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HomeMy WebLinkAboutWQ0034987_HISTORICAL MONITORING REPORTS_20170123K Hog Production Division January 16th, 2017 ATTN: Non -Discharge Compliance Unit DENR Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: December 2016 Monthly Report Foxfire Trailer Wash Permit No. WQ0034987 Bladen / Cumberland County P.O. Box 856 Warsaw, NC 28398 Tel: 910-293-9364 Fax:910-293-4130 Please fmd enclosed the NDMLR, NDAR-1, and NDMR form for the month of December 2016 for the above mentioned facility. If you have any questions regarding the monthly report, please do not hesitate to call me at 910-276-0648, ext. 64463 or e-mail me at mcudd@smithfield.com. Sincerely, / 9 o rn Mike Cudd; Land Nutrient Management > = �,� f3 ,,� i FORM: NDA -1 10-13 NODISCHARGE APPLICATION REPORT (NDAR-1) Page N- of A11 4•:7 i FacilityName: Fox Fire Trailer Wash County: BladenDecember1 . irrigation Field • occur I Area (acres): Area *res): Area (acres): at this facility? []YES ENO Cover •. .. • .. •_ • •. .. • •• •. Hourly Rate (in): Hourly Rate (in): Hourly Rate (in-): Hourly Rate (in): Annual Rate (in): Annual Rate (in): Annual Rate (in): Annual Rate (in): Field Irrigated? ®_—®_-I■ ®__M _ Monthly"adin. 0%///// • • • %/////// 0%////% 1111110111111%////// 0%////// 111111=11//////% 0%///// • • • i FORM: NDAR-1110-13 NON DISCHARGE i PPLICATiON REPORT (NDAR-1) I Page of Did the application rates exceed the limits in Attachment i of y ur permit? [2]Compliant [loon -Compliant Were adequate measures taken to -prevent effiuent ponding in or runoff from the sites? mcompriant I]Ncn-Compliant Was a suitable vegetativeI cover maintained on all sites as specified in your permit? OCompnant ONon-Compliant Were'all setback listed. Lin your permit maintained for every application to each -permitted site? i DCompllant ❑Non -Compliant Were all freeboads mal9fained in accordance;w►ith the specified freeboard heights in your permit? OCompllant Mon-Cmnpllant If the facility is non -co pliant, please explain In the space below the reasori(s) the facility wJs not in compliance. Provide in your explanation the dates) of the non-compliance and describe the corrective ' i B • Action(s) taken. Attach additional shoots if necessary. Transferred no gallons from White Ohk j I Truck wash (WQ0014091) to;Foxfire Truck wash I during the month of November 2016. I I i jOperator in , esponsible Charge (ORC) Certification i Permitteit Certification IORC: Lee Matihe s Permittee: Murphy Brown LLC I !Certlflcation No.: � 995905 signing Official: Andy James i 9 9 lGradea Sl S Phone Number. 910-21!7-5211 i ! Signing Official's Title: Marketing & Logistic Manager Tarheel ' jFlas the ORC changed!since the p '' vious NDAR-1? ❑Yes 2No I Phone Number: 910-865-1 ermit Exp.: 12/31/16 I Signal jre Date, gnatu�e Date By this q9i al) re, i certify that his report is accurate and complete to the best or my knowledge. I cartlfy, under penalty a law, that tpfi document and all attach nehts were prepared under my dlrecllon or supervision In accordance with a "system designed to assure t9al all quallfled personnel pr6peny gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, c(tho,;e persons directly responsible for gathering the information, the Ini ormation aubmitted Is, to the best of my knowledge and banal, true, accurate, and complete. I am aware that there are significant ' I penalties for submitting false information, including the possibility of fines and Imprisonment for knowing violations. Mall Original and Two Copies to: j Division of water Resources In atlon Processing Unit I 1617 Mail Service Center Raleigh; North Carolina 27699.1617 i � FORM: NDMLR 08-11 ' NON -DISCHARGE MASS LOADING REPORT (NDMLR) r Page of Permit No.: WQ0 34987 Facility Name: Fox Fire Trailer Wa i h County: Bladen Month: December Year: 2016 Field Name: 01 Field,Name: 02 - Field Name: 03 Field Name: SUB 1 Field Name: Area (acres): �pp 3.23 Area (acres):: 2;29.. Alea (acres): 3.21 Area (acres)::;. 456 ,, Area (acres): Cover Crop(s): 0J seed/Bermud Cover Crop(s): s verseed/Bermud Cover Crop(s): Overseed/Bermud Cover Crop(sf: ' Ove eed/Bermud` Cover Crop(s): Load Type: PAN I., d pe. PAN;. Load Type: PAN Load;Typ,, PAN ; Load Type: Field Loaded? ❑BYES ONO Field Loaded? DYES �No Field Loaded? DYES Otvo Field Loaded? DYES pNo � Field Loaded? DYES ONO Q j > ° Z 4 > c.� � a Q ,,M -.1 a a ,, JE 16 a o A E=J ! Month Ibs/ac Ibs/ac Ibs/ac Ibslac Ibs/ac Ibs/ac Ibs/ac " Ibs/ac' Ibs/ac Ibs/ac January 1 3.7 3.7 "`12'8 �0 12.8'"� 10.3 10.3 0.0 0.0'` February 10.0 3.7 :",26.7. 39.5: 20.2 30.5 O:0, 0.0 . March 1 0.0 3.7 0.0 39.5 0.0 .30.5 0.0 0.0 April 14.3 8.0 0.0+ 39.5 0.0 30.5 0.0` 0.0 ! May 116.5 25.5 8.5- 48.0,y. 13.0 43.5 0.& 0.0 I June 1 0.0 25.5 �..0.0� 48.0 ; 0.0 43.5 - 0.0 Q.O ! July . 1 0.0 25.5 0.0 48.0 0.0 43.5 0.0 0.0 August 0.0 25.5 �'" 0.0 48.0 �' 0.0 ' 43.5 0.0 0:0 l September s 0.0 - 0 25.5 •0.0 48.0 0.0 43.5 OD .90 ! October 1 0.0 25.5 9.5 57.5 , 14.7 58.2 0.0: 0.0 ! November 1 0.0 25.5 0.0 57.5 I, 0.0 58.2 0.0 0:0 I December 1 0.0 25.5 0.0, 57.5 0.0 58.2 0.0' 0.0 FORM: NDML 08-t� ;NON-�ISCHARGE MASS LOADING REPORT (NDMLR). Page of I- I i I Did the mass Ib ding rats exceed the limits in Attachment B of your permit? ©ocomplIant ONon-Compl"rint If the, facility is nonlcornpftant, please explain in the space below the reason(s) the facility W> s not In compliance. Provide in your explanation the date(s) pf the non-compliance and describe'the corrective M i bctionks) iaken: attach additional sheets if necessary. j ' p Opera t • r in Responsible Charge (ORC) Certification 1 Permittee Certification ,ORC: Lee MItthews I Permittee: 1 Murphy Brown LL'C u .Certification Number- 95905 i Signing Official: 'es And Jt3 trade: Phone Number.,91217• I2 Slgriing Official's Mile: Marketing & Logistic Manger Tarheel -Has the ORC chang(1 since rite p evious NOMLR? Elyse ; ONO. Phone No.: 910-865-1310 Permit Exp.: 12/31/16 ignature ` Date Signature Date By this shgnature, I ce 3 that this report is ncourrata and complete to the best of my knowledge.. I certify, under penalty of law, that this doeument,andlei attachmentsware prepared under my dlrectlon or supervision In d accordance wlth a system designed to asstirethat all qualffied personnel properly gathered end evaluated the information submitted, Based on mylnquiry of the person or persons who manage the system, or those persons directly i responelble for gathering the Information, the iihfonnation submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am evrere that therelare.slgriflcant penalties for submltting false Information, Including the i I j possibility, of fines and -imprisonment for knowing vlolatons. i Mail Ori inai and Two Copies to: 1 Ip� 9 Divlslon of Water Resources II i Inforniation Processing Unit `. ii 1617 Mail Service Center 4 Raleigh, North Carolina 27ti99=1617 ; i ' FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page of !II Permit No.: WQ0034987 Facility Name: Fox Fire trailer Wash County: Bladen Month: December Year: 2016 PPI: 00�1 Flow Measuring Point: ❑influent 2Effluent El No Flow Parameter Monitoring Point: ❑Influent EEfFlueni El Groundwater Lowering ❑Surface Water Parameter Code --► 5665o 00400 00610 00625 - 00620 00666 N t C N 0 t p �F- O0 �- I E Q ~YZ: Z F- p. j o a 24-hr, , .. lhrs &0 su I mg/L mg/L mg/L mg/L 1 0, i n . Q n 3 04 F 4 0 I 5 15:00 10.5 0 6 � 7 09:00 : 1 1 01 8 01 9 ;0 j F 10 11 0� 12;0 C 13 14 16:00 j0.5 0 I 15 0 i 16 0 y �. 17 xo .. j 18 0 I j 19 0 ( t 20 ;0 21 ' 14:30 10.5 : .< 22 1 .0 23 1 0 240�. 25-..:- 26 0 „ 27 15:00 10.5 '0 �- 28 p �. 29 30 01 31 0 j Average: �0) • Average: d Month Total:.(gal) 01 Daily Maximum: 12-month total (gal) 478,300 Daily Minimum: 1 SamplingType: Recorder Sampling Type: Grab` I Grab Grab Grab Grab` 12 Month Total Limit .3,577,600 Monthly Avg. Limit: Daily Limit: { ! I Sample Frequency: contingous Sample Frequency: 3 x year ", 3 x Year 3 x year 3 x Year 3 x year p � � h P l Iq i I Page , of FORM: NDMR 1;t)-13 NOI�11-13ISCHARGE MONITORING REPORT (NDMR) i Sampling Person(s) I Certified Laboratories i I i Y Name: Mitchell I Mcdonald j Nam®: NCDA Name: Lee Matthews I I Name: Enviro Chem ;Does fall monitor°ng dataland sampling: feequencies meet tke•reciuirements in Attachment A of you r perr ,t? Ocurnptant nNon-Compliant if th I facility is non-2mpliant, pi so explain in the space below the reason(s) the faI ility was not In compliance. Provide in your explanation the date(s} of the non-compliance and describe the corrective I I L '..../t..n/�\ i.Lcn hAmrh nAdif -1 ahaafa If nPr�aa'J n/ i f i i I 1 I I i I I I„I II: IlOperator iii Responsible Charge (ORC) Certification I I PermittEie Certification t ORC: Lee Mat4hews I Permittee: Murphy Brown LLC 'Certification No. 995905 " Signing Official: Andy James Grade: . SI Phone Number:. 910-217-5211 : i Signing officiars Title: Marketing A Logistic Manager Terheel Has.the ORC changled Ince the p evious NDMR? 13ves ON. I I Phone Number: 910-865-1310 Permit Expiration: 12/31/2016 "A I ure Date , Sig ture I ; Date ' Signa Ig` By this signature, I certify th l t this report Is eccvrrete and complete to the best at my knowledge. under penalty of law, t this doclmrent and all attachments wereprepared under 'dlrectton or supervision in t certify, p y mf' P i i accordance with a system designed to assure that all gd.allited personnel properly gathered and evaluated the information submlled. Based on.my Inquiry of tha person orpersons wlio manage the system, at those persons drecdy responsibta far gathertrtg theildormai[an, the informaton submfttad Is, to the best of my knowledge and belief, true, accurate, and complete. t am aware that there are signircent penaftlesforsubmitting false friformatlon, Including the posstblRy Wince and Imprisonment for . i knov.ini Vlalations. Mail Orl�lnal and TW a Copies to: 8 (Divislon of Water Resources { NI lnfonr atlon Processing Unit lR i 1617 Mail Service Center Raleigh,. Ni orth Carolina.27699.1617 1 1 B E ARM ft-mulodd � ���A Hog Production Division P.O. Box 856 Warsaw, NC 28398 Tel: 910-293-9364 Fax: 910-293-4130 December 19th, 2016 ATTN: Non -Discharge Compliance Unit DENR Division of Water Quality ` 1617 Mail Service Center `G Raleigh, NC 27699-1617 ` Subject: November 2016 Monthly Report Foxfire Trailer Wash o Permit No. WQ0034987 Bladen / Cumberland County Please find enclosed the NDMLR, NDAR-1, and NDMR form for the month of November 2016 for the above mentioned facility. If you have any questions regarding the monthly report, please do not hesitate to call me at 910-276-0648, ext. 64463 or e-mail me at meudd@smiffifield.com. Sincerely, Mike Cudd — x --- -_ Land Nutrient Management FORM: NDAR-1 10-13 I NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of Permit No.: ltll 4•: • - - r Wash County: Bladen Month: November • at DYES irrigation this occur,: facility? ED NO Field Name: Area (acres): Hour"ate (in): Field Area Cover Hourly Name: (acres): Crop: Rate (in): 3.('?l Brtda L__LField Area Name: (acr C= Field Irrigated? n Field Irrigated? YES ONO mmm m mmmmm mm mm m mmmm mm mmmmm mmmm �iii ��—� ���� �■��� mm ®= M®� m mom m� mm m mmm � ���� ���� �■�� ���� ®___ __---- mm Eau mm FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDARA ) Did the application ratessexceed the limits in Attachment B of your permit? Paga Were adequate measures taken to prevent effluent ponding in or runoff from the sites? [Drnmprant Dfbn-Canpaard Was a suitable vegetative cover ,maintained on all sites as specified in your permit? Otmpra.x Qrrorrtempeen: Were all setbacks listed in your permit maintained for every application to each permitter! site? Were all freeboards maintained in accordance with the specified freeboard heights in your permit? mcompsaa [3laar�plant lithe facility is noncompliant, please explain in the space below the reasons) the facility was net In compilance, Provide in Your Elc•TFaent ❑n1a,-tsrpnanr iransfeaed no galtens from White Oak Truck wash (WQOOidr39n se .� T... �..__� _. 1'o explanation the date(s) of the non compliance and describe the corrective acUe -- taken. Attach additionaisheets if necessary. Operator in Responslble Charge (ORC) certificatlon ORC: Lee Matthews i CO!"01:211on No,: 995905 : Grade: Sl Phone Number: 910-217-521 t Has the ORC changed since the previous Nf3kR.J? /J 13Yes iah~o 6 / a/ [' / By U5s 5ilue Date seoLaxa!a and comprate to fhe best of r•ry k=-4odSa. Perrolitoo Certification Permittoe: Murphy Brown LLC Signing OtUGU: Andy James signing OtRalars'Ttio: Marketing & Logistic Manager Tarhael Phone Humber: 910-865-,31 Permit Exp.- 12/31196 1,z /Y-�( 1 ce , under na cf taW aunt tdia' Qaie rY P� a71 !a Umcm and 5900 chmalu Wets +itha"emdesigned1013 svMMaII4aairladpe=rsr! mn�reduld tedUvor UV reformt:11Subtn ills i.Da3cdanM N4aslrofthe r-monorpa=sitro oe ftsopaiheredandawlu3tedlhalnromwLcnaabm4lcd I3racdonmy inh'matlan submitted Is. to t►x D are system, a lhosa parson; dxccrly respw=Va ror gall• 19 the WOMabork rho bast of my fate vlcdgo and herd, fnsa, aocurala. and oompbm. t am ago Hurt mamaro aan�eant prnatHoa la : ubmUnq false LiformntkwL Mwra am possliwityarfges and hpilmmaM forknm*g VotabM,_, Mail,Original and T1ero Copies to; t7ivislon of Water Resources Information Processing Unit 1617 Mall Service Center Raleigh, NI}rth Carolina 27699-1617 i FORM: NDMLR 08-11 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page of Permit No.: WQ0034987 r Facility Name: Fox Fire Trailer Wash County: Bladen Month: November Year: 2016 Field Name: 01 Field Name: 02 Field Name: 03 Field Name: U SUB1 Field Name: Area (acres): 3.23 Area (acres): 2.29 Area (acres): 3.21 Area (acres): ) 4.56° Area (acres): Cover Crop(s): i. Overseed/Bermud Cover Crop(s): Overseed/Bermud Cover Crop(s): Overseed/Bermud Cover Crop(s): " Ovled/Bermud Cover Crop(s): Load Type: PAN Load Type: PAN Load Type: PAN Load Type: PAN Load Type: Field Loaded? ❑YES ❑� NO Field Loaded? ❑Yis ONO Field Loaded? ❑YES ONO Field Loaded? DYES CJNO Field Loaded? DYES ONO z a a I , a a °1 r Z> os >d o va o� 0=a- o 3Qa o� 3a E� v n Month Ibs/ac Ibs/ac Ibs/ac' lbs/ac Ibs/ac Ibs/ac Ibs/ac Il Ibs/ac Ibs/ac Ibs/ac January 3.7 3.7 12.8 12.8 10.3 10.3 '0.0 0.0 February 0.0 3.7 26.7 39.5 20.2 30.5 0.0 0.0 March 0.0 3.7 0.0 39.5 0.0 30.5 0.0 0.0 April 4.3 8.0 0.0; 39.5 0.0 30.5 0.0 0.0 May 16.5 25.5 8.5 48.0 13.0 43.5 00 0.0 June 0.0 25.5 0.0 '48.0 0.0 43.5 0.0 0.0 July 0.0 25.5 0:0 48.0 0.0 43.5 0 0 0.0 August 0.0 i 25.5 0.0 48.0 0.0 43.5 0:0 0.0' September 0.0 25.5 0.0 48.0 0.0 43.5 0:0 0.0 October 0.0 li 25.5 9.5 0 ` 57.5 14.7 58.2 0.0 �,, 0.0, November 0.0 25.5 0.0 57.5 0.0 58.2 0:0 0.0' December FaRtVl; NDMLR 08-11 NON -DISCHARGE MASS LOADING REPORT (NDMLR) • Page - of Did the mass loading rates exceed the limits in Attachment I3 of your permit? If the facility is non•compllant, please explain in the space WOW the Mason(s) the facility was not in compliance. Provide in ottr explanation the dato(�Rrmpllarst CiNon{omphaa actlon(s) taken. Attach additional sheets it necessary, s} e[ the non-compliance and describe the corrective Operatorin Respousibfo Charge (ORC) Cord ication aRc: Lee Matthews Permittee Certincauon 1'crtrlitiea: Certification Number. ggargp5 Murphy Brown LLC Signing Oificial: Grdde; $j Andy James Phone Number; 910-217-5211 signing Oftiars Title: Marketing & Logistic Manger Tarheei Has the 0110 changed since the previous NDMI.R? Dyes C7rso Phone No,; 910.865-13 PcrmltExp.: 12I31l16 Signature l V Date Signature By this sy7aaU rc, t CUM that tiffs rrpal ra arwrra n aid camptata fo QV but Of MY kmvicdg e. 1 1 , Date ry rsxtcrgettaryafla., thtsdoo=emandasatmmmonxwera aocatdonut►tithaWA'arododOnodtoassarathatdlgU&Iod ryParedwdarraydantoa4AMIeethe In 0 s s4rgtad•BOs04onftVln4WryofMaYom=Orper--4=%ghoMMU OfaIha .ortn &oPaMadlhe respaau4ieforpattredrylhalMamatteo thok"rMZVOnaub-Mucd1:6loUmbbestofTrWknawknjnoWberet,&VY oCWrato, comprete.Iamawomthat them urn vGn.f=nipwat69ttorsubmlttbgfrt,soIrt<ormgtra hcladbaIho paau'D QY of G-ws taut imprisaurcnl fx icrcwinp %ictisons. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh. North Carolina 276SO.1617 FORM: NDMR 10-13 WQ0034987 001 —► 01E° o O hrs 0.5 0.5 0.5 0.5 0.5 0.5 0.5 Average: (gal) (gal) Type: Limit I Facility Name: Flow Measuring Point: ❑influent 50050 G 0 0 , p -p 0 p p p p 0 p' p po p p p p. 0 0 „ p 0 ` 0 p 0 0 0, u p 0' 0 p 0 p 0 Average: 0 Daily Maximum: 643,365 Daily Minimum: Recorder Sampling Type: 3,577,000 Monthly Avg. Limit: Daily Limit: Continuous Sample Frequency: NON -DISCHARGE Fox Fire Trailer Wash (]Effluent El No 610 00400 00 E E Q su mg/L 6.94 64.3 64.30 64.30 64.30 Grab Grab 3 xyear 3 x Year MONITORING flow 00625 � ?U Yz mg/L' 92.2 n #REF? 92.2Q 92020 1 Grab 3 x year Parameter 620 mg/L 0 0.00 0.00 0.00 I26:80 Grab 3 x Year REPORT (NDMR) Page of county: Bladen Month: November Year: 2016 MonitoringPoint: ❑Influent ❑Effluent El Groundwater Lowering ❑Surface Water 00665 - p. O.W . U) a; mg/L 26.8 26.80 26.80 Grab 3 xyear Permit No.: PPI: Parameter Code > P O 24-hr 1 2 3 4 14:00 5 6 7 8 9 12:00 10 11 12 13 14 15:30 15 16 17 18 08:00 19 20 21 09:30 22 23 24 25 15:30 26 27 28 29 30 09:00 31 Month Total: 12-month total Sampling 12 Month Total Sample Frequency: FORM: NDMR 10-13 Sampling Porson(s) NON -DISCHARGE MONITORING REPORT (NDMR) Page of Name: Mitchell McDonald; Certi[iod Laboratories Name: NCDA Name: Lee Matthews ; Name: Enviro Chem Does all monitoring data',and Sampling frequencies meet the requirements in Attachment A of your.permtj? orAmpn„� !f the facility is non-companl, please explain In the space below the reason(s) the fae[titywas not Incompliance. Provide In your explanation a0t[o!I(s) taken. Attach additional shesis if necesseriy, exPianatlon the date(S) of the non-compliance a nd descmhe the corregive Operator in Rosponsiblo Charge (ORO) Certi[[cation ORc: Lee Matthews Certification No.: ggggQ� Grade: 51 -�Phonv Number. 910-217-5211 Has the ORC changed sinca the pi avious NDMR? Oyes ONO Signature Date sy tlsa rlgn�tua,1 cart {y lhat ittis raped 1Sacamat0 aad ComP:eto loft best of my l w#bdga. Pormlttee Certiricallon Pormitteu: Murphy Brown LLC - Signing 0Mclal! Andy James " Signing officials Milo: Marketing & LRglstic ManagerTarheel Phono Number, 910-8ii 31Q Permit Ex lratlon: P 12/3/12016 �� _'Iel 7 l& Date 1 certify, undcrFarsekyo! ! Ihis doCettren! andp7 altathmatia 1"M prcPoMd eMdor MYc MctbnorsuperYisio..j h octsrtSvm math asystem de4ftcd to asarrothat rdt qua711cd PMsateoi W°PMOr9atharad Cerdevatuatcd ft kdormadcn sabrNttcd. BRSC I my SAW Y ct the Person orp=ms utto managa the sys om or those parsong timely eesP"Ukb for *—fi q the hlormayon. the Woomoon rubmitad is, to e4 host rimy krwvyadgo and bak1. tree. s=rrola. artd Complete, ! nm WW"O Ctat lboM We r3rirRl al per46M for at+bmdtiog fase irdorMaU^ hWU tay lee pnstals]ity of nnaa an impr4sonma�t for Mail Original and Two Copies to: Dlvlslon of Water Resources Information Processing Unit 1617 Matt Service center Raleigh, North Carolina 27699.1617 SUBMIT County Telephone#:,A`b� &A3 No. of wells to be sampled: Date sample collected: \�- I ` —1 W Well Diameter: `< _ In. Screened Interval: _ft . to_ft. Relative M.P. Elevation: ft. 2RMIT Number:L"UQS ` '1 Vplratlon Date: 1o(� 31—,Jn m-Dlschefge v��/l UIC )DES Other 'PE OF PERMITTED OPERATION BEING MONITORED (Q'Cagoon ❑ Remedlation: Infiltration Gallery ED-Spray Field ❑ Remedlation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: WAS pH o0400: GG . olunits Temp. 000fo: °C DRY at Spec. Cond. 000e4: µMhos time of sampllr Odor 000e6: check Appearance here: 1 ' I�I �"at- �aboretory Name: �u'\�Ol�h2.(`(� Certification No. and colloidal concentrations. Nitrite (NO2) as N 00e16 mg/L Pb - Lead olo61 uglL Nitrate (NO3) as N 00620 <— mg/L Zn -Zinc 01002 mglL Phosphorus: Total as P 006e6 mg/L Orthophosphate 70607 mglL Other (Specify Campo _ s,ano Concentration Units): Al - Aluminum 01105 mg/L J Be - Barium 01007 = ug/L Ce - Calcium 0091e o mg/L uglL Cd -Cadmium 01027_ Chromium: Total 01034 0 r' uglL nrl ORGANICS: (by GC, GC/MS, HPLC) Cu - Copper 01042—��� � w uUIL (Specify teat and method #. ATTACH LAB REPORT.) Fe - Iron 01046 +— o uglL Lab Report Attached? ❑ Yes (1) ❑ No (0) Hg - Mercury 71e00 z mg/L VOC 7e73 , method # K - PotaSSIUm 00037 rag/L , method # Mg - Magnesium 00927—�� method # Mn - Manganese o1066 a uglL method # NI - Nickel 01067 _ ug1L Pffh ient Total VOCe: mg/L VOC Removal% ER QUALITY MONITORING: ROPORT FORM a Name: Name (If different): act Person: 1�l CC LocatlonlSite Name Depth: dJ ft. h to Water Level 8254e: ft. below measuring point Luring Point Is ft. above land surface me of water pumpadlballed before sampling: — mn! ffa COD 00336 mg/L Coliform: MF Fecal 31016 C /100mL Coliform: MF Total 31604 1100mL (Nora: Use MPN method for highly Mbllde.-Ples) r solved Sollds:Total 70300 91 mg/L pH (Lab) 00403 units TOC 00e80 �_ mglL Chloride 00940 L S mg/L Arsenic 01002 ug/L Grease and 011s 00552 mg/L Phenol 32730 �_ uglL Sulfate 00e45 mg/L ecific Conductance 000e6 a�—mg/L µMhos Total Ammonla 00610 (Ammonia Nitrogen: Missile N; Ammonia NIIm9en, Dreg TKN as N oos26 For Remedlation Systems Only (Attach Lab ER QUALITY MONITORING: REPORTFORM Facility Name: Permit Name (If act Person: Location/Site k FORM ON county 'd�to� c Telephone#:°��li` ,Mo. of wells to be sampled: J n-Discharge UIC 'DES Other PE OF PERMITTED OPERATION BEING MONITORED 8-Lagoon ❑ Remedlatlon: Inflltration Gallery &,Spray Field ❑ Remedlatlon: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION ``--\\ Date aempla collected: �i" - �� �w�_ FIELD ANALYSES: 0. ac WAS DRY at NELL ID NUMBER (from Permit): Depth: `�ft. Well Diameter:,in. pH c0a00:,��lnite Temp. 00010: µ hO6 time of Nell to Water Level 826ae:��ft. below measuring point Screened Interval: —ft. to —ft. Spec. Cond. 000e4: sampling, 7epth Measuring Point Is_ft. above land surface Relative M.P. Elevation: k. Odor cootie: O check here: ✓olume of water pumped/bailed before sampling: c les for metals were collected unfllterad: ❑ YES gallons ❑ NO and field acidified: ❑ ❑ NO Appearance ❑ Sam LABORATORYI FOR TIO _ 6 l_ U. /YES L^per abofatory Name: Cl\U l d.� It �6C $(vim Certification No. Date sample analyzed: PARAMETERS NOTE: Value should ailed dl solved nd colloidal concentrations. mglL pb -Lead o1061 uglL GOD 00336 mg1L Coliform: MF Fecal 31816 G t_p /100mL Nitrite (NO2) as N coals Nitrate (NO3) as N 00820 G Q, a. mg1L Zn -Zinc 01092 mg1L , mglL Coliform: MF Total 31504 1100ml- Phosphorus: Total asp cloee MPN for hlBhly lmbldsamples) Orthophosphate 70807 mg1L Other (Specify Campond Concentration Units): {{jjVV (Note: Use method Sollds:Total 7o3co g� mg/L AI- Aluminum 011a6 mg/L )lssolveu units Be - Barium o1007 ug)L pH (Lab) 004e3 mg/L Ca - Calcium ooele mglL TOC ooeso Chlorideooeao L_ s_mg/L Cd - Cadmium 01027 ugfL Arsenic at002�_uglL Chromium: Total01034 �_uglL mglL ORGANICS: (by GC, GC/MS, HPLC) Grease and �__ mg/L Cu - Copper 01042 ug IL (Specify test and method #. ATTAC H LAB REPORT.) Phenol z7so 32730 ugfL of —m Fe -Iron close uglL Lab Report Attached? ❑ Yes(l) ❑ No(0) Sulfate 00e46 _,�_ g IL µMhos Hg -Mercury 71 eao K - Magnesium aoe37 �_ mg/L VOC 7e73 , method # method # Ipeclfic Conductance 00006 Ammonia cost G ONmg/L M Magnesium 0oez7 a mg/L , method # Total (Ammonia Nitrogen; NNses N; Ammonia Nllre ITa1e11 Mn-Manganese ot9es ugfL uglL ,method#�_ TKN as N coeze —_ mg/L NI- Nlckel0tce7 mglL Effluent Total VOCs: mglL VOC Removal% For Remedlatlon Systems Only (Attach Lab Reports): Influent Total VOCs: l tQ/lQ2.i °stet l Slgnaturs of erlmuee to. Authorized Apantl Permllt (or ulhorized Agentl Name and Title - Please nt arOlVO� 812013 G� tU1�J G -59 Rev. ER QUALITY MONITORING: REPORT FORM Facility Name: Permit Name (If act Person: LocatlonlSlte t. PLING INFORinATIUly LID NUMBER (from rPr��errmit): Depth: 3_=�ft. h to Water Level B2646: ?1, ft. below measuring point curing Paint is .Z_ft. above land surface Is - me of water pumpadlballed before sampling: _,ram COD 00335 mglL Coliform: MF Fecal 31016 /100ml- Coliform: MF Total 31504 /100mi- (Not,: ll,e MPN method for highly turbid samples) solved SOIIds:Total 70300 ol— --mg/L PH (Lab) 00403 unite TOC caeso mglL Chloride 00940 G. S mglL Arsenic M02 uglL Grease and Oils 00502 mglL Phenol 32730 uglL Sulfate 00945 mg/L ecific Conductance conga µMhos Total Ammonia uoslo=_mglL (Ammonia Nitrogen; NHsee N; Ammonia Nltmgen, Total) TKN as N 00626 m91L For Remedlatlon Systems Only (Attach Lab INIUM GW-59 Rev. B12013 ON YELLOW PAPER ONLY County Telephone#: `A W 6� lJ No. of wells to be sampled: Date sample collected: j Well Diameter: In. Screened Interval: _ft. to _ft. Relative M.P. Elevation: ft. gallons D�1�V��Laboretory Name: � `\j 1(O qLN Y I aAd colloidal concentrations. Nitrite (NO2) as N coats mglL Nitrate (1,103) as N 00020 e— 01 0 a mg/L Phosphorus: Total as P coess mg/L Orthophosphate 70ao7 mglL Al - Aluminum 011ca mg/L Be - Barlum 01a07 uglL Ca - Calcium node mglL Cd - Cadmium 01027 ugtL Chromium: Total 01034 uglL Cu - Copper 01042 mglL Fe - Iron 01046 uglL Hg - Mercury 71900 ugli- K - Potassium 00937 mg/L Mg - Magneslum 00927 mg/L Mn - Manganese 01066 uglL NI - Nickel 01067 ug/L Influent Total VOCs: M Number: Date: in -Discharge UIC 'DES Other PE OF PERMITTED OPERATION BEING MONITORED lKS-9con ❑ Remedletion: Infiltration Gallery spray Field ❑ Remedletion: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: ^ Temp. o,°C VIIA, DRY at PH co400a;units coot0: , time ofsampling, Spec. Cond. conga: µMhos Odor cocoa: check Appearance here: Certification No. Pb - Lead olo61 ug/L Zn - Zinc 01092 mglL Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify teat and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 71173 , method # method # method # method # Effluent Total VOCs: i mg/L VOC 1111!I111111MM WIT FORM ON YELLOW PAPER ONLY ?R QUALITY MONITORING: REPORT FORM Name: Name (if t Address: act Person: Location/Site L ID NUMBER (from ^Perrmmit): N1 `W Depth: �ft. i to Water Level e254e:61 Q ft. below measuring point luring Point Is ft. above land surface Tie of water pumped/balled before sampling: 1-5 ..-- 4— �.re enllarfad unfiltered: ❑ YES F— County Telephone#: 110-d 13- CNo. of wells to be sampled: Date sample collected: \1- j(+ — t 6 Well Diameter: in. Screened Interval: —ft. to _ft. Relative M.P. Elevation: ft. gallons its sample analyzed: - - - - ( -ON Laboratory Name: L_A\U0�1-0�� \RAMETERS NOTE: Valu s shou d reflect issolved and colloidal concentrations. COD uo33e mg/L Nitrite (NO2) as N costs mglL Coliform: MF Fecal 31e16 C /100ml- Nitrate (NO3) as N 00620 , j mg/L Coliform: MF Total 31804 /100mL Phosphorus: Total as P 00eee mg/L (Note: Use MPN method for Mghlyturbid samples) Orthophosphate 70507 mglL solved Sollds:Total 70300 mg/L Al -Aluminum o11as mg/L pH (Lab) 00403 units Be - Barium 01007 ug/L TOC ooees mg/L Ce - Calcium 0091e mg/L Chloride 00940 S mg/L Cd - Cadmium 01027 uglL Arsenic 01002 ugll- Chromium: Total 01034 uglL Grease and Oils 00562 mg1L Cu - Copper 01042 mg/L ug/L Phenol 32730 uglL Fe - Iron 0104e uglL Sulfate 00e45 mg/L Hg - Mercury 71e00 mg/L ecific Conductance 000es µMhos K - Potassium 00937 mg/L Total Ammonia coalo�� m IL 9 Mg - Magnesium 00927 uglL (Ammonia Nitrogen; NHyes N; Ammanle Numgen, Total) Mn - Manganese Gloss mg/L NI - Nickel 01007 ugll- TKN as N 00625 For Remedlatlon Systems Only (Attach Lab GW-59 Rev. 812013 Influent Total VOCs: LF t #k �! • mg/L n-Discharge UIC IDES Other 'PE OF PERMITTED OPERATION BEING MONITORED ki Lagoon ❑ Remedlatlon: Infiltration Gallery ��y Field ❑ Remedlatlon: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: pH o0acos�aunits Temp. 000lo °C VVAb DRY at Spec. Cond. 000e4: µMhos time of sampling, Odor 000es: i check Appearance here:❑ Certification No. Pb - Lead otoel ug/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): C�J y ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 , method # method # method # method # Effluent Total VOCs: mglL VOC Removal% 1 1—/G� GW-59A COMPLIANCE REPORT FORM Permit #V V �� (Ssbndf one each morsirorirsg period with GW-59 forms.) I Enter date monitoring results were due. WIII this monitoring report (GW59 and GW59A) YES Nq be submitted after the established due date? 2 Was any required informa[ios missing os the GW-59 report forms? YES NO IF the answer to question t or 2 is `YES', list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in seed of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? Ijthe answer is "Yes", contact the Regional Offlcejor guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is 'NO ; sk p to section 8. If the answer to question 4 Is "YES" list the affected wells individually with constituent(s) and concentrations) exceedin stan s in the space provided below: fnW—�1 5 For the constituents identified in question 4 above, havelstandards been exceeded previously for the YES NO same conetituent(s) In the same well(s) in the last two years? If the answer to question 5 is 'NO" skip to section 8. If the answer to question 5Is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concen (s) reported, and sample collection date reach occurre (,,or the last two years). I -as —Is I s. 6 Y M n� t t 1 h 2�3-1s )5 6.0f) I --ts 5,19 1(-rat-is 5��6 '1-6-1s 3-Irrs �O-s=(6 S9 -�5-l6 S,3a 5�.@4 - 6 Are the monitoring wells listed in section 5 totaled at or be and the review boundary? NO N the answer is "YES" a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. N the answer is "NO", monitoring wells may be Improperly located; contact the Regional Office. 7 Is the permittse implementing previously approved actions required by the Division involving this YES -CO groundwater quality problem? If the answer to question 7 is 'YES', describe those actions in the space provided below. N the answer to question 7 Is "NO" contact the Regional Office within 90 days: an evaluation may be required to determine the imaact the waste dfsoosal system Is having at the review and compliance boundaries surroundina this facility. Failure to do so may sublets the permWee to a Notice of Violation, fines, andlorpenaldes. g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. lfiaie��t.1®grrladoe�_ �'--' �asesrailm�id��heoo:subhndfed in this w rahtpmihtar Y�i��tg16� bi�. SignaturediffIttee (or Authorized Agent) Data GW-59A 12/8/2003 _..._._......._............_.....__........ ..... . OUNDWATER QUALITY MONITORING: MPLIANCE REPORT FORM Please 'ILITY INFORMATION .�•-a;� lity Name: �d�<� nit Name (if different) lk act Person: Location/Site Name SUBMIT FORM ON YELLQW PAPER ONLY pe PERMIT Number: WAt)GMMExpiratlon Date: 1 1— avl \ Non-Diecharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED County ITd-Lagoon ❑• Remediatlon: Infiltration Gallery Ra-1pray Field ❑ Remediatlon: Telephone#: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: No. of wells to be sampled: PLINO INFORMATJ� Date sample collected: R— '" FIELD ANALYSES: �1 oC VVA.7 DRY' at LID NUMBER (from Well Diameter: ` in. pH aaaoo$�aunits Temp. a0ot0: d time of �PeCrmit):�` Depth: o� ft.µMhos ft below measuring point - Screened Interval: ft. to ft. Spec. Cond. aoaea: S sampling, check h to Water Level ez6646: �- • Is ft. above land surface Relative M.P. Elevation: ft. Odor ooae6: Appearance here: Suring Point me of water pumpedlbeiled before saS -�r-T gallons rmpling: ran end Raid anidified: ❑ YES Ll2r NO COD 00336 Collform: MF Fecal 31616 /100ml- Coliform: MF Total 31604 /100ml- (Note: Uee MPN method for highly turbid Samples) Solids:Total 70300 mg/L isolved _ PH (Lab) 00403 units TOC aneso mg/L Chloride 130840 mg/L Arsenic 011302 ug1L Grease and Oils aoaea mg/L Phenol 32730 uglL Sulfate 00e46 mg/L µMhosg6 ieclfic Conductance 0013 mg/L Total Ammonia anal (Ammonia Nitrogen, NH3 as N: Ammonia N Mogen, Total) TKN as N 00626 mg/L For Remedlatlon Systems � 1\t11 CO•K� Certification No. `► ►"_ j,,19 aboratory Name: and colloidal concentrations. mg/L Pb - Lead mass uglL Nitrite (No2) as N cools Zn -Zinc 010e2 mglL Nitrate (NO3) as N 00020ED 17 Phosphorus: Total es P ooae6 n `- / R other (Specify C' I pounds and Concentration Units): Orthophosphate 70607 AI -Aluminum otfc6 mglL AUb �IIZ 016 Ba - Barium o1a07 , Ce - Calcium 00e16 mg/L Cd - Cadmium of o27 Awe 4 Chromium: Total 01034FAYETT NAL Cu - Copper o1o42 mg Fe - Iron 01046 uglL Hg - Mercury 79e00 uglL K - Potassium 00037 mg/L Mg - Magnesium 00e27 mg1L Mn - Manganese 01066 uglL N.I - Nickel ota67 uglL — hmr�ead? HPLC) ATTACH LAB REPORT.) ;Mi 4 Yes (1) ❑ No (0) VOC 7e73 , method # method # method # method # .....n VAC Removal% ER QUALITY MONITORING: REPORT FORM Facility Name: Permit Name (If act Person: Location/Site PLING INFOmnn/a-'ME L ID NUMBER (from as s a — Depth: a ft. n to Water Level 82046:�,ft. below measuring point curing Point is,_ft• above land surface me of water pumped/belled before sampling: A r-- i�t:�sat✓ COD 00335 mg/L Coliform: MF Fecal31si6 -G CoD 1100mL Coliform: MF Total 31504 /100ML (Note: Use MPN method for highly turbid eemples) solved Solids:Total 70300 _ 9mli— mg/L PH (Lab) 00403 units TOC 00ee0 mg/L Chloride 00840 mglL Arsenic 01002 uglL Grease and Oils 00082 mg1L Phenol 32730 ug1L Sulfate 00046 mg/L ecific Conductance noose µMhos Total Ammonia ao910 G , mg/L (Ammonia Nitrogen: NHaas N; Ammanie Nitrogen, Total) TKN as N 00025 mg/L For Rerinedlation Systems Oniy.(Attach Lab Reports): J FORM ON of wells to be sampled: PAPER ONLY Date sample collected: �" 5 Well Diameter: I_ In. Screened Interval: ft. to ft. Relative M.P. Elevation: ft. gallons LaboratoryName: C.3N\1)`(4ZCJr�I _1-/G and colloidal concentrations. Nitrite (NO2) as N 00815 mg/L Nitrate (NOs) as N 00e20 O mg/L Phosphorus: Total as P ooese mg/L Orthophosphate 70607 mglL Al -Aluminum 01100 mg/L Ba - Barium 01007 uglL Ca -Calcium 0061e mg/L Cd - Cadmium 01027 _ ug& Chromium: Total 01034 ugly Cu - Copper 01042 mg/L Fe - Iron 01046 uglL Hg - Mercury 71800 uglL K - Potassium 00e37 mg/L Mg - Magnesium uoe27 mg1L Mn - Manganese 01066 ug1L NI - Nickel oias7 ug1L IRIIIIIT Number."%5M)&I Expiration Date: X;d, -SI-otU/ in -Discharge UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED P7-Cagoon ❑• Remediatlon: Infiltration Gallery Eg-Spray Field ❑ Remediatlon: ❑ Rotary, Distributor ❑ Lend Application of Sludge ❑ Water Source Hest Pump ❑ Other: FIELD ANALYSES: WAS pH a0005� units Temp. 00010 C°C DRY at Spec. Cond. ooaea: PMhos time ofsampling, Odor allase: e. check Appearance T here: El Certification No. Pb - Lead most uglL Zn - Zinc 01092 mg/L Other (specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 , method # method # method # method # Influent Total VOCs: mg1L Effluent Total srml (ar Autharlasd . cent), ., .,. , • :, •. mg/L VOC Removal% !�11111111LIM VL= Rev. 812013 Ont ortuas t TER QUALITY MONITORING: E REPORT FORM Name: Name act Person: v '^ Location/Site,Name .%c'.c� 0.q o1OY �. PLINO INFORMATION ,L ID NUMBER (from Permit): Depth: qjQ - ft• h to Water Level 82649: 0ft. below measuring point Suring Point Is —ft• above land surface me of water pumpedibelled before sampling: ;Ite sample analyzed: - - u .. T a ' IRAIIIIETERS NOTE: Vallileg s ould a tact dlssolV COD w33a. mg/L Coliform; MF Fecal 31e1a /100mL Coliform: MF Total 31604 /100mL (Note: Use MPN method for Fighly Wrbld samples) solved Sollds:Total70300 SS�L� mg/L PH (Lab) 00403 units TOC 00880 mg1L. Chloride 00040 G s mg/L Arsenic 01002 ug1L Grease and Oils da66z mglL Phenol 327ao uglL Sulfate 00946 mg/L ecific Conductance o0096 µMhos Total Ammonia ooslo Q mg/L (AmmoNa Nitrogen; NH3as N; AmMonla Nltmoo Total) TKN as N 00625 mg/L FORM ON YELLOW PAPER ONLY rpe PERMIT Number:VSy P31-fl I )Expiration Date: ►Q I-° RQ i Non -Discharge UIC NPDES Other FHTpF PERMITTED OPERATION BEING MONITORED County goon ❑• Remedlatlon: Infiltration Gallery ray Field ❑ Remedlatlon: Telephone#: — 13 El Rotary Distributor ❑ Land Application of Sludge No. of wells to be sampled: ❑ Water source Heat Pump El Other: ` S- G FIELD ANALYSES' WAS Date sample collected: ( Well Diameter: In. pH a0400: $units Temp. ammo. a °C DRY at time of Screened Interval: ft. to ft, Spec. Cond. 00094'. µ Mhos sampling, Relative M.P. Elevation: ft. Odor aoosa: check gallons Appearance here: ❑ NO and fleld acidified: ❑ YES �I'NO _ Q Laboratory Name: 'ao (b c)r�e.'\ Certification No. _ >1 colloidal concentrations. Nitrite (NO2) as N aoe16 mg/L Pb - Lead 01061 uglL Nitrate (NO3) as N oas2a In_Z�_ mg/L Zn - Zinc alas2 mg/L Phosphorus: Total as P 00886 mg/L Orthophosphate 70607 mg/L Al -Aluminum alias mg/L Be - Barium 01007 uglL Ca - Calcium 00916 mg/L Cd - Cadmium 01027 uglL Chromium: Total 01034 uglL Cu - Copper 01042 mg/L Fe - Iron 01046 uglL Hg - Mercury 71900 uglL K - Potassium 00837 mg/L Mg - Magnesium 00827 mg/L Mn - Manganese Gloss ug1L NI - Nickel o1as7 uglL For Remedlatlon Systems Only.(Attach Lab Reports): Influent 1 \ \,a A. .A .oa1C \IT I Rev. 812013 Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify teat and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 , method # method # method # method # VOCS: _ mg/L Effluent Total VOCs: mg/L VOC Removals/° .P a _ ..... — ._.,..-_,_..... __........................................................ _....... ER QUALITY MONITORING. REPORT FORM Name: Name (if different): act Person: Location/Site or FORM No. of wells to be sampled: PAPER ONLY in -Discharge UIC IDES Other PEOF PERMITTED OPERATION BEING MONITORED M-ragoon ❑. Remedlation: Infiltration Gallery "ray Field ❑ Remedietion: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION ``� , _ �W �, Date sample collected: �" 5_ - ` `o FIELD ANALYSES: eC WELL ID NUMBER (from Per a:� Well Diameter: � In. H ooaoc:Q 3 5units Temp. 000lo: p �+�" Mhos Well Depth: ft. Depth to Water Level e2e4e: ft. below measuring point °1,3 Screened Interval: ft. to ft. Spec. Cond. aoaea: µ Measuring Point is Z_ft. above land surface Relative MPElevation: Elevation: ft. Odor cocoa: Appearance gallons Volume of water pumped/balled before sampling: 9._ n vcc Itlin Ito sample analyzed:" -Q -b - l - t a � a tRAMETERS NOTE:l e Vas si ould r fiect dlssolvE COD come mg/L Collform: MF Fecal 31WG (,p , /100mL Collform: MF Total 31604 /100mL (Note: Uee MPN method for Eighty lurbld aemptes) solved Solids:Total 70300 L 8 S mg/L pH (Lab) 00403 units TOC coeeo mg/L Chloride 00840 mg/L Arsenic 01002 _ uglL Grease and Oils coee2 mg/L Phenol 32730 uglL Sulfate 00946 mg/L ecific Conductance otlom µMhos Total Ammonia oaelo d- O mg/L (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) TKN as N o0626 mg/L For Remediation Systems Only (Attach Lab Reports): [-(S Laboratory Name: tZ" % and colloidal concentrations. Nitrite (NO2) as N coals mg/L Nitrate (NO3). as N 00e20 (� \ mg/L Phosphorus: Total as P aosee mg/L Orthophosphate 70807 mg/L Al -Aluminum 01105 mg/L Be - Barium MOM uglL Ca - Calcium coals mg/L Cd - Cadmium 01027 uglL Chromium: Total 01034 uglL Cu - Copper o1oa2 mg/L Fe - Iron oloae uglL Hg - Mercury 71e00 uglL K - Potassium 00937 mg/L Mg - Magnesium ooe27 mg1L Mn - Manganese o1ae8 uglL NI - Nickel =67 uglL Certification No. Pb - Lead oloel ugiL Zn - Zinc 010e2 mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7e73 , method # method* method # method # -------------- Effluent Total VOCs; mg/L DRY at time of sampling, here: VOC Removal% .........:.....:.. SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: 6OMPLIANCE REPORT FORM �ACILITY INFORMATION -acillty Name: permit Name (if different): Contact Person: \\%'L Well Location/Site Name SAMPLING_INFORMAT120 WELL ID NUMBER (from Parmit): W Well Depth: 4S ft. Depth to Water Level e2sae: � ,l ft. below measuring point Measuring Point is 3 ft. above land surfaces Volume of water pumped/bailed before sampling_ were YES Date sample analyzed: 3— S- � �' �- a� PARAMETERS NOTE: V ues hou d ref ect dissolve COD ao33e mg/L Coliform: MF Fecal stele /100mL PERMIT County Telephone# O -973" No. of wells to be sampled: Date sample collected: Well Diameter: in. Screened Interval: ft. to ft. Relative M.P. Elevation: ft. gallons NO and field acidified: ❑ YES Date: n-Discharge UIC 'DES Other PE OF PERMITTED OPERATION BEING MONITORED 2as oon ❑• Remediatlon: Infiltration Gallery 'Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: %9 Laboratory Name:\ {bc�sti id colloidal concentrations. FIELD ANALYSES: II WAU PH 00400:S,9 Cunits Temp. 0ooto l °C DRY at Spec. Cond. 00094: µMhos time of sampling, Odor 000ea: check Appearance ` here:0 Certification No. Nitrite (NO2) as N noels mg/L Pb - Lead most uglL Nitrate (NO3) as N oowo Q, S3 mg/L Zn - Zinc 01092 mg/L Re i Coliform: MF Total 31504 /100mL Phosphorus: Total as P oases mg/L (Note: Use MPN method for highly turbid Samples) Orthophosphate 70807 mg/L Ived Sollds:Total 7d3oo olo n mg/L PH (Lab) 00403 units TOC aoseo mg/L Chloride 00e40 6 mg/L Arsenic 01002 ug/L Grease and Oils 005e2 mg/L Phenol 3273o ug/L Sulfate oosas mg/L fic Conductance 000ea µMhos Total Ammonia =10 O , 3 mg/L (Ammonia Nitrogen; N1­13as N; Ammonia Nitrogen, Tolaq TWM ac AI nringn mg/L AI -Aluminum o11os mg/L Be - Barium 01007 ugly Ca - Calcium ooelo -- mg/L Cd - Cadmium 01027 AN?y uglL Chromium: Total 01034 ZU16 uglL Cu - Copper 01042 _ mg/L Fe --Iron 01045 uglL Hg - Mercury 71900 ug/L K - Potassium 00937 mg/L Mg - Magnesium 00927 mg/L Mn - Manganese 010e5 uglL Ni - Nickel 01057 ug/L For Remedlation Systems Only (Attach Lab Reports): Influent Total Other (Specify Corm tQgwbhcentratlon Units): FAYFTTFN/Ii I F= PiF f- Ti9, ORGANICS: (by GC, GC/MS,'HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7e73 , method # method # method # method # mg/L Effluent Total VOCs: mgft_ vw mallm 121 so v i l U 1 loyll, ` t Sian aiuy f a (or Authorized Agent) ed Agent) Name and Title -Please print or tYpa Rev. 812013 nlroww( SUBMIT FORM ON 94 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM or Facility Name: _1 Permit Name (if different): _ Facility Addre s: J S tY) Contact Person: 0.1 Well Location/Site Name 1 County Telephone#: b " 13 -_.3O No. of wells to be sampled: Number: Date: in -Discharge UIC IDES Other PE OF PERMITTED OPERATION BEING MONITORED Pa-Cagoon ❑ Remediation: Infiltration Gallery Lt3-Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION �� - 11 Date sample collected: �� l` 1 FIELD ANALYSES: IT VMLL WAS WELL ID NUMBER (from Permit): er ft. Well Diameter: 9 in. units Temp. ao:13 ► 8 eC pH ooaooron aol DRY at WEII Depth: ,_ Depth to Water Level e2eae: S� ft. below measuring point Screened Interval ft. to . ft. Spec. Cond. 000sa: µ Mhos time of sampling, Measuring Point is '27 ft above land surface Relative M.P. Elevation: ft. Odor 000sa: 2� check Volume of water pumped/bailed before sampling: S gallons Appearance \ here:❑ Samples for metals were collected unfiltered: ❑ YES Al 2A ❑ NO and field acidified: ❑ YES Nri�10 LABORATORY INFORMATION Date sample analyzed: 3- 3 ` " J - C' Laboratory Name: E� Jt' �6C �2M Certification No. PARAMETERS NOTE: V lues shou d reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N ooels mg/L Pb - Lead aril ug1L I /100mi Nitrate (NO3) as N Iiii o (N 11 mg/L Zn - Zinc 01092 mg/L Coliform. MF Feca 31s1s Coliform: MF Total 31504 /100mL Phosphorus: Total as P ooess mg/L (Note: Use MPN method for hlghlyturbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): isolved Solids:Total 70300 6 mg/L Al - Aluminum all o5 mg/L pH (Lab) 00403 units Be - Barium 01007 ug1L TOC ameo mg/L Ca - Calcium 01391a mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug1L Arsenic 01002 ug1L Chromium: Total 01034 ug1L mg/L ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils 00552 mg/L Cu - Copper 01042 ug/L (Specify test and method #. ATTACH LAB REPORT.) Phenol 3273o ug1L Fe - Iron 01045 ug1L Lab Report Attached? ❑ Yes (1) ❑ No (0) Sulfate 00945 mg/L Hg -Mercury 719oa mg/L VOC 7a73 , method # ecific Conductance ooam µMhos m 9 /L K - Potassium 00937 Mg - Magnesium 00927 mg/L , method # Total Ammonia aoelo ,3 � ug1L , method # (Ammonia Nitrogen; NH3 as N; Ammania Nltmgen, Total) Mn - Manganese o1a55 method # /L Ni - Nickel 01067 ug1L , TKN as N oos2s - m9 For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mglL Effluent Total VOCs: mg/L VOC _ s wR��mr,nnmr-rr�rtmn non unn ni ,,,, �iST71iTiTi�ilYll7aIDj 10 Ma - I— r g- or We I V GW-59 Rev. B12013 r......_.._..._,,...._._...,....---........_..._..__,._.�........,..._.._.._. ........---._..,,_..�__ .._....w.... ....... .._. .i.._..................... , _... _ ..._......._, ..... .... ........... FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING COMPLIANCE REPORT FORM FACILITY INFORMATION Please Prin Clead or a Facility Name: To�c`�� Permit Name (if different): Facility Address: S Qi (Street) 2� - ilYi � (Slele� (ZIP) Contact Person: C Well Location/Site Name SAMPLING INFORmw-rwr, 1`\ WELL ID NUMBER (from Permit): Well Depth: � is—ft• Depth to Water Level 82546: . Jj ft. below measuring point Measuring Point is 3 ft. above land surfaces Volume of water pumped/bailed before sampling: Samoles for metals were collected unfiltered: ❑YES ❑ COD 00335 mg/L Coliform: MF Fecal 31515 L 1 /100mL Coliform: MF Total 31504 /100mL (Note: Use MPN method for highly turbid samples) isolved Solids:Total 703130 SS mg/L PH (Lab) 00403 units TOC 006e0 mg/L Chloride 00940 C S mg/L Arsenic 01002 ug1L Grease and 011s 00552 mg/L Phenol 32730 ug1L Sulfate 00945 mg/L ecific Conductance 00095 µMhos Total Ammonia oo510 mg/L (Ammonia Nitrogen', NH3as N: Ammonia Nitrogen, Total) TKN as N 00625 mg/L For Remediation Systems Only (Attach. Lab Reports): YPa County 4' Telephone#: q l Q- a,93 - 5330 No. of wells to be sampled: Date sample collected: 6 Well Diameter: In. Screened Interval: ft. to . ft. Relative M.P. Elevation: ft. gallons NO and Laboratory Name: FA kd (_ i and colloidal concentrations. Nitrite (NO2) as N ooels mg/L Nitrate (NO3) as N 0002o mg/L Phosphorus: Total as P 00685 mg/L Orthophosphate 70507 mg/L Al - Aluminum ol105 mg/L Ba - Barium of o07 uglL. Ca - Calcium 0091s mg/L Cd - Cadmium 01027 ug1L Chromium: Total 01034 uglL Cu - Copper 01042 mg/L Fe - Iron 01045 ug/L Hg.- Mercury 71900 u911- K - Potassium 00937 mg/L Mg - Magnesium 00e27 mg/L Mn - Manganese 01055 ug1L Ni - Nickel 010e7 ug/L Influent Total VOCs: Number: in -Discharge UIC 'DES Other 'PE,OF PERMITTED OPERATION BEING MONITORED ,_,., La oon El. Remediation: Infiltration Gallery M Spray Field ❑ Remediation: M Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: 00400.�, units Temp. u0010: C, �o eC WA5 DRY at PH time Spec. Cond. 00094: µMhos sampling, Odor 000ss: check Appearance here: ❑ Certification No. 7 Pb - Lead o1o51 uglL Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7e73 , method # method # method # method # mg/L Effluent Total VOCs: mg/L VOC Removal%_ or uthorized Alaent) Name and Tilis -Please print or type GW-59 Rev.81=3 N A/ 1 (\Q". / \PA c. SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Facility Name: Permit Name (if different): Contact Person: Well Location/Site Name County Telephone#: "fit u — No. of wells to be sampled: SAMPLING INFORMATION WELL ID NUMBER (from ^Permit):"W ` Date sample collected: 3 Well Depth: o(s ft. Well Diameter: in. (Depth to Water Level e2646: 10-,� ft. below measuring point Screened Interval: ft. to . ft. ''Measuring Point is ft above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: _ gallons IRMIT Number:Expiration Date: in -Discharge UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED 0 -bqi—coon ❑ Remediation: Infiltration Gallery L3-SlYray Field ❑ Remediation: III Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: pH o04005-LSunits Temp. oomo: S 6 eC Spec. Cond. 000e4: µMhos Odor 000e5: 6 2� ,�,/ Appearance ` )Ies for metals were collected unfiltered: ❑ YES AZ ❑ NO and field acidified: El YES URINO 3RATORY INFORMATION I sample analyzed:3— R_ a,3 3,3- -8 ar3' 1(�!5 LaboratoryName: 1)it r� C,i�prr1 Certification No. 4METERS NOTE: Vkhtes.4hould reffloctdissolved and colloidal concentrations. COD 00335 mg/L Coliform: MF Fecal 31616 �-_ 1 C11 /100mL Coliform: MF Total 31504 /100mL (Note: Use MPN method for highly turbid samples) issolved Solids:Total 70300 ' mg/L pH (Lab) 00403 units TOC ooseo mg/L Chloride 00e40mg/L Arsenic 01002 ug/L Grease and Oils 00552 mg/L Phenol 3273o uglL Sulfate 00945 mg/L Specific Conductance ooass µMhos Total Ammonia aoelo a mg/L (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) TKN as N 00625 mg/L Nitrite (NO2) as N ooe15 mg/L Pb -Lead o1o51 uglL Nitrate (NO3) as N 00620 Q ., 3 8 mg/L Zn - Zinc o1og2 mg/L Phosphorus: Total as P ooee5 mg/L Orthophosphate 7051317 mg/L Al -Aluminum ol105 mg/L Be - Barium 01007 uglL Ce - Calcium aoele mg/L Cd - Cadmium o1o27 uglL Chromium: Total 01034 ug/L Cu - Copper 01042 mg/L Fe - Iron 01045 ug/L Hg - Mercury 71900 ug1L K - Potassium 00937 mg/L Mg - Magnesium 00927 mg/L Mn - Manganese olom ug1L NI - Nickel 01067 ug/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 , method # method # method # method # DRY at time of sampling, check here: For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal is LJ 1V 1 \1 I %X.4 ad Agent) Name and TWO - Please print or type Rev.8/2013 A rSir i� -/� i- a3-ls 0-4;- S s W-� - S Lk - ll-IS 4t 6s 11-3--1S� sit FORM: NDMLR 08-11 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page of Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: October Year: 2016 Field Name: 01 [ ietd N rhe: 02 Field Name: 03 Field Name; � BUBJ� .: Field Name: Area (acres): 3.23 Area (acres}: v,2.29 ' Area (acres): 3.21 Area (acres):: 4 56f � �. Area (acres): Cover Crop(s): Overseed/Bermud Cover Gropes} Otrerseed(Berniud Cover Crop(s): Overseed/Bermud Cover Crops) , veeedlBerrnGtl Cover Crop(s): Load Type: p PAN Lo' d T' pe PAN Load Type: PAN Load hype ,:PAN `K Load Type: Field Loaded? DYES pNoie►'toadecf?, , ❑Y'�,. = Field Loaded? ❑YES �Noia1d�Ccsaded? ❑Y� C�IiO."Field Loaded? ❑YES ❑No Z ate.+ J N m E Z v Z .,-rt.J N O Z J m Z v a w.` -I N >. Z v w d E J Month Ibs/ac Ibs/ac (b C _ 'Ibs/ac,, Ibs/ac Ibs/ac . #bs/ac_ .' .Ibs/ac;� __ .: Ibs/ac Ibs/ac January 3.7 3.7 G2, •,` 12.8. 10.3 10.3 O 0, February 0.0 3.7 2 7 * ,, 39,5, 20.2 30.5 ; 00 March 0.0 3.7 .00 ,�� �'9 5 0.0 30.5,. April 4.3 8.0 0 4 = � '39 5- 0.0 30.5 May 16.5 25.50, 13.0 43.5 ; 0.0�:,. 0,0", , June 0.0 25.5� 48.0 ; 0.0 43.5 `,0.0` 0.0: July 0.0 25.5 AA 48,0 0.0 43.5 August 0.0 25.5 v c480°`• 0.0 43.5..O.a 0.0` September 0.0 25.5 400, 0.0 43.5,,0.4 October 0.0 25.5 9,5°� a �57.;,°, ,�, 14.7 58.2 -_ Q.0 November;`: December D FORM: NDMLR OB-11 NON -DISCHARGE MASS LOADING REPORT (NDMLR) page of Did the mass loading rates exceed the limits in Attachment B of your permit? dCWP3z1t%1 Chan-UT4iMm If the facility Is non-compllant, please explain in the space below the reasons) the facIlity ryas not in compliance. Provide in your explanation the date(s) of the non•compilance and describe the corrective aciion(s) taken. Attach additional sheets If necessary. Operator in Responsible Charge (ORC) Certification I Permitter: Certification ORC: Lee Matthews Certification Number. 