/2016
Chloromethane
SM 62600
< 0.50 pg/L
12/9/2016
cis-1,2-Dichloroethene
SM 6200C
< 0.50 pg/L
12/9/2016
cis- 1, 3-Dich loropropene
5M 6200C
< 0.50 pg/L
12/9/2016
Dibromochloromethane
SM 6200C
< 0.50 pg/L
12/9/2016
Dibromomethane
SM 6200c
< 0.50 pg/L
12/9/2016
Dichlorodifluoromethane
SM 62000
< 0.50 pg/L
12/9/2016
Ethylbenzene
SM 62000
< 0.50 pg/L
12/9/2016
Report#:: 2016-17309
Page 5 of 12

e 8 Y 'c
�env�irtc�i' t
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab o 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 o 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax
[e-mail]
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Date of Report: Jan 18, 2017
Customer PO #:
Customer ID: 08100044
Report #: 2016-17309
Project ID: Monitoring Well
Hexachlorobutadiene
SM 62000
< 0.50 pg/L
12/9/2016
Isopropylbenzene
SM 6200C
< 0.50 pg/L
12/9/2016
M+P Xylene
SM 6200c
< 1.00 pg/L
12/9/2016
Methylene chloride
SM 62000
< 0.50 pg/L
12/9/2016
Naphthalene
SM 62000
< 0.50 pg/L
12/9/2016
n-Butylbenzene
SM 62000
< 0.50 pg/L
12/9/2016
n-Propylbenzene
SM 6200c
< 0.50 pg/L
12/9/2016
ortho-Xylene
SM 6200c
< 0.50 pg/L
12/9/2016
p-Isopropyltoluene
SM 6200c
< 0.50 pg/L
12/9/2016
sec-Butylbenzene
SM 6200c
< 0.50 pg/L
12/9/2016
Styrene
SM 6200c
< 0.50 pg/L
12/9/2016
tert-Butylbenzene
SM 6200c
< 0.50 pg/L
12/9/2016
Tetrachloroethene
SM 62000
< 0.50 pg/L
12/9/2016
Toluene
SM 620oc
< 0.50 pg/L
12/9/2016
Trans-1,2-Dichloroethene
SM 6200c
< 0.50 pg/L
12/9/2016
Trans-1,3-dichloropropene
SM 6200c
< 0.50 pg/L
12/9/2016
Trichloroethene
SM 6200c
< 0.50 pg/L
12/9/2016
Trichlorofluoromethane
SM 6200c
< 0.50 pg/L
12/9/2016
Vinyl chloride
SM 6200c
< 0.50 pg/L
12/9/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2
0.12 mg/L
12/02/2016
Nitrate+Nitrite-Nitrogen
EPA 353.2
< 0.02 mg/L
12/07/2016
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
12/15/2016
Report #:: 2016-17309 Page 6 of 12

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab ° 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Date of Report: Jan 18, 2017
Customer PO #:
Customer ID: 08100044
Report #: 2016-17309
Project ID: Monitoring Well
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
16-41719 Site: 2C
12/2/2016 12:36 PM Water Larry Young
Test
Method
Results Date Analyzed
Arsenic
EPA 200.7
0.012mg/L
12/07/2016
Cadmium
EPA 200.7
<0.005mg/L
01/04/2017
Chromium
EPA 200.7
0.046 mg/L
12/07/2016
Cobalt
EPA 200.7
0.037 mg/L
12/07/2016
Copper
EPA 200.7
0.015 mg/L
12/07/2016
Lead
EPA 200.7
<0.01 mg/L
12/07/2016
Magnesium
EPA 200.7
26.1 mg/L
12/07/2016
Nickel
EPA 200.7
0.056 mg/L
12/07/2016
Selenium
EPA 200.7
<0.01 mg/L
12/07/2016
Zinc
EPA 200.7
0.069 mg/L
12/07/2016
Mercury
EPA 245.1
<0.0002mg/L
12/04/2016
Ammonia Nitrogen
EPA 350.1
0.9 mg/L
12/03/2016
Total Dissolved Solids (TDS)
SM 2540 C
753 mg/L
12/05/2016
Chloride
SM 4500 ci E
12 mg/L
12/06/2016
pH
SM 4500 H B
6.81 units
01/18/2017
Total Phosphorus
SM 4500 P F
0.80 mg/L
12/10/2016
1,1,1,2 -Tetrachloroethane
SM 62000
< 0.50 pg/L
12/9/2016
1,1,1 -Trichloroethane
SM 62000
< 0.50 pg/L
12/9/2016
1,1,2,2 -Tetrachloroethane
SM 62000
< 0.50 pg/L
12/9/2016
1,1,2=Trichloroethane
SM 62000
< 0.50 pg/L
r
12/9/2016
1,1-Dichloroethane
SM 62000
< 0.50 pg/L
12/9/2016
1, 1 -Dichloroethene
SM 62000
< 0.50 pg/L
12/9/2016
1,1-Dichloropropene
SM 62000
< 0.50 pg/L
12/9/2016
1,2,3-Trichlor6benzene
SM 62000
< 0.50 pg/L
12/9/2016
1,2,3-Trichloropropane
SM 62000
< 0.50 pg/L
12/9/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/9/2016
Report#:: 2016-17309 Page 7 of 12

DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Environmental Chemists, Inco
6602 Windmill Way, Wilmington, NC 28405 m 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ® 910.347.5843 Lab/Fax
info@envi ronmentalchemists.com
Date of Report: Jan 18, 2017
Customer PO #:
Customer ID: 08100044
Report #: 2016-17309
Project ID: Monitoring Well
1,2,4-Trimethylbenzene
SM 62000
< 0.50 pg/L
12/9/2016
1,2-Dibromo-3-Chloropropane
SM 6200C
< 0.50 pg/L
12/9/2016
1,2-Dibromoethane
SM 6200c
< 0.50 pg/L
12/9/20161
1,2 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/912016,
2/912016-
1,2-Dichloroethane
1,2-Dichloroethane
sM 6200c
< 0.50 pg/L
12/9/2016
1,2-Dichloropropane
SM 6200c
< 0.50 pg/L
12/9/2016
1,3,5-Trimethylbenzene
SM 6200c
< 0.50 pg/L
12/9/2016
1,3 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/9/2016
1,3-Dichloropropane
SM 6200c
< 0.50 pg/L
12/9/2016
1,4 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/9/2016
2,2-Dichloropropane
SM 6200c
< 0.50 pg/L
12/9/2016
2-Chlorotoluene
SM 6200c
< 0.50 pg/L
12/9/2016
4-Chlorotoluene
SM 6200c
< 0.50 pg/L
12/9/2016
Benzene
SM 6200c
< 0.50 pg/L
12/9/2016
Bromobenzene
SM 6200c
< 0.50 pg/L
12/9/2016
Bromochloromethane
SM 6200c
< 0.50 pg/L
12/9/2016
Bromodichloromethane
SM 6200c
< 0.50 pg/L
12/9/2016
Bromoform
SM 6200c
< 0.50 pg/L
12/9/2016
Bromomethane
SM 6200c
< 0.50 pg/L
12/9/2016
Carbon tetrachloride
SM 6200c
< 0.50 pg/L
12/9/2016
Chlorobenzene
SM 6200c
< 0.50 pg/L
12/9/2016
Chloroethane
SM 6200c
< 0.50 pg/L
12/9/2016
Chloroform
SM 6200c
< 0.50 pg/L
12/9/2016
Chloromethane
SM 6200c
< 0.50 pg/L
12/9/2016
cis-1,2-Dichloroethene
SM 6200c
< 0.50 pg/L
12/9/2016
cis-1,3-Dichloropropene
SM 6200c
< 0.50 pg/L
12/9/2016
Dibromochloromethane
SM 6200c
< 0.50 pg/L
12/9/2016
Dibromomethane
SM 6200c
< 0.50 pg/L
12/9/2016
Dichlorodifluoromethane
SM 5200c
< 0.50 pg/L
12/9/2016
Ethylbenzene
SM 6200c
< 0.50 pg/L
12/9/2016
Report #:: 2016-17309
Page 8 of 12

ANALYTICAL & CONSULTING CHEMISTS
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Environmental Chemists, Inc®
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, lvianteo, NC 27954 e 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Jan 18, 2017
Customer PO #:
Customer ID: 08100044
Report #: 2016-17309
Project ID: Monitoring Well
Hexachlorobutadiene
SM 62000
< 0.50 pg/L
12/9/2016
Isopropylbenzene
SM 6200C
< 0.50 pg/L
12/9/2016
M+P Xylene
SM 6200C
< 1.00 pg/L
12/9/2016
Methylene chloride.
SM 6200c
< 0.50 pg/L
12/9/2016
Naphthalene
SM 62000
< 0.50 pg/L
12/9/2016
n-Butylbenzene
SM 62000
< 0.50 pg/L
12/9/2016
n-Propylbenzene
SM 62000
< 0.50 pg/L
12/9/2016
ortho-Xylene
SM 6200C
< 0.50 pg/L
12/9/2016
p-Isopropyltoluene
SM 6200c
< 0.50 pg/L
12/9/2016
sec-Butylbenzene
SM 62000
< 0.50 pg/L
12/9/2016
Styrene
SM 62000
< 0.50 pg/L
12/9/2016
tert-Butylbenzene
SM 62000
< 0.50 pg/L
12/9/2016
Tetrachloroethene
SM 6200c
< 0.50 pg/L
12/9/2016
Toluene
SM 62000
< 0.50 pg/L
12/9/2016
Trans-1,2-Dichloroethene
SM 6200c
< 0.50 pg/L
12/9/2016
Trans-1,3-dichloropropene
SM 6200c
< 0.50 pg/L
12/9/2016
Trichloroethene
SM 6200C
< 0.50 ltg/L
12/9/2016
Trichlorofluoromethane
SM 6200c
< 0.50 pg/L
12/9/2016
Vinyl chloride
SM 6200c
< 0.50 pg/L
12/9/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2
0.51 mg/L
12/02/2016
Nitrate+Nitrite-Nitrogen
EPA 353.2
0.14 mg/L
12/07/2016
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
12/15/2016
Report *: 2016-17309 Page 9 of 12