995905 Grade; SI Phone Number: 910-217-5211 Has the ORC changed since the provlous NDMLR? Oyes Callo signature @v l9s srgnalure 1 eeriity that Uds mpon rs atmLymto Ew complete to the best crmy ka.dedgc. Permittao; Murphy Brown. LLC signing OfficTal: Andy James STgning Ofiiclal's Title; Marketing & Lagistia MangerTerheel Phone No.: 910-865-1310 / --) Permit 6xp.: 12/31/16 Date , ature hate 1 carfily, under penally o! knr. t s donrmetd and ol; olgchmcnts xara prepared tatdtr my tsteUlm orsupettisrort r oxcrdaaeo Wth a system si5ned to Tests that an quaRled pwsauW propertyyatt:aied and evabated the Irforara%on st bmltted. Based on mylmulry al the parson crpersons �Ao rastago Um system. orthose pus= lav respo;w'hlo far9athcriry the Inramatian, the tefotmaran sutrni.".cd !s. to tT+o castor my xnov�ledge Tad txEct, tree, sarurare, and eomfMm I an ueram That them are aigdfiant Penatdes far suymltdig lalsn inrormaSw brkdhg the passbi'Gy of rmes artd hPdsmment for kite- nng vla'atbas. Mail Original and Two Copies to: Division or Water Resources information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: October Year: 2016 Did irrigation occur, Field Name: 1 Field Name: 2 Field Name: +y� Field Name: SUB1 Area (acres): 3.23 Area (acres): 2.29 Area (acres): 3: 1 Area (acres): 4.56 at ti11S facility? Cover Crop: Bermuda Cover Crop: Bermuda Cover Crop: Berdluda Cover Crop: Bermuda ❑YES ONO Hourly Rate (in): 0.5 Hourly Rate (in): 0.5 Hourly Rate (in): 0[� Hourly Rate (in): 0.5 Annual Rate (in): 21.2 Annual Rate (in): 21.2 Annual Rate (in): 21.2 Annual Rate (in): 21.2 Weather Freeboard Field Irrigated? OYES ONO Field Irrigated? OYES ONO Field Irrigated? OYES ONO Field Irrigated? OYES 2NO ❑>. ° cL°y� N °m°' d ~ rma L a m`' ❑H a. ° , aa ❑ m Lh L- v 0 '° E 2 °° . a > E - >.° ° X0 0 ° O M '- rn C v J E >. 7 C °vrn m=> J EN d E I m O E 7 o 0 ° 'a G o m °EE 3 Z. rnC�o E o X 'vJE 3 °F in ft ft . gal min in in gal min in in gal min in in gal min in in 1 U 2 3 4 5 6 7 7 8 9 10 13 3.58 11 12 13 3.58 14 15 16 17 18 191 C 1 88 2.67 1 75,960 360 0.87 0.15 20 C 85 3 75,960 360 0.87 0.15 21 C 80 85,455 405 0.98 0.15 22 C 65 1 24,982 49 0.40 0.40 35,018 71 0.40 0.34 23 24 251 C 1 70 59,332 118 0.95 0.49 83,168 167 0.95 0.34 261 C 1 72 59,332 118 0.95 0.49 83,168 167 0.95 0.34 271 C 1 79 0 37,473 74 0.60 0.49 52,527 - 106 0.60 0.34 28 C 81 4.25 37,473 74 0.60 0.49 52,527 106 0.60 0.34 29 C 80 43,718 87 0.70 0.48 61,282 123 0.70 0.34 30 C 71 47,882 81 0.77 0.57 67,118 114 0.77 0.41 31 Monthly Loading: 0 0.00 310,192 4.99 672,183 7.71 0 0.00 12 Month Floating Total (in): 6.99 16.57 18.35 0.00 FORIA NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of Did the application rates exceed the limits in Attachment B of your permit? Occinpttant [311on-Wn;0aa4 Were adequate measures taken to prevent effluent ponding in or runoff from the sites? QCamptant 11No1.oxnprmrt Was a suitable vegetative cover maintained on all sites as specified in your permit? [ia=*nt Mon-0ompliant Were all setbacks listed in your permit maintained for every application to each permitted site? Elcb[rprar4 ONan-C)omplWa Were all freeboards maintained in accordance with the specified freeboard Freights in your permit? 21 ampran: Qnon-comoliam If the facility Is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective acuonts) tauten. Auacri aaantonai sneers a necessary. 511,500 gallons from White Oak hunk wash (WQ0014091) to F61ire Tiuck wash during the month of October2016. Operator in Responsible charge (ORC) Cardication Permitteo Certification ORC: Lee Matthews permittoo: Murphy Brown LLC Certification No.: 995905 Signing Official, Andy James Grado. Si Phone Humber 910-217-5211 signing Officlal's Title: Marketing & Logistic Manager Terheel Has tho ORC changed since the previous NDAR-1? ❑ws END Phone Number. 910-$65-1310 p rmit Exp.: 12/31/16 SI ure Date Signature Date By iFCS situ are,1 teryty thus this tCactt is IICCafiatf! and ecmp:eta la the best Ci my !ulaYMlgm I certf y under petally t4 Ivv, det tf3s moral arrd at anachauaats ware pepare t1 under my dsect!on orsvp�usron N atdarxo w„h a system desip.-,ed to assure that ep QUalrM ptraomd prcpady awimrad oral evataated"Infcrm lion imbrnYtad. aasad on my tnqufry of Ilia person or Fmom who mWina the system, er U*.a parsons dLTcdy ros;o%b:e for glhamg the Wormndoa, the hforma9an subn'alled ts, to tho best d my im*dga and bola:, true, acaurato, urd complotm I am aware the1 there are a:9n1rcant perait:es far srbettrg falso Irfo=W. o4 hC4..4rg U* FC (Nity of raa and in gisonmoa: for 3umft vioblions. Mail original and Two Copies to: Division of Water Resources Informatlon Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 a Hog Production Division November 14th, 2016 ATTN: Non -Discharge Compliance Unit DENR Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: October 2016 Monthly Report Foxfire Trailer Wash Permit No. WQ0034987 Bladen / Cumberland County P.O. BOX 856 Warsaw, NC 28398 Tel: 910-293-9364 Fax:910-293-4130 Please find enclosed the NDMLR, NDAR-I, and NDMR form for the month of October 2016 for the above mentioned facility. If you have any questions regarding the monthly report, please do not hesitate to call me at 910-276-0648, ext. 64463 or e-mail me at mcuddgsmithfield.com . Sincerely, Mike Cudd Land Nutrient Management FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page Permit No.: •11 4•:7 Facility Name: Fox Fire Trailer Wash County: BladenOctober - - 1 Flow Measuring Point: DInfluent P Effluent 0 No flow Parameter Monitoring Point: [Influent OEffluent El Groundwater Lowering E]Surfke Water • 1 1 1 1 1 1 1 ® 1 1 �' ------- ®--- 1 12 Month Total 111 • .------�--®- FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page of Sampling Person(s) Certlflod Laboratories Nama: Mitchell McDonald Name: NCDA Name: Lee Matthews Name: Enviro Chem Does all monitoring data and sampling frequencies meet the requirements in AttachmentA of your permit? amp nt 0Nal<)Dnatant If the facility is non-compriant, please explain In the space below the reason(s) the facility vats not in compliance, Provide In your explanullon the date(Q (d the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator In Responsible Charge (ORCI Certification Permittee Codification ORC.' Lee Matthews Permittee: Murphy Brown !LC Certification No.; 995905 Signing Officlal: Andy James Grade: Si Phone Number. 910-217-52-11 Signing official's 7itto: Marketing & Lo c Manager Tarheel Has the ORC changed since the previous NDMR? Dyes 2No Phone Number. 9 5-131 Permit Expiration: 12/3112016 4�/0 Signature Date Signatur Date By Nis stgnakrra. I rzr y that Us mart is mmmate and eomp:em to the bar at my MoWedga 1 cartiiy, wtdar pernity cr 1a:v, Lhnt tHs doa[mat! Md rig AtL�hmonis svcto prrpa:ad undar mydreedoit orutpar+t[stoa n axe dwea Kith a system dos.Gnad to aware that all quclVed personal pmpary gathered and ovalWed to L�ro[mation sabraftd. Based an my k gtsry or the pe=norpersons vt[D mange the system, cr uma parsons drectty responsata tar gatl-kQ the L1Qnnafaa, tho Ntama6m C.:bmi'ted ls. to tho bust d my kDWodge and t:atia1. true. uc=ata, and eamptefo. l wm asvare Ctal ftm rro Ior s btnt ng Id so infoonaMa. In u&Q tho possibl�yar rner. and Impracnmcnt I= knming viaot:ans. Mall Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mall 5ervlce Center Ralalgh, North Carollna 276991617 FORM: NDMLR 08-11 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page Permit No.: W00034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: September Year: 2016 Field Name: 01 Field Name: 02 Field Name: 03 Field Name: SUB1 Field Name: Area (acres): 3.23 Area (acres): 2.29 Area (acres): 3.21 Area (acres): 4.56 Area (acres): Cover Crop(s): Overseed/Bermud Cover Crop(s): Overseed/Bermud' Cover Crop(s): Overseed/Bermud Cover Crop(s): Overseed/Bermud Cover Crop(s): Load Type: PAN Load Type: PAN Load Type: PAN Load Type: d PAN Load Type: Field Loaded? El YES El NO Field Loaded? OYES ONO Field Loaded? ❑YES ONO Field Loaded? ❑YES EINO Field Loaded? ❑YES El NO .O. EL a `O+ J O m �6 J E Z 7(L A >` N r J O.. '- m � J 0 Z O (L a T Y J C v 'Z f4 10 J Z O a. a s a s w J 0Q O v f° J (} R f1J1 E Z 3 Q a o J A w 00 m '� -o O E J 7 Month Ibs/ac Ibs/ac Ibs/ac Ibs/ac Ibs/ac Ibs/ac Ibs/ac [I Ibs/ac Ibs/ac Ibs/ac January 3.7 3.7 12.8 12.8 10.3 10.3 0.0 U0.0 February 0.0 3.7 26.7 39.5 20.2 30.5 0.0 0.0 March 0.0 3.7 0.0 n 39.5 0.0 30.5 0.0 0.0 April 4.3 8.0 0.0 39.5 0.0 30.5 0.0 0.0 May 16.5 25.5 8.5 48.0 13.0 43.5 0.0 j( 0.0 June 0.0 25.5 0.0 48.0 0.0 43.5 0.0 0.0 July 0.0 25.5 0.0 48.0 0.0 43.5 0.0 0.0 August 0.0 25.5 0.0 {I 48.0 0.0 43.5 0.0 0.0 September 0.0 25.5 0.0 48.0 0.0 43.5 0.0 0.0 October n November December FORM; NDMLR 08-11 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page of Did the mass loading rates exceed the limits in Attachment B of your permit? ❑+Compliant []Non -Compliant If the facility Is non-compilant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective I:aKen. NRacn aoulUunal annam n Operator in Responsible charge (ORC) Certification Permittee Certification ORc: Lee Matthews Parmittee` Murphy Brown LLC Certification Number: 995905 Signing Official: Andy James Grade: SI Phone Number: 910-217-521 1 Signing Official's Title: Marketing & Logistic Manger Tarheel Has the ORC changed since the previous NDMLR? ores 9lNo Phone No.: 910-865-131 Permit i_xp.: r /12/31/16 Signature Date Signature Date By this signature, I ca4fy that We report is accurrate and complete to the beat at my knowledge. I certify, under penalty of >ev, that this document and a0 attachments were prepared under my direewn or supervision In accordance with a system designed to assure that an qualified persorrat property gathered and evaluated the information submitted. Based on my Inquiry of the person or persons who manage the system, or Move persons directly responsible for gathering the Information, the Irdotmat submitted Is, to the best of my knowledge and belief, true, accurate, and complete. i am aware first there are significant penalties for submitting false Information, Including the Possibility offines and imprisonment for knowing vloiartons. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of Permit No.: WQ0034987 Facility Name: Fox- Trailer_•- -• - •- Did irrigation Field Name - occur Area (acres): at this facility? Cover Crop: F. MIMMllllll Cover Crop. DYES 21NO Hourly Rate (inY Hourly Rate (in): WMMMKMVVMJ��� Annual Rate (iny Annual Rate (in): . • . • . • . . ■ !7 •Field Irrigated?■ !7 • .. • ■ !7 • • • . . ■ !7 • 110HIMMMM N G . in r//,/ • •.. • �j///// 1 •• j///////�j////j� 1 11 111 j////// 1VON// 1 11 11 FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Did the application rates *exceed the limits in Attachment B of your permit? Were adequate measures taken to prevent effluent ponding in or runoff from the sites? Was a suitable vegetative cover maintained on all sites as specified In your permit? Were all setbacks listed In your permit maintained for every application to each permitted site? Were all freeboards maintained in accordance with the specified freeboard heights in your permit? Page of incompliant QNon-Compliant incompliant ❑Non -Compliant OCUmpllant ❑Nan -Compliant pCompliam []Non -Compliant QCampllant t7Nan•[ampliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not In compliance. Provide In your explanation the dates) of the non-compliance and describe the corrective wKen. muaw aaumvn®r snouts u Operator In Responsibie Charge (ORC) Certification Parmittee Certification ORC: Lee Matthews Permlttee: Murphy Brown LLC Certification No.: 995905 Signing Official: Andy James Grade: SI Phone Number: 910-217-5211 Signing Official's Title: Marketing & Logistic Manager Tarheel Has the ORC changed sines the previous NDAR-1? []Yes ONo Phone Number. 910-865- 31.6 .1 Permit Exp.: 12/31/16 ignature Date /this -Signature Date By this signature, I certify, that this report is aacurrata and complete to the best of my knowledge. I cerilyr, under penalty of lawument and ell attachments were prepared under my direction or supervision in accordance with asystem designed toasualified personnel properly gathered and evaluated the Information submitted. Based on my Inquiry of the person or persons who manage the syatem; or those persons directly responsible for gathering the information, the information submitted Is, to the beat or my knowledge and belief, true, accurate, and complete. I am aware that there are signMleant penalties for aubmaang false fnfarmatton, including the possibility of fines and imprisonment for knowing violations. Mail Original and TWO Copies to: Division of Water Resources. Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 mithfi6ld, 60PAt .Hog Production Division October 19th, 2016 ATTN: Non -Discharge Compliance Unit DENR Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: September 2016 Monthly Report Foxfire Trailer Wash Permit No. WQ0034987 Bladen / Cumberland County ti o0v 1;5 o ® o P.O. Box 856 Warsaw, NC 28398 Tel: 910-293-9364 Fax: 910-293-4130 Please find enclosed the NDMLR, NDAR-1, and NDMR form for the month of September 2016 for the above mentioned facility. If you have any questions regarding the monthly report, please do not hesitate to call me at 910-276-0648, ext. 64463 or e-mail me at meudd@smithfield.com. Sincerely, Mike Cudd Land Nutrient Management FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page of Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: September 11 Flow Measuring •. ■ ■ •. ■ !7 ■ ■ • 1 o �� a■ �®�®ate �®� Month Total:.. 0 .. ----------®- Total12 Month e e / --®---® ®-®- FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page of Sampling Persons) Certified Laboratories Name: Mitchell McDonald Name: NCDA Name: Lee Matthews Name: Enviro Chem Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permits IJtnmpriam �•° -y'°- - if the facility is non -compliant, please explain in the space below the reason(s) the facility was not In compliance. Provide in your explanation the date(s) of the non-compliance and describe the correct a action(s) taken. Attach additional sheets If necessary. Operator in Responsible Charge (ORC) Certification Parmittee Certification ORC: Lee Matthews Permittee: Murphy Brown LLC Certification No.: 995905 Signing Official: Andy James Grade: Si Phone Number: 910-217-5211 Signing Official's Title: Marketing & Logistic Manager Tarheei Has the ORO changed since the previous NDMR7 Oyes RIM Phone Number. 910-865-1310 Permit Expiration: 12/31/2016 Zee, zlze4_=� Ad• l7-/ Signature Bate Signature Hate By this signature, I certify that this report Is eccurrato and complete to the best of my knowledge. I certify, under pang 01 law, that this document and all attachments were prepared under my direction or supervision In accardaneewilh a system designed to saeurs that all qualified personnel prop6rly gathered and evaluated the Information submitted, Based an my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the Information, the Information submitted le, to the best of my knowledge and belief, true, accurate, end complete. I am aware that them are signrloantpenalties for submfillng false Information, including the possli ty of fines and Imprisonment for knowing violations, Mail Original and Two Copies to: Division of Water Resources information Processing Unit 1617 Mall Service Center Raleigh, North Carolina 27699-1617 FORM: NDMLR 08-11 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page of Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: August Year: 2016 Field Name: 01 Field Name: 02 Field Name: 03 Field Name: SUB1 Field Name: Area (acres): 3.23 Area (acres): 2.29 Area (acres): 3.21 Area (acres): 4.56 Area (acres): Cover Crop(s): Overseed/Bermud Cover Crop(s): Overseed/Bermud Cover Crop(s): Overseed/Bermud Cover Crop(s): Overseed/Bermud Cover Crop(s): Load Type: PAN Load Type: PAN Load Type: PAN Load Type: r PAN Load Type: Field Loaded? OYES RINo Field Loaded? ❑Y6ONO Field Loaded? OYES ONO Field Loaded? ❑YE� ENO Field Loaded? OYES ONO ��.. Q IL >. c 0 > J Q v IL ¢ � ; n � � i a a R c 0ti >0 Q a Q R �' ,: � Q t� IL ao J 0 >M M �in E ti Month Ibslac Ibs/ac Ibs/ac u Ibslac Ibs/ac Ibs/ac Ibs/ac Ibs/ac Ibs/ac Ibs/ac January 3.7 3.7 12.8 12.8 10.3 10.3 0.0 11 0.0 February 0.0 3.7 26,7 39.5 = 20.2 30.5 O.Q:. 0.0 March 0.0 3.7 0.0 39.5 0.0 30.5 0.0 0.0 April 4.3 8.0 0.0 39.5 0.0 30.5 0.0 0.0 May 16.5 25.5 8.5 11 48.0 13.0 43.5 0.0 d 1 0.0 June 0.0 25.5 0:0 48.0 ` 0.0 43.5 0.0 0.0 July 0.0 25.5 0.0 48.0 0.0 43.5 0.0 0.0 August 0.0 25.5 0.0 48.0 0.0 43.5 0.0 0.0 September October November December FORM: NDMLR 08-11 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page of Did the mass loading rates exceed the limits in Attachment B of your permit? oCompliant ❑Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective raKen. Hiram auumunal sneets It necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Lee Matthews Permittee: Murphy Brown LLC Certification Number: 995905 Signing Official: Andy James Grade: SI Phone Number: 910-217-5211 Signing Officials Title: Marketing & Logistic Manger Tarheel Has the ORC changed since the previous NDMLR? Dyes ONo Phone No.: 910-865- 10 Permit Exp.: 12/31/16 Signature By this signature, I certify that this report is accurrate and complete to the best of my knowledge. r� Date Signature Date I certify, under pe Zoflaw, t this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of Permit No.: Q11 4•:7 Facility Name: Fox Fire .•- • 1 . irrigation • occur Area (acres): Area (acres): Area (ac res�. Area (acres): at this facility? Cover Crop: Cov er Crop: Cover Crop: DYES RINO Hourly Rate (in): Annual Rate (in): Annual Rate (iny Annual Rate (in): Annual Rate (in): Field Irrigated? Field Irrigated?, Field Irrigated? MMMMMM IMMIMIMME M1=1M1MI1M IMME=MEN �M�EM ®�MMMM ���ME ���ME e�� ®IMMMM NMM�� � EMISM NMINMISMISM 0IMM MM MI=NMMME M1=1M1MI1M IMME=MME ®___ __ -_-- ---- --- ---- m IMMM MM IMMEMMME IMME=M �=M=IMEM m IMMM MM M1=EMMI1M M1=E®� �M�NM ® IMMM 0M ���� ���ME ��� ��M� M ___ _ _ --- -__- -_- ---- ME MIMEMM -_-- -_- ---- ®___ __ ---- -_-- -_-ISM -_-- ®___---� -__- -_-� -_-- ®___ �_ --- -_-- -__ME ---- ® ___ _E ---_ -_-- -_-� ---- m ___ _ ---- ---- -_- -_-- m --_ __ ---- ---- ---- ---- ® -_© __ -_ME- ---- ---- ---- •n t h j///// �i////j.. llllll� j////// 1111M 11111i///// 1 1/ j///////.=11111 111111 j///// / 11J. • n t h F I •. t i n • T • i/////// j///// j/////%�j//////jAi//////,: j//////�11W////Ji/////// j///// ME1 j/////// FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of Did the application rates exceed the limits in Attachment B of your permit? El Compliant ❑Non -Compliant Were adequate measures taken to prevent effluent ponding in or runoff from the sites? OCompliant ❑Non -Compliant Was a suitable vegetative cover maintained on all sites as specified in your permit? ElCompliant []Non -Compliant Were all setbacks listed in your permit maintained for every application to each permitted site? (]Compliant ❑Non -Compliant Were all freeboards maintained in accordance with the specified freeboard heights in your permit? (]Compliant ❑Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective taKen. HLtacn aaaniona1 sneers IT necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Lee Matthews Permittee: Murphy Brown LLC Certification No.: 995905 Signing Official: Andy James Grade: SI Phone Number: 910-217-5211 Signing Official's Title: Marketing & Logistic Manager Tarheel Has the ORC changed since the previous NDAR-1? ❑Yes ONo Phone Number: 910-865-1310 Permit Exp.: 12/31/16 Signature Date Signature Date Zthis By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of , that document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 smiltMl idia. Hog Production Division September 12th, 2016 ATTN: Non -Discharge Compliance Unit DENR Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: August 2016 Monthly Report Foxfire Trailer Wash Permit No. WQ0034987 Bladen / Cumberland County P.O. Box 856 Warsaw, NC 28398 Tel: 910-293-9364 Fax:910-293-4130 Please find enclosed the NDMLR, NDAR-1, and NDMR form for the month of August 2016 for the above mentioned facility. If you have any questions regarding the monthly report, please do not hesitate to call me at 910-276-0648, ext. 64463 or e-mail me at mcudd a,smithfield.com . Sincerely, ;5 cry Mike Cudd rn0 v 0 Land Nutrient Management FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page of Permit No.: loll 4•:7 Facility Name: Fox Fire Trailer. -•-n Month: AugustI . Flow Measuring Point: DInfluent [Z Effluent 0 No flow Parameter Monitoring Point: ElInfluent 21 Effluent El Groundwater Lowering L1 Surface Water • • : • i Ag 'I m 1 1 ---------- Month Total: 0 WHY .. ®-®- FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page of Sampling Person(s) Certified Laboratories Name: Mitchell McDonald Name: NCDA Name: Lee Matthews Name: Enviro Chem Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? OCompliant ❑Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Lee Matthews Permittee: Murphy Brown LLC Certification No.: 995905 Signing Official: Andy James Grade: SI Phone Number: 910-217-5211 Signing Official's Title: Marketing & Logistic Manager Tarheel Has the ORC changed since the previous NDMR? ❑Yes ONo Phone Number: 910-865-131 Permit Expiration: 12/31/2016 Signature Date ignature Date By this signature, I certify that this report is accurrate and complete to the best o` my knowledge. I certify, under penalty aw, that this document and all attachments were prepared under my direction or supervision in accordance with a sy em designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 o; nthd+t 600A tllA. PK-** Hog Production Division P.O. Box 856 Warsaw, NC 28398 Tel: 910-293-9364 JaZ10-293-4130 o August 14th, 2016 o = a � CZ)C f7i o ATTN: Non -Discharge Compliance Unit DENR Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: July 2016 Monthly Report Foxfire Trailer Wash Permit No. WQ0034987 Bladen / Ciunberland County Please find enclosed the NDMLR, NDAR-1, and NDDJR form for the month of July 2016 for the above mentioned facility. If you have any questions regarding the monthly report, please do not hesitate to call me at 910-276-0648, ext. 64463 or e-mail me at mcudd e,smithfield.com . Sincerely, Mike Cudd Land Nutrient Management RECEIVED DEQ/D WR AUG 2 3 2016 FAYETTEVILLERROONAL OFFICE FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) rage — or Permit No.: W00034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: July Year: 2016 Field Name Field Name: 2 Xm­ �Icl�_ Field Name: SUB1 Did irrigation occur iq ,!q!Name* 4.56 Area (acres) 3 23r Area (acres): 2.29 Area (acres): at this facility? Cover Crop: Bermuda C_rgp.,� Cover Crop: Beirmida Bemuda �t­Bel b lf,_ _v, Hourly Rate (in): 0.5 Hourly Fatkis Q� R� zj' ,,Zt� Hourly Rate (in): 0.5 DYES ONO _ 'R — Annual [Rate (in): 21.2 Annual Rate (in): 21.2 HWI- ON6�,, Field Irrigated? OYES Elmo Field Irrigated? DYES ONO Weather-i Freeboard ­11 �iil %1 1 c,,.y 'Ci E E 2 S E E .2 E W 32 0 M M , 0 0 0 0 Ll!;", 0 0 0 M M: 0 (n C1 ......... it ft gal min in in gal g min in in 55 1 2 -A 3 4 , q. 7 8 9 Z;r 10 0,, Z", 12 0.2 13 14 7 tA iYi ��V_ 5�, 16 0.2 17 0.3 18 i FMr...3'tiS i 19 20 7 21 7 22 tKI n 23 241 1 0.5 L Ir." W k�.-i.:. ,F.IWJ 251 1 7, ..... 26 ;�i' 27 �4 j 'j, 28 1 x _2,00 29 irt _6 30 31 5, �2, W_,,v —6,0-0 0 0.00 T gq�� �, r, 1 0 A 13.46 FORM: NDMR 1G•13 NON -DISCHARGE MONITORING REPORT (NDMR) Pago -_ of_ Sampling Porson(s) Car iDed Laboratories Name: Mitchell McDonald Name: NCDA Name: Lee Matthews Name: Enviro Chem Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? Qmmp Lmt otlaa-Complrrt If 61a facility Is nonsompllant please explain In the space below the reason($) the Provide In your explanalion the dales) of the non-compliance and dese6be the corredtve Operator in Responsible Charga (ORD) Codification Parmittee Certl6caDon ORc: Lee Matthews Permhtee: Murphy Brown LLC CorGRca6on No.: 995905 signing official: Andy James Grade: SI Phone Number. 91 D-217S211 signing otgclal's'rlGa; Marketing & Logistic ManagerTarheel Has the ORCchanged strimthe previous NOMR7 Dyes Ono Phone Number.-655-131 PermitFxplrallam 12/31/2016 ,� � e��6 signature Dale signature Dale eYNBSgmsm,lcc[tymal ells rtryiertmaewermoand ca,tpkto to di¢Ixs:almy FnarkQao. lanify. undar Wbsv,UmlUisdxameaand ona-arNmanm%vam propomdmdermyellmdonwskfervBhn In accordineaW nasysleat daeaned toassumt1otnt gmrfad ptmometprepa6yyalnrcdard mralualed the Jal mo'+an wbmllad. [lased on mylMuly Of Ileperm orpe mWho mm[t5alhesyatrnr, or thosapftmOm dlccUympoulloror gaihc.Ma lhctEamndai. tho lnPormaEwsntmiUed ls.to"bail a'myFraN.od=aandadu!. bua,aClaaal9, ardeanrralm l am mvaremalUla[eamskndxaR pa9ahltsfor wbm:tllg fd9a Wamatlnn.LttluddaUs: posslUllycr fina9 mdLrprlsonmml{c fufa.J.np lidst:ars. Mall Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27659-1617 FORM: NDMLR 08-11 NON -DISCHARGE MASS LOADING REPORT (NDMLR) vage_OT— ., Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash county: Bladen month: July Year: 2016 Fie Id Name: 03 Field Name: Field m Field Name: 01 Field Area (acres): 3.23 Ar6i$ (derdi) V, Area (acres): 3.21 4 "1 Area (acres). Area (acres): ­Xt�, Cover Crop(s): Overseed/Bermucl; pover1urcp r Cover Crop(s): Overseed/Bermudi !;;oyg�y r -5 uai rNae Cover Crop(s): over CrOp(sy 0 N ad Type: Load PAN AR, V41 Load Type: L, Type: Load Type: PAN Field Loaded? DYES RNO 7S Field Loaded? DYES ONO Field Loaded? Field Loaded? DYES RINO I& v- - z z > 0 < a. > a. o r, JV�%dj 9or 0 z o E z E E 0 U lbsfac lbs) ac�j, 7 lbs/ac lbs/ac Month lbsfac lbs/ac January 3.7 3.7 10.3 10.3 '0 February 0.0 3.7 267,, 4,; " - � !�. '. 20.2 30.5 �O 7R-,L"­-,:1 March 0.0 37 Iz , 101"0": "r­3915, I 'L ,, , , 0.0 30.5 .0 April 4.3 8 0 � 0.0 30.5 May 16.5 5 13.0 June _00--25.5 ­30-0i 0.0 435 -VQE" July 0.0 255 00 43.5 August 11�� 311�1� 0 September October November December FORM: NDMLR 08-11 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page _ of _ Did the mass loading rates exceed the limits in Attachment B of your permit? compliant Dren-compliant If the facility Is noncompliant, please explain in the space below the reason(s)the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective raven. nueura Operator in Responsible Charge (ORC) Certification ORC: Lee Matthews Certification Number: 995905 Grade: Sit Phone Number: 910-217-5211 Has the ORC changed since the previous NDMLR? Oyes Grin jzwe�I Signature Ely Ilds Signature. I codit, that this report Is accunme are complete to :he besl of my xeovAedge. Permittee Cartincatiom Permittee: Murphy Brown LLC Signing Official: Andy James Signing Official's Title: Marketing & Logistic Manger Tarheel Phone No.: 910-865- Permit Exp.- �j12/31116 t✓J Date signature Date I eeniy; under ponaey of I tnds document me all anadrmems we:a prepared under my direction or superimMn In aeeardarme with o am designod to araure Nm all quoteed penormel properly gathered and evaluated the Information submittal, eased an my Inquiry of the person or persons who manage tha system, or thew Pomona dmdy responsible forgathering the Information, the Infoanallen eubmleed Is, to the beat of my mWedge and beliV. tore. accnrale, and conferee.. i rim nine float glom are aignieeant penallma Po: aubmilfng Wan IMbrmallon, inobding the posagYOty of MCs and Imprisonment for knowing violations, Mall original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh North Carolina27699-1617 FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) I -age _ of Permit No.: WQ0034987 I Facility Name: Fox Fire Trailer Wash I County: Bladen Month: July Year: 2016 PPI" 001 Flow Measuring Point: Oin0uent OEfOuent ❑No now Parameter Monitoring Point: ❑Influent 2oriuent ❑Groundwater Lowering ❑Surface Water Parameter Code —►,: 50050 � - OU400 00610 +a 00625z: 00620 +f'00665k,,^ f $ r w '1 ." �L, ly�r 't yzl ❑ 0 E 0: 0yLL}+ O k -0 1 C.. O Q } i`. ,r ey a3?'', x.! �, 'Y.n •i .G .,=. 24-hr hrs �, GPD„d1 =-Sur;.; mglL t_,m91L`_; mg1L 1 wkS 0 �' ,.'..'� ea' C , a v ".. ? t4 t 4 Y+* i ,�`1''i s3 `aL v� sl• 2 '(` ,0,., { tt:j. , 4.5 3 eL SyO}h.r~`.� c.f"•�'µE� d.,. k4 ad_°i... +r1 M1;~ 0 � � 4 ?: "` �._�z `_' �. 1fn.: s. _i ,3>_'.a_.:,5 _ s t a , o+ r wr r v 6 14:00 0.5 7 y 0✓ti`.n x.� i y �'k Tn':' `.lr j x-ti.:i Ili r .t�..'; • 10 h;' '?«- ., ti0 }rY .,,r .l'. ': u .a§s. ::lm( (.. eta .Tc.ii t,a Iwo Ji r ' 11 s'C✓<r0^�` u4 (.. t'.� th' L`x,: wL '�I ::;L c - + yr e3,4 4 21.6 p a al 1 A,` 0.32 131 1 141 13'30 1 3"-``s.3;0,-C �.r2..z,� 3°fl' ....,,:���^v: EMT::w ., 15 ,.O.o. , h"s" 1 y *:;?_1 18 17 u;"y u0�li .y , �:< �: ,� ?� t ` ' w r":18 a.::.:.R2 k r 0 nii L s.. re -J L: .. tirl lu• �,i r .s. t rJ aF;`ti+:. > ,�+; 19 .�;! ,e O�11 Y .ul.k". l i'i ..Y"::.: � 'Y.a..nr . Ky::. r+ ��fr.�+;.:. !ti 4 n�K.✓,". .1 :.A � _T( 20 16:00 05 .._Q?. ?.t t-.a•:'_4 - ,..3x w.;a ...w,? _,-� td"..,..t, _._fit 5sp e r :- } r w! s ,_.��w v ., n':' i x%' ; lk'', i!; '1 -"r ..�a s.: "}•Y 22 ^� GO U- �..ul d`i3.:Y.aua3 r <.u,"'� n -ay <.a �b..vd},.EK , ^` ;i 4d 23 .I•^_ ._ L o c 24 09:30 0.5 t r a:+ Orv, ,le:"-Y _AI ? .,. f h ..I •5fiS' r�; " t ? w <7161 - M; i� ! f1 1 .F •r >w ..in 25 t 0 r ',. :1 n•m, e•,t a; If xh':, t ":I 26 27 28 14:00 0.5 L;! yl ..ea:'.a .au>.E?::e L[.. 29 �✓',✓ rn�OF ' �.71 F •C, Ve !_ :_-c^'�` '... .. a?v v Yea .s� '1f," Y''1 v e,,.S.a�.'.7„2 ••u ��..P :.:.Y M1l.. 30 O i 31 a Average: Average: '"' „dkl 21.50 i' #,REFIT:;• 0.32 a ;34,4Q?;' Month Total: (gal) OQ „�� Daily Maximum „'_ s 21.50 I 11,'4t00p'i 0.32 12-month total (gal) I1}455(423( Daily Minimum 21.50 ,°,T1'4P00!,! 0.32 _ 344;Q•. , ;`�','".�9a r""�.'�i'`,' Sr,:, `A v`_,'d',t•?:>:;"� Sampling Type: fRecordeY• Sampling Type «,.,_Graby;I Grab j, �Giab,;� Grab 'Grab':"ti? 1. _abss_..z[s•`ku. !j,„ "" "'' Fs ss 4. wSi 12 Month Total Limit '357« Avg. Lrmrt - ' IN, Sample Frequency: s�� "' , '>< ;bpn6nuousi Daily Limit:* Sample Frequency .,,3t yearv,k 3xYear w 3z!year,,;, 3xYear V. y. FORM: NDAR-t 10.13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Did the application rates exceed the limits in Attachment B of your permit? Were adequate measures taken to prevent effluent pending in or runoff from the sites? Was a suitable vegetative cover maintained on all sites as specified in your permit? Were all setbacks listed in your permit maintained for every application to each permitted site? Were all freeboards maintained in accordance with the specified freeboard heights in your permit? Page _ar_ mcompsart ONM11=01W.. ElEmplant ORW,Qmp@nt ecampuant OVWcA:TPnmt ecomptbnt ❑Non{amPyart eCarp1na ONan-0impiM if the facility Is non -compliant, please explain In the space below Ilia renson(s) the facility was not In compliance. Provide in your explanation the dato(s)ofthe non•complbnceand describe Ilia corrective actlantsl taken. Attach addittonal sheets if necessapl. Oporatorin Responsible Charge (ORC) Certification Penalties, certification ORC: Lee Matthews Parminee: Murphy Brown LLC Cortincatfon No.: 995905 SigningOfgcial: And)r James Grade: SI PhonoNumbor. 910-217-5211 slaningofficlalsTftlo: Marketing& Logistic ManagerTarheel Has Ilia ORC changed since tiro provrous NDAR-i? 13ya qha Phone Number: 910-865-1310 P imp.. 12/31/16 [ ,C�/� Sign re vote Slgnatare Date "is ggmlvm,lmrdy Nnidismpodisaxurmtasid mmPlatetothobest o:'my lamdadgo. I"OV, ttndMorpawdyetlam,YrelNkd cat and al aeadimeelsWmpapa[d urdtemydmCinnormper&bn h=AJ06 n wul asyatam dashmodto omumtnal gWrfiodperaanrotpmpadygn!xxod and a kmtod tea lydmrwwn subm➢lad. aasadunmy irgrraumsapanda or persmxtfi. tonasxhornslgioedg6Aed Well, W wd cimW9rotarp ia1e%airdoanat�ttna uda�maliai sWMIM is, to Ono tgsl otmyfatt.J.odgo eM txgef, lnw, aGmle. end eompkt¢ 1 nm mwm lnalhoroamrigNrimrt potallias rxwSniting Ww Intonnatlq; Lx3rd'np the pdrsbLy of Ines rndlmFdaanmont rarlmm:rg Nabdaas. Mall original and'iWo Copies to: Division of Wator Resources information Processing Unit 1617 Mail Service Center Ralcig% North Carolina 27699-1617 m#hfi-d W Hog Production Division July 18th, 2016 ATTN: Non -Discharge Compliance Unit DENR Division of Water Quality 1617,Mail Service Center Raleigh, NC 27699-1617 Subject: June 2016 Monthly Report Foxfire Trailer Wash Permit No. WQ0034987 Bladen / Cumberland County P.O. Box 856 Warsaw, NC 28398 Tel: 910-293-9364 Fax:910-293-4130 Please find enclosed the NDMLR, NDAR-1, and NDMR form for the month of June 2016 for the above mentioned facility. If you have any questions regarding the monthly report, please -do not hesitate to call me at 910-276-0648, ext. 64463 or e-mail me at mcudd@smithfield.com. Sincerely �G/�%ri,-� Mike Cudd Land Nutrient Management RECEIVED DEQ/DWR AUG 01 2016 WQROS FAYETTEVILLE REGIONAL OFFICE Page ___of_—~^ PermitNo.: WQ0034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: June Year: 2016 Did irrigation Field Name: SuBi occur at this facility? Cover Crop: Bermuda r, ff"�� Er Cover Crop: Bermuda tp Hour y R to ( n) Hourly Rate (in): 0.5 Annual Rate (in): Annual Rate (in): 21.2 Weather Freeboard d,'ftr,1,Pft ield Irr gated? DYES (ONO wid 'r"r . ..... 'R` Field Irrigated? DYES ONO T�:F 4" ian ft It gal min in in gal min in in tg E4 IC M, yj Nf 10 , 12 14 SVL 17 19 20 21 22 23 25 26 28 30 =xlo�046 12 Month Floating Total (in): *,, V, e FORM: NDAR-1 10.13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Did the application rates exceed the limits in Attachment B of your permit? Paso _ of_ f]canp9an[ 17Ndaoimp➢art Were adequate nieasures taken to prevent effluent pending in or runoff from the sites? (3comphant QNMo Mmptaat Was a suitable vegetative cover maintained on all sites as specified in your permit? L)oxnpatrc 17Namc m tant Were ail setbacks listed in your permit maintained for every application to each permitted site? Mcw*nt of oarmwreat Were all freeboards maintained in accordance with the specified freeboard heights in your permit? Elcxnpunt E31im- mplant If the facility is non•compllant, please explain In the space bebw The mason(s) the facility was not in compliance, Provide inyour explanation the date(s) of thrnon-complianw and describe the correarwe: adlonls) taken. Attach additional sheets If nocassary. _ Opmaloyln Responsible Charge (ORC) Certification Pormittoa Cortlileation ORCr Lee Matthews PatmlNea: Murphy Brown LLC Certification No.: 995905 Signing official: Andy James Grade: 'St PhonaNumber: 910-217-5211 Signing Official's Title; Marketing &LaglstiDManagerTarhed Has the OROchanged since the prevrousNDARA? Uy� pro PhoneNumbor. 910-885-1310 PonnitExp.! 12/31/16 Signature Date sylasdonel o, trMay that aistcpodrsomxra;a andmmpNa1oLhabastararykrv�!edad, penalti as far whnrlr'ig Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service center Raleigh, North Carolina 27699-1617 15_1d Date eased en my I rvrtrvl. rvurviLrc Uo-i! NUN-UlbUMAKUL MAW, LUAUINU KCYUKI (NUMLK) raye_or I Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: June Year: 2016 Field Name: 01 F,ield�,Name'; 02 Field Name: 03 FieltltName-: h :° SllB1„ Field Name: �ii,�,,. -"t:� Area (acres): 3.23 Rr•ea(aGres) :ii'r , ,,.k ` 2?29 's Area (acres): 3.21 AieaS,(acres),µ' �s�W2615, Area (acres): 'n v x Cover Crop(s): Overseed/Bermud Cover Crop(s);.,,, 'Overseed/Bermud-Cover .+ Crop(s): OverseedlBennud x .n�aS C.olv�enCropx(s)z},J Ove tse,�ewd/Bermud Cover Crop(s): ism 'u... _ ` a£.! N-*Yaf,�r Load Type: PAN adlType," ��PAN, ' Load Type: PAN LoedlTjype;;, �,����PNFN ?„]y Load Type: P-ML Field Loaded? DYES ❑NO Field Loaded_ 'OYES pNo Field Loaded? OYES ❑NO F,eltlLoa`ded?, r�r�YES x',gNop� Field Loaded? DYES ONO b Z ', Z¢.4 n..x i», ) 4 ♦ x 9 'O Z a Nl 4 m 4 a d e m m J Ot, j Z Z 2q 1_ t t0t`3i ra St0 Zt �s., O O J o a it A arr , F r }E`a o r r o E o Q , toy Y334r c o e� 4n U a, U !'' )�trev µ�., a i o Month Ibs/ac Ibslac ,,' Ibs/.aC„ . '`�_",I63lac,^ Ibs/ac Ibs/ac Flbs/ac�*, "eVk'k, AJISOC S ,,,; Ibs/ac Ibs/ac January 3.7 3.7 10.3 10.3 !'i ,".- aA.".Oe"�`,v �4i'-M.N.Ji0'Ola i February 0.0 3.7 20.2 30.5 March 0.0 3.7 39 5f _ }s` 0.0 30.5« April 4.3 6.0 ,,r= *Y.5010 `^; 0.0 305 `i''R.',0`QSL':.°Ji...�,:k✓°;7a070:a;.,1?..":1 . May 16.5 25 5 r 8 5!„ � dt 4'tl Or x '.-� 13.0 43.5 �; +,x,,�0e0xN'j+�,w,`" 25 5 ` 0 '„s.' y r 0.0 43.5 June 0.0 h�0 ...,..., e48�0, Julylr� August r-_ss'r,` ? ','',:t -`, s .. i�.a 4 i� °i .'A„1r c IERIM rwl1 y September October November .'..'>i December FORM: NOMiRU8-ti NON -DISCHARGE MASS LOADING REPORT (NDMLR) Did the mass loading rates exceed the limits in Attachment B of your permit? Page_of_ Ommpteu ORcmomnribnl if the facility is noncompliant, pleaso explain In the space below the reason(s) the facility was not in compliance. Provide In your explanation the dale(s) ofthe noncompliance and drscnbe the corrome actiontsl taken. Attach additional sheets if necas law. Operntarin Responsible Charge (ORC) Carti6rallon Pomlittco Certification ORC: Lee Matthew:; Permittae: Murphy Brown LLC Certification Number: 995905 Signing Official: Andy James Grade: SI Phone Number. 910-217-5211 Signing OfOclal's Title: Marketing & Log(slie MangerTarheel Has the ORC changed since the previous NDMLR? OYes ON. Phone No.: 910-865- Pcmtit Exp.: 12131116 Signatuto Dote Signature _ Date ayaissgnaP�te, Icurerthot lFisropet is amnalonndeomphto to the bestdroyknumiadae len[Gy,uMgpahmty .itWl lHStba,mam and 0altodaaeN Avert, maned mdQmyd'aaedonormpaMsbnin axonfonm Wtl, a cystem dasknod to oMuro Ilu:arqua kd portamMpmpetyllaNnN and WS-Udela ' Warmas msukmhted.rased onofinp¢yntlhe ponanarpnr.,onsxfiommaeelhcaysltsn. alma pma4 ultttiy faspsnsMa jxpracNgthm kdc,mation. tholdomwronmWiTLed IS, lothokastoll y-nodedaoaM b6at, tmq ' atsaalO,oMmmptolalamal'I�mlMl thlfe eta s*;N-C dpe=UnformbmtttvJfalsnldorndim.feWSne tho pnsa ft or fnesarAMptsmmenl torknmttng Yiolaftm Mail Original and Two Copies to: Division of Water Resources lnfonnatfon Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699.1617 rumm{. {vumrt m-la NVN-UIOUHAMI M MUNII VKINU KCYVKI (NUIVIK) rcyc_oi_ ., Permit No.: WQ0034987 I Facility Name: Fox Fire Trailer Wash I County: Bladen Month: June Year: 2016 PPI: 001 Flow Measuring Point: ❑influent DEffluent ❑No Flow Parameter Monitoring Point: ❑Influent E Effluent ❑Groundwater lowering ❑Surface water Parameter Code —► i'�,50050 +4§ r,'.0_040,0�;. 00610 L 00,625x� 00620 ' 00659t; o i Q E"3+ U .O E y K ?`; 's ' -5..vl j t-'m1� m U r<o :S r St rF*4, +N 24-hr hrs ":. GPD.._:; ,.• ."._su'_d...F m IL 9 r .'m�IL: mg/L am ILA;" .. _ 9 I.! ,.. , 1 s0. '�•.iy.•, ✓;��. I .,,rr _ ' �,.��:i r«ii.r,i ..e �? ,4¢f `i6.4. 3 1 15:00 0.5 f�` ,0,'i 4 5 i+,. gip. ., r 6 r+'.ro_ 0 , +ry_ s 7 14:00 0.5 H "= pr' '�' s, .a 9 12:00 0.5 ^".., 0 r.. ...., ry-+. y..3 ,�d3 ...°. . t.-A`75_. + i c;.v4 ;.:r tm n - +y r•sY aa 10 11 12 0•rs?: '� .�4�:...: :i u3a•:�L�? > . .. ;a'f\ 3��.,.�.;SC r> ua.�'h`.T�As."_G 13 14 15 I:r�..,'F0 s`::t �i3' s.:aA ' S {:•�, ra.Y':un."w.'.;x u.rd i. Y...«^3� v1�.Y :J e' ..4Y,�it:uf 16 15:00 0.5 17 �'_ •p...'n ,S, k...' .1 1 aj.i�_...Ji L`. �..L a. }s hJ:.. RtA! "( 4:y y` ''y 18 F. .,p �.qt: r�,e fvWY.. rl F �:b �. ,. .i.:':. +4;Y is aYFL V4L •u,t>G..:> L'L.r..i.r.'+._ 19 jam• pn +�... )f. t,eYc *e,..,. wl i.._I'. Jt`_' f.3 . ..fit. ':r6 ..c:F t :e'.AM,r. 20 F r 21 , 22 �0 'ice'„ ;w�a ...ee .,.t.. •W'>���. ).. 23 24 15:30 0.5 25 tP:... 0, Ji r r:r, i'l S .nl.�_ A wl,:'r tl rp .�. he• xs j ;Ih 1r t!{ 26 27 0 �r ZH �F, . Ig; _ ;y "^ .� fuv ..,. e.:.5'A ] �....rL7'_t^' 29 30 12:00 0 5 _ fly. : 2 31 Average ° 0?, h Average: i Month Total (gal) . 0?a ,.a' Daily Maximum. 12-month total (gal)%107,6{018t; Daily Minimum ��,.`•; *,,. ?x,) t.:.d. r`;r,: oL<'i r. ., +.::r' ,5 '; t.r.." a [i xF'_,.(.x. +1; r: inS�b�l Sampling Type: :,"+RecpNkff'! Sampling Type ;Grab' r Gmb c G"ra5`;':tj Grab ,+;,G(aff); ; 12 Month Total Limit "3;5727,001).. Monthly Avg. Limit ` '"„ �, - �, �, �'•;' ,', iM�"„ `+„ _`��`F ? *'� `' fii 1.�,: ..1 % Daily Limit: _ _.;� ..�.. ._v, _„xx,., _•-.s- _ .-.x..-�.. Sample Frequency. adonbnubus Sample Frequency ).3x,year;? 3x Year „3,xyear,:%. 3x Year 3rX,yea' v `511v4„•Ar ';,w „ °:•: r :dC ,ur er FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Sampling Porson(s) Certified Laboratories Name: Mitchell McDonald Name: NCDA Name: Lee Matthews Name: Enviro Chem Page_of^_ Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? 17cmPrIart ManO omp7aa If the facility is non•compliatrl, please explain in the space balmy the mason(s) the facility was not In compliance. provide In your explanallan tho dalo(s) otthe non-compltanco and desuiba the corrective acgonfs) taken. Attach additional sheets if necessary. Operatorin Responsible Chargo(ORC) Cerlificagon Permittee Codification - ORc: Lee Matthews Permittoe: Murphy Brown LLC Certification No,: 996905 signing official; Andy James Grade: Sl Phone Number- 910-217-5211 signing ot6claft'rivo: Marketing & Logistic ManagerTerheel Has the ORCchanged since the previous NbMR? aym Glue Phone Number- 910-365- 10 PermILExpirallon: 12f312016 "gnatum Dale • signature Data eYWs s'gn¢Nm,rax¢fyttmt uJs r¢p¢rt laaxuamnmam;rpkt¢toN¢S¢sldmytnam¢age 1mu7y. WcrpmyyIX v, aettNsdawmmtand a7a:larlsamtstrcrp pteparntl uwerrryauenem¢rapmisfentn gsmrdenmxihasys dcagnna foassv¢IMlat qual0'as persnrnNprap¢ryg¢ihmrdaM nrdml¢tlyq 4dartnar¢a led. aas¢donmyfnq yattn¢perso:l pan. dWng bastatapethe.edSem,d WW, e=a1rlymspnilal.I ,gsmMing W¢ htamatiai, @ninlanmGonsuGn4adis,to apbast armyNmN.nrt7gand Odltf, CVn, ncnuato, orA mmp¢la.l an _ aaar¢aNt th¢m aie &pn'fi�rlpen31i�u 7afsu6a¢lpap fals¢lntorrnafim, trlutllq Ihapos5h11ty IXencamdimpdswnrntfs gpdm Y.d¢1mi Mail Original and Two copies to: Division of Water Resources Information Processing Unit 1617 Mall Service Canter Raleigh, North Carolina 27699-1617 ;•Smithfielct d fooA. i� T Hog Production Division June 7th, 2016 ATTN: Non -Discharge Cc DENR Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: May 2016 Monthly Report Foxfire Trailer Wash Permit No. WQ0034987 1\RW11�'v1��C Unit Bladen / Cumberland County P.O. Box 856 Warsaw, NC 28398 Tel: 910-293-9364 Fax:910-293-4130 RECEIVED DEQ/DWR JUN 2 0 2016 WROS FAYETTEVIL E REEGIIONAL OFFICE Please find enclosed the NDMLR, NDAR-1, and NDMR form for the month of May 2016 for the above mentioned facility. If you have any questions regarding the monthly report, please do not hesitate to call me at 910-276-0648, ext. 64463 or e-mail me at meudd@smithfield.com. Sincerely, Mike Cudd Land Nutrient Management FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page _ of _ ,id Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash County: Biaden I Month: May Year: 2016 Field Name: - 1 Field Name: 2 Field Name: . .,3 Field Name: SUB1 Did ICtlgatlOfl OCCUt Area (acres): ,_ 3.23 Area (acres): 2.29 Area (acres)- 3.21 Area (acres): 4.56 at this facility? Cover Crop: Bermuda ' Cover Crop: Bermuda 77, -Cover Crops- Bermuda Cover Crop: Bermuda DYES ONO - _Hourly Rate (in): - T5' - - Hourly Rate (in): 0.5 Hourly Rate (ia), - - 0.5 7' Hourly Rate (in): 0.5 Annual, Rate' (in): '- - 21.2 Annual Rate (in): 21.2 ' Annual Rate (In):_' 21:2- Annual Rate (in): 21.2 Weather Freeboard ,- Field Irrigated? [DYES-'EINO', _ Field Irrigated? ❑YES ONO . '-Field Irri gate,?-•OYEs:_ ONO r' Field Irrigated? OYES ONO T3:FE 7 H. m 'E a °, a •d m 'Ern F, •- �, C� 'm 'v 0. o E �'rn O -C E. �i° °; m o a a� �. °. o a > Q wrn U E H .rn �. C- A m 0 J E m C E m K o J W, E.. E T g o a �' i Q 0« 2 Ern !- - t rn • �. C i"a 9 O B J E' S. °r .� c- -c ._ E o a. ° p„ ,_S J. o.2 w E. a o a D Q v m«u E m I- °� a r'v 'mo O ,ry E 5? ii °t2'f ft ft , - gal min in in" gal min in in - gal min in in gal min in in 1 2 C 85 0.3 4.17 87,200 400 0.99 015 3 2.3 3.58 5 C 64 4.17 80,660 - 370. _ `0.92 0.15 -- 6 - 8- 9 C 89 12,000 60 0.19 0.19 11 4.17 12 C 89 5 72,000 ' 360 ` 0.82. ' .0.14 ' „78;480 , 360 =. 0:90" -0.15 - 13 C 83 0.5 5.5 48,000!. 240. 0.55 0.14. - 58.860 270'-. 0.68 ., -,015- 14 15 16 C 74 6.5 ' � "' 60,000 300 0.96 0.19 -78,480, 360 '. - 0.90 _., _0.15': 17 C 77 57,000 285 0.92 0.19 `62,130. '.28,,. •. 0.71, ., •0.15 18 0.2 19 6.67 20 22 0.5 23 24 25 .._. . . 26 6.67 _. .. • - 27 - 28TO +, 29 1.3 L�7,271�950-, 31 0.5 ;. .. 0.00 0.00' REM ; t MonthlyLoadiny 12 Month Floating Totai (in): 287,8601f,--3.28 „ ' 129,000 ,, 2.07 13.46 „: 3.19„ ; _.12.45� 0 FORM: NOAR•1 1a.13 NON -DISCHARGE APPLICATION REPORT (NDAR•1) Page_ of_,_ Did the application rates exceed the limits in Attachment B of your permit? Were adequate measures taken to prevent effluent pending in or runoff from the sites? Was a suitable vegetative cover maintained on all sites as specified in your permit? Were all setbacks listed in your permit maintained for every application to each permitted site? Were all freeboards maintained in accordance with the specified freeboard heights in your permit? Orappfunt ONani'cmpaan: 120 npf"r2 ❑Nai�OympGanL l Canoart 111MCadplent rdexnp'art ONm{anplant 2Cernpr= ONCAM11poart It the facility Is nolrcomplianl, please explain In the space belowthe mason(s) the TarSJay was not In cempllanco, Provide In yourexpfanatlon the date(s) or the non-compliance and describe the correctiv.: Operator In Responsible Charge (ORC) Certification Permlhaa Certification ORc: Lee Matthews Permittec: Murphy Brown LLC Cortilicatton No.: 935305 Signing official: Andy James Grade: SI Phone Number, 910-217-5211 signing official's Title: Markeling & Logistic Manager Tarheel Has the ORC changed since the previous KDAR-1? ayes ONO phone Numhar. glo-865-131 Farmit ex p.: 12131116 G�/� nalum pate Signature Dale DyW.ssl3Nlva,l Ccdiy1na11:.d repxlfaacPlmJlaaM aproplel➢lodxt hest of myk%Yctlgu I cerpy. M)W panty ul WYaal and al=ChM..M1r%vale WRMcd under my dtncdan ors¢pervueon Lis rdarra yt= tv.th n syalOm designed to astSOd peer➢oMl popoay o¢therod and avoWed e,a hyormatin Su6nuulcO. UpSLE M ny Lwuay➢tthep¢rson arpmms nCd manage aw syzlam, a Naw penmsdrectyrcspadak fcr Baewprg Irw Infamaaon Ino Mamalcns¢➢mi11M Is,toa:o➢aeat mylapKCdgaanaIxiaf.hw,➢ :mla,am vynp'¢te lam eNatpL1p11hCfC arc 51pn,=n: rbrnt.�Osrasahndldng lalso WonralMn, hlcbcin9 LM pa:'3rily c7fm¢s aid Impdwamonl larMo.Nng vtowona. Mall Original and Two Copies to: Division orWatar Resources Information Processing Unit 1617 Mall Service Center Raleigh, North Carolina 27699-1617 FORM: NOMLR 08-11 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page _ of Permit No.: W00034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: May Year: 2016 Field Name: 01 Field Name:. - Field Name: 03 Field.Na '::ASUB Field Name; Area (acres): 3.23 (acres) w Area (acres): 3.21 Arq'a'(act re' .-s is 6' Area (acres): Cover Crop(s): Overseed/Bermudi Cdidr7Ci66(6).7­ Ov&rse_ed/66miUdi Cover Crop(s): Overseed/Bermud o (s'�. ,&,,'D_ver's'e!'dA Cover ir'p 66ufdi Cover Crop(s): Load Type: PAN LoadTypo:: . . ... PAN Load Type: PAN Load Type: Field Loaded? DYES ONO Field Loaded?',L Y ",".O 'g`S1. Field Loaded? OYES ONO Field Loa'dlecl?OYES',- ❑No4 Field Loaded? OYES ONO z > 0 > 2: 0 0 o s� 0 E Z 0 E Ez 0 0 0 0 IK- Month lbs/ac lbs ac jlbslac •,:_, ,-_'4bs1acv vlr� lbs/ac lbs/ac -jbsla6, lbs/ac lbs/ac January 3.7 3.7 12A 10.3 10.3 '0.0 7, February 0.0 3.7 26.7.--, 3 20.2 qn 9 0.0 .0 March 0.0 3.7 0.0;J� 39:5, 0.0 30.6 O;Q�1', 7 April 4.3 8.0 o 0.,_° t,W5 0.0 30.5 "j, 110 0 May 16.5 25.5 A8.0, '4, 13.0 43.5 __0 cl June July o ' August September October December FORM: NDNILR 06.11 NON -DISCHARGE MASS LOADING REPORT (NI)MLR) . Page_ of_ Did the mass loading rates exceed the limits in Attachment B of your permit? Mmmplam 13Nw-mnpunt If the facility is non- omptiant, pleasa explain In are space bolmv the reasons) the faclUty was not In compliance. Provide In your explanation the date(s) oflhe oon•compllonco and describe the conective tanen.nuucu ecmuonmsnacts Operator in Responsible Charge tORC) Certification Permittoe Certification ORO: Lee Matthews Permittoo; Murphy Brown LLC Certification Number: 995905 signing official: Andy James cmde: SI Phone Number. 910-217-5211 signing otOclars Title: Marketing & Logistic Manger Tarheel Has the ORC changed since the previous NDMIR? Oves EINe Phone No.: 91D•665- Permit Pap.: 12/31/16 Signature Data Signature Date a'fmic9amlum.1u;tN Wl:nb npaM1 lsaaetnaloat7 eomplolate the ace{olmyknarlrosa. Icaa•wpanisbnn tho aa:umla, Mall Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mall Service Canter Raleigh, North Carollno 27699-1617 on ORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page _ of Permit No.: WQ003 987 1 Facility Name: Fox Fire Trailer Wash County: Bladen Month: May Year: 2016 PPI: 001 Flow Measuring Point: OInfluent ElEffluent D No flow Parameter Monitoring Point: DInfluent ElEffluent ElGroundwater Lowering ElSurface Water Parameter Code b► 600so 00400'. 00610 �00625 00620 f006651�1 2: E p 0 E if L) W 0 0 0 0 E S < 24-hr hm GPD� Su mg/L mig/L mg/L mg/L, 0. 2 16:00 1.6 0 3 0 4 -0 5 6 11:00 1 0 7 0 0 9 17:30 0.5 1 0'. 101 1 1 0 0 13 14:30 2 0 7,, FORM, NOMR10.13 NON -DISCHARGE MONITORING REPORT (NDMR) Paso _ of Sampling Person(s) Certiftod Laboratories Name: Mitchell McDonald Name: NCDA Name: Lee Matthews Name: Enviro Chem __ _._ ..._...._....�. �...,, ...,...r,.,.y .. c4m-i sea, Mons. It to iuc(ulrunienl5 in Naacriment A oI your permit? Ccoslpaam ❑Na Cnmp¢a:n If the facility is nen-compaant, plaaso explain In the space belovi the masons) the facility was not in compliance. Provide lnyourexplanailon the date(s)ofthe noncomphanco and desofibo the cooecthro action(s) tahen.Altnch additional sheets If necessary. Ope;,'ator in Responsible Charge (ORC) Carllfieatioa Permidna Cortifiention ORc: Lee Matthews Pormittce: Murphy Brown LLC Certification No,; 995005 signing Official: Andy James Grade: SI Phone Number. 910-217-5211 signing officials 7Ulo: Marketing & Logistic Manager Terheei Has the OrRochanged since the previous NDMR? Elves Onro 910B555-1310 Permit Explration: 1213112016 :PhonoNumbar Sianatum Date Signaler C../ �� aysaaslpnaaea.Icedrythat asmpad �a==tam.dWmpleta to"best al mytmmrkdaa Icelty under on". Wt➢Oa dcmmmtandana:tachmemskcm ra fed atdetat duttyonors sion in attattln Mui a sysian designed to asssm thata7gmaI u penarndptoptygal➢reia l m1natm lho Normatiaa w➢mated. aasca asmylrgatyal ale po:sanorpetsomwho manage t➢e syZpn. ocalKgpeCAns dyedyrppomlalo of,, gaala'mg tan in:omsaansl, ihn lnIQ=L'M3U!sm11ed Is. to lha bastdmyrnn+Y.nd2n and hater. la¢ aces;¢, and Mmp'nt0. I am mri9thal tomeIYoy7nYlaflXy41a5ni faraataaliliaghYa lllapais➢ay MLrtasand Imp:Imut%l to. vlobUsn&kl7.sdag YamY,lb VIi111YGM1i Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mall service Canter Raleigh, North Carolina 27699.1617 > ithfidd A A, wq Hog Production Division May 12th, 2016 AT TN: Non -Discharge Compliance Unit DENK Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: Apr112016 Monthly Report Foxfire Trailer Wash Permit No. WQ0034987 Bladen / Cumberland County P.O. Box 856 Warsaw, NC 28398 Tel: 910-293-9364 Fax:910-293-4130 Please find enclosed the NDMLR, NDAR-1, and NTDMR form for the month of April 2016 for the above mentioned facility. If you have any questions regarding the monthly report, please do not hesitate to call me at 910-276-0648, ext. 64463 or e-mail me at mcudd smithfield.com . Sincerely, RECEIVED DEQ/DWR MAY 2 4 2016 Mike Cudd Land Nutrient Management �__ OROS ETTEVILLE REGIONAL OFFICE FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page —of •+ ,r Permit No.: WQ0034987 Facility Name Fox Fire Trailer Wash County Bladen Month April Year: 2016 1FielgaName P r r`;,1 ' Field Name: 2 st Field Name: Did irrigation ,r C ,, s SU81 occur ar'Area r(acres" 3 3 `` Area ( acres) 2.29 Area acres' ) i 3}51^ " Area acres): (: ' '( 4.56 at this facility?) Cover Crop: Bermuda �,Y< Cover�Ci;op a _,"y Bermuda .rF'x , r.",fCover,Crop y- T Berri uda!�r Cover Crop: Bermuda FJou (}n) ?. Hourly Rate (in): 0.5 IjourlyRate {rn)i 0 St, Hourly Rate (in): 0.5 OYES ❑NO yly�Rate ,, N,•_ ;0 b� �,, _, N �•r E,•:,+ y Ahn'Y1al°Rate�`(m)**''""`21 2-' Annual Rate (in): 21.2 Annual Rate (in): 21.2 z 'i Weather Freeboard 4rigated7 Field Irrigated? OYES D+NO + ¢-�Yes,.!t,ip Nos`') Field Irrigated? OYES ONO lOYESy }'tOrvo'�.i! r(Freld9lrngatedy?y E a i,p' mra, >, vt , rz, �mry{ E4 m1 m y v rn E T QNytN u TC �C N ..TE BEd o, a ,, y z Sm� Em Ot ° } E1' , =E a ^^ AE y Fin o N2O 2 s ❑ p o o a F- � ❑ p � = p , }oa rry�:, ❑r Ot Nt 2ll >Q1=❑J`�=J iQ J rJ i�Q JA4{ IJ ft ftri; in in a•��,'v`gaI? rmin„c,- in in dg_7;inzT „rn„Y ,;. gal min a'!; m_ ,,,, k,.:, m z.; gal min 1 i'=: `�a. "{,61.::..i `eS ,!>s'C..