ye�nvr�o�h�
b � �
ANALYTICAL & CONSULTING CHEMISTS
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention: Larry Young
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab 0 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 o 910.347.5843 Lab/Fax
infoivenvironmentalchemists.com
Date of Report: Jan 18, 2017
Customer PO #:
Customer ID: 08100044
Report #: 2016-17309
Project ID: Monitoring Well
Lab ID Sample ID:
16-41720 Site: 2d
Test
Collect Date/Time
12/2/2016 1:20 PM
Method
Matrix Sampled by
Water Larry Young
Results Date Analyzed
Arsenic
EPA 2001
<0.01 mg/L
12/05/2016
Cadmium
EPA 200.7
<0.005mg/L
01/04/2017
Chromium
EPA 200.7
0.010 mg/L
12/05/2016
Cobalt
EPA 200.7
<0.01 mg/L
12/05/2016
Copper
EPA 200.7
<0.01 mg/L
1210512016
Lead
EPA 200.7
<0.01 mg/L
12/05/2016
Magnesium
EPA 200.7
7.76 mg/L
12/07/2016
Nickel
EPA 200.7
<0.01 mg/L
12/05/2016
Selenium
EPA 200.7
<0.01 mg/L
12/05/2016
Zinc
EPA 200.7
<0.01 mg/L
12/05/2016
Mercury
EPA 245.1
<0.0002 mg/L
12/04/2016
Ammonia Nitrogen
EPA 350.1
157 mg/L
12/05/2016
Total Dissolved Solids (TDS)
SM 2540 C
678 mg/L
12/05/2016
Chloride
SM 4500 Ct E
42 mg/L
12%06/2016
pH
SM 4500 H e
7.53 units
01/18/2017
Total Phosphorus
SM 4500 P F
< 0.04 mg/L
12/10/2016
1,1,1,2 -Tetrachloroethane
SM 62000
< 0.50 tag/L
12/7/2016
1,1,1 -Trichloroethane
SM 6200C
< 0.50 tag/L
12/7/2016
1,1,2,2 -Tetrachloroethane
SM 62000
< 0.50 tag/L
12/7/2016
1,1,2 -Trichloroethane
SM 62000
< 0.50 tag/L
12/7/2016
1,1-Dichloroethane
SM 62000
< 0.50 tag/L
12/7/2016
1,1-Dichloroethene
SM 62000
< 0.50 tag/L
12/7/2016
1, 1 -Dichloropropene
SM 6200c
< 0.50 tag/L
12/7/2016
1,2,3-Trichlorobenzene
SM 62000
< 0.50 tag/L
12/7/2016
1,2,3-Trichloropropane
SM 62000
< 0.50 tag/L
1217/2016
1,2,4-Trichlorobenzene
SM 62000
< 0.50 tag/L
12/7/2016
Report #:: 2016-17309 Page 10 of 12

ANALYTICAL & CONSULTING CHEMISTS
77
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ° 910.392.0223 Lab L 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ° 252.473.5702 Lab/Pax
255-A Wilmington Highway, Jacksonville, NC 28540 1, 910.347.5843 Lab/Fax
[e-mail]
DAK Americas
Date of Report: Jan 18, 2017
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington IVC 28405
Customer ID: 08100044
Attention: Larry Young
Report #: 2016-17309
Project ID: Monitoring Well
1,2,4-Trimethylbenzene
SM 62000
< 0.50 pg/L
121712016
1,2-Dibromo-3-Chloropropane
SM 62000
< 0.50 pg/L
12/7/2016
1,2-Dibromoethane
SM 6200C
< 0.50 pg/L
12/7/2016
1,2 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/7/2016
1,2-Dichloroethane
SM 62000
< 0.50 pg%L
12/7/2016
1,2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/7/2016
1,3,5-Trimethylbenzene
SM 62000
< 0.50 pg/L
12/7/2016
1,3 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/7/2016
1,3-Dichloropropane
SM 62000
< 0.50 pg/L
12/7/2016
1,4 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/7/2016
2,2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/7/2016
2-Chlorotoluene
SM 62000
< 0.50 pg/L
12/7/2016
4-Chlorotoluene
SM 62000
< 0.50 pg/L
12/7/2016
Benzene
SM 62000
< 0.50 pg/L
12/7/2016
Bromobenzene
SM 62000
< 0.50 pg/L
12/7/2016
Bromochloromethane
SM 62000
< 0.50 pg/L
12/7/2016
Bromodichloromethane
SM 62000
< 0.50 pg/L
12/7/2016
Bromoform
SM 62000
< 0.50 pg/L
12/7/2016
Bromomethane
SM 62000
< 0.50 pg/L
12/7/2016
Carbon tetrachloride
SM 62000
< 0.50 pg/L
12/7/2016
Chlorobenzene
SM 62000
< 0.50 pg/L
12/7/2016
Chloroethane
SM 62000
< 0.50 pg/L
12/7/2016
Chloroform
SM 6200C
< 0.50 pg/L
12/7/2016
Chloromethane
SM 6200C
< 0.50 pg/L
12/7/2016
cis-1,2-Dichloroethene
SM 62000
< 0.50 pg/L
12/7/2016
cis-1,3-Dichloropropene
SM 62000
< 0.50 pg/L
12/7/2016
Dibromochloromethane
SM 62000
< 0.50 pg/L
12/7/2016
Dibromomethane
SM 6200C
< 0.50 pg/L
12/7/2016
Dichlorodifluoromethane
SM 62000
< 0.50 pg/L
12/7/2016
Ethylbenzene
SM 62000
< 0.50 pg/L
12/7/2016
Report #:: 2016-17309
Page 11 of 12

l i ffi a.,
.� en¢�viroche�
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab O 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
DAK Americas
Date of Report: Jan 18, 2017
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention: Larry Young
Report #: 2016-17309
Project ID: Monitoring Well
Hexachlorobutadiene
SM 6200C
< 0.50 pg/L
12/7/2016
Isopropylbenzene
SM 6200c
< 0.50 pg/L
12/7/2016
M+P Xylene
SM 6200c
< 1.00 pg/L
12/7/2016
Methylene chloride
SM 6200c
< 0.50 pg/L
12/7/2016
Naphthalene
SM 6200c
< 0.50 pg/L
12/7/2016
n-Butylbenzene
SM 6200c
< 0.50 pg/L
12/7/2016
n-Propylbenzene
SM 62000
< 0.50 pg/L
12/7/2016
ortho-Xylene
SM 6200c
< 0.50 pg/L
12/7/2016
p-Isopropyltoluene
SM 6200c
< 0.50 pg/L
12/7/2016
sec-Butylbenzene
SM 6200c
< 0.50 pg/L
12/7/2016
Styrene
SM 6200c
< 0.50 pg/L
12/7/2016
tert-Butylbenzene
SM 62000
< 0.50 pg/L
12/7/2016
Tetrachloroethene
SM 62000
< 0.50 pg/L
12/7/2016
Toluene
SM 6200c
< 0.50 pg/L
12/7/2016
Trans-1,2-Dichloroethene
SM 62000
< 0.50 pg/L
12/7/2016
Trans-1,3-dichloropropene
SM 6200c
< 0.50 pg/L
12/7/2016
Trichloroethene
SM 62000
< 0.50 pg/L
12/7/2016
Trichlorofluoromethane
SM 6200C
< 0.50 pg/L
12/7/2016
Vinyl chloride
SM 62000
< 0.50 pg/L
12/7/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 0.09 mg/L 12/02/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/07/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2016
Comment:
Reviewed by:
P
Report #:: 2016-17309 Page 12 of 12

`"u. � � •. °gyp ya.s�aa$:
g
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab o 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
DAK Americas
Date of Report: Jan 18, 2017
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention:
Report #: 2016-17594
Project ID: Monitoring Well
Lab ID Sample ID: DAK
Collect Date/Time Matrix Sampled by
16-42401 Site: 2E
12/7/2016 2:36 PM Water Larry Young
Test Method
Results Date Analyzed
Arsenic EPA 200.7
<0.03 mg/L
12/19/2016
Reporting limit elevated due to matrix interference.
Cadmium EPA 200.7
<0.03 mg/L
12/19/2016
Reporting limit elevated due to matrix interference.
Chromium EPA 200.7
0.051 mg/L
12/19/2016
Reporting limit elevated due to matrix interference.
Cobalt EPA 200.7
<0.03 mg/L
12/19/2016
Reporting limit elevated due to matrix interference.
Copper EPA 200.7
<0.03 mg/L
12/19/2016
Reporting limit elevated due to matrix interference.
Lead EPA 200.7
<0.03 mg/L
12/19/2016
Reporting limit elevated due to matrix interference.
Magnesium EPA 2007
3.31 mg/L
12/15/2016
Nickel EPA 200.7
<0.03mg/L
12/19/2016
Reporting limit elevated due to matrix interference.
Selenium EPA 200.7
<0.03 mg/L
12/19/2016
Reporting limit elevated due to matrix interference.
Zinc EPA 200.7
<0.03 mg/L
12/19/2016
Reporting limit elevated due to matrix interference.
Mercury EPA 245.1
<0.0002 mg/L
12/16/2016
Ammonia Nitrogen EPA 350.1
9.5 mg/L
12/09/2016
Nitrite Nitrogen EPA 353.2
0.21 mg/L
12/08/2016
Total Dissolved Solids (TDS) SM 2540 c
138 mg/L
12/08/2016
Chloride SM 4500 Cl E
< 5 mg/L
12/13/2016
pH SM 4500 H s
5.89 units
01/18/2017
Total Phosphorus SM 4500 P F
1.42 mg/L
1 2/1 012 0 1 6
1,1,1,2 -Tetrachloroethane SM 6200c
< 0.50 pg/L
12/11/2016
1,1,1 -Trichloroethane SM 6200c
< 0.50 pg/L
12/1112016
1,1,2,2 -Tetrachloroethane SM 6200C
<0.50pg/L
12/11/2016
Report #:: 2016-17594
Page 4 of 7

b
eng roti -he
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inco
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab ® 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
DAK Americas
Date of Report: Jan 18, 2017
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention:
Report #: 2016-17594
Project ID: Monitoring Well
1,1,2 -Trichloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,1-Dichloroethane
SM 62000
< 0.50 pg/L
12/11/2016
1,1-Dichloroethene
SM 62000
< 0.50 pg/L
12/11/2016
1,1-Dichloropropene
SM 62000
< 0.50 pg/L
12/11/2016
1,2,3-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2,3-Trichloropropane
SM 6200C
< 0.50 pg/L
12/11/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2,4-Trimethylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2-Dibromo-3-Chloropropane
SM 62000
< 0.50 pg/L
12/11/2016
1,2-Dibromoethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,2 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2-Dichloroethane
SM 62000
< 0.50 pg/L
12/11/2016
1,2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/11/2016
1, 3,5-Trimethyl benzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,3 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/11/2016
1,3-Dichloropropane
SM 6200C
< 0.50 pg/L
12/11/2016
1,4 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/11/2016
2,2-Dichloropropane
SM 6200c
< 0.50 pg/L
12/11/2016
2-Chlorotoluene
SM 6200c
< 0.50 pg/L
12/11/2016
4-Chlorotoluene
SM 62000
< 0.50 pg/L
12/11/2016
Benzene
SM 6200c
< 0.50 pg/L
12/11/2016
Bromobenzene
SM 62000
< 0.50 pg/L
12/11/2016
Bromochloromethane
SM 62000
< 0.50 pg/L
12/11/2016
Bromodichloromethane
SM 6200C
< 0.50 pg/L
12/11/2016
Bromoform
SM 62000
< 0.50 pg/L
12/11/2016
Bromomethane
SM 6200c
< 0.50 pg/L
12/11/2016
Carbon tetrachloride
SM 62000
< 0.50 pg/L
12/11/2016
Chlorobenzene
SM 6200c
< 0.50 pg/L
12/11/2016
Chloroethane
SM 6200c
< 0.50 pg/L
12/11/2016
Chloroform
SM 6200c
< 0.50 pg/L
12/11/2016
Report M: 2016-17594
Page 5 of 7
0