�'.t�i. s*Gr... .ad±u'h ! vli ti�N•'.i 2 0.5 3 x7 ^r;:', �.a�'.s as fi ":: 6 .. .• v.�.._-}Y: t 6 3.5 +:,`,.0 .. : «'�' ?i9 '•`, :i. i ,.t;.:.'. U "', ax.;a i u F"ry ,�:;�u_ 1 ram,`°) a.?�r!: 7 0.3 ?" i.!a _ T`_.t' .a tra9 ,F..�-t:. crF.�w,.c �^. �:.�i,.,: 't?w'.` 41 icr.'.�•.. ai;'$! 8 "Y5 t?� 4G ':l S t6. _.U.cl.'�"4 .5 , .k'2 9A •9A 1..4. •, .•T 9 en ith A 4i i y M Y" 'K S' 'iJ , xr. i:. +i ,w ,:. t.:.�,a. ...iss ....:ic. n;4'v.n4 10 x`.«ur .', Crvn� cLC..u,. ,".5:27 t+++ �;..' uz u%1 }i 12 .. i}.11 , tt ° u:.i , 1 r'.'_..ulA Ew.E.0 i'.-a,.pia 13 0.5 rLIL? s r Mi 1 ...�i_s:.:": � i { `" - i� i>n..,!.,.,.v s' 4 14 3.33 15 '� 16 .J•t �+. -fa .., .kr� w,. .x. ,.'L. ... k .t-.as• :,. r__., n3 N3� _. 18 n 19 20 21 22 3.42 fi n-a 23 1.2 3.33 ��;r� ,. �a.-: *1 k'`x ... t,,.,,,_,; iU.•.t,Y_.''.�.>r!...x .�,,,n�<,,. v`,xr :� lgx rw:,• 24 xs^:� '•'�t p r i +"_; ,.r .irk T `rn-,; n.0 irr `.�L�'.=�a=:,.<". 25 r•,v a'. 3. ,..,<r,..r•..,. w� z .§�nt�; ,1 _,.+e11.*o,. 26 's.',i, ,a,�':Y..!,... ! ,_- .i: ,vu: 27 ., am!I s ,<.. ::. , ! l,r`.R Wn 2�. 'a-h } �."h r�«i 1:+..ta.i,b%l�a`!n fl..•11:''n;, a�,.iti 28 C 87 3.83 6,5,;'400t' 0 7"5�} 15i,. ki "?,)• +t �' L + - ' l ><.'3'D0+' ,., a y. 40 }Y•T , -4' ;.z :3 „',� u°' u: , 29 30 wn, n,r '.t ._.,, ?s.. in'r -. t•,r re c.:- ,( ' ,lo"tf 31 Monthly Loading 65y400`a 0+7,5y,,� ? 0 0.00 y ~;y= ' - ,,;,' ,,✓, �;. ..k's"€,{ ��.ii:.•:Ow>.:!":,. ,,,• ,'}:a,,0i0,0� „ D 0.00 12 Month Floating Total (In) ,AK 58F;-, ?'x 17.41 +ib' �* M =xis *`c,,14188". ; ... "`. ', °^ `s'r' „' ... "". 0.00 " '`3 '✓ .�:>; .> .,i10 _ r�'"' : .'...: , a w,. : FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page _Of_ �> Did the application rates exceed the limits in Attachment B of your permit? Were adequate measures taken to prevent effluent ponding in or runoff from the sites? Was a suitable vegetative cover maintained on all sites as specified in your permit? Were all setbacks listed in your permit maintained for every application to each permitted site? Were all freeboards maintained in accordance with the specified freeboard heights in your permit? E Compliant ❑Non -Compliant OCompliant ❑NorrCompllant ElCompliant ❑Non -Compliant El Compliant ❑Nan -Compliant OCompliant ❑Non-Compfant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. . Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Lee Matthews Permittee: Murphy Brown LLC Certification No.: 995905 Signing Official: Andy James Grade: SI Phone Number: 910-217-5211 Signing Official's Title: Marketing & Logistic Manager Tarheel Has the ORC changed since the previous NDARA? Ayes EINp Phone Number: 910-865-1310 Permit Exp.: 12/31/16 Signature - Date Signature Date By this signature, I certify that this report is accunale and complete to the best of my knowledge. I certify, under penal aw, that this document and all attachments were prepared under my direction or supervision in accordance with a system deslg d to assure that a0 quaffed personnel properly gathered and evaluated the information submitted. Based on my Inquiry of the person or persons who manage the system, or those persons directly responsible forgathering the Information, the Information submitted is, to the best of my knowledge and belief, true, accumte, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and Imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 t-UKIVI: NUfVILK U6-1 1 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page —of — -, Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash County: Bladeri Month: April Year: 2016 Field Name: 01 U, Field Name: 03 Field Name: Area (acres): 3.23 ,0' Area (acres): 3.21 Area (acres): OverseedfBermudz 20 . Cover Crop(s): Overseed/Bermuciz er, Cover Crop(s): vve rseecutserrgud, Cover Crop(s): Load Type: PAN Load Type: PAN Load Type: Field Loaded? OYES 2NO Field 7U!T, Field Loaded? DYES 121 NO 099,_� Field Loaded? DYES ONO �i", "I , z Z, -1.1 - I z Z M '11Z,',1)111�' o (L 0 :E o z 0 Z Z, 0 CO E 0 U 0 et Month lbslac lbs/ac lbs/ac lbs/ac lbsfac lbs/ac January 3.7 3.7 2f 10.3 10.3 February 0.0 3.7 j 20.2 30.5 "TQ March 0.0 3.7 0.0 30.5 MN�15 I w, April 4.3 8.0 0.0 30.5 0 p01V May is r June zmv_, July August September October November December YUKNI: NUMLK t1tYl l NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page _ ot_ -, Did the mass loading rates exceed the limits in Attachment B of your permit? 17Compliant ❑Non-comphant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not In compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Lee Matthews Permittee: Murphy Brown LLC Certification Number: 995905 Signing Official: Andy James Grade: SI Phone Number: 910-217-5211 Signing Official's Title: Marketing & Logistic Manger Tarheel Has the ORC changed since the previous NDMLR? ❑Yes ONO Phone No.: 9 - 65-1310 ermit Exp.: 12/31//1166 �{ Signature Date Signature Date By He signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty law, mat this document and all attachments were prepared under my direction or supervision In accordance with a system designed to assure that all quaffed personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person orpersons who manage the system, or those persons directly responsible forgathering the information, the information submitted Is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, Including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mai( Service Center Raleigh, North Carolina 27699-1617 f-ORM: NUMK 1U-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page _ of _ I Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: April Year: 2016 PPI: 77Flow Measuring Point: ❑Influent ElEffluent El No Flow Parameter Monitoring Point: Dinfluent OO Effluent ❑Groundwater towering ❑Surface Water Parameter Code —► i^5005i0s r, i')0,0400h:j 00610 t 110kfi25"e 00620 >, N 6N E W U C O 4 =tr 3;i; y o - 1`a``�' f T'}H' ie, 1 # <p,t -A '¢ J. :. ,y E Q YOtdfa. }jL _ &Nt L 'i' 3^;v0 i0. x 'r i L . ti t, 'f^.,. i k a=" w fav {3'5 ! xa V'`e, 'i �rs+r',''m'i :r'•'a.'(t 'A ka 1✓'luiAr d% 4Y z e'yt f 4'Y.`r a :. 24-hr hrs ri:,�G,PDr i' }::ssu 1�1 mglL Wrm'91L'nO mg1L 2 14:00 1 3 '.w,y �69.. 5 ff 4 _..__ :av <iss,2aal 5 +. ,. "s.. s0 2 w ...P,.,. a� vzs r a - cefi :#.Y.' 6 09:00 0 5.:";3 4 k YSbK f av�.�a,t.,ar1 eL 7 12:00 0.5 NINE 4u,'.r. 6 i+ t* [•'� Me M»14.1'z'.. AS 4v(ii r't'ii! 9 N 1g ! h� n# P£i ,.. 5 '^y� �ilv:� wyi _ 44 '+ i ..i. � .< 12 a5:. 01:£y .?.F... �.y"•.x^+�',, 3",6,..a..KSiIV,a arc ,ra.T'�..'a 13 12:00 05 0'�i^ g-sµ ..r; xt�xu'rky"" s r�s ;':^a- S atih 14 16:00 05 i0`. f_ _.a. but r.4._ry trl+' .sj..Y'^""+'�,"i .s.'m5'p r:•. a,�'LL,a, 15 �`:�e ,0i II...' e s of !7 n ;"I ','n� ,e„;! �i,:... :t.s:� ,{1.,. < a , k:,A�^..t t, w ,[� �kXaV.e$ =•m- 16 17 1' n6, .%.. �'f .:w f ;:S ...La 'VSe •�iG�.�'u.uuli� il;';�Yq'`F} 1:i ( A°�'.5�.�"�.Su^. 19 {'t r0,„ 1::."t _ ix;E,s k.. ,1-ir<�3. c.. ..e n4- x v7„s€F�,,, .12,. _.:.I:Y .sr-4, sw-. k,C .rrti x:;T� 4 ,�.. ..5+'S �:<k� �t Tr 1„x 1✓�r 20 `.,.t..0..<' Mm�x +�*n;>al �s�, . ?;�s'�,�ur':; �:n svca��� ,>?�_-. .�: �,1:' 21 li...:;'I<y 22 14:00 0.5 r �, ', Y..aa.::'avl �Ebfla a.._+Pill 23 15:00 0.5 sYiz ar ..?„g� 4e,r ..}v 24a...n0.,ifi.'i .'�`" n"?'. n r<,+;'i• wuti�ae�'i ar:f. M...]l:; ld�a°Mv:;�„'i 26 ! rS'.+3_: i. " .i^1':aix.:.G! —^n :i s+�'�.�,_sir f. `a 1 ii] s Y' !` y N `"k 26xY %asLr ..r'�w_t 27 - « Oks; i4 '� _ F... ,ra, w% >_ ... .v! .!1✓..:....:, ;sir w fi ti ..m+t ,4LziS 28 i+ `.�.�0&a: ,'�3*?;i t.... ,_s er eM-' t,ud�r1 _. `s'.."t.,x '^ 29 08:00 1.5 �`r �0 2i - s'_r;�. xv'Ym".d x, ,y w d-� :Y., R,r, v.•9. 4.�.I�xrt * r 30 0,, }'ur:.'.i'a t ' .y:.,..� : � z 'k -.7..5'."' 'id. x mky.. a„u.s tF •"it n i ¢ 31 y".s}�S.. -'" 4'� .z'ri ti,:ir `a,. .,..:»Sw'I 79;w'*`,s1a< vAt'x Average k" 3,tr'I,:;; Average: Total(9al)_ I- Dail Maximum:Month .,%mY.!'.,b 1},u +"+' 12-month total (gal) s"2; JGIs1?525, Daily Minimum ,.if7,. ;i 6.., t ^,`'' '6 `c.'t'S {f �G, �a_..:^� "`.'."v-s�".`ya �.w �i� <t {"r.'s Sampling Type fiecorder". Sampling Type ..,+.,Grab,` Grab t•,uGfab_•-1 Grab '},G,ra¢Yr"j$ z,rHEa?,, 12 Month Total Limit 77Q0,0,`' Monthly Avg. Limit Daily Limit: Sample Frequency: jGonnusSample Frequency 3xYear 3xYear rar,-Z, 1 FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page _of_ Sampling Person(s) Certified Laboratories Name: Mitchell McDonald Name: NCDA Name: Lee Matthews Name: Enviro Chem Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? OCompliant ❑Non -compliant If the facility is non -compliant, please explain In the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Certification Perm ittee Certification ORC: Lee Matthews Permittee: Murphy Brown LLC Certification No.: 995905 Signing Official: Andy James Grade: Si Phone Number: 910-217-5211 Signing Official's Title: Marketing & Logistic Manager Tarheel Has the ORC changed since the previous NDMR? Ores 0+1,10 Phone Number: 910- 6 10 Permit Expiration: 12131/2016 Signature Date Signature Date By this signature, I certify that this report Is accurtate and complete to the best of my knowledge. I certify, under pen ty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel property gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the Information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false Informaton, Including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 _ N SMit A iM, Hog Production Division April 14, 2016 ATTN: Non -Discharge Compliance Unit o h bo DENR y a Division of Water Quality rn 1617. Mail Service Center 2 Raleigh, NC 27699-1617 Subject: March 2016 Monthly Report Foxfire Trailer Wash Permit No. WQ0034987 Bladen / Cumberland County P.O. Box 856 Warsaw, NC 283% Tel: 910-293-9364 Fax:910-293-4130 Please find enclosed the NDMLR, NDAR-1, and NDMR form for the month of March 2016 for the above mentioned facility. If you have any questions regarding the monthly report, please do not hesitate to call me at 910-276-0648, ext. 64463 or e-mail me at meudd@smithfield.com . Sincerely, Mike Cudd Land Nutrient Management RECEIVED DEQ/DWR APR 2 5 2016 FAYETTEVIL EOREGGIIONAL OFFICE FORM: NDAR-1 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page — of _. " Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: March Year: 2016 Field Name: 2 k!,� Field Name: SUB1 Did irrigation occur Area (acres): 2.29 4 g Area (acres): 4.56 at this facility? ;,Bermuda Cover Crop; Bermuda Lr NXIMINMORM� Cover Crop: Bermuda Cover Crop yc ; ; P1y1e1A�_1RPJ 1. - �. DYES EINO Hourly Rate (in): 0.5. Qff ED Hourly Rate (in): 0.6 4 Annual Rate (in): 21.2 Annual Rate (in): 21.2 Weather Freeboard y`Oves:y 'ONO+ "_ Field Irrigated? OYES IJNO 'raFre7tlfllrryigate�dl�(OwEs YtkNOs ri1 Field Irrigated? ❑vEs ONO AFMeId,)Irygated? 0 X� . ..... . E E = 0 U 12 E E m 11-k:11 E .2 E•P.T 0 M 0 X 0 0 ti IV - I 0 M 0 X 0 'm M = E > ­w ?L11 > F in ft ft gal min in in' t"A �51Z:ffl M ,2�i ;6�' 6M gal min in in 21 5 f1 "T "M Fg.Pr ....... 61- 1 W. w N BSU. 3 4.25 "�& 11 4 0.5 6 Y­­ -i r_P Uz'.k:£4j . AF�� 01M Z 4� 6 7 H 10M 5—_OU9 FPN, 'I 9 TnmyJ? MM nigM U 10D IR IMP I 10 11 4.08 T�—�n *Em is �n 12 1 '^ 1S� 5A Fg— '-I.i 13 1 v5 14 L5 t16 17 �0 Q2 �.`51� 18 4 MUM i�U Ow 19 t �, �--s z,5 20 21 22 In 23 24 3.75 Ilk M 25 N 26 :Mp, U 27 28 0.5 q �.Kb U 29 30 31 3.67 114Nj "Zia RUP5v'i _0 6�0.00:� Monthly Loading: "M011 �IAIAMA_e 0 0.00 OQTW� !!�Ix �T� n, 0, '777,70- 12 Month Floating Total (in): 41 m6wAft "A�-,88 0. 0 0 V—mw FORM NDAR-1 10.13 NON -DISCHARGE APPLICATION REPORT (NOAR 1) Did the application rates exceed the limits in Attachment B of your permit? Page_of_ uCanpiam ❑Nan-0ompian•. Were adequate measures taken to prevent effluent ponding in or runoff from the sites? 2cempranc ❑Noo-[ompian Was a suitable Vegetative cover maintained on all sites as specified in your permit? mmmprua ONamompram Were all setbacks listed in your permit maintained for every application to each permitted site? Riamprart C3Nt Ccmprark Were all freeboards maintained in accordance with the specified freeboard heights in your permit? Eltkmpaera Oncmoynpv= If the facility is non-compllant• please explain In the space belmv the reasons) the facility was not to compliance. Provide in your explanation the dale(s) of the non•compliar¢o and dosedbo the cormcfivo action is) taken, Attach additional sheets it nace=ry. _ Operatorin Responsible charge (ORC) Certification 11 Porminoo Certification ORC: Lee Matthews Certification No.: 995905 Grade: GI Phone Number. 910-217-5211 Has the ORC changedsince the previous IJDAR-12 Ovm qvc Signature Date [iytb'a skpinere, l ealajleotthisrax,lhneeir,¢I¢ana =pkta la awtxsiolmykion:etlaa. Parmltteo:. Murphy Brown LLC Signing ofticlak Andy James Signing Official's 7111a: Phone Number. Marketing & Logistic Manager Tarheel Pcrm)tExp.: 12131/16 Data of Ipo person orpea %ft=290 tbo ayslam, rralosopersmaareoymrpnemn raraaumaaguc mramm lai submWea [s,to No 6osl of my )nwVaaaeatd 6etat Ime. accumla, nr4 mmplale. I am exam aul them amsl pradtlearx v�ml:ling Ueldannaft% Irwoirg umpassNEV of f=sm 1mp6scAmeit farinos-ng Y46arl9. Mall Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail service Center Raleigh, North Carollna27699-1617 FUKM: NUMLK08-11 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page _of_.1 Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash county: Bladen Month: March Year: 2016 01 tit �w,,,,� Field Name: 03'ieldName 7a;' 9 W`bxi?y Field Name: Field Name: FieldyName, at"02r rtiSU81 Area 3.23 A'rea�(acres) 2,29.? ¢ Area (acres):- 321 - Aiea)(acres)',;{;,;;,+';'t`_4,°56"",°�,i` Area (acres): (acres): �`'e(rfryF �' .4} n Rb I'�u, Cover Crop(s): Overseed/Bermud s ,al .�isQA' Cover Crop(s). wOverseed/Bermud: r*3n Cover Crop(s): Overseed/Bermud Cove Crops r�.� Ovr.rseedfBerSnud, Cover Crop(s): MY ^+kr&,x Load Type: PAN 4 LoadFlyp`e r,;'�wi I '' ' PF�N,, r Load Type: PAN L;oadFT,ype °� ' PANT+` Load 7 e: Type: i ,�r�X,a,� , ;.- Field Loaded? DYES - ONO F eldnLoaded?�x n' ONES? ' , Field Loaded? DYES ONO F eld,rLoadedy7^�,xNp QYFS '.* ONo,�;:E/ Field Loaded? ❑Yes ONO z�ONo` s 'w.w1 i,. 5 qc t' ry iy i 1 l� k un Z •� 00 tl 4 1 �'O ,0, rvp N d L. a A J r ti� aY e �T IA hYUL1NM10 r i Jt it N O = RnY -' m{��' H} �"4GE U!'Y.yA,i Jyr�S aer O A J Z E T Lt;O u4 1 "r,*'w J yF, y''OSSZ x..c '.. k' E E W O J O Z E p',: 'G1L'x^O.S'�Ra!"o sikY,c:c J...S;''ES G' �fi Z°#i1 -Vh E O E J a"' k'xtYf c o o �j �.'�. ci Month Ibs/ac Ibs/ac jay y21159 ac,''=x F „�,�, Itislac, .0 rq.' Ibs/ac Ibs/ac „d`:s t`181bslac z x, ` st `(S,Ipslacv 'e'«# Ibslac Ibs/ac January 3.7 37 ';, 10.3 10.3 lay)u�u+eit4y0t�'1J1$31�w:�f'�,;:",If�,00r7�TM1�,�*'," February 0.0 37 tir T 26'7,;�a 1i .�a.:l•,3,95 cri,_?i 20.2 30.5 Ce"Qk''�'ir+0?9i ya'nSFi,"�L'r'RuwiJ'r_O Oc .+�ae?S! 3 7 Oro "-' Tl' 5.,z'_, 0.0 30.5 �Si-0!Otv".t7.t'' Iit. March 0.0 .,x.._ : > ..__�:39 M:� Apriln..."^ <y May Z5_i:i.r-,. June July : 3'"� �... •. r-,.� t ,� fdY- "�Syn a h a ,;,erP„ 5 y'�r. ni*'r- e �r l August )i'`s sx °� �c."!.. .y a4� -a".%� �e aiu`wk kiS.AnawYs""'.S��i�'s,It.3^:a'-'t..`!.i�.�x<,ti::3: September October �.2u4 x�' Y::A;�r ," a° IS' ~~;.,' ,.x T'�,}x"`Js;.,Ji;'��ra .i''t. uha'i'zs' November '7 JS�^�`x 'rt:..,:5h`� /`",.,t ,.; ,1;r ?Erkkl�.'�,.",:I.x�rN n?'_," wvl mg,.�,�'�a.r�r ,December FORM: NDMLR 011.11 NON -DISCHARGE MASS LOADING REPORT (NOMLR) Page _ of _- Did the mass loading rates exceed the limits in Attachment i4 of your permit? pmmpcmt QNm<bmPMrX V the faa ltly Is nnn•comollant. nteaso explain in the spare belmv the reason(s) the facility eras not In compliance. Provide In your explanation the date(s) of the non-compliance and describe the corrective Mon. A1taCn annlpenal SmCeIG Oporalor in Responsible Charge (ORC) Certification Farrington Cor incation ORC: Lee Matthews Pormlttco: Murphy Brown LLC Cortlncation Number. ,995905 Signing Official: Andy .tallies Grade: Sl Phone Number. 910-217-5211 Signing Official's Title., Marketing&LCglstir. Merger Tarheel Has the ORC changed since the previous NOMLR? t7Ycs pro Phone No.: 910-85513 Permit Exp.: 12/31115 Signatura Dale Signature Dale eYaissignalum.S atdYywatlHsmpa:lsaaaaraloantl rmlplolato Nenosld myMmdCda0. [aNy, utdcpelultyoi Mv,thatUiv dowmorl mdoaollndlmmtsgsm prty0.vd untlormy6too6m tt-^.apuni�ontrl n®rdaltasstm ncntom tlosklnetl to assuta Noln3 aualfintl rotsornol PopoMBa:nnrodmd a+aWatee ale mspoo,ala for tinum n9 the rdorm-wn a0.lnalo, andmVeta. I am al'Am W P=%b1tyd Mail original and Two Copies to: Division of Water Resources Information Processing Unit 1s17 Mail Service Center Raleigh, North Carolina 27699-1617 ixt rnalho FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page _ of Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash county: Bladen Month: March Year: 2016 PPI: 001 Flow Measuring Point: Dinfluent ElEfDuent DNo flow Parameter Monitoring Point: Dinfluent El Effluent ❑Groundwater lowering ❑Surface Water Parameter Code —►'!� 5Dd50s e= >, m ❑ '- m a` E U 1- O N E 2 f w U❑ K O O Vey 41.t vtc i , Y ti11 i. r 3rs' ,.s ^° LLt az :^) e r uA { it r 11, {'4 w'f \ k i,.,` r < , a �' ', v "" lhy, do d i +* kLl .�, bl,. G o E E E �e .:h I t i�i � d « a rnr' o. 3.- j,�, �A".J « S .tl7dV1''�'r ^, iG• r'S'. F@J tom,;} I kb fj.�. 24-hr him IKI,GPD_;.;: mglL glL,l mg/L A.4e.5nJ_ eu" 2 3 14:00 0.5 7,74 � _r�1 U.;;r.M �:3 3` �i:� " - L"A"a,.-x:S 5,8 4 15:30 0.5 1Mc_u. 5 � `T"�Oies� u� a.'t�:.a a.,..w : th- Fi aMS',< '+r.<s ,'�:'• �vu,,w :�,. �',Z � y .#i�_'i.�.ty 6 i:,,5r543,.<' <<%.,c r. ?'.: t r:.._Y....a Rv..:.a« si �.u,4:..'1,';:ir:t ...c...:.9' 7 37.4 „ .; 49 6c%,�;. 0.17 ,..22•;9�:'i i. S."i u.a',4r.1"i G';,fa„f�..-: ,;;-t: �.r 4'.�.; 8 m`5 i9,1463, 9 .9+007r •, r-. r z',., r v^,'.r�s� 1 t Y' tmtn i'.. .:+'q 10 11 12:00 1 12 >. 0 r K rt'7''0 vA..,r. 13 14 9,423�,., �^ 15 8 49949 +,� r ;l Y ":: h,Fu .,x y.- r {:; r r;h ",In _ti' _ rMitl 16 _ y10 265 . .-.aY :tC..,-: t, 1.=,".t... .:l ?" tLL il.'frW, t.. I..i._14.t _ i 5' k'rU 17 i,11 s. 18 13:00 0.5 9069yy;":;...�`,".. 19 20 r '10 <.ur x,. . e,� =a ;'--a^e :a a t e- t'�" xr f a', f 3F` �r •§ F`£'': 21 22 23 10:00 1 - ,7,"7,794., 16,„S',::rL: '! / ! w 24 15:30 0.5 ,x L`4G1>NYV. ,.,t 25 ;, 10,35]2", ,c �,✓ a s rr^'''r '''!t>"1"u ": xrs`;^a' a ,N' 26 ., 27 28 09:00 0.5 29 30 „ 9'970<' .. , '' t z ktii,c. .GAF«n 'i _._ _,,. x.. wi r...,,_:3r].,, v , v m.,,?t s� 31 'it53 .ta,lSr ..1 SU`eN.. -,tu '.lvnadit 1%1 �e w,ii vat- �bYM1 k .I.1 Average: i_�,7,t258;:,�; Average: "';, 37.40 k, „#REF,+e) 0.17 ,�„22,a'9Dc" °, ty!",,.,�+; t.u$r4�,n;� Month Total: (gal) ;. t'225,0,Q1i� Daily Maximum 37.40 ,�„49',60u e'i 0.1722k90!'}! 12-month total (gal) ¢2 34,1''926'( Daily Minimum n.?„; ,.f 37.40 0.17 Sampling Type: Sampling Type: Grab ut,"`,.=G,iabi,�''.;? Grab 12 Month Total Limit ,577$60OF Monthly Avg. Limit: w`"„�..,,,.,,--." r ';i;;,,„y-: y" „`,,ab- , h�,;'rn,�:";�k _`yr s . Daily Limit: sF wr.' .,a;, 7 g Ne ., u_."v 13"`.�=, t'1:: uu 'r -� x 'Y +.`»...: 'C�s"� -i3 arrJ,c <ta.. ��j 3' z Sample Frequency: ,:Con4nuous'r Sample Frequency .8 z,yeay "; 3xYear „,.3'zyear„� 3xYear r, z3{i{,year,r1 ^�{.,y 4x�. FORM: NOMR 1043 NON -DISCHARGE MONITORING REPORT (NDMR) Page _ of Sampling Parsonts) Carilfied t.abomtorlas Name: ' Mitchell McDonald Name: NCDA Name: Lee Matthews Name: Enviro Chem Does all monitoring data and sampling frequencies meet the requirements in AttachmentA of your permit? Emmprant @.hndLmpaarl If thefooility is non -compliant, please explain in lhn spoca below the raasan(s) the faellitywas not to compliance. Provide to your explanation the date(s)of the non-comptianco and doseriba the corrective acoantsf rurcen. Ar,aan Operator in Responsible ChnMo (ORC) certification Porminea Certification ORC: Lee Ma(thevis Permidea: Murphy Brown LLC Cortification No,: 995905 Signing Official: Andy James Grade: SI Phone Number- 910-217-5211 signing offccial'sTigo: Marketing & Logistic Mamgeriarheet Has tba ORC changed since the previous NDMR? L]yes ONO Phone Number, i0-865-1310 Permit Expiration: 12131120% // Signature Date E9n re Dale nyaJzs'gnnlmn,locrGrYlh¢lUtis repofits ocsena!¢rndcaTpkter¢Cr¢b�tetrrylnaiActlae. Imlay,1 ml and an nim:tnem%yci) pmpzred mclarmy6-ccU¢n"=T=Wmki aoxedaamNehanyslemtl¢ti to assure Eisranqual9edpr+sarnd gopatya¢UtaadaYallnlcd U:OlNomaGen suhminatl. nasedm myhgJryarUapersanorFcrsansnta manae¢lan sy5101n, arUnsepnrsaa a'.rccLyreSporarKnl¢: yetnerL:g ttw fnfwmivUpt Lhc htamnUm sJxNUM is.l¢ Ltia Rs1 W myfaw�Ncaa¢ andbaiaL wa,acauOl¢, rnd e¢mphla I am oC¢Irlermyyx-'umi9lncp¢ssroUllywrrx>: fin¢Mlclsarmam axnro aatexYa rca sla nlptrwnbsfaonrNchI, for Karim abhuonGmc Mail Original and Two CDplos to' Division of Water Rosaurzr Information Processing Unit 1617 Mall Service Center Raleigh, With Carolina 27699-1617 19 Sxni Hog Production Division March 8, 2016 ATTN: Non -Discharge Compliance DENR Division of Water Quality 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: February 2016 MonthlyReport Foxfire Trailer Wash Permit No. WQ0034987 Bladen / Cumberland County P.O. Box,856 Warsaw, NC 28396 Tel: 910-293-9364 Fax:910-293-4130 IREC DE6 6VEF VIR APR 1 92016 FAYETTEVIL E4E 'O NAL OFFICE . Please find enclosed the NDMLR, NDAR-1, and NDMR form for the month of February 2016 for the above mentioned facility. If you have any questions regarding the monthly report, please do not hesitate to call me at 910-276-0648, ext. 64463 or e-mail me at mcudd@smithfield.com. Sincerely, Mike Cudd Land Nutrient Management 1­ URM: NUAK-1 I U-1;3 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page_ of_ %', Permit No.: W00034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: February Year: 2016 Field Name: 2 g Field. Name. irrigation occur Did irriga W.7 SUB1 Area (acres): 2.29 Area (acres): 4.56 at this facility? G d ..... .. . I P:, Cover Crop: Overseed Cover Crop: Overseed BYES Elmo 6f5f,-7; uHourly Rate (in); 0.5 7 Hourly Rate n): 0.5 Annual Rate (in): Field Irrigated? 21.2 l 13YES RINO Annual Rate.(rn) 1 Annual Rate (in): 21.2 Alffi ...... ... gNJUNON,'j Weather -�: Freeboard &F Field Irrigated? 2YES ONO I �11-1.ik '�S iz E E2 r E E .2 T 0 X 0 M E E 0 > w 0 0 0 a 0 0 M V > J. ft ft a1v gal min in in gal min in in 7 2 3 4.25 4 1.5 4.08 5 1.5 7, 6 7 1 3.83 E a 8 0.4 t .rlsm 2MM 0- Ef 9 0.2 10 3.75 r-i all - - - 11 W� T�i� �5� 12 14 15 R E�9= 16 1.5 3.42 17 18 19 C 55 gz, 6 0,000 300 0.9E, 0.19 A 6 5 0 L7,1�-.,jj - -11�zll 6 20 C 63 4.17 60,000 300 0.96 0.19 21 C 69 4.75 60.000 300 0.96 0.19 22 23 0.4 -t� U'�r,l>! 1Z 24 0.5 4.67 25 0.5 rU tM'l tl'Uj X 27 28 i Z5K 29 3014 IRIIE31�1 tli� ttm- Zis& a. 31 Monthly Loading 'Of�VP`n 1 180,000 176w 2.89 Mimi -0 e#.7 0.00 U- 74 12 Month Floating Total (n):IM�Ly- 'IY, rKMPJlM=Wj 17.4 I 1�Wgmxwwz 0.00 Amalmg FORM: NDAR•1 10.13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) page - of - Did the application rates exceed the limits in Attachment B of your permit? Were adequate measures taken to prevent effluent ponding in or runoff from the sites? Was a suitable vegetative cover maintained on all sites as specified in your permit? Were all setbacks listed in your permit maintained for every application to each permitted site? Were all freeboards maintained in accordance with the specified freeboard heights in your permit? GlUmplarc Otion O mpupt g' o=ram OKW+{ plknL Ocompruot l7Non-Qmp7a.t Ecamplant ONaaamyJa:t elcwnplant Uzimconpinm li the facility Is noncompliant, please explain In the space below the reoson(s) the facility was not in compliance. Provide In your explanation the dates) of the noncompliance and describe the corrective actlon(s) taken. Attach addigonel sheets It necessary. Oporator in Responsible Charge (ORO) CertlCication Permittee Certification ORO: Lee Matthews Permluea; Murphy Brown LLC Cortittaallon No.; 995905 signing official: Andy James Grade: SI Phone Number. 910-217-5211 Signing Official's7ltlo: Marketing& Logistic Manager Tarheel liar the ORC changed since the previous NDAR•t? Oyu, Mno Phone Number: 910.865-13 Pannitap.: 12131/16 nature Dale Signature Date aytlf4s!9 arum, IMIVY IVIS mFatlsartrmlo aid compinloto Um bmtoraryknmticdac. Ie[s5y,imdvprnahyaflmv, dwt dca:mam nnan[atlaChmpaS WcmFrcpprcd untle-nryG2c6onots�perv[dmin asardhmoo With a syr..amdaslaned la assum ear al Quatasd panatnolpepM)yn•JmMd atd owlratnt era Wmrztlan srr:mignd. aosada:tmy Irquryarure parsonorpersansNnorhuswnodn.yslem,vlMso rl=s *00M rosassblt taraotlxMa aminf m Uea, tha Ytsma7ehrsubmated lC Ioe+pOCsi otmy krcnY.edpaard bet{o6 Rv. axhtato,and wmgc:a I umvwranul rhoro am s1an1r=r9 pchtJtic.raa�mEllaa ra15a Iffpanaten.bfGrdlrg 1Mpca]IptNyolefasatd Imphmmhyhi for glmWhp lielCCni Mall original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 276994617 rumor. +vu+vrLrc uo-+, NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page_ of_ Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: February Year: 2016 Field Name: 01 Field+Name slip t',02 ,�.,a� Field Name: 03 F e dENameRx„J w �rSU61"Svc'$ ! Field Name: Area;(acres)+s +`ti Y`" 4�58 `P' Area (acres): 3.23 zM Area (acres): 3.21 Area (acres): ��Fx any-^. raarr,��. � ' 6 gm C ymi'`Y-' _ OverseeBermud Cover Crop(s): verseed/BermudCoveFCrop(s): CoverCropffld Cover Crop(s): Load Type: PAN Loatl/Type`„ .�, + k 5 °P,� Load Type: PAN t. ad Type, Load Type: a y.L' 1 Field Loaded? DYES ❑N0 Field Loaded? OYES ❑No Frejd�'Loade`d?`^+++DYES" .;r7o"` '_ Field Loaded? DYES ENO s , e ' ' - " " '' rK ""'k4'z Figltl,Lo"a�dedT, OlYsp NoyM 1, ,. Z k 11 x # c4 it m > ) -gj0 E W11. ZnE .O� � a 11Vr a �.,'u` Month Ibs/ac Ibslac+r Ibs/acrt5ltis/.ac`P;:=i Ibs/ac Ibs/ac t;j,A.j12�8'; ?�� rr („ da v 12,8 "',un ;3 10.3 103v 4„rlbs/aca r�,, ti F"a�` �1� I n, Ibs/ac Ibs/ac January 3.7 3.7 February 0.0 3.7 6 7�14 i �. �,*a 39°5l , „r", 20.2 30.5 "`,' �' rOxO',q ` wv,y rt'x'� ¢, * `e,Y F R:.4' R' N3 su3Q'Da a March c- r''` *. r.: KiO2112 April May June G 4aw w4 4Lw G%Y Y' 5^r3 % �l July Augustin: + Sxss'..'•+i .0 .::{'ax �`rv1"mw,.ztariis.',L s'7r�"`�'"'i't September !=t,',�,-rr'`�` ^.; ushi•'tn'.'..'K': �'cn'¢3 Octob iy .uu 88,ia*s: November December F;,.r W �,..� A' ? ,u� *s:3�'.,'.._ . r r ,1su0 ....r�n"wa r� 1 FORM: NDMI.R 06.11 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page __ of __ Did the mass loading rates exceed the limits in Attachment B of your permit? Qevnprar MNmCornpllant If the facility is non-complianl, please explaln In the space below the mason(s) the fadlitywas not in compliance. Provide In your explanation the date(s) of the non-compliance and describe the corrective edion(s) taken. Attach additional sheets if necossaw_ Operator In Responsible Charge (ORC) Codification Pormittoe Certi9cution ORC: Lee Matthews Permitteo: Murphy Brown LLC Cortlfication Number. 995905 signing official: Andy James Grade: SI Phone Number. 910-217-5211 Signing Official's Title: Marketing & LDglstla Manger Tarheel Has the ORC changed since the previous NDMLR7 gres ONo Phone No,: 910-B65-1310 Pornit Exp.: 12131t15 Signature Data S nolure Dale 6yWs sO011M,ICa*0011 hre,xnlaem,anlamd mmplcleto the bead myX=Ial9c. Io�Cry,uMcneaaflvOfmy. tent tat: d a,lmd,n,nxrm,nt<..n,..rmn.,.r���..M,..n.,..,w.............,.,..,- =Ple,o, Mall Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mall Service Center Raleigh, North Carolina 27699.1617 gq=cd tbeaefjruo, mrbNra dw I -OHM: NUMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Page _ of Permit No.: WQ0034987 I Facility Name: Fox Fire Trailer Wash I County: Bladen Month: February Year: 2016 PPI: 001 Flow Measuring Point: Clinfluent ElEffluent oNoflow Parameter Monitoring Point: Oinfluent ElEffluent OGroundwater Lowering OSurface Water Parameter Code i 2!9006"' 00610 0062 75' 2 < E 0 r M Ci 0ti, ✓E p, 0 E < Z' f 24-hr hrs mg/L (m4/L'`— mg/L rp 4rr 1 p','31:1 it 2 3 15:00 0.5 J!27155Q, 4 5 6 7 . ..... , , .", �. 8 12:00 0.5 "�:61 Re -_ .1. 10 16:00 0-5 11 12 13 a2� 14 15 ONE, ;INV� E."11,71,51 I MIR 16 12:30 1 17 18 19 15:00 1 1.5 20 16:30 1 77-<11' 8,z & 21 14:00 2 ZI M.-T, A 22 23 24 25 15:00 0.5 26 27 Ifie, 'Oal 28 29 30i Average: Month Total: (gal) 12-month total (gal) 2,96 466J i-'2V2,92,7e' Average: Daily Maximum: Daily Minimum: Sampling Type: jF%dqrd(ft Sampling Type: Grab Grab 12 Month Total Limit Sample Frequency (3�57,7q0 ,qhtg Monthly Avg. Limit: Daily Limit: Sample Frequency gn3,xayeary 'Zi X�b 3 x Year P v FORM: NDMR 10-13 NON -DISCHARGE MONITORING REPORT (NDMR) Pago—of„_ Sampling Parson(s) Certified Laboratotlos Name: Mitchell McDonald Name: NCDA Name: Lee Matthews Name: Enviro Chem "--- -" - ---� •• •••�••r. ••••y o.a un+—liplirry ucr{ucnues tneeLtne requirements In AttacllrnentA of your permit? Olzma;an: 13-VwR%mc;saac If the facility is non -compliant, please explain in the space belowthe reason(s)the facility Was act Incompliance. Provide in your explanation the dele(s) of the non-complianco and describe Me corierAiva action(s) taken. Attach additional sheets if necessary. Operator in Responsible Charge (ORC) Carillication Patmihoa Certification ORC: Lee Matthews Pcrmiltee: Murphy Brown LLC Certifical(on No.: 995905 Signing Official: Andy James Guide: SI Phone Number. 910-217-5211 signing official's litio: Marketing & Logistic Manager Tarheel Has the ORC changed since the previous NDMR? LiYes 171N0 Phone Number; 910-865.1 Parmit Expiration: 12/3112016 Signature Date Si lure Dale ay mtmglmue, l ceNfy Nat afsrcpatis arcnlrem and anp:WelothoaoslarmykrmNadg0. ImVWY,"arpenalyarlav, t ui5mavnemand ma:mchmmis%wro pteparndhnMd yd:r¢ivatedstpervis5n In acpNancatvgha ayslemdasignad to essmo Halal gwtredrwraoanef ptapedr grchm,dandevofuolN the W.ammem aCm4lM. easad onrryNgnSyel Lhvpersanapetss�vAsrrsrmgctnosysfcm,shlosa porsohs dlady s; MM'�'^(or lulha:iq ma Warmaap,, a:ataroam5cn abriflan[s, to Iho baT. elr;,ykrxtk`�a�om,n `xi'W,Ins, aeasale,antlmm,�'ele 1 om avevnwt tseru a.•esignC�rymahksfasunnAS�p Ia1;vlKcrmatcn, ifcLGna Gha p�n'sltyolfntsnrtl Imp55rnmcrt 2r h1MVa Vla:mrtt,s Mail Original and Two copies to: Division of Water Resources Information Processing Unit 1617 Mall Service Center Raleigh, North Carolina 27699.1617 Smithfteld Hog Production Division February, 2016 ATTN: Non -Discharge Compliance Unit RFC -El ��C.d DENR L.d Division of Water Quality FE91.7 2016 1617 Mail Service Center INROR Ral igh, NC 27699 1617 AM7NpRo ESSINGONIT Subject: January 2016 Monthly Report Foxfire Trailer Wash Permit No. WQ0034987 Bladen / Cumberland County P.O. Box 856 Warsaw, SC 28308 Tel:910-293-9364 Fax:910-293-4130 Please find enclosed the NDMLR, NDAR-1, and NDMR form for the month of January 2016 for the above mentioned facility. If you have any questions regarding the monthly report, please do not hesitate to call me at 910-276-0648, ext. 64463 or e-mail me at mcudd@smithfield.com. Sincerely, �O Mike Cudd Land Nutrient Management RECEIVED DEQ/DWR FEB 232016 FAYETfEVIL E�R�ONAL OFFICE t*UK1`A: NUAK-1 1 U-1 3 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page _ of Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: January Year: 2016 Did irrigation 7 Field Name: 2 Field Name: SUB1 occur 3 Ew Area (acres): 2.29 Area at this facility. 7 (acres): 456 Cover crop: overseed .. .... Cover Crop: Overseed OYES ONO AHMt (Mn Hourly Rate (in): 0.5 our] in Hourly Rate (in): 0.5 5t iA Mal, Annual Rate (in): 21.2 — Annual— Rate (in):21.2 Weather Freeboard bld Irrigated? lit Field Irrigated? OYES ONO "a aFieid°Irngated� O, ES SON X Field Irrigated? OYES BNO '3 0 0 E 0 E 'a �u E :Ej E o M S=m rpm 2 g M I 0 t > 0 a P > 0 0 P WED_� F in gal min in in W gal min in in 0.5x.A J.t 2 3 IG 4 C 48 3.67 70 0.95 0.21 '4 'A Z�& Ak 6 C 49 4 '—N tE 1,500 300 0.99 0.20 7kr,z C 51 _C1,500 55,350 _3( )0 270 99 0.89 0.20 0.20 C 51 5 9 C 55 5.42 55,350 270 �T.89 0.,0 10 11��IIIMM �i� M 0A Q, N1 t!"IF Z, T2 13 TUM Naaft ........... 0 14 5.17 ........ ........... is MEE 9M M ­n RE ow, "ml 16 0.4 �F 125N 17Y.k n 1, 00 18 0.4 19 Q�,! 31L,,,, 20 4.92 7777 22 23 Mwo 24 0.6 --------------------------- 25 26 it 27 T8 0.3 _M MIM 0m '-wee r t t,tz,,l,,,,t,— -X1 .7 T9 301 Monthly Loa Floating Tote 04.71 ff�IAIIA IP 0 ON"147" 12 Month tt F�1;.520" LM4_ 'It'n, FORM: NDARA 10-13 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Did the application rates exceed the limits in Attachment B of your permit? Were adequate measures taken to prevent effluent ponding in or runoff from the sites? Was a suitable vegetative cover maintained on all sites as specified in your permit? } Page � oT__ 121C mMraa ERwroonprant Elcomp6vc UXMIICwnpilant lacompiant ❑NwrCemplant Were all setbacks Iisted in your permit maintained for every application to each permitted site? Qowaplat ❑NQn,QGM larr Were all freeboards maintained in accordance with the specified freeboard heights in your permit? peompltnt ElhVnCwnpilent irthe radlay is non•complhim, please explain rn the space below the reason(s) the facIrdy Was not to compliance. Provide In your explanation the date(s) of the non-compliance and describe the comoclIve aclion(s) taken. Attach additional sheets If necessary, operator in Respoasiblo Charge(ORC) Certification II Permittao Cort16catlon ORCr Lee Matthews Certification No.: 995905 Grade: Si Phone Number. 910-2175211 Has the ORC changed since the previous NDAR-12 ays MKo �L - /a•/G Signature Date 13rthi3si9Mtam,1M*lhai WS MPM tenevnele erdornpkicio$e hcstormyba Yledge. _-- - -I--- Murphy Brown LLC SigningcMcial: Andy,lannes signing of Tciai'sTlua: Marketing & Logistic Manager Tarheel Phone Number. 910-865-1310 „Pormlt Lxp.: 12/31/16 Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail service Center Raleigh, North Carolina 27699.1617 Data o racaendna Ne lewmatbnthe tams . fulmlThemacahnirzar4 nMllalalmrirPvidnlioru. rUrtrvr: rvu1VrLK uo=r*i NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page of Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: January Year: 2016 Field Name: 01 FeldiMame' �'� t { t*ri;02j :`� Field Name: 03 Field'`Name k{�„SUBRt r , �: Field Name: Area (acres): 3.23 Areav(a'cres)"`_�' - a - 7r"` 3229 '��'=="t Area (acres): 3.21 A eaxac�e`s °�?u°" '` '"'r'` ( ) b,4 56 Area (acres): Cover Crop(s): Overseed ro Cover'Crop(s) �Overseed� Cover Crop(s): Overseed s Y.rr'� F" '''° ,ti CoveiCro p _ )r •d0*e seed ., Cover Crop(s): l,t,r tg"m--" Load Type: PAN Load�Type M1 u�`, x xt ,�;PAN,.� k i Load Type: PAN Load Type: Field Loaded?' +SOYF�",+-. ,❑Noy[-�' �. W''!'$�av,,�k, lE.. a'1 Ytt+•i'�\ �'Y ! 14I Field Loaded? DYES ONO Field Loaded? DYES ❑No Field�Loaded?''ai" OrL57,r� �lIONo�, �.' Field Loaded? DYES ONO Z Z > O JV J j_ DO _E E Z. o o E U Month Ibs/ac Ibslac ' ,` ilbs/ac,?:,`;'� ,.=„16s/ac ", I Ibs/ac Ibs/ac n i_ "'Ibs ac :;. a '� ""` ; ' .x ( e "%,e a,llbslacyv,xy lt . M Ibs/ac Ibslac January 3.7 3.7 '?glr�z 128�'�`_....?1 ig 10.3 .G, r.r_1,. 10.3 February Y�,. �7 n� i�rvy`i.i� "r;,K rill -ni March 1ii: 3 �Pkil A F.FM 6 fit, Yi $ m��...( `�� ♦♦ { :)k April May .>'✓, t✓ a �` az- .Nz y June ...�' �i-'E,.m'-_• . 3.4 JUIY L, '� tLaW '..., '` aW +v ..;3"(Yaa�3_xr��al w..,i August September ` t P' k z.c't i..�s`t4'i2 October we«`.wi)l�l�fn'Y�l�n4frr�"i NovemberyG;`r� December FORM: NDMLR 06.11 NON -DISCHARGE MASS LOADING REPORT (NDMLR) Page — or -D id the mass loading rates exceed the limits in Attachment B of your permit? lac malhint EINi Gbmpltmt If the fadllty Is noncompliant, planse oxpidln In the space below the reoson(s) the fadrVwU riot In compliance. Provide In your ekpiana6on the date(s) of the non-compliance and describe the comarliva action(s) taken. Attach oddilionaisheets if necosanrv. Operator In Responsible Charge (ORC) Certification Parmittan cor06cation ORC: Lee Matthews PormlNee: Murphy Brown LLC Cor6ncation Number: 995905 signing Olficlal: Andy James Grade: SI Phone Number: 910-2175211 signing official's nee: Marketing & Logistic Manger Tarheel Has the ORCchanged since thuprevious NDMLR? LlYes ohb Phonallo,-, 910-865-1310 __,—a;ormitExp.: 12131/16 Signature Ely Ws slgmlum, tosrVftl Ihtsrepotis ar No u,d rxmpbtalo mobox: of rry Km*daa. Data s' ere Dale Ica,ary,,mdcrpcnoty&Lmula document cadolartarmmcnatwo atpatcd undrny dicc9on orwpgv ncwroaara sY1L1am1amtlosAlnad bassuatintal amcnadtwnomd tsxaMrmthated aM avalua<edV a 10.vmccmgeto. Mall Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 276994617 NON -DISCHARGE MONITORING REPORT (NDMR) Page —of _ Permit No.: WQ0034987 Facility Name: Fox Fire Trailer Wash County: Bladen Month: January Year: 2016 PPi: 001 Flow Measuring Point: ❑wnuent I]EfBuent ONO now parameter MonitoringPoint: ❑Innuent D+EfOuent EIGroundwater Lowering ❑Surface water Parameter Code �r?50050rx"- '00400 �: 00610 c00625 r=' 00620 N a Y! R 4- 'i (v_' N x 3'. F a ¢ E ~ LL_ d" s s ` p O O u r r ' " Yt•-� k; Z ~ Or Gee g7 r rk r.. z t'S . t ! , k"^}ri O 4 QE 24-hr mglL ;„inglLr+ mg/L - ... 2 Y>}fr oU '. Y �'i'h`.f: 3 YY. }T g 3v -i§i..�.l:!y }Y Syg "K•Sa-�.:, t� Cs i'...`` Y'Y.. 13 In a 31 4 :14:00 5 6862 as 7 12:00 1.5 8�i 4s' �`I✓T` drx" e K s.: Ym' iS t 9 16.30 15 "C.cn: ,�� ,: 19 11 `. 12_12 13 13; 025 ' �( v ai# n t �ry 14 08:00 05 12°2y6 tc 4 pf' ?f i9 u+ t f� 15 1;:'11174° �n"?u i w roc: :..;'. t F's`3rwS,+..^r.i'.L• ';:a.�r..zw.�;".,.,�.��2.t..'; 16 ra 17 18 `':11r659 Ys +':�*- „ - 19 20 21 ;12 689 '�. 22 15:30 0.5 ♦7_ ra � f- d z+C �•` v) ,. S S L V4't w, I u Fi i:Y ♦� s c; ,* ire Im F -.k ;,mx'.> 8hr1( YI � ` 4^r f r; ,.�.N 'ry Y L vV CYl i _I t A�t'k tU s 23 24 dw 25 26 27N15t 28 %`� rr'e rr yy E, MUM >,,"t X� v .. s , ,t 5�a r�', '> . 29 12:00 1.5 a2 b84 , 30 31 Average i y7Fl870 �ti Average: Month Total (gal) , 243 9'2 Daily Maximum 12-monthtotal (gal)2j537645NDaily Minimum: >��, �,.4� �„ ti 't��,,ryt,H ra�?z�l � ,3n 01;1 Sampling Type xRecorde Sampling Type: `pGrab Grab Grati vFs Grab n„GrabrUt; S'ais...x,'t 12 Month Total Limit 3577 000- Monthly Avg. Limit * r�� �;; y.ac >'.xx, y ;; 3 , a Daily Limit: { x s i �i n e I N ` Sample Frequency hConhnu'o`i�s Sample Frequency X3 z;year 3 x Year 3 x yearn;; 3 x Year�'- r> , FORM: NDMR 10.13 NON -DISCHARGE MONITORING REPORT (NDMR) Page__ of_ Sampling Parson(--) Cortlnad Laboratories Name: Mitchell McDonald Name: NCDA Name: Lee Matthews Name: Envko Chem L+oes an monnoring nam ana sampling rrequencres meetthe requirements in Attachment A of your permit? Ocmlpriam E3"M-Qnpe'1 lithe facility is non -compliant, please explain in the space belmv the mason(s) the factlilytvas not In compliance. Provide Inyoorexptanotlon Ihedato(s) of the non-comphance and descnbetha corrective actionts) Won. Attach additional shoots if necessam. Oporatorin Rosponslble Chargo (oRC) Ccrtt6callon Pernittaa Cortinoalion CRC- Lee Matthews Ponnit(ev: Murphy Brown LLC Certification No.: 995905 signing Official: Andy James Grade: Sl Phone Number. 910-217-5211 Signing Offlclal's title: Marketing & Logistic ManagerTarheel Has thoORC changodslnce the previous NDMR? Byes ONO Phone Number. 910-865-131 Pormltexpimtlon: 12/31/2016 a->D-,rS Signature Dale signature Date 9yads ignaMm, I maylhat this reponis=rrele mid Gamp1eleto tloecs:ofmy batleden 10cry,lmlerpcmtry Lnv,leal nts dawmoel and allaUaefnerls%%"pmpamd M&rmyd.'0Cdcn nrvrgorvaim in accadarra WI 43yslemde62110 toassem Ihatnageolhtlpmanatpmpadyaalbemd aar evalmioe thetuommson Gahm;dad,emadcnmy+ iy of axe parsonarpasansnteomonaao Wbsystwn, folr --?hare--mmton,mtell mMrrbttllafasr,Luc. mdmrejlCe.yOamdsCpsmpmR m 4"M mvmNalthm 0re519PcnLsfrabrn?g ftlsainrarmatxxe, Udadhathe pozsL7ityof facaargimpdsomrwnthr gtnnirva Y.cradna. Mail Original and Two Copies to: Division of Water Resources Inrormatton Processing Unit 1617 Mail Service Center Rateigh, North Carolina 27699-1617 FORM ON YELLOW PAPER ONLY 110�r =R QUALITY MONITORING: REPORT FORM Facility Name: Permit Name (if act Person: AMI Location/Site Name pe PERMIT Numbee(ti}4`UO3`_987 Expiration Date: J dT ( Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED Coun a ® Lagoon 0• Remediation: Infiltration Gallery I Ua-S-pray Field ❑ Remediation: Telephone#: 3 --S330 ❑ Rotary Distributor ❑ Land: Application of Sludge No. of wells to be sampled: ft ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION �e�n , \ WELL ID NUMBER (from Permit): ``\W"___ Date sample collected: U—Q3 - IS FIELD ANALYSES: QQ ' l� DC WAS DRY at Well Depth: .S it Well Diameter: _in. pH aoaao: bnits Temp. 00010: time of Depth to Water Level e264e: _ ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. oaoea: µ Mhos sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor ooae6: O 2_1 check Volume of water pumped/balled before sampling: _ gallons Appearance �(� IQ here: S I f tail were collected unflltered• ❑YES MA ❑ NO and field acidified: ❑ YES NO am es or me LABORATORY INFORMATIONs'U ay'� 1�-3�, �a �.L'�:1 ta�� laboratory Name: 1�rOC�i�Q�yy� Certification No. Date sample analyzed 11 as .,\ PARAMETERS NOTE: Valubs sho Id refl et dls oived and colloidal. concentrations. - COD ooam mg/L Nitrite (NO2) as N aoe15 mg/L Pb -Lead o1ae1 uglL Coliform: MF Fecal 31als Cod , /100mL Nitrate (NO3) as N oaszo 133 mg/L Zn - Zinc 01092 mg/L Conform: MF Total 315o4 (Note: Use MPN method for highly turbid samples) /100ml- Phosphorus: Total as P oases Orthophosphate 70607 mgiL mg/L Other (Specify Compounds and Concentration Units): )Issolved Solids:Total 70300 a o 3 mg/L Al -Aluminum o11o6 mglL pH (Lab) amm un Be - Barium 01007 uglL TOC ooeeo mNEW lum 00816 mglL lum 01027 - Chloride poeao �o m!1�t9�(,� g� Arsenic 01002 se and Oils 00552 Greaak . — ug/L ) C um: Total 01024 Iv-' ' o � �� -Copper 01oaz _ �, ANICS: (by GC, GC/MS, HPLC) m91 � iL- 8 2 pectfy test and method #. ATTACH LAB REPORT.) Phenol 32730 ft _ Fe - Iron 01046 iqWSulfate mg/L rcury 71800 � SECTI(4i b Report Attached? ❑ Yes (1) ❑ No (0) a0946 _ pacific Conductance 000es µMhos K - Potassium 00937 ,InlGnenentti ,method # 10WOCIMONT - ; method # Total Ammonia ooelo G 0 . � m /L Mg - Magnesium ooe27 g mg/L method # (Ammonia Nitrogen; NH30e N; Ammonle Nitrogen, Total) Mn - Manganese o1056 uglL _ -- method # TKN as N 00626 mg/L Ni - Nickel 01087 uglL , mg1L VOC Removal%, For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mglL Effluent Total VOCs: r Bd Agent) Name ana t me - rierino plea U, %TVW Rev.8/2013rLQ��� SUBMIT FORM ON PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if different): (Street) act Person: Q Location/Site Name k or County Telephone#: 11 01J3 No. of wells to be sampled: PERMIT Number: Date: Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED 9—Moon ❑ Remediation: Infiltration Gallery (I -Stray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: If 0 SAMPLING INFORMATION ,, �`` Date sample collected: �'" J S W''" FIELD ANALYSES: q r� WAS DRY WELL ID NUMBER (from ermit): �� Well Diameter: in. � q pH ooaoo:, l � units Temp. 000lo: (r I °C at Well Depth: "L._ft• Depth to Water Level e2546: (�_ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 000m: check Volume of water pumped/bailed before sampling: S gallons ..,� Appearance here:❑ Samples for metals were collected unfiltered: ElYES ElNO and field acidified: ❑ YES IIQ NO LABORATORY INFORMATION �1 I j lq-%�o atory Name: fy 1 �O�II`fi,(tL I Certification No. Date sample analyzed: R- 3 �-a a - l� PARAMETERS NOTE: Valdes sho Id refl ct dissolved and colloidal concentrations. Pb - Lead wo51 ug1L COD 00335' mg/L Nitrite (NO2) as N oos15 mg/L Coliform: MF Fecal 31616 G C p /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L Other (Specify Compounds and Concentration Units): (Note; Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L issolved Solids:Total 70300 p mg/L All - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 u91L TOC 00680 mg/L Ca - Calcium oo91s mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug1L Chromium: Total 01034 ug/L mg/L ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils 00552 mg/L Cu - Copper 01042 ug/L (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 ug/L mg/L Fe - Iron 01045 Hg - Mercury 71900 uglL Lab Report Attached? ❑ Yes (1) ❑ No (0) Sulfate 00945 pecific Conductance 000m µMhos K - Potassium 00937 mg/L VOC 7e73 method # method # Total Ammonia ooslo C. mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese o1 o55 ug/L ,method # TKN as N 00525 mg/L Ni - Nickel 01067 uglL method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCS: • mg/L MR ME HIRMP, Effluent Total VOCs: • • ■ • • • mg/L• • VOC Removal% •. IN �1 e 1 a (Date) _/ Permitte o Authorize Agent) Name and Title - Please print or type Signature of Pe or Authorized Agent) GW-59 Rev. 812013 ( �C/`^� Y v t-UKM UN YtLLUW FAK--K TER QUALITY MONITORING: E REPORT FORM t Facility Name: " Permit Name (if different): Fa cHit Address: _sL , Ma d`� (city) Contact Person: 0.\ Well Location/Site Name arerrrr.nvv u�rvcnnrw'� WELL ID NUMBER (from Permit): �w� J Well Depth: fLS__ft. Depth to Water Level e2546:1),f) _ft. below measuring point Measuring Point is 3 ft. above land surfaces Volume of water pumped/bailed before sampling: Samples for metals were collected unfiltered: ❑ YES . ❑ sample COD oo335 mg/L Coliform: MF Fecal 31616 CO /100mL Coliform: MF Total 31604 /100mL (Note: Use MPN method for highly turbid samples) (solved Solids:Total 70300 ' p�-� mg/L pH (Lab) 00403 units TOC ooeso mg/L Chloride ooeso < S mg/L Arsenic 01002 ug/L Grease and. Oils 00652 mg/L Phenol 32730 ug/L Sulfate 00945 mg/L ecific Conductance 000ss µMhos Total Ammonia ooeso O-mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen; Total) TKN as N 00625 mg/L For Remediation Systems Only (Attach Lab Reports): 'Pe PERMIT Number: Wk�UU&PfW.Expiration Date: - 1 W— ; j / — a(U 4 Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED CountyL Lagoon ❑ Remediation: Infiltration Gallery L—pray Field ❑ Remediation: Telephone#: _Ll— ag 3 '—' 57330 ❑ RotaryDistributor ❑ Land Application of Sludge No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other. Date sample collected: It� oC3 Well Diameter: in. Screened interval: ft. to ft. Relative M.P. Elevation: ft. gallons NO and field acidified: ❑ YES ' Laboratory Name: LAJ and colloidal concentrations. Nitrite (NO2) as N 00615 mg/L Nitrate (NO3) as N ooeso C) mg/L Phosphorus: Total as P ooess mg/L Orthophosphate 70507 mg/L. Al -Aluminum o11os mg/L Ba - Barium 01007 uglL Ca - Calcium 00916 mg/L Cd - Cadmium 01027 uglL Chromium: Total 01034 ug/L Cu - Copper 01042 _ mg/L Fe - Iron 01045 ug/L Hg - Mercury 71900 ug/L K - Potassium 00937 mg/L Mg - Magnesium oos27 mg/L Mn- Manganese o1o55 ug/L Ni - Nickel 01067 ug/L FIELD ANALYSES: jp nn pH 00400:�8units Temp. 000l0: ! 8t dam.°C Spec. Cond. 00094: µMhos Odor owas: Appearance Certification No. R Pb - Lead most ug/L. Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC; GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 , method # method # method # method # innuent i utai vvVa. +nyl� ­.1.. -"-- ' ---- DRY at time of sampling, mg/L VOC Removal% methods of analysis by a la - au -fs El ad Aqent) Narne and'Title Please print 8r type Rev. 8/2013 • -" SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: /� �� la � ,'r, '�� , � L's� +� �< s � `• � 1` I`,'YY �'r'jl ��� ; 1 COMPLIANCE REPORT FORM FACILITY INFORMATION Please PrinYclearly orType ` PERMIT Number'. � $� Expiration Date: Facility Name: � O X� �� �� a.�r �� L1S `(� Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: er O TYPE OF PERMITTED OPERATION BEING MONITORED ( o. �\ (Streeq 3 � 1 County l Tragoon ❑. Remediation: Infiltration Gallery (Ci ) I'Swe) (zip) &I -Spray Field ❑ Remediation: " 1 Telephone#: \d`��e�''s ❑ Rotary Distributor El Land Application of Sludge Contact Person: C Well Location/Site Name R No. of wells to be sampled: 1� _ ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION �n , r� y Date sample collected: I �T o�3 ~"F FIELD ANALYSES: IT wtLL WAS WELL ID NUMBER (from PPermit): \� -" ft. Well Diameter: � in. pH oo4oa-S. units Temp. 00010: • S -C DRY at Well Depth: o(S Depth to Water Level e2sas: , ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. o0094:, µMhos time of sampling,. Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor ooses: Appearance CRC' check here:0 Volume of water pumped/balled before sampling: gallons Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑YES O LABORATORY INFORMATION /� a 0 f I \a 111, `a t_1sLaboratoryName: 1�\ %J Certification No. Date sample analyzed: 3 PARAMETERS NOTE: ValLks should re ect dissolved and colloidal concentrations. N mg/L Pb - Lead most ug/L COD ao335 mg/L Nitrite (NO2) as ooele Coliform: MF Fecal 31616 S (\ 1141 w /100ml- Nitrate (NO3) as N ooma Q 13 mg/L Zn -- Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as'P 00865 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 l 6 % mg/L Al -Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC ooseo mg/L Ca - Calcium ooses mg/L Chloride 00940 Jr mg/L Cd - Cadmium 01027 ug1L Arsenic 01002 ug/L Chromium: Total 01034 ug/L mg/L ORGANICS: (by GC, GC/MS, HPLC) Grease and Oils 00552 mg/L Cu- Copper 01042 Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Phenol 32730 ug/L mg/L Hg - Mercury 71800 ug1L Lab Report Attached? ❑ Yes (1) ❑ No (0) Sulfate 00945 µMhos K - Potassium 00937 mg/L VOC 7e73 , method # pecific Conductance ooses Total Ammonia ooslo C7 . mg/L Mg - Magnesium 0o927 mg/L , method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese oloes ug/L method # a • 1-certify That, to the best of my knowledge and belief, the informal on•submitted in this report is trice, accur DWR=certified laboratory. I am aware that there are�•significant penalties [Or submitting false information, Permittee Qr A (horized Agent) Name and Title -please print or type GW--Rev. 8/2013 Eq; (til°.1�(� mg/L Effluent Total VOCs: mg/L VOC Removal% methodsa, and - cbmplete, and that tile laboratory analytical data was prodLiCed Using approved of analysis by a ClUding thep of fines and imprisonment. •. . 7 1 a — &� s Signature4Peeer Authorized Agent) (Date) `0cN I - ) S �e \ was too c�,1 (o o "L d- was t 5a l� or, is "Tt St tS ere e 1 co 111 a o'L. .,......... .... .........,-._.._ _.._.._-..._...,__......... ....... _.._ ,._._..a..._._._.....,...,_.,�,:......._M:..,_.,._ �__...._._......... ... -..._.._..........._....._......,_.............. ........ _ __._......_................. SUBMIT FORM ON YELLO PAPER ONLY TER QUALITY MONITORING: E REPORT FORM FACILITY INFORMATION ---���Please Pdnt Clead ZpqPERMIT Number: MM_3 �"�$)Explratlon Date: Faclllty Name: OX�C2� �z �l� � S h Non-Discharge. UIC ermit Name (if different): Perms P (if NPDES Other - @C TYPE OF PERMITTED OPERATION BEING MONITORED Add Facillt(srreeq G County M [y'Cagoon ❑ Remediation: infiltration Gallery I—Fily) __(scare) (Zip) Q �� 1J f$i\\Lt Telephone#,%(�— of S _—S_13 (3 L9'§pray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge Contact Person: � No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: Well Location/Site Name _ tram armll If WELL SAMPLING INFORMATION �\ Date sample collected: — FIELD ANALYSES: WAS WELL ID NUMBER (from Permit): ��\W�` Rb ft. Well Diameter. in. Q pH aoao0-5-y-1 units Temp. 0oolo: p °C DRY at Well Depth: Depth to Water Level e264eft. below measuring point Screened Interval: ft. to ft. Spec. Cond. aoaea: µMhos slamf Ing, p Measuring Point Is S ft. above land surface Relative, M.P. Elevation: ft. Odor ooae6: check Volume of before sampling: a 0 gallons Appearance here: water pumped/bailed Samples for metals were collected unfiltered: ❑ YES N A ❑ NO and field acidified: ❑ YES 92rN0 LABORATORY INFORMATION /--�� \ Date sample analyzed: , -� ' 1 — Laboratory Name: erw �O�erc�\ Certification No. O� ■APAMPTGslA INInTIF!VaIdamshdLildreflifetdisselved and cellbidal concentrations. COD 00335 mg/L Collform: MF Fecal 31616 /100ml_ Coliform: MF Total 31604 /100mL (Note: Use MPN method for highly turbidsamples) isolved Solids:Total 7osoo , \ d� mg/L pH (Lab) 00403 units TOC ooeso mg/L Chloride 00940 0 _ mg1L Arsenic 01002 ug1L Grease and Oils 00562 mg/L Phenol 32730 uglL Sulfate 00946 mg/L lecific Conductance o0096 µMhos Total Ammonia ooelo mg/L (Ammonle Nitrogen; NH3 as N; Ammonle Nltmgen, Total) TKN as N 00026 mg/L For Remedlation Systems Only (Attach Lab Reports): Nitrite (NO2) as N ooels mg/L Pb- Lead o1o61 ug/L Nitrate (NO3) as N oos2o , S mg/L Zn Zinc 01092 mg/L Phosphorus: Total nrthnnhnsnl .