en�i ,-,O' X g
- �- • �q
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ° 910.392.0223 Lab ° 910.392.4424 Fax
710 Sowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ® 910.347.5843 Lab/Fax
[e-mail]
DAK Americas
Date of Report: Jan 18, 2017
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention:
Report #: 2016-17594
Project ID: Monitoring Well
Chloromethane
SM 62000
< 0.50 ug/L
12/11/2016
cis- 1, 2-Dichloroethene
SM 62000
< 0.50 pg/L
12/11/2016
cis-1,3-Dichloropropene
SM 6200C
<0.50ug/L
12/11/2016
Dibromochloromethane
SM 6200C
< 0.50 pg/L
12/11/2016
Dibromomethane
SM 6200c
< 0.50 pg/L
12/11/2016
Dichlorodifluoromethane
SM 62000
< 0.50 ug/L
12/11/2016
Ethylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
Hexachlorobutadiene
SM 6200C
< 0.50 pg/L
12/11/2016
Isopropylbenzene
SM 62000
< 0.50 pg/L
12/11/2016
M+P Xylene
SM 62000
< 1.00 pg/L
12/11/2016
Methylene chloride
SM 6200c
< 0.50 pg/L
12/11/2016
Naphthalene
SM 62000
< 0.50 pg/L
12/11/2016
n-Butylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
n-Propylbenzene
SM 6200c
< 0.50 pg/L
12/11/2016
ortho-Xylene
SM 6200C
< 0,50 pg/L
12/11/2016
p-Isopropyltoluene
SM 62000
< 0.50 pg/L
12/11/2016
sec-Butylbenzene
SM 6200c
< 0.50 pg/L
12/11/2016
Styrene
SM 6200c
< 0.50 pg/L
12111/2016
tert-Butylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
Tetrachloroethene
SM 6200c
< 0.50 pg/L
12/11/2016
Toluene
SM 62000
< 0.50 pg/L
12/11/2016
Trans-1,2-Dichloroethene
SM 6200C
<0.50pg/L
12/11/2016
Trans-1,3-dichloropropene
SM 6200c
<0.50pg/L
12/11/2016
Trichloroethene
SM 62000
< 0.50 pg/L
12/11/2016
Trichlorofluoromethane
SM 6200c
< 0.50 pg/L
12/11/2016
Vinyl chloride
SM 62000
< 0.50 pg/L
12/11/2016
Nitrate Nitrogen (Calc)
Nitrate+Nitrite-Nitrogen
EPA 353.2
0.13 mg/L
12/08/2016
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
12/20/2016
Report #:: 2016-17594 Page 6 of 7

.�ervirochen
ANALYTICAL & CONSULTING CHEMISTS
DAK Americas
1205 Culbreth Drive Suite 200
Wilmington NC 28405
Attention:
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab ° 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax
Comment:(� c,
Reviewed by:UR�1
[e-mail]
environmentalchemists.com
Date of Report: Jan 18, 2017
Customer PO #:
Customer ID: 08100044
Report #: 2016-17594
Project ID: Monitoring Well
Report #:: 2016-17594
Page 7 of 7

I
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab ® 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ° 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
DAK Americas
Date of Report: Jan 18, 2017
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention:
Report #: 2016-17594
Project ID: Monitoring Well
Lab ID Sample ID: DAK
Collect Date/Time Matrix Sampled by
16-42395 Site: 3A
12/7/2016 12:28 PM Water Larry Young
Test
Method
Results Date Analyzed
Arsenic
EPA 200.7
<0.01 mg/L
12/14/2016
Cadmium
EPA 200.7
<0.005mg/L
01/04/2017
Chromium
EPA 200.7
<0.01 mg/L
12/14/2016
Cobalt
EPA 200.7
<0.01 mg/L
12/14/2016
Copper
EPA 200.7
<0.01 mg/L
12/14/2016
Lead
EPA 200.7
<0.01 mg/L
12/14/2016
Magnesium
EPA 200.7
1.26 mg/L
12/15/2016
Nickel
EPA 200.7
<0.01 mg/L
12/14/2016
Selenium
EPA 200.7
<0.01 mg/L
12/14/2016
Zinc
EPA 200.7
0.013 mg/L
12/14/2016
Mercury
EPA 245.1
<0.0002 mg/L
12/16/2016
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
12/08/2016
Nitrite Nitrogen
EPA 353.2
0.03 mg/L
12/08/2016
Total Dissolved Solids (TDS)
SM 2540 c
47 mg/L
12/08/2016
Chloride
SM 4500 CI E
< 5 mg/L
12/13/2016
pH
SM 4500 H B
6.69 units
01/18/2017
Total Phosphorus
SM 4500 P F
0.51 mg/L
12/10/2016
1,1,1,2 -Tetrachloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,1,1 -Trichloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,1,2,2 -Tetrachloroethane
SM 62000
< 0.50 pg/L _,
12/11/2016/
1,1,2 -Trichloroethane
SM 6200C
< 0.50 pg/L
12111/2016
1,1-Dichloroethane
SM 6200C
< 0.50 Ng/L
12/11/2016
1,1-Dichloroethene
SM 6200c
< 0.50 pg/L
12/11/2016
1
1,1-Dichloropropene
SM 6200C
< 0.50 Ng/L
12/11/2016
1,2,3-Trichlorobenzene
SM 62000
< 0.50 pg/L
12/11/2016
1,2,3-Trichloropropane
SM 6200C
<0.50pg/L
12/11/2016
Report *: 2016-17594
Page 1 of 7