�` Compounds and Concentration Units): All - Alumii Ba - Ba Ca - Cak Cd - Cadn Chromium: I Cu - Co Fe - Hg - Met K - Potasi Mg - Magne Mn - Mangal NI-N Influent Total (o Authorized Aaentl Name and Tille - Please print or type GW-69 Rev.8/2013 method #. ATTACH LAB REPORT.) hed? ❑ Yes (1) ❑ No (0) method # method # method # method # mg/L VOC Removal% CNIIIIF« SUE ON YELLOW PAPER ONLY WOUNDWATER QUALITY MONITORING: :OMPLIANCE REPORT FORM ACILITY INFORMATION ( T Please PdntCle yor e scillty Name: k-� Cam+ oz - ermit Name (if different): act Person: Location/Site PLING INFORMATION M L ID NUMBER (from Permit): `"� — Depth: ft. h to Water Level ezeae: 8,� ft. below measuring point luring Point is a ft. above land surface me of water pumped/bailed before sampling•. _�Q oles for metals were collected unfiltered: [� YES ❑ l3,1) 15 - COD ooms mg/L Collform: MF Fecal we1e �1, /100ml- Coliform: MF Total 31604 /100mL (Note: Use MPN method far highly turbld sempies) lssolved Solids:Total 7o3ao 1)9 mg/L pH (Lab) 00403 units TOC noeeo mg/L Chloride ooeao mg/L Arsenic 01002 uglL Grease and Oils 00652 mg/L Phenol 3273o ug1L . Sulfate 00945 mg/L 'pecific Conductance 00098 = µMhos Total Ammonia oaelo 0. m91L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Toteq TKN as N 00826 _ mg/L For Remediation Systems Only (Attach Lab Reports): County ,No. of wells to be sampled: Number:kjRWSjj!9'1 Expiration Date: Non -Discharge UIC NPDES Other TYPE OF PERMITTED. OPERATION BEING MONITORED M'Cagoon ❑ Remediation: Infiltration Gallery M-76pray Field ❑ Remediatlon: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample collected: ' i _ C — I s Well Diameter. _2L_ In. Screened Interval: ft. to ft. Relative-M.P. Elevation: fL gallons field Laboratory Name: C-)[\y\ \ ouryc, and colloidal concentrations. Nitrite (NO2) as N ooele mg/L Nitrate (NO3) as N ooe2o a mg/L Phosphorus: Total as P cases mg1L Orthophosphate 701107 mgn- AI -Aluminum o11oe mg/L Be - Barium 01007 uglL Ca - Calcium 00e1a mg/L Cd - Cadmium 01027 ug/L Chromium: Total 01034 ug1L Cu - Copper 01042 mg1L Fe - Iron 010411 ug1L Hg - Mercury 71soo ug/L K - Potassium 00937 mg1L Mg - Magnesium oos27 mg/L Mn - Manganese olaas uglL NI - Nickel 010e7 ug1L Influent Total VOCs: FIELD ANALYSES: WAS pH 00400:,S0 units Temp. aomo: aC DRY at Spec. Cond. oaaea: µMhos time of sampling, Odor ooaae: check Appearance G eR (^ here: Certification No. Pb - Lead most ug1L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7e73 ,, method # method # method # method # Effluent Total VOC6: mg1L VOC Removal% _14- ad Anent) Name and Title - Please print or type Rev. 812013 D q� c%e r- � v SUBMIT FORM __,___..�_...._.......................... ..._... ___..._.......__... ___._._ ONLY ONLY TER QUALITY MONITORING: E REPORT FORM Facility Name: Permit Name (if different): act Person: VS0, Location/Site Name County Telephone#:'W� - a 3 — No, of wells to be sampled:. W lRMIT Number:,A1j003 kk9$tl Expiration Date: V d- S i- ;AC n-Discharge UIC 'DES Other Es F PERMITTED OPERATION BEING MONITORED agoon ❑• Remediation: Infiltration Gallery pray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION 2 WELL ID NUMBER (from Permit):J , C Date sample collected: N FIELD ANALYSES: „ ..--- WAS Sft. Well Diameter: In. pH oa400S►3Sunits Temp. oowo: 11, S eC at Well Depth: Depth to Water Level e2s4e: ft. below measuring point _ Screened Interval: ft. to ft. Spec. Cond. 00004'. µMhos tDRY ime of sampling, Measuring Point is ft. above land surface Relative-M.P. Elevation: ft. Odor aloes: J)i 011Q , check Volume of water pumped/balled before sampling: ao gallons Appearance on here:a Camniae fnr mafatc warn collected unfiltered: ❑ YES Al -A ❑ NO and field acidified: ❑ YES [60 _ Date sample an PARAMETERS COD oa33e mg/L Collform: MF Fecal 31sie /100mL Collform: MF Total 31504 /100mL (Note: Use MPN method forhlghiy turbid.9almples) 0 Iissoived Solids:Total 703oo 10 , mg/L pH (Lab) 00403 units TOC ooseo mg/L Chloride 00e40 mg/L Arsenic 01002 ug1L Grease and Oils 00662 mg/L Phenol 3273o ug/L Sulfate 00945 mg/L Specific Conductance oDoss µMhos Total Ammonia oama G �j a mg/L (AmmoNa Nitrogen; 'NH3 as N; Ammonia Nlb09en,101e11 TKN as N 00e25 - mg/L For Remediation Systems Only (Attach Lab Reports): P-2..diiii JS Laboratory Name: 'G l U l I OCiYW,rY� and colloidal concentrations. Nitrite (NO2) as N ooeis mg/L Nitrate (NO3) as N oas2o \ mg/L Phosphorus: Total as P oases mg/L Orthophosphate 70607 mg/L Al -Aluminum o11os mglL Be - Barium 01007 uglL Ca - Calcium aoeie mg/L Cd - Cadmium 01027 uglL Chromium: Total 01034 uglL Cu - Copper 01042 mg/L Fe - Iron 01046 ug/L Hg - Mercury 71900 ug1L K - Potassium 00937 mg/L Mg - Magnesium oo927 mg/L Mn - Manganese aloes ug1L NI - Nickel oias7 ug1L Certification No. Pb Lead 010s1 uglL Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (byGC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab ReportAttached? ❑ Yes (1) ❑ No (0) VOC 7e73 method # method # method # method # Influent Total VOCs: mg1L Effluent Total VOC.s: mg/L VOC Removal% Rev. 812013 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER_ QUALITY MONITORING: COMPLIANCE REPORT FORM Name: Name (If 9ct Person: Location/Slte Name )IATION (from Permit): — Depth: QL 5ft- 1 to Water Level e264e: R,`l ft. below measuring point Luring Point is Zft. above land surface ne of water pumped/bailed before sampling: aO for COD oo336 mg/L Coliform: MF Fecal 31816 /100mL Collform: MF Total 31604 /100mL (Note: Use MPNmethod for highly turbid samples) ;solved Solids:Total 70306 of O mg/L pH (Lab) 00403 units TOC oosso mg/L Chloride aa940 mg/L Arsenic 01002 uglL Grease and Oils ooae2 mg/L Phenol 32730 ug1L Sulfate 00945 mg/L tecific Conductance-=95 µMhos Total Ammonia oaelo-p, ra. mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Tatal) TKN as N 00026 mg/L For Remediation Systems Only (Attach Lab Reports): N - Ili t d flits Please print or I YES NO - t 5— ( S LaboratoryName: t--I \ t l QkL4 W4 ` and colloidal concentrations. Nitrite (NO2) as N ooe16 mg/L Nitrate (NO3) as N 00e20mg/L Phosphorus: Total as P ooes5„ mg/L County No. of wells to be sampled: PERMIT Number:VA043`t`1F3'Expiration Date: Vck- tsl- c101 Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED tMagoon ❑• Remediation: Infiltration Gallery t3"9p-ray Field ❑ Remediation: Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample collected: b Well Diameter: in. Screened Interval: ft. to ft. Relative-M.P. Elevation: ft. U` Orthophosphate 70607 mg/L AI -Aluminum o11o5 mg/L Be - Barium 01007 _ ug1L Ca - Calcium 0091e mg/L Cd - Cadmium 01027 ug1L Chromium: Total 01034 ug1L Cu - Copper 01042 mg/L Fe - Iron 01046 uglL Hg - Mercury 71900 ug1L K - Potassium 00937 - mg/L Mg - Magnesium oo927 mg/L Mn- Manganese 01065 ug& NI - Nickel 01067 uglL FIELD ANALYSES: p� pH ooaoo4� units Temp. 00010: �°C Spec. Cond. 00084: µMhos Odor 0ooe5: �0 Appearance Q � Certification No. Pb - Lead o1os1 'uglL Zn - Zinc o1092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ yes(l) ❑ No(0) VOC 7873 , method # method # method # method # Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC DRY at time of —,1+ — ❑� GW-59 Rev.81201 auotvu t runivl UN Ttt_LUW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Name: Name (If act Person: *k\C( Location/Site Name County Telephone#: `Nit - 41 "� — No. of wells to be sampled:. PERMIT Number:%04%%!3 "%q Expiration Date: Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED Ltt'Lagoon ❑• Remediation: Infiltration Gallery ®-Sp'ray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other. WELL ID NUMBER (from Permit): Date sample collected: 3 �" i i '� t S Well Depth: S ft. I g,'7� of �1z o Well Diameter. o` in. Depth to Water Level e2546: %a fL below measuring point Screened Interval: ft. to ft. Measuring Point is S ft. above land surface Relative M.P. Elevation: ft. Volume of water pumped/bailed before sampling: 1 j gallons ,Samples for metals were collected unfiltered: ❑ YES A ❑ NO and field acidified: ❑ YES M-90 sample analyzed: 1 1 .2 - I a,34 c3,19 k3' COD 00335 mg/L Collform: MF Fecal 31616 G GS . /100ml- Coliform: MF Total 31504 1100ml- (Note: Use MPN method for highly turbidsamples) solved Solids:Total 70300 mg/L pH (Lab) 00403 units TOC oosso mg/L Chloride 00940 �� mg/L Arsenic 01002 uglL Grease and Oils 00562 mg/L Phenol 32730 ug/L Sulfate 0094s mg/L 3cific Conductance 000gs µMhos Total Ammonia 0oslo Q, mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total TKN as N 0os2s mg/L P'i s Laboratory Name: _ E_C\y '� M (Y� II and colloidal concentrations. Njtrite,(NO2);as_N.00el6 mg/L trate (NO3) as N oos2o Phosphorus: Total`as P=ooass a- - _, _. mg/L Orthophosphate 70507 » '~ mg/L Al - Aluminum oil os mg/L Be - Barium 01007 uglL Ca - Calcium 009is mg/L Cd - Cadmium 01027 ug/L Chromium: Total 01034 ug/L Cu - Copper 01042 mg/L Fe - Iron 01046 _ ug/L Hg - Mercury 71900 ug/L K - Potassium 00e37 mg/L Mg - Magnesium oo927 mg/L Mn - Manganese oioss ug/L Ni - Nickel 01087 ug/L FIELD ANALYSES: WAS pH 00400: S units �," Temp. 000io: 17, ply°C DRY at Spec. Cond. 00004: µMhos time of Odor 0ooss: sampling, check Appearance C, eCt C` here: El Certification No. Pb - Lead olosi ug/L Zn - Zinc 01092 mg/L Cj nd Concentration Units): waterQuaft Reabnal Ppeiaffans.,Secgon �` - t.. i ag ona ®ffics ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 , method # method # method # method # For Remedlatlon Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% SUBMIT FORM ON PAPER ONLY TER QUALITY MONITORING: E REPORT FORM Name: Name (if act Person: Location/Site Name County Telephone#: Mk) -C1 13 - ,- No. of wells to be sampled: PERMIT Number:M%N4ti%rfxpiration Date: on -Discharge UIC PDES Other YPE OF PERMITTED OPERATION BEING MONITORED n- goon ❑ Remediation: Infiltration Gallery B-9pray Field ❑ Remediation: ❑ Rotary Distributor El Land Application of Sludge ❑ Water Source Heat Pump ❑ Other. L ID N INFORMATION M L ID NUMBER (from Permit): \``��' Date sample collected: 3 l — (S FIELD ANALYSES: Temp. 00010: I S aC WAS DRY at Depth: �ft. C2/ OF HL 0� Well Diameter: in. pH o0400S. units time of 1 to Water Level 82546:_ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: µ Mhos sampling, wring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: `ii check ne of water pumped/bailed before sampling: gallons ©' 1EK0 Appearance a xr" here:❑ pies for metals were collected unfiltered: ElYES ❑ NO and field acidified: ❑ YES ORATORY INFORMATION sample analyzed:3,(1►3-( _ j -����5 � Laboratory Name: C,�1�SS C�j�@.(� Certification No. C� 1+ .—�— � AIIIIGTL'13Q mATC�cKni1tri rP_fiP_C1' efiannived and colloidal concentrations. COD 00335 mg/L Coliform: MF Fecal 3161e f# CA /100mL Coliform: MF Total 31504 /100mL (Note: Use MPN method far highly turbid samples) lissolved Solids:Total 70300 M mg/L pH(Lab) 00403 units TOC ooem mg/L Chloride 00940 l 4 mg/L Arsenic olom ug1L Grease and Oils 0o552 mg/L Phenol 32730 ug/L Sulfate 00945 mg/L ipecific Conductance 00095 µMhos Total Ammonia ooalo L Q , mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) TKN as,N 00625 mg/L For Remedlation Systems Only (Attach Lab Reports): - i7ertify 1117t, to the best or my signicicant penalties o - .... `.r(� Permitte o uthorized Agent) Name and Title -Please print or We GW-59 Rev.812013 Nitrite (NO2) as N o0915 mg/L Pb - Lead moss ug/L Nitrate (NO3) as N 00620 Q ` mg/L Zn - Zinc 01092 mg/L Phosphorus: Total as P 008e5 mg/L Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Al -Aluminum o1105 mg/L Be - Barium 01007 ug/L Ca - Calcium 0091e mg/L Cd - Cadmium 01027 ug/L Chromium: Total 01034 ug/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) K - Potassium 00937 mg/L VOC 7e73 , method # Mg - Magnesium oo927 mg/L method # Mn - Manganese olo55 ug/L method # Ni - Nickel 01067 ug/L , method # Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% -/C-l5 'R QUALITY MONITORING: REPORT FORM Name: Name (if act Person: C Location/Site Name SUBMIT FORM ON YELLOW PAPER ONLY • v It I, Vls JN w• or Type PERMIT Number: n4jg) Expiration Date: Non -Discharge UIC INPDES Other Telephone#:��0�' No. of wells to be sampled: PE OF PERMITTED OPERATION BEING MONITORED P-Cagoon ❑• Remediation: Infiltration Gallery 2-Way Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION \\`` WELL ID NUMBER (from Permit): w" Date sample collected: l l S FIELD ANALYSES: ooaooS Qnits Temp. aoo�o: �C WAS DRY at Well Depth: 0 s ft: - (f 9, 9 ' o /= HZ 6) Well Diameter: �_ in. pH µMhos time of Depth to Water Level e2e48: g. ft. below measuring point Screened Interval: ft to ft. Spec. Cond. oaoea: sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft Odor aoom: 2. Appearance QatC- check here, Volume of water pumped/bailed before sampling:_gallons Et Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES -N6 Date sample analyzed_ PARAMETERS NOTE: Vt COD 00335 mg/L Coliform: MF Fecal 31616 L /100mI_ Coliform: MF Total 31804 /100mL (Note: Use MPN method for highly turbid samples) isolved Solids:Total 70300 mg/L pH (Lab) 00403 units TOC aoseo mg/L Chloride 00e40 < s _ mg/L Arsenic 01002 ug/L Grease and 011s 005e2 mg/L Phenol 32730 ug/L Sulfate 00945 mg/L iecific Conductance a -pass. µMhos Total Ammonia ooelo < O, mg/L (Ammonia Nitrogen; NH3 as N; Ammonla Nitrogen,Total): TKN as N 00626 mg/L For Remediation Systems Only (Attach Lab Reports): L-IS Laboratory Name:y\ I and colloidal concentrations. Nitrite (NO2) as N oos16 mg/L Nitrate (NO3) as N 00820 mg/L Phosphorus: Total as P oases mg/L Orthophosphate 70e07 . mg/L Al -Aluminum o11os mg/L Be - Barium 01007 uglL Ca - Calcium ooele mg/L Cd - Cadmium olo27 uglL Chromium: Total MOM uglL Cu - Copper 01042 mg/L Fe - Iron oloas ug/L. Hg - Mercury 71900 ug/L K - Potassium 00937 mg/L Mg - Magnesium ooe27 mgiL Mn - Manganese oloes ugn- Ni - Nickel 01087 ug1L Certification No. Pb - Lead o1o61 ug/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7e73 method # method # method # method # Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% _/4; GW-69 Rev.812013 FORM ON YELLOW PAPER ONLY QUALITY MONITORING: PORT FORM Facility Name: Permit Name (if act Person: Location/Site Telephone#:010' M3—,S3&) A-99o. of wells to be sampled: PERMIT Number:(Wd3-tjtfi Expiration Date: t d" ;5 1 - d,u Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED OR -Lagoon ❑ Remediation: Infiltration Gallery Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other. PILING INFORMATiUN L ID NUMBER (from Permit): "" Date sample,collected: �i'- 1 �- is Depth: ft. C % , g r 0 f-�� o� Well Diameter: ' in. i to Water Level e2646.__ ft. below measuring point Screened Interval: ft. to ft. luring Point is 3 ft. above land surface Relative M.P. Elevation: ft. ne of water pumped/bailed before sampling: �_ gallons oles for metals were collected unfiltered: ❑ YES NA ❑ NO and field acidified: ❑ YES V(4O -16, 3- COD amm mg/L Coliform: MF Fecal 31616 t C61, /100ml- Coliform: MF Total 31604 /100mL (Note: Use MPN method for highly turbidsamples) (solved Solids:Total 70300_ mg/L pH (Lab) 00403 units TOC ooeso mg/L Chloride 00940 Lf q. mg/L Arsenic olom ug/L Grease and Oils 0osm mg/L Phenol 3273o uglL Sulfate 00945 mg/L iecific Conductance 000es µMhos Total Ammonia ooeso < Q , mg/L (Ammonia Nitrogen; NH3 as N, Ammonia Nitrogen, Total) TKN as N oo626 mg/L For Remediation Systems (Attach Lab Reports): FIELD ANALYSES: pH 00400. %(:2&nits Spec. Cond. 00004: Odor 000es: `-1111,6-Y1e� check Appearance q r-^ here: Temp. 000% (S. 6 °C DRY at µMhos time of -- c�mnlin =►s Laboratory Name: &0 r-oefneaf N� Certification No. and colloidal concentrations. Nitrit"NOAcas=N-o Gm-- - mg/L Pb - Lead of osi ug/L itrate (NO3) as N oos2a 2LQ mg Zn - Zinc 01092 mg/L Phosphorus: TotirdWP>-aoes6- _ _ _ m8T /L D Orthophosphate 70.607 M" Tn9/L Other (Specify Compounds and Concentration Units): Al -Aluminum 01105 mg/L Be - Barium 01007 ug1L Ca - Calcium aosle mg/L Cd - Cadmium 01027 uglL Chromium: Total MOM uglL Cu- Copper 01042 mg/L Fe - Iron 01045 uglL Hg - Mercury 71900 ug1L K - Potassium 00e37 mg/L Mg - Magnesium ao927 mg/L Mn - Manganese al ass ug/L N1- Nickel 01087 uglL ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑' No (0) VOC 7873 , method # - method # method # method # Influent Total VOCs: mg/L Effluent Total VOCs: VOC Removal% ad Agent) Name Rev. 812013 and Title - Please print or type www.encolabs.com ANALYTICAL RESULTS scriptiont 141666-10 MW-8 Lab Sample ID:CSO0133-10 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12131/14 13:03 Work Order: C500133 Projeck: Genral Subcontract Sampled'.By:CLIENT IV+ Iatile Organic Compounds by GCMS • ^ - ENC.O Cary cert/fied analyfe (NC 591] Analyte FCAS Number] Results Flag Units DF MDL POL Batch Method Analyzed Ay Notes 1,1,1,2 7etrachloroethane[630-20-6]^ < 0.091 ug/L 1 0.091 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:17 MSZ 1,1,1-Trichloroethane [71-55-6]1 < 0.15 ug/L 1 D.15 0.50 5AO8010 EPA 82606/62301) 01/08/15 14:17 MSZ 1,1,2,2-Tetrachicroethane [79-34-5]^ < 0.085 ug/L 1 0.085 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:17 MSZ 1,1,2=rrichloroethane(79-00-5]^ < 0.068 ug/L 1 0.068 0.50 5A08010 EPA 82606/6230D 01/08/15-14:17 h1Sz 1,1-Dichloroelhane(75-34-3]^ < 0.050 ug/L 1 0.050 0.50 5AO8010 EPA 8260B16230D 01/08/15 14:17 M57. 1,1-1)ichloroethene[75-35.4]^ < 0.15 ug/L 1 0.15 0.50 SA08010 EPA 82608/6230D 01/08/15 14:17 MSZ 1,1-Dichloropropene[563-58-6]'• < 0.063 ug/L 1 0.063 0.50 5AO8010 EPA 826013/6230D 01/08/15 14:17 MSZ 1,2,3-Tr61orobenzene [87-61-6]A < 0.25 ug/L 1 0.25 0.50 SA08010 EPA 826013/62301) 01/08/15 14:17 MSZ 1,2,3-Tiichloropropane(96-18-4]^ < 0.15 ug/L 1 0.15 0.50' 5AO8010 EPA 8260B/6230D 01/08/15 14:17 MSZ 1,2,4-Trichlorobenzene [120-82-1]^ < 0.097 ug/L 1 0.097 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:17 MSZ 1,2,4-Tr imethylbenzene[95-63-6]^' < 0.067 ug/L 1 0.067 0.50, 5AO8010 EPA 82608/62301) 01/08/15 14:17 MSZ 1,2-Dibromo-3-chioropropane [96-12-8]^ . < 0.48 ug/L 1 0.48 0.50 5A08010 EPA 8260B/6230D 01/08/15 14:17 MSZ 1,2-Dibromoethane [106-93-4]1, < 0.27 ug/L 1 0.27 0.50 SA08010 EPA 8260B/6230D 01/08/15 14:17 MS7. 1,2-Dichlorohenzene [95-50-1]^ < 0.062 ug/L 1 0.062 0.50 5AO8010 EPA 826013/62301) 01/08/I5 14:17 MSZ 1,2-D161oroethane(107-06-2]^ < 0.082 ug/L 1 0.082 0.50 5A08010 EPA 826013/62301) 01/08/15 14:17 MSZ 1,2-Diciloropropane[78-87-S]^ < 0.098 ug/L 1 0.098 0.50 5AO8010 EPA 82606/62301) 01/08/15 14:17 MSZ 1.3,S-Trimethylbenzene[108-67-8]^ < 0.10 ug/L 1 0.10 0.50 5AO8010 EPA 82608/6230D O1!08/1S 14:17 MSZ 1,3-Dichlorobenzene[541-73-1]^ < 0.092 ug/L 1 0.092 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:17 MSZ 1,3-Dichloropropane[142-28-9]1, < 0.15 ug/L 1 0.15 0.50 .5A08010 EPA 8260B/6230D 01/08/15 14:17 MR, 1,4-Dictilorobenzene [106-46-7]^ < 0.10 ug/L 1 0.10 0.50 5A08010 EPA 8260B/6230D 01/08/15 14:17 MSZ 2,2-Dichloropropane [594-20-7]^ < 0.12 ug/L 1 0.12 0.50 5A08010 EPA 82608/6230D 01/08/15 14:17 MSZ 2-Chlorotoluene[95-49-B]^' < 0.10 ug/L 1 0.10 0:50' 5A08010 EPA 82608/6230D 01/08/15 14:17 MSZ 4-Chlorbtoluene[106-43.4]^ < 0.10 ug/L 1 0.10 0.50 5A08010 EPA 8260B/6230D 01/08/15 14:17 MSZ 4-Isopropyltoluene199-87 61^- < 0.066 ug/L 1 0.06.6 0.50 5A08010 EPA 82608/6230D 01/08/15 14:17 MSZ Benzene[71-43-2]^ < 0.050 ug/L 1 0.050 .0.50 5AO8010 EPA 82606/62301) 01/08j15 14:17 MS7. Bromot�enzene[108-86-1]^ < 0.13 ug/L 1 0.13 0.50 SA08010 EPA 82608/6230D 01/08/15 14:77 MSZ BromoclhIloromethane [74-97-5]^ < 0.11 ug/L 1 0.11 0.50 5AO8010 EPA 82606/6230D 01/08/15 !4:17 MSI. Brom.4chloromethane(75-27-4)^ < 0:010 ug/L 1 0.010 0.50 5AO8010 EPA 82608/62300 01/06/15 14:17 NIS.'- Bromoform [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 SA08010 EPA 8260B/6230D 01/08/15 14:17 r•152 Bromon ethane(74-83-9]^ < 0.28 ug/L 1 0.28 0.50 5AO8010 EPA 8260B16230D 01/08/15 14:17 M57. Carbon Tetrachloride [56-7.3-5]^ < 0.082 ug/L 1 0.082 0.50 SA09010 EPA 8Z60B/6J_30D 01/08/15 14:17 MSZ Chlorotienzene [108-90-7]^ < 0.069_ ug/L 1 . 0.069 '0.50 5A08010 EPA 87.60B/6230D 01/08/15 14:17 1457. Chloroethane[75-00-3]^ < 0.18 ug/L 1 0.18 0.50 5A08010 EPA 8260B16230D 01/08/15 14:17 145Z Chloroform [67-66.3]^ < 0.083 ug/L 1 0.083 0.50 5AO8010 EPA 82608/62301) 01/08/15.11:17 MSZ Chloromethane(74-87-3]^ < 0.050 ug/L 1 0.050 - 0.50 5A08010 EPA 82608/6230D 01/08/15 14:17 MSZ cisrl,J.,Pichloroethene [156-59-2]^ < 0.075 ug/L 1 0.075 0.50 SA08010 EPA 82608/6230D 01/08/15 14:17 h157. . cis-1,3-bichloropropene[10061-01-5]^ < 0.073 ug/L 1 0.073 . 0.50 SA08010 EPA 82608/6230D 01/08/15 14:17 MSZ Dibrombchloromethane (124-48-1]^ < 0.067 ug/L 1 0.067 O.SO SA08010 EPA 82606/6230D 01/08/15 14:17 MS2 Dibromomethane (74-95-3]A < 0.13 " ug/L 1 0.13 0.50 SA08010 EPA 82606/6230D 01/08/15 14:17 MSZ DichImodi0uoromethane(75-71-8]^ < 0.091 ug/L 1 0.091 0.50 5AO8010 EPA 8260B16230D 01/08/15 14:17 M57. Ethylberizene[100-41-4]^ < 0.16 ug/L 1 0.10 0.50 5AO8010 EPA 82608/62301) 01/08/15 14:17 MSZ Hexachlorobutadiene[87-68-3]^ < 0.15 ug/L 1 0.15 0.50 5AO8010 EPA 82606/62301) .01/08/15.14:17 MSZ Isopro�ylEther (108-20-3]^ < 0.20 ug/L 1 0.20 0.50 5A08010 EPA 82.606/6230D 01/08/15 11:17 MR - Isopropylbenzene [98-82-8],^ < 0.13 ug/L 1 0.13 0.50 SA08010 EPA 8260B/6230D 01/08/15 14:17 h1SZ m;p-Xyjenes[108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 -O.SO.,. SA06010 EPA'82608/6230D O1/08/15 14:17 MSZ Methylene Chloride[75-09-2]^ < 0.070 ug/L 1 0.070 0.50 5AO8010 EPA 82608/6230D . 01/08/15 14:17 MS2 Methyl;:tert-Butyl Ether(1634.04-4]^ < 0.12 ug/L 1 0.12 0.50 SA08010 EPA 826013/6230D 01/08/15 14:17 MSZ Naphthalene[91.20-3]^ < 0.086 ug/L 1 0.086 0.50 SA08010 EPA 8260B/6230D 01/08/15 14:17 MSZ FINAL This report relates only to the sample as.raceived by the laboratory, and may only be reproduced in full. "age 22 or 39 www.encolabs.com ANALYTICAL RESULTS --� ;ription: 141660-10 MW-8 Lab Sample ID:C500133-10 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 13:03 Work Order: C500133 Project: Genral Subcontract Sampled By:CLIENT IVolatile Organic Compounds by GCMS 1 ^ - ENCO Cary certified analyte [NC 591] Analvte fCAS Number? n-Butyll,Benzene[104 Sl-8]^ n-PropyBenzene(104-I-8] ^ o-Xylene[95-47-6]A sec-Butylbenzene (135-98-8]1 Styrene [100-42-5]'• tert-Butylbenzene[98 06 6]^ Tetrachloroethene (127-18-4)^ Results < 0.074 < 0.074 < 0.088 < 0.053 < 0.082 < 0.094 < 0.094 Flag Units ug/L ug/L ug/L ug/L ug/L ug/L ug/L DF 1 1 1 1 1 1 1 MDL 0.074 0.073 0.088 0.053 0.082 0.094 0.099 PPOL 0.50 0.50 0.50 0.50 0.50 0.50 0.50 Batch 5A08010 5AO8010 SA08010 5A08010 5AO8010 SA08010 5AO8010 Method EPA 8260B/6230D EPA 8260B/6230D EPA 82608/6230D EPA 82.60B/6230D EPA 8260B/6230D EPA 8260B/6230D EPA 8260B162300 Analyzed 01/08/15 14:17 01/08/15 14:17 O1/08/15 14:17 01/08/15 14:17 01/08/15 14:17 01/08/15 14:17 01/08/15 14:17 1!y Notes MSZ MSZ MSZ MSZ MS;_, MSZ MSZ Toluene [108-88-3]^ trans- l;2-Dichloroethene [156-60-5]^ trans-113-Dichloropropene[10061-02-6]^ < 0.053 < 0.11 < 0.080 ug/L ug/L ug/L 1 1 1 0.053 0.11 0.080 0.50 0.50 0.50 SA08010 SA08010 5AO8010 EPA 82.608/6230D EPA 8260B/6230D EPA 8260B/6230D 01/08/15 14:17 01/08/15 14:17 O1/08/15 14:17 MSZ MSZ MSZ Trchloroethene[79 01 6]^ < 0.13 ug/L 1 0.13 0.50 5AO8010 EPA 8260B/62300 01/08/15 14:17 MSZ Trichlorofluoromethane[75-69-4]^ < 0.15 ug/L 1 0.15 0.50 5A08010 EPA 82.608/6230D 01/08/15 14:17 MSZ Vinyl chloride [75-01-4]^ Xylenes (Total) [L330 20-7]^ < 0.083 < 0.22 ug/L ug/L 1 1 0.083 0.22 0.50 0.50 5AO8010 SA08010 EPA 8260B/6230D EPA 82606/62300 01/08/15 14:17 01/08/15 14:17 MSZ hISZ Surrogates 4-Bromo[luorobenzene Dibronio[luoromethane Toluene d8 I Results 53 52 57 DF I 1 1 Spike Lvl % Re c % Rec Limits Batch 5A08010 5A08010 5A08010 Method EPA 8260BI6230C EPA 8260816230C EPA 8260B16230L Analyzed O1108115 14:17 0110611514:17 01108115 14:17 jgy Notes NsZ A15Z h15Z 53-136 67-129 59-134 106916 105 % 115 % 50.0 50.0 50.0 FINAL Phis report relates only to the sample as received by the laboratory, and may only be reproduced in full. i'a<]e 23 of 39 Description: 141660-11 MW-14 Matrix: Ground Water Project: Genral Subcontract ANALYTICAL RESULTS Lab. Sample ID:C500133-1,1 Sampled:12/31/14 111S Sampled By:CLIENT www.encolabs.com Received: 01/05/15 14:06 Work Order: C500133 V latile Organic Compounds by GCMS ^ - ENCO Cary cer147ed ar a fe [NC 5911 Analyt6 rCAS Numberi Results Flaq Units DF. MDL POLL Batch Method Analyzed Ay Notes 1,1,1,2 Tetrachloroethane [630-20-6]^ < 0.091 ug/L 1 0.091 . 0.50 5A08010 EPA 82.60B/62301) 01/08/15 14:46 MS7 1,1,1-T ichloroethane [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5A08010 EPA 82608/62.30D 01/08/15 14:46 MSZ 1,1,2,2;Tetrachloroethane [79-34 5]^ < 0.085 ug/L 1 0.085 0.50 5A08010 EPA 826013/6230D 01/08/15 14:46 MSZ 1,1,2-Trichloroethane [79-00-5]^ < 0.068 ug%L 1 0.068 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:46 h15Z 1,1-Diclhloroethane [75-34-3]^ < 0.050 ug/L:, 1 0.050 0.50 5A08010 EPA 8260B/6230D 01/08/15 14:46 MSz 1,1-Dichloroethene[75-35-4]^ < 0.15 ug/L 1 0.15 -0.50 5A08010 EPA 8260B/6230D 01/08/15 14:46 MSz 1,1-Dichloropropene[563-58-6]^ < 0.063 ug/L 1 0.063 0.50 5AO8010 EPA 82608/6230D 01/08/15 14:46 MSZ [87-61;6] 1,2,A < 0.25 ug/L 1 0.25 _ 0.50 5A08010 EPA 8260B/6230D 01/08/15 14:46 MS 3,2,3-T ichloropropane (96-18-4]^ < 0.15 ug/L 1 0.15 0.50 5A08010 EPA 8260B/6230D 01/08/15 14:46 MS7 • 1,2,4-T ichlorobenzene [120-82-1]^ < 0.097 ug/L 1 0.097 0.50 5A08010 EPA 8260B/6230D .01/08/15 14:46 MSZ 1,2,4-Timethylbehzene[95-63-6]^ < 0.067 ug/L 1 0.067 0.50 SA08010 EPA 82603/6230D 01/08/15 14:46 MSZ 1,2-1)i4omo-3-chloropropane (96-12-8]^ < 0.48 ug/L 1 0.48 0.50 5A08010 EPA 826013/62301) 01/08/15 14:46 MSz < 0.27 ug/L 1 0.27 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:46 MS7- 1,2-Dibromoethane[106-93-4]^ 1,2-Dic lorobenzene[95;50-1]^. < 0.062 ug/L 1 0.062 0.50 5AO8010 EPA 8260B/62301) - 01/08/1S 14:46 MSZ 1,2-DiclIiloroethane(107-06-2]^ 00.082 ug/L 1 0.082 �0.50 SA08010 EPA 8260B/6230D 01/08/15 14:46 MSZ 1,2-Dichloropropane[78.87-5]A < 0.098 ug/L 1 .0.098 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:46 MSZ 1,3,5- imethylbenzene [108-67-8]A < 0.10 ug/L -1 0.10 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:46 MS7 1,3-Dic ilorobenzene[541-73-1]^ < 0.092 ug/L 1 0.092 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:46 MSz 1,3-Dic iloropropane (142-28.9]A < 0.15 ug/L 1 0.15 0.50 SA08010 EPA 82606/6230D 01/08/15 14:46 MSZ 1,4-Dic il6robenzene[106-46-7]^ 2 0.10 ug/L 1 0.10 0.50 5AO8010 EPA 8260B16230D 01/08/15 14:46 MSZ 7]^ < 0.12 ug/L 1 0.,12 0.50 5AO8010 EPA 8260B/6230D 01/08115 14:46 MS7_ 2,2;Dichloropropane[594-20 < 0.10 ug/L 1. 0.10 0.50 5AO8010 EPA 82608/6230D 01/08/I5 14:46 MSZ 2-Chlor6toluene(95-49-8]^ [106-43.4]^ - < 0.10 ug/L 1 0.10 0.50 5AO8010 EPA 8260816230D 01/08/1S 14:46 MSZ 4-Chloro[oluene 11sop` pyltoluene[99-87-6]^ < 0.066 ug/L Y 0.066 0.50 5A080101 EPA 82608/6230D 01/08J15 14:46 MSZ < 0.050 ug/L 1 0.050 0.50 5A08010 EPA 8260B/6230D 01/08/15 14:46 MSz Benzere [71-43-2]^ • < 0,13 ug/L 1 -0.13 .0.50 5A08010 EPA 8260B/6230D 01/08/15 14:46 MSz BromolbIenzene [108-86-1]^ Bromoc[74-97s5]•• < 0.11 ug/L 1 0.11 0.50 5A08010 EPA 82606/6230D 01/08/15 14:46 h1SZ l+Ihloromethane Bromodichloromethane [75 27-4]^ < 0.010 ug/L 1 - 0.010 0.50 5AO8010 EPA 82608/6230D 01/08/15 14:46 MSZ < 0.20 ug/L 1, 0.20 0.50 SA08010 EPA 8260B/6230D 01/08/15 14:46 MSZ Bromofl�orm [75-25-2]^ Bromohtethane [74-83-9]^ < 0.28 ug/L 1 0.28 0.50 5A08010 EPA. 8260B/6230D 01/08/15 14:46 MSZ CarborTetrachloride[5. 5]^ <.0.082 ug/L 1 0.082 -0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:46 msz i. Chlorobenzene[108-'96-7]^' < 0.069 ug/L 1 0.069 0.50 SA08010 EPA 82606/6230D 01/08/15 14:46 MS7 Chloroethane[75 00 3]^ < 0.18 ug/L 1 0.18 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:46 MSz Chloro orm.'[67-66-3] < 0.083_ ug/L 1 0.083 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:46 MSZ Chloro ethahe[74-87-3]^ < 0.050 ug/L 1 0.050 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:46 MSZ cis-1,2 D,ichlorcethene(156-59-2)^ < 0.075 ug/L 1 0.075 0.50 5AO8010 EPA 8260B16230D 01/08/15 14:46 MSZ cis-1,3 Dichloropropene[10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:46 MSz Dibron ochloromethane[124-.48-1]^ < 0.067 ug/L 1 0.067 0.50 5A08010 EPA 82606/6230D 01/08/15 14:46 MSz Dibro omethare[74-95-3]A < 0.13 ug/L 1 0.13 0.50 SA08010 EPA 8260B/6230D 01/08/15 14:46 MSz DichlolodiFluoromethane[75-71-8]^ < 0.091 ug/L 1 0.091 0.50• 5A08010 EPA 8260B/6230D 01/08/15 14:46 MS7. EthyZnzene(100-41-4]^ < 0.10 ug/L 1 0.10 0.50 5A08010 EPA 8260B/6230D 01/08/15 14:46 h1Sz HexacNlorobutadiene[87-68-31^ < 0.15 ug/L 1 0.15 0.50 SA08010 EPA 8260B/6230D .01/08/15 14:46 hISZ Isopro ,ylEther[108-20.3]^ < 0.20 ug/l. 1 0.20 0.50 SA08010 EPA 8260B/6230D 01/08/15 14:46 Msz Isopro vlbenzene198-82-8]^ < 0.13 ug/L 1 0.13 0.50 5A08010 EPA 82608/6230D 01/08/15 14:++6 MS7 m,p-Xylenes[108-38.3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:46 MSZ Methylene Chloride [75-09-2]^ < 0..18 ug/L 1 0.070 0.50 5A08010 EPA 8260B/62300 01/08/15 14:46 MSZ Methy!-tert-Butyl Ether[1634-04-4]^ < 0.12 ug/L 1 0.12 0.50 5A08010 EPA 82.608/6230D Ol/OS/15 14:46 MSz Napht6alene[91-20-3]^ < 0.086 ug/L 1 0.086 0.50 5A080.10 EPA 8260B/6230D 01/08/I5 14:46 MS7. This report relates only to the sample as received by the laboratory, and may only be reproduced in full. rage 2n of 39 FINAL I I - • i iwzt i www.encolabs.com ANALYTICAL RESULTS Description: 141660-11 MW-14 Lab Sample ID:C500133-11 Received: 01/05/15 14:06 Matrix: Ground Water Sampled;12/31/14 13:15 Work Order: C500133 Project: Genral Subcontract Sampled By:CLIENT latile Organic Compounds by GCMS ^ - £NCO Cary ceRi(ed analyte [NC 591J n-Butyl Benzene [104-51-8]^ n-Prop i Benzene [103-65-1]^ o-Xylene [95-47-6]^ sec-Butylbenzene (135-98-8]^ Styrene (100-42-5] ^ tert-Butylbenzene [98-06-6]^ Tetrachioroethene (127-18-4]^ Toluene (108-88-3]^ trans- l f 2-Dichloroethene [156-60-5] ^ trans-lj3-Dichloropropene [10061-02-6]^ Trichlor ethene [79-01-6]^ Trichloiofluoromethane [75-69-4]^ Vinyl chloride [75-01-4]^ Xylene (Total) (1330-20-7]^ Surro ales 4-Brorrilo/luorobenzene Dibrorriofluoromethane Toluenl-d8 Results < 0.074 < 0.073 < 0.088 < 0.053 < 0.082 < 0.094 < 0.099 < 0.053 < 0.11 < 0,080 < 0.13 < 0.15 < 0.083 < 0.22 Flaa Units DF MDL POL Batch Method Analyzed §y Notes ug/L 1 0.074 0.50 SA08010 EPA 8260B/6230D 01/08/15 14:46 MSZ ug/L 1 0.073 0.50 5A06010 EPA 82606/62300 01/08/15 14:46 MSZ ug/L 1 0.088 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:46 MSZ ug/L 1 0.053 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:46 MSZ ug/L 1 0.082 0.50 5AO8010 EPA 82.60B/6230D 01/08/15 14:46 MSZ ug/L 1 0.094 0.50 SA08010 EPA 8260B16230D 01/08/15 14:46 MSZ ug/L 1 0.099 0.50 5A08010 EPA 8260B/62300 01/08/15 14:46 MSZ ug/L 1 0.053 0.50 5AO8010 EPA 8260B/6230D 01/08/15 14:46 MSZ ug/L 1 0.11 0.50 5AO8010 EPA 82608/6230D 01/08/15 14:46 MSZ ug/L 1 0.080 0.50 5AO8010 EPA 82606/6230D 01/08/15 14:46 MSZ ug/L 1 0.13 0.50 5A08010 EPA 82608/6230D 01/08/15 14:46 MSZ ug/L 1 0.15 0.50 SA08010 EPA 8260B/6230D 01/08/15 14:46 MS7 ug/L 1 0.083 0.50 5A08010 EPA 8260B/6230D 01/08/15 14:46 MSZ ug/L 1 0.22 0.50 SA08010 EPA 8260B/6230D 01/08/1S 14:46 MSZ Resu/tr OF Spike Lvl o/n Re c o/a Rec Limits Batch Method Analyzed fy Notes 55 1 50.0 109 % 53-136 5A08010 EPA 8260B/6230L 0110811514.46 AISZ 53 1 50.0 107 % 67-129 5AO8010 EPA 826OB16230C 01108/1514:46 MSZ 59 1 50.0 118 % 59-134 5AO8010 EPA 826OB16230C 01108115 14:46 MSZ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 39 www.encolabs.com ANALYTICAL RESULTS. De ripti.cm: 141660°12, MW-15. Lab Sample ID: C50013 31-12 Received: 01/05/1 5 14:06 Matrix: Ground Water Sampled: 12/31/14 13:23 Work Order: C50.0133. Project: Genral Subcontract Sampled By:CLIENT IVolatile Organic C6mpounds by GCMS ^r-C, ENCO Cary certiried analyte (NC 591) 4nalyl AS Numberl' Results Flaq mniifl aF MDL POL Batch Method Analyzed Ay Notes 1,1,1,2 Te I trachloroethane[630-20-6]^ < 0.091 ug/L 1 0.091 0.50 5A09017 EPA 8260B/6230D 01/09/15 16:09 MSz 1,1,1-Tr ichioroethan6 [71-55-6]A < 0.15 ug/L 1 0.15 0.50 5AO9017 EPA 826013/6230D 01/09/15 16:09 msz 1,1,22 Tetrachloroethane (79-34-5)^ < 0.085 ug/L 1 0.085 0.50 5AO9017 EPA 8260B/6230D 01/09/15 16:09 msz 1,1,2:T ichloroethane [79-00-5]1 < 0.068 ug/L 1 0.068 0.50 5A091017 EPA 826OB/6230D 01/09/15,16.09 NISZ 1,1-Qic loroethane [75-34-3]A < 0.050 ug/L 1 0.050 0.50 5AO9017 EPA 826013/6230D 01/09/15 16:09 MSz 1,I-Dic loroerhene [75-35-1]^ < 0.15 ug/L - I 0.15 0.50 5A09017 EPA 8260B/6230D 01'/09115 16:09 MS7 i,I-Diciloropropene (563-58L6]A < 0.063 ug/L 1 0.063 0.50 5AO9017 EPA 8260B/6230D 01/01/15 16:09 MSz 1,2,3-T�Ichlorobenzene (8.7-,j61-6]A < 0.25 ug/L 1 0.25 0.50 SA09017 EPA 8260B16230D 01/09/15 16:09 msz 1.2,21-Tfichloropropane (96-18741A < 0.15 ug/L 1 0.1-5- 0.50 5AO9017 EPA 8260B/6230D 01/09/15 16:09 msz 1,2,47 ichlorobenzene (120-82-I)A < 0.097 ug/L - 0.097 0.50 5AO9017 EPA 82608/6230.D 01/09/15 16:09 MSz 1,2, 1 4r imdthylbenzelne 195-63-,61^ < 0.067 ug/L 1 0.067 0.50 5AD9017 EPA 826013/6230D 01/09/15 16:09 I'lSz 1,2-Di romo-3-chloropropane (96-12-81^ < 0.48 ug/L 1 0.48 0.50 5AO9017 EPA 8260B/6230D 01/09/15 16:09 -MSZ '1,2-D,j ' romoethane [106-93-41^ < 0.27 ug/L. 0.27 0.50 5A09017 EPA 826013/6230D 01/09/15 16:09 msz 1,2-Dic,korobenzene [95-50-1]^ < O.OU ug/L 1 0.062 0.50 5AO9017 EPA 826OB/6230D 01/09/15 16:09 MSz 1,2-Dickloroethane (10'7-0&2]A < 0.082 ug/L 1 0.082 0.50 SA09017 EPA 826013/6230D 01/09/15 16:09 msz ,1,2-Dichloropropane (78-87m5)1� < 0.098 ug/L 0.098 0.50 SA09017 EPA 8260B/6230D 01109/15 16:09 msz 1,3,5'-Trimethylbenzene (I08-67-8]^ < 0.10 ug/L ..1 0.10 0.50 SA09017 EPA 826013/6230D 01/09115 16:09 msz 1,3-Di lorobenzene [541-73-1]^ < 0.092 uq/L 1 0.092 0.50 ,5A09017 EPA 8260B/6230D 01/09/15 16:09 msz 3 1,-Dii1orojiropane (142-28-91^ < 0.1 5 ug/L 1 0.15 0.50 5AO9017 EPA 826013/6230D. 01/09/15 16:09 msz l-Die-Dic I hlorobenzene [10&46-7]^ 1 < 0.10 ug/L 1 0.10 0.50 5A09017 EPA 8260B/6230D 01109115 16:09 MSz 2,2-Cichloropropane (594-20-71A < 0.1,2 ug/L 1 0.12 0.50 5AO9017 EPA 826013/62301) 01109/15 16:09 msz 2-Chlo�,otolu . ene [95-49-.8]^ < 0.10 ug/L 0.10 0.5 0 SA09017 EPA 826013/6230D 01/09/15 16:09 MSz 4mChlo otoluene (106-43-4]A < 0.10 uq/L 1 0.10 . 0.50 SA09017 EPA 8260B/6230D 01/09/15 16:09 Nlsz 4-Iso -87-61A pipyltoluene [99 < 0.066 ug/L 1 0.066 0.50 5AO9017 EPA 8260B/6230D 01/09/15 16:09 MSz Benze e [71w43-2]^ < 0.050 ug/L 1 0.050 0.50 5AO9017 EPA 8260B/6230D 01/09/15 16:09 msz Brom. enzene [108-86-1]^ < 0.13 ug/L 1 0.13 0.50 5AO9017 EPA 8260B/6230D 01/09/15 16:09 MSz Bromo:hloromethane [74-97-5]A < 0.11 ug/L 1 0.11 0.50 5AO9017 EPA 82608 . /6230D 01/09/15 16:09 lVlSz Bromo ichloromethane (75-27-4)^ < 0.010 ug/L 1 0.010 0.50 SA09017 EPA 826013/62301) 01/09/15 16:09 MSz Bromobrm [75-25-2]^ < 0.20 ug/L 0.20 0.50 5A09017 EPA 8260B/6230D 01/09/15 16:09, MSz Bro , monethane (74-83-9]A < 0.28 ug/L 1 0.28 0.50 5A09Oi7 EPA 826013/6230D 01/09/15 16:09 MSZ Carbor Tetrachloride (56- . 23-5]^ ;c 0.082 ug/L 1 0.082 0.50 5A09017 EPA 8260B/6230D 01/09/15 16:09 MS7 Chloro)enz - ene [108-90-7]A < 0.069 ug/L 1 0.069 0.50 5A09017 EPA 826013/6230D 01/09115 16:09 lVlSz Chlorthane [75-00-3]A 0.18 uq/L - 1 0.18 1 0.50 SA09017 EPA 82606/6230D OI/09/15 16:09- MSz T Chloroform [67-66-3]A < 0.083 ug/L ' 1 0.083 0.50 5AO9017 EPA 826013/6230D 01/09/15 16:09 MSz. Chloro�nethane [74-87-3]^ < 0.050 ug/L 1 0.050 0.50 5A09017 EPA 8260B16230D 01/09/15 16:09 MSz cis-1, Dichloroethene [156-59m21A < 0.075 ug/L 1 0.075 0.50 SA09017 EPA 8260B/6230D 01/09/15 16:09 msz - cis-1, Dichloropropene [10061-01-5]A < 0.073 ug/L 1 0.073 0.50 SA09017 EPA 8260B/6230D O1/09/15 16:09 MSz Dibromochloromethane [124-48-11A < 0.067 ug/L 1 0.067 0.50 5AO9017 EPA 8260B/6230D 01/06/15 16:09 1%i5z Dibromomethane (74-95-31.^ < 0.13 ug/L .1 0.13 0.50 SA09017, EPA 826OB/6230D 01/09/15 16:09 MSz Dichlo oclifluoromethane (75-71-8]A < 0.091 ug/L 1 0.091 0.50 5A09017 EPA 8260B/6230D 01/09/15 16:09 MS7- Ethyl nzene (100-41-4]A < 0.10 ug/L. 1 0.10 0.50 5AO9017 EPA 8.26013/6230D 01i09/15 16:09 MSZ Hexacilorobutadiene [87-68-3]^ < 0.15 ug/L A 0.15 0.50 5AO9017 'EPA 8 260B/G23 OD 01/09/15 16:C9 MS, lsoprpyl Ether (108-20-31,` <, 0.20 6g/1- 1 0.20 0.50 5AO9017 I EPA 8260616230D 01/09/15 16:09 M5Z Isoprc pylbenzene [98-82-8] A < 0.13 ug/L 1 0.13 0.50 5AO9017 EPA 826OB/6230D 01/09/15 16:09 PIS7 M,P-X denes [108-38-3/106-42-3]" < 0.18 ug/L 1 0.18 0.50 5AO9017 EPA 826OB16230D - 01/09115 16:09 Hsz Meth y ene Chloride (75-092]^ < 0.070 ug/L 1 0.070 0.50 5A09017 EPA 826013/6230D 01/09/15 16:09 NISZ Methtert-Butyl Ether (1634-04-4]A � - < 0.12 ug/L 1 '0:12 0.50. 5A69017 EPA 826OB/6230D 01/09/15 16:09 MSz Napht ialene'(91-20-31A < 0.086 ug/L 1 0.086 0.50 5AO9017 EPA 8260B/6230D 01/09115 16:09 msz FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I 'age 26 o: 39 ANALYTICAL RESULTS I �cription: 141660-12 MW-15 Lab Sample ID:C500133-12 Matrix: Ground Water Sampled:12/31/14 13:23 Project: Genral Subcontract Sampled By:CLIENT r" 0, www.encolabs.com Received: 01/05/15 14:06 Work Order: C500133 (Volatile organic Compounds by GCMS Analvl^fCAS ENCO Cary certified analyre (NC 5911 Numberl Benzene[104-51-8]^ Benzene [103-65-1]^ [95-47-6]^ (135-98-8]^ [100-42-5]^ 06-6]^ oroethene[127-18-4]^ [108-88-3]^ 2-Dichloroethene (156-60-5]^ 3-Dichloropropene[10061-02-6]^ Results Flag < 0.074 < 0.073 < 0.088 < 0.053 < 0.082 < 0.094 < 0.099 < 0.053 < 0.11 < 0.080 < 0.13 Units ug/L ug/L ug/L ug/L ug/1- ug/L ug/L ug/L ug/l. ug/L ug/L DF 1 1 1 1 1 1 1 1 1 1 1 MDL 0.074 0.073 0.088 0.053 0.082 0.094 0.099 0.053 0.11 0.080 0.13 pPOL 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 0.50 Batch 5A09017 5A09017 5AO9017 5AO9017 5A09017 5A09017 5AO9017 SA09017 5AO9017 5AO9017 5A09017 EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA EPA Method 8260B/6230D 8260B/6230D 8260B/6230D 82.60B/6230D 82606/62.30D 8260B/6230D 8260B/6230D 8260B/6230D 8260B/6230D 82606/62300 8260B/6230D Analyzed 01/09/15 16:09 01/09/15 16:09 01/09/15 16:09 01/09/15 16:09 01/09/15 16:09 01/09/15 16:09 01/09/15 16:09 01/09/15 16:09 01/09/15 16:09 01/09/15 16:09 01/09/15 16:09 Notes t•1SZ MSZ MSZ MSZ h1S7 MSZ MSZ MSZ MSZ MSZ MSZ n-Butyl n-Prop] o-Xylene sec-But�lbenzene Styren tert-Bulbenzene[98 Tetract Toluen trans-1 trans-1 Trichlooethene[79-01-6]^ TrichloIofluoromethane[75-69-4]^ Vinyl [75-01-4]^ < 0.15 < 0.083 ug/L ug/L 1 1 0.15 0.083 0.50 0.50 SA09017 SA09017 EPA EPA 8260B/6230D 82606/6230D 01/09/15 01/09/15 16:09 16:09 MSZ MSZ c'loride Xylene5(Total)[1330 20-7]^ < 0.22 ug/L 1 0.22 0.50 5AO9017 EPA 8260B/6230D 01/09/15 16:09 MSZ Resultr OF Spike Ly/ % Re c % Rec Limits Batch Method Analyzed ffy Notes 55 1 50.0 109 % 53-136 5AO9017 EPA 826OB/6230L 01/09/15 1609 A/5Z 52 1 50.0 105 96 67-129 5A09017 EPA 826OB16230C 01;09/15 16:09 %ISZ 59 1 50.0 118 % 59-134 5AO9017 EPA 826OB16230L 01109115 16:09 A15Z FlNAI. This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 39 www.encolabs.com ANALYTICAL RESULTS Description- 141660-04 MW-17 Lab Sample ID:C500133-04 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 12:06 Work Order: C500133 Project: Genral Subcontract - Sampled By: CLIENT latile Organic Compounds by GCMS ^ • ENIo Cary certired ana/yte INC 5911 1,,1,1,2 etrachloroethane [630-20-6]^ 1,1,1- .tI hloroethane [ 71-55-6] ^ 1,1,2,2{Fetrachloroethane [79-34-5]^ 1;1,2-Tffrrll.ichloroethane [79-00-5]^ -1,1-Dicilorcethane [75-34-31^ 1,1-Dichiloroethene [75-35-4]A 1,1-Dichloropropene [563-58-6]^ 1,2,3-T ichlorobenzene [87-61-6]^ 1,2,3-T ichloropropane [96-18-4]^ 1,2;+T ichlorobenzene [120-82-1]^ 1,2,4-T imethylbenzene [95-63-61^ 1,2-Dib omo-3-chloropropane [96-12-8]^ 1,2-Dib omoethane [106-93-4]^ 1,2-Dic ilorobenzene [95-50-1]A 1,2-Dicloroethane [107-06-2]^ 1,2-DickIoropropane [78-87-5]^ 1,3,5-TFimethylbenzene [108-67-8]^ 1,3-Dic Ilorobenzene [541-73-1]^ 1,3-Dic iloropropane (142-28-91^ 1,4-Dic ilorobenzene [ 106=46-71^ 2,2-Dic loropropane (594-20.7]^ 2-Chlo toluene [95-49-8]^ 4-ChloI toluene [106.43-41^ 4-lsoprppyltoluene, 199-87,61A Bence ]e [71-43-2]^ Bromobenzene [108-86-11^ Bromochloromethane (74-97-5]^ Bromcaichloromethane [75-27-4]^ Bromo orm [75-25-2]^ Bromo ethane [74-83-9]^ Carboni Tetrachloride [56-23-S]^ Chloro¢enzene [108-90-71^ Chloroe thane [75-00-3]^ Chloroform [67-66-3]^ Chloro{nethane [74-87-31^ cis-1,2 Dichloroethene [156-59-2]^ cis-1,3 Dichloropropene [10061-01-5]^ Dibro ochloromethane [129A8-1]^ Dibro omethane [74-95-3]^ DichlotodiFluoromethane [75-.71-81^ Ethylll�Inzene [100.41-4]^ Hexaclnlorobutadiene [87-68-3]^ Isopro yl Ether [108-20-3]^ Isopro ylbenzene (98-82-B]^ m,p-X lenes [108-38-3/106-42-3]^ Methyene Chloride [75-09-2]^ Methy-tert-Butyl Ether [1634-04-41^ Naphthalene [91-20-3]^ ] FINAL t l Resultr Flag Units DF MDL 4 Batch Method Analyzed < 0.091 ug/L 1 0.091 0.50 5AO6013 EPA 82606/6230D 01/06/15 17:41 < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 8260B/6230D 01/06/15 17:41 < 0.085 ug/L 1 0.085 0.50 SA06013 EPA 8260B/6230D 01/06/15 11:41 < 0.068 ug/L 1 0.068 0.50 5A06013 EPA 82608/6230D 01/06/15 17:41 < 0.050 ug/L 1 0.050 0.50 SA06013 EPA 82600/6230D 01/06/15 17:41 < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 8260B/6230D 01/06/15 17:41 < 0.063 ug/L 1 0.063 0.50 SA06013 EPA 8260B/6230D 01/06/15 17:41 < 0.25 ug/L 1 0.25 0.50 5A06013 EPA 8260B/62300 01/06/15 17:41 < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 82608/62301) 01/06/15 17:41 < 0.097 ug/L 1 0.097 0.50 SA06013 EPA 8260B16230D 01/06/15 17:41 < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 82606/6230D 01/06/15 17:41 < 0.48 ug/L 1 0.48 0.50 5A06013 EPA 8260B/6230D 01/06/15 17:41 < 0.27 ug/L 1 0.27 0.50 5A06013 EPA 8260B/6230D 01/06/15 17:41 < 0.062 ug/L ] 0.062 0.50 5A06013 EPA 8260B/6230D1 01/06/15 17:41 < 0.082 ug/L 1 0.082 0.50 SA06013 EPA 82606/6230D 01/06/15 17:41 < 0.098 ug/L 1 0.098 0.50 SA06013 EPA 8260B/6230D 01/06/15 17:41 < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 82.60616230D 01/06/15 17:41 < 0.092 ug/L 1 0.092 0.50 5AO6013 EPA 82606/6230D 01/06/15 17:41 < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 82.608/6230D 01/06/15 1/:41 < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 8260B/6230D 01/06/15 17:11 < 0.12 ug/L 1 0.12 0.50 5A06013 EPA 82.60B/6230D 01/06/15 17:41 < 0:10 ug/L 1 0.10 0.50 5AO6013 EPA 82606/62301D 01/06/15 17:41 < 0.10 ug/L I - 0.10 0.50 5AO6013 EPA 8260B/6230D 01/06/15 17:41 < 0.066 ug/L - 1 0.066 0.50 5AO6013 EPA 8260816230D 01/06/15 17:41 < 0.050 ug/L 1 0.050 0.50 5AO6013 EPA 8260B/62301) 01/06/15 17:41 < 0.13 ug/L 1 0.13 0.50 5AO6013 EPA 8260B/6230D 01/06/15 17:41 < 0.11 ug/L 1 0.11 0.50 SA06013 EPA 8260B/6230D 01/06/15 17:41 < 0.010 ug/L 1 0.010 0.50, 5AO6013 EPA 8260B/6230D 01/06/15 17:41 < 0.20. ug/L 1 0.20 0.50 5A06013 EPA 8260B16230D 01/06/15 17:41 < 0.28 ug/L 1 0.28 0.50 SA06013 EPA 82608/6230D 01/06/15 17:41 < 0.082 ug/L 1 0.082 0.S0 5AO6013 EPA 82608/62.30D 01/06/15 17:41 < 0.069 ug/L 1 0.069 0.50 5AO6013 EPA 8260B/6230D 01/06/15 17:41 < 0.18 ug/L 1 0.18 0.50 5A06013 EPA 82608/6230D 01/06/15 17:41 < 0.083 ug/L 1 0.083 0.50 - 5A06013 EPA 8260B/6230D 01/06/15 t7:41 < 0.050 ug/L 1 `0.050 0.50 5A06013 EPA 826013/62301) 01/06/15 17:41 < 0.075 ug/L 1 0.075 0.50 5AO6013 EPA 8260B/6230D 01/06/15 17:41 < 0.073 ug/L 1 0.073 0:50 5AO6013 EPA 8260B/6230D 01/06/15 17:41 < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 82608/6230D 01/06/15 17:41 < 0.13 ug/L 1 0.13 ' 0.50 :, 5AO6013 EPA 8260B!6230D 01/06/15 17:41 < 0.091 ug/1- 1 0.091 0.50 5AO6013 FPA 82608/62..300 01/06/15 17:41 < 0.10 ug/L 1 0.10 0.50 .5A06013 EPA 8266B/6230D 01/06/15 17:41 < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 82606/6230D 01/06/15 17:41 < 0.20 ug/L 1 0.20 0.50 5A06013 EPA82606/6230D 01/06/15 17:41 < 0.13 ug/L• 1 0.13 0.50 5A06013 EPA 8260B/6230D 01/06/15 17:41 < 0.18 ug/L. 1 0.18 0.50 . 5AO6013 EPA 8260B/6230D 01/06/15 17:41 < 0.070 Lig/L 1 0.070 ' 0.50 SA06013 EPA 8260B16230D 01/06/15 17:41 < 0.12 ug/I. 1 0.12 0.50. 5AO6013 EPA 8260B/6230D 01/06/15 17:41 < 0.086 ug/I- 1 0.086 0.50 5AO6013 EPA 82606/6230D 01/06/15 17:41 This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Notes M57 MS7 NISI: MSz MSz Ms7. MSz MSz MSz- MSz MSz M57- M5z MSz MSz MSz MSz MSz MSz.. M57 NIS7 MSz MSz MSz MSz MSz MSz MSz MSz MSz MSz MSz MSz MSz MSZ MSz MSz MSz M57- Ms7 NISI MSz MSz MSz MSz MSz MSz MS7 Page to.of 39 ANALYTICAL RESULTS scription: 141660-04 MW-17 Lab Sample ID:C500133-04 Matrix: Ground Water Sam pied: 12/31/14 12:06 Project: Genral Subcontract Sampled By:CLIENT olatile Organic Compounds by GCMS ^ - ENCO Cary certified dnalyte (NC 591 j www.encolabs.com Received: 01/05/15 14:06 Work Order: C500133 Anal�e rCAS N.,nberl Benzene[104-51-8)^ Results < 0.074 Flag Units ug/L DF 1 MDL 0.071 PQL 0.50 Batch 5AO6013 EPA Method 8260B/6230D Analyzed 01/06/15 17:41 n-ButyJ n-Proo,yl Benzene (103-65-1] ^ < 0.073 ug/L 1 0.073 0.50 SA06013 EPA 82608/6230D 01/06/15 17:41 o-Xyle e[95-47-6]^ < 0.088 ug/L 1 0.088 0.50 5AO6013 EPA 8260B/6230D 01/06/15 17:41 sec-Bi tylbenzene[135-98-8]^ < 0.053 ug/L 1 0.053 0.50 5A06013 EPA 82608/6230D 01/06/15 17:41 Styren e[100-42-51^ < 0.082 ug/L 1 0.082 0.50 5AO6013 EPA 82.60B/6230D 01/06/15 17:41 tert-B1ltylbenzene (98-06-6]^ < 0.094 ug/L 1 0.094 0.50 5AO6013 EPA 8260B/6230D 01/06/15 17:41 TetrachIloroethene[127-18-4)^ < 0.099 ug/L 1 0.099 0.50 SA06013 EPA 82606/6230D 01/06/15 17:41 Toluer�e[108-83-3]^ < 0.053 ug/L 1 0.053 0.50 SA06013 EPA 8260B/6230D 01/06/15 17:41 trans-I,2-Dichloroethene [156-60-5]^ < 0.11 ug/L 1 0.11 0.50 5AO6013 EPA 82608/6230D 01/06/15 17:41 Vans-1,3-Dichloropropene[10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 5AO6013 EPA 82606/6230D 01/06/15 17:41 TrichldlIroethene [79-01-6]^ < 0.13 ug/L 1 0.13 0.50 5A06013 EPA 8260B/6230D 01/06/15 17:41 Trichldrofluoromethane [75-69-4]^ < 0.15 ug/I. 1 0.15 0.50 5A06013 EPA 8260B/6230D 01/06/15 17:41 Vinyl chloride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 SA06013 EPA 8260B/6230D 01/06/15 17:41 Xylenels (Total) [1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 5AO6013 EPA 82608/6230D 01/06/15 17:41 Surr ates Resu/ts OF Saike Lv/ % Rec % Rec Limits Batch Method Analyzed 4-Brorinofluorobenzene 59 1 50.0 117 % 53-136 5A06013 EPA 6260B16230L 01106115 17:41 Dibromofluoromethane 57 1 50.0 114 % 67-129 5A06013 EPA 8260B16230C 01106115 17:41 r'oluewe-d8 1 1 59 1 50.0 118 % 59-134 5A06013 EPA 8260B16230L 01106115 17:41 Notes MS7 MSZ h1SZ MSZ 1SZ MSZ MSZ MSZ MSZ MSZ MSZ MS7. MSZ MSZ By Notes M5Z MSZ MSZ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. "age 11 of 39 www.encolabs.com ANALYTICAL RESULTS :ription: 141660-01 MW-19 Lab Sample ID:C500133-01 Received: 01/05/15 14:06 Matrix: Ground Water Sampled;12/31/14 11:25 Work Order: C500133 Project: Genral Subcontract Sampled By:CLIENT V latile Organic Compounds by GCMS ^ ENCO Cary ceRiried analyre (NC 5911 - Analyt, rCAS Number - etrachloroethane[630-20-6]^ Results Flan - < 0.091 Units ug/L DF 1 MDL 0.091 POL 0.50 Batch 5A06013 Method EPA 82606/6230D Analyzed 01/06/15 16:11 _By - Notes MSz 1,1,1,2 1,1,1-Tichloroethane[71-55-6]^ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 8260B/6230D 01/06/15 16:11 MSZ 1,1,2,2 Tetrachloroethane [79-34-5]^ < 0.085 ug/L -1. 0.085 0.50 5A06013 EPA 8260B16230D 01/06/15 16:11 MSZ 1,1,2-Tichloroethane[79-00-5]^ < 0.068 ug/L 1 0.068 0.50 5AO6013 EPA 82608/62301) 01/06/15 16:11 MSZ 1,1-Dic floroethane [75-34-3]^ < 0.050 ug/L 1 0.050 .0.50 SA06013 EPA 82608/62301) 01/06/15 16:11 MSZ 1,1-Dic iloroethene[75-35-4]^ < 0.15 ug/L i 0.15 - 0.50 SA06013 EPA 82606/6230D 01/06/15 16:11 MSZ 1,1-Dic floropropene[563-58-6]^ < 0.063 ug/L 1 0.063 0.50 '5A06013 EPA 826013/6230D 01/06/15 16:11 MSZ 1,2,3-Tichlorobenzene(87.61-6]^ < 0.25 ug/L 1 0.25 0.50 5AO6013 EPA 82606/6230D 01/06/15 16:11 MSZ 1,2,3rT ichloropropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 8260B/6230D 01/06/15 16:11 MSZ 1,2,4-T ichlorobenzene [120-82-1]^ < 0.097 ug/L 1 0.097 0.50 5AO6013 EPA 82608/62301) 01/06/15 16:11 MSz 1,2,4-Timethylbenzene[95-63-6]^ < 0.067 ug/L 1 0.067 0.50 5A06013 EPA 8260B/62300 01/06/15:16:11 MSZ 1,2-Dib omo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 5AO6013 EPA 826013/6230D 01/06/15 16:11 MSz 1,2-Dib omoethane [106-93-4]^ < 0.27 .ug/L 1. 0.27 0.50 5A06013 EPA 82608/62301) 01/06/15 16:11 MSZ 1,2-Dic iforobenzene[95-50-1]^ < 0.062 ug/L 1 0.062 0.50 5AO6013 EPA 82608/6230D 01/06/15 16:11 hISZ 1,2-Dir.loroethane[107-06-2]^ < 0.082 ug/L 1 0.082 0.50 5AO6013 EPA 82606/6230D 01/06/J5 16:11 MSZ 1,2-Dic floropropane[78-87-5]^ < 0.098 ug/L, 1. 0.098 0.50 5A06013 EPA 82.6OB16230D 01/06/15 16:11 M57 1,3,5-T imethylbenzene [108-67-8]^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 82606/62.301) 01/06115 16:11 MS7 1,3-Dic ilorobenzene[511-73-1]^ < 0.092 ug/L 1 0.092 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:11 IISL 1,3-Dic loropropane[142-28-9]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 82608/6230D 01/06/15 16:11 MSz 1,4-Dic lorobenzene [106-46-7]^ < 0.10 _ ug/L 1 0.10 0.50 5AO6013 EPA 82606/6230D 01/06/15 16:11 MS7. 2,2-Dic iloropropane[594-20-7]^ < 0.12 ug/L 1 0.12 0.50 SA06013 EPA 82606/6230D 01/06/15 16:11 MSZ' 2-Chlor otoluene [95-49-8]^ < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 826013/6230D 01/06/15 16:11 r-15Z 4-Chlor otoluene (106-43.4]^ < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 82.60B/6230D. 01/06/15 16:11 MSz 4-Isop ,pyltoluene[99-87-6]^ < 0.066' ug/L -1 0.066 0.50 SA06013 EPA 82608/6230D 01/06/15 16:11 hlSz Benze (71-43-2]^ < 0.050 ug/L 1 0.050 0.50 5A06013 EPA 8260B/6230D 01/06/15 16:11 NISz Bromo enzene(108-86-1]^ < 0.13 ug/L 1 0.13 0:50 SA06013 EPA 82608/6230D 01/06j15 16:11 MSZ Bromo hloromethane[74-97-5]^ < 0.11 ug/L 1 0.11 0.50 5A06013 EPA 82606/6230D 01/06/15 16:11 MSz Bromo ichloromethane [75-27-4]^ < 0.010 ug/L 1 0.010 0.50 5A06013 EPA 82606/6230D 01/06/15 16:11 MSZ Bromo orm (75-25-2]^ < 0.20 ug/L 1 0.20 0.50 5A06013 EPA 82606/6230D 01/06/15 16:11 MSz Bromo ethane[74-83-9]^ < 0.28 ug/L 1 0.28 0.50 5AO6013 EPA 826013/6230D, 01/06/15 16:11, MSZ Carbor Tet rachloride (56-23-5]^ < 0.082 ug/L 1 0.082 0.50 5A06013 EPA 8260B/6230D 01/06/15 16:11 MSz Chloro enzene'[108-90-7]^ < 0.069 ug/L 1 0.069 0.50 5AO6013 EPA 826013/62301) 01/06/15 16:11 MSz Chloro thane[75-00-3]^ < 0.18 ug/L 1 0.18 0.50 5AO6013 EPA 82608/62301). 01/06/15 16AI MSz Chloro orm (67-66.3)^ < 0.083 ug/L 1 0.083 0.50 SA06013 EPA 82608/6230D 01/06/15 16:11 MSZ Chloro ethane[74-87-3]^ < 0.050 ug/L - 1 0.050 0.50 5AO6013 EPA 82.60B/6230D 01/06/15 16:11 MS7. cis-1,2 Dichloroethene [156-59-2]^ < 0.075 ug/L 1- 0.075 0.50 5A06013 EPA 8260B/6230D 01/06/15 16:11 M57. cis-1,3 Dichloropropene(10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 5A06013 EPA 82608/6230D 01/06/15 16:11 MSz. Dibro ochloromethane [124-48-1]^ < 0.067 ug/L 1 0.067 0.50 -5A06013 EPA 826013/6230D 01/06/15 16:11 MSZ Dibrorr omethane [74-95-3]^ <'0.13 ug/L 1 0.13 0.50 5A06013 EPA 82608/6230D .01/06/15 16:11 hISZ Dichlo difluoromethane [75-7178]^ < 0.091 ug/I. .1 0.091 0.50 5A06013 FPA 826013/62301) 01/06/15 16:11 MS7. Ethylb nzene[100-41-4]^ < 0.10 ug/L 1 0.10 0.50 SA06013 EPA 82606/6230D 01/06/15-16:11 MR Hexac lorobutadiene[87-68-3]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 82608/6230D 01/06/15 16:11 MSZ lsopro yl Ether [108-20-3]^ < 0.20 ug/l. 1 0.20 0.50' -5A06013 EPA 8260B16230D 01/06/15 16:11 MSZ isopro ylbenzene (98-82-8]^ < 0.13 ug/L 1 0.13 0.50 5A06013 EPA 8260B/62301) 01/06/15 16:11 MSZ m,p-X lenes [108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:11 MSZ Methyl ne Chloride (75-09-2]^ < 0.070 ug/L 1 0.070 0.50 SA06013 EPA 8260B/6230D 01/06/15 16:11 MSz Methyl tert-ButylEther (1634-04-4]^ < 0.12 ug/L 1 0.12 0.50 5A06013 EPA 826013/6230D 01/06/15 16:11 MSZ Napht alene(91-20-3]^ < 0.086 ug/L 1 0.086 0.50. 