}�envi'roc��iem
= :a
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab s 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ® 910.347.5843 Lab/Fax
[e-mail]
DAK Americas
Date of Report: Jan 18, 2017
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention:
Report #: 2016-17594
Project ID: Monitoring Well
1,2,4-Trichlorobenzene
SM 62000
< 0.50 pg/L
12/11/2016
1,2,4-Trimethylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2-Dibromo-3-Chloropropane
SM 62000
< 0.50 pg/L
12/11/2016
1,2-Dibromoethene
SM 62000
< 0.50 pg/L
12/11/2016
1,2 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2-Dichloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,2-Dichloropropane
SM 62000
< 0.50 pg/L
12/11/2016
1,3,5-Trimethylbenzene
SM 62000
< 0.50 pg/L
12/11/2016
1,3 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/11/2016
1,3-Dichloropropane
SM 6200c
< 0.50 pg/L
12/11/2016
1,4 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/11/2016
2,2-Dichloropropane
SM 6200c
< 0.50 pg/L
12/11/2016
2-Chlorotoluene
SM 6200c
< 0.50 pg/L
12/11/2016
4-Chlorotoluene
SM 62000
< 0.50 pg/L
12/11/2016
Benzene
SM 62000
< 0.50 pg/L
12/11/2016
Bromobenzene
SM 6200c
< 0.50 pg/L
12/11/2016
Bromochloromethane
SM 6200c
< 0.50 pg/L
12/11/2016
Bromodichloromethane
SM 62000
< 0.50 pg/L
12/11/2016
Bromoform
SM 62000
< 0.50 pg/L
12/11/2016
Bromomethane
SM 62000
< 0.50 pg/L
12/11/2016
Carbon tetrachloride
SM 62000
< 0.50 pg/L
12/11/2016
Chlorobenzene
SM 6200c
< 0.50 pg/L
12/11/2016
Chloroethane
SM 62000
< 0.50 pg/L
12/11/2016
Chloroform
SM 6200C
< 0.50 pg/L
1211112016
Chloromethane
SM 62000
< 0.50 pg/L
12/11/2016
cis-1,2-Dichloroethene
SM 6200C
< 0.50 pg/L
12/11/2016
cis- 1, 3-Dichloropropene
SM 6200C
< 0.50 pg/L
12/11/2016
Dibromochloromethane
SM 62000
< 0.50 pg/L
12/11/2016
Dibromomethane
SM 62000
< 0.50 pg/L
12/11/2016
Dichlorodifluoromethane
SM 62000
< 0.50 pg/L
12/11/2016
Report A: 2016-17594
Page 2 of 7

env�roclien�. k�F
ANALYTICAL & CONSULTING CHEMISTS
Environmental _Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab ° 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ° 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
DAK Americas
Date of Report: Jan 18, 2017
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC '28405
Customer ID: 08100044
Attention:
Report #: 2016-17594
Project ID: Monitoring Well
Ethylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
Hexachlorobutadiene
SM 62000
< 0.50 pg/L
12/11/2016
Isopropylbenzene
SM 5200C
< 0.50 pg/L
12/11/2016
M+P Xylene
SM 6200C
< 1.00 pg/L
12/11/2016
Methylene chloride
SM 6200C
< 0.50 pg/L
12/11/2016
Naphthalene
SM 62000
< 0.50 pg/L
12/11/2016
n-Butylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
n-Propylbenzene
SM 6200c
< 0.50 pg/L
12/11/2016
ortho-Xylene
SM 6200c
< 0.50 pg/L'
12/11/2016
p-Isopropyltoluene
SM 6200c
< 0.50 Ng/L
12/11/2016
sec-Butylbenzene
SM 6200c
< 0.50 pg/L
12/11/2016
Styrene
SM 6200c
< 0.50 pg/L
12/11/2016
tert-Butylbenzene,
SM 6200c
< 0.50 pg/L
12/11/2016
Tetrachloroethene
SM 6200c
< 0.50 pg/L
12/11/2016
Toluene
SM 62000
< 0.50 pg/L
12/11/2016
Trans-1,2-Dichloroethene
SM 6200c
< 0.50 pg/L
12/11/2016
Trans-1,3-dichloropropene
SM 6200c
< 0.50 pg/L
12/11/2016
Trichloroethene
SM 6200C
< 0.50 pg/L
12/11/2016
'Trichlorofluoromethane
SM 62000
< 0.50 pg/L
12/11/2016
Vinyl chloride
SM 6200c
< 0.50 pg/L
12/11/2016
Nitrate Nitrogen (Calc)
Nitrate+Nitrite-Nitrogen
EPA 353.2
< 0.02 mg/L
12/08/2016
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
12/20/2016
I
Report #:: 2016-17594 Page 3 of 7