5AO6013 EPA 82606/62301) 01/06/15 16:11 MSz FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 39 �'"° ��ac 9 1� fa°^'E "P�,�`.e-sue• `s www.encolabs.com ANALYTICAL RESULTS :ription: 141660-01 MW-19 Lab Sample ID:C500133-01 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 11:25 Work Order: C500133 Project: Genral Subcontract Sampled By:CLIENT olatile Organic Compounds by GCMS 1 ^ - ENCO Cary ceniBed analyre [NC 591] n-Buty Benzene [104-51-8]^ n-Prop I Benzene [103.65-1]^ o-Xyle a [95-47-6]^ sec-Bu (benzene [135-98-8]^ Styren [100-42-5]^ tert-BL tylbenzene [98-06-6]^ Tetrac iloroethene [127-18-4]^ Tolue a [108-88-3]^ trans- ,2-Dichloroethene [156-60-5]^ trans- ,3-Dichloropropene [10061-02-6]^ Trichic roethene (79-01-6]^ 'irichl rofluoromethane [75-69-4]^ Vinyl chloride [75-01-4]^ Xylen (Total)[1330-20-7]^ Results Flaa Units DF MDL POLL Batch Method Analyzed 1y Notes < 0.074 ug/L 1 0.074 0.50 SA06013 EPA 8260B/6230D 01/06/15 16:11 MSZ < 0.073 ug/L 1 0.073 0.50 5AO6013 EPA 8260B/6230D 01/06/IS 16:11 MSZ < 0.088 ug/L 1 0.088 0.50 5A06013 EPA 8260B/6230D 01/06/15 16:11 N1SZ < 0.053 ug/L 1 0.053 0.50 SA06013 EPA 8260B/6230D 01/06/15 16:11 NIS7. < 0.082 ug/L 1 0.082 0.50 5A06013 EPA 8260R/6230D 01/06/1S 16:11 MSZ < 0.094 ug/L 1 0.091 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:11 h1S7- < 0.099 ug/L 1 0.099 0.50 5A06013 EPA 8260B/6230D 01/06/15 16:11 MSZ < 0.053 ug/L 1 0.053 0.50 SA06013 EPA 8260B/6230D 01/06/15 16:11 MSZ < 0.11 ug/L 1 0.11 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:11 MSZ < 0.080 ug/L 1 0.080 0.50 SA06013 EPA 82606/62300 01/06/15 16:11 MSZ < 0.13 ug/L 1 0.13 0.50 SA06013 EPA 8260B/6230D 01/06/15 16:11 I.1SZ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:11 MSZ- < 0.083 ug/L 1 0.083 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:11 h1SZ- < 0.22 ug/L 1 0.22 0.50 5A06013 EPA 8260B/6230D 01/06/15 16:11 I4iZ Resu/tr DE Spike Lvl °7o Re c % Rec Limits Batch Method Analyze By Notes 58 1 50.0 117 % 53-136 5AO6013 EPA 6260516230C 01106115 16:11 M5Z 55 1 50.0 111 % 67-129 5AO6013 EPA 8260816230C 01106115 16: 11 A151 61 1 50.0 122 % 59-134 5AO6013 EPA V..6OB16230C 01106115 16:11 'N-SZ- FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 39 tip, �} iFS �t iiG61.. i ? ,' www.encolabs.com ANALYTICAL RESULTS :ription• 141660-02 MW-20 Lab Sample ID:C500133-02 Received:. 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 11:37 Work Order: C500133 Project: Genral Subcontract Sampled By:CLIENT . Volatile Organic Compounds by GCMS ENCO Cary certified analyle INC 5911 ^rCAS - - Analvt� Numberl Results Flag Units ' DF • MDL POE Batch Method Analyzed Notes 1,1,1,21retrachloroethane [630-20-6]^ < 0.091 ug/I- 1 0.091 0.50 5AO6013 EPA 8260B16230D 01/06/15 t6:42. r45z 1,1,1-Tlichloroethane.[71.55-6]^ < 0.15 ug/L 1 0.15 0.50 SA06013 FPA 8260B/6230D 01/06/15 16:42 11S7 1,1,2,21Tetrachloroethane [79-34-5]^ < 0.085 ug/L 1 0.085 0.50 5A06013 EPA 826OB/6230D 01/06/15 16:42 MSZ 1,1,2-T ichloroethane (79-00-5]^ < 0.068 ug/L 1 0.068 0.50 5A06013 EPA 826OB/6230D 01/06/15 16:42 MSz 1,1-Die iloroethane(75-34-3)^ < 0.050 ug/L 1 0.050 0.50 5A06013 EPA 826OB/6230D 01/06/15 16:42 htSz 1,1-Diclloroethene (75-35-4]^ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 8260B/6230D 01/06/15 16:42 t45Z 1, 1 -Dichloropropene (563- 58-6]^ < 0.063 ug/L 1 0.063 0.50 5AO6013 EPA 826OB/6230D 01/06/15 16:42 MSz 1,2,3-Tichlorobenzene (87-61-6]^ < 0.25 ug/L 1 0.25 0.50 5A06013 EPA 8260B/6230D 01/06/15 16:42 MSz 1,2,3-T ichloropropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 8260B/6230D 01/06/15 16:42 MSz 1,2,4-T�ichlorobenzene [120*82-1]^ < 0.097 ug/L 1 0.097 0.50 SA06013 'EPA 8260B16230D 01/06/15 16:42 MSz 1,2,4-Trlmethylbenzene [95-63-6]^ < 0.067 ug/L 1 0.067 0.50 5A06013 EPA 8260B/6230D 01/06/15 16:42 MSz 1,2-Dib omo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:42. MSz 1,2-Dib omoethane1106-93-4]^ < 0.27 ug/L 1 0.27 0.50 5AO6013 EPA 82608/6230D 01/06/15 16:42 MS7. 1,2-Dic lorobenzene[95-50-1]^ < 0.062 ug/L 1 0.062 0.50 5A06013 EPA 8260B/6230D 01/06/15 16:42 MS7. 1,2-Dichloroethane[107-06-21^, < 0.082 ug/L 1 0.082 0.50 - 5A06013 EPA 8260B/6230D 01/06/15 16:42 MSZ 1,2-Dic loropropane (78-87-5]^ < 0.098 ug/L 1, 0.098 0.50 5A06013 'EPA 8260B16230D 01/06/15 16:42 MSz 1,3,5-T1l!rimethylbenzene[108-67-8]^ < 0.10 ug/L 1 0.10 0.50 5AO6013 FPA 826OB16230D 01/06115.16:112 MSZ 1,3-Dichlorobenzene (541-73-1]^ < 0.092 ug/L' 1 0.092 0.50 5A06013 -EPA 82606/6230D 01/06/15 16:42 MSz 1,3-Dic loropropane[142-28-9]^ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 8260B/6230D 01/06/15 16:42 MSz 1,4-Dic ilorobenzene,[106-46-71^ < 0.10 ug/L 1 0.10 0.50, 5A06013 EPA 826OB/6230D 01/06/15 16:42 MSZ 2,2-Di loropropane[594-20-71^ < 0.12 ug/L 1 0.12 0.50 5A06013 EPA 8260B/6230D 01/06/15 16:42 MSZ 2-Chlonotoluene[95-49-8)^ < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:42 MSz 4-Chlo otoluene[106-43-4)^ < 0.10 ug/L t 0.10 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:42 MSZ 4-Isop opyltoluene[99,-V-.61- < 0.066 ug/L 1 0.066 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:42 MSz Benze e[71-43-2]^ < 0.050 ug/L 1 0.050 0.50 5A06013 EPA 8260B/62.30D 01/06/15 t6:42 Msz Bromo enzene[108-86-1]^ < 0.13 ug/L 1 0.13 0.50 5A06013 EPA 82608/6230D 01/06/15 16:42 MSz Bromo hloromethane(74-97-5]^ < 0.11 ug/L 1. 0.11 0.50 5A06013 EPA 82608/6230D 01/06/15 16:42 MSZ Bromo lichloromethane [75-27-4]^ < 0.010 ug/L 1 0.010 0.50 SA06013 EPA 8260B/6230D 01/06/15 16:42 MSz Bromororm [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 5A06013 EPA 8260B/6230D 01/06/15 16:42 MSz Bromokethane[74-83-9]^ < 0.28 ugJL 1 0.28 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:42 MSz Carbo"I Tetrachloride [56-23-5]^ < 0.082 ug/L 1 : 0.082 - 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:42 MSz Chlorobenzene[108-90-7]^ < 0.069 ug/L 1 0.069 0.50 5A06013 EPA 8260B162.30D 01/06/15 15:42 MS7 Chlor4thane[75-00-3]^ < 0.18 ug/L 1 0.18 0.50 5A06013 EPA 8260B16236D 01/06/15 16:42 hlSz Chloroform [67-66.3]^ < 0.083 ug/L 1 0083 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:42 hlSz ChloroJmJ ethane [74-87-3]^ < 0.050 ug/L 1 6.050 O.SO SA06013 EPA 82608/6230D 01/06/15 16:42 MSz cis-1,2-Dichloroethene [156-59-2]^ < 0.075 ug/L 1 0.075 0.50 SA06013 EPA 8260B/6230D 01/06/15 16:42 M57. cis-1,3ILLDichloropropene [10061-01-5)^ < 0.073 ug/L 1 0.073 0.50 SA06013 EPA 8260B/6230D 01/06/1S 16:42 MSz Dibropi6chloromethane[124-48-1]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 8260B/6230D 01/06/1S 16:42 14Sz Dibrorliomethane [74-95.3]^ - < 0.13 ug/l. 1 0.13 0.50 SA06013 EPA 82606/6230D 01/06/1S 16:42 MSz Dichloiodifiuoromethane 175-71-81^ < 0.091 ug/L 1 0.091 0.50 5AO6013 EPA 826OB/6230D 01/06/15 16:42 h157- - EthylbeInzene[100-41.4)^ < 0.10 ug/L ' I. 0.10 0,50 SA06013 EPA 8260B16230D 01/06/15 L6:42 MSZ Hexachlorobut6diene (87-68-3]^ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 8260B/62300 01/06/15 16:42 MSz Isopropyl Ether [108-20-31^ < 0.20 ug/L ' 1 0.20 0.50 SAD6013 EPA 8260B/6230D 01/06/15 16:42 hlSz Isopr ylbenzene[98-82-8]^ < 0.13 ug/L 1 0.13 0.50 5A06013 EPA 8260B/6230D 01/06/15 16:42 MSZ m,p-X lenes[108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 SA06013 EPA 82606/6230D 01/06/1S 16:42 MSz Methyene Chloride [75-09-2]^. < 0.070 ug/L 1 0.070 0.50 5A06013 EPA 8260B/6230D 01/06/1S 16:42 MSz Methyl-tert Butyl Ether [1634,04 4]^ < 0.12 ugJL 1 0.12 0.50 5A06013 '5A06013 EPA B2608/6230D 01/06/15 16:4% MS Naphthalene [91-20-31^ < 0.086 ugJL 1 0.086 0.50 EPA 8260B/6230C� 01/06/15 i 6:42 M57. •4 FINAL - 1 This report relates only to the sample as received by the laboratory; and may only be reproduced in full. Page 6 0! 39 i s 4 � y www.encolabs.com ANALYTICAL RESULTS ription•. 141660-02 MW-20- Lab. SampleID:CS00133-02 Received: 01/05/1514:06 Matrix: Ground Water Sampled:12/31/14 11:37 Work Order: CS00133 Project: Genral Subcontract Sampled By: CLIENT Volatile Organic Compounds by GCMS ^ - f.NCO Cary certified ana/yte [NC 5911 AnalytI fCASNumber] Results Flaci Units DF MDL POL Batch Method Analyzed _By Notes n-Butyl/ senzene[104-51-8]^ < 0.074 ug/L 1 0.074 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:42 MSZ n-Propy] Benzene[103-65-1]^ < 0.073 ug/L 1 0.073 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:42 MSZ o-XylenE[95-47-6]^ < 0.088 ug/L 1 0.088 0.50 5AO6013 EPA 8260B/62300 01/06/15 16:42 MSZ sec-Butylbenzene[135-98-8]^ < 0.053 ug/L 1 0.053 0.50 5A06013 EPA 8260B16230D 01/06/15 16:42 h1SZ Styrene.[100-42-5]^. < 0.082 ug/L 1 0.082 0.50 5A06013 EPA 8260B/6230D 01/06/15 16:42 MSZ tert-Butylbenzene [98-06-6]^ < 0.094 ug/L 1 0.094 0.50 5A06013 EPA 8260B/6230D 01/06/15 16:42 MS7 Tetrachloroe[hene[127-18-4]^ < 0.099 ug/L 1 0.099 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:42 h1SZ Toluene[108-88-3]^ < 0.053 ug/L 1 0,053 0.50 SA06013 EPA 82608/6230D 01/06/15 16:42 MSZ 1 0.11 0.50 SA06013 EPA 8260B/6230D 01/06/15 16:42 MSZ trans-IJ2-Dichloroethene [156-60-5]^ < 0.11 ug/L trans -I [10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 5AO6013 EPA 8260B/6230D 01/06/15 16:42 MSZ Trichlorbethene[79-01-6]^ I3-Dichloropropene < 0.13 ug/L 1 0.13 0.50 SA06013 EPA 8260616230D 01/06/15 16:42 MSZ Trichlof ofluoromethane[75-69-4]^ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 8260B/6230D 01/06/15 16:42 MSZ. Vinyl c loride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 5A06013 EPA 8260B16230D 01/06/15 16:42 MSZ Xylene,(Total)[1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 5AO6013 EPA 82606/6230D 01/06/15 16:42 HSZ Results OF Spike Lvl % Re c °7o Rec Limits Batch Method Analyze d �gy Notes 58 I 50.0 116 % 53-136 5AO6013 EPA 8260816230C 01106115 16:42 A15Z 56 1 50.0 112 % 67-129 5AO6013 EPA 826OB16230C 01/06/15 16.-42 ^1517 59 1 50.0 119 % 59-134 5AO6013 EPA 82608/6230L 01106115 16:42 A/SZ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 39 r �Cam j4,V lw www.encolabs.com ANALYTICAL RESULTS Delcription• 141160-07 MW-24 Lab Sample ID:C500133-07 Received: 01/05/15 14:06 Matrix: -Ground Water Sampled:12/31/14 12:34 Work Order: C500133 Project: Genral Subcontract Sampled By:CLIENT IVblatile Organic Compounds by GCMS ^ • ENCO Cary certiried analyte [NC 591] Anal t CAS Number Results Flag Units DF MDL 4 Batch Method Analyzed Notes 1,1,1,2 etrachloroethane [630-20-6]^ < 0.091 ug/L 1 0.091 0.50 SA06013 EPA 8260B/623OD 01/06/15 19:08 MSz 1,1,1-T ichloroethane [71-55-6]^ ' < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 8260B/6230D 01'/06115 19:08 MSZ 1,1,2,2 Tetrachlordethane[79=34-5]^ < 0.085 ug/L 1 0.085 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:08 MSZ 1,1,2-T{1chloroethane [79-00-5]^ - < 0.068 ug/L 1 0.068 0.50 SA06013 EPA 82608/6230D 01/06/15 19:08 MSZ 1,1-0iciloroethane[75-34-3]^ < 0.050 ug/L 1 0.050 0.50 SA06013 EPA 8260B/623OD 01/06/15 19:08 MSZ 1,1-Dic hIloroethene[75-35-4]^ < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 826013/6230D 01/06/15 15:08 MSZ 1,1-Dic(1loropropene(563-58-61^ < 0.063 ug/L 1 0.063 0.50 5AO6013 EPA.8,260B/6230D 01/06/15 19:08 MSZ 1,2,3-T ichlorobenzene[87-61-6]^ < 0.25 ug/L 1 0.25 0.50 SA06013 EPA 8260B/6230D 01/06/15 19:08 MSz 1,2,3-Tichloropropane(96-18-4]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 82606/6230D 01/06/15 19:08 MS7. 1,2,4-Tichlorobenzene(120-82-1]^ < 0.097 ug/L 1 0.097 0.50 5A06013 EPA 8260B16230D 01/06/15 19:08 MSZ 1,2,4-Trimethylbenzene [95-63-6]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 8260B/6230D 01/06115 19:08 MSz 1,2 Dib�omo-3-chloropropane.(96.12-8]A < 0.48. ug/L 1 0.48 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:08 MSZ 1,2-Dib omoe[hane[106-93-4]^ < 0.27 ug/L 1 0.2.7 0.50 SA06013 EPA 8260B/62-3OD 01/06/15 19:08 MS7. 1,2-Dic lorobenzene[95-50-1]^ < 0.062 ug/L 1 0.062 0.50 5AO6013 EPA 6260B/62301) 01/06/15 19:08 MSz 1,2-Dic loroethane(10.7-06.2]^ < 0.082 ug/L . 1 0.082 0.50 5A06013 ,EPA 82608/6230D 01/06/15 19:08 MSz 1,2-Dic�loropropane[78-87-5]^ < 0.098 ug/L 1 0.098 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:08 MSz 1,3,5-T imethylbenzene 1108-67-81^ < 0.10 ug/L 1 0.10 0.50- 5A06013 EPA 8260B/62301) 01/06/15 19:08 MS7 -1,3-Dic ilorobenzene,[541-73-1]^ < 0.092 - ug/L 1 0,092 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:08 Msz 1,3-Dic loropropane (142-28-9]•` < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 8260B16230D 01/06/15 19:08 MSZ 1,4-Dic lorobenzene(106-46-7]^ < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 82608/6230D 01/06/15 19:08 MS7. 2,2-DiclIloropropane'[594-20-7]^ < 0.12 ug/L 1 0.12 0.50 5AO6013 EPA 82608/6230D 01/06/15 19:08 MS7 2-Chlolotoluene (95-49-8]^ < 0.10 ug/L 1 0.10 0.50 SA06013 EPA 82608/6230D 01/06/15 19:08 MSz 4-ChlorrllloItoluene[106-43-4]^ < 0.10 ug/L 1 -0.10 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:08 MSZ 4-lsopiopyltoluene(99-87-6]^ < 0.066 ug/L 1 0.066 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:08 MSZ Benzerje[71-43-2]^ < 0.050 ug/L 1 0.050 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:08 MSZ Brorn: enzene[108-86-1]^ < 0.13 ug/L 1 0.13 0.50 5AO6013 EPA 8260B/623OD 01/06/15 19:08 MSZ Brorn hloromethane[74-97-S]^ < 0.11 ug/L 1 0.11 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:08 MSz Brorn: ichloromethane [75-27-4,]A < 0.010 ug/L 1 0.010 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:08 MS7- Brorn orm (75-25-2]^ < 0.20 ug/L 1 0.20 0.50 5AO6013 EPA 8260B/6230D 01/06115 19:08 MSz Brorn ethane[74-83-9]^ < 0.28 ug/L 1 0.28 0.50 5AO6013 EPA 8260B/623OD 01/06/15 19:08 MSZ Carbon Tetrachloride (56-23-S]^ < 0.082 ug/L 1 0.082 0.50 SA06013 EPA 8260B/6230D 01/06/15 19:08 MSz. Chlorobenzene[108-90-7]^ < 0.069 ug/L 1 0.069 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:08 MS7. Chlorole thane [75-00-3]^ < 0.18 ug/L I 0.18 - 0.50 5AO6013 EPA 82608/6230D 01/06/15 19:08 MSZ Chloroform [67-66-3]^ < 0.083 ug/L 1 0.083 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:08 MSZ ChloroiiDichloropropene nethane[74-87-3]^ < 0.050 ug/L 1 0.050 0.50, 5A06013 EPA 82606/6230D 01/06/15 19:03 MSZ cis-1,Dichloroethene (156-59 2]^ < 0.075 ug/1. 1 0.075 0.50 SA06013 EPA 82.608/6230D 01/06/15 19:08 MS7 cis- 1,, [10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 5AO6013 EPA 8260B/623OD 61/06/15 19:08 MSZ Dibro ochloromethane.[124-48-1]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:08 MSZ Dibro omethane [74-95-3]^ < 0.13 ug/L 1 0.13 0.50 -5A06013 EPA 8260B/6230D 01/06/15 19:08 MSZ Dichlo [75-71-8]^ < 0.091 ug/L 1 0.091 0.50 5A06013 EPA 82606/62301) 01/06/15 19:08 MSZ Ethylbenzene(100 {Iodifluoromethane 41 4]^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 8260B/6230D ' 01/06/15 19:08 MSZ Hexachlorobutadiene [87-68-3]^ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 8260B/6230D 01/06/15 19:08 MSZ Isopro ylEther [108-20-3]^, < 0.20 ug/L 1 0.20 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:08 MSz Isopro ylbenzene [98-82-8]^ < 0.13 ug/L 1 0.13 0.50 5A06013 EPA 6260B/6230D 01/06/15 19:08 MSZ n1,p-Xylenes[108-38-3/106-42-3]^ < 0.18 ug/I. 1 0.18 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:08 MSZ ' Methylene Chloride [75-09-2]^ < 0.070 ug/L 1 0.070' , 0.50 - SA06013 'EPA 8260B16230D 01/06/15 19:08 MSZ Methy-tert-Butyl Ether [1634-04-4]A < 0.12 ug/I. 1 0.12 0.50 SA06013 EPA 8260B16230D 01/06/15 19:08 MSZ Napht ialene[91-20-3]^ < 0.086 ug/L 1 0.086 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:08 MSz FINALThis i report relates only to the sample as received by the laboratory, - and may only be reproduced in full. Page 16 of 39 www.encolabs.com ANALYTICAL RESULTS ription: 141660-07 MW-24 Lab Sample ID:C500133-07 Received: 01/05/1S 14:06 Matrix: Ground Water Sampled:12/31/14 12:34 Work Order: CS00133 Project: Genral Subcontract Sampled By:CLIENT IV�Iatile Organic Compounds by GCMS ^ - ENCO Cary certified analyze [NC 5911 I Results Flag Units DF MDL Batch Method Analyzed Note Analyte n-Butyl rCAS Number] Benzene(104-51-8]^ < 0.074 ug/L 1 0.074 0.50 5AO6013 EPA 826OB16230D 01/06/15 19:08 MSZ n-Propyl Benzene [103-65-1]^ < 0.073 ug/L 1 0.073 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:08 MSZ o-Xylerle(95-47-6]^ I < 0.088 ug/L 1 0.068 0.50 SA06013 EPA 8260B/6230D 01/06/15 19:08 MSZ sec-Butylbenzene[135-98-8]^ < 0.053 ug/L 1 0.053 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:08 MSZ Styrene[100 42 5]^ < 0.082 ug/L 1 0.082 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:08 MSZ to t-Bu,(100-42- [98 06.6]^ < 0.094 ug/L 1 0.094 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:08 MSZ. Tetraciloroethene[127-18-4]^ < 0.099 ug/L 1 0.099 0.50 SA06013. EPA 82608/6230D O1/06/15 19:08 h15Z Toluen2[108-88 3]^ < 0.053 ug/L 1 0.053 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:08 h1SL trans- lI,2-Dichloroethene [156-60-5]^ < 0.11 ug/L 1 0.11 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:08 MSZ- trans ( -Dichloropropene[10061-02-6]'^ < 0.080 ug/L 1 0.080 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:08 MSZ Trichlo oethene[79-01-6]^ < 0.13 ug/L 1 0.13 0.50 5AO6013 EPA 82606/6230D 01/06/15 19:08 MSZ Trichlo ofluoromethane (75-69-4]^ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 8260B/6230D 01/06/15 19:08 MSZ Vinyl c loride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 SA06013 EPA 8260B/6230D 01/06/15 19:08 MSZ_ Xylenes (Total) [1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:08 MSZ Results OF Spike Lv/ % Re c % Rec Limits Batch Method Analyze d By Notes 59 1 50.0 119 % 53-136 5AO6013 EPA 926OB16230r- 011061-15 19:08 MSZ 57 1 50.0 114 % 67-129 5AO6013 EPA 826OB16230C 01106115 19:08 11151, 61 1 50.0 122 % 59-134 5AO6013 EPA 8260816230L 01106115 19:08 A15Z FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 39 www.encolabs.com ANALYTICAL RESULTS 1 D cription: 14.1660=08. MW-25 Lab Sample ID:C500133-'08 Received: 01/05/15 14:06 Matrix: Ground Water -Sampled: 12/31/14 12:49 Work Order: C500133 Project: Genral Subcontract Sampled By: CLIENT (Volatile Organic Compounds by GCMS ^ - ENCO Cary ce,6 ed analyte (NC 591 J Anal 2 rCAS Numberl Tetrachloroethane [630-20-6]^ Results Fla_ a < 0.091 Units ug/L DF 1 MDL 0.091 POL 0.50 Batch 5AO6013 Method EPA 82608/6230D Analyzed 01/06/15 19:37 Ay Notes MSZ 1,1,1,2 1,1,1-Tichloroethane[71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:37 MSz 1,1,2,2 Tetrachloroethane [79-34-5]^ < 0.085 ug/L 1 0.085 0.50 .SA06013 EPA 8260B/6230D 01/06/15 19:37 MSZ 1,1,2-Tichloroethane[79.00-5]^ < 0.068 ug/L 1 0.068 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:37 MSz 1,1-Dic floroethane[75-34-3]^ < 0.050 ug/L 1 0.050 0.50 5A06013 EPA 82608/6230D 01/06/15 19:37 MSZ 1,1-Dic floroethene[75-35-4]^ < OAS ug/L 1 0.15 0.50 SA06013 EPA 82608/62301) 01/06/15 19:37 MSZ I,1-.Dichloropropene[563-58-61^ < 0.063 ug/L 1 0.063 0.50 - 5AO6013 EPA 82608/62301) 01/06/15 19:37 MSZ' 1,2,3-Tichlorobenzene(V-61-6]^ < 0.25 ug/L 1 0.25 0.50 SA06013 EPA 82608/62301) 01/06/15 19:37 MSZ 1,2,3-T-ichloropropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 82608/62301D 01/06/1-5 19:37 MSZ 1,2,4-T_ ichlorobenzene[120-82-1]^ < 0.097 ug/L 1 0.097 0.50 5AO6013 EPA 8260616230D 01/06/15 19:37 MSz 1,2,4- imethylbenzene (95-63-6]^ < 0.067 ug/L 1 0.067 0.50 5A06013 EPA 82606/6230D 01(06/15 19:37 M5Z 1,2-Di omo; 3-chloropropane, [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 SA06013 EPA 82606/62301) 01/06/15 19:37 h1S7- 1,2-Dib omoethane[106-9.3-4]^ < 0.27 ug/L 1 0.27 0.50 5A06013 EPA 82608/6230D 01/06/15 19:37 MSz 1,2-Dic lorobenzene[95-50-1]^ < 0.062 ug/L 1 0.062 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:37 MSz 112-Dic loroethane[107-06-2]^ < 0.082 ug/L 1 0.082 0.50 SA06013 EPA 8260B/6230D 01/06/15 19:37 MSz 1,2-Dic loropropane[78-87-5]^ < 0.098 ug/L 1 0.098 0.50 5AO6013 EPA 826OB/6230D 01/06/15 19:37 MSZ 1,3,5- imethylbenzene[108-67-8)^ < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 82606/6230D 01/06/15 19:37 M57- 1,3-Dic lorobenzene[541-73-11^ < 0.092 ug/L 1 0.092 0.50 5AO6013 EPA 8260B16230D 01/06/15 19:37 MSZ 1,3-Dic loropropane[142-28-9]^ < OAS ug/L 1 0.15 0.50 SA06013 EPA 8260B/6230D 01/06/15 19:37 MSZ 1,4-Dic lorobenzene[106-46-7]^ < 0.10 ug/L 1 0.10 0.50 SA06013 EPA 82608/62301) 01/06/15 19:37 MSZ 2,2-Dic loropropane[594-20-7]^ < 0.12 ug/L 1 0.12 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:37 MSZ 2-Chl0 Ptoluene[95-49-8]^ < 0.10 ug/L 1 0.10 - 0.50 5A06013 EPA 826013/6230D 01/06/15 19:37 MSz 4-Chlo toluene(106-43-4]^ < 0.10 ug/L 1 0.10 0.50 SA06013 EPA 8260B16230D 01/06/15 19:37 MSZ 4-(sop pyltoluene[99-87-6]^ < 0.066 ug/L 1 0.066 0.50 5AO6013 EPA 826013/62301) 01/06/15 19:37 MSZ Benze e[71-43-2]^ < 0.050 ug/L 1 0.050 0.50 5AO6013 EPA 8260B/62300 01/06/15 19:37 MSZ Bromo )enzene[108-86-1)^ < 0.13 ug/L 1 0.13 0.50 SA06013 EPA 82608/6230D 01/06/15 19:37 hlsz Bromo hloromethane [74.97-51A < 0.11 ug/L 1 0.11 0.50 5AO6013 EPA 82606/6230D 01/06i 15 19:37 MSz Bromo fichloromethane(75-27-4]^ < 0.010 ug/L 1 0.010 0.50 5AO6013 EPA 826013/6230D 01/06/15 19:37 MSz Bromolorm [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 SA06013 EPA 8260Bi6230D 01/06/1S 19:37 MSZ Bromo nethane[74-83-9]^ < 0.28 ug/L 1 0.28 0.50 5AO6013 EPA 82606/62301) 01/06/15 19:37 MSZ Carbon Tetrachloride[56-23-51^ < 0.082 ug/L 1 0.082 0.50 5AO6013 EPA 8260B16230D '01/06/15 19:37 MSz Chlorobenzene[108.90-7)^ < 0.069 ug/L 1 0.069 0.50 5AO6013 EPA 82606/6230D 01/06/15 19:37 MSz Chlorol thane [75-00-3]^ < 0.18 ug/L 1 0.18 0.50 5AO6013 EPA 826013/62301) 01/06/15 19:37 MSz Chloroflorm [67-66-3]A < 0.083 ug/L 1 .0.083 0.50 5A06013 EPA 82608/6230D 01/06/15 19:37 h1SZ Chlorotnethane[74-87-3]^ < 0.050 ug/1 1 0.050 0.50 5AO6013 EPA 826OB162300 01/06/15 19:37 MSZ cis-1,2 Dichloroethene [156-59-2]^ < 0.075 ug/L 1 0.075 0.50 5AO6013 EPA 8260B/6230D . 01/06/15 19:37 M57 cis-1,3 Dichloropropene110061-01-5]^ < 0.073 ug/L 1 -0.073 0.50 SA06013 EPA 8260B/6230D 01/06/15 19:37 MSZ Dibron ochloromethane[124-48-I]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 8260B16230D 01/06/15 19:37 MSZ Dibrorr omethane (74-95-3]A < 0.13 ug/L 1 0.13 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:37 MSZ Dichlo di0uoromethane[75-71-8]^ < 0.091 ug/L 1 0.091 0.50 5AO6013 EPA 826013/62301) 01/06/15 19:37 MSz Ethylb nzene[100-41-4]^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 8260B/62300 01/06/15 19:37 MSZ Hexac lorobutadiene[87-68-3]^ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 82608/6230D 01/06/15 19:37 MSZ Isopro ylEther [108-20-3]^ < 0.20 _ ug/L 1 0.20 0.50 SA06013 EPA 82608/6230D 01/06/15 19:37 M57-. Isopro ylbenzene[98-82-8]^ < 0.13 ug/L 1• 0.13 0.50 5AO6013 EPA 82608/6230D 01/06/15 19:37 MSZ m,p-X) lenes[108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 5A06013 EPA 82608/62301) 01/06/15 19:37 MSz Methyl ne Chloride[75-09-2]^ < 0.070 ug/L 1 0.070 0.50 5AO6013 EPA 82608/62.30D 01/06/15 19:37 MSZ Methyl tert-Butyl Ether [1634-04-4]^ < 0.12 ug/L 1 0:12 0:50 5AO6013 EPA 82608/62301) - 01/06/15 19:37 MSz Naphtlalene[91-20-31^ < 0.086 ug/L 1 0.086 0.50 5AO6013 EPA 826OB/6230D 01/06/15 19:37 M57 FINAL This, report relates only to the sample as received by the laboratory, and may only be"reproduced in full. Page 18 of 39 www.encolabs.com ANALYTICAL RESULTS ;cription: 141660-08 MW-25 Lab Sample ID:C500133-08 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 12:49 Work Order: C500133 Project: Genral Subcontract Sampled By: CLIENT latile Organic Compounds by GCMS ^ - ENCO Cary ce.4iled ana/yte [NC 591] n-Butyl Benzene [104-51-8]^ n-Prop I Benzene [103-65-1]^ o-Xylem [95-47-6]^ sec-Bu (benzene [135-98-B]^ Styrene [100-42-51^ tent-BuIylbenzene [98-06-6]^ TetrachIloroethene [127-J8-4]^ Tolueni108-88-3]^ trans-1 2-Dichloroethene [156-60-5]^ trans-1 3-Dichloropropene [10061-02-6]^ Trichloioethene [79-01-6]^ TrichlolPonuoromethane [75-69-4]^ Vinyl cloride [75-01-4]^ Xylene, (Total) [1330-20-7]^ Results < 0.074 < 0.073 < 0.088 < 0.053 < 0.082 < 0.094 < 0.099 < O.OS3 < 0.11 < 0.080 < 0.13 < 0.1s < 0.083 < 0.22 Flaa Units DF MDL PDL Batch Method Analyzed AM Notes ug/L 1 0.074 0.50 SA06013 EPA 8260B/6230D 01/06/15 19:37 MSZ ug/L 1 0.073 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:37 MSZ ug/L 1 0.088 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:37 MSZ ug/L 1 0.053 0.50 5A06013 EPA 8260B16230D 01/06/15 19:37 MSZ ug/L 1 0.082 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:37 MSZ ug/L 1 0.094 0.50 5A06013 EPA 8260B/6230D 01/06/15 19:37 MSZ ug/L 1 0.099 0.50 5A06013 EPA 82606/6230D 01/06/15 19:37 h1SZ ug/L 1 0.053 0.50 SA06013 EPA 8260B/6230D 01/06/15 19:37 NISI. ug/L 1 0.11 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:37 MSZ ug/L 1 0.080 0.50 5A06013 EPA 82606/62300 01/06/15 19:37 MSZ ug/L 1 0.13 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:37 MSZ ug/L 1 0.15 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:37 MSZ ug/L 1 0.083 0.50 5AO6013 EPA 8260B/6230D 01/06.115 19:37 N157- ug/L J 0.22 0.50 5AO6013 EPA 8260B/6230D 01/06/15 19:37 FlSZ Resultr DF Spike Lvl % Re c % Rec Limits Batch Method Analyzed By Notes 58 I 50.0 11796 53-136 5A06013 EPA 9260B16230C 01/06/15 19:37 AISZ 55 1 50.0 110 % 67-I29 5A06013 EPA 8260816230L 01/06/15 l9.,37 A15Z 61 1 50.0 123 % 59-134 5A06013 EPA 8260B16230L 01106115 19:37 AISZ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. _ Page 19 of 39 www.encolabs.com ANALYTICAL RESULTS Description: 141660.-05 ,MW-26 Lab Sample ID:C500133-05 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 12:16 Work Order: C500133 Project: Genral Subcontract Sampled By:CL1ENT IV�Iatile L Organic Compounds by GCMS ^ - ENCO CaryceRified analyre [NC 59I] . Anal CAS Numberl [630-20.6]^ Results Flag < 0.091 Units ug/L DF 1 MDL 0.091 PQL 0.50 Batch SA06013 EPA Method 8260B/6230D Analyzed 01/06/15 18:10 _By Notes MSZ 1,1,1,2IITetrachloroethane 1,1,1-Tiichloroethane[71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 8260B/6230D 01/06/15 18:10 MSZ 1,1,2,2.Tetrachloroethane[79-34-5]^ < 0.085 ug/L 1 0.085 0.50 5A06013 EPA 8260B/6230D 01/06/15 18:10 MSZ 1,1,2-Tiichloroethane [79-00.5]^ < 0.068 ug/L 1 0.068 0.50 5AO6013 EPA 82608/6230D 01/06/15 18:10 MR 1,1-Dichloroethane(75-34-3]^ < 0.050 ug/L 1 0.050 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:10 MS7. 1,1-Diciloroethene (75-35-4]A < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:10 MSZ 1,1-Dichloropropene(563-56.6]^ < 0.063 ug/L 1 0.063 0.50 5A06013 EPA 8260B/6230D 01/06/15 18:10 MSZ 1,2,3-T ichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0.25 0.50 SA06013 EPA 82608/6230D 01/06/15 18:10 MSZ 1,2,3-T ichloropropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.50. SA06013 EPA 8260B/6230D 01/06/15 18:10 MS7. 1,2,4-Tichlorobenzene(120782-1]^ < 0.097 ug/L 1 0.097 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:10 MSZ 1,2,4-Timethylbenzene.[95-63-6]^ < 0.067 ug/L 1 0.067 6.50 5AO6013 EPA 82608/6230D 01/06/15 18:10 - NSZ 1,2-Dib omo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 SA06013 EPA 826OB16230D 01/06/1S 18:10 M11SZ 1,2-Dib omoethane(106-93-4]^ < 0.27 ug/L 1 = 0.27 0.50 5A06013 EPA 8260B16230D 01/06/15 18:10 MSZ 1,2-DicI lorobenzene[95-50-1]^ < 0.062 ug/L 1 0.062 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:10 MSZ 1,2-Dichloroethane(107-06-2]^ < 0.082 ug/L 1 0.082 0.50 SA06013 EPA 8260B/6230D 01/06/15 18:10 MSZ 1,2-Dicllhloropropane(78-87-5]^ < 0.098 ug/L 1 0.098 .0.50 5A06013 EPA 82608/6230D 01/06/15 18:10 MS7 1,3,5-T imethylbenzene [108-67-81A < 0.10 ug/L 1 0.10 0.50 SA06013 EPA 6260B162.300 01/06/15 18:10 MSZ 1,3-Dic ilorobenzene[541-73-1]^ < 0.092 ug/L 1 0.092 0.50 5AO6013 EPA 8260B16230D 01/06/15 18:10 Msz 1,3-Dic floropropane(142-28-9]A < 0.15 ug/L t 0.15 0.50 5A06013 EPA 826013/6730D .01/06/15 13:10 I'lS2 1,4=Dic ilorobenzene(106-46-7]^ < 0.10 ug/L 1 0.10 0.50 - 5A06013 EPA 82603/6230D 01/06/15 18:,1D MSZ 2,2-Dic loropropane(594-20-7]^ < 0.12 ug/L 1 0.12 0.50 5AO6013 EPA 8260B16230D 01/06/15 18:10 MS7. 2-Chlor toluene[95-49-81^ < 0.10 ug/L 1 0.10 0.50 SA06013 EPA 82608/6230D 01/06/15 18:10 MS2 4-Chlor toluene[106-43-4]^ - < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:10 MSZ 4-Isopr pyltoluene[99,-87-6]^ < 0.066 ug/L 1 0.066 0.50 SA06013 EPA 8260B/6230D 01/06/15 18:10 MSZ Benzen [71-43-2]^ < 0.050 ug/L 1 0.050 0.50 5A06013 EPA 82608/6230D 01/06/15 18:10 MSZ Bromot enzene[108-86-1]^ < 0.13 ug/L 1 0.13 0.50 5A06013 EPA 82608/6230D 01/06/15 18:10 MSZ Bromo hloromethane[74-97-5]^ < 0.11 ug/L 1 0.11 '0.50 5A06013 EPA 8260B/6230D 01/06/15 18:10 MSZ Bromo ichloromethane (75-27-41^ < 0.010 ug/L 1 0.010 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:10 MSZ BromoI rm [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 5AO6013 EPA 82606/62300 01/06/15 18:10 MSZ Bromorhethane[74-83-9]^ < 0.28 u9/L 1 0.28 0.50 5A06013 EPA 8260B/6230D 01/06/15 18:10 MSZ Cat nlTetrachloride [56-23-53^ < 0.082 ug/L 1 0.082 0.50 5A06013 EPA 8260B/6230D 01/06/15 I8:10 MS7- Chlorol}enzene[106-90-7]^ < 0.069 ug/L 1 0,069 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:10 MS7- Chlorithane[75-00-3J^ < 0.18 ug/L 1 0.18 0.50 5A06013 EPA 826013/6230D 01/06/15 18:10 . MSZ Chlorolbrm [67-66-3]A < 0.083 ug/L 1 0.083 0.50 5A06013 EPA 8260B/6230D 01/06/15 18:10 MSz Chlorollethane(74-87-3]^ < 0.050 ug/L 1 0.050 - 0.50 5A060i3 EPA 82.60B/62301) 01/06/15 18:10 MSZ cis=1,2-Dichloroethene [156.59-2]^ < 0.075 ug/L 1 0.075 0.50 5AO6013 EPA 82606/6230D 01/06/15 18:10 MSZ cis- 1,3-Dichloropropene[10061-01-5]^ < 0.073 ug/L 1. 0.073 0.50 SA06013 EPA 8260B/6230D 01/06/15 18:10 MSZ Dibromochloromethane [.124-48-1]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 82608/62301) 01/06/15 18:10 MSZ Dibro omethane [74-95-3]^ < 0.13 ug/L 1 0.13 0.56 5AO6013 EPA 8260B/6230D 01/06/15 18:10 MSZ Dichlor difluoromethane[75-71-8]^ < 0.091 ug/L 1 .0.091 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:10 MS7. Ethylb nzene[100-41.4]^ < 0.10 ugjL .1 0.10 0.50 5A06013 EPA 8260B/6230D 01/06/15 18:10 MSZ Hexac lorobutadiene[87-68-3]^ < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 82605/6230D 01/06/15 13:10 MSZ IsoproIyl Ether (108.20-31^ <:0.20 ` ug/L 1 0.20 0.50 SA06013 EPA 82600/62301D 01/06/15 18:10 MS7 Isopro y1benzene[98.82-8]^ < 0.13 ug/L 1 0.13 0.50 5A06013 EPA 8260B/6230D 01/06/15 18:10 MS7 m,P-X enes[10.8-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 -0.50 SA06013 EPA-8260B/62300 01/06/15 18:10 MSZ Meth yl)Ine Chloride(75-09-2]^ < 0.070 ug/L 1 0.070 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:10 MSZ Methylltert-Butyl Ether(1634-04-4]^ < 0.12 ug/L 1 0.12 0.50 5A06013 EPA 8260B/6230D 01/06/15 18:10 MSZ Naphthalene[91-20-31^ < 0.086 ug/L 1 0.086 0.50 .5A06013 EPA 8260B/6230D 01/06/15 18:10 M57. FINAL. phis report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 39 ANALYTICAL RESULTS cription: 141660-05 MW-26 Lab Sample ID: C500133-05 Matrix: Ground Water Sampled:12/31/14 12:16 Project: Genral Subcontract Sampled By: CLIENT latile Organic Compounds by GCMS A - ENCO Cary ceniried analyte [NC 591] n-ButyllBenzene [104-51-8]^ n-Propyl Benzene [103-65-1]^ o-XYIenIe [95-47-6]^ sec-13-�lbenzene [135-98-8]^ Styrene [100-42-5]1, tert-Butylbenzene [98-06-6]^ TetrachIloroethene [127-18-4]^ i'oluene [108-88.3]^ Vans-1�2-Dichloroethene [156-60-5]^ i trans-lf3-Dichloropropene [10061-02-6]^ Trichlo oethene [79-01.6]^ Trichlo olluoromethane [75-69-4]^ Vinyl c loride [75-01-4]^ Xylene, (Total) [1330-20-7]^ Results Flaa Units DF MDL POL < 0.074 ug/L 1 0.074 0.50 < 0.073 ug/L 1 0.073 0.50 < 0.088 ug/L 1 0.088 0.50 < 0.053 ug/L 1 0.053 0.50 < 0.082 ug/L 1 0.082 0.50 < 0.094 ug/L 1 0.094 0.50 < 0.099 ug/L 1 0.099 0.50 < 0.053 ug/L 1 0.053 0.50 < 0.11 ug/L 1 0.11 0.50 < 0.080 ug/L 1 0.080 0.50 < 0.13 ug/L 1 0.13 0.50 < 0.15 ug/L 1 0.15 0.50 < 0.083 ug/L 1 0.083 0.50 < 0.22 ug/L 1 0.22 0.50 Results DF Spike L yl % Rec % Rec Limits 60 1 50.0 120 010 53-136 57 1 50.0 115 % 67-129 60 i 50.0 119 % 59-134 R� www.encolabs.com Received: 01/05/15 14:06 Work order: C500133 Batch Method Analyzed 5A06013 EPA 8260B/6230D 01/06/15 18:10 SA06013 EPA 826013/6230D 01/06/15 18:10 5AO6013 EPA 8260B16230D 01/06/15 18:10 5AO6013 EPA 826013/6230D 01/06/15 18:10 SA06013 EPA 826013/6230D 01/06/15 18:10 SA06013 EPA 826013/6230D 01/06/15 18:10 SA06013 EPA 8260B/6230D 01/06/15 18:10 5A06013 EPA 8260B/6230D 01/06/15 18:10 5AO6013 EPA 82608/6230D 01/06/15 18:10 5AD6013 EPA 82606/6230D 01/06/15 18:10 SA06013 EPA 8260B/6230D 01/06/15 18:10 SA06013 EPA 82608/6230D 01/06/15 18:10 5AO6013 EPA 82608/6230D 01/06/15 18:10 5A06013 EPA 8260B/6230D 01/06/15 18:10 Batch Method Analyzed 5A06013 EPA 8260B162301- 01106115 18-•10 5A06013 EPA 8260B16230C 01106115 IR.'10 5A06013 EPA 8260816230L 01106115 18:10 By Notes MSz MSz MSz MSz MSz MSz MSz hlSz MSz MSz MSz hlSz MSz MSz By Notes Af57. P157 � 157 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full, i'39e 13'If 39 14 1 www.encolabs.com ANALYTICAL RESULTS Description: 141660-03 MW-27 Lab.Sample ID:C500133-03 Received: 01/05/15 14:06 matrix: Ground Water Sampled:l2/31/14 11:57 Work Order: C500133 Project: Genral Subcontract Sampled By: CLIENT (Volatile Organic Compounds by GCMS ^ - ENCO Cary Certified analyte-[NC 591] Analvte fCAS Numberl Results Flag Units DF MDL Batch Method Analyzed Notes 1,1,1,2-,Tetrachloroethane [630-20-6]^ < 0.091 ug/1- 1 0.091 0.S0 5AO6013 EPA 6260B/6230D 01/06/15 17:11 r•1S7 1,1,1-Tlichloroethane [71-55-6]^ < 0.15 ug/L 1 0:15 0.50 5AO6013 EPA 826013/6230D 01/06/15 17:11 MS7 1,1,2,2 Tetrachloroethane [79-34-5]^ < 0.085 - ug/L 1 0.085 0.50 - . SA06013 EPA 8260B/6230D 01/06/15 l7:11 MSZ 1,1,2-Trichloroethane (79-00>5)^ < 0.068 ug/L 1 0.068 0.50 -5A06013 EPA 82606/6230D 01/06/15 1/:11 MSZ 1,1-Dichloroettiane [75 34-3]^ < 0.050 ug/L 1 0.050 0.50 SA06013' EPA 8260B/6230D 01/06/15 17:11 MSZ 1,1-Dichloroethene (75-35-4]^ < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 8260B/6230D 01/06/I5 17:11 MSZ 1,1-Dichloropropene[563-58-61^ < 0.063 ug/L 1 0.063 0.50 5A06013 EPA 8260B/6230D 01/06/15 17:11 MSZ 1,2,3-Trichlorobenzene [87-61-6]1 < 0.25 ug/L 1 0.25 0.50 SA06013 EPA 82608/6230D 01/06/15 17:11 MSZ 1,2,3-Tiichloropropane [96-18-4]^ < 0.15 ug/L 1 - 0.15 0.50 5AO6013 EPA 8260B/6230D 01/06/15 17:11 MSZ 1,2,4 Trichlorobenzene[120 82 1]^ < 0.097 ug/L i 0.097 0.50 5AO6013 EPA 8260B/6230D 01/06/15 17:11 MSZ " 1,2,4-Tiimethylbenzene [95 63 6]^ < 0.067 ug/L 1 b.067 0.80 ` 5AO6013 EPA 8260B/6230D 01/06/15 17:11 MSZ 1,2-Dibromo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 5A06013 EPA 82608/6230D 01/06/15 17:11 I.15Z 1,2-D14omoethane(106-93-4)^ < 0.27 ,ug/L 1 0.27 0.50 5A06013 EPA 8260B/6230D 01/06/15 17:11 MS7 i 1,2-Dichlorobenzene [95-50.1.1^ < 0.062 ug/L• 1 0.062 0.50 . SA06013 EPA 8260B/6230D 01/06/15 17:11 MSZ 1,2-Dichloroethane(107-06-21^ < 0.082 ug/L 1 0.082 0.50 5AO6013 EPA 8260B/6230D 01/06/15 17:11 MSZ 1,2-Dichloropropane[78-87-5]^ < 0.098 ug/L- 1 0.098 0.50 5A06013 FPA 826013/62301) 01/06/15 17:11 MS7 1,3,5-Tiimethylbenzene [108-67-8]^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 82608/6230D 01/06/15 17:IA MSZ 1,3-Dicp}lorobenzene [541-73-1]•` < 0.092 u9/L 1 0.092 0.50 SA06013 EPA 8260B/6230D 01/06/I5 17:11 MSZ 1,3-Dichloropropane [142-28-91^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 8260B/6230D 01/06/15 17:11 MSZ 1,4-DiclllhI�lorobenzene [106.46-7]^ < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 82606/6230D 01/06/15 17:11 MSZ < 0.12 ug/L" 1 0.12 0.50 5A06013 EPA 8260B/6230D 01/06/15 17:11 MSZ 2,2-Dichloropropane[594-20-7]^ 2.Chloro[oluene (95-49-8]^ < 0.10 ug/L 1 0.10 0.50 SA06013 EPA 826013/62301) 01/06/15 17:11 h1SZ 4-Chlorotoluene[106-43-4]^ < 0.10 ug/L 1 0:10 A.50 5AO6013 EPA 82.608/6230D 01/06/15 17:11 MSZ 4-Isopropyltoluene [99-87-6]^ < 0.066 ug/L 1 0.066 0.50 5A06013 EPA 82608/6230D 01/06/15 17:11 MSZ Benzene [71-43-2]^ < 0.050 ug/L 1 .0.050 0.50 5A06013 EPA 82.606/62.300 01/06/15 17:11 MSZ Bromobenzene[108-86-11^ < 0.13 ug%L 1 0.13 0.50 5AO6013 EPA 82608/6230D - 01/06/15 1-7:11 MSZ Bromochloromethane 174-97-51^ < 0.11 ug/L 1 0.11 0.50 5AO6013 EPA 8260B/6230D 01/06/15 17:11 MSZ 0romodichloromethane [75 27 .4]^ < 0.010 ug/L i 0.010 0.50 5A06013 EPA 82606/6230D 01/06/15 17:11 MSZ 8romoform [75-25-21^ , < 0.20 ug/L 1 - 0.20 0.S0 5AO6013 EPA 6260B/6230D 01/06/15 17:11 MSZ Bromornethane[74-83-93^ < 0.28 ug/L 1 0.28 0.50 SA06013 EPA 82606/6230D . 01/06/15 17:11 MSZ CarbonI'Tetrachloride [56.23-5]'• < 0.082 ug/L 1 0.082 0.50 5AO6013 EPA 82606/6230D 01/06/15 17:11 M57- Chlorobenzene [ 108-90- 71^ < 0.069 utj/L 1 0.069 0.50 5AO6013 EPA 82.60B/62300 01/06115 17:11 M57 -Chloroethane[75-00-3]A < 0.18 ug/L 1 0.18 0.50 5AO6013 EPA 82608/62301) 01/06/15 17:11 MSZ chloroform [67c66-3]^ ug/L 1 0.083 0.50 5A06013 EPA 82606/6230D 01/06/15 11:11 I.15Z Chloromethane[74-87-3]^ ug/L 1 0.050 0.50 5A06013 EPA 82.60B/6230D 01/06/15 17:11 MSZ cis-1,2IDichlorcethene [156-59-2]^. < 0.075 big/L 1 0.075 0.50 SA06013 EPA 8260B/6230D 01/06/15 17:11 MSZ cis-1,3(Dichloropropene[10061-01-5]^ < 0.073 ug/L 1. 0.073 '0.50 5A06013 EPA 8260B/6230D 01/06/15 17:11 MSZ Dibronr [124-48-1]^ < 0.067 big/L 1 0.067 0.50 , 5A06013 EPA.8260B/6230D 01/06/15 17:11 MsZ llochloromethane m Dibroomethane [74-95-31^ < 0.13 ug/L 1 0.13 0.50 SA06013 EPA 8260B/6230D 01/06/15 17:11 MS7 DichlorodiFluoromethane[75-71.81^ < 0.091 ug/L I 0.091 0.50 5A06013 EPA 8260B/6230D 01/06/15 17:11 MsZ Ethylbenzene [100-41-4]^ < 0.1b ug/L 1 0.10 0.50 5A06013 EPA b260B/6230D O1/06l15 17:11 MSZ Hexaclilorobutadiene [87.68-3] ` < 0.15 ug/L-- 1 0.15 0.50 5A06013 EPA 82606/6230D 01/06/15 1/:11 MSZ Isopropvl Ether[108-20-31A < 0.20 ug/1- 1 '0.20 0.50 5A06013 EPA 8260B/62301) 01/06/15 17:11 MS7 Isopropylbenzene[98-82-8]A < 0.13 ug%L. 1 0.13 0.50 5AO6013 EPA 8260B/6230D 01/06/15 17:11 MSZ m,p-Xylenes [108-38-3/106-4273]^ < 0.18 ug/L 1 0.18 0.50 5AO6013 EPA 8260B/623OD 01/06/15 17:11 MSZ Methylene Chloride[75-09-2]^ < 0.070 ug/L 1 0.070 0.50 SA06013 EPA 8260B/6230D 01/06/15 17:11 MSZ l Methyl-tort-0utyl Ether [ 1634-04-4]^ < 0.12-, ug/L 1 0.12 0.50 5A06013 EPA 8260B/6230D 01/06/15 17:11 MSZ , Naphthalene[91-20-3]^ < 0.086 •ug/L 1 0.096 0.50 5AO6013 'EPA 8260B/6230D 01/06/15 17:11 M57- FINAL This report relates only to the sample as recewed by the laboratory, and may only be reproduced in full. -. Page 8 of 39 rX www.encolabs.com ANALYTICAL RESULTS V Description: 141660-03 MW-27 Lab Sample ID:C500133-03 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 11:57 Work Order: C500133 Project: Genral Subcontract Sampled By:CLIENT (Volatile Organic Compounds by GCMS 1 ' ' - ENCO Cary certified analyte [NC 5911 Analyte rCAS Number l Results Flaa Units DF MDL Q Batch Method Analyzed By Notes n-Buty]lBenzene[104-51-8]^ < 0.074 ug/L 1 0.074 0.50 SA06013 EPA 82608/6230D 01/06/15 17:11 MS7 n-PropylBenzene [103-65-1]^ < 0.073 ug/L 1 0.073 0.50 5A06013 EPA 8260B/6230D 01/06/15 17:11 MSZ o-Xylene[95-47-6]^ < 0.088 ug/L 1 0.068 0.50 SA06013 EPA 8260B/6230D 01/06/15 17:11 NSZ sec-Burylbenzene(135-98-8]^ < 0.053 ug/L 1 0.053 0.50 5AO6013 EPA 8260B/6230D 01/06115 17:11 MSZ Styrene l[100-42-5]^ < 0.082 ug/L 1 0.082 0.50 5A06013 EPA 8260B/6230D 01/06/15 t7:11 MSZ tert-Butylbenzene[98-06-6]^ < 0.094 ug/L 1 0.094 0.50 5A06013 EPA 82608/6230D 01/06115 17:11 MSZ retrachloroethene [127-18-4]^ < 0.099 ug/L 1 0.099 0.50 SA06013 EPA 8260B/6230D 01/06/15 17:11 MSZ Toluene [108 88 3]^ trans-1,'2-Dichloroethene [156-60-5]^ trans- 0-Dichloropropene[10061-02-6]^ < 0.053 < 0.11 < 0.080 ugJL ug/L ug/L 1 1 1 0.053 0.11 0.080 0.50 0.50 0.50 5A06013 5AO6013 SA06013 EPA 8260B16230D EPA 8260B/6230D EPA 8260B/6230D 01/06/15 17:11 01/06/15 17:11 01/06/15 17:11 MSZ MSZ MSZ Trichloroethene[79-01-6]^ TrichloroFluoromethane [75 69 4]^ Vinyl chloride [75-01-4]^ < 0.13 < 0.15 < 0.083 ug/L ug/L ug/L 1 1 1 0.13 0.15 0.063 0.50 0.50 0.50 SA06013 5A06013 SA06013 EPA 826OB16230D EPA 8260B/6230D EPA 82.60B/6230D 01/06/15 17:11 01/06/15 t7:11 01/06/15 17:11 MSZ MSZ I.1S7. Xylenes (Total) [1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 SA06013 EPA 8260B/6230D 01/06/15 17:11 MSZ surrouates 4-BromoHuorobenzene Results 57 OF 1 Spike Lvl % Re c % Rec Lim Batch 5A06013 Method EPA 826OB16230C Analyzed 01106115 17:11 §y Notes A15Z 53-136 114 % 50.0 Dibromofluoromethane Toluene-d8 57 60 1 1 50.0 50.0 113 % 120 % 67-129 59-134 SA06013 5A06013 EPA 8Z60B/6230L EPA 826OB16230L 01/06/75 I7 I l 01106115 17:11 A157. AlSZ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 39 www.encolabs.com ANALYTICAL RESULTS �cription: 141660-09 MW-28 Lab Sample ID:C500133-09 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 12:54 Work Order: C500133 Project: Genral Subcontract Sampled By:CLIENT V latile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyt rCAS Number . etrachloroethane [630-20.6]^ Results Flaa < 0.091 Units ug/L DF 1 MDL 0.091 POL 0.50 Batch SA08010 EPA Method 82606/6230D Analyzed 61/08/15 13:48 By Notes MSZ 1,1,1,2 1,1,1-T�ichloroethane (71-55-6]^ < 0.15 ug/L 1 0.15 0.50" 5A08010 EPA 8260B/6230D 01/08/15 13:48 MSz 1,1,2,2-Tetrachloroethane [79-34-5]^ < 0.08S ug/L 1 0.085 0.50 5AO8010 EPA 8260B/6230D 01/08/15 13:48 MSz 1,1,2-Ttichloroethane [79-00-5]^ < 0.068 ug/L 1 0.068 0.50 SA08010 EPA 8260B/6230D 01/08/15 13:48 MSz I,1-DicMlloroethane[75-34-3]^ < 0.050 ug/L 1 0.050 0.50 5A08010 EPA 8260B/6230D 01/08/15 13:48 MSz 1,1-Did loroethene[75-35-4]^. < 0.15 ug/L 1 0.15 0.50 SA08010 EPA 8260B/6230D 01/08/15 13:48 MSz 1,1-Diclhloropropene [563-58-6]^ < 0.063 ug/L 1 0.063 0.50 SA08010 EPA 8260B/6230D 01/08/15 13:48 MSz 1,2,3-T ichlorobenzene (87-61-6]^ < 0.25 ug/L 1 0.25 0.50 SA08010 EPA 82606/6230D 01/08/15 13:48 MSZ 1,2,3-Tlichloropropane[96-18-4]^ < 0.15 ug/L 1 0.15 0.50 5AO8010 EPA 8260B/162300 01/08/15 13:48 MSZ 1,2,4-Ttichlorobenzene[120-82-1]^ < 0.097 ug/L 1 0.097 0.50 SA08010 EPA 82606/6230D 01/08/15 13:48 MSz 1,2,4-T�imethylbenzene[95-63-6]^ < 0.067 ug/L 1 0.067 0.50 5A08010 EPA 8260B/6230D 01/08/15 13:48 r•ISZ 1,2-Di1b omo-3-chloropropane [96-12-81" < 0.48 ug/L 1 0.48 0.50 5AO8010 EPA 82608/6230D 01/08/15 13:48 MSZ: 1,2-Dib omoethane(106-93-4]^, < 0.27 ug/L 1 0.27 - 0.50 5A08010 EPA 8260B/6230D 01/08/15 13:48 MSz 1,2-Dic lorobenzene[95-50-1]^ < 0.062 ug/L 1 0.062 . 0.50 5AO8010 EPA 8260B/6230D 01/08/15 13:48 MSZ 1,2-Dicf�loroethane [i07-06-2]^ < 0.082 ug/L 1 0.082 0.50 5AO8010 EPA 8260B/6230Q 01/08/15 13:48 I-ISZ 1,2-Dichloropropane[78-87-5]^ < 0.098 ug/L 1 0.098 0.50 SA08010 EPA 82600/6230D 01/08/15 13:48 MSz 1,3,5-Thmethylbenzene[108-67-8]^ < 0.10 ug/L- 1 0.10 0.50 5AO8010 EPA 82606/62300 01/08/15 13:48 MSz I 1,3-Dicilorobenzene [541-73-1]^ < 0.092 ug/L 1 0.092' 0.50- SA08010 EPA 8260B/62300 01/08/15 13:48 MSz 1,3-Dichloropropane[142-28-9]^ < 0.15 ug/L 1 0.15 0.50 5A08010 EPA 8260B/6230D 01/08/1S 13:48 r45z 1,4-Diclhlorobenzene[106.46-7]^ < 0.10 ug/L 1 0.10 0.50 5A08010 EPA 8260B/623DD 01/08/15 13:48 MSz 2,2-DicPoloropropane (594-20-7]^ < 0.12 ug/L 1 0.12 0.50 5A08010 EPA 8260B/6230D 01/08/15 13:48 MSz 2-Chlor toluene(95-49-8]^ < 0.10 ug/L 1 0.10 0.50 5AO8010 EPA 8260B/6230D 01/08/15 13:48 MSZ 4-Chlor . toluene[106-43-4]A < 0.10 ug/L 1 0.10 0.so 5AO8010 EPA 8260B/6230D 01/08/15 13:48 MSZ 4-Isopr pyltoluene [99-87-61^ < 0.066 ug/L 1 0.066 0.50 ' SA08010 EPA 8260B/6230D 01/08/15 13:48 MSz BenzeneI [71.43-2]^ < 0.050 ug/L 1 0.050 0.50 5AO8010 EPA 8260B/6230D 01/08/15 13:48 r4Sz Bromodenzene[108-86.1]^ < 0.13 ug/L 1 •0.13 0.50 SA03010 EPA 8260B/62300 " 01/08/15 13:48 MSZ BromocnIloromethane[74-97-5]^ < 0.11 ug/L ] '. 0.11 :0.50 5AO8010 EPA 8260B/6230D 01/08/15 13:48 rIsz Bromodichloromethane [75-27-4]^ < 0.010 ug/L 1 0.010 0.50 5AO8010 EPA 8260B16230D 01/08/15 13:48 I-ISZ Bromof rm [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 SA08010 EPA 8260B/6230D 01/08/15 13:46 MSZ Bromolethane[74-83-9]^ < 0.28 ug/L 1 0.28 0.50 5AO8010 EPA 8260B/6230D 01/08/15 13:48 MSz Carbon Tetrachloride [56.23-5]^ < 0.082 ug/L 1 0.082 0.50 SA08010 EPA 8260B/6230D 01/08/15 13:48 MS7 ChloroI nzene(108-90-7]^ < 0.069 ug/L 1 0.069 0.50 5AO8010 EPA 82.60B/6230D 01/08/15 13:48 MSz ChloroEthane[75-00-3]^ < 0.18 ug/L 1 ] 0.18 0.50 5AO8010 EPA 8260B/,6230D 01/08/15 13:48 MSZ Chlorof{ilbbIrm [67-66=3]^ < 0.083 ug/L ] 0.083 0.50 SA08010 EPA 8.260B/6230D *01/08/15 UAS MSZ Chloror ethane[74-87-3]^ < 0.050 ug/L 1. 0.050 0.50 5A08010 EPA 8260B/6230D 01/08/15 13:48 MSX cis-1,2- ichloroethene[156.59-2]^ < 0.075 ug/L 1 0.075 0.50 5AO8010 EPA 8260B/6230D 01/08/15 13:48 MSZ cis-1,3- ichloropropene[10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 5AO8010 EPA 826013/6230D 01/08/15 13:48 MSz Dibrom chloromethane[124-48-1]^ < 0.067 ug/L 1 0.067 0.50 SA08010 EPA 8260B/6230D 01/08/15 13:48 MSZ Dibrom methane[74-95-3]^ < 0.13 ug/L 1" 0.13 0.50 5A08010- EPA 8260B/6230D 01/08/15 13:48 MSZ Dichlor diFluoromethane[75-71-8]^ < 0.091 ug/L 1 0.091 0.50 5AO8010 EPA 82606/6230D 01/08/15 13:48 MSz Ethylbe zene [100-41-4]^ < 0.10 ug/L - 1 0.10 0.50 5A08010 EPA 82606/6230D 01/08/15 13:48 MSZ Hexach orobutadiene[87-68-3]^ < 0.15 ug/L 1 0.15 0.50 5AO8010 EPA 8260B/6230C ' 01/08/15 13:48 MSZ Isopropyl Ether[108-20-3]^ < 0.20 ug/L 1 0.20 0.50 SA08010 EPA 8260B/6230D 01/08/15 13:48 MSZ Isoproplylbenzene [98-82-8]^ < 0.13 ug/L '1 0.13 O.SO SA08010 EPA 82.608/6230D 0.1/08/15 13:4S MS7. m,p-Xylenes[108-38-3/106-42-3]^ " < 0.18 ug/L 1 0.18 0.50• 5A08010 EPA 826013/6230D 01/08/15 13:48 MSZ Methyl ne Chloride [75.09-2]^ < 0.070 ug/L 1 0.070 0.50 SA08010 EPA 82608/6230D 01/08/15 13:48 MSz Methyl- ert-Butyl Ether [1634-04-9]^ < 0.12 ug/L 1 0.12 0.50 5AO8010 EPA 8260B/6230D 01/08115 13:48 MSz Naphthalene[91-20-3]^ < 0.086 ug/L 1 0.086 .0.50 5AO8010 EPA 8260B/62300 01/08/15 13:48 MSZ. FINAL I This report relates only to the sample as received by the laboratory, . and may only be reproduced in full. I'age 20 of 3!� www.encolabs.com ANALYTICAL RESULTS �W :ription• 141660-09 MW-28 Lab Sample ID:C500133-09 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 12:54 Work Order: C500133 Project: Genral Subcontract Sampled By:CLIENT IV�Iatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte /NC 5911 Analvtk fCAS Numberl Benzene(104-51-8)^ Results < 0.074 Flag Units ug/L DF 1 MDL 0.074 POLL 0.50 Batch 5AO8010 Method EPA 8260B/6230D Analyzed 01/08/15 13:48 By Notes MSZ n-Butyl n-Prop IBenzene[103-65-1)^ < 0.073 ug/L 1 0.073 0.50 5AO8010 EPA 8260B/6230D 01/08/15 13:48 MSZ 0-Xyle (95-47-6]- < 0.088 ug/L 1 0.088 0.50 5AO8010 EPA 8260B/623ob 01/08/15 13:48 MSZ sec-Butylbenzene[135-98-8]^ < 0.053 ug/L 1 0.053 0.50 SA08010 EPA 8260B/6230D 01/08/1S 13:48 MSZ Styrene []00-42-5]^ < 0.082 ug/L 1 0.082 0.50 5AO8010 EPA 8260B/6230D 01/08/15 13:48 MSZ tert-Bu ylbenzene [98-06-6]^ < 0.094 ug/L 1 0.094 0.50 SA08010 EPA 8260B/6230D 01/08/15 13:48 MSZ- Tetrac loroethene(127-18-4]^ < 0.099 ug/L 1 0.099 0.50 5A08010 EPA 8260B/6230D 01/08/15 13:48 MSZ Toluene [108-88-3]^ < 0.053 ug/L 1 0.053 0.50 5AO8010 EPA 8260B/6230D 01/08/15 13:48 MSZ trans- 1`2-Dichloroethene[156-60-5]^ < 0.11 ug/L 1 0.11 0.50 5AO8010 EPA 82606/6230D 01/08/15 13:48 MSZ trans-1 3-Dichloropropene [10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 SA08010 EPA 82608/6230D 01/08/15 13:48 MSZ TrichlolIoethene[79-01-6)^ < 0.13 ug/L 1 0.13 0.50 5A08010 EPA 8260B/6230D 01/08/15 13:48 MSZ TrichloioFluoromethane[75-69-4]^ < 0.15 ug/L 1 0.15 0.50 SA08010 EPA 82608/6230D 01/08/15 13:48 MSZ Vinyl clloride [75-01-41^ < 0.083 ug/1- 1 0,083 0.50 SA08010 EPA 82608/6230D 01/08/15 13:48 MSZ Xylene Ttl) [1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 SA08010 EPA 8260B/6230D 01/08/15 13:•18 %ISZ Surro L-t""' ofluorobenzene Results 54 DF 1 Spike Lvl 50.0 % Re c 108 % 010 Rec Limits 53-136 Batch 5A08010 Method EPA 8260816130E Analyzed 01106115 13:48 AY Notes A15Z 4-8roa Dibroa ofluoromethane 53 1 50.0 106 % 67-129 5A08010 EPA 8260816230L 0110811513:48 AISZ Tnhran -r/R 58 1 50.0 117 % 59-134 5AO8010 EPA 826OB16230L 0110811513148 M5Z FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 39 www.encolabs.com ANALYTICAL. RESULTS :ription: 141660-06 MW-29 Lab Sample ID:C500133-06 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 12:26 Work Order: C500133 Project: Genral Subcontract Sampled By: CLIENT (Volatile Organic Compounds by GCMS { ^ - -NCO Cary cwtified ana/yfe (NC 591) - - - Anal(CAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed py Notes 1,1,1,2ITetrachloroethane[630-20-6]^ < 0.091 ug/L 1. 0.091 0.50 5A06013 EPA 82608/6230D 01/06/15 18:39 MSz 1,1,,1-Tiichloroethane (71-55-6]'• < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 82.608/6230D 01/06/15 18:39 MSz 1,1,2,2]Tetrachloroethane [79-34-5]^ < 0.085 ug/L 1 0.085 0.50 5A06013 EPA 8260B16230D 01/06/15 18:39 MSZ 1,1,2-Tichloroethane[79.00-5]^ < 0.068 ug/L 1 0.068 0.50 5A06013 EPA 8260B/6230D 01/06/15 13:39 MSZ 1,1-Dic < 0.050 ug/L 1 0.050 0.50 5AO6013 EPA'82608/6230D 01/06/15 18:39 MSZ lllhloroelhane[75-34-3]^ 1,1-Dichh!loroethene [75.35-4]^ < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 8260B/6230D 01/06/15 18:39 MSZ 1,1-Dic hloropropene[563-58-6]^ < 0.063 ug/L 1 0.063 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 MSz 1,2,3-Trichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0.25 0.50 SA06013 EPA 8260B/6230D 01/06/15 18:39 MSz. 1,2,3-Tiichloropropane[96-18,4]^ < 0.15 ug/L ] 0.15 0.50 y5AO6013 EPA 8260B/6230D 01/06/15 18:39 MSZ 1,2,4-TIichlorobenzene [120-82-1]^ < 0.097 ug/L 1 0.097 0.50 : 5A06013. EPA 8260B/6230D 01/06/1S 18:39 MSZ 1,2,4-Tr imethylbenzene[95.-63-6]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 826OB/62300 01/06/15 I8:39 MSZ 1,2-Dibl-omo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 MSZ 1,2-Dibomoethane[106-93-41^ < 0.27 ug/L 1 0.27 0.50 5A06013 EPA 82608/6230D 01/06/15 18:39 MSz 1,2-Dic florobenzene[95-50-1]^ < 0.062 ug/L 1 0.062 0.50 SA06013 EPA 8260B/6230D 01/06/15 18:39 MSz 1,2-Dic loroethane[107-06-2]A < 0.082 ug/L 1 0.082 0.50 SA06013 EPA 8260B/6230D 01/06/15 18:39 MSZ 1,2-Diciloropropane[78-87-5]^ < 0.098 ug/L 1 0.098 0.50 5A06013 EPA 826OB/6230D 01/06/15 18:39 MSZ 1,3,5-Trimethylbenzene[108-67-8]^ < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 82-608/6230D 01/06/15 18:39 M57. 1,3-Dic hlorobenzene[541-73-1]^ < 0.092 ug/L 1 0.092 0.50 5A06013 EPA 8260B/6230D 01/06/15 18:39 MSZ 1,3-Diclhloropropane [142-28-9]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 82608/62.30D 01/06/15 18:39 MR < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 h157- 1,4-DielIhlorobenzene (106-4677]^ 2,2-Di. loropropane[594-20-7]^ < 0.12 ug/L. 1 0.12 0.50 SA06013 EPA 8260B/6230D 01/06/15 18:39 Ms7- 2-Chlolotoluene[95-49-8]^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 8260B/6230D 01/06/15 18:39 MSZ 4-Chloiotoluene[106-43-4]^ < 0.10 ug/L ] 0.10 0.50 5A06013 EPA 82606/6230D 01/06/15 18:39 MSZ 4-Isoprffopyltoluene[99-87-6]^ < 0.066 ug/L 1 0.066 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 M5z Benzerie[71-43-2]^ < 0.050 ug/L 1 0.050 0.50 5A06013 EPA 8260B/62.30D 01/06/15 18:39 MSZ I Bromobenzene[108-86-1]^ < 0.13 ug/L 1 0.13 0.50 SA06013 EPA 8260B/6230D 01/06/15 18:39 MSZ BromolChloromethane [74-97-5]^ < 0.11 ug/L 1, 0.11 0.50 5AO6013 EPA 82608/62301) 01/06/15 18:39 h1SZ BromoltlIichloromethane [75-27-4]^ < 0.010 ug/L ] 0.010 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 MSZ Bromoform [75 25-2]^ < 0.20 ug/L 1 0.20 0.50 5AO6013 EPA 8260B16230D 01/06/15 18:39 MSZ Bmmol ethane[74.83-9]^ < 0.28 ug/L 1 U 28 0.50 5A06013 EPA 82606/6230D 01/06/15 18:39 MSz Carbor Tetrachloride [56-23-5]^ < 0.082 ug/L 1 0.682 0.50 SA06013 EPA 8260B/6230D 01/06/15 18:39 MSZ Chloro11116enzene[108-90-7]^ • < 0.069 ug/L 1 0.069 0.50 SA06013 EPA 8260B/6230D 01/06/15 18:39 MSZ Chloro{ethane[75-00-3]^ < 0.18 ug/L 1 0.18 0.50 SA06013 EPA 82608/6230D 01/06/15 18:39 MSZ Chloroform [67-66-3]^ < 0.083 ug/L 1 0.083 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 MSZ Chloronethane[74-87-3]^ < 0.050 ug/l. 1 0.050 0.50 SA06013 EPA 826OB/6230D O1/06/15 18:39 r•1S7 cis-1,2I Dichloroethene [156 59 2]^ <"0.075 ug/1- 1 0.075 0.50 5A06013 EPA 82608/6230D 01/06/15 18:39 M57. cis-1, Dichloropropene [16061-01-5]^ < 0.073 ug/L 1 '0.073 0.50 .,5AO6013 EPA 87.60B/6230D 01/06/15'18:39 MSZ Dibrorllochloromethane[124-48-1]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 32606/6230D 01/06/15 18:39 r4SZ Dibromome[hane [74-95-3] ^ < 0.13 ug/L 1 0.13 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 MS7 Dichloiodi0uoromethane[75'71-8]^ < 0.091 ug/L 1 0.091 0.50 5AO6013 EPA 82608/6230D 01/06/15 18:39 MSZ E[hylbenzene[100 41 4]^ c0.10 ug/L 1 0.10 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 MSZ Hexachlorobutadiene[87-68-3]^ < 0.15 ug/L 1 .0.15 0.50 5AO6013 EPA 8260B/62.30D 01/06/15 18:39 P'.Sz Isopropyl Ether[108-20-3]^ < 0.20 ug/L 1 0.20 0.50 5A06013 EPA 8260B/6230D 01/06/15 18:39 MSz IsoproIpylbenzene[98-82-8]^ < 0.13 ug/L 1 0.13 0.50 SA06013 EPA 82608/6230D 01/06/15 18:39 MSz m,p-X'lenes[108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 5A06.013 EPA 82608/6230D 01/06/15 18:39 MSL Methyllene Chloride[75-09-2]A < 0.070 ug/L 1 0.070 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 MSZ Methyl -tent -Butyl Ether [ 1634-04-4]^ < 0.12 ug/L 1 0.12 0.50 5AO6013 EPA 8260B16230D 01/06/15 18:39 MSz. Naphthalene[91-20-3]^ < 0.086 ug/L 1 0.086 0.50 5AO6013 EPA 82608/6230D 01/06/15 18:39 MSz. i FINAL- 1 This report relates only to the sample as received by the laboratory, and may only be reproduced in full.. - 'age 14 or 39 I f E [4N[�� C` G.. I www.encolabs.com I ANALYTICAL RESULTS srg�.v cription- 141660 06 MW-29 Matrix: Ground Water Lab Sample ID:C500133-06 Sam pied: 12/31/14 12:26 Received: 01/05/15 14:06 Work Order: CS00133 ! Project: Genral Subcontract Sampled By: CLIENT IV' latile Organic Compounds by GCMS I ^ - ENCO Cary certified ana/yte [NC 591) Anal vte rCAS Number] Results Flag Units DF MDL POL Batch Method Analyzed Ay Notes n-Butyl6enzene [104-51-8]^ < 0.074 ug/L 1 0.074 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 M57 n-PropyI Benzene [103-65-1]^ < 0.073 ug/L 1 0.073 0.50 5AO6013 EPA 8260B16230D 01/06/15 18:39 MSZ o-Xylene[95-47-6]^ < 0.088 ug/L 1 0.088 0.50 5A06013 EPA 82606/62300 01/06/15 18:39 MSZ sec-Butylbenzene(135-98-8]^ < 0.053 ug/L 1 0.053 0.50 5A06013 EPA 8260B/6230D 01/06/15 18:39 MSZ Styrene[100-42-5]^ < 0.082 ug/L 1 0.082 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 MSZ tert-Butylbenzene[98-06-6]^ < 0.094 ug/L 1 0.094 0.50 SA06013 EPA 8260B/62300 01/06/15 18:39 MSZ Tetrachloroethene(127-18-4]^ < 0.099 ug/L 1 0.099 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 MSZ Toluene(108-88-3]^ < 0.053 ug/L 1 0.053 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 MSZ trans-lj2-Dichloroethene [156-60-5]^ < 0.11 ug/L 1 0.11 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 MS7. brans- IJI3-Dichloropropene[10061.02-6]^ < 0.080 ug/L 1 0.080 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 F1SZ Trichlorbethene[79-01-6]^ < 0.13 ug/L 1 0.13 0.50 5AO6013 EPA 8260B/6230D 01/06/15 18:39 MSZ Trichlorbfluoromethane[75-69-4]^ < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 8260B/6230D 01/06/15 18:39 MSZ Vinyl chloride [75-01-4]^ < 0.083 ug/L 1 0.033 0.50 5A06013 EPA 8260B16230D 01/06/15 18:39 MSZ Xylenes (Total) [ 1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 SA06013 EPA 8260B/6230D 01/06/15 18:39 h1SZ i Surro ates Resu/ts OF Spike Lvl % Rec % Rec Limits Batch Method Analyzed Ay Notes 9-19rorrio/luorobenzene 59 1 50.0 118 % 53-136 5A06013 EPA 52606/6230L 0I/06/I5 /5:39 h15Z Dibromofluorornethane 58 1 50.0 116 96 67-129 5AO6013 EPA 82608/6230C 01106115 18:39 n9SZ Toluene-d8 61 1 50.0 122 % 59-13d 5AO6013 EP11 826OB16230L 01/06/I5 I3:39 415Z FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Paqe 15 of 39 www.encolabs.com ANALYTICAL RESULTS De$cription: 14166242 MW-31 Lab Sample ID:CS00132-12 Received: 01/05/15 14:06. Matrix: Ground Water Sampled:12/31/14 16:13 Work Order: CS00132 - Project: Genral Subcontract Sampled By: CLIENT Volatile Organic Compounds by GCMS ENCO Cary certi?IW analyte /NC 591] • ' Analyt�^rCASNumber] Results Flag Units DF. MDL Q Batch Method Analyzed gy Notes 1,1,1,21Tetrachloroethane[630-20-6]^ < 0.091 ug/L 1 0.091 0.50 5AO6013 EPA 82608/62301) 01/06/15 14:15 MSz - 1,1,1-Ttichloroethane [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 82608/6230D 01/06/15 14:15 MSZ 1,1,2,2!Tetrachloroethane (79-34-5)^ < 0.085 ug/L 1 0.085 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:15 MSZ 1,1,2-T ichloroethane [79-00-5]^ < 0.068 ug/L 1 0.068 0.50 5A06013 EPA 82608/6230D 01/06/15 14:15 MR 1,1-Dicl�loroethane [75-34-3]^ < 0.050 ug/L 1 0.050 0.50 5A06013 FPA 82608/6230D 01/06/15 1.1.15 M17 1,1-DichhIloroethene [75-35-4]^ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 826oi3/6230D 01/06/15 14:15 ' r•15Z 1,1-Dicploropropene[563-58-6]^ < 0.063 ug/L I 0.063 0.50 5A06013 EPA 8260B%62301) 01/06/15 14:15 MR 1,2,3-Trichlorobenzene (87-61-6]^ < 0.25 ug/L 1 0.25 0.50 5A06013 I -PA 82.60B/623OD' O1/06/15 I,:1:, MSL 1,2,3.Tiichloropropane (96-18-4]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 8260B/6230D 01/06/.15 14:15 MS7.. 1,2,4-4ichlorobenzene [120-82-1]^ < 0.097 ug/L 1 0.097 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:15 MSZ 1,2,4 Trimethylbenzene[95 63 6]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 8260B/6230D 01/06/15 14:15 MSZ 1,2-Digomo-3-chloropropane [96 12-8]^ < 0.48 ug/L 1 0.48 0.50 5AO6013 17PA 82.606/6230D 01/06/i5 14 15 PIS/ 1,2-DibFomoethane [106-93-4]^ < 0.27 ug/L 1 0.27 0.50 SA06013 EPA 826OB/6230D 01/06/15 14:15 MSZ 1,2-Dic�lorobenzene[95-50-1]^ < 0.062 ug/L 1 0.062 0.50 SA06013 EPA 8260B16230D 01/06/15 14:15 MSZ 1,2-Dic loroethane [][07-06-2]^ < 0.082 ug/L 1 0.082 0.50 SA06013 EPA 8260B/6230D 01/06/15 14:15 I.1SZ 1,2 Dic�lloropropane [78-87-5]^ < 0.098 ug/L 1 0.098 0.50 SA06013 EPA 8260B16230D . 01/06/15 14:1S MSZ 1,3,5-Trimethylbenzene [108-67-8]^ < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 82608/6230D 01/06/15 14:15 MS7. 1,3-Dichlorobenzene [541-73-1]^ < 0.092 ug/L I 0.092 0.50 5AO6013 EPA 82608/62301) 01/06/15 14:15 MSz 1,3-Dichloropropane [142-26-9]•^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 82600/6230D 01/06/15 14:15 MSZ 1,4-Dic lorobenzene[106.46-7]^ < 0.10 ug/L 1 0.10 0.50 SA06013 EPA 8260B/6230D 01/06/15 14:15 M57. 2,2-DidI loropropane[594.20-7]^ < 0.12 ug/L l 0.i2 0.50 5AO6013 EPA 826OB/6230D 01/0u/15 14:1., MSZ 2-Chlolotoluene(95-49-8]^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 82608/6230D 01/06/15 14:15 MSZ 4-Chlo Iotoluene [106 43 4]^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:15 14SZ 4-IsoP [99-87-6]^ < 0,066 ug/L 1 0.066 0.50 5AO6013 EPA 826OB/6230D 01/06/15 14:15 MSZ Iopyltoluene Benzer1e[71-43-2]^ < 0.050 ug/L 1 0.050 0.50 5AO6013 EPA 82606/6230D 01/06/15 14:15 MS7 Bromo enzene[108-86-1]^ < 0.13 ug/L 1 0.13 0.50 5AO6013 EPA 826OB/6230D 01/06/15 14:15 MSZ Brom(: (74-97-5]•^ < 0.11 ug/L 1 0.11 0.50 5AO6013 EPA 82608/6230D 01/06/15 14:15 MSz Ihloromethane Bromotlichloromethane [75-27-4]^ < 0.010 ug/L 1 0.010 0.50 SA06013 EPA 82608/6230D 01/06/15 11:15 r•15Z Bromoform [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 5AO6013 EPA 8.260B/6230D 01/06115 14:15 r•15Z Bromomethane [74-83.9]^ < 0.28 ug/L 1 0.28 0.50 5A06013 EPA 8260B16230D 01/06/15 14:15 Msz Carbor Tetrachloride[56-23-5]^, < 0.082 ug/L 1 0.082 0.50 5A06013 EPA 82606/6230D 01/06/15 14:15 MSz Chloro enzene [10B-90-7]^ < 0.069 ug/L 1 0.069 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:15 h1SZ Chlor thane(75-00-3]^ < 0.18 ug/L 1 0.18 0.50 5AO6013 EPA 8260B16230D .01/06/15 14:15 h15Z Chloro orm [67-66-3]^ < 0.083 ug/L 1 0.083 0.50 SA06013 EPA 8260B/6230D 01/06/15 14:15 MSz Chioromethane[74-87-3]^ < 0.050 ug/L 1 0.050 0.50 5AO6013 EPA 8260B/6230D 01/06/15 14:15 MS7. i cis- 1,Dichloroethene 2{- [156-59-2]^ - < 0.075 ug/L 1 0.075 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:15 MS7. cis-1,31IDichloropropene [1006.1-01-5]^ < 0.073 ug/L 1 0.073 0.50 _ 5AO6013 EPA 8260B/6230D 01/06/15 14:15 r•15Z Dibronlochloromethane [124-48-1]^ < 0.067 ug/L 1' 0.067 0.50 SA06013 EPA 82606/6230D 01/06/15 14:15 MSZ Dibron omethane [74-95-3]A < 0.13 ug/L 1 0.13 0.50 5A06013 EPA 82.60B/6230D 01/06/15 14:15 MSZ DichlJodi0uoromethane[75-71-8]^ < 0.091 ug/L 1 0.091 0.50 5AO6013 EPA 82606/6230D 01/06/15 14:15 MS7 Ethylb nzene[100-41•-4]^ < 0.10 ug/L 1 0.10 O.SO 5A06013 EPA 82608/62300 01/06/15 14:15 14SZ Hexachlorobutadiene (87-68'-3)^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 82608/6230D 01/06/15 14:15 MS'I_ Isopro yl Ether[108.20-3]^ < 0.20 ug/L 1 0.26 ' 0.50 SA06013 EPA 82608/62300 01/06/15 14:15 MS7. Isopro ylbenzene[98-82-8]^ < 0.13 ug/L 1 0.13 0.50 SA06013 EPA 8260B/6230D 01/06/15 14:15 t45Z m,p-Xylenes(108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 SA06013 EPA 82608/6230D 01/06115 14:15 I.15"l. Methyene Chloride[75-09-2]^ < 0.070 ug/L 1 0.070 0.50 SA06013 EPA 82608/6230D 01/06/15 14:15 M5Z Methy -tent-Butyl Ether[1634-04-4]^ < 0.12 ug/L 1 0.12 0.50 5A06013 EPA 82608/6230D 01/06/15 14:15 MSZ Napht alene(91-20-3]^ < 0.086 ug/L L O.OS6 0.50 5A06013 EPA 826OB/6230D 01/06/15 14:15 1.1SZ e i i This report relates only to the sample as received by the laboratory, and may only be reproduced in full. :'age lc u1 t FINAL i - ,w' �.S'-e��-zmamsadf� www.encolabs.com i ANALYTICAL RESULTS �cription: 141662-12 MW-31 Lab Sample ID:C500132-12 Received: 01/OS/15 14:06 Matrix: Ground Water Sampled:12/31/14 16:13 Work Order: C500132 Project: Genral Subcontract Sampled By: CLIENT IVblatile Organic Compounds by GCMS j ^ - ENCO Cary certified analyze [NC 591] n-ButylllBenzene [104-51-8]^ n-Prop)l Benzene [103-65-1]^ o-Xylere (95-47-6]1, sec-64lbenzene [135-98-8]^ styrene [100-42-5]^ tert-Butylbenzene [98-06-6]^ Tetrachloroethe.ne [127-18-4]^ Toluene (108-88-3]^ trans-l!2-Dichloroethene [156-60-5]^ trans-1 3-Dichloropropene (10061-02-6]^ Trichloioethene [79-01-6]^ Trichloiofluoromethane (75-69-4]^ Vinyl chloride (75-01-4]^ Xylene5 (Total) [1330-20-7]^ Surr ates 4-B(Or» Of/UOrObenZene Dibro7fluoromethane Iblue i -d8 I I Results Flag Units DF MDL PPOL Batch Method Analyzed Ay Notes < 0.074 ug/L 1 0.074 0.50 SA06013 EPA 826OB16230D 01/06/15 14:15 MS7. < 0.073 ug/L 1 0.073 0.50 5AD6013 EPA V.60B/6230D 01/06/15 14:15 ",157 < 0.088 ug/L 1 0.088 0.50 5AD6013 EPA 8260B/6230D 01/06/15 14:IS N1SZ < 0.053 ug/L 1 0.053 0.50 SA06013 EPA 82.608/6230D 01/06/15 14:15 i.IsZ < 0.082 ug/L 1 0.082 0.50 5A06013 EPA 82.608/6230D 01/06/15 1,115 MS7 < 0.094 ug/L 1 0.091 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:15 N1SZ < 0.099 ug/L 1 0.099 0.50 5A06013 EPA 82608/6230D 01/06/15 14:15 N1SZ < 0.053 ug/L 1 0.053 0.50 5A06013 EPA 82.60B/6230D 01/06/15 14:15 MS7 < 0.11 ug/L 1 0.11 0.50 5AO6013 EPA 826013/6230D 01/06/15 1-1:1S N152. < 0.080 ug/L 1 0.080 0.50 5A06013 EPA 8260B/6230D 01/06/15 1,1:15 MSZ < 0.13 ug/L 1 0.13 0.50 5AO6013 EPA 8260B/6230D 01/06/15 14:15 MSZ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 8260B16230D 01/06/15 14. 15 N15i: < 0.083 ug/L 1 0.083 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:15 MSZ < 0.22 ug/L 1 0.22 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:15 MSZ Results DF Spike Lv/ % Re c % Rec Lim itr Batch Method Ana/vzed By Notes 58 1 50.0 116 % 53-136 5A06013 EPA 8260816230L 011061115 14:1.5 A15T. 54 1 50.0 10916 67-129 5A06013 EPA 3260B116230L 01106,115 14:15 MSZ 58 1 50.0 117 % 59-134 5A06013 EPA V.60816230L O1106115 14.15 MS.7 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. rage 27 u1 a 1 eF,m� % 1 t'9 :ITS. z`'YLt www.encolabs.com ANALYTICAL RESULTS lcription: 141662-11 MW-32 Lab Sample ID:C500132-11 Received: 01/05/15, 14:06 Matrix: Ground Water Sampled:12/31/14 16:02 Work Order: C500132 Project: Genral Subcontract Sampled By:CLIENT JVbIati[e Organic Compounds by GCMS I ^ - ENC0 Cary certified analyre [NC 591] AnalvtL rCAS Numbed Results Flaa Units DF MDL PQL Batch Method Analyzed _By Notes 1,1,1,2�Tetrachloroethane[630-20-6]^ ." < 0.091 ug/L 1 O.b91 0.50 5A06013 EPA 8260B/6230D 01/06/15 13:45 MSz 1,1,1-T ichloroethane [71755-6]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:45 MSZ - 1,1,2,2�Tetrachloroethane (79-34-5]^ < 0.085 ug/L 1 0.085 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:45 ' MSZ 1,1,2-T ichloroethane [79-00-.5]" < 0.068 - ug/L 1 0.068 0.50 5A06013 EPA 8260B/6230D 01/06/15 11-15 M52 1,1-Dic floroethane[75-34-3]^ < 0.050 uq/L 1 0.050 0.50 5AO6013 EPA 826OB/62.30D 01/06/15 13:45 MS7 1,]-Diclhloroethene [75-35-9]^ < 0.15 u9/L 1 0.15 0.50 5A06013 EPA 8260B/6230D 0I/06/15 113:45 h157 1,1-D clhIloropropene[563.58-6]^ < 0.063 ug/L 1 0.063 0.50 SA06013 EPA 3260B/6230D O1/06/18 13:45 145z '1,2,3-Tiichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0.2.5 0.50 SA06013 EPA 82.606/6230D 01/06/15 13:-15 Ns/ 1,2,3-T�ichloropropane [96-18-4]^ < 0.15 ug/L 1 OAS 0.50 5A06013 EPA 8260B/62.30D 01/06/15 13:45 MS7. 1,2,4-Trichlorobenzene[120-82-1]^ < 0.097 . ug/L 1 0.097 0.50 SA06013 EPA 82608/6230D 01/06/15 13:45 h15Z 1,2,4-T{ imethylbenzene [95-63=6]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:45 Msz 1,2-Dib�omo-3-chloropropane (96-12-8)^ < 0.48 ug/L 1 0.48 0.50 SA06013 EPA 82608/6230D 01/06/15 13:45 ^t57 1,2-Diblromoethane [106793-41^ < 0.27 ug/L 1 0.27 0,50 5A06013 EPA 82.608/62.30D 01/06/15 13:45 MSz. 1,2-DiclhIlorobenzene [95-50-1]^ < 0.062 ug/L 1 0.062 0.50 5A06013 EPA 8260B/6230D 01/06/15 13:45 t:15Z 1,2-bici1oroethane(107.06-2)^ < 0.082 ug/L 1 0.082 0.50 5AO6013 EPA 826OB/6230D 01/06/15 13:45 MS7. 1,2-DicI loeopropane(78-87-51^ < 0.098 ug/L 1 0.098 0.50 SA06013 EPA 82608/6230D 01/06/15 13:45 t45Z 1,3,5-Tiimethylbenzene [108-67-8]^ < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 8260B16230D ' 01/06/15 13:45 MSZ 1,3-Dicplorobenzene[541-73-1]^ < 0.092 ug/L 1 0.092 0.50 5A06013 EPA 8260B/6230D 01/06/15 13:45 h1Sz 1,3-Dicllljlloropropane[142-28-9]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 8260P/6230D 01/06/15 13:45. MSZ 1,4-1 ilorobenzene [106-46-71^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 82606/6230D 01/06/15 13:45 1.1SZ 2,2-Dich Iloropropane [S94-20-7]A < 0.12 ug/L 1 0.12. 0.50 5A06013 EPA 826OB/6230D 01/06/15 13:•15 h157 2-Chlototoluene(95-49-8]^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 8260B/6230D 01/06/15 13:45 MSZ 4-ChloIotoluene(106-43-4)^ < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:45 MSz 4-Isopropyltoluene[99-B7-6]^ < 0.066 ug/L 1 0.066 0.50 5A06013 EPA 8260B/6Z30D 01/06/15 13:45 MSz Benze�e[71-43-2]^ < 0.050 ug/L 1 0.050 0.50 5AO6013 EPA 826OB/6230D 01/06/15 13:45 t45Z BromolbIenzene [108-86-1]^ < 0.13 ug/L 1 0.13 0.50 5A06013 EPA 8260B/6230D 01/06/15 13:45 MSZ Bromothloromethane [74-97-S]^ < 0.11 ug/L 7 0.11 0.50 '5A06013 EPA 8260B/6230D 01/06/15 11,15 h1SZ Bromo tlichloromethane[75.27-4]^ < 0.010 ug/L 1 0.010 0.50 5AO6013 EPA 826DR/6230D 01/06/15 13:45 MS7 Bromo brm [75-25-2]^ < 0.20 ug/L 1 0.20 ' 0.50 5AO6013 EPA 9260B/6230D 01/06/1511-IS MSZ Bromo nethane[74-83-9)^ < 0.28 ug/L 1 0.28 0.50 SA06013 EPA 8260B/6230D 01/06/15 11-15 hISL Carbor Tetrachloride [56-23-5]^ < 0.082 ug/L 1 0.082 0.50 5A06013 EPA 82608/6230D 01/06/15 13:45 MSz Chlorobenzene[108-90-7]^ II < 0.069 ug/L 1 0.069 0.50 5A06013 EPA 82.6OB/62.30D 01/06/15 13:45 M57 Chlorolthane[75-00.3]^ < 0.18 ug/L 1 0.18 0.50 SA06013 EPA 8260B/6230D 01/06/15 13:45 MSz Chloroform [67-66-3]^ < 0.083 ug/L 1 0.083 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:45 MSZ Chloro{n ethane [74-87-3]^ < 0.050 ug/L 1 0.050 0.50 5AO6013 EPA 8260816230D 01/06/15 13:45 MSZ cis-1,2.Dichloroethene [156-59-2]^. < 0.075 ug/L 1 0.075 0.50 5AO6013 EPA 8260B/6230D 01/06/15.13:45 h157 cis- 1,3-Dichloropropene[10061-01-5]^ < 0.073 ug/L -1 0.073 0.50 SA06013 EPA 8260B/6230D 01/06/15 13:45 MSZ Dibronli h1oromethane[124-48-1]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 8260B162300 01/06/15 13:45 MSz Dibrorf omethane [74-95-3]^ < 0.13 ug/L 1 0.13 0.50 5A06013 EPA 826OB/6230D , 01/06/15 13:45 h15Z Dichlo odifluoromethane [75-71-8]^ < 0.091 ug/L _ 1 0.091 ' 0.50 5A06013 EPA 82608/62-30D- 01/06/1'5 13:45 MSZ Ethylb,nzene[100-41-4]^ < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA B260B/6230D 01/06/15 13:45 MRHexaclhIlorobutadiene[87-68.3]A < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 82.60B/6230D 01/06/15 13:45 MSZ Isopr yl,Ether (108-20-3)^ < 0.20 ug/L 1 0.20 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:45 MSZ Isopr y1benzene[98-82-81^ < 0.13 ug/L 1 0.13 0.50 SA0601.3 EPA-8260B/6230D 01/06/15 13:45 MS7 m,p-X{denes[108-38-3/106-42-3)^ < 0.18 ug/L I 0.19 0.50 4A06011 EPA 826013/62300 01106/li 11,45 h1SZ Methyllene Chloride (7S-09-2)^ < 0.070 ug/L I 0.070 0.50 5A0601.3 EPA 8260B/6i30D 01/0t. I S 13:•IS :aSL Methy-tert-Butyl Ether[1634-04-41^ <0.12 ug/L 1 0.12 0.50 5AO6013 EPA 82.600/6230D 01/06/15 13:45 MSZ. Napht alene[91-20-3)^ < 0.086 ug/L 1 0.086 0.50 5A06013 EPA 82.60B/6230D 01/06/15 13:45 MS7 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. - Page 2' O1 --r..xcexr::-ib�>-�•::�e:�..c.».xvxvwrs•c� www.encolabs.com � ANALYfICALRESULTS I Description: 141662-11 MW-32 Lab Sample ID:C500132-11 Received: 01/05/15 14:06 i Matrix: Ground Water Sampled:12/31/14 16:02 Work order: C500132 Project: Genral Subcontract Sampled By: CLIENT (Volatile Organic Compounds by GCMS f ^ - £NCO Cary cartiried aralyte [NC 591] Analvte [CAS Numberl Results Flag Units DF MDL POL Batch Method Analyzed By Notes n-Butyl Benzene[104-51-81^ < 0.074 ug/L 1 0.074 0.50 5AO6013 EPA 82606/6230D 01/06/15 13:45 MS2 n-Prop�l Benzene [103-65-1]^ < 0.073 ug/L 1 0.073 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:45 MS7 o-XyleAe [95-47-6]^ < 0.088 ug/L 1 0.0BB 0.50 5A06013 EPA 82606/6230D 01/06/15 13:45 MSL sec-Rutylbenzene [135-98.8]^ < 0.053 ug/L 1 0.053 0.50 5A06013 EPA 82.60B/6230D 01/06/15 13:45 PlSZ Styrene [100-42-5]^ < 0.082 ug/L 1 0.082 0.50 5AO6013 EPA 82.60B/6230D 01/06/15 13:45 MS7. tert-Butylbenzene[98-06-6]A < 0.094 ug/L 1 0.094 0.50 5A06013 EPA 8260B/6230D 01/06/15 13:45 MS7 Tetrachloroethene[127-18-4)^ < 0.099 ug/L 1 0.099 0.50 SAD6013 EPA 8260B/6230D 01/06/15 13.45 MSL 'roluerte [108-88-3]^ < 0.0S3 ug/L 1 0.053 0.50 SA06013 i PA 8260B/62301) 01/06/IS 13 •1': r45/ transl! 2-Dichloroethene [156-60-5]^ < 0.11 ug/I 1 0.11 0.50 5AD6013 FPA 8260R/6230D 01/06/15 13:45 MS7 trans-1,3-Dichloropropene [10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 SA06013 EPA 8260B/6230D 01/06/15 13:45 MSZ Trichloroethene[79-01-6]^ < 0.13 ug/L 1 0.13 0.50 5A06013 EPA 8260B/6230D 01/06/15 13:45 MSZ Trichloirofluoromethane[75-69-4]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 8260B/62300 01/06/15 13W5 MS/ Vinyl chloride [75-01-4]^ < 0.083 ug/L 1 0.083- 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:45 M57 Xylene.L(Total)[1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:45 MSZ i Surrogates Results OF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed By Notes 4-Bromofluorobenzene 58 1 50.0 115 % 53-136 5AO6013 EPA 9260616230L 01106115 13:45 +lSZ Dibromofluoromethane 56 1 50.0 112 46 67-129 5AO6013 EPA 82606,16230L 01106115 13:45 A15Z 7-oluene-d8 I 59 1 50.0 118 % 59-134 5AO6013 EPA 8260816230C 01106115 13:45 1%157- FINAL This report relates only to the sample as received by the laboratory, and may only be reproauced in full. I- is L {alp ly fwww.encolabs.com f ANALYT'ICQL RESULTS _ De}cflption: 141662-10 MWr33 Lab Sample ID:C500132-10 Received: 01/05/15 14:06 • Matrix: Ground Water Sampled: 15:41 Work order. C500132 , Project: Genral Subcontract Sampled.By:CLIENT Volatile Organic Compounds by GCMS -^ - ENCO Cary Certified analyte [NC 591] Analvtel KAS Number Results Flag Units DF MDL PPOL Batch Method Analvzed By Notes i 1,1,1,21,Tetrachloroeth6ne[630-20-61^ < 0.091 ug/L 1 0.091 0.50 5AO5015 'EPA 82608/62301) 01/05/15 21:30 MSz 1,1,1-Trichloroethane(71-55-6]^ < 0.15 ug/L 1 0.15 .0.50 5AD5015 EPA 82606/6230D .01•/05/15 21:30 MS7- 1,1,2,2{Tetrachloroethane[79-34-5]^ < 0.085 ug/L 1 0.085 0.50 SA05015 EPA 8260B/6230D 01/05/15 21:30 MSz 1,1,2-T�ichloroethane [79-00-5]A <.0.068 ug/L 1 0.068 0.50' 5A05015 EPA 82.606/62301) 01/05/15 21:30 MSz 1,1 Dicf loroethane [75 3A-3]^ < 0.050 ug/L 1 0.050 0.50 5AO5015 EPA 32.608/6230D 01/05/15 21:30 MS7. 1,1-Diclftloroethene[75.35-4]^ < 0.15 ug/L 1 0.15 0.50 SA05015 EPA 8260B/62301) 01/05/15 21:30 MS7 1,1-Dichloropropene[563-58-6]^ < 0.063 - ug/L 1 0.063 0.50 SA05015 EPA 82608/6230D 01/05/15 21:30 MSL 1,2,3-Trichlorobenzene(87-61-61^ < 0.25 ug/L 1 0.25 0.50 5AO501S EPA 82608/6230D 01/05/15 21:30 msz 1,2,3-T1ichloropropane (96-18-4]^ < 0.15 ug/L 1 0.15 0.50" SA05015 EPA 8260B/6230D 01/05/15 21:30 h1SZ- 1,2,4-Trichlorobenzene[120 82-1]^ < 0.097 ug/L 1 0.097 0.56 5AO5015 EPA 8260B/623oo bl/05/15 21:30 MSZ 1,2,4 Trimethylbenzene (95 63 6)^ < 0.067 ug/L 1 0.067 6.50 5A05015 EPA 8260B/6230D 01/05/15 21:30 MSz 1,2-1)i4omo-3-chloropropane [96-12-8]^ < 0.48 ug/L - 1 0.48 0.50 5A05015 LPA 82608/6230D 01/05/15 21:30 htsz 1,2-Ditxomoethane[106-93-4]^ < 0.27 ug/L 1 - 0.27 0.50 5AO5015 FPA 82608/62301) 01/05/15 21:30 r457 1,2-Dichlorobehzene[95.50-1]^ < 0.062 ug/L 1 0.062 -. 0.50 5AO5015 EPA 826013/6230D 01/OS/15 21:30 htsz 1,2-Dichloroethane [107-06-2]A < 0.082 ug/L 1 0.032 0.50 SA0501S EPA 8260B16230D 01/OSJ15 21:30 _ MSZ 1,2-Dichloropropane[78-87-5]^ < 0.098 ug/L 1 0.098 0.50, SA05015 EPA 8260B/6230D 01/05/15 21:30 MSz 1,3,5-Trimethylbenzene [108-67-8]^ < 0.10 ug/L - 1 0.10 0.50 5AO5015 EPA 826 , /6230D 01/05/15 21:30 MSz 1,3-Dicrylorobenzene[541 73 1J^ < 0.092 ug/L 1 0.092 0.50 5AO5015 EPA 8260B/6230D 01/05/15 21:30 MSZ ' 1,3-DiclIllhloropropane[142-28-9]^ < 0.15 ug/L 1 0.15 0.50 5A05015 EPA 82608/6230D 01/05/15 21:30 MSZ 1,4-Dichlorobenzene[106-46-7]^ <-0:10 ug/L 1 0.10 0.50 5A05015 EPA 826OB/6230D O1/05/15 21:30 MSz 2,2-DiclIhloropropane [594..20-7]^ < 0.12 ug/L 1' 0.12 0.50 5A05015 EPA 8260B/6230D 01/05/15 21:30 msz_ 2-Chlorptoluene [95.49-8]A < 0.10 ug/L - 1 0:10 0.50 5A05015 EPA 826OB/6230D 01/05/15 21:30 MSz 4-Chlojotoluene[106-43-4]^ < 0.10 ug/L 1 .0.10 0.50 5AOSO15 EPA 826OB/6230D 01/05/15 21:30 MSz 4-IsoprIopyltoluene [99-87-6]^ < 0.066 ug/L 1 0.066 .'0.50 5AO5015 EPA 8260B/6130D Ol/05/15 21:30 MSZ Benzetie(71-43-2]A < 0.050 ug/L 1 0.050 0.50 5A05015 EPA 82606/6230D 01/05/15 21:30 h1S7 BromolbIenzene[108-86-1]^ < 0.13 ug/L 11, 0.13 0150 5AO5015 EPA 8260B/6230D 01/05/15 21:30 r•15Z Bromothlorbmethane [74-97-5J^ < 0.11 ug/L 1 0.11 0.50 5AOS015 LPA 82608/62300 01/05/15 21:3,0 t•tSZ Bromo ichloromethane [75-27-41^ < 0.010 ug/L 1 - 0.010 . " 0.50 5A05015 EPA 8260R/6230D 01/05/15 21:30 h1s7 Brrm [75-25-23^ < 0.20 ug/L 1 0.20 0.50 5A05015 EPA 8260B/6230D 01/05/15 21:30 - t45Z Bromolrlethane [74=83.9]^ < 0.28 ug/L 1' 0.28. 0.50 5A05015 EPA 826OB/6230D .01/05/15 21:30 MSz CarboniTetrachloride [56-23-5]A < 0.082 ug/L 1 0.082 0.50 5A05o15 EPA 8260B/6230D 01/0S/15 21:30 I%1sz Chlo4enzene [108-90-7]^ < 0.069 ug/L 1' 0.069 0.50 5A05015 EPA 8260B/6230D 01/05/15 21:36 MS7 Chlorolthane(75-00-3)^ < 0.18 _ug/L 1 0.18 0.50 5AO5015 EPA 8260B/6230D 01/05/15 21:30 h1Sz Chloroform [67-66-3]^ < 0.083 ug/L 1 0.083 0.50 5AO5015 EPA 82608/6230D 01/05/15 21:30 MSZ• Chlorofnethane [74-87-3]^ < 0.050 ug/L - 1 '` 0.050 0.50 SA05015 EPA 8260B/6230D 01'/05/15 21.30 MSZ cis- 1,2{Dichloroethene[156-59-2]^ < 0.075 ug/L 1 0.075 0.50 51AO5015 EPA 8260B16236D 01/05/15 21:30 MSZ cis- l,3,Dichloropropene(10061-01-5]A < 0.073 ug/L 1 0.073 '- 0.50 SA05015 EPA 8260B/6230D 01/05/15 21:30 msz D_ibromochloromethane[124-48-1]^ < 0:067 ug/L 1 0.067, .0.50 ,. 5A05015 EPA 82606/6230D 01/05/15 21:30 MSz Dibromomethane [74-95-3]^ < 0.13 - ug/L 1 ' 0.13 0.50 5AO5015 EPA 82606/6230D 01/05/15 21:30 MSZ Dichlo'iodiFluoromethane•[75-71=8]^ < 0.091 ug/L 1, 0.091 0.50 ' - 5AO5015 EPA 826013/6230D - 01/05/15 21:30 MSZ Ethylb6zene[100-41-4]^ < 0.10 ug/L 1 ,0:10 0.50 SA05015 EPA 8260B16230D 01/05/15 21:30 MSZ. Hexach,lorobutadiene[87-68-3]^ < 0.15 - ug/L 1, ,:0.15 0.50- 5AO5015 EPA 82606/62301) 01/05/15 21:30 MSZ Isopro�lyl Ether [108-20-31A < 0.20 ug/1- -1 0.20 0.50 5AO5015 FPA 8260B/62300 01/05/15 "21-30 MS7 Isopropylbenzene (9B-82-8]^ < 0.13 ug/L 1 0.13 0.50 5AO5015 FPA 8260B,6230D 01/05[:15 21c30 h157 , m,p-Xyllenes [108-38-3/106-42-3]A < 0.18 ug/L 1 0.18. 0.50 5AO5O15 EPA 8260B,;6230D 01/05/15 2t3p fLS7 Methylene Chloride [75-09-2]^ < 0.070 ug/L 1 ;. 0.070 0.50 5AO5015 EPA 8260B/6230D 01/05/15 21:30 msz Methyl-tert-Butyl-Ether[1639-04-4]^ < 0.12 ug/L 1 0.12 0.50,. 5AO5015, EPA'•826OB/6230D 01/05/15 21:30_ MSZ Naphthalene [91-20-3]^ < 0.086 ug/L 1 0.086 0.50_ SA05015 EPA 82608/62301) 01/65/15 21:30 M57- FINAL , - - This report relates only to the. sample -as received by the laboratory, and mayonly.be reproduced in:'full. Wage 22 of 41 www.encolabs.com ANALYTICAL RESULTS :ription: 141662-10 MW-33 Lab Sample ID:C500132-10 Received: 01/05/IS 14:06 Matrix: Ground Water Sampled:12/31/14 15:41 Work Order: C500132 Project: Genral Subcontract Sampled By: CLIENT (Volatile Organic Compounds by GCMS ^ - ENCO Cary certified aaalyte [NC 591] Analvte FCAS Numberl Results Flaa Units DF MDL POL Batch Method Analyzed Ay Notes n-Buty;Benzene [104-51-8]^ < 0.074 ug/L 1 0.071 0.50 5AO5015 FPA 8260B/6230D 01/05/15 71:30 n157 n-PropylBenzene (103-65-1]^ < 0.073 ug/L 1 0.073 0.50 5AO5015 EPA 826OB/6230D 01/05/15 21:30 MS7- o-Xylene[95-47-6]^ < 0.088 ug/L 1 0.088 0.50 5AO5015 EPA 8260B/6230D 01/05/15 21:30 MSZ sec-Buiylbenzene[135-98-8]^ < 0.OS3 ug/L 1 0.053 0.50 5AO5015 EPA 826OB/6230D 01/05/15 21:30 t15Z Styrene[100-42-5]^ < 0.082 ug/L 1 0.082 0.50 5AO5015 EPA 826OB/6230D 01/05/15 21:30 MS7 tert-Bultylbenzene [98-06-6]^ < 0.094 ug/L 1 0.094 0.50 5AO5015 EPA 8260B/6230D 01/05/15 11:30 h157. Tetrachloroethene[127-18-4]^ < 0.099 ug/L 1 0.099 0.50 SA05015 EPA 82608/62300 01/05r15 21.30 :IS/_ Toluene (108-88-3]^ < 0.053 ug/L 1 0.053 0.50 5AO5015 FPA 82.6OB/6230D 01/OSi1S ?1:30 MS/ trans-1,2-Dichloroethene [156-60-5]^ < 0.11 ug/1 1 0.11 0.50 5A05015 FPA 976OR/6230D 01/09/15 ?1 3n t•IS7 trans-1,3-Dichloropropene [10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 SACSOIS EPA 82606/6230D 01,/05/15 21:30 :•15Z Trichloroethene[79-01-6]^ < 0.13 ug/L 1 0.13 0.50 SA05015 EPA 8260B/6230D 01/05/15 21:30 f•15Z Trichlorofluoromethane[75-69-4]^ < 0.15 ug/L 1 0.15 0.50 5AO5015 EPA 826OB/6230D 01/05/15 21:30 MS/ Vinyl chloride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 5AO5015 EPA 87.6013/6230D 01/05/15 21:30 MS7 Xylenes(Total)[1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 5AO5015 EPA 8260B/62301) 01/05/15 21:30 MR SurrOpates 4-Bromofluorobenzene Dibro I fluoromethane roluene-d8 Results jQF SpikeLv/ o Re c %Rec Limits Batch Method Analyzed By Notes 55 1 50.0 109 % 53-136 5AO5015 EPA 8260816230C 01/05/15 21:30 AtSZ 53 1 50.0 106 % 67-129 5AO5015 EPA 8260816230C 01105115 21:30 A15Z 59 1 50.0 119 % 59-134 5A05015 EPA 62608/67.30L 01105115 21:30 AtS2 FINAL l"his report relates only to the sample as received by the laoora[ory, and may only be reproduced in full "a(19 /' of 41 iwww.encolabs.com ANALYTICAL RESULTS Description: 141662-13 MWr34 lab Sample ID:C500132-13 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 16:25 Work Order: C500132 Project: Genral Subcontract Sampled By: CLIENT JVbIatile Organic Compounds by GCMS j ^ - ENCO Cary cerVAB d analyre (NC 591 J Analvth iCAS Numbed (630-20-6]^ Resultr Flag < 0.091 Units ug/L DF 1 MDL 0.091 POL 0.50 Batch SA06013 Method EPA 82.608/62.30D Analyzed 01/06/15 14:44 _By Notes MS7 1,1,1,2]Tetrachloroethane 1,1,1-Tlichloroethane [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:44 MSz 1,1,2,2-Tetrachloroe1hane[79-34r5]^ < 0.085 ug/L 1 0.085 0.50 SA06013 EPA 8260B/6230D 01/06/15 14:41 MSz 1,1,2-Tiichloroethane(79-00-5]^ < 0.068 ug/L 1 0.068 0.50 5A06013 EPA 82608/6230D 01/06/15 14:44 MSz 1,1-Dicploroethane[75-34-3]^ < 0.050 ug/L 1 o.b50 0.50 5AO6013 FPA 82606/62.300 01/06/15 14:44 MS7- 1,]-DiclllhIloroethene [75-35-4]^ < 0.15 ug/L 1 0.15 0.S0 SA06013 FPA 82.60B/62.30D 01/06/15 14:44 PIS" 1,1-Dichloropropene[563758-6]^ < 0.063 ug/L 1 0.063 0.50 SA06013 L-PA 82606/6230D 01/06/15 14:44 MSz 1,2,3-T�ichlorobenzene(87-61-61^ < 0.25 ug/L 1 .0.25 0.50 5A06013 EPA 8260B16230D 01/06/15 14:44 MSZ 1,2,3-Tiichlorcpropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 82600/6230D 01/06/15 14:44 MS7 1,2,4-Tichlorobenzene(120-82-11^ < 0.097 ug/L 1 0.097 0.50 5AO6013 EPA 82608/62301) 01/06/15 14:44 MSz 1,2,4-Timethylbenzene[95-63-6]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 82606/6230D 01/06/15 14:44 MSz 1,2-Dib omo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 5A06013 -EPA 82608/62301) 01/06/15 14:44 MSz 1,2-Dib omoethane [106-93r41^ < 0.27 ug/L 1 0.27 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:44 MS7. 1,2-Dic florobenzene [95-50-1]^ < 0.062 ug/L 1 0.062 0.50' 5AO6013 EPA 8260B/6230D 01/06/15 14:44 MSz 1,2-Dic loroethane[107-06r2]^ < 0.082 ug/L 1 0.082 0.50 SA06013 EPA 82606/6230D 01/06/15 14:41 P15Z 1,2-Dic loropropane [78-87-5] A' < 0.098 ug/L 1 0.098 0.50 SA06013 EPA 8260B/6230D 01/06/15 14:44 MSz 1,3,5-T imethylbenzene (108-67.8)^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 82608/6230D O1/06/15 14:44 MS7. 1,3-Dic lcrobenzene.[541-73'1]^ < 0.092 ug/L 1 0.092 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:44 MSz 1,37Dic iloropropane[142-28-9]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 8260B/6230D 01/06/15 14:44 MSz 1,4-Dic ilorobenzene [106-46-7]^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:44 MSz 2,2-Dic iloroprDpane [594-20-7]^ < 0.12 ug/L 1 0.12 0.50 5A06013 EPA 8260B/62:30D 01/06/15 14:44 MS7 2-Chlo toluene[95-49-8]^ < 0.10 ug/L 1 0.10 0.50 SA06013 EPA 82608/62300 01/06/15 1-1:-14 MSZ 4-Chlor)toluene(106-43-4]^ < 0.10 tig/L 1, 0.10 0.50 5AO6013 EPA 82.608/6230D 01/06/15 14:44 f•15z 4-Isopr6pyltoluene[99-87-6]^. < 0.066- ug/L 1 0,066 0.50 5A06013 EPA 8260B16230D 01/06/15 14:44 A15" BenzenlI (71-43-2]^ < 0.050' ug/L 1 0.050 0.50 5AO6013 EPA 82.60B/6230D 01/06/15 14:44 P15z BromotSenzene(108-86-1]^ < 0.13 ug/L 1 0.13 •0.50 SA06013 EPA 8260B/6230D 01/06/15 14:44 MSz Bromo hloromethane (74-97-5]^ < 0.11 ug/L 1 0.11 0.50 5AO6013 EPA 87.608/62301) 01/06/15 14:44 MSz Bromo ichloromethane (75-27-4]^ < 0.010 ug/L 1 0.010 0.50 5A06013 EPA 82.60B/6230D 01/06/15 14:44 MSz Bromo rm [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 5AO6013 EPA 8260B/62.30D 01/06/19 14:44 MSz Bromo ethane [74-83-9]^ < 0.28 ug/L 1 0.28 0.50 5A06013 EPA 82.60B/6230D 01/06,115 14:44 PISZ Carbon Tetrachloride[56-23-5]^ < 0.082 ug/L 1 0.082 0.50 5A06013 EPA 8260B/6230D 01/06/15 14t44 MS7 Chloro6enzene[108-90.7]^ < 0.069 ug/L 1 0.069 0.50 5AO6013 EPA 8260B/6230D ol/06/15 14:44 MSZ Chloroethane(75-00-3]^ < 0.18 ug/L 1 0.18 0.50 5A06013 EPA 8260B16230D 01/06/15 14:44 MSz Chloroklrm (67-66-3)^ < 0.083 ug/L 1 0.083 0.50 5A06013 EPA 826013/6230D 01/06/15 14:44 MSZ' Chloro ethane(74r87-3]^ - < 0.050' ug/L 1 0.050 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:44 MSz cis-1,2 Dichloroethene [156-59-2]^, < 0.075 ug/L 1 0.075 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:44 MSz cis- 1,3,Dichloropropene.[10061-01-S]^ < 0.073 ug/L , 1 0,073 OSO 5AO6013 EPA 82606/6230D 01/06/15 14:44 MSz Dibro ochloromethane [124-48-1]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 82606/6230D 01/06/15 14:44 hISZ Dibro+meihane [74-95-3j^ < 0.13 ug/L 1 0.13 0.50 -5A06013 EPA 8260B/62.30D 01/06/15 14:44 MS7 DichlorlbIdi0uoromethane [75-71.8]^ < 0.091 ug/L 1 0.091 0.50 .5A06013 EPA 8260B/6230D 01/06/15 14:44 MS7 Ethylb@nzene[100.41-4]^ - < 0.10 ug/L 1. 0.10 0.50 SA06013 EPA 8260B/6230D 01/06/15 14:44 MSZ Hexacfilorobutadiene [87-68-311, < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 8260B/6230D 01/06/15 14:44 MSZ Isoproplyl Ether [108-20-3]^ < 0.20 ug/L 1 0.20 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:44 M57- Isopropylbenzene[98-82-8]^ < 0.13 •ug/L 1 . 0.13 0.50 SA06013 .EPA 8260B/6230D 01/06/15 14:44 MS7 m,p-Xylenes(108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 SA06013 EPA 8260B/6230D 01/06/15 14:44 MSZ Methyl2ne Chloride [75-09-2]^ < 0.070 ug/L I 0.070 0.50 SA06013 EPA 82.608/62300 01/06/15 14:44 MSC Methyltert-ButylEther[1634-04-41^ < 0.12 ug/L 1 0.12. 0.50 5AO6013 EPA 8260B/6230D 01/06/15 14;44 MSz Naphtl�alene[91-20-3]^ < 0.086 ug/L 1 0.086 •' 0.50 5A06013 FPA 8260B/6230D 01/06/15 14:44 MS7 FINAL - This report relates only to the sample as received by the laboratory, and may,only be reproduced in full. '-age. 28 of 41. I www.encolabs.com i ANALYTICAL RESULTS scription: 141662-13 MW-34 Lab Sample ID:C500132 13 Received: 01/05/15 14:06 I Sam led:12 31 14 16:25 Work Order: C500132 Matrix: Ground Water P / / Project: Genral Subcontract Sampled By: CLIENT (Volatile Organic Compounds by GCMS ^ - ENCO Cary certified ana/yte INC 591 J Analyt� [CAS Number] Results Flag Units DF MDL PPOL, Batch Method Analyzed 11y Notes n-ButyllBenzene[104-51-8]^ < 0.074 ug/L 1 0.074 0.50 5AO6013 EPA 82.60B/6730D 01/06/15 14-44 MS7 n-PropylBenzene[103-65-1]^ < 0.073 ug/L 1 0.073 0.50 5A06013 EPA R2606/6230D 01/06/15 14•+I MSZ o-Xylen�[95-47-6]^ < 0.088 ug/L 1 0.088 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:44 h15Z sec -But blbenzene[135-98-8]^ < 0.053 ug/L 1 0.053 0.50 SA06013 EPA 8260B/62.30D 01/06/15 14:44 MSZ Styren [100-42-5]^ < 0.082 ug/L 1 0.082 0.50 5AO6013 EPA 8260B/6230D 01/06/15 L-1:44 MS7. ten-Butylbenzene[98-06-6]^ < 0.094 ug/L 1 0.094 0.50 5AO6013 EPA 8260B/6230D 01/06/15 14:44 MSZ Tetrachiloroethene[127-18-4]^ < 0.099 ug/L 1 0.099 0.50 5AO6013 EPA 8260B/6230D 01/06/15 14:44 MSZ Toluen�[108-88-3]^ < 0.053 ug/L 1 0.053 0.50 5A06013 EPA 8260B/6230D 01/06/15 14:44 MS/ trans-1l2-Dichloroethene [156-60-5]^ < 0.11 ug/L 1 0.11 0.50 5A06013 EPA 8260B/6230D 01/06/15 14 44 MS7 trans-113-Dichloropropene [10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 5A06013 EPA 8260B/6230D 01/06/15 14.411 I,1SZ IrichloPethene [79-01-6]^ < 0.13 ug/L I 0.13 0.50 5A06013 LPA 82606/6230D 01/06/Io 14:44 raSZ Trichlolofluoromethane[75-69-4]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 8260B/6230D 01/06/15 14:44 MSZ Vinyl chloride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 5AO6013 EPA 82608/6230D 01/06/15 14.41 h1S7 XyleneS(Total)[1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 5AO6013 EPA 8260B/6230D 01/06/15 14:44 MSZ OP Spike I o Re c o Rec Limits Batch Method Analyzed py Notes Surrol ales ofluorobenzene Results 56 1 50.0 113 % 53-136 5AO6013 EPA 826OB16230L 01106115 14:44 AI5Z 4-8ror DibromIoduoromethane 56 1 50.0 113 % 67.129 5AO6013 EPA 826OB16230C 01106115 14.44 N5Z Toluen6-d8 60 1 50.0 11966 59-134 5AO6013 CPA 8260B/6230E 01106115 t-P-14 ^15Z FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. °'age 7B ui 4 1 - www.encolabs.com ANALYTICAL RESULTS De cription• 141662-14 MW-35 Lab Sample ID:C500132-14 Received: 01/0S/15 14:06 Matrix: Ground Water Sampled:12/31/14 16:40 Work Order: C500132 Project: Genral Subcontract Sampled By:CLIENT IVblatile Organic Compounds by GCMS ^ - ENCO Cary certified an,slyte (NC 5911 AnalytL rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed _By Notes 1,1,1,2 Tetrachloroethane [630-20-6]^ < 0.091 ug/L 1 0.091 0.50 SA06013 EPA 8260B/6230D 01/06/15 15:13 M57 1,1,1-T ichloroethane [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 82.6013/6230D 01/06/15 1S:13 MS7 1,1,2,2 Tetrachloroethane (79-3-1-5]^ < 0.085 ug/L 1 0.085 0.S0 5A06013 EPA 82606/6230D 01/06/15 15:13 h1Sz 1,1,2-T ichloroethane [79-00-5]^ < 0.068 ug/L 1 0.068 0.50 5A06013 EPA 8260B/6230D 01/06/15 1S:13 MSZ 1,1-DiclItloroethane[75-34-3]^ < 0.050 ug/L 1 0.050 0.50 SA06013 EPA 82608/6230D 01/06/15 15:13 MSZ 1,1-Dicj loroethene [75-35-4]^ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 8260B/6230D 01/06/15 15:1.3 MS7 1,1-Dicllllffiill»loropropene[563-58-6]•` < 0.063 ug/L 1 0.063 0.50 SA06013 EPA 82608/62301D 01/06/15 15:13 MSZ 1,2,3-Trichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0.25 0.50 5A06013 EPA 826OB/6230D 01/06/15 15:13 MSZ 1,2,3-irichloropropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 8260B/6230D 01/06/15 15:13 MS7. 1,2,4-lrichlorobenzene [120-82-1]^ < 0.097 ug/L 1 0.097 0.50 5AO6013 EPA 82606/6230D 01/06/1.5 15:13 MSZ 1,2;4-Trimethylbenzene [95-63-6]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 826OB/6230D 01/06/15 15:13 MSZ 1,2-DiblIromo-3-chloropropane (96-12-8)^ < 0.48 ug/L 1 0.48 0.50 5A06013 EPA 826OB/6230D 01/06/15 15:13 MSZ 1,2-Difiromoethane [106-93-4]^ < 0.27 ug/L 1 0.27 0.50 5AO6013 EPA 82606/6230D 01/06/15 15:13 h15Z 1,2-Di hlorobenzene[95-50-1]^ < 0.062 ug/L 1 0.062 0.50 5AO6013 EPA 82606/6230D 01/06/15 15:13 MSZ 1,2-Di hloroethane(107-06-2]^ < 0.082 ug/L 1 0.082 O.SO 5AO6013 EPA 82606/62301D 01/0611S 15:13 MSz 1,2-Di hloropropane[78-87-5]^ < 0.098 ug/L 1 0.098 0.50 SA06013 EPA 8260B16230D 01/06/15 1S:13 MSz 1,3,5-Tlrimethylbenzene[108-67-8]^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 82606/6230D 01/06/15 15:13 MSz 1,3-DiGlIhlorobenzene(541-73-1]^ < 0.092 ug/L 1 0.092 0.50 5A06013 EPA 8260B16230D 01/06/15 15:13 MSZ 1,3-DidIhloropropane[142-28-9]^ < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 82608/6230D 01/06/15 15:13 MSz 1,4-Didhlorobenzene[106-46-7]^ < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 82606/62.30D 01/06/15 15:13 MSz 2,2-Di( hloropropane(594-20-7]^ < 0.12 ug/L 1 0.12 0.50 5A06Oi3 FPA 8260R/62.30r) 01/06/!:i15 13 r457 2-Chlo otoluene[95-49-8]^ < 0.10 ug/L 1 0.10 0.50 SA06013 EPA 8260816230D 01/06/15 15:13 MSZ 4-Chlo otoluene [106-43-4]^ < 0.10 ug/L 1 0.10 0.50 SA06013 EPA 82.606/6230D 01/06/15 15:13 Msz 4-Iso+pyltoluene[99-87-6]^ < 0.066 ug/L 1 0.066 0.50 SA06013 EPA 82608/62301D 01/06/15 15:13 MSz Benzene[71-43-2]^ < 0.050 ug/L 1 0.050 0.50 5A06013 EPA 8260B162300 01/06/15 15:13 MSZ Bromolbenzene[108-86-1]^ < 0.13 ug/L 1 0.13 0.50 5A06013 EPA 8260B/6230D 01/06/15 t5:13 MSZ BromcIchloromethane[74-97-5]^ < 0.11 ug/L 1 0.11 0.50 SA06013 EPA 82608/62301) 01/06/15 15:13 MSZ Bromddichloromethane[75-27-4]^ < 0.010 ug/L 1 0.010 0.50 SA06013 EPA 82608/62301) 01/06/15 1S:13 MS7. BromdlIform (75-25-21^ < 0.20 ug/L 1 0.20 0.50 SA06013 EPA 8260B/6230D 01/06/15 15:13 Msz Bromcmethane[74-83-9]^ < 0.28 ug/L 1 0.28 0.50 SA06013 EPA 82608/6230D 01/06/15 15:13 14Sz Carbon Tetrachloride (56-23-5]^ < 0.082 ug/L 1 0.082 0.50 5AO6013 FPA 82.608/62301) 01/06/15 15:13 h1SZ Chlorcbenzene[108-90-71^ < 0.069 ug/L 1 0.069 0.50 5A06013 EPA 8260B/6230D 01/06/15 15:13 MSZ Chlorc�ethane [75-00-31^ < 0.18 ug/L 1 0.18 0.50 SA06013 EPA 8260B/6230D 01/06/15 15:13 MSZ Chlordform [67-66-3]^ < 0.083 ug/L 1 0.083 0.50 5AO6013 EPA 82608/6230D 01/06/15 15:13 MS-L Chlor :methane [74-87-3]^ < 0.050 ug/L 1 0.050 0.50 5AO6013 EPA 8260B/6230D 01/06/15 15:13 MS-L cis-1,-Dichloroethene[156-59-2]^ < 0.075 ug/L 1 0.075 0.50 5AO6013 EPA 82606/6230D 01/06/15 15:13 MSz cis-1,-Dichloropropene[10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 5A06013 EPA 826OB16230D 01/06/15 15:13 MS7. Dibro ochloromethane[124-48-1]^ < 0.067 ug/L 1 0.067 0.50 SA06013 EPA 8260B/6230D 01/06/15 15:13 . I.15Z Dibro) omethane[74-95-3]^ < 0.13 ug/L 1 0.13 0.50 SA06013 EPA 826OB/6230D 01/06/15 15:13 h1S7. DichldlIrodifluoromethane [75-71-81^ < 0.091 ug/L 1 0.091 0.50 SA06013 EPA 8260B/6230D 01/06,115 15:13 f•1S7 Ethyl fienzene[100-41-4]^ < 0.10 ug/L 1 0.10 0.50 SA06013 EPA 82608/6230D 01/06/15 15:1.3 MSZ Hexitl•h!orobutadiene[87-68-31^ < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 82.606/6230D 01/06/15 15:13 MSZ IsoprOpylEther [108-20-3]^ < 0.20 ug/L 1 0.20 0.50 5A06013 EPA 82606/6230D 01/06/15 15:13 MS7. Isopropylbenzene [98-82-8]^ < 0.13 ug/L 1 0.13 0.50 5A06013 FPA 8260B/62.30D 01/06/15 15:13 MSZ m,p-)}ylenes[108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 SA06013 EPA 8260B/6230D 01/06/15 15:13 MSZ Methllene Chloride [75-09-2]^ < 0.070 ug/L 1 0.070 0.50 5A06013 EPA 82608/6230D 01/06/15 t5:13 I•isz Meth I-tert-Butyl Ether [1634-04-4]^ < 0.12 ug/L 1 0.12 0.50 5A06013 EPA 8260B16230D 01/06/15 15:13 MSZ Naphthalene [91-20-3]A < 0.086 ug/L 1 0.086 0.50 5AO6013 EPA 826OB/6230D O1/06/15 15:13 blS7 This report relates only to the sample as received by the laboratory, and may only be reproduced in full. "age 30 of t FINAL -53:. ma's:.-.s.s-3arsa_:. ,o..•-,�.. 7 n0,,t www.encolabs.com ANALYTICAL RESULTS i I cription: 141662-14 MW-35 Lab Sample ID:C500132-14 Received: 01,105/15 14:06 Matrix: Ground Water Sampled:12/31/14 16:40 Work Order: C500132 Project: Genial Subcontract Sampled By:CLIENT IVolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte (NC 5911 Analyte [CAS Numberl Results Flaq Units DF MDL PPL Batch Method Analyzed _By Notes n-Butyl Benzene[104-51-8]^ < 0.074 ug/L 1 0.074 0.50 SA06013 EPA 8260B16230D 01/06/15 15:13 MSZ n-Prop�lBenzene [103-65-1J^ < 0.073 ug/L 1 0.073 0.50 SA06013 FPA 876118/6730P 0,1/K':5 15-i3 `-t57 o-Xylenle[95-47-6]`• < 0.088 ug/L 1 0.088 0.50 5A06013 EPA 8260B/6230D 01/06/15 15.13 MSZ sec-Butlylbenzene[135-98-8]^ < 0.053 ug/L 1 0.053 0.50 5A06013 LPA 8260B/62300 01/06/15 15:13 MSZ StyrenA[100-42-5]^ < 0.082 ug/L 1 0.082 0.50 5A06013 FPA 8260B/6230D 01/06/15 15:13 MSZ tert-Burylbenzene [98-06.6]^ < 0.091 ug/L 1 0.094 0.50 5AO6013 EPA 8260B/62:30D 01/06/15 IS:13 MSZ Tetracljloroethene[127-18-4]^ < 0.099 ug/L 1 0.099 0.50 5AO6013 EPA 8260B/6230D 01/06/15 15:13 MSZ Toluene[108-88-3]A < 0.053 ug/L 1 0.053 0.50 SA06013 EPA 82606/6230D 01/06/15 15:13 MSZ trans-1`2-Dichloroethene [156-60-S]^ < 0.11 ug/L 1 0.11 0.50 5AO6013 EPA 82.60B/6230D 01/06/15 15:13 MSZ trans- 1,,3-Dichloropropene[10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 5A06013 EPA 82605/6230D 01/06115 15:1i [aSZ TrichlorlIoethene[79-01-6]^ < 0.13 ug/L 1 0.13 0.50 5AO6013 EPA 8260B/6230D 01/06/15 15:13 MSZ Trichlo ofluoromethane [75-69-4]^ < 0.15 ug/L 1 0.15 0.50 SA06013 EPA 87-60B/6230D 01/06/15 15-13 MSZ Vinyl c loride[75-01-4]^ < 0.083 ug/L 1 0.083 0.50 5AO6013 EPA 82.60B16230D 01/06/15 15:13 MSZ Xylene,(Total)[1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 5AO6013 EPA 8260B/6230D 01/06/15 15:13 MSZ Resu/Ls OF Spike Lvl % Re c % Rec Limits Batch Method Analyzed By Notes 56 1 50.0 113 % 53-136 5AO6013 EPA 8260816230C 0110611515:13 h15Z 55 1 50.0 110 % 67-129 5AO6013 EPA 826OB16230C 01106/15 15:13 AISZ 59 1 50.0 118 0/ 59-134 5A06013 FPA 82608/62306 01/06,11515:1 > '%15Z FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page Jt of I I www.encolabs.com - --- - ANALYTICAL RESULTS scription• 141662-15 MW-36 Lab Sample ID:C500132-15 - Received: 01/05/15 14:06 Matrix: Ground Water -Sampled:12/31/14 16:57 Work Order: C500132 Project: Genral Subcontract Sampled By: CLIENT IVolatile Organic Compounds by GCMS ^ - ENCO Cary certified anaiyle [NC 591 J Analyte fCAS Numbed Results Flag Units DF . MDL PPOL Batch Method Analyzed 1y Notes 1,1,1,2,Tetrachloroethane [630-20-61^ < 0.091 ug/L 1 0.091 0.50 5AO6013 EPA 8260B/6230D 01/06/15 15:42 MSZ 1,1,1-Trichloroethane [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 82.60B/6230D 01/06/15 15:42 MSZ. 1, 1,2,2 'Tetrachloroethane [79-34-5]^ < 0.085 ug/L 1 0.085 0.50 SA06013 EPA 8260B/6230D 01/66/15 15:42 MSZ 1,1,2-Tr'ichloroethane (79-00.5]^ < 0.068 ug/L 1 0.068 0.50 5AO6013 EPA 8260B/6230D 01/06/15 15:42 MSZ 1,1-Di8loroethane(75-34-3]^ < 0.050 ug/L 1. 0.050 0.50 5A060.13 EPA 8260B/6230D 01/06/15 15:42 MSZ. 1,1-Dichloroethene(75-35-4]A < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 8260B/6230D 01/06/15'15:47 M57. 1,1-Dichloropropene [563-58-6]^ < 0.063 ug/L 1 0.063 0.50 5AO6013 EPA 82608/6230D 01/06/15 15:42 MSZ 1,2,3-Trichlorobenzene [87.61-6)^ < 0.25 ug/L 1 0.25 0.50 5AO6013 EPA 82.606/6230D 01/06/15 15:42 MSZ 1,2,3-Trichloropropane [96-18-4]A < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 82.60B/623o6 01/06/15 15:42 MSZ 1,2,4-Trichlorobenzene[120-82-1]^ < 0.097 ug/L 1 0.097 0.50 5A06013 EPA 82606/6230D 01/06/15 15:42 h1SZ 1,2,4-Trimethylbenzene[95-63-6]^ < 0.067 ug/L 1 0.067 0.50 5A06013 EPA 8260B16230D 01/06/15 15:42 MSZ 1,2-Dib'romo-3-chloropropane [96-12-B]A < 0.48 ug/L 1 0.48 0.50 SA06013 EPA 82608/6230D 01/06/15 15:42 MSZ 1,2-Dib'romoethane [106-93-4]^ < 0.27 ug/L 1 0.27 0.50 5AO6013 EPA 82608/6230D 01/06/15 15:42 MSZ 1,2-Dichlorobenzene[95-50-1]^ < 0.062 ug/L 1 -0.062 0.50 5AO6013 EPA 8260B/6230D 01/06/15 15:42 MSZ 1,2-Dich1oroethane(107-06-2]^ < 0.082 ug/L 1 0.082 0.50 5AO6013 EPA 8260B/6230D 01/06/15 15:42 M5Z 1,2-Dichloropropane[78-87-5]^ < 0.098 ug/L 1 0.098 0.50 5AO6013 EPA 8260B/6230D 01/06/15 15:42 MSZ. 1,3,5-Trimethylbenzene[108-67-8]A < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 8260B/6230D 01/06/15 15:42 MSZ 1,3-Dichlorobenzene [541-73-1]•` < 0.092 ug/L 1 0.092 0.50 5AO6013 EPA 82606/6230D 01/06/15 15:42 MSZ 1,3-Dfchloropropane (142-28-9]`` < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 8260B/6230D 01/06/15 15:42 MSZ 1,4-Dichlorobenzene [106-46-7)^ < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 82606/6230D 01/06/15 15:42 MSZ 2,2-Dichloropropane [594-20-7]•1 < 0.12 ug/L 1 0.12 0.50 5A06013 EPA 82.60B/6230D 01/06/15 15:42 MS,7 2-Chlorntoluene [95-49-8]^ < 0.10 ug/L l 0.10 0.50 SA06013 EPA 82.60B16230D 01/06/15 15:42 MSZ 4-Chlorotoluene[106-43-41^ < 0.10 ug/L 1 0.to 0.50 5AO6013 EPA 82.606/6230D 01/06/15 15:42 MSZ 4-lsopropyltoluene[99-87-6]^ . < 0.066 ug/L 1 0.066 0.50 5A06013 EPA 8260B/6230D 01/06/15 15:42 MSZ Benzene [71-43-2]^ < 0.050 ug/L 1 0.050 0.50 5AO6013 EPA 8260B/62.30D 01/06/15 15:42 ttSZ Bromo6enzene(108-86-I]^. < 0.13 ug/L 1 0.13 0.50 SA06013 EPA 62608/62301) 01/06/15 15:42 MSZ Bromoehloromethane [74-97-5]^ < 0.11 ug/L 1 0.11 0.50 5AO6013 EPA 8260B/6230D 01/06/15 15:42 NISZ Bromodichloromethane [75-27-4]^ < 0.010 ug/L 1 0.010 0.50 5AO6013 EPA 82608/6230D 01/06/15 15:42 MSZ Bromoform [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 SA06013 EPA 8260B/6230D 01/06/15 15:42 MSZ Bromomethane[74-83.9]^ < 0.28 ug/L 1 0.28 0.50, 5A06013 EPA 82608/6230D 01/06/15 15:4.2 MSZ Carbon' Tetrachloride [56-23-5]A < 0.082 ug/L 1 0.082 0.50 5A06013 EPA 8260B/6230D 01/06/15 15:42 MSZ Chlorobenzene[108-90-7]^ < 0.069 ug/L 1 0.069 0.50 5A06013 EPA 8260B/6230D 01/06/15 15:42 MSZ Chloroethane(75-00-3)^ < 0.18 ug/L 1 0.18 0.50 SA06013 EPA 82608/62301) 01/06/15 15:42 'MSZ Chloroform.(67-66-3.]A < 0.083 ug/L 1 0.083 0.50 SA06013 EPA 82608/6230D 01/06/15 15:42 MSZ Chloromethane[74-87-3]^ < 0.050 ug/L 1 0.050 0.50 5A06013 EPA 8260B/6230D 01/06/15 15:42 MS7 cis-1,2-Dichloroethene [156-59-2]^ < 0.075 ug/L 1 0.075 0.50 5AO6013 EPA 82608/6230D 01/06/15 15:42 MSZ cis-1,3-Dichloropropene[10061-01-5]A < 0.073 ug/L 1 0.073 0.50. SA06013 EPA 8260B/6230D 01/06/15 15:42 MSZ Dibromochloromethane [124,48-1]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 8260B/6230D 01/06/[5 15:42 r•1SZ Dibromomethane [74-95-3]^ < 0.13 ug/L 1 0.13 0.50 SA06013 rPA 8260B/6230D 01/06/15 15:42 n1S7 Dichlorodi0uoromethane [75-71-8]^ < 0.091 ug/L 1 0.091 0.50 5AO6013 EPA 826OB162.30D 01/06/15 15:42 MS7. Ethylbenzene[I00 41 4]^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 82606/6230D 01/06/15 15:42 MSZ Hexacilorobutadiene[87-68-3]^ < 0.15 ug/L 1 0.15 0.5o SA06013 EPA 8260B/6230D 01/06/15 15:42 MSZ Isopropyl Ether[108-20-31^ < 0..20 ug/L 1 0.20 0.50 5A06013 EPA 82608/6230D 01/06/15 15:42 MSZ Isopropylbenzene[98-82-8]^ < 0.13 ug/L 1 - 0.13 0.50 5A06013 EPA 82608/6230D 01/06/15 15:42 MSZ m,p-Xylenes[108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 5AO6013 EPA 82608/6230D 01/06/15 15:42 MSZ Methylene Chloride [75-09-2]A < 0.070 ug/L 1 0.070 0.50 5AO6013 EPA 8260B/62301) 01/06/15 15:42 NISI Methyl-tert-Butyl Ether [1634-03-9]^ < 0.12 ug/L 1 0.12 0.50 5AO6013 EPA 8260B/6230D 01/06/15 15:42 MSZ Naphthalene[91-20-3)^ < 0.086 ug/L 1 0.086 0.50 5AO6013" EPA 8260B/6230D 01/06/15 15:42 MSZ. FINAL - This report relates only to the sample as received by the laboratory• and may only be reproduced in full.. Page 32 or 41 I ANALYTICAL RESULTS 0 Description: 141662-15 MW-36 Matrix: Ground Water Project: Genral Subcontract Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Lab Sample ID:C500132-15 Sampled: 12/31/14 16:57 Sampled By:CUENT Analyte rCAS Number"! Results Flaa Units DF MDL POL n-Butyl'Benzene [104-51-8]^ < 0.074 ug/L 1 0.074 0.50 n-Propyl Benzene [103-65-1]^ < 0.073 ug/I. I 0.073 0.50 o-Xylene [95-47.61^ < 0.088 ug/L 1 0.088 0.50 sec-Butylbenzene [135-98-8]^ < 0.053 ug/L 1 0.053 0.50 Styrene [100-42-5]^ < 0.082 ug/L 1 0.082 0.50 tert-Butylbenzene [98-06-6]^ < 0.094 ug/L 1 0.094 0.50 Tetrachloroethene [127-18-4]^ < 0.099 ug/L 1 0.099 0.50 Toluene [108-88-3]^ < 0.053 ug/L 1 0.053 0.50 trans-1,2-Dichloroethene [156-60-5]^ < 0.11 ug/L 1 0.11 0.50 trans-1,3-Dichloropropene [10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 Trichloroethene [79-01-6]^ < 0.13 ug/L 1 0.13 0.50 Trichlorofluoromethane [75-69-4]^ < 0.15 ug/L 1 0.15 0.50 Vinyl chloride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 Xylenes(Total)[1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 Surrogates Resu/tr DF Soike L vl % Re c % Rec Limitr 4-Bromofluorobenzene 58 1 50.0 117 % 53-136 oibrorriofluoromethane 57 1 50.0 114 V. 67-129 toluene-d8 61 1 50.0 122 % 59-134 c0. i, :..ems:_--„�_ ��:ti.:�_ — •�, www.encolabs.com Received: 01/05/15 14:06 Work Order: C500132 Batch Method Analyzed 5AO6013 EPA 82.60B/62.30D 01/06/15 15:42 5A06013 FPA 8260R/62300 01/0611515:42 5AD6013 EPA 82606/6230D 01/06/15 15:42 5A06013 EPA 82608/G230D 01/06/15 15:42 SA06013 EPA 8260B/6230D 01/06/15 15:12 SA06013 EPA 82.60B/6230D 01/06/15 15:12 5A06013 EPA 8260B/6230D 01/06/15 15:42 SA06013 EPA 8260B16230D 01/06/15 15:42 SA06013 FPA 8260B/6230D 01/06/15 15:42 5A06013 EPA 82606/6230D 01/06/15 15:42 5AO6013 EPA 6260816230D 01/06/15 15:42 SA06013 EPA 82608/6230D 01/06/15 15:42 5A06013 EPA 8260B/6230D 01/06/15 15:42 5A06013 EPA 82608/6230D 01/06/15 15:42 Batch Method Analyzed 5A06013 EPA 8260B16230C 01106115 15:42 5A06013 CPA 826OB16230C 01106,115 15:42 5A06013 CPA 8260B16730L 01106115 15:4.2 By Notes MSZ h1S7 r4SZ MSZ MSZ h15Z MSZ MSZ MS7 MSZ f45Z M57- MSZ MSZ y Notes A15Z A15Z M51 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 33 of 4 1 k'O.W'R`.._r"•`..RiYH. fiTu .cda0j�r www.encolabs.com ANALYTICAL RESULTS De cription: 141660 13 MW 37 Lab Sample ID:C500133-13 Received: 01/05/15 11:06 Matrix: Ground Water Sampled:12/31/14 13:40 Work Order: C500133 Project: Genral Subcontract Sampled By:CLIENT JVQIatile Organic Compounds by GCMS , - ENCO Cary certified analyte [NC 5.911 III Analyte rCAS Numberl (630-20-6)^ Results Flaa < 0.091 Units ug/L DF 1 MDL 0.091 P L 0.50 Batch 5A08010 Method EPA 8260B/6230D Analyzed 01/08/15 15;•14 1�y Notes MSZ 1,1,1,21.retrachloroethane 1,1,1-Ttlichloroethane [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:44 MS7 1,1,2,2 etrachloroethane [79-34-5]^ < 0.085 ug/L 1 0.085 0.50 5A08010 EPA 8260B/6230D 01/08/15 15:44 MSZ 1,1,2-TiI ichloroethane[79-00-5]^ < 0.068 ug/L i 0.068 0.50 5AO8010 EPA 826OB/6230D 01/08/15 15:44 MSZ 1,1-Dic < 0.050 ug/L 1 0.050 0.50 5A08010 EPA 82606/6230D 01/08/15 15:44 MS7 lloroethane[75-34-3]^ 1,1-Dichloroethene[75-35-4]^ < 0.15 ug/L 1 0.15 0.50 SA08010 EPA 8260B/6230D 01/08/15 15:44 MS7- 1,1-Dic loropropene[563-58 6]^ < 0.063 ug/L 1 0.063 0.50 SA08010 EPA 8260B/6230D 01/08/15 15:44 MSZ 1,2,3-T ichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0.25 0.50 5A08010 EPA 8260B/6230D 01/08/15 15:44 MSL 1,2,3-Tiichloropropane(96-18-4]^ < 0.15 ug/L 0.15 0.50 5AO8010 EPA 8260Bi62.30D 01/08/15 15:44 MSZ 1,2,4-T ichlorobenzene [120-82-1]^ < 0.097 ug/L 1 0.097 0.50 SA08010 EPA 8260B/6230D 01/08/15 15:+1 MSz 1,2,4-T imethylbenzene (95-63-6]^ < 0.067 ug/L 1 0.067 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:44 MSz 1,2-Dib omo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:44 MSZ 1,2-Dib omoethane[106-93-4]^ < 0.27 ug/L 1 0.27 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:41 MSZ 1,2-Dic ilorobenzene [95-50-1]^ < 0.062 ug/L 1 0.062 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:44 MSZ 1,2-Dic hloroethane[107-06-2]^ < 0.082 ug/L 1 0.082 0.50 5AO8010 EPA 82606/6230D 01/08/15 15:44 MSZ 1,2-Dic hloropropane[78-87-5]^ < 0.098 ug/L 1 0.098 0.50 5A08010 EPA 8260B/6230D 01/08/15 15:44 I.157. 1,3,5-T imethylbenzene [108-67-8]^ < 0.10 ug/L 1 0.10 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:44 MSZ 1,37Dichlorobenzene [541-73-1]^ < 0.092 ug/L 1 0.092 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:44 MSZ 1,3-Dic iloropropane[142-28-9]^ < 0.15 ug/L 1 0.15 0.50 SA08010 EPA 8260B/6230D 01/08/15 15:44 h1SZ 1,4-Dicllorobenzene[106-46-7]^ < 0.10 ug/L 1 0.10 0.50 5A08010 EPA 826013/6230D 01/08/15 15:44 MSZ < 0.12 ug/L 1 0.12 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:44 MS7 2,2-DiclhIloropropane[594-20-7]^ 2-Chlorptoluene[95-49-B]^ < 0.10 ug/L 1 0.10 0.50 SA08010 EPA 8260B/6230D 01/08/15 15:44 h1SZ 4-Chlorll)toluene[106-43-4]^ < 0.10 ug/L 1 0.10 0.50 5A03010 EPA 8260B/6230D 01/08/15 15:44 MSZ 4-Isopr¢pyltoluene[99-87-6]^ < 0.066 ug/L 1 0.066 0.50 SA08010 EPA 8260B/6230D 01/08/15 15:44 hISZ < 0.050 ug/L 1 0.050 0.50 5AO8010 EPA 826OB/6230D 01/08/15 15:41 MS7 Oenzen2[71-43-2]^ Bromot enzene[108-86-1]^ < 0.13 ug/1- 1 O.i3 0.50 5AO8010 LPA 8260B/62300 01/08/15 15.44 Hsz Bromo hloromethane(74-97-5]^ < 0.11 ug/L 1 0.11 0.50 5A08010 EPA 8260B/6230D 01/08/15 15:44 MR Bromo ichloromethane[75-27-4]^ < 0.010 ug/L 1 0.010 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:41 MSZ Bromo rm [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 SA08010 EPA 8260B/6230D 01/08/15 15:44 MSz Bromo ethane [74-83-9]^ < 0.28 ug/L 1 0.28 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:44 Msz Carbon Tetrachloride [56-23-5]^ < 0.082 ug/L 1 0.082 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:44 MS'7- Chloro enzene[108-90-7]^ < 0.069 ug/L 1 0.069 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:44 M57_ Chloro thane[75-00-3]^ < 0.18 ug/L 1 0.18 0.50 SA08010 EPA 8260B/6230D 01/08/15 15:44 MSZ Chloro rm [67-66-3J^ < 0.083 ug/L 1 0.083 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:44 MSz Chloro ethane[74-87-3]^ < 0.050 ug/L 1 0.050 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:44 MSZ cis-1,2 Dichloroethene [156-59-2]^ < 0.075 ug/L 1 0.075 0.50 5A08010 EPA 8260B/6230D 01/08/15 15:44 1-isz cis-1,3.Dichloropropene[10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 SA08010 EPA 8260B16230D 01/08/15 15:44 MSZ Dibro ochloromethane[124-48-1]^ < 0.067 ug/L 1 0.067 0.50 SA08010 EPA 8260B/6230D 01/08/15 15:44 MSZ Dibro omethane [74-95-3]^ < 0.13 ug/L 1 0.13 0.50 5A08010 EPA 82.606/6230D 01/08/15 15:44 msz Dichlor diFluoromethane[75-71-8]^ < 0.091 ug/L 1 0.091 0.50 SA08010 FPA 8260B/6230D 01/08/15 15-44 MSZ Ethylb nzene [100-41-4p' < 0.10 ug/L 1 0.10 0.50 5A08010 1-PA 8260B/6230D 01108/I5 15:44 4Sz Hexac lorobutadiene [87-68-3]^ < 0.15 ug/L 1 0.15 0.50 SA03010 EPA 826OB/6230D 01/08/15 15:14 r•15L lsoprotl Ether[108-20-3]^ < 0.20 ug/l. 1 0.20 0.50 5A08010 EPA 826OB/6230D 01/08/15 15 44 I S7 Isopro ylbenzene [98-82-8]^ < 0.13 ug/L '_ 0.13 0.50 SA08010 EPA 82606/6230D 01/08/15 15:44 MSZ < 0.18 ug/L 1 0.18 0.50 5AO8010 EPA 826OB/6230D 01/08,115 15:44 f•15Z m,p-Xylenes Methyl [108-38-3/106-42-3]^ ne Chloride (75-09-2]^ < 0.070 ug/L 1 0.070 0.s0 SA08010 EPA 8260B/6230D 01/08/15 1S:44 h1SZ Methyl tert-Butyl Ether[1634-04-4]^ < 0.12 ug/L 1 0.12 0.50 5AO8010 EPA 8260B/6230D 01/08/15 15:41 MSZ Naphtt alene[91-20-3]^ < 0.086 ug/L 1 0.086 0.50 5AO8010 EPA 826OB/6230D 01/08/15 15W4 MS7 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Faye 26. o 3� -ription: 141660-13 MW-37 Matrix: Ground Water Project: Genral Subcontract latile Organic Compounds by GCMS ^ . ENco Cary certified analyte [NC 5911 n-Butyl Benzene [104-51-8]^ n-Prop I Benzene [103765-1]^ o-Xylene [95-47-6]^ sec-Bu (benzene [135-98-8]^ Styren [100-42-5]^ tert-Bu ylbenzene [98-06.6]^ Tetrac loroethene [127-18-4]^ Toluen [108-88-3]^ trans-1 2-Dichloroethene [156-60-5]^ trans-1 3-Dichloropropene [10061-02,6]^ Trichlo oethene [79-01-6]^ Trichlo ofluoromethane [75-69-4]^ Vinyl chloride [75-01-4]^ Xylene (Total) [1330-20-7]^ ANALYTICAL RESULTS Lab Sample ID:C500133-13 Sampled:12/31/14 13:40 Sampled By:CLIENT Results Flaa Units DF MDL PP L < 0.074 ug/L 1 0.074 0.50 < 0.073 ug/L 1 0.073 0.50 < 0.088 ug/L 1 0.088 0.50 < 0.053 ug/L 1 0.053 0.50 < 0.082 ug/L 1 0.082 0.50 < 0.094 ug/L 1 0.094 0.50 < 0.099 ug/L 1 0.099 0.50 < 0.053 ug/L 1 0.053 0.50 < 0.11 ug/L 1 0.11 0.50 < 0.080 ug/L 1 0.080 0.50 < 0.13 ug/L 1 0.13 0.50 < 0.15 ug/L 1 0.15 0.50 < 0.083 ug/L 1 0.083 0.50 < 0.22 ug/L 1 0.22 0.50 Resu/tr DF Spike Lvl °7o Re c °7o Rec Limits 56 1 50.0 11196 53-136 51 1 50.0 103 96 67-129 58 1 50.0 116 % 59-134 IA N www.encolabs.com Received: 01/05/15 14:06 Work Order: C500133 Batch Method Analyzed 5AO8010 EPA 8260B/6230D 01/08/15 15:44 5AO8010 EPA 8260B/6230D 01/08/15 15:44 5AO8010 EPA 82606/62300 01/08/15 15:44 5A08010 EPA 82606/6230D 01/08/15 15:44 5AO8010 EPA 8260B/6230D 01/08/15 15:44 5A08010 EPA 82.60B/6230D 01/08/15 15:4-1 5AO8010 EPA 8260B/6230D 01/08/15 15:41 5A08010 EPA 82608/6230D 01/08/15 15:44 5A08010 EPA 82606/6230D 01/08/15 15:44 5AO8010 EPA 8260B/6230D 01/08/15 15:44 5AO8010 EPA 8260B/6230D 01/08/15 15:44 5AO8010 EPA 8260B/6230D 01/08/15 15:44 5A08010 EPA 8260B/6230D 01/08/15 15:44 SA08010 EPA 8260B/6230D 01/08/15 15:44 Batch Method Ana/vzed 5A08010 EPA 8260B/6230L 01108115 15:44 5A08010 EPA 826OB16230L 01/08/15 15:44 5AO8010 EPA 326OB16230C 0110811515:44 AM Notes MSZ MSZ MSZ MSZ MSZ MSZ MSZ MSZ MSZ MSZ MSZ MSZ MSZ MSZ Ay Notes MsZ h15Z A157- FINAL This report relates only to the sample as receivedby the laboratory, and may only be reproduced in full. pag^ : P or "9 1 're O S..S n ir.L tri m -.s y -017 www,encolabs.com ANALYTICAL RESULTS Description: 141662-09 MW-38 Lab Sample ID: C500 132-09 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 15:28 Work Order: C500132 Project: Genral Subcontract Sampled By: CLIENT IVolatile Organic Compounds by GCMS ENCO Cary ceRified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PPOL Batch Method Analyzed py Notes 1,1,1,22Tetrachloroethane [630-20-6]^ < 0.091 ug/L 1 0.091 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:59 h1SZ 1,1,1-Trichloroethane[71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5AO5015 EPA 826013/6230D 01/05/15 20:59 MSz 1,1,2,2-Tetrachloroethane[79-34-5]^ < 0.085 ug/L 1 0.085 0.50 5AO5015 EPA 826013/6230D 01/05/15 20:59 MSz 1,1,2-Trichloroethane [79-00-5]'• < 0.068 ug/L 1 0.068 0.50 SA05015 EPA 826013/6230D 01/05/15 20:59 MSz < 0.050 ug/L 1 0.050 0.50 5ADS015 EPA 8260B/62.30D 01/05/15 2D:59 nIS7 1,1-Dichloroethane [75-34-3]^ 1,1-Dichloroethene [75-35-4]^ < 0.15 ug/L 1 0.15 0.50 SA05015 EPA 82608/6230D 01/05/15 20:59 MSZ 1,1-Dichloropropene[563-58-6]^ < 0.063 ug/L 1 0.063 0.50 5A05015 EPA 826013/6230D 01/05/15 20:59 MSz 1,2,3 Trichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0.25 0.50 SA05015 EPA 82608/6230D 01/05/15 20:59 1115z 1,2,3-Trichloropropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.50 5AO5015 EPA 82606/62301) 01/05/15 20:59 h1S7. 1,2,4-Trichlorobenzene[120-82-1]^ < 0.097 ug/L 1 0.097 0.50 SA05015 EPA 826013/62301) 01/05/15 20:59 MSz 1,2,4-Trimethylbenzene[95-63-6]^ < 0.067 ug/L I 0.067 0.50 5A05015 EPA 82608/6230D 01/05/15 20:59 MSz 1,2-Dibiromo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 5AO5015 FPA 8260B/62.30D 03/05/15 2.0:59 MS7- 1,2-Dibromoethane[106-93-4]^ < 0.27 ug/L 1 0.27 0.50 5A05015 EPA 82608/6230D 01/05/15 20:59 f4S7- 1,2-Dici llorobenzene[95-50-1)^ < 0.062 ug/L 1 0.062 0.50 5A0501S EPA 8260B/6230D 01/05/15 20:59 MSZ 1,2-Dickloroe[hane[107-06-2]^ < 0.082 ug/L 1 0.082 0.50 5A05015 EPA 8260B/6230D 01/05/15 20:59 MSZ 1,2-Dichloropropane[78-87-5]^ < 0.098 ug/L 1 0.098 0.50 5AO5015 EPA 826013/6230D 01/05/15 20:59 MSZ 1,3,5-T�imethylbenzene[108-67-8]^ < 0.10 ug/L 1 0.10 0.50 SAD5015 EPA 8260B/6230D 01/05/15 20:59 M57- 1,3-Dichlorobenzene[541-73-1]•` < 0.092 ug/L 1 0.092 0.50 5AO5015 EPA 826OB/6230D 01/05/15 20:59 MSZ 1,3-Dichloropropane[142-28-9]^ < 0.15 ug/L 1 0.15 0.50 SA05015 EPA 8260B/6230D 01/05/15 20:59 MSZ 1,4-Dichlorobenzene[106-46-7]^ < 0.10 ug/L 1 0.10 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:59 MSz 2,2-Dichloropropane[594-20-7]^ < 0.12 ug/L 1 0.12 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:59 MSZ 2-Chlorotoluene (95-49-8]^ < 0.10 ug/L 1 0.10 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:59 MSZ 4-Chlorotoluene[106-43-4]^ < 0.10 ug/L 1 0.10 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:59 MSZ 4-Isopropyltoluene[99-87-6]^ < 0.066 ug/L 1 0.066 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:59 °ISZ Benzene [71-43-2]^ < 0.050 ug/L 1 0.050 0.50 SA05015 EPA 826OB/6230D 01/05/15 20:59 I.157 Bromobenzene [108-86-1]^ < 0.13 ug/L 1 0.13 0.50 5AO5015 EPA 8260B/62300 01/05/15 20:59 N157 Bromochloromethane (74-97-5]^ < 0.11 ug/L 1 0.11 0.50 5AO501S EPA 8260B/6230D 01/05/15 20:59 msz Bromodichloromethane [75-27-4]^ < 0.010 ug/1. 1 0.010 0.50 SA05015 FPA 82606/6230D 01/05/1S 20:59 f-Isz Bromoform [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 5AO501S EPA 8260B/6230D 01/05/15 20:59 F15Z Bromomethane[74-83-9]^ < 0.28 ug/L 1 0.28 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:59 MSZ Carbon Tetrachloride [S6-23-5]1• < 0.082 ug/L 1 0.082 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:59 Msz Chlorobenzene[108-90-7]^ < 0.069 ug/L 1 0.069 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:59 r11S7 Chloroethane[75-00-3]^ < 0.18 ug/L 1 0.18 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:59 MSZ Chloroform [67-66-3)^ < 0.083 ug/L 1 0.033 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:59 r-15z Chloromethane(74-87-3]^ < 0.050 ug/L 1 0.050 0.50 SA05015 EPA 82608/62301) 01/05/15 20:59 MSz_ cis-1,2-Dichloroethene [156-59-2]^ < 0.075 ug/L 1 0.075 0.50 5AO5015 EPA 826OB/62300 01/05/15 20:59 MSZ cis-1,3 Dichloropropene[10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 5A05015 EPA 826013/62301) 01/05/15 20:59 MSz Dibromochloromethane [124-48-1]^ < 0.067 ug/L 1 0.067 0.50 5AO5015 EPA 82606/6230D 01/05/15 20:59 MSZ Dibrortiomethane[74-95-3]^ < 0.13 ug/L 1 0.13 0.50 5A05015 EPA 8260B/6230D 01/05/1S 20:59 MS7 DichlorodiFluoromethane[75-71-8]^ < 0.091 ug/L 1 0.091 0.50 5A05015 EPA 82608/6230D 01/05/15 20:59 M57 Ethylbenzene[100-41-4]^ < 0.10 ug/L 1 0.10 0.50 SA05015 EPA 82608/6230D 01/05/15 20:59 MSZ Hexachlorobutadiene [87-68-3]^ < 0.15 ug/L 1 0.15 0.50 5A05015 EPA 82508/6230D 01/05/1S 20 S9 r•157. Isopropyl Etherf108-2.0-3)^ < 0.20 ug/L. 1 0.20 0.50 SA05015 FPA 826OB/6230D 01/05115!0 59 IIS7 Isopropylbenzene[98-82-8]^ < 0.13 ug/L 1 0.13 0.50 5AO5015 EPA 8260Bi6230D 01/05i15 20 59 MS7 m,p-Xylenes[108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 SA05015 EPA 82600/6230D 01/0S/I5 20:SU r45Z Methylene Chloride [75-09-2]^ < 0.070 ug/L 1 0.070 0.50 J5A05015 EPA 82.60B/6230D 01/05/15 20:59 r-15z Methyl-tert-ButylEther [1634-04-4]^ < 0.12 ug/L 1 0.12 0.50 5AO5015 EPA 82608/6230D 01/05/15 20:59 MSZ Naphthalene[91-20-3]^ < 0.086 ug/L 1 0.086 0.50 5A05015 EPA 826OB16230D 01/0S/15 20:59 MSz FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 41 """" encolabs.com — --- --- — _--- -------- -- �� ANALYTICAL RESULTS Description: 141662-09 MW-38 Lab Sample ID:C500132-09 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 15:28 Work Order: C500132 Project: Genral Subcontract Sampled By: CLIENT (Volatile Organic Compounds by GCMS _A ^ - ENCO Cary cerr fled analyte [NC 5911 Analyte rCAS Number] Results Flag Units DF MDL PDL, Batch Method Analyzed By Notes n-ButylBenzene[104-51-8]^ < 0.074 ug/L 1 0.074 0.50 SA05015 EPA 8260B/6230D 01/05/15 20:59 MSZ n-Propyl Benzene[103-65-1J^ < 0.073 ug/L 1 0.073 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:59 MS7 o-Xylene[95-47-6]^ < 0.088 ug/L 1 0.088 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:59 MSZ sec-Butylbenzene[135-98-8]^ < 0.053 ug/L 1 0.053 0.50 5AO5015 EPA 82605/6230D 01/05/15 20:59 MSZ Styrene,[100-42-5]^ < 0.082 ug/L 1 0.082 0.50 SA05015 EPA 826OB/6230D 01/05/15 20:59 MSZ tert-Butylbenzene[98-06-6]^ < 0.094 ug/L 1 0.094 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:59 MSZ Tetrachloroethene[127-18-41^ < 0.099 ug/L 1 0.099 0.50 5AO5015 EPA 8260B/62300 01/05/15 20:59 r•ISZ Toluene[108-88-31^ < 0.053 ug/L 1 0.053 0.50 5AO5015 LPA 8260B/62.30D 01/05/15 20:59MSl trans-l;2-Dichloroethene [156-60-51^ e 0.11 ug/L 1 0.11 0.50 5AO5015 EPA 8260816230D 01/05/15 20:59 MSZ. trans- 1;3-Dichloropropene [10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 5AO5015 EPA 8260B/6230D 01/OS/15 20:59 MSZ. Trichloroethene[79-01-6]^ < 0.13 ug/L 1 0.13 0.50 SA05015 EPA 82606/6230D 01/05/15 20:59 h1SZ Trichloiofluoromethane[75-69-4]^ < 0.15 ug/L 1 0.15 0.50 5AO5015 EPA 8260B/6230D 01/OS/15 20:59 MSZ Vinyl chloride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 SA05015 EPA 8260B/6230D 01/05/15 20:59 MSZ Xylenei(Total)[1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 SA05015 EPA 826OB/6230D 01/05/15 20:59 MSZ Surro ates Resu/ts OF Spike Lvl o Re c o Rec Limits Batch Method Ana/vzed ffy Notes 4-Broniofiuorobenzene 56 1 5p.0 112 % 53-136 5A05015 EPA 826OB16230C 01105115 20:59 M5Z Dibromofluoromethane 55 1 50.0 110 % 67-129 5AO5015 EPA 8260316230C 01105115 20.59 /1/5Z 1 50.0 118 % 59-134 5AO5015 EPA 8260816230C 01105115 20:59 MSZ Toluene-d8 59 FINAL This report relates only to the sample as received by the laboratory, and may only be reproducer) in full. Page 21 of 41 ;E , I www.encolabs.com ANALYTICAL RESULTS Description: 141662-08 MW-39 Lab Sample ID:C500132-08 Received: 01,105/15 14:06 ,Matrix: Ground Water - Sampled:12/31/14 1S:21 Work Order: C500132 Project: Genral Subcontract Sampled By:CLIENT Volatile Organic Compounds by-GCMS. ' ^ • ENCO Cary certified analyze (NC 5911 Analyte fCAS Numbed Results Flag Units DF MDL PQL Batch MethodAnalyze Py Notes 1,1,1,2-'Tetrachloroethane [630-20-6]^ < 0.091 ug/L, 1 0.091 0.50 5AO5015 EPA 8260B/6230D 01/05/1S 20:28 MSZ 1,1,1-Trichloroethane [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5AO501S EPA 82606/6230D 01/05/15 2028 MSz 1,1,2,2 Tetrachl6roethane [79-34-5]^ < 0.085 ug/L ri 0.08S 0.50 5AO5015 EPA 826OB/623OD- 01/05/15 20'r28 MSZ 1,1,27Trichloroethane [79-00-5]^ < 0.068 ug/L 1 0.068 0.50 SA05015 EPA 8260B/623dD 01/05/15 20:28 MSZ 1,)-Dichloroethane[75-34-3]^ . < 0.050 ug/L 1 0.050 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20;28 MSZ 1,1-Dichloroethene.[Z5-35-4].A < 0.15 ug/L 1 0.15 0.50 SA05015 'EPA 8260B/6230D 01/05/15 20:28 MSZ 1',1-Dichloropropene[563-58-6]^ < 0.063 ug/L 1 0.063 0.50 5AO5015 EPA 8260B/62301) 01/05/15 20:28 MSZ 1,2,3-Trichlorobenzene [87-61-6]^ < 0.25 ug/L 1' 0.25 0.50 5AOS015 EPA 8260B/6230D 01/05/15 20:28 MSZ 1,2,3-Trichloropropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.50 5A05'015 EPA 8260B/6230D 01/05/15 20:2.8 MS7. 1,2,4-Trichlorobenzene[120-82.1]^" < 0.097 ug/L 1 0.097 0.50 5AO5015 EPA 8260B16230D 01/05/15 20:28 MSZ 1,2,4-Tlimethylbenzene[95-63-6]^ < 0.067 ug/L 1 0.067 0.50 5A05015 EPA 82608/6230D 01/05/15 2025 hISL 1,2-1)if romp-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 5AO5015 EPA 82.60B/623ob 01/05/15 20:2.8 MSZ 1,2-Dibrornoethane[106-9374]^ < 0.27 ug/L 1 0.27 0.50 5AO5015 EPA'82.608/6230D 01/05/15 20:28 MS7. 1,2-Dichlorobenzene[95-50-1]^ .. < 0:062 ug/L 1 0.062 0.50 SA0501S EPA 8260B/6230D 01/OS/15 20:28 MSZ 1,2-DichWoethane[107-06-2]A < 0.082 ug/L 1 0.082 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:28 MSZ 1,2-Dicfiloropropane[78-8Z S]^ < 0.098 ug/L ., 1 0.098 0.50 5AO5015, EPA 8260B/6230D 01/05/15 20:28 MSZ 1,3, S-Triiriethylbenzene'[ 108-67-8] < 0.10 ug/L 1 -0.10 0.50 5A05015 - EPA:826OB/6230D 01/05/15 20:28 MSZ 1,3-Dichlorobenzene[541-73-11^. < 0.092 ug/L 1 - 0.092 0.50 5AO5015 EPA 82606/6230D 01/05/15 20:28 MSZ 1,3-Dichloropropane-[142-28-91^ < 0.15 ug/L 1 0.15 0.50 5AO5015 EPA 82606/6230D 01/05/15 20:28 MSZ 1,471Dichl6robenzene[106-46.7]^ < 0.10 ug/L 1 0.10 ,. 0.50 5AO5015 EPA 82606/6230D 01/05/15 20:28 M5Z 2,2-Dicfiloropropane [594-20-7]^ < 0.12 ug/L -1 ' .0.12 0.50 5A05015 EPA 82606/6230D 01/OS/15 20:28 MSZ 2-Chlorotoluene(95-49-8]^ < 0.10 ug/L 1 0.10 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:28 MSZ 4-Chlorotoluene [106-43-9]^. < 0.10 ug/L 1 0.10 0.50 SA05015 EPA 8260B/6230D 01/05/15 20:28 MSZ 4-Isopropyltoluene[99-87-6]A < 0.066 ug/L 1 0.066 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:28 MSZ Benzene[71-43-2]^ < 0:050 ug/L 1 0.050 0.50 . 5AO5015 EPA 82608/62.301) 01/05/15 20:28 MSZ 'Bromobehzene[108-86-1]^ < 0.13 ug/L 1 0:13 0.50 5A05015 EPA 82608/6230D 01/05/15 20:28 MSZ Bromochloromethane[74-97-5]^ < 0.11 ug/L 1 0.11 0.50 5AO5015 EPA 82.6OB/6230D 01/05/15 20:28 MSZ Bromodichloromethane [75-27-4]^ < 0.010 ug/L 1 0.010 0.50 SA05015 EPA 8260B/6230D 01/05/15 20:28 MSZ Bromoform [75-25-2]^ < 0.20 ug/L 1 0.20 0i50 5AO5015 EPA 8260B/6230D Ol/O5/15 20:28 MSZ Bromomethane[74-83-9]^. < 0.28 ug/L 1; 0.28 0.50 5AO5015 EPA 82606/6230D 01/6/15 20:28 MST Carbon Tetrachloride [56-23-5]^ < 0:082 ug/L 1 0.082 0.50 5AO5015 EPA 82606/62301) 01/05J15 20:28 MSz Chlorobenzene[108-90-7]^ - < 0.069 ug/L 1 0.069 0.50 5A05015 EPA 87608/62.30D 01/05/15 20:28 MS7. Chloroethane[75-00-3]^ < 0.18 ugJL I 0.18 0.50 5A05015 EPA 82608/6230D 01/05/15 2028 hISZ Chloroform [67-66-3]^ < 0.083 ug/L 1 0.083 0.50 5AO5015 EPA 82606/623OD 01/05/15 20:28 -MSZ Chloromethane[74-87-3]A .' < 0.050 ug/L :.1 0.050 0.50 5A05015 EPA 826013/62301) 01/05/15 20:28 MSZ - cis- 1,2'-Dichloroethene[156-59-2]^' < 0.075 ug/L 1 0.075 0.50 5AO5015 EPA 8260B/62300 01/05/15 20:28 MSZ cis- 1;3;Dichloropropene[10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 SA05015 'EPA 82606/6230D 01/05/15 20:28 MSZ Dibromochloromethane [124-48-1]^ < 0.067 ug/L 1 0.067 0:50 5A05015 EPA 8260B/6230D 01105/15 20:28 MSZ Dibromomethane[74-95-31^ < 0.13 ug/L 1 0.13 0.50 SAOS015 EPA 82608/6230D 01/05/15 20:28 MSZ,, DichlorodiFluorometIKane [75-71-81^ < 0.091 ug/L 1 0.091 0.50 5AO5015 EPA 82606/62301) 01105115 20:28 MSZ Ethylb6nzene[100-41-4]^ < 0.10 ug/L 1 0.10 0.50. 5AO5015 .EPA 8260B/6230D 01/05/15 20:28 MSZ Hexact lorobutadiene [87-68-3]^ < 0.15 ug/L 1 0.15 0.50 5A05015 EPA,82608/6230D 01/05/15 2028 MSZ Isopropyl Ether [108 20-3]^ < 0.20 ug/L 1 0.20 0.50 5AO5015 EPA 82.60B/62300 01/05/15 20:28 MSZ Isopropylbenzene [98-82-81^ e 0.13 ug/L 1 0.13 0.50 5A05015 EPA 82608/62.30D 01/OS715 20:28 MS7 m,p-Xylenes[108-3B-3/106-42-31^ c 0.18 ug/L 1 0.18 ` -0.50 5AO5015 EPA 8260B/6230D 01/0511:5 20:28 MSZ Methylene Chloride [75-09-2]A < 0.070 ug/L 1 0.070 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:28 MSZ MethylFtert-Butyl Ether [1634-04-4]^ < 0.12 ug/L 1 0.12 0.50 _ 5AO5015 EPA 8260B/6230D 01/05/15 20:28 MSZ Napht6alene[91-20-3]^ < 0.086 ug/L 1 0.086 0.50, 5AO5015 EPA,8260B/6230D 01/05/15 20:28 M57- - FINAL This report relates only to the sample as received by the.laboratory, .and may only be reproduced in Pull. Page 18 of 41 te. www.encolabs.com ANALYTICAL RESULTS Description: 141662-08 MW-39 Lab Sample ID:C500132-08 Received: 01/05/ I S 14:06 Matrix: Ground Water Sampled:12/31/14 15:21 Work Order: C500132 Project: Genral Subcontract Sampled By: CLIENT (Volatile Organic Compounds by GCMS ' ^ - ENCO Cary ce/tiried ana/yte [NC 591] Analyte rCAS Numberl Results Flan Units DF MDL Q Batch Method Analyzed By Notes n-Butyl Benzene[104-51-8]^ < 0.074 ug/L 1 0.074 0.50 5A05015 EPA 8260B/6230D 01/05/15 20:28 t•1SZ n-Propyl Benzene [103-65-1]^ < 0.073 ug/L 1 0.073 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:28 MSZ o-Xyldne[95-47-6]^ < 0.088 ug/L 1 0.088 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:28 MSZ sec-Butylbenzene[135-98-8]^ < 0.053 ug/L 1 0.053 0.50 5AO5015 EPA 82606/62.30D 01/05/15 20:28 1.15Z Styrene[100-42-5]^ < 0.082 ug/L 1 0.082 0.50 5AO5015 EPA 8260B/62.30D 01/05/15 20:28 MSZ. tert-Butylbenzenet98-06-6]^ < 0.094 ug/L 1 0.09.1 0.50 5A05015 EPA 8260B/6230D 01/05/15 20:28 MSZ. Tetrachloroethene[127-18-4]^ < 0.099 ug/L 1 0.099 0.50 5AO5015 LPA 82606/6230D 01/05/15 20.2S MSZ Toluene[108-88-3]^ < 0.053 ug/L 1 0.053 0.50 SA05015 EPA 8260B/62.30D 01/05/15 20:23 h1S7 trans-1,2-Dichloroethene [156-60-5]^ < 0.11 ug/L 1 0.11 0.50 5AO5015 EPA 8260B/62.30D 01/05/i5 20:2S 111SZ. trans-1,3-Dichloropropene[10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:28 %lSZ Trichloroethene[79-01-6]^ < 0.13 ug/L 1 0.13 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:28 MSZ Trichlorofluoromethane[75-69-4]^ < 0.15 ug/L 1 0.15 0.50 5A05015 EPA 82608/6230D 01/05/15 20:28 MSZ Vinyl chloride [75-01-4)^ < 0.083 ug/L 1 0.083 0.50 5AO5015 EPA 8260B/62300 01/05/15 20:28 %1S7 Xylenes(Total)[1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 5AO5015 EPA 8260B/6230D 01/05/15 20:29 MSZ Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyze d By Notes 4-29romofluorobenzene 56 1 50.0 113 % 53-136 5A05015 EPA 8260816230L 01/05/15 20:26 A15Z Dibromofluoromethane 54 1 50.0 108 % 67-129 5A05015 EPA 8260B16230C O1105115 20.28 A15Z T2luene-0 59 1 50.0 117 4b 59-134 5A05015 EPA 8.260616Z30L 01/03/1` ?l� �s 5•i FINAL This report relates only to the sample as received oy the. laboratory, and may only be reproduced in lull. Page ' 9 of 4 1 Description: 141662-06 MW-40 Matrix: Ground Water Project: Genral Subcontract ANALYTICAL RESULTS -� Lab Sample 3D:C500132-06 Sampled: 12/31/14 14:58 Sampled By:CLIENT . r ] pf grz� u www.encolabs.com Received: 01 /05/ 15 11:06 Work Order: C500132 IV61atile Organic Compounds by GCMS ^ - ENCO Cary certified analyfe [NC 591] Analvte rCAS Numberl Results Flan Units DF MDL PPOL Batch Method 'Analyzed 1y Notes 1,1,1,2-,Tetrachlorcethane [630-20-6]^ < 0.091 ug/L 1 0.091 0.50 5AO6013 EPA 82608/6230D 01/06/15 13:16 MSZ 1,1,1-Teichloroethane[71 55 6]^ < 0.15 ug/L 1 0.15 0.50 5A06013 EPA •8260B/6230D 01/06/15 13:16 MSZ 1,1,2,2-iTetrachloroethane [79-34-5]^ < 0.085 ug/L 1 0.085 0.50 SA06013 EPA 82608/6230D O1/06/15 t3:16 MSZ 1,1,2-Trichloroethane [79-00-5]1• < 0.068 ug/L 1 0.068 0.50 5AO6013 EPA 82.60B/6230D -01/06/15 13:16 Msz. 1,1-Dic'tloroethane [75 34-3]^ < 0.050 ug/L 1 0.050 0.50 SA06013 EPA 8260B/6230D 01/06/15 13:16 MSZ 1,1-Dichloroethene [75-35-4]^ < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 8260B/6230D 01/06/15 13:16 MS7 1,1-Dichloropropene[563-58-6]^ < 0.063 ug/L 1 0.063 0.50 5A06013 EPA 82606/6230D 01/06/15 13:16 MSz 1,2,3 T�ichlarobenzene [87-61-6]^ < 0.25 ug/L 1 0.25 0.50 SA06013 EPA 8260B/6230D 01/06/15 13:16 MSZ 1,2,3-TIichloropropane (96-18-4]^ < 0.15 ug/L 1 0.15 0.50 . 5A06013 EPA 8260B/6230D 01/06/15 13:16 MSZ 1,2,4-Trichlorobenzene[120-82-1]^ < 0.097 ug/L 1 0.097 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:16 MSZ 1,2,4-T'�imethylbenzene[95-63-6]^ < 0.067. ug/L 1 0.067 0.50 SA06013 EPA 8260B/6230D 01/06/15 13:16 MSZ 1,2-Dibromo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 SA06013 EPA 8260B/6230D 01/06/15 13:16 MSZ 1,2-Dibromoethane[106-93-4]^ < 0.27 ug/L 1 0.27 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:16 MSZ 1,2-Dichlorobenzene[95-5.0-1]^ < 0.062 ug/L 1 0.062 '0.S0 SA06013 EPA 8260B/6230D 01/06/15 13:16 MSZ 1,2-DicIhioroethane(107-06.2)^ < 0.082 ug/L 1 0.082, 0.S0 5AO6013 EPA 8260B/6230D 01/06/15 13:16 MSZ 1,2-Dichloropropane[78-87-5]^ < 0.098 ug/L 1 0.098 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:16 MSZ 1,3,5-Trimethylbenzene[108-67-8]^ < 0.10 ug/L, 1 0.10 0.50 5AO6013 EPA 8260B/6230D. 01/06/15 13:16 MSZ 1,3-Dichlorobenzene[541-73-1].^ < 0.092 ug/L 1 0.092 0.50 5AO6013, EPA 8260B/6230D 01/06/15 13:16 MSZ 1,3-Dichloropropane [142-28-9] ^ < 0.15 ug/L' 1 0.15 0.50 5A06013 EPA 8260B/6230D 01/06/15 13:16 MSZ 1,4-Dichlorobenzene [106-46-7]•^ < 0.10 ug/L 1 0.10 0.50 5AO6013 EPA 82608/6230D 01/06l15 13:16 h15Z 2,2-Dic61oropropane(594-20-7)^ < 0.12 ug/L 1 0.12 0.50 5A06013 EPA 82608/6230D 01/06/15 13:16 MSZ 2-Chlorotoluene[95-49-B]^ < 6.10 ug/L 1 0.10 0.50 SA06013 EPA 82608/6230D 01/06/15 13:16 h1sZ < 0.10 ug/L 1 0.10 - 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:16 I.1SZ 4-Chlorlotoluene[106-43-4]^ 4-Isop [99-87-6]^ < 0.066 ug/L 1 0.066 0.50 5A06013 EPA 8260B/6230D 01/06/15 13:16 M5z Iopyltoluene Benzen�e[71-43-2]^ < 0.050 ug/L 1 0.050 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:16 MSz Bromo6enzene[108-86-1]^ < 0.13 ug/L 1 0.13 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:16 _ MS"!. Bromochloromethane (74-97-5]^ < 0.11 ug/L 1 0.11 0.50 SA06013 EPA 82606/62301) 01/06/15 13:16 MSz. Bromodichloromethane r75-27-41^ < 0.010 ug/L .1 0.010 0.50 5A06013 EPA 82.60B/6230D 01/06/15 13:16 MSZ Bromo orm [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 SA06013 EPA 8260B/6230D 01/06/15 13:16 fizz Bromomethane [74-83-9]^. < 0.28 ug/L 1 0.28 0.50 5A06013 EPA 8260B/6230D 01/06/15 13:16 MS"L Carbon Tetrachloride [56-23-5]^ < 0.082 ug/L 1 0.082 0.50 5A06013 EPA 82.60B/6230D 01/06/15 13:16- NISZ Chlorobenzene[108 90 7]^ < 0.069 ug/L 1 0.069 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:16 MSZ Chlorocethane[75-00-3]^ < 0.18 ug/L 1 0.18 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:16 MSZ Chloroform [67-66-3]^ < 0.083 ug/L 1 0.083 0.50 5A06013 EPA 8260B/6230D 01/06/15 13:16 MSZ Chloromethane[74-B7-3]^ - < 0.050 ug/L 1 0.050 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:16 MSz ^ cis-1,2�Dichloroethene,[156-59-2] � < 0.075 ug/L 1 0.075 0.50 SA06013 EPA 8260B/6230D EPA,8260B/6230D 01/06/15 13:16 MS7_ < 0.073 ug/L 1 0.073 0.50 . SA06013 EPA 8260B16230D 01/06/15 13:16 MSZ Dibromochloromethane [124-48-1]^ < 0.067 ug/L 1 0.067 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:16 t4sZ Dibromomethane [74.95-3]^ < 6.13 ug/L 1 0.13 0:50 5A06013 EPA 8260B/6230D 01/06/15 13:16 MSZ Dichlor..odifluoromethane[75-71-8]^ < 0.091 ug/L 1 0.091 0.50, SA06013 EPA.8260816230D 01/06/15 13:16 MS7 Ethylbenzene[100-41-4]^ < 0.10 ug/L 1 0.10 0.50 SA06013 EPA 8260B/6230D 01/06J15 !3:16 MS7. Hexachlorobutadiene[87-68-3]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 82606/6230D 01/06/15 13:16 hlSZ Isopropyl Ether[108 20 3]^ < 0.20 ug/L 1 0.20 0.50 5A06013, EPA 82608/6230D 01/06/15 13:16 MSZ Isopropylbenzene[98-82-8]^ < 0.13 ug/L 1 0.13 0.50 SA06013. EPA 82.608/6230D O1/06/15 t3:16 615% m,p-Xylenes [108-38-3/106-42-3]^ < 0.18 ugJL 1 0.18 0.50 5AO6013 EPA 8260B16230D 01/06115 13:16 1.15Z Methylene Chloride [75-09-2]^ < 0.070 ug/L 1 0.070 0.50 5AO6013 'EPA 82608!6230D 01/06/1S !3:16 MSZ Methyl-tert-Butyl Ether [1634-04-4]^ < 0.12 ug/L 1 0.12 0.50 5AO6013 EPA 8260B16230D 01/06/15 13:16 MSZ Naphthalene [91.20 3]^ < 0.086 ug/L 1 0.086 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:16 MS7 This report relates only to the sample as received by the laboratory, and may only be reproduced in full. - i'ago IA. of 41 FINAL I ANALYTICAL RESULTS I Description: 141662-06 MW-40 Matrix: Ground Water j Project: Genral Subcontract Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte (NC 5911 Analyte rCAS Numbed Results n-ButyliBenzene [104-51-8]^ < 0.074 n-Propyl Benzene [103-65-1]^ < 0.073 o-Xylen'e [95-47-6]^ < 0.088 sec-But!1benzene [135-98-8]^ < 0.053 Styrene [100-42-5]^ < 0.082 tert-Buiylbenzene [98-06-6]^ < 0.094 Tetracliloroethene [127-18-4]^ < 0.099 Toluene (108-88-3]^ < 0.053 trans-1',2-Dichloroethene [ 156-6D-5]^ < 0.11 trans-1,3-Dichloropropene [10061.02-6]^ < 0.080 Trichloroethene [79-01-6]^ < 0.13 Trichloiofluoromethane [75-69-4]^ < 0.15 Vinyl chloride [75-01-4]^ < 0.083 Xylenes(Total)[1330-20-7]^ < 0.22 Surrd ates Results 4-Bromofluorobenzene 58 Oibromofluoromethane 56 Toluene-d8 S9 Lab Sample ID:C500132-06 Sampled: 12131/14 14:58 Sampled By: CLIENT www.encolabs.com Received: 01/05/15 14:06 Work order: C500132 FIa4 Units DF MDL PPOL- Batch Method Anal Ay Notes ug/L 1 0.074 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:16 MSZ ug/L 1 0.073 0.50 5AO6013 EPA 82.60B/6230D 01/06/15 13:16 h15Z ug/L 1 0.088 0.50 5AO6013 LPA 8260B/6230D 01/06115 13:16 MSZ ug/L 1 0.053 0.50 SA06013 EPA 8260B/6230D 01/06/15 13:16 MSZ ug/L 1 0.082 0.50 5AO6013 EPA 82.6OB162.30D 01/06/15 13:16 MSZ ug/L 1 0.094 0.50 SA06013 EPA 82.60B/6230D 01/06/15 13:16 MSZ ug/L 1 0.099 0.50 5AO6013 EPA 82606/6230D 01/06/15 13:16 MSZ ug/L 1 0.053 0.50 bA06013 EPA 8260B/6230D 01/06/15 13:16 MSZ ug/I 1 0.11 0.50 5AO6013 FPA 82608/5230D 01106/1; 1 i tip h1S7 ug/L 1 0.080 0.50 5AO6013 EPA 82608/5230D 01/06/15 13:16 MSZ ug/L 1 0.13 0.50 5A06013 EPA 82606/6230D 01/06/15 13:16 I.15Z ug/L 1 0.15 0.50 5AO6013 EPA 8260B/6230D 01/06/15 13:16 h1SZ ug/L 1 0.083 0.50 SA06013 EPA 8260B/6230D 01/06/15 13:16 MSZ. ug/L 1 0.22 0.50 5A06013 EPA 8260B/6230D 01/06/15 13:16 MSZ OF Spike Lvl °7o Re c % Rec Limits Batch Method Analyze d Ay Notes 1 50.0 117 % 53-136 5AD6013 EPA 826OB16230C 01106115 13:16 A15Z 1 50.0 112 % 67-i29 5AD6013 EPA 8260B/6230L 01106115 13:16 m5Z 1 50.0 118 % 59-134 5AO6013 EPA 82608/6230L 01106115 13:16 A:5Z FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. rage 15 0l at µ� 1;� www.encolabs.com ANALYTICAL RESULTS De cription: 141662-05 MW-41 Lab Sample ID:C500132-OS Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 14:44 Work Order: C500132 Project: Genral Subcontract Sampled By: CLIENT Vi6latile Organic Compounds by GCMS ^ - ENCO Cary cer ified analyte (NC 5911 Anal A Number Tetrachloroethane [630-20-6]^ Results Flag < 0.091 Units ug/L DF 1 MDL 0.091 PPOL 0.50 Batch SA06013 Method EPA 82.60B/6230D Analyzed 01/06/15 20:06 §y Notes MSZ. 1,1,1,2 1,1,1-T�ichloroethane [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5A06013 EPA 8260B/6230D 01/06/15 20:06 MSz 1,1,2,2 Tetrachloroethane (79-34-5]^ < 0.085 ug/L 1 0.085 0.50 5AO6013 EPA 8260B/6230D 01/06/15 20:06 f-ISZ 1,1,2.T�ich.loroethane [79-00-5]^ < 0.068 ug/L 1 0.068 0.50 5A06013 EPA 82608/6230D 01/06/15 20:06 MSz 1,1-Dicll'loroethane[75-34-3]^ < 0.050 ug/L 1 0.050 0.50 5A06013 EPA 82608/6230D 01/06/15 20:06 MSz 1,1-Dichloroethene (75-35-4]^ < 0.15 ug/L 1 0.15 .0.50 SA06013 EPA 82606/62301) 01/06/15 2.0:06 MSz 1,1-Dichloropropene[563.58,-6]^ < 0.063 ug/L 1 0.063 0.50-5A06013 EPA 8260B/6230D 01/06/15 20:06 MSz 1,2,3-T ichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0.25 0.50 SA06013 EPA 82.606/6230D 01/06/15 20:06 MSz 1,2,3-Tichloropropane[96-18-4]^ < 0.15 ug/L 1 0.15 '0.50 5AO6013 EPA 8260B/6230D 01/06/15 20:b6 M5L 1,2,4-Tichlorobenzene[120-82-1]^ < 0.097 ug/L 1 0.097 0.50 5AO6013 EPA 826013/62301) 01/06/15 20:06 MSz 1,2,4-Timethylbenzene[95-63-6]^ < 0.067 - ug/L 1 0.067 0.50 SA06013 EPA 8260B/6230D 01/06/15 20:06 MSL 1,2-Dib omo-3-chloropropane'[96-12-8]^ < 0.48 ug/L 1 0.48 0.50 SA06013 EPA 82606/6230D, 01/06/15 20:06 MSz 1,2-Dib omoethane[106-93-4]^ < 0.27 ug/L 1 0.27 0.50 5A06013 EPA 82608/6230D 01/06/15 20:06 MSz 1,2-Dic lorobenzene [95-50'-1]^ < 0.062 ug/L 1 0.062 0.50 5AO6013 EPA 8260B/6230D 01/06/15 20:06 i•ISZ 1,2-Dic loroethane[107-06-2]^ < 0.082' ug/L 1 0.082 0.50 SA06013 EPA 82608/6230D 01/06/15 20:06 MSz 1,2-Dic I ropropane(78-87-5]^ < 0.098 ug/L 1 0.098 0.50 5AO6013 EPA 82608/6230D 01/06/15 20:06 MSz 1,3,5-T�imethylbenzene[168-67-8]^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 82606/6230D 01/06/15 20:06 MSZ 1,3-Dic ilorobenzene[541-73-1]^ < 0.092 ug/L 1 0.092 0.50 SA06013 EPA 8260B/6230D 01/06/15 20:06 MSZ 1,3-Dic iloropropane(142-28-9]^ < 0.15 ug/L 1 0;15 0.50 -5A06013 EPA 8260B/6230D 01/06/15 20:06 MSz 1,4-Dic ilorobenzene[106-46-7]^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 82606/6230D '01/06/15 20:06 MSZ. 2,2-1)ic iloropropane[594-20-71^ < 0.12 ug/L 1 0.12 0.50 SA06013 EPA 8260B/6230D .01/06115 20:06 MSZ 2-Chlor toluene[95-49.8]^ < 0.10 ug/L 1- 0.10 0.50 SA06013 EPA 82606/6230D 01/06/15 20:06 t15z 4-Chlor Dtol6ene[106-43-4]^ < 6.10 ug/L 1 0.10 0.50 5AO6013 EPA 82606/6230D 01/06/15 20:06 MSz 4 lsopr pyltoluene [99 87 6]^ < 0.066 ug/L 1 0.066 0.50 5AO6013 EPA 8260B/62300 01/06/15 20:06 MSZ -Benien (71-43-21^ < 0.050 ug/L 1. 0.050 0.50 5AO6013 EPA 82606/6230D 01/06/15 20:06 MSZ Bromd enzene[108-86-I]^ < 0.13 ug/L t 0.13 0.50 5AO6013 EPA 82606/6230D 01/06/15 20:06 MSZ Bromo hloromethane (74-97-5]^ < 0.11 ug/L 1 0.11 0.50 5AO6013 EPA 8260B/6230D 01/06/15 20:06 MSz . Bromo ichloromethane [75-27-4]^ < 0.010 ug/L 1 0.010 0.50 - 5A06013 EPA 82608/6230D 01/06/15 20:06 MSz Bromofbrm [75-25-2]^' < 0.20 ug/L 1 0.20 0.50 SA06013 EPA 8260B/6230D 01/06/15 20:06 t•ISZ Bromomethane[74-83-9]^ < 0.28 ug/L 1 0.28 0.50 SA06013 EPA 82608/62301) 01/06/15 20:06 MSZ Carbon Tetrachloride [56-23-5]^ < 0.082 ug/L 1 UK 0.50 5AO6013 EPA 8260B/6230D 01/06/1S 20:06 MSZ Chlonot lenzene[10.8-90-7]^ < 0.069 ug/L 1 0.069 0.50 5AO6013 EPA 826013/62301) 01/06/15 20:06 MSZ Ch-lor thane[75-00-3]^ < 0.18 ug/L 1 0.18 0.50 5A06013 EPA 8260B/6230D 01/06/15 20:06 MSz Chloro rm [67-66-3]^ < 0.083 ug/L 1 0.083 0.50 SA06013 EPA 8260B/6230D 01/06/15 20:06 MSZ Chloro ethane[74-87-3]^ < 0.050 ug/L 1 0.050 0.50 5AO6013 EPA 8260B16230D 01/06/15 20:06 MSz cis-1,2 Dichloroethene[156-59-2]^ < 0.075 ug/L 1 0.075 0.50 5A06013 EPA 8260B/6230D 01/06/15 20:06 MSz cis-1,3 Dic hloropropene[10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 SA06013 EPA 82608/6230D 01/06/15 20:06 MSZ Dibro ochloromethane [124-48-1]^ < 0.067 ug/L 1 0.067 0.50 5A06013 EPA 8260B/6230D 01/06/15 20:06 MSz Dibro omethane[74-95-3]^ < 0.13 ug/L 1 0.13 0.50 SA06013 EPA 8260B/6230D 01/06/15 20:06 MS7 Dichlor diFluoromethane [75-71-8]^ < 0.091 ug/L 1 0.091 0.50 5AO6013 EPA 8260B/62300 01/06/15 20:06 MSz Ethylb nzene [100-41-4]^ < 0.10 ug/L 1 0.10 0.50 5A06013 EPA 826013/62301) 01/06/15 20:06 MR Hexac lorobutadiene [87-68-3]^ < 0.15 ug/L 1 0.15 0.50'. 5AO6013 EPA 8260B162.3OD' 01/06/15 20:06 MSZ Isopro ylEther [108-20-3]^ < 0.20 ug/L 1 0.20 0.50 5AO6013 EPA 82.608/6230D 01/06/15 20:06 MS7 Isopro ylbenzene [98-82-8]^ < 0.13 ug/I. 1 0.13 0.50 5AO6013 EPA 82.60B16230D 01/06/15 20-06 MSZ m,p-X lenes[108-38-3/106-42-3]^ < 0.18 ug/L 1 0.13 0.50 SA06013 EPA 8260B16230D 01/06/15 20:06 ht52 Methyl�ne Chloride [75-09-2]^ < 0.070 ug/L 1 0.070 0.50 SA06013 EPA 8260B/62301) 01/06/15 20:06 I•ISz Methyl tert-Butyl Ether [1634,04-4]^ < 0.12 ug/L 1 0.12 0.50 5AO6013 EPA 8260B/6230D 01/06/15 20:06 MSZ Napl[ alene[91-20-3]^ < 0.086 ug/L 1 0.086 0.50 5A06013 EPA 82608/6230D 01/06/15 20:06 114S7 FINAL _ - I This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page '" o: <: www.encolabs.com ANALYTICAL RESULTS :ription• 141662-05 MW-41 Lab Sample ID:C500132-05 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 14:44 Work Order: C500132 Project: Genral Subcontract Sampled By: CLIENT IVblatile Organic Compounds by GCMS J ENCO Cary certified analyte (NC 5911 ^1CAS Anal t Number l Results Flag Units DF MDL PPL Batch Method 'Analyzed 1� Notes n-Butyl Benzene[104-51-8]^ < 0.074 ug/L 1 0.074 0.50 5AD6013 EPA 8260B/6230D 01/06/15 20:06 N157. n-Prop Benzene[103-65-1]^ < 0.073 ug/L 1 0.073 0.50 SA06013 EPA 826OB/6230D 01/06/15 ?0:06 h1SZ o-Xylen2I[95-47-6]^ < 0.088 ug/L 1 0.088 0.50 SA06013 EPA 8260B/6230D 01/06/15 20:06 bISZ sec-Butjllbenzene[135-98-81^ < 0.053 ug/L 1 0.053 0.50 5AO6013 EPA 8260B/6230D 01/06/15 20:06 MSZ Styren [100-42-5]^ < 0.082 ug/L 1 0.082 0.50 5AO6013 EPA 8260B/6230D 01/06/15 20:06 f•15Z tert-Bulbenzene[98-06-6]^ < 0.094 ug/L 1 0.094 0.50 SA06013 EPA 82606/6230D 01/06/15 20:06 MSZ TetrachlllIlloroethene [127-18-4]^ < 0.099 ug/L 7 0.099 0.50 5A06013 EPA 82608/6230D 01/06/15 20:06 MSZ Toluen( [108-88-3]^ < 0.053 ug/L 1 0.053 0.50 SA06013 EPA 82608/6230D 01/06/15 ?D:06 MSZ trans- 1, 2-Dichloroethene [156-60-5]^ < 0.11 _ ug/I. 1 o.i1 0.50 SA06013 EPA 826013/62301) 01/06/15 '0:^6 MSZ trans- 1, 3-Dichloropropene [10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 5AO6013 EPA 8260B/6230D 01/06/15 20:06 f•15Z Trichlo ethene [79-01-6)^ < 0.13 ug/L 1 0.13 0.50 5A06013 EPA 8260B/6230D 01/06/15 20:06 ntSZ Trichlor ofluoromethane[75-69-4]^ < 0.15 ug/L 1 0.15 0.50 5AO6013 EPA 82608/6230D 01/06/15 20:06 h1SZ Vinyl c loride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 5A06013 EPA 8260B/6230D 01/06/15 20:06 MSZ Xylene.(Total)[1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 5AO6013 EPA 8260B/6230D 01/06/15 20:06 r•ISZ Results OF Spike Lvl % Rec 0/n Rec Limits Batch Method Analyzed �gy Notes 58 1 50.0 116 °n 53-136 5AO6013 EPA 82606/6230L 01106115 2006 ASSZ 58 1 50.0 116 % 67-129 5AO6013 EPA 826OB16230L 01/06/1520:06 AISZ 62 1 50.0 125 % 59-134 5AO6013 EPA 826OB16230C 01/06/15 20:06 h15Z This report relates only to the sample as received by the laboratory, and may only be reproduced in full. :,age "f of 4 , . www.encolabs.com ANALYTICAL RESULTS cription• 141662-04.MW-42 • Lab Sample ID:C500132-04 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 14:30 Work Order: C500132 Project: Genral Subcontract Sampled By:CLIENT IVblatile Organic Compounds by GCMS ^ - fNCO Cary rertilred analyte [NC 5911 Anal rCASNumberl Results Flan Units DF MDL Q Batch Method Analyzed _By Notes 1,1,1,2 etrachlorcethane [630-20-6]^ < 0.091 ug/L 1 0:091 0.50 5AO5015 EPA. 8260B/6230D 01/05/15 18:25 I•ISz 1,1,1-Tiichloroethane [71-55-6]^ < 0.15 ug/L - 1 0.15 0.50 5A05015 EPA 8260B/6230D 01/05/15 18:25 MSz 1,1,2,217etrachloroethane[79-34-5]^ < 0.085 ug/L 1 0.085 0.50 5AO5015 EPA 82608/6230D 01/05/15 18:25 MSZ 1,1,2-Tfllichloroethane[79-00.5)^ <'0.068 ug/L 11" 0.068 0.50 5AOS015 EPA 82608/6230D O1/O5/15 18:25 MSZ 1,1-DicLroethane[75-34-3)^ < 0.050 ug/L 1 0.050 0.50 5A05015 EPA 8260B/6230D 01/05/15 18:25 h1SZ 1,1-Diclloroethene[75-35-4)^ < 0.15 ug/L 1 0.15 0.50 5AO5015 EPA 82608/6230D 01/05/15 18:25 MSz 1,1-Dichioropropene[563-58-6]" < 0.063 ug/L 1 0.063 0.50 5A05015 EPA 8260B16230D 01/05/15 18:25 hIST 1,2,3-T ichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0.25 , 0.50 5AO5015 EPA 8260B/6230D 01/05/15 18:25 Hs/ 1,2,3-Tichloropropane[96-18-4]^ < 0.15 ug/L 1 0.15 0.50 5A05015 EPA 82606/6230D 01/05/15 18:2.5 MS7. 1,2,4-T�ichiorobenzene[120-82-1]^ < 0.097 ug/L 1 0.097 0.50 5A05015 EPA 8260B/6230D 01/05115 18:25 MSZ 1,2,4-TlIimethylbenzene [95-63-6]^ < 0.067 ug/L 1 0.067 0.50 5AO5015 EPA 8260B/6230D 01/05/15 18:25 Msz 1;2-Dibtomo-3-chloropropane (96-12-8)^ < 0.48 ug/L 1 0.48 0.5o SA05015 EPA 82608/62301) 01/05/15-18:2.5 145z 1,2-Dibfomoethane [106-93.4]^' < 0.27 ug/L 11 0.27 0.50 SA05015 FPA 82.608/62301) 01/05/15 18:25 MS7 1,2-Dicl1I1orobenzene[95-50-1]^ < 0.062 ug/L 1 0.062 0.50 5AO5015 EPA 8260B/6230D 01/05/I5 18:25 hlSz 1,2-Diciloroethane(107-06-2)^. < 0.082 ug/L 1 0.082. 0.50 5AO5015 EPA 82608/6230D 01/05/15 18:25 M5Z 1,2-Dichloropropane[78-87-5]^ < 0.098 ug/L 1 0.098 0.50 5AOS015 EPA 8260B/6230D 01/05/15 18:25 145Z 1,3,5-Timethylbenzene[10B-67-8]^ < 0.10 ug/L 1 0.10 0.50 SA05015 EPA 826013/6230D 01/05/15 18:25. MSZ 1,3-0ic iiorobenzene [541-73-1]^ < 0.092 ug/L 1 0.092 0.50 SA05015 EPA 826013/62301) 01/05/15 18:25 MSz 1,3-Dic loropropane[142r28-9]^ < 0.15 ug/L 1 .0:15 0.50 5AO5015 EPA 82608/62301) 01!05/15 18:25 MSz 1,4-Dic,lorobenzene [106-46-7]^ < 0.10 ug/L 1 0.10 0.50 SA05015 EPA 82.606/6230D 01/05/15 13:25 MS7- i 2,2-Diclhloropropane [594-20-7]^ < 0.12 ug/L 1 0.12 0.50 5AO5015 EPA 82.608/62300 01/05/15 18:25 MSZ 2-ChlorlbItoluene[95-49-B]^ < 0.10 ug/L 1 0.10 0.50 5AO5015 EPA 826013/6230D 01/05/15 18:25 MSZ 4-Chlorbtoluene[i06-43-4]^' < 0.10 ug/L 1. 0.10 0.50 5AO5015 EPA 82.608/62301) 01/05/15 18:25 I'lSZ 4-Isopr pyltoluene[99-87-6]^ < 0.066 ug/L 1 .0.066 0.50 5AO5015 -EPA 826OB/6230D 01/05/15 18:25 MSZ Benzeilh[71-43-2]^ < 0.050 ug/L 1 0.050 0.50 SA05015 EPA 8260B/6230D 01/05/15 18:25 t45Z Bromodenzene[108-86-1]^ < 0.13 ug/L '1 0.13 0.'50 5AO5015 EPA 82606/6230D 01/05/15 18:25 MSZ BromolIloromethane [74-97-5]^ < 0.11 ug/L 1 0.11 0.50 5AO5015 EPA 826013/6230D 01/05/15 18:7.5 MSZ bromodichloromethane [75,-27-41^ < 0.010 ug/I. 1 0.010 0.50 5A05015 EPA 82608/6230D 01/05/15 1S 25 ; 57 Bromof�rm [75-25-2]^ < 0.20 ug/L <1 0.20 0.50 5AO5015 EPA 82606/6230D 01/05/15 18:25 MSZ Bromorilethane (74-83-9]^ < 0.28 ug/L 1 0.28 0.50 5A05015 FPA 82608/6230D 01/05/15 1 1: 25 hISZ " Carbon Tetrachloride [56-23-S]^ < 0.082 ug/I 1. 0.082 0.50 5AO5015 FPA 82.608/6230D 01/05/15 18,25 %Isz Chloro_ nzene![108-90-7]^ < 0.069 ug/L 1 0.069 0.50 5AO5015 EPA 8260B/6230D 01/05/15 18:25 r•IS7. Chlor hane[75-00-3]^ < 0.18 ug/L 1 0.18 0.50 5AO5015 EPA 82606/6230D 01/65/15 18:25 MSZ Chlorof rm [67-66-3]^ < 0.083 ug/L 1 0.083 0.50 5AO5015 EPA 8260B/6230D 01/05/15 18:25 MSZ Chlorom.ehare (74-87-3)^ < 0.050 ug/L 1 0.050 0.50 5A05015 EPA 82608/62301) 01/05/15 18:25 MSZ cis-1,2- ichloroethene(156-59r2)^ <.0.075 ug/L 1 0.075 0.50 5AO5015 EPA 82608/62301) 01/05/15 18:25 MSZ cis-1,3- ichloropropene[10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 SAOS015 EPA 82608/6230D 01/05/15 18:25 MSZ Dibromochloromethane[124-48-1]^ < 0.067 ug/L 1- 0,067 0.50 SA05015 EPA 826013/6230D 01/05/15 18:25 MSZ Dibrom methane [74-95r3]^ , < 0.13 ug/L 1 0.13 0.50 SA05015 EPA 8260B/6230D 01/05/15 18:25 hISZ Dichlor di0uoromethane[75-71-B]^ < 0.091 ug/L 1 0.091 0.50 - 5AO5015 EPA 8260B/6230D 01/05/15 18:25 M57 Ethylbe zene[100-41-4]^ < 0.10 ug/L 1 0.10 0.50 SA05015 EPA 82608/6230D 01/05/1S 18:25 MSZ Hexach orobutadiene [87-68-3]^ < 0.15 ug/L 1. 0.15 0.50 5AO5015 EPA 82608/6230D 01/05/15 18:25 MSz Isopro I Ether[108-20-3]1 0.20 ug/L 1 0.20 0.50 + 5AO5015 EPA 82608/6230D 01/05/15 18`:25 MS7 .< Isopro;Ibenzene[98-82-8)^ < 0.13 ug/L 1 0.13 0.50 5A05015 EPA 82.60B/6230D 01/05/115 18:25 MSZ m,p-Xyl�Ines [108-38-3/106-42-3]^ < 0.16 ug/L 1 0.18 0.50 5A05015 EPA 82608/62300 01/05/15 18:25 I•ISL Methylene Chloride[75-09-2]^ < 0.070 ug/L 1 0.070 0.50 5AO5015 EPA 82608/6230D 01/05/15 18:2.5 MSZ Methyl- ert-Butyl Ether[ 1634-04-4]A < 0.12 ug/L 1 0.12 0.50 5AO5015 EPA 8260B/62.3ob 01/05/15 18:25 MSZ Naphthllene[91-20-3]^ < 0.086 ug/L 1 0.086 ,- 0.50 .5AO5015 EPA 82606/62301) 01/05/15 18:2.5 M57. FINAL. This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 4. Ae 3k S3 °r `t www.encolabs.com t ANALYTICAL RESULTS y ;ription: 141662-04 MW-42 Lab Sample ID:C500132-04 Received: 01/OS/15 14:06 Matrix: Ground Water Sampled:12/31/14 14:30 Work Order: C500132 Project: Genral Subcontract Sampled By: CLIENT IVblatile Organic Compounds by GCMS J ^ - ENCO Cary cerrirred analyre [NC 591] Anal CAS Numb r Results Flaa Units DF MDL PPL Batch Method Analyzed fly Notes n-ButyllBenzene[104-51-8]^ < 0.074 ug/L 1 0.074 0.50 5AO5015 EPA 8260B/6230D 01,05/15 18:25 r•ISZ n-PropyII Benzene [103-65-1]^ < 0.073 ug/L 1 0.073 0.50 5AO5015 EPA 8260B/6230D 01/05/15 18:25 MSZ o-Xylene [95-47-6]^ < 0.088 ug/L 1 0.088 0.50 5A05015 EPA 8260B16230D 01/05/15 18:25 NISI sec-ButlIilbenzene[135-98-8]^ < 0,053 ug/L 1 0.053 0.50 5AO5015 EPA 8260B/6230D 01/05/15 18:25 MSZ Styrene[100-42-5]^ < 0.082 ug/L 1 0.082 0.50 5AO5015 EPA 82608/6230D 01/05/15 18:25 MSZ tert-Bu ylbenzene[98-06-6]^ < 0.094 ug/L 1 0.094 0.50 SA05015 EPA 8260B/6230D 01/05/15 18:25 MSZ Tetrachloroethene[127-18-4]^ < 0.099 ug/L 1 0.099 0.50 5AO5015 EPA 8260B/6230D 01/05/15 18:25 r•15Z Toluen,[108-88-3]^ < 0.053 ug/L 1 0.053 0.50 5AO5015 EPA 8260B/6230D 01/05/15 18:25 MSZ i trans-d2-Dichloroethene [156-60-5]^ < 0.11 ug/I 1 0.11 0.50 SA05015 FPA 82608/6230D 01/05/15 18:25 MS7 trans- 1 i 3-Dichloropropene [10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 5A05015 EPA 82606/6230D 01/05/15 18:25 tSZ. Tdchlo oethene[79-01-6]^ < 0.13 ug/L 1 0.13 0.50 5AO5015 EPA 82606/6230D 01/05/IS 18:25 MSZ Trichlo ofluoromethane [75-69-4]^ < 0.15 ug/L 1 0.15 0.50 5A05015 EPA 8260B/6230D 01/05/15 18:25 MSZ Vinylchloride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 5AO5015 EPA 8260B/6230D 01/05/15 18:25 MSZ_ Xylene (Total)[1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 5AO5015 EPA 8260B/6230D 01/05/15 18:25 MSZ Results OF Soike Lvl % Re c % Rec Limits Batch Method Analyzed —BY Notes 56 1 50.0 112 % 53-136 5AO5015 EPA 826OB16230L 01105,,115 18:25 A1SZ 51 1 50.0 101 9" 67-129 5AO5015 EPA 826OB16230C 01105115 18:25 M11SZ 59 1 50.0 116 % 59-134 5AO5015 EPA 826OB16230C 01105115 18:25 M5Z FINAL This report relates only to the Sample as received by the laboratory, and may only be reproduced in full. Page 1' of c www.encolabs.com ANALYTICAL RESULTS i 5cription• 141662-02 MW-43 Lab Sample ID:C500132-02 Received: 01/05/15 14:06 I Matrix: Ground Water Sampled:12/31/14 14:06 Work Order: C500132 I Project: Genral Subcontract Sampled By: CLIENT , IVblatile Organic Compounds by GCMS f ^ - ENCO Cary cL&rled analyte [NC 5911 Anal to rCAS Number] Results Flaa Units DF - _ MDL PAL Batch Method Analyzed _By Note 2ITetrachloroethane [630-20r6]^ < 0.091 ug/L 1 0.091 0.50 SA05015 EPA 82608/6230D 01/05/15 17:2.2 MS7- 1,1,1-Trichl t0h,anee [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5A05015 EPA 8260B/6230D 01/05/15 17:22 MSz 1,1,2,21 etrachloroethane [79-34-5]^ < 0.085 ug/L 1 06085 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:22 MSZ 1,1,2-Tiichloroethane[79-00-5]^ < 0.068 ug/L 1 0.068 0.50 5AO5015 EPA 826OB/6230D 01/05/15 17:22 MSZ 1,1-Dichloroethane [75-34-3]A < 0.050 ug/L 1 0.OSO 0.50 5AOS015 EPA 82608/6230D 01/05/15 17:22 MSZ 1,1-Dichloroethene[75-35-4]^ < 0.15 ug/L 1 0.15 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:22 MSZ I,1-Dichloropropene [563-58-6]^ < 0.063 ug/L 1 0.063 0.50 5A05015 EPA 8260B/6230D 01/05/15 17:22 MSZ 1,2,3-Trichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0.25 0.50 5AO5015 EPA 8260B16230D 01/05/15 17:22 MSZ 1,2,3-Trlichloropropane[96-18-4]^ < 0.15 ug/L 1 0.15 0.50 SA05015 EPA 8260B16230D 01/OS/15 17:22 msz i 1,2,4-Trj�ichlorobenzene(120-82-1]^ < 0.097 ug/L 1 0.097 0.50 5AO5015 EPA 8260B16230D 01/05/15 17:22 MSZ < 0.067 ug/L 1 0.067 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:22 MSZ 1,2;4-Tfimethylbenzene[95-63-6]^ 1,2 Dib�omo-3 chloropropane [96 12-8]^ < 0.48 ug/L 1 0.48 0.50 5AO5015 EPA 826OB/6230D 01/05/15 17:22 MSZ 1,2-Dibromoethane[106-93-4]^ < 0.27 ug/L 1 0.27 0.50 5A05015 EPA 8260B/6230D 01/05/15 17:22 MSZ 1,2-DiclhIlorobenzene[95-50-1]A < 0.062 ug/L 1 0.062 0.50 SA05015 EPA 82608/6230D 01/05/15 17:22 MSZ 0.082 ug/L 1 0.082 0.50 5AO5015 EPA 82606/6230D 01/05/15 17:22 lmsz 1,2-Dicfiloroethane[107-06-2]^ .< < 0,098 ug/L 1 0.098 0'.50 SA05015 EPA 8260B/6230D 01/05/15 17:22 hlSz 1,2-D41oropropane[78-87-5]^ 1,3,5-Thrnethylbenzene[108-67-8]^ < 0.10 ug/L 1 0.10 0.50 5AO5015 EPA 82606/6230D 01/05/15 17:22 hIS7 , 1,3-Dichlorobe6zene [541-73-1]^ . < 0.092 ug/L 1 0.092 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:22 MSZ 1,3 Dic�lloropropane [142 28 9]^ < 0.15 ug/L 1 0.15 0.50' .5AO5015 EPA 8260B16230D 01/05/15 17:22 MSZ 1,4-Dichlorobenzene [106-46-7]^ < 0.10 ug/L 1 0.10 0.50 5A05015 EPA 82608/6230D 01/05/15 17:22 MSZ 2,2-Dicloloropropane[594-20-7]^- < 0.12 ug/L 1 0.12 0.50 5A05015 EPA 82608/6230D 01/05/15 17:22 MSZ 2-Chlorptoluene [95-49-8]^ < 0.10 ug/L 1 0.10 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:22 MSZ .4-Chlorffotoluene[106-43-4]^ < 0.10 ug/L 1 0.10 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:22 MSZ 4-Isopropyltoluene[99-87-6]A < 0.066 ug/L 1 0.066 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:22 MSZ Benzenl [71-43-2]^ < 0.050 ug/L 1, 0.050 0.50 5A05015 EPA 8260B/6230D 01/05/15 17:22 MSZ Bromobenzene(108-86-1]^ < 0.13 ug/L 1 0.13 0.50 5A05015 EPA 8260B/6236D 01/05/15 17:22 MSZ Bromoghloromethane[74-97-5]'• < 0.11 ug/L 1 0.11 0.50 5A05015 EPA 8260B/6230D 01/05/15 17:22 MSz Bromodichloromethane [75-27.4]^ < 0.010 ug/L 1 0.010 0.50 5A05015 EPA 8260B/6230D 01/05/15 17:22 MS7. eromof�rm [75-25-2]" < 0.20 ug/L 1 0.20 0.50' 5A05015 EPA 82606/62301) 01/05J15 i7:22 h1SZ Bromorllethane [74-83-9]^ < 0.28, ug/L 1 0.28 0.50 5AOS015 EPA 8260B/6230D 01/05/15 17:22 h157. lllTetrachloride [56-23-5]^ Carbon < 0.082 ug/L 1 0.082 0.50 SA05015 EPA 8260B/6230D 01/OS/15 17:22 MSZ Chlorotenzene(108-90-71A < 0.069 ug/L 1 0.069 0.50 .5AO5015 FPA 8J-60B/6230D 01/05/15 i7:22 MSz Chloro2l[hane [75-00-3]" < 0.18 ug/L 1 0.18 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:22 M7. 5 Chloroform (67-66-3]^ < 0.083 ug/L 1 0.083 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:22 MS7 Chloror'ethane[74-87-3]^ < 0.050 ug/L 1 0.050 0.50 SA05015 EPA 82608/6230D 01/05/15 17:22 MS7_ cis•1,2.IDichloroethene [156-59-2]^ < 0.075 ug/L 1 0.075 0.50 5AO5015 EPA 8260B/6230D 01/05/15 1722 MSZ cis-1,3IDichloropropene [10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 -5AO5015 EPA 8260B/6230D 01/05,115 17:22 h1S", DibromIochloromethane [124-48-1]^ < 0.067 ug/L 1 0.067 ' 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:22 f•ISz Dibrombmethane [74-95.3]^ < 0.13 ug/L 1 0.13 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:22 MS7- Dichlorodifluoromethane [75-71-8]^. < 0.091 . ug/L 1 0.091 0.50 5A05015 EPA 8260B/6230D 01/05/15 17:2..2 M1i57 EthylbeInzene [100-41-4]^ < 0.10 ug/L 1 0.10 0.50 .5A05015 EPA 82608/6230D 01/05/15 17:22 MSz Hexachllorobutadiene[87-68-3]^ < 0.15 ug/L 1 0.15 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:22 MSZ Isopropyl Ether[108-20-3]^ < 0.20 ug/L 1 0.20 0.50 5AO5015 EPA 8260B16230D 01/05/15 17:22 MSz Isopropylbenzene [98-82-8]^ < 0.13 ug/L 1 0.13 MO 5A05015 EPA 8260B/6230D 01/05/15 17:22 MSZ m,p-Xylenes[108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 5AO5015 EPA 8260B/6230D 01/05/1S 17:22 1.1SZ I Methylene Chloride [75-09-2]^ < 0.070 . ug/L' 1 0.070 0.50 5A05015 EPA 82608/6230D 01/05/15 17:22 MSZ Mel:Zltert-Butyl Ether [1634=04-4]^ < 0.12 ug/L 1 0.12 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:22 MSZ Naphthalene[91-20-3]^ < 0.086 ug/1- 1 0.086 0.50 5AO5015 EPA 82608/62301) 01/05/15 17:22 MS7 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. page 6 of n+ www.enco(abs.com ANALYTICAL RESULTS scription: 141662 02 MW 43 Lab Sample ID:CS00132-02 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 14:06 Work Order: C500132 Project: Genral Subcontract Sampled By: CLIENT iv?latile Organic Compounds by GCMS _ 1 ^ - ENCO Cary ceitiBed analyte fNC 5911 Results Flaa Units DF MDL Batch Method Analyzed Notes Analvte rCAS Numberl n-Butyl-51-8]^ < 0.074 ug/L 1 0.074 0.50 5A05015 EPA 82608/6230D 01/05/15 17:2-2 MSZ n-PropylBenzene [103-65-1]^ < 0.073 ug/L 1 0.073 O.SO SA05015 EPA 8260B/6230D 01/05A5 17:22 MSZ o-Xylene[95-47-6]^ - < 0.088 ug/L 1 0.088 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:22 MSZ sec-Butylbenzene[135-98-8]^ < 0.053 ug/L 1 0.053 O.SO 5AO5015 EPA 8260B/6230D 01/05/15 17:22 MSZ < 0.082 ug/L 1 0.082 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:22 MSZ Styrene:[100-42-5]^ tert-Burylbenzene[98 06 6]^ < 0.094 ug/L 1 0.094 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:22 MSZ Tetrachloroetene[9hene 27-18 4]^ < 0.099 ug/L 1 0.099 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:22 MSZ 'roluene[108-88-3]^ < 0.053 ug/L 1 0.053 0.50 SA05015 EPA 82608/6230D 01/05/15 17:22 MSZ trans- lj2-Dichloroethene [156-60-5]^ < 0.11 ug/L 1 0.11 0.50 5AO5015 EPA 826OB/6230D 01/05/15 17:22 MSZ lj3-Dichloropropene[10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:22 MSZ trans- Trichlorjjoethene[79-01-6]^ < 0.13 ug/L 1 0.13 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:22 hISZ 0.15 ug/L 1 0.15 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:22 M52 TrichlotoFluoromethane[75 69-4]^ < 01-4]^ < 0.083 ug/L 1 0.083 0.50 5A05015 EPA 8260B(6230D 01/05/15 17:22 MSZ Vinyl chloride [75 Xylenes (Total) (1330-20-7] ^ < 0,22 ug/L 1 0.22 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:22 MSZ Results OF Spike Lvl % Re c °7o Rec Lim itr Batch Method Analyzed By Notes Surrogates 53 1 50.0 106 % 53-136 SA05015 EPA 82608/6130L 01/05/I5 17:12 hISL 4-Bromofluorobenzene I 52 1 50.0 105 % 67-129 5AO5015 EPA 826OB16230C 01/05/15 17:22 ^!SZ Dibrom ofluoromethane 59 1 50.0 118 % 59-134 5A05015 EPA 3260816230C 01105,115 17:'2 ^r5Z Toluene-d8 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page ! of •: i w.ww.encolabs.c_om ANALYTICAL RESULTS Aption: 141662703 MW-44 Lab Sample ID:C500132-03 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 14:21 Work Order: C500132 Project: Genral Subcontract Sampled By:CLIENT IVolatile Organic Compounds by GCMS i ^ • ENCO Cary certified ana/yre [NC 5911 - - AnalvtleI rCAS Number] Results Flaa Units DF MDL POL Batch Method Analyzed Py Notes 1,1,1,2-Tetrachlordethane[630-20-6]^ < 0.091 ug/L 1 0.091 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSZ 1,1,1-T-ichlorcethane [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5A05015 EPA 8260B/6230D .01/05/15 17:53 MSz 1,1,2,2-Tetrachloroethane (79-34-5)^ < 0.085 ug/L 1 0.085 0:50 . 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSz 1,1,2-Tiichloroethane [79=(30-5)A, < 0.068 ug/L 1 0.068 0.50 5AO5015 EPA 8260B16230D 01/05/15 17:53 MSZ 1,1-Dic loroethane[75-34-3]^ < 0.050 ug/L 1 _ 0.050 0.50 5A05015 EPA 82608/6230D 01/05/15 17:53 MSZ 1,1-Dic Ioroethenej75-35-4]^ < 0.15 ug/L 1 0.15 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSz 1,1•Dic�Ioropropene[563.58-6]^ < 0.063 ug/L 1 0.063 0.50 SA05015 EPA 8260B/6230D 01/05/15 11:53 MSZ 1,43-Thchlorobenzene (87-61-6)^ < 0.25 ug/L 1 0.25 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSz < 0.15 ug/L 1 0.15 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:53 MSz 1,2,3- ichloropropane [96-18-4]^ 1,2,4-Tlichlorobenzene[120-82-1]^ < 0.097 ug/L ' 1 0.097 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSz 1,2,4-Tr imethylbenzene(95-63-6]^ < 0.067 ug/L 1 0.067 0.50 5AO5015 EPA 826OB/6230D 01/05/15 17:53 MSZ 1,2-Dib omo-3-chloropropane,[96-1278]^. < 0.48 ug/L 1 0.48 0.50 5AO5015 EPA 826OB/6230D 01/05/15 17:53 MSZ 1,2-Dib omoethane[106-93-4]^ < 0.27 ug/L 1 0.27 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:53 MSZ 1,2-Dichlorobenzene(95-50-1]^ < 0.062 ug/L 1 0.062 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:53 MSZ 1,2-Dichloroethane(107-06-2]^ < 0.082 ug/L - 1 0.082 0.50 SA05015 EPA 8260B/6230D, 01/05/15 17:53 I,ISZ 1,2-Dichloropropane[78 87-5]^ < 0.098 ug/L 1 0.098 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSZ 1,3,5-Timethylbenzene [108-67-8]^ < 0.10 ug/L 1 0.10 0.50 5AO5015 EPA 8260B/6230D .01/05/15 17:53 MSZ 1;3-Dichlorobenzene[541-73-1]^ < 0.092 ug/L 1 0.092 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:53 MSZ 1,3-Dichloropropane(142-28-9]^ < 0.15 ug/L 1 0.15 0.50 5A05015 EPA 826DB/6230D 01/05/15 17:53 MSZ 1,4-DicIlorobenzene (106-46=7]^ < 0.10 ug/L 1 0.10 0.50 SA05015 EPA 82606/6230D 01/05/15 17:53 MSz 2,7.-Dichloropropane(594-20-.7]^ < 0.12 ug/L 1 0.12 0.50 5AO5015 EPA 8260B16230D 01/05/15 17:53 MSz. 2-Chlorotoluene[95-49-8]^ < 0.10 ug/L I 0.10 0.50 SA05015 EPA 82606/6230D 01/05/15 17:53 MSZ 4-Chlor toluene[106-43-4]^ < 0.10 ug/L 1 0.10 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSz 4 Isopropyltoluene[99-87 6]^ < 0.066 ug/L ` - 1 0.066 . 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSZ 6enzene[71 43 2]^ < 0.050 ug/L 1 0.050 0.50 5AO5015 'EPA 82606/6230D 01/05/15 17:53 MSZ bromot enzene[108-86-1]^ < 0.13 ug/L 1 0.13 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSz Bromo hloromethane [74-97-5]1• < 0.11 ug/L 1 0.11 0.50 SA05015 EPA 82608/6230D 01/05/15 17:53 MSz Bromo ichloromethane [75-27-4)^ < 0.010 ug/L 1 0.010. 0.50 5AO5015 EPA 8260B/6230D 61/05/15 17:53 MS7. Bromo prm (75-25-2)^ < 0.20 ug/L 1 0.20 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSL Brom8Tethane [74-83-9]^ < 0.28 ug/L 1 0.28 0.50 5A05015 EPA 826OB/6230D 01/05/15 17:53 MS-L Carbon Tetrachloride(56-23-5)^, < 0.082 ug/L ' 1 0.082 0.50 5AOSO15 EPA 8260B/6230D 01/05/IS 17:53 MSZ ChloiJenzene[108-90-7)^ < 0.069 ug/L 1 0.069 0.50 5AO5015 EPA 82608/6230D 01/05/15 17:53 msz Chloro2thwe (75-00-3]^ < 0.18 ug/L 1 0.18 0.50 5AO5015 EPA 82606/6230D 01/05/15 17:53 MSZ Chlorbf'rm [67-66-3)^ < 0.083 ug/L 1 0.083 0.50 SA05015 EPA 8260B/6230D O1/OS/15 17:53 MSZ Chlororhethane [74-87-3]^ < 0.050 ug/L 1 0.050 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSZ cis- 1,21j Dichloroethene[156-59-2]^ < 0.075 ug/L 1 0.075 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:53 MSz cis-1,31 Dichloropropene [10061-01-S]^ < 0.073 ug/L_ 1 0.073 0.50' SA05015 EPA 8260B/6230D 01/05/15 17:53 MSZ Dibromochloromethane[124-48-1]^ < 0.067 ug/L 1 0.067 0.50 5A05015 EPA 8260B/6230D 01/05/15 17:53 M52 Dibro I methahe [74-95.3]^ < 0.13 ug/L 1 0.13 0.50 ' 5AO5015 EPA 8260B/6230D - 01/05/15 17:53 MSZ Dichlor6di0uoromethane[75-71-B]^ < 0.091 ug/L 1 0.091 0.50 5A05015 EPA 8260B/6230D 01/05/15 17:53 MSz Ethylb4Inzene[100-41-4)^ < 0.10 ug/L 1 0.10 0.50 5AO5015 EPA 82606/6230D 01/05/15 17c53 MSz Hexactllorobutadiene [87-68-3]1- < 0.15 ug/L 1 0.15 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:53 MSz IsoproffpyIEther(108.20-3]^ < 0.20 ug/L 1 0.20 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:53 MSz IsopropIylbenzene [9B-82-8]^ < 0.13 ug/L 1 0.13 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MS7. m,p-Xylenes[108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 1.151 Methylene Chloncle [75-09-2)^ < 0.070 ug/L 1 0.070 0.50 5A05015 EPA 8260B/6230D 01/05/15 17:53 MSz Methyltert-Butyl Ether[1634-04.4]^ < 0.12 ug/L 1 0.12, ,0.50 5AO5015_ EPA 82606/623DD 01/05/15 17:53 MS7. Naphthalene191-20-3]^ < 0.086 ug/L 1 0.086 0.50 5AO5015 EPA 82608/6230D 01/05/15 17:53 nisz FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 11 1} � ry \ � I pia 'i �' , •'� tjr www.encolabs.com ANALYTICAL RESULTS —� Deiscription: 141662-03 MW-44 Lab Sample ID:C500132-03 Received: 01/05/15 14:06 Matrix: Ground Water Sam pled:12/31/14 14:21 Work Order: C500132 Project: Genral Subcontract Sampled By:CLIENT IVblatile Organic Compounds by GCMS i i ^ - ENCO Cary certibed analyte [NC 5911 Analvtle rCAS Numberl Results Flaa Units DF MDL PPOL Batch Method Analyzed —BY Notes n-ButyliBenzene [104-51-8]^ < 0.074 ug/L 1 0.074 0.50 5AO5015 EPA 8260B16230D 01/05/15 17:53 MSZ n-PropyIBenzene [103-65-1]^ < 0.073 ug/L 1 0.073 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:53 MSZ o-Xylerje [95-47-6]^ < 0.088 ug/L 1 0.088 0.50 5A05015 EPA 8260B/6230D 01/05/15 17:53 MsZ sec-Butylbenzene[135 98 8]^ < 0.053 ug/L 1 0.053 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSZ StyrenleI[100-42-5]^ < 0.082 ug/L 1 0.082 O.SO 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MS7 tent-But,Ibenzene[98-06-6]^ < 0.094 ug/L 1 0.094 0.50 SA05015 EPA 8260B/6230D 01/05/15 17:53 MSZ Tetracliloroethene[127-18-4]^ < 0.099 ug/L 1 0.099 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSZ Toluene[108-88-3]^ < 0.053 ug/L 1 0.053 0.50 SA05015 EPA 82608/6230D 01/05(15 17:53 ht5l trans-)I,2-Dichloroethene [156-60-5]^ < 0.11 ug/L 1 0.11 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 htSZ trans-1,3-Dichloropropene[10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSZ Trichloroethene[79-01-6]^ < 0.13 ug/L 1 0.13 0.50 5AO5015 LPA 8260B/6230D 01/05,15 11:53 HSZ Trichlorofluoromethane [75-69-41^ < 0.15 ug/1- 1 0.15 0.50 5A05015 EPA 82.60B/6230D 01/05/15 17:53 MSZ. Vinyl chloride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 5AO5015 EPA 8260B/6230D 01/05/15 17:53 MSZ Xylene8(Total)[1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 5A05015 EPA 8260B/6230D 01/05/15 17:53 I.15Z Surr�afes Resu/tr DF Spike Lv/ o Rec % Rec Lim itr Batch Method Analyzed fy Notes 4-8ro nofluorobenzene 53 1 50.0 106 4/n 53-136 5A05015 EPA 9260616230C 01105115 17.53 A15Z Dibro nofluoromethane 54 1 50.0 107 V.67-129 5AO5015 fK7 82600/6230L 01105115 1,753 �1� ? Toluene-d8 I 60 1 50.0 119 % 59-134 5AD5015 EPA 8260B/6230L 0110511 J7.53 157 FINAL This report relates only to the sample as receved by the laboratory, and may only be reproduced in full. Page 9 of a I www.encolabs.com I ANALYTICAL RESULTS Description: 141662_01 MW-45 Lab Sample ID:C500132-01 Received: 03/05/15 14:06 Matrix- Ground Water Sampled:-12/31/14 13:57 Work Order: C500132 { Project: Genral Subcontract - Sampled By:CLIENT IVbiatile Organic Compounds by GCMS ^ - E-0 Cary C-ti-analyre (NC 5911 - Analvte fCAS Numbed Results Flag Units DF MDL iQ Batch Method Analyzed BBt Notes 1,1,1,2Fetrachloroethane [630-20-6]^ < 0.091 ug/L 1 0.091 0.50 SA05015 EPA 8260B/6230D 01/05/15 16:52 i457. 1,1,1-Tiichloroethane [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5AO5015 EPA 8260B/6230D 01/05/15 16:52 MSZ 1,1,2,2lTetrachlorcethane [79-34-5]^ < 0.085 ug/L 1 ' 0.085 0.50 5A05015 EPA 82608[6230D 01/05/15 16:52 MSZ 1,f;2-Tr [79-00-5]^ < 0.068 ug/L 1 0.068 0.50 SA05015 EPA 8260B/6230D 01/05/15 16:52 MSZ 1,] Dichloroethane[75 34-3]^ < 0.050 ug/L 1 0.050 0.50 5AO5015 EPA 8260B/6230D 01/05/19 16:52 MSZ 1,1-Dichloroethene[75 35-4]^ < 0.15 ug/L 1 0.15 0.50 5AO5015 EPA 8260B/6230D 01/05/15 16:52 MSZ 1,1-Dichloropropene[563-58-6]^ < 0.063 ug/L 1 0.063 0.50 5AO5015 EPA 8260B/6230D 01/05/15 16:52 MSZ 1,2,3-1{ichlorobenzene[87-61-61^ < 0.25 ug/L 1 0.25 0.50 5AO5015 EPA 8260B/6230D 01105/15 16:52 MSZ 1,2,3-T�ichloropropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.50 5AO5015 EPA 8260B/6230D 01/05/15 16:52 MSZ 1,2,4-Tr'ichlorobenzene[120-82-1]^ < 0.097 ug/L 1 0.097 0.50 5AO5015 EPA 8260B/6230D 01/05/15 16:52 MSZ 1,2,4-Tiiimethylbenzene(95-63-6]^ < 0.067 ug/L 1' 0.067 0.50 5AO5015 EPA 82608/6230D 01/05/15 16:52 MSZ 1,2-Dibh-3-chioropropane[96-12-8]^ < 0.48 ug/L 1 0.48 0.50 5AO5015 EPA 82608/6230D 01/05/15 16:52 MSZ 1,2-Di4omoethane1106-93:4]^ < 0.27 ug/L 1 0.27 0.50 5A05015 EPA 8260B/6230D 01/05/15 16:52 MSZ 1,2-Dichlorobenzene[95-50-1J^ < 0.062 ug/L 1 0.062 0.50 5A05015 EPA 82606/6230D 01/05/15 16:52 MSZ 1,2-Dic,lloroethane(107-06-2]^ < 0.082 ug/L 1 0.082 0.50 5AO5015 EPA 8260B/6230D 01/05/15 16:52 MSZ 1,2-Ditoropropane(78-87.5)^ < 0.098 ug/L 1 0.098 0.50 SA0501S EPA 82606/6230D 01/05/15 16:52. MS7- 1,3,5-Tkmethylbenzene[108-67-8]^ < 0.10 ug/L 1 0.10 0.50 5A05015 EPA 82608/6230D 01/05/15 16:52 M57- 1,3-Dichlorobenzene[541-73-1]^ < 0.092 ug/L 1 0.092 0.50 SA05015 EPA 8260B/6230D 01/05/15 16:52 MSZ 1,3-Dichloropropane[142-28-9]^ < 0.15 ug/L 1 0.15 0.50 5A050.15 EPA 8260B/6230D 01/05/15 16:52 MSZ 114-D41orobenzene(106-46-7J^ < 0.10 ug/L 1, 0.10 0.50 5AO5015 EPA 82608/62301) 01/05/15 16:52 MSZ 2,2-Dic�loropropane.(594-20-7]•` < 0.12 ug/L 1' 0.12 0.50 5AO5015 EPA 8260B/6230D 01/05/15 16:52 MSZ 2-Chlorutoluene[95-49-8]^ < 6.10 ug/L ] 0.10 0.50 5AO5015 EPA 8260B/6230D 01/05/15 16:52 MSZ 4-Chlorotoluene(106-43-4]^ < 0.10 ug/L 1 ' 0.10 0.50 5AO5015 EPA 82.608/6230D 01/05/15 16:52 NISZ 4-Isoprupyltoluene[99-87-6]^ < 0.066 ug/L 1 :'0.066 0.50 5AO5015 EPA 82606/6230D 01/05/15 16:52 MSZ BenzenleI(71-43-2]^ < 0.050 ug/L 1 0.050 0.50: 5A05015 EPA 8260B/6230D 01/05/15 16:52. MS7. BromotSenzene[108.86-1]^ < 0.13 ug/L 1 0.13 0.50 5A05015 EPA 8260B/6230D 01/05/15 16:52 MSZ" Bromotlhloromethane [74-97:5]^ < 0.11' ug/L 1 0.11 0.50 5A05015 EPA 8260B/6230D' 01/05/15 16:52 MSZ BromodlI ichloromethane [75-27-4]^ < 0.010 ug/L 1 0.010 0.50 5A05015 EPA 8260B/6230D 01/05/15 16:52 MSZ Bromoform 175-25-2]^ < 0.20 ug/L 1 0.20 0.50 5AO5015 EPA 82608/62301) 01/05/15 16:52 MSZ Bromornethane [74-83=9]^ < 0.28 ug/L 1 0.28 0.50. 5AO5015 EPA 82606/62301) 01/05/15 16:52 MSZ Carbon' Tetrachloride(56-23-5]^ < 0.082 ug/L 1 0.082 0.50 5AO5015 EPA 8260B/6230D 01/05/15 16:52 MSZ Chlorobenzene[10B-90-7]^ < 0.069 ug/L 1 0.069 0.50 5AO5015 EPA 8260B/6?.30D 01/05/15 16:52 MSZ Chloroelthane[75-00-3]^ < 0.18 ug/L 1 0.18 0.50 SA05015 EPA 8260B/6230D 01/05/15 16:52 145Z ChlororIIorm [67-66-3]^ < 0.083 ug/L 1 0.083 0.50 5A05015 EPA 8260B/6230D 01/05/15 16:52 l'isz Chlorol ethane[74-87.3]^ < 0.050 ug/L 1 0.050 0.50 5AO5015 EPA -82608/6230D 01/05/15 16:52 MSZ cis-1,2IDichloroethene[156-59 2]^ < 0.075 ug/L 1 0.075 0.50 5AO5015 EPA 82608/6230D 01/05/15 16:52 MSZ cis-1,3,Dichloropropene[10061-01-5]^ < 0.073 ug/L 1 0.073 0:50 SA05015 'EPA 8260B/6230D 01/05/15 16:52 MSZ Dibroniochloromethane[124 48-1]^ < 0.067 ug/L 1 0.067 0.50 5AO5015 EPA 82606/6230D 01/05/15 16:52 MSZ Dibroniomethane [74-95-3]^ < 0.13 ug/L 1. 0.13 0.50 ' 5AO5015 EPA 82..60B/6230D 01/05/15 16:52 MS7. Dichlo diFluoromethane [75-71-81^ < 0.091 ug/L 1 1.0.091 0.50 5AO5015 FPA 82608/6230D 01/05/15 16:52 MS7. ff Ethylbenzene[100-41-4]^ < 0.10 ug/L 1• 0.10 0:50 SA05015 EPA 8260B/6230D 01/05/15 16:5? MSZ Hexac ilorobutadiene [87-68-3]^ < 0.15 ug/L 1 0.15 0.50 SA05015 EPA 8260B/6230D 01/05/15 16:S2 MSZ ]sopropylEther [108-20-3]^ < 0.20 ug/L 1 0.20 0.50 5AO5015 EPA 8260B/6230D 01/0S/15 16:52 MSZ IsoproI lbenzene [98-82-8]^ < 0.13 ug/L 1 0.13 0.S0 5AO5015 EPA 8260B/6230D 01/05/15 16:52 MSz m,p-XVllenes(108.38-3/106-42-3]^ < 0.18 ug/L 1 0.18 '0.50 SA05015 EPA 8260B/6230D 01/05/15 16:52 MSZ Methylene Chloride [75-09-2]^ < 0.070 ug/L.. ' 1 0.070 0.50' 5A05015 ,EPA 8260B/6230D 01/05/15 16:52 MSZ Methyttert Butyl Ether[1634-04-4]^ < 0.12 ug/L 1, 0.12 0.50 5A0501S EPA 8.260B16230D 01/05/15 16:52 MSZ Naphtlialene[91-20-3]^ < 0.086 ug/L 1 0.086 0.50 5A05015 EPA 82600/6230D 01/05/15 16:52 MSZ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 41 Description: 141662-01 MW-45 Matrix: Ground Water I Project: Genral Subcontract ANALYTICAL RESULTS Lab Sample ID:C500132-01 Sampled:l2/31/14 13:57 Sampled By:CLIENT va3^.cmvnv:.. www.encolabs.com Received: 01/05/1S 14:06 Work Order: C500132 Volatile Organic Compounds by GCMS I ^ - ENCo Cary certified analyfe [NC 5911 ResultsFluUnits DF MDL PAL Batch Method Analyzed � o es Analvte rCAS Numberl < 0.074 ug/L 1 0.074 0.50 SA05015 EPA 8260B16230D 01/05/15 16:S7 MS7 n-ButylfBenzene(104-51-8]^ n-PropyIBenzene [103-65-1]^ < 0.073 ug/L 1 0.073 0.50 SA05015 EPA 8260B/6230D 01/05/15 15:52 MSZ < 0.088 ug/L 1 0.088 0.50 5AO5015 EPA 8260B16230D 01/05/15 16:52 MSZ o-Xylene [95-47-6]^ < 0.053 ug/L 1 0.053 0.50 SA05015 EPA 826OB16230D 01/05/15 16:52 N1SZ sec-Butylbenzene[135-98-8]^ ug/L 1 0.082 0.50 5AO501S EPA 8260B/6230D 01/05/15 16:52 MSZ Styrene1[100-42-5]^ < 0.082 ug/L 1 0.094 0.50 5AO5015 EPA 8260B/62300 01/05/15 16:52 MSZ tert-Butylbenzene(98-06-6]^ < 0.094 ug/L 1 0.099 0.50 SA05015 EPA 8260B/6230D 01/05/15 16:52 MSZ Tetrachloroethene[127-18 41^ < 0.099 Toluene[108-88-3]^ < 0.053 ug/L 1 0.053 0.50, 5AO5015 EPA 82608/6230D 01/05/15 16:52 MSZ trans-l;2-Dichloroe[hene[156-60 5]^ < 0.11 ug/L 1 0.11 0.50 5AO5015 EPA 8260B/6230D 01/05/15 16:52 MSZ trans-1,3-Dichloropropene[10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 5A05015 EPA 8260B/6230D 01/05/15 16:52 MSZ < 0.13 ug/L 1 0.13 0.50 5AO5015 EPA 8260B/6230D 01/05/15 16:52 MSZ Trichloroethene [79-01-6]^ ug/L 1 0.15 0.50 SA05015 EPA 8260B/6230D 01/05/15 16:52 h15L Trichloioftuoromethane [75-69-4]^ < 0.15 ug/L 1 0.083 0.50 SA05015 EPA 8260B/6230D 01/05/15 16:52 MS7. vinyl chloride [75-01-4]^ < 0.083 Xylenes(Total)[1330-20-71^ < 0.22 ug/L 1 0.22 0.50 SA05015 EPA 82608/6230D Ol/OS/15 16:52 MSZ Resu/Gs DP Soike Lvl % Re c % Rec Lim itr Batch Method Analyzed —BY Notes Surrogates 54 1 50.0 108 %. 53-136 5AO5015 EPA 826oB/623oL 01105115 16:52 M5Z 4-8rolnoRuorobenzene Dibrornofluoromethane 52 1 50.0 10591. 67-I29 SA05015 Ef:1 82606/6230L 01/OS/1516:SZ Al Z 59 1 50.0 117 % 59-134 5A05015 EPA 8260B/6230L 01/05/I5 16:52 hiSZ Toluene-d8 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 4 i l` www.encolab.s.com ANALYTICAL RESULTS, Lab Sample ID:C500132-07 Received: 01105/1514:06 D cription: 141662-07 MW-46 sampled:12/31/14 15:11 Work Order: C500132 Matrix: Ground -Water Project: Genral Subcontract Sampled By: CLIENT - V ladle Organic Compounds by GCMS ^ - ENCO Cary certifiedd analyte [NC 591J Flaw Units DF MDL PPOL Batch Method Analyzed _By Notes Anal a rCAS Number Tetrachloroethane[630-20.6]^ Resul < 0.091 ug/L 1 0.091 0.50 5AOSOIS EPA 8260B/6230D 01/05/15 19:57 MSz 1,1,1,2 1,1,1-T ichloroethane (71-55-6]^ < 0.15 ug/L 1 0.15 0.50 5AO5015 EPA 8260B/6230D 01/05/15 19:57 MSZ 1,1,2,2 Tetrachloroethane (79-34-5]^ < 0.085 ug/L 1 0.085 0.50 5AO5015 EPA 8260B/6230D 01/05/15 19:57 MSZ 1,1,2-Tichloroethane[79-00-5]^ < 0.068 ug/L 1 0.068 0.50 5AO5015 EPA 8260B/62300 01/05/15 19:57 h15Z 1,1-Dic iloroethane (75-34-3]^ < 0.050 ug/L t 0.050 0.50 5AO5015 EPA 82.608/6230D 01/05/15 19:57 MSZ 1,1-Dic loroethene [75-3S-4]^ < US ug/L '1 0.15 0.50 SA05015 EPA 82608/6230D 01/05/15 19:5.7 MSz 1,1-Dic Ioroproperie [563-58-6]^ < 0.063 ug/L 1 0.063 0.50 5AO5015 EPA 8260B16230D 01/05/15 19:57 MSz. 1,2,3-T ichlorobenzene (87-61-6]^ < 0.25 ug/L 1 0.25 0.50 5AO5015 EPA 82.60B/6230D 01/05/15 19:5i r•iSz 1,2,3-T ichloropropane [96-18-4]^ < 0.15 ug/L 1 - 0.15 0.50 SA05015 EPA 826013/62301) 01/05/15 19:57 MSz 1,2,4-Tichlorobenzene[120-82-1]^ < 0.097 ug/L 1 0.097 0.50 5AO5015 EPA 82606/6230D O1/05/1S 19:57 MSz 1,2,4-T imethylbenzene (95r63-6]^ < 0.067 ug/L 1 0.067 0.50 SA05015 EPA 8260B/6230D 01/05/15 19:57 MSZ 1,2-Dib omo-3-chloropropane.[96-12-8]^ < 0.48 ug/L 1 0.48 0.50 5AO5015 EPA 82606/6230D 01/05/15 19:57 MSz 1,2-Dib omoethane[106-93-4]^ < 0.27 ug/L 1 0.27 0.50 5A05015 EPA 82606/6230D 01/05/15 19:57 M57- 1,2-Dic lorobenzene [95-50-1]^ <•0.062 ug/L 1 0.062 0.50 5AO5015 EPA 8260B/6230D 01/05/15 19:57 MSZ 1,2-Dic loroethane (107-06=2]^ < 0.082 ug/L 1 0.082 0.50 5AO5015 EPA 8260B/6230D 01/OS/15 19:57 hiS2 1,2-Dic loropropane(78-87-5]^ < 0.098 ug/L 1 0.098 0.50 5AO5015 EPA 82606/6230D 01/05/15 19:57 MSz 1,3,5- imethylbenzene[108-67-8]^ < 0.10 ug/L 1 0.10 0.50 5A05015 EPA 826OB/6230D 01/05/15 19:57 MS7 1,3-Dic lcrobenzene[541-73.1]^ < 0.092 ug/L 1 0.092 0.50 5AO5015 EPA 82608/6230D 01/OS/15 19:57 MSz 1,3-Dic iloropropane(142-28-9]^ < 0.15 ug/L 1 0.15 0.50 5AO501S EPA 8260B/6230D 01/OS/15 19:57 MSZ 1,4-Dic ilorobenzene[106-46-7]^ < 0.10 ug/L 1 0.10 0.50 5A05015 EPA 8260B/6230D 01/05/15 19:57 MSZ 2,2-Dic loropropane.(594-2077]^ < 0.12 ug/L 1 0.12 0.50 5AO5015 EPA 82608/62:30D 01/05/15 19:57 h1S7. 2•Chlo toluene[95-49 8]^ < 0.10 ug/L 1 0.10 0.50 5AO5015 [PA 8260B16230D 01/05/15 19:57 MSZ 4-Chlo toluene(106-43-A]^ < 0.10 ug/L 1 0.10 0..50 5AO5015 EPA 8266B/6230D 01/05/15 19:57 HSz 4-Isop pyltoluene[99-87-6]^ < 0.066 ug/L 1 0.066 0.50 5AO5015 EPA 82608/6230D 01/05/15 19:57 MSz Benien [71-43-2]^ < 0.050 ug/L 1 0.050 0.50 5AO5015 EPA 82606/6230D 01/05/15 19:57 M Sz Brom6t enzene[108.86-1]^ < 0.13 ug/L 1 0.13 0.50 5AO5015 EPA 8260B/6230D 01/05/15 19:57 MSZ Bromo hloromethane(74-97-5]^ < 0.11 ug/L 1 - 0.11 0.50 5A05015 EPA 82608/62301) 01/05/15 19:57 MSz Bromo ichloromethane (75.27-4]^ < 0.010 ug/L 1 0.010. 0.50 5A05015 EPA 8260B/6230D 01/05/15 19:57 MSZ Bromo rm [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 SA05015 EPA 82608/6230D 01/05/15 19:51 h1SZ Bromor iethane(74-83.9)A < 0.28 ug/L 1 0.28 0.50 SA05015 EPA 82606/62301) 01/05/15 19:57 MSz Carbon Tetrachloride [56-23-5]^ < 0.082 ug/L 1 0.082 0.50 5AO5015 EPA 8260B/6230D 19:57 MS7. Chloro enzene[108-90-7]A < 0.069 ug/L 1 0.069 0:50 5AO5015 EPA 82-6OB/6230D 01/05/15 l/OSJ1S 19:SZ MS7 Chloroi th6ne(75-00-3)^ < 0.18 ug/L 1 0.18 0.50 5AO5015 EPA 8260B/6230D 01/05/15 19:57 MSz Chlorot rm [67-66-3]^ < 0.083 ug/L 1 0.033 0.50 .5AO50IS EPA 8260B/6230D 01/05115 19:57 MSz Chloror iethane(74-87-3]^ < 0.050 ug/L 1 0.050. 0.50 5AO5015 EPA 82608/6230D 01/05/15 19:57 MS7- cis-1,2- Dichloroethene(156-59-2]^ < 0.075 ug/L 1 0.075 0.50 5AO5015 EPA 82608/62300 01/05/15 19:57 MSZ cis-1,3- ichloropropene [10061-01-5)^ < 0.073 ug/L 1 0.073 '0.50 SA05015 EPA 82606/6230D 01/05/15 19:57 hisz Dibrorn r-hloromethane[124=48.1]^ < 0.067 ug/L 1 0.067 0.50 5AO5015 EPA 8260B/6230D 01/05/15 19:57 MSZ Dibrom methane[74-95-3]^ < 0.13 ug/L 1 0.13 0.50 5AO5015 EPA 82608/62.301) 01/05/15 19:57 hlsz Dichlor diflucromethane (75-71-8]^ < 0.091 ug/L 1 0.091 0.50 5A05015 EPA 82608/6230D 01/05/15 19:57 MS7 Ethylbe iene[100-41-4]^ < 0.10 ug/L 1 0.10 0.50 5AO5015 EPA 8260B/6230D -01/05/15 19:57 MSz Hexach orobutadiene(87-68-3]^ < 0.15 ug/L 1 0.15 0.50 5AO5015 EPA 82608/62301) 01/05/15 19:57 hISZ Isopro ylEther [108-20-3]^ < 0.20 ug/L 1 0.20 0.50 5A05015 EPA 8260B/6230D 01/05)15 19:51 MS'l- Isopro y1benzene[98-82-8]^ < 0.13 ug/L 1 0.13 0.50 5AO5015 EPA 82.608/62.30D 01/05/15 19:57 h157_ m,p-Xy enes(108-38-31106-42-3]^ < 0.18 ug/L L 0.18 0.50 5AD5015 EPA 8260616230D 01/05/15 19:51 his- Methyl ne Chloride (75.09-2)^ < 0.070 ug/L ] 0.070 0.50 SA05015 EPA 826DB/62300 01/05/15 19:5i 115z Methyl ert-ButylEther [1634-04-4]^ < 0.12 ug/L 1 0.12 0.50 5A05015 EPA 8760B/62300 01/05/15 19:57 MS7 Napht alene [9i-20-3]^ ug/L i 0.086 0.50 5A05015 EPA 82608/6230D 01/05/15 19:57 MSZ FINAL This report relates only to the sample as received by the laboratory, and. may only be reproduced in full. Page 16 or a 1 .st+-c - v� 'v '. S.k�,swNwwssmrcn.'. www.encolabs.com ANALYTICAL RESULTS I ascription• 141662-07 MW-46 Lab Sample ID:C500132-07 Received: 01/05/15 14:06 Matrix: Ground Water Sampled:12/31/14 15:11 Work Order: C500132 Project: Genral Subcontract Sampled By: CLIENT I %olatile Organic Compounds by GCMS I ^ - ENCO Cary certified analyte [NC 591] n-Buhi l Benzene [104-51-8]^ n-Propyl Benzene [103-65-1]A o-Xyleihe [95-47-6]^ sec-Bjtylbenzene [135-98-8]^ St r e [100-42-5]^ tert-BItylbenzene [98-06-6]^ Tetra hloroethene [127-18.43^ ToluelIe [108-88-3]^ trans- 1,2-Dichloroethene [156-60-5]^ trans-6-Dichloropropene [10061.02-6]^ TrichlollIroethene [79-01-6]^ Trichldro0uoromethane [75-69-4]^ Vinyl dhloride [75-01-4]^ Xylen�s (Total) [1330-20-7]^ Results Flan Units DF MDL PQL < 0.074 ug/L 1 0.074 0.50 < 0.073 ug/L 1 0.073 0.50 < 0.088 ug/L 1 0.088 0.50 < 0.053 ug/L 1 0.053 0.50 < 0.082 ug/L 1 0.082 0.50 < 0.094 ug/L 1 0.094 0.50 < 0.099 ug/L 1 0.099 0.50 < 0.053 ug/L 1 0.053 0.50 < 0.11 ug/L 1 0.11 0.50 < 0.080 ug/L 1 0.080 0.50 < 0.13 ug/L 1 0.13 0.50 < 0.15 ug/L 1 0.15 0.50 < 0.083 ug/L 1 0.083 0.50 < 0.22 ug/L 1 0.22 0.50 Resu/ts OF Soike Lv/ % Rec % Rec Limits 57 1 50.0 114 % 53-136 55 1 50.0 110 % 67-129 58 1 50.0 115 % 59-134 Batch Method Analyzed 5AO5015 EPA 8260B/6230D 01/05/15 19:57 5A05015 EPA 8260B/6230D 01/05/15 19:57 SA05015 EPA 82606/6230D 01/05/15 19:57 5AO5015 EPA 82608/6230D 01/05/15 19:57 5AO5015 EPA 8260B/6230D 01/05/15 19:57 SA05015 EPA 8260B/6230D 01/05/15 19:57 5AO5015 EPA 8260B/6230D 01/05/15 19:57 5AO5015 EPA 82608/6230D 01/05/15 19:57 5AO5015 EPA 8260B/6230D 01/05/15 19:57 5AO5015 EPA 8260B/6230D 01/05/15 19:57 5A05015 EPA 82608/6230D 01/05/15 19:57 5AO5015 EPA 82.608/6230D 01/05/15 19:57 5AO5015 EPA 82608/6230D 01/05/15 19:57 5AO5015 EPA 8260B/6230D 01/05/15 19:57 Batch Method Analyzed 5A05015 EPA 826OB/6230L 01105115 19:57 5AO5015 EPA 826OB16230C 01105115 19.'57 5A05015 EPA 826OB16230L 01105115 19.,57 By Notes MSZ MSZ MSZ MSZ MS7. MSZ MSZ MSZ MS7. MSZ I.1SZ MS/ MS7 MSZ By Notes h15Z AiSZ A15Z FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in Full. Paq+: 1 7 of c I SUBMIT FORM ON YELLUVII IYHrtF( UMT GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM (Facility Name: Permit Name (if act Person: �Ca Location/Site Name PILING INFUMIJA r Iury ``\\ L ID NUMBER (from Permit):w`� Depth: 'Q S ft• h to water Level 5254e: S ft. below measuring point curing Point is 3 ft. above land surface me of water pumped/bailed before sampling: ` Samples for metals were collected unfiltered: ❑ YES Ni LABORATORY INFORMATION �t. -1� Date sample analyzed: \- -� �� i ��- 0 A- S_ PARAMETERS NOTE: Values should reflect dissolve COD ao335 mg/L Coliform: MF Fecal 31515 G ep /100ml- Coliform: MF Total 31504 /100ml- (Note: Use MPN method for highly turbid samples) issolved Solids:Total 70300 3 1 o mg/L pH (Lab) 00403 units TOC oosso mg/L Chloride 00e40 of mg/L Arsenic 01002 ug/L Grease and Oils 00552 mg/L Phenol 32730 ug/L Sulfate 00945 mg/L pecific Conductance 000e5 µMhos Total Ammonia oaslo mg/L (Ammonia Nitrogen; NH30s'9; Ammonia Nitrogen, Total) TKN as N 00525 mg/L For Remediation systems only tAlalacn uao RnNul ww. Telephone#: -�\y - d.\J J No. of wells to be sampled: PERMIT Number:Wtj� 03�-J%9 Expiration Date: { of 3I - oAQI Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED M-Ci­goon ❑ Remediation: Infiltration Gallery [9-9p--ray Field ❑ Remediation: El Rotary Distributor ❑ Land Application of Sludge Date sample collected: W_ Well Diameter: in. Screened Interval: ft. to ft. Relative M.P. Elevation: ft. gallons. NO and field acidified: ❑ YES ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: wAo pH 0oao045�,tO units Temp. 000lo: 19°C DRY at Spec. Cond. 000ea: µMhos time ofsampling, Odor o0095: _fvs v check Appearance q(\ here:❑ Laboratory Name: colloidal concentrations. Nitrite (NO2) as N oasis mg/L Pb -Lead o1o51 Nitrate (NO3) as N aos20 3 mg/L Zn - Zinc 010e2 Certification No. 1 ug/L mg/L Phosphorus: Total as P 00565 mg/L mg/L Other (Specify Corr@&ffi&i,9i01Cai�ent 6ba Units): Orthophosphate 70507 Vuater Qk:a ity r yet �1 Al - Aluminum o1105 mg/L Ba - Barium 01007 ug/L Ca - Calcium noels � VA_ Cd - Cadmium 01027 ILu Chromium: Total 01034 Cu - Copper o1aa2 r, r1�N ORGANICS: (by GC, GC/MS, HPLC) Fe -Iron 01045 (Specify test and method #. ATTACH LAB REPORT.) �SIN�b Report Attached? ❑ Yes(l) ❑ NO(0) Hg - Mercury 71900 uglL K - Potassium 00937 mg/L VOC 7873 , method # Mg - Magnesium oo927 mg/L , method # Mn - Manganese o105$ ug/L , method # Ni - Nickel 01057 ug/L , method # _:.. ..a -r_41 vnn.' me/L Effluent Total VOCs: mg/L VOC Removal% ---v-/.5/ �_U _ v\a ed Agent) Name and Title - lease print or type Rev. 8/2013t SUBMIT ON YELLOW PAPER ONLY Name: Name (if ER QUALITY MONITORING: REPORT FORM L Contact Person: Well Location/Site Name_ SAMPLING INFORMATION WELL ID NUMBER (from Permit): (Nell Depth: �_s ft• Depth to Water Level 8254e: ,$ft. below measuring point Measuring Point is _ ft. above land surfaces Volume of water pumped/bailed before sampling: satnoies for metals were collected unfiltered: ❑YES dA ❑ sample analyzed; COD 00335 mg/L Coliform: MF Fecal 31616 t+�1, /100mL Pe PERMIT Number:0003 11 81)Expiration Date: ! a' 3 l — d U 1-to Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED County om4_ [tMaagoon ❑ Remediation: Infiltration Gallery spray Field ❑ Remediation: Telephone#: Mr 533 ❑Rotary Distributor ❑ Land Application of Sludge No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: Date sample collected: FIELD ANALYSES: 8 6 eC WAS DRY at Well Diameter: ' , in. pH ooaoo (o units Temp. eaolo: � time of Screened Interval: ft. to ft. Spec. Cond. 00094: µMhos sampling, Relative M.P. Elevation: ft. Odor moan: `1\ s✓ check gallons Appearance 0C0.RS e- here:❑ NO and field acidified: ❑ YES M-161 �6 Certification No. Laboratory Name: Ci\ �\e-(vim I colloidal concentrations. Nitrite (NO2) as N ooe15 mg/L Pb -Lead o�os� ug/L Nitrate (NO3) as N 00e20 % So mg/L Zn - Zinc olo92 mglL Coliform: MF Total 31504 /100mL Phosphorus: Total as P ooee5 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L isolved Solids:Total 70300 o` mg/L Al - Aluminum all 05 mg/L pH {Lab) 00403 units Be - Barium 01007 uglL TOC ooeso mg/L Chloride oogao S mg/L Arsenic 01002 ug/L Grease and Oils 00552 mg/L Phenol 32730 ug/L Sulfate 0.0945 mg/L Specific Conductance 00095 µMhos Total Ammonia ooe10 �� mg/L (Ammonia Nitrogen; NH3as jr.Ammonia Nitrogen, Total) TKN as N ooe25 mg/L For Remediation Systems Only (Attach Lab Reports): Ca - Calcium 00916 mg/L Cd - Cadmium 01027 ug1L Chromium: Total 01034 ug1L Cu - Copper 01042 mg/L Fe - Iron 01045 ug/L Hg - Mercury 71800 ug/L K - Potassium 00937- mg/L. Mg - Magnesium oo927 mg/L Mn - Manganese 01055 ug1L Ni - Nickel 01087 ug/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7e73 , method # method # method # method # influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%, — /s :d Agent) Name and TI a Please print or tvpe 1 Rev. 812013 SUBMIT FORM ON YELLOW PAPER ONLY i GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Name: Name (if different): act Person: Location/Site Name C WELL ID NUMBER (from Permit): �U�-�J Well Depth: Depth to Water Level e25ae:��ft. below measuring point Measuring Point is a ft. above land surface Volume of waterpumped/bailed before sampling: Samples for metals were collected unfiltered: ❑ YES t\)A ❑ or Type PERMIT Number(, Qo63Ln$gExpiration Date: (d— 6k- o101 S� Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED _ County_ lagoon ElRemediation: Infiltration Gallery B-Spray Field ❑ Remediation: _ Telephone#: ❑ Rotary Distributor ❑ Land Application of Sludge No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: Date sample collected: A 11 — kl� FIELD ANALYSES: WAS Well Diameter: a in. pH 00400:U units Temp. 0oolo: a0, QC DRY at Screened Interval: ft. to ft. Spec. Cond. 000ga: µMhos time of sampling, Relative M.P. Elevation: ft. Odor 000e5: check gallons Appearance O here:❑ NO and field acidified: ❑ YES It NO )RATORY INFORMATION sample analyzed: 3 - -7 �� l- - Laboratory Name: \Crs 1MeTCI2C WiTP• va ipm _ hnuld reflect dl solved and colloidal concentrations. COD 00335 mg/L Coliform: MF Fecal 31616 Z j I'a /100mL Coliform: MF Total 31604 /100mL (Note: Use MPN method for highly turbid samples) isolved Solids:Total 70300 SO mg/L pH (Lab) 00403 units TOC 00680 mg/L Chloride 00940 mg/L Arsenic 01002 ug/L Grease and Oils 00552 mg/L Phenol 32730 ug/L Sulfate 00945 mg/L )ecific Conductance wogs µMhos Total Ammonia ooseo 0 ,I lk mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen. Total) TKN as N 00625 mg/L For Remedlation Systems Only (Attach Lab Reports): Certification No. l T Nitrite (NO2) as N owm mg/L Pb - Lead wo51 ug/L Nitrate (NO3) as N aowo Q p r mg/L Zn - Zinc wom mg/L Phosphorus: Total as P oases mg/L Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Al -Aluminum o11o5 mg/L Ba - Barium 01007 ug/L Ca - Calcium oogle mg/L Cd - Cadmium 01027 ug/L Chromium: Total 01034 uglL Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) K - Potassium 00937 mg/L VOC 7873 , method # Mg - Magnesium 00927 mg/L , method # Mn - Manganese o1o55 ug/L method # Ni - Nickel 01087 ug/L , method # Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% IQ is Rev. 8/2013 or We k411 WUMI 11-UKM UN YtLLUVV rHrCK U,vt-i TER QUALITY MONITORING: E REPORT FORM FACILITY INFORMATION Please Print Clearly or \Type Facility Name: )aX� re, Permit Name (if different): _ act Person: Location/Site 5AIYIF' UM2 11YrWMIV10%11%jw WELL ID NUMBER (from Permit): � Well Depth: � S ft. Depth to Water Level e2546:_9&:S_ff. below measuring point Measuring Point is ft. above land surface Is of water pumped/bailed before sampling: Sample's for metals were collected unfiltered: ❑ YES A ❑ Date sample analyzed: Ik-'l IXk-113) k\ tn- PARAMETERS NOTE: V lues shout reflec dlssolvi COD 00335 mg/L Coliform: MF Fecal 31616 1 � /100ml- Coliform: MF Total 31504 /100ml- (Note: Use MPN method for highly turbid samples) (solved Solids:Total 70300 `� mg/L pH (Lab) 00403 units TOC aoseo mg/L Chloride 00940 mg/L Arsenic 01002 ug1L Grease and 011s 00552 mg/L Phenol 32730 _ ug1L Sulfate 00946 mg/L iecific Conductance 00095 µMhos Total Ammonia ooslo C Q, 'c� mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Totap TKN as N 00625 mg/L Telephone#:-\\y"d,15 No. of wells to be sampled: Date sample collected: 11 3 `" l kf Well Diameter: in. Screened Interval: ft. to ft. Relative M.P. Elevation: ft. gallons field acidified: ❑ 9RMIT Number:W%l 3M%q Expiration Date: I c - 31 o1(i )n-Discharge UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED 021.8goon ❑ Remediation: Infiltration Gallery CR"'Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: WA5 pH ooaoo:S.S$units Temp. 000lo: QCJ, ('°C DRY at Spec. Cond. 00094: µMhos time of sampling, Odor 000es: check Appearance here:❑ Laboratory Name: U\ M G e4y"- Certification No. I y colloidal concentrations. Nitrite (NO2) as N 00815 mg/L Pb - Lead o1o51 ug/L Nitrate (NO3) as N 00620 a �(-\ mg/L Zn - Zinc 01092 mg/L Phosphorus: Total as P owas mg/L Orthophosphate 70507 mg/L Al - Aluminum o11os mg/L Ba - Barium o1oo7 ug1L Ca - Calcium oo916 mg/L Cd - Cadmium of o27 uglL Chromium: Total 01034 ug/L Cu - Copper 01042 mg/L Fe - Iron 01045 ug1L Hg - Mercury 71900 ug/L K - Potassium 00937 mg/L Mg - Magnesium oo927 mg/L Mn - Manganese 01055 ug1L Ni - Nickel 01067 ug/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7e73 , method # method # method # method # mn/l VOC Removal% For Remediation Systems only (Attacn i-ao Kepons): nm=11L I /\err vvva. 15 — (o Authorized Agent) Name and Title - Please print or tVPe Sian7lttee (or Authnfl GW-59 Rev. 812013 E`q-, V I-� CD O SUBMIT FORM PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Permit Name (if act Person: VWN Location/Site Name I SAMPLING INFORMATIVN WELL ID NUMBER (from Permit): � M\ nell.Depth: S ft. Depth to Water Level 82846: ftbelow measuring point Measuring Point is ft. above land surface Volume of water pumped/bailed before sampling: Samples for metals were collected unfiltered:_ ❑ YES ❑ sample analyzed:%l-' 1 j 1-_6j'1"Z _ l' COD 00335 mg/L Coliform: MF Fecal 31616 C t /100mL Coliform: MF Total 31504 /1'OOmL (Note: Use MPN method for highly turbid samples) issoived Solids:Total 70300 3q cn,, mg/L pH (Lab) 00403 units TOC oaeeo mg/L Chloride 00940 3 mg/L Arsenic 01002 ug/L Grease and 011s 00652 mg/L Phenol 32730 ug/L Sulfate 00845. mg/L >pecific Conductance 000gs µMhos Total Ammonia ooeio G Q , mg/L. (Ammonia Nitrogen; N%as N; Ammonia Nitrogen, Total) TKN as N 00625 mg/L For Remedlation Systems Only (Attach Lab Reports): Type County AM- S33o No. of wells to be sampled: PERMIT Number: Date: in -Discharge UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED [,���,,-L—�agoon ElRemediation: Infiltration Gallery CTSpray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample collected: t_ FIELD ANALYSES: °C WAS DRY at Well Diameter: G�, in. pH ooaoo:S, j units Temp. 000i4m Screened Interval: ft. to ft. Spec. Cond. 00094: µMhos time ofsampling, Relative M.P. Elevation: ft. Odor 000m: _11 e— check gallons Appearance F0 W'-' here: NO and field acidified: ❑ YES thq0- 'o�—f Laboratory Name: V-\ -' t`n and colloidal concentrations. Nitrite (NO2) as N 00615 mg/L Nitrate (NO3) as. N 00620 5S. mg/L Phosphorus: Total as P 00665 mg/L Orthophosphate 70507 mg1L AI -Aluminum 01105 mg/L Ba - Barium 01007 ug/L Ca - Calcium 00916 mg1L Cd - Cadmium o1 o27 ug/L Chromium: Total 01034 ug1L Cu - Copper 01042 mg1L Fe - Iron 01045 ug/L Hg - Mercury 71900 ug/L K - Potassium-00937 mg/L. Mg - Magnesium 00827 mg/L Mn - Manganese ol0ss ug/L Ni - Nickel 01067 ug/L --• N'U7'"' ?1VI-IUIIY► ad Aqent) Name a d Title - Please print or type Rev. 812013 mgwNr 9,(•' Influent Total VOCs: 1 Certification No. Pb - Lead moss Zn - Zinc oio92 ug/L z mg/L Other (Specify Compounds and Concentration Units) n ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.)" Lab Report Attached? ❑ Yes (1) ❑ No (0) VOC 7873 , method # method # method # method # mg1L Effluent Total VOCs: mg/L VOC Removal% W NIE v, SUBMIT FORM ON PAPER ONLY ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM LITY INFORMATIO T lPlease PrinitC arty or Type tyName: OX�1� "OIiIK�' I�+JOl��j1hh it Name (if different): ty Address: 3A (street) 3 6 1 County Ci ) ' \,,3 (stale) Ir (Zip) r�q act Person: "C�\ w�10 e l` T phone#: �� of i Location/Site Name S§at n . of wells to be sampled: PERMIT Number: Moi)31 j 81Expiration Date: Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon ❑ Remediation: Infiltration Gallery Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: J�[L ID NUMBER (from Permit): W� d� Date sample collected: I j'� Depth: • 0 Well Diameter: in. 1 to Water Level 82546: , ft. below measuring point Screened Interval: ft. to ft. curing Point is ft. above land surface Relative M.P. Elevation: ft. ne of water pumped/bailed before sampling: gallons )les for metals were collected unfiltered: ❑ YES /J A ❑ NO e Date sample an PARAMETERS COD 00335 mg/L Coliform: MF Fecal 31615 C CO /100mL Coliform: MF Total 31504 /100mL (Note: Use MPN method for highly turbid samples) isolvedSolids:Total 70300 l mg/L pH (Lab) 00403 units TOC aoseo mg/L Chloride oogao 7 mg/L Arsenic 01002 ug/L Grease and Oils 00552 mg/L Phenol 32730 ug/L Sulfate 00945 mg/L )ecific Conductance 000m µMhos Total Ammonia oomo G (7r mg/L (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) TKN as N 00625 mg/L For Remediation Systems Only (Attach Lab Reports): ❑ YES FIELD ANALYSES: pH 0oaoo:S,Sjunits Spec. Cond. 00094:. Temp. 000lo: o�, °C DRY at µMhos time of Odor 00085: check Appearance here:❑ Laboratory Name: E VW coG Certification No. \� Il and colloidal concentrations. Nitrite (NO2) as N o=5 mg/L Pb - Lead wom ug/L Nitrate (NO3) as N 00520 25, 9 G mg/L Zn - Zinc 01092 mg/L Phosphorus: Total as P 00555 mg/L Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Al -Aluminum olim mg/L Ba - Barium 01007 ug/L Ca - Calcium oog15 mg/L Cd - Cadmium oio27 ug/L Chromium: Total 01034 ug/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) K - Potassium oo93-7 mg/L VOC 7873 method # Mg - Magnesium 00927 mg/L , method # Mn - Manganese 01055 ug/L , method # Ni - Nickel 01057 ug/L method # Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Rev. 8/2013 v SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM or Facility Name: Permit Name (if different): Contact Person: Well Location/Site Name Telephone#:T 0- of 13 - No. of wells to be sampled: PLING INFORMATION p� ,, ``\\ � (� II L ID NUMBER (from Permit): \v \w Date sample collected: — I — it FIELD ANALYSES: Depth: `4�j_ft Well Diameter: in. pH 00400:�5,- 0 units Temp. 000lo: a0► °C h to Water Level 8254s: q 3 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: µMhos curing Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor 000m: `1) O'11P✓ me of water pumped/bailed before sampling: gallons Appearance OY"Qnqk) pies for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES Lrl NO PERMIT Number: W3Q6't1TS')Expiration Date: Ja— dC Non -Discharge UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED 81 Lagoon ❑ Remediation: Infiltration Gallery ®'Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample an PARAMETERS 16-19-11. q- COD 00335 mg/L Coliform: MF Fecal 31616 G /100ml- Coliform: MF Total 31504 /100mL (Note: Use MPN method for highly turbid samples) .solved Solids:Total 70300 � (� mg/L pH (Lab) 00403 units TOC oowa mg/L Chloride 00940 mg/L Arsenic 01002 ug►L Grease and Oils 00552 mg/L Phenol 32730 ugiL Sulfate 00945 _ mg/L iecific Conductance =95 µMhos Total Ammonia ooslo G 0, . mg/L (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) TKN as N 00625 mg/L For Remediation Systems Only (Attach Lab Reports): Laboratory Name: ��Cojvv� and colloidal concentrations. Nitrite (NO2) as N 00615 mg/L Pb - Lead o1051 Nitrate (NO3) as N 00620 S 3 mg/L Zn = Zinc 01092. Phosphorus: Total as P ooam mg/L Certification No. ug1L mg/L DRY at time of sampling, check here:❑ Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): AI -Aluminum o1105 mg/L Ba - Barium of ooi ug/L Ca - Calcium 00915 mg/L Cd - Cadmium 01027 ugiL Chromium: Total 01034 ugiL Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Fe - Iron 01045 ugiL (Specify test and method #. ATTACH LAB' REPORT.) Hg - Mercury 71900 ug1L Lab Report Attached? ❑ Yes (1) ❑ No (0) K - Potassium 00937 mg/L VOC 7873 , method # Mg - Magnesium oo927 mg/L method # Mn - Manganese o1055 ug/L method # uglL method # A NI - Nickel a,aot Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% r.r� ad Agent) Name and Title - Please print or We Rev.8/2013 p�\ �`(�� V SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: NEW isaT 1 �rNl�iao�f�rNt�erN;<! 0 �'apo{�Gass etV�;�%�o�fuvPT��t���i4iifea�an IN�c�dlgTipN;l�hlacf u�y(T COMPLIANCE REPORT FORM � � � � �ei�G Please Print Clearly or Type FACILITY INFORMATION r 1 \ PERMIT Number:"�41tExplration Date: _3 - 1 Facility Name: Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 3 TYPE OF PERMITTED OPERATION BEING MONITORED (street) County ,R= P Lagoon ❑ Remediation: Infiltration Gallery ly) (state) (zip) p,1 E Spray Field El Remediation: Contact Person: Cq� � Telephone#:- - 993 - S 0 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name C No. of wells to be sampled: Lt ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION WELL ID NUMBER (from Permit): N4�)_ 1 Date sample collected: -•;i - l FIELD ANALYSES: If WELL WAS Well Depth: � S ft. Well Diameter: In. pH 00400:�_,11 units Temp. 0o010A0, °C DRY at Depth to Water Level 82546: IS ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 000sa: µMhos time of sampling, Measuring Point is ft. above land surface S Relative M.P. Elevation: ft. Odor 000a5: -'61a si check Volume of water pumped/bailed before sampling: gallons Appearance -� here:❑ Samples for metals were collected unfiltered: ❑ YES nj A ❑ NO and field acidified: ❑ YES IBC LABORATORY INFORMATION 1 Date sample analyzed: -`1 tl' -- �-�� - 11 - aR-1 `f Laboratory Name: Ey cio&n-N-1- Certification No. PARAMETERS NOTE: Values should reflect dis olved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oos15 mg/L Pb - Lead wo51 ug/L Coliform: MF Fecal 31616 G r CO /100mL Nitrate (NO3) as N 00520 as * mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P ooss5 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 a3 0 mg/L All -Aluminum 01105 mg/L pH (Lab) 00403 units Be - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium oogls mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug1L Chromium: Total 01034 ug/L Grease and 011s 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730' ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7e73 , method.#. Total Ammonia ooslo < ri. r2l,' mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00525 mg/L Ni - Nickel 01057 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mgtL trnuent total vuGs: ty!L vvv ncnwvais I , • print or type Rev. 8/2013 POP - Environmental Chemists; Inc; 6602 Windmill Way •Wilmington, NC 28405 i (910) 392-0223 (Lab) (910) 392-4424 (Fax) 710 Bowsert6wri Road • Mant6d, INC 27-954 (252) 473-5702' ANALYTICAL;& CONSULTING CHEMISTS NCDENR::DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Murphy Brown; LW Date of.Report: .J,ul. 23j 2014. Post Office Box 856 Customer PO # Warsaw NC 28398 Customer ID: 08110011 Attention: Kraig Westerbeek Report#: 2014-07977 Project ID: 'F xiire Welis Lab ID Sample.ID: 14-19642 *Site:�M-_'T3 Test Collect.-Date/Time. 7/7/201.4 11:20 AM Method Matrix Sampled by Water Zach Owen Results_ Date -Analyzed :Color color :Brown 07/07/2014 Depth` to water, ft. Depth to Water, Ft: 1:1.7-feet 07-107/2014. Ammonia_ Nitrogen •EPA350.1. <.01mg/L 07/6912014 Gallons bailed before sampling p g Gallons Bailed' before sampling 5,0;gallons; 07/07/2014 Odor Qualitative: None 07/07/2014 Total Dissolved Solids'(TDS) sM2540.0 37: mg/L 07/09/2014 Temperature SM 2550 B 20:7 C 07/07/2014 Chloride SM4500Cl,E 32mg/L 07/22/2014 PH SM 4500 H b: 5.1.7 units :07/07/2014 Fecal .Colifdrm SM 9222R MF <1'-Colonies1100mL 0710.7/2014 Nitrate Nitrogen (Cale) Nitrite: Nitrogen EPA 353:2 < 0.02 mg/L. 07/08/2014 Nitrate+Nitrite-Nitrogen. EPA 353.21 45.7mg/L 07%10/2614 Nitrate Nitrogen Subtraction _Method 45.7 ng/L 0:7I17/2014 Reportk 2014-07977 Pagel of4. t j, i Environmental Chemists Inc: 6602 Windmill Way •—v90oston (;' 405 ,. (910) 392-0223 (Lab) • -(910) 392-4424 (Faz) S-M),; 710 Bowoitown Road * Mante'o', NC 27954 j _ (252) 473.6702' ' ANALYTICAL &;CONSULTING; ,CHEMISTS NCDENR. DWQ`CERTIFICATE #94. DLS CERTIFICATE #37729, Murphy Brown, LLC Date of: -Report: -Jul 23,2014 Post. Office Box 856- Customer P0.#: Warsaw NC 28398 Customer ID.: 0811001'1 Attention: Kraig Westerbeek Report'#: 2014 07077 Project;ID: o " Lab ID Sample ID: Collect:Date/Time Matrix Sampled by 14-19643- Site 7/7/2014 11 645 AM Water lach Owen Test Method. Results Dafe..Arialyzed'. , Color color Tan 07/07/2014 '" Depth, to. water, ft; oePib to Waie.Ft, A feet 07/07/2014- Ammohia Nitrogen EOA,3561' 07/09/2014 Gallons bailed before sampling. callbm Baiied-beforesampling 6 0,9016ns 07/07/2014 g Odor 'Qualitative None o7/07/2b!4 5 Total Dissolved Solids {TDS) sM'25ao;c 114 mg/L. 07/09120.1`4 Tem'perafure 5M;z55o,a+ 22:1:C , 07/07(20.14 ` Chloride ,SM4500Ci`E `16, ng/L 07/22/20,14 'pH' SM, 4500'H B ; --559un'its 07/07/201'4- Fecal Coliform aM 9222R,MF <1, Colonies1100mL '07/07/2014 1. - r: Nitrate Nitrogen (Cale) Nitrite' Nitrogen EP^353z <.0.02 mg/L 07/08/20-14 Nitrate+Nitrite-Nitroqen EPA3532 9.96,Mg/,L 071,16/.2014 Nitrate Nitiogen %Subtraction.Method 9.st mgjL 07/1712014, Pag Report # ,20l4r07977 e 2rof 4 Environmental Chemists, Inc: • 6602 Winamill Way • Wilming#on, NC 28405 (910) 392-0223 (Lab) (910) 392=4424 (Fax) SM 710 Bowsertown,,Road •-Manteo,;NC 27954 ANALYTICAL &CONSULTING (252):473-5702 CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS.CRRTIFICATE.#37729 Murphy Brown, LLC Date of;Report Jul 23,-2014 Post Office. Box 856 Customer PO..#: Warsaw NC, 28398 Customer ID: 081'go 1:1 Attention: Kraig Westerbeek Report#:; 2014,07977 Project;ID: (Foxfire=lNells_ Lab ID Sample ID: Collect Date/Time Matrix. Sampled by 14-19:644 Site: V_V 3 7/7/2014 12.05 PM Water Zach Owen Test Method Results Date -Analyzed Color Color Orange 07/0712014: Depth to water, ft. Depth to water, Ft. 9.7 feet `07/07/2014 Ammonia Nitrogen EPA 350.1 < 02 mg/L 07/09/2014 Gallons bailed before_ sampling Gallons Bailed. before sampling 5.0 gallohs 07/07/2014 Odor Quaiitabve None 67/07/2014 Total Dissolved Solids,(T,DS) sM-2540-C 103 mg/.L 07/09/2014 Temperature sM 2550:B 20.TC 0.7107/2014 Chloride sM 4500 ct E 14 mg/L 07/22/2014 pH SM 4500 H B 5.23 units 07%07/2014 Fecal Coliform sM.92221)'W <1 Colonies/100mL 07/0712014 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353:2 < 0.02 mg/i 07/08/.2014 Nitrate+'Nitrite-Nitrogen EPA353.2 1.53rhg/L 07/16/2014 Nitrate Nitrogen subtraction Method 1.53 mglL 07/1:7/2014 f t 't l Report #:: 2014.07977 Page.3 of 4 ,II,`I� Environmental Chemists., Inc. 660. Windmill I �—mill Way, W6Y y, 4 Wilming!Qn,,'NC.2W5 (910)392-0223(L4'b) - (910)-392441-4(Fax) sm 710B.owsertown Road *'Mcknteo;NC,,27954 (252) 03-5702 ANALYTICA L.-k!0ONSULTING' CHEMISTS -NC,DENR:,DWO.-CERTIFICATE-#94. DLS CERTIFICATE #37729' Murphy Brown, L.Lq. Date of Report: Jul 23, 2014 Post, Office Box,866 Custorher PO4: Warsaw NC 28398 Customer ID: 08110011 Attention: Kraig.Westerbeek Report #: 2014-07977, Project1b: (F6—xfiFe—Wdll9'D Lab, ID Sample,,ID: — ------------ Collect Date/Time Matrix Sampled by, — 14-19645 Vie,:A - 4 7/7/20-1-4. 10,'30 AM Wafer Zach Owen Test Method Results Date Analyzed' Color 'Color Tan 07107/2014 Depth to water,_ ft. Depth t6.Waldr', Ft 9.,31eet b7/0.7/2014 Ammonia Nitrogen ..EPA-340..1 <02mgil- 07/09/201 4 Gallons, bailed before sampling. :Gallons Bailed before sampling 5.0 gallons- 07/07/2014 Odor Qualitative N6ne: 0710712014 Total Dissolved Sollds;(TDS.) SM 2540 C 230 mq/'L' 07iW201[4 Temperature SM 2550 B, 20.8.0 07L07/2014, Chloride *45,00 d ,37 mg/L 07/2212014 pH SMA500 H,R 4.91 units. 01/07/2014 Fecal C , olif&rn 'SM 9222D'MF <1'(jolonies/100mL- 0 . VOVOIA' Nitrate Nitrogen (Cale) K Nitrite Nitrogen EPA 3.513.2 < 0'.02 mgiL 07/,08/2014 Nitrate+NitriterNitrogen EPA-30.2 22.7 mg/L 07/10/2014 Nitrate Nitrogen Subtraction Method 22.7 mg/L 07/17/20.14 Comment: Reviewed by: kwu(3, Report#::, 1014-'67917 Pag6A oF4 - W-O Analytical $ Consulting; Chemists STSINC windmill Way WFgton,44ENVIRONMENTAL CHEMI OFFICE 91.0=392-0213'AX910=392-442NCDENR:.DWQ CERTIFICATION # 94 NCDHHS: DL S.CERTIFICATION #.37729 info@environmentalchemists.com rni I �rrlcnnl nnlri 'rI-Init�l' nG (`1 rc`rftTiY CLIENT: Murphy -Brown, LLC PROJECT NAME: F..oxFi're. Trailer Wash REPORT NO /1-/ - 2172 ADDRESS: CONTACT NAME:, PO NO: REPORT TO: Kraig Westertieek`-. PHONE/FAX: C,OPY'TO: email: ,C_.......L.d Q.:• _ .,:.-P:.• COOAPI FTVPP-.I = Inflivarif F:= FfflYienf_-W =-Weill-.ST = Stream_ So =,Soil. SL = Sludge. Other: Sample Identification Collection �,F E `o o o ccia c.` r E Q ow ca Q; �z PRESERVATION ANALYSISREQUESTED Date. Time Temp z z = N _' o i 0 i 0 ~ o Well: ( ,c pG- C. P )=�1 W y X'. TDS, NO2, CI G: G Depth to water. NO, C P X NH3, NO3 G G Gallons Bailed:. C P X Fecal Coliform G G � pH (field,):J'/ C. P G, G odor: 4 e C P G G color. itow^ C P G G C P G G C P G` G C P G G C, P G G Total of.4:wells due March, July; November Transfer Relinquished By:. Date/Time Received By: Date/Time 1. 2.' • Temperature whery Receei�rv�ed: mil? Accepted: Z����_Date: rcesample rcequesiea: Delivered By:,c'� l/mow Received B.. %G7`t`-1 Time: l�C� Comments: TURNAROUND: 02 n rn ay , Nq 28405 r4J4 ENVIRONC MENTAL HEMIST66 S�, INC OFFICE': 910-392-:0223'FAXMing�qn910-392-4424 @ Analytical.&- . Consul . fing ChemistsNCDENR: DWQ CERTIFICATIO14 # 94 NCDHHS: DILS CERTIFICATION,# 37729 info-(,.nvironmeritaicti-i?�ists.c.om COLLECTION AND CHAIN OF CUSTODY CLIENT.t Mulephy=WoWn,, LLG PROJECT NAME: FoAre Trailer Wash REPORT NO: 79 7 2 ADDRESS: CONTACT NAME:. PG NO REPORT7,0- KraigMesterbeek PHONE/FAX: COPY TO: email* Samnled Bv.- ALr`.' C SAMPLE TYPE:, f= Influent, E = Effluent; VV ST Soil, SL -- SItIdge,'Pth.er: Sample Identification E 5, 00 0 0 M 03 .2 PRESERVATION' ANALYSIS REQUESTED Date Time- Tdmp, Uj z 0 0 U) 0 z 0 w, Uj VVell: c P S X TDS, NO2, C1 G G Depth to water: ja( P x 7 NH3, NO3 G G Gallons Bailed: 3, c P x Fecal Coliform G G r c- pH (fieId):--.,,)5 c P G G odor: Abnt c P G G color: fA,- rV �c P -G G C P G c -Q P G G- C P G G, c P G G Total of 4 wells due March', July, Novemb& Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2.- Temperature when Received:. Accepted: v 4 dsaffipIe R6quest6d: Delivered BY: Received Bk- Date'.. 1,4 Time: I LoW Comments: TVRNAR&ND: .1 Windi-W.My. jton, NC 28405 ENVIRONMENTAL CHEMISTS, IN-C OFFICE: 910' 39270223 FMlminAX-91,0-392-4424- NCbENk.; DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 infog6fivir,6nrrieiiiW[ctferrilsts.com Analytical & Consulting Pherfiists d—r)I 1 =r-TIr1M AMn rn4Aim r)0- rn I-qT(-)nY CLIENT: KurphymBrowh,:LLG PROJECT NAME:, FLbkfire Trailer Wash REPORTNG. 75 2-2 A , DORE S . S: 'CONTACTNAME , PO NO:. REPORT TO: Kraig Wes�t&46bk COPY TO! -. 'PE: I = Irifluent. E Efflueiit.W�-'Well.ST=St�eai-b-.SO�--Sbil.�SL= Azamnhmef R'vr- In r-7r" ( . " A SAMPLE :Sludge,. -Other: Sample Identification Collection a, 11 E 5, cn ' 0 - E, 0' P 0`e: 01 'E 9 1*3 J PRESERVATION ANALYSIS REQUESTED Date Time. Temp 0 z 0 z z -q 1 0 Well- x TDS NO2-, C1 G Depth to water: XL 2- NH3, NO3 G G Gallons Bailed: C .1 1 x Focal Coliform G OH (field): 5 1 1 G G odor; ^k-tg- C P- G G color. Urdoqe;1 P1. G G' C P C R G G: C —.P G C P G Total'& 4 wdlls.due March, July, November Transfer Relinquished By: Date/Time Received By: Datemme 1. 2. Temperature when Received: Q'sa Acceptecl: V L _Kejecteq: !-,esampie Kegueiea:: Time:.[ JRNA II ND' BY: Received B. Date: y ' R I TI Nn- 6604 Windm.ii-1,•Way,.Wilmington, NC'28406, A ENVI�RONM�ENTAL'CH--EM-1""S-,,—T--S.,,,,l�N.,-,Co 'OFFICE-I9lO�392�;0223�FAX�91OL392-"24 NCDF14R: DVVCk CERTli:ICATION #44'NCDAHS jmol DLS CERTIFICATION,037729.�. Anal�,ticial &,ton_s'Ulfifig CpWitfS', rfNIA =rTInK[ At-jn.rWAIKInr,'m mtmv CLIENT: -MbrphY=Rr ni.'LLCr PRWEb-TNAME.-, Fore TrailerWhA. REPORT,79.7 ADDKEst'._ CONTACT NAME: REPORTTMwaij Wd��ptoedk PHONE/,FAX, -COPY'TO.-' Ofnail; 0-r.r. *�TVOV P- ='Inibionf "F =,FfHtipnt_ W=WdLST = "G-4, mStream-SO = Soil. SL ='Sludoe-Other: SumpleIdentification Collection E 12 �00 ao 0 0 CAD .0, 6� m 8 "83 Z I E W 24! -PRESERVATIOW ANALYMSREQUESTED Date Time T O'mp ' " 0 0 � C, z g 0 !Nell: .. :C p G G Depth to Water: p XIINH3, 2,1 NW G 0411oh.s Bailed: X Fecal Coliform, G G OH (field); C p I I I G odor. p color, 'C' G G C, p G G G p G 'G Total of wdlls'dtie March, July,, November Transfee, Relirtqui'shed By- Datdrime Received By: DaielTime Temperature when, Received! O.t W Accepted: .,,DeliVdred By: Received —Time: )ENVIRONMENTAL CHEMISTS.,, INC. P.O. BOX 1037 WRIGHTSVIELLE BEACH;. NCO$480 USA PLEASEE USE THET.Q.,130X., Voice: 910-;391-0k3%, FOR, ALL REMITTANCES. Fax Kq-3924424: E-Mail: teres-a@environnientalchemis'ts.com THANK YOU. Bill To: MURPHY FARMS, INC.' AMYELMORE P.O. BOX 856 WARSAW, W 28398 INVOICE 0ICE NU-MBE.R 1.08,230 Invoice-Datet 41d 31, a44: .Customer 111 Customer PO OZ,5110011 16KIFIRE-MW 1+EDERALID4 5648,9437.9 -- .Paymenf-Terrns Net 3o,'_ AYS Ship -Date Due: Date &114: 9/30A-4 7/7h4: Quantity .Description uhick4b Ath6Wit REPORT #2014-07977 FOXF IRE TRAILER WASH --MONITORING WELLS DATESAMPLED: 07/07/2014 4;oo TEM,PEIZKFUPE,,,COLOTI,,ODOK-(rOXFtIRL,.PNLY-INCLUDFDONCOLLECTION'rE-E,) 4.00 AMMONIA NITROGEN 15;00 6o.00 4.00 TDS 15.01 6 6o.00 00,CHLORIDE 15.00 6o.00 4.00 PH y 15,90 60.00, 4.00 C FECAL OPLIFURK 20.0.0 86.60, 4.00 i NITRATE NITROGEN 2900 86.60 4,601 MONITOR WELL COLLECTIONS 90;00 36o.06 NONSEK 6N ALL REMITTANCES Im ORDER TOPROPERL Y APPL Y'.TJ YOUR ACCOUNT. VALL TERESA WOLFE OR FRAN GODLEY 9 9-10-392-0223 FOR QUESTIONS. Subtbtal" -780.60 . Payment/Cre�qk'.Appfie.d Total Amount Dice 760,moo