RE,5;A�
Envir®nn' ntal Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 a 910.392.0223 Lab e 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax
[e-mail]
DAK Americas Date of Report: Jan 16, 2017
1205 Culbreth Drive Suite 200 Customer PO #:
Wilmington NC 28405 Customer ID: 08100044
Attention: Larry Young Report #: 2017-00134
Project ID: Monitoring Well
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
17-00320 Site: 2a 1/4/2017 11:30 AM Water Larry Young
Test Method Results Date Analyzed
Nitrate+Nitrite-Nitrogen EPA 353.2 1< 0.02 mg/L 01/05/2017
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
17-00322 Site: 2b 1/4/2017 12:10 PM Water Larry Young
Test Method Results Date Analyzed
Ammonia Nitrogen EPA 350.1 83.5 mg/L 01/05/2017
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
17-00323 Site: 2E 1/4/2017 10:30 AM Water Larry Young
Test Method Results Date Analyzed
Arsenic
EPA 200.7
<0.01 mg/L
01/06/2017
Cadmium
EPA 200.7
<0.005 mg/L
01/09/2017
Chromium
EPA 200.7
0.021 mg/L
01/06/2017
Cobalt
EPA 200.7
<0.01 mg/L
01/10/2017
Copper
EPA 200.7
<0.01 mg/L
01/06/2017
Lead
EPA 200.7
<0.01 mg/L
01/06/2017
Magnesium
EPA 200.7
2.25 mg/L
01/06/2017
Nickel
EPA 200.7
0.012 mg/L
01/06/2017
Selenium
EPA 200.7
<0.01 mg/L
01/06/2017
Zinc
EPA 200.7
0.026 mg/L
01/06/2017
Mercury
EPA 245.1
<0.0002 mg/L
01105/2017
Ammonia Nitrogen
EPA 350.1
1.2 mg/L
01/05/2017
Report A: 2017-00134 �--- - --

erivrochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab @ 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
DAK Americas
Date of Report: Jan 16, 2017
1205 Culbreth Drive Suite 200
Customer PO #:
Wilmington NC 28405
Customer ID: 08100044
Attention: Larry Young
Report #: 2017-00134
Project ID: Monitoring Well
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
17-00324 Site: 2d
1/4/2017 10:53 AM Water Larry Young
Test
Method
Results Date Analyzed
Ammonia Nitrogen
EPA 350.1
12.8 mg/L 01/05/2017
Nitrate+Nitrite-Nitrogen
EPA 353.2
< 0.02 mg/L 01/05/2017
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
17-00325 Site: 2c
1/4/2017 12:40 PM Water Larry Young
Test
Method
Results Date Analyzed
Arsenic
EPA 200.7
<0.01 mg/L 01/06/2017
Comment:
Reviewed by:
0
Reportt: 2017-00134 Paae 2 of 2

` ' x'F "- ��� ENVIRONMENTAL CHEMISTS, INC
6802 Windmill Way Wilmington, NC 28405 Analytical & Consulting Chemists NCDENR: DWQ CERTERICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 OFFICE: 810-392-0223 FAX [phone]
COLLECTION AND CHAIN OF CUSTODY
CLIENT: DAK AMERICAS, -LLC
PROJECT NAME: Monitoring Wells REPORT NO:
ADDRESS:
CONTACT NAME: i7fA4(— O NO:
d
= E
REPORT TO: HONEIFAX:
PRESERVATION
COPY TO: E-MAIL:
Sampled By: G o 69 SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample identification
Coilecti n
N
LL
d
= E
PRESERVATION
ANALYSIS REQUESTED
Date Time
Tem
a
oS
Well: A
,
GG
Depth:
C P
A,
G
Field H:
G ! G
° r
x
401111W,NO3, TOP-- Rid
-A
Gallons Bailed:
C P
G G
Well:
X
,
G G�
Depthe
C P
, Se,
G G
Field H:
4
kA)
C P
.
X
A -m liti PW 177,
NH3, NO3, .0
r ®
G
Gallons Bailed:
C P
G G
C P
G G
C P
I
ITT
G G
NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.2 ppm or 1098) in the field at the time -of collection. See reverse for instructions
Transfer Relinquished By: Date/Time Received By: Date/Time
1.
2.
Temperature When
Delivered Bye,
Comments:
W
By:
le Re n'ested•
—'-- :" Time:
TURNAROUND: L

4 ` 4 ar ENVIRONMENTAL CHEMISTS, INC
"MIN 6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
Analytical & Consulting Chemists NCDENR: DWQ CERTERICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
f_AI i ct'TIARI Ahir% ruAM nc nr iew%r%
CLIENT: DAK AMERICAS, LLC
PROJECT NAME: Monitoring Wells
REPORT NO:
ADDRESS:
CONTACT NAME: v 11t 47U
PO NO:
PHONEIFAX:
PRESERVATION
REPORT TO:
COPY TO:
E-MAIL:
SarnDled Bv: Z i4-,K�',eL t.,- ®11 Llf,2 r� s .0" cense° a woc. ° lA/ — \M/_u
Sample Identification
Collection
F,,
J13Date
c
o o
c W
PRESERVATION
ANALYSIS REQUESTED
Time
Tem
s
x
0
Well:
G
Depth:
°
C
G
X
As; Cd, Cr, Co, Cu, Pb, Mg,Hg, Ni, Se,
Zn
r» -
Field H:
C
G
ftl/)A P//'i A%/ T
Gallons Bailed:
C P
1
7
G G
Well: 4z
G G�
Depth:
C P
--�
G GIV
Field H:
�4
f
X
�NH3, 03 110-1-77
cil`i'
- ,�
G G
Gallons Bailed: .
P
G G
C P
GG
C P
G G
NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.2 ppm or less) In the field at the time of collection. See reverse for Instructions
Transfer Relinquished By; Date/Time Received By: Datef ime
9. /- - 0
2.
. - Mar. us
Delivered
Comment,
Requested:
Time- `
JRNAROUND:

Analytical & Consulting Chemists
4 Wo
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTERICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
~% r-.^.rr'r%u ewr.n J-UAIAI AC CI wrt,%r1V
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
CLIENT: DAK AMERICAS, LLC
PROJECT NAME: Monitoring Wells
REPORT NO:
ADDRESS:
CONTACT NAME:
PO NO:
s W
` ° m
o �a
REPORT TO:
PHONEIFAX:
PRESERVATION
COPY TO:
E-MAIL:
Sampled By:
a SAMPLE TYPE: I= Influent,
E =Effluent, W = Well, 5T = Stream, Su = avn, *L. = 0wayn, Vu1e:r..
Sample Identification
Colle tion
Date Time Temps
_
° L
.2
s W
` ° m
o �a
t
uE
(9
ow
m
�z
PRESERVATION
ANALYSIS REQUESTED
�
_
�
a
�
{�
o
Well:
,
G G�
Depth:
Field pH:'
X
— O
G' G''
C P
G G
Gallons Bailed:
C P
Chloride, TDS, NO2
As, Cd, Cr, Co, Cu, Pb, Mg,Hg, Ni, Se,
Zn
NH3, NO3, TP
G G
Well:
De the
Field H:
X
X
X
G G
C P
G G
C P
G G
Gallons Bailed:
C P
X
VOC (62008
G G
C I P
G G
C P
G G
NOTICE . DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.2 ppm or less) In. the field at the time of collection. See reverse for Instructions
Transfer Relinquished By: Date/Ti a Received By: Date/Time
'Z' oecgmnlo RaanauaQf r11 .,.
Temperature he eceived:` .�.�t. /�cceptea: � �i ecu• ���°••r•- .---�-------
Delivered R`�• /��-� -�- �-- Received By: Date: ' G Time:
t'--ZI- TURNAROUND:

Environmental Chemists, Inc.
envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax
snn 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
DAK Americas Date of Report: Jan 03, 2017
1205 Culbreth Drive Suite 200 Customer PO #:
Wilmington NC 28405 Customer ID: 08100044
Attention: Larry Young Report M 2016-18415
Project ID: Monitoring Well
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-44212 Site: MW2B 12/21/2016 10:30 AM Water Larry Young
Test Method Results Date Analyzed
Total Dissolved Solids (TDS)
SM 2540 C
509 mg/L 12/22/2016
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
16-44213 Site: MW2C
12/21/2016 11:00 AM
Water Larry Young
Test
Method
Results Date Analyzed
Total Dissolved Solids (TDS)
SM 2540 C
461 mg/L 12/22/2016
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
16-44214 Site: MW21D
12/21/2016 11:30 AM
Water Larry Young
Test
Method
Results Date Analyzed
Total Dissolved Solids (TDS)
SM 2540 C
846 mg/L 12/22/2016
Comment:
Reviewed by: p
Report #:: 2016-18415 Page 1 of 1

1N
Analytical 8, Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTERICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Win Imill Way Wilmington, NC 28406
OFFICE: 910-392-0223 FAX [phone]
CLIENT DAK AMERICAS, LLC
PROJECT NAME: Monitoring Wells
REPORT NO:
ADDRESS
CONTACT NAME: 0Zwti,,--
PO NO:
1REPORT
TO ��9
PHONE/FAX:
Date Time
COPY TO:
E-MAIL:, oC./!1 ,yi• ,
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = So 1, SL = Sludge, Other:
DM
Sample Identification
Collection
y
E �T
ui
w
E `o `o
o v
91 W
m g
PRESERVATION
ANALYSIS REQUESTED
Date Time
Temp
z
o
0
o
w
Well:
O
o�
•2-
X
7 TDS
/ o3a .
G :` G
Depth:
P
X
r Co Cu, Pb, Mg,Hg, Ni, Se,
Zn `"'�---
G G
Field pH:
C _.. P
G G
Gallons Bailed:
C '; P
X
G :; G
Well: IV 02 4f
p `
G
o
X
,TD�,S
Depth:
C ` P
-�-
G G
Field pH:
C' P
G ';: G
Gallons Bailed:
C P
V
G G
C P
G ki G
C P
G G
NOTICE - DECHLORINATION:Samples for Ammonia, TQ, Cyanide, Phenol and Bacteria must be dechlorinated (0.2 ppm or less) in the field at the time. of collection. See reverse for instructions
Transfer elinquished By: Date/Time Received By:
bate/Time
2.
Temperature when . eceived:,7eC- ,� Accepted: '� Rejected: Resample Requested:
Delivered By' �-Received;By: Date: IZ .?-(�V--,—Time:.t30-)
Comments: TURNAROUND: