WQ0032016_Monitoring - 11-2016_20170103

SUBMIT
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
Name: Rose Hill Plantation Development, LLC
Name (if different): Rose Hill Plantation Development, LLC
Address: 3041 New Leicester Highway
ster ""' NC 28748 County Buncombe
act Person: Bob Basi Telephone#: [phone]
Location/Site Name: Well #1 (MW A on GW -1 b) No. of wells to be sampled: 4
ONLY
PERMIT Number:
NPDES
-L ID NUMBER (from Permit): MW -1 Date sample collected: 11/1.5/16
1 Depth: 69 ft. Well Diameter: 2" in.
th to Water Level: 38.06 ft. below measuring point Screened Interval: 49 ft. to 69 ft.
isuring Point is 2.5 ff. above land surface Relative M.P. Elevation: ft.
Ime of water pumped/bailed before sampling: gallons
toles for metals were collected unfiltered: ❑YES ❑ NO and field acidified: DYES ❑ NO
analyzed:
tAMETERS NOTE: Value_ s should reflect dissolve
COD
mg/I
Coliform: MF Fecal
<10 11 00m
Coliform: MF Total
11 00m
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
69 mg/I
pH (when analyzed)
units
TOC
<1.0 mg/I
Chloride
<1.0 m9/1
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
µMhos
Total Ammonia
<0.10 mg/I
(Ammonia Nitrogen; N%as N; Ammonia Nitrogen, Total)
TKN as N mg/I
Expiration Date: y�su«I
_ UIC
Other W00032016
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ® Other: Surface Irrigation
FIELD ANALYSES:
pH 6.4 units Temp.15.55.5 °C
Spec. Cond. µMhos
Odor None
Appearance Cloudy
Laboratory Name: Pace Analytical
colloidal concentrations.
Nitrite (NO2) as N mg/l Pb - Lead
Nitrate (NO3) as N <0.020 mg/I Zn - Zinc
Phosphorus: Total as'P
mg/I
Orthophosphate
mg/I
All - Aluminum
mg/I
Ba - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
rng/I
Ni - Nickel
mg/f
For Remediation Systems Only (Attach Lab Reports): Influent. Total VOCs:
Certification No. 40
mg/I
mg/I
JAN Q
Other (Specify Compounds and Concentration Units):
t
r
ORGANICS: Qft"
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ER Yes (1) ❑ No (0)
VOC , method #
Effluent Total VOCs:
method #
method #
, method #
mg/L VOC Removal%o
Bob Barr, Authorized Agent 1/t/m— ( 2130I < <P
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW -59 Rev. 112007
at
of
R

SUBMIT FORM ON YELLOW PAPER ONLY
NDWATER QUALITY MONITORING
LIANCE REPORT FORM
LITY INFORMATION Please Print Clearly or Type
ty Name: Rose Hill Plantation Development, LLC
it Name (if different): Rose Hill Plantation Development, LLC
ty Address: 3041 New Leicester HigNjay
:ester "E`'' NC 28748 County Buncombe
-.
act Person: Bob Barr Telephone#: [phone]
Location/Site Name: Well #2(MW B on GW -1 b) No. of wells to be sampled: 4
PERMIT Number: Expiration Date:
Non -Discharge _ UIC _
NPDES Other 1/VUUU3ZU1b
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑Remediation: Infiltration Gallery
❑ Spray Field IJ Remediation:
❑ Rotary Distributor El Land Application of Sludge
El Water Source 'Heat Pump ®Other: Surface Irrigation
L ID NUMBER (from Permit): MW -2_
Date sample collected: 11/15/16
FIELD ANALYSES:
Dissolved Solids: Total
WAS
Depth: 30 ft.
Well Diameter: 2" in.
pH 6.0 units Temp.
14.5 °G
DRY _at
i to Water Level: _ 15.24 ft. below measuring point
Screened Interval: 10 ft. to 30 ft.
—
Spec. Cond.
µMhos
time of
sampling,
,uring Point is 2.5 ft. above land surface
Relative M.P. Elevations ft.
Odor none
mg/I
check
ne of water pumped/bailed before sampling: _
gallons
Appearance muddy
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen,Total)
here:
)les for metals. were collected unfiltered: CIYES
❑ NO and field acidified: ❑ YES ❑ NO
)RATO Y INFORMATION
sample analyzed: 11/15/16 to 12/2/1.6
Laboratory Name: Pace Analytical
Certification No.
40
aMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/1
Nitrite (NO2) as N mg/I
Pb - Lead
mg/1
Coliform: MF Fecal <10.0 1100ml
Nitrate (NO3) as N 0.091 mg/1
Zn - Zinc
mg/1
Coliform: MF Total
/100ml
(Note: Use MPNmethod for highly turbid samples)
Dissolved Solids: Total
7.9.0 mg/1
pH (when analyzed)
units
TOC
<10 mg/I
Chloride
2.1 mg/I
Arsenic
mg/I
Grease and Oils
mg/l
Phenol _
mg/I
Sulfate
mg/I
Specific Conductance
v.Mhos
Total Ammonia
<0.10 mg/I
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen,Total)
TKN as N mgll
Phosphorus: Total as P mg/I
Orthophosphate mg/1 Other (Specify Compounds and Concentration Units):
AI -Aluminum mg/l
Ba - Barium
mg/I
Ca - Calcium
mg/I'
Cd - Cadmium
mg/l
Chromium: Total
mg/I
Cu = Copper
mg/I
Fe- Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg11
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Ni -,Nickel
mg/I.
For Remediation Systems Only (Attach Lacs Reports): Influent Total VOCs:
ORGANICS: (by GC; GC/MS; HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ® Yes (1) ❑ No (0)
VOC method
mg/L Effluent Total VOCs:
method #
method #
method #
mg/L VOC Removal%
Bob Barr, Authorized Agent V VkW`- _ 2-1301 ( �-
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date)'
GW -59 Rev. 1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
For Remediation'Systems Only (Attach Lab Reports): Influent Total VOCs:
Bob Barr, Authorized Agent
Permittee (or Authorized Agent) Name and Title- Please print or type.
GW=59 Rev. '112007
Effluent Total VOCs:
VOC Removal%
2.13°11,6
Elm
��:.
GROUNDWATER (,QUALITY MONITORING:
v�o�o��� G� ,��
"t
COMPLIANCE REPORT FORM.,,
I�, ; . Ks r�t� {+ :. ..
FACILITY INFORMATION Please Print rint ClnType ype,
PERMIT Number: Expiration Date: 9/30/2012
Facility Name: Rose Hill Plantation Development, LLC
_ _
Non -Discharge UIC
Permit Name (if different): Rose Hill Plantation Development,_ LLC -
NPDES Other WQ0032016
Facility Address: 3041 New Leicester Highway
_
TYPE OF PERMITTED OPERATION BEING MONITORED
Leicester _'"` ° NC 28748
County Buncombe
•E1 Lagoon. ❑ Remediation: .Infiltration Gallery
l❑ Spray Field ❑ Remediation:
Contact Person: 'Bob Barr -
Telephone#: [phone]
_
❑• Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Well #3 New
No., of wells to be sampled: 4
❑ Water Source Heat Pump ❑X Other: Surface Irrigation
-
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW#3B
Date sample collected: 11/15/16
FIELD ANALYSES:
WAS
Well Depth: 14 ft.
Well Diameter: 2" in.
pH 6.5 units Temp. 15.5 °C
DRY at
Depth to Water Level: 5.15•ft. below measuring point
Screened Interval: 4 ft. to
14 ft. Spec. Cond. µMhos
- -
time of
sampling,
Measuring Point is 0 ft. above land surface
Relative M.P. Elevation: ft;
Odor none _ . -
check
Volume of water pumped/bailed before sampling:
gallons
Appearance cloudy
here:
Samples for metals were collected unfiltered: El YES --,ONO
- -and field acidified: ❑ YES ❑ NO
LABORATORY INFORIPiIATION
Date sample analyzed: 11/15/16 to 12/2/16
Laboratory Name: Pace Analytical
Certification No. 40
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mg/i
Nitrite (NO2) as N
mg/I
Pb - Leadmg/I
Coliform_ MF Fecal X2.0 /100MI
Nitrate (NO3) as N X0.020' mg/l
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use-PN,method for highly turbid samples)
'Ortt10pt10Sphate
mg/I
Other (Specify Compounds and Concentration Units_),
Dissolved Solids: Total, 72.0 mg/I
AI -Aluminum _
mg/I
pH (when analyzed) units
Ba -'Barium
,mg/I
TOC _ - 1.5_ mg/1
Ca - Calcium
mg/I
Chloride 2.8 mg/1
Cd - Cadmium
mg/I
Arsenic mg/1
Chromium: Total
mg/l
Grease and, Oils mg/I
Cu - Copper -
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/l'
Fe - Iron _
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/I
Hg - Mercury
mgt
Report Attached? RI Yes (1`) ❑ No (0)
Specific Conductance µMhos
K - Potassium
mg/1
VOC _ _ method #
Total Ammonia _ <0.10 mg/I'
Mg'- Magnesium
mg/1
method #
(Ammonia Nitrogen; NH3asN, Ammonia Nitrogen, Tota)
Mn -Manganese
mg/I
method #
TKN as N mg/l
Ni =Nickel
mg/I
method #
For Remediation'Systems Only (Attach Lab Reports): Influent Total VOCs:
Bob Barr, Authorized Agent
Permittee (or Authorized Agent) Name and Title- Please print or type.
GW=59 Rev. '112007
Effluent Total VOCs:
VOC Removal%
2.13°11,6

GW -',-)9.A. C ONIP1. IA C'P REPORT CORM Permit #' a co ('o
(Submit one each monitoring period with t;W59 forms.)
IIAI�I�
1-%
1
Enter date monitoring results were due. ( Will this monitoring report (GW -59 and GW -59A)
YES
be submitted after the established due date?
2
Was any required information missing on the GW -59 report forms?
YES
O
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Officefor guidance.
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES". list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines, and/or penalties.
g
The person completing this portion (GW -59A) of the monitoring report should sign below and submit this
form with GW -59 forms for required wells to the address provided at the top of the current GW -59 form.
l Hbcknowledge #hittfheaboy� )nfe�rtvtafiipn was evaIua#ecl and the �nioiYfa#{an stbtnitted in this
a
Campt+ance Repart GW-a9Aj,dsrtte and cnnnte e #o,the bestynowle.ge... .. ;. µ.......;.,Vi
reporeret,(y
12 3d l�
Signature of Permittee (or Authorized Agent) Date
GW -59A 12/8/2003

aceAnalXical
www.pacelabs.com
1
December 03, 2016
Mr. Robert Barr
RPB Systems Inc.
P.O. Box 1325
Asheville, NC 28802
RE: Project: Rose Hill MW 11/15
Pace Project No.: 92319771
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Dear Mr. Barr:
Enclosed are the analytical results for sample(s) received by the laboratory on November 15, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
�'��i°y�y�.,it�..,`�.fJ_ISt,.,��4�-,'.�.'f'•��i's'vJ
Denise Trantham
denise.trantham @pacelabs.com
Project Manager
Enclosures
cc: Rick Swilling, RPB Systems Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

aceAnalXical
www.pacelabs.com
Rick Swilling
RPB Systems Inc.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Project Number: 92319771

aceAnalytical
www.pacelabs.com
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

_, ;aceAnalyfical`�
/ www..pacelabs.com
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
Rose Hill MW 11/15
92319771 a
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92319771001
MW -1
SM 6200B
CAH
63
PASI-C
SM 2540C
MJS1
1
PASI-A
SM 9222D
KDF1
1
PASI-A
EPA 350.1 1993 Rev 2.0
DMN
1
PASI-A
EPA 353.2
WRC
1
PASI-A
SM 4500 -CI -E
WRC
1
PASI-A
SM 5310B
AES2
1
PASI-A
92319771002
MW -2
SM 6200B
CAH
63
PASI-C
SM 2540C
MJS1
1
PASI-A
SM 9222D
KDF1
1
PASI-A
EPA 350.1 1993 Rev 2.0
DMN
1
PASI-A
EPA 353.2
WRC
1
PASI-A
SM 4500 -CI -E
WRC
1
PASI-A
SM 53108
AES2
1
PASI-A
92319771003
MW -3B
SM 6200B
CAH
63
PASI-C
SM 2540C
MJS1
1
PASI-A
SM 9222D
KDF1
1
PASI-A
EPA 350.1 1993 Rev 2.0
DMN
1
PASI-A
EPA 353.2
WRC
1
PASI-A
SM 4500 -CI -E
WRC
1
PASI-A
SM 5310B
AES2
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC

aceAnalytical
- www.padelabs.com
Y -
ANALYTICAL RESULTS
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
,[phone]
Sample: MW -1 Lab ID: 92319771001 Collected: 11/15/16 14:30 Received: 11/15/16 15:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data Analytical Method
Collected By
Mark
1
11/18/16 08:55
Swann
Collected Date
11/15/16
1
11/18/16 08:55
Collected Time
14:30
1
11/18/16 08:55
Field pH
6.4
Std. Units
0.10
1
11/18/16 08:55
Field Temperature
15.5
deg C
0.50
1
11/18/16 08:55
Static Water Level
38.061
feet
1
11/18/16 08:55
Total Well Depth
15.5
feet
1
11/18/16 08:55
Gallons
Turbidity
153.1
NTU
1.0
1
11/18/16 08:55
Odor
No odor
1
11/18/16 08:55
Appearance
Cloudy
1
11/18/16 08:55
6200B MSV
Analytical Method:
SM 6200B
Benzene
ND
ug/L
0.50
1
11/16/1620:40 71-43-2
Bromobenzene
ND
ug/L
0.50
1
11/16/1620:40 108-86-1
Bromochloromethane
ND
ug/L
0.50
1
11/16/16 20:40 74-97-5
Bromod ichloromethane
ND
ug/L
0.50
1
11/16/16 20:40 75-27-4
Bromoform
ND
ug/L
0.50
-1
11/16/16 20:40 75-25-2
Bromomethane
ND
ug/L
5.0
1
11/16/1620:40 74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
11/16/1620:40 104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
11/16/1620:40 135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
11/16/1620:40 98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
11/16/16 20:40 56-23-5
Chlorobertzene
ND
ug/L
0.50
1
11/16/1620:40 108-90-7
Chloroethane
ND
ug/L
1.0
1
11/16/1620:40 75-00-3
Chloroform
ND
ug/L
0.50
1
11/16/16 20:40 67-66-3
Chloromethane
ND
ug/L
1.0
1
11/16/16 20:40 74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
11/16/16 20:40 95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
11/16/1620:40 106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
11/16/1620:40 96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
11/16/16 20:40 124-48-1
1,2-Dibromoethane(EDB)
ND
ug/L
0.50
1
11/16/1620:40 106-93-4
Dibromomethane
ND
ug/L
0.50
1
11/16/16 20:40 74-95-3
1,2 -Dichlorobenzene
ND
ug/L
0.50
1
11/16/1620:40 95-50-1
1,3 -Dichlorobenzene
ND
ug/L
0.50
1
11/16/1620:40 541-73-1
1,4 -Dichlorobenzene
ND
ug/L
0.50
1
11/16/1620:40 106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
11/16/1620:40 75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
11/16/1620:40 75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
11/16/1620:40 107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
11/16/1620:40 75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
11/16/1620:40 156-59-2
trans- l,2-Dichloroethene
ND
ug/L
0.50.
1
11/16/1620:40 156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
11/16/1620:40 78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
11/16/1620:40 142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
11/16/1620:40 594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
11/16/1620:40 563-58-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.

aceAnalytical
www.pacelabs com
ANALYTICAL RESULTS
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW -1 Lab ID: 92319771001 Collected: 11/15/16 14:30 Received: 11/15/16 15:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
cis-1,3-Dichloropropene
trans- 1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2 -Tetrachloroethane
1,1,2,2 -Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobe nzene
1,2,4-Trichlorobe nzene
1,1,1 -Trichloroethane
1,1,2 -Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o -Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-13romofluorobenzene (S)
Toluene -d8 (S)
2540C Total Dissolved Solids
Total Dissolved Solids
M1310 9222D Fecal Coliform AVL
Fecal Coliforms
350.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
Date: 12/03/2016 12:15 AM
Analytical Method: SM 6200B
ND
ug/L
0.50 1
ND
ug/L
0.50 1
ND
ug/L
0.50 1
ND
ug/L
0.50 1
ND
ug/L
2.0 1
ND
ug/L
0.50 1
ND
ug/L
2.0 1
ND
ug/L
0.50 1
ND
ug/L
2.0 1
ND
ug/L
0.50 1
ND
ug/L
0.50 1
ND
ug/L
0.50 1
ND
ug/L
0.50 1
ND
ug/L
0.50 1
ND
ug/L
0.50 1
ND
ug/L
2.0 1
ND
ug/L
2.0 1
ND
ug/L
0.50 1
ND
ug/L .
0.50 1
ND
ug/L
0.50 1
ND
ug/L
1.0 1
ND
ug/L
0.50 1
ND
ug/L
0.50 1
ND
ug/L
0.50 1
ND ...:...
ug/L
1.0 1
ND
ug/L
1.0 1
ND
ug/L
0.50 1
91
%
70-130 1
98
%
70-130 1
97
%
70-130 1
Analytical Method: SM 2540C
69.0 mg/L 25.0 1
Analytical Method: SM 9222D
ND CFU/100 mL 10.0 10
Analytical Method: EPA 350.1 1993 Rev 2.0
ND mg/L 0.10 1
Analytical Method: EPA 353.2
ND mg/L 0.020 1
Analytical Method: SM 4500 -CI -E
ND mg/L 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
11/16/1620:40 10061-01-5
11/16/1620:40 10061-02-6
11/16/1620:40 108-20-3
11/16/1620:40 100-41-4
11/16/1620:40 87-68-3
11/16/16 20:40 98-82-8
11/16/16 20:40 75-09-2
11/16/16 20:40 1634-04-4
11/16/1620:40 91-20-3
11/16/16 20:40 103-65-1
11/16/16 20:40 100-42-5
11/16/16 20:40 630-20-6
11/16/16 20:40 79-34-5
11/16/16 20:40 127-18-4
11/16/16 20:40 108-88-3
11/16/16 20:40 87-61-6
11/16/16 20:40 120-82-1
11/16/16 20:40 71-55-6
11/16/16 20:40 79-00-5
11/16/1620:40 79-01-6
11/16/16 20:40 75-69-4
11/16/16 20:40 96-18-4
11/16/16 20:40 95-63-6
11/16/16 20:40 108-67-8
.:.........:.--
.-..
11/16/16 20:40 75-01-4
11/16/1620:40 179601-23-1
11/16/16 20:40 95-47-6
11/16/1620:40 17060-07-0
11/16/1620:40 460-00-4
11/16/1620:40 2037-26-5
11/17/16 17:27
11/15/16 16:00
12/02/16 16:41 7664-41-7
11/15/16 22:13
11/21/1622:49 16887-00-6

aceAnalytical
wmvpacelabsxom
ANALYTICAL RESULTS
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW -1 Lab ID: 92319771001 Collected: 11/15/16 14:30 Received: 11/15/16 15:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
53108 TOC Analytical Method: SM 53108
Total Organic Carbon ND mg/L 1.0 1 12/01/16 23:49 7440-44-0
REPORT OF LABORATORY ANALYSIS
. This report shall not be reproduced, except in full,
Date: 12/03/2016 1 2:15 AM without the written consent of Pace Analytical Services, LLC.

ace Analytical'
www.pacelabs.com
r
ANALYTICAL RESULTS
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW -2 Lab ID: 92319771002 Collected: 11/15/16 14:15 Received: 11/15/16 15:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
Monitoring Well Data Analytical Method
Collected By
Mark
11/18/16 08:58
Swann
11/18/16 08:58
Collected Date
11/15/2016
11/18/16 08:58
Collected Time
14:15
11/18/16 08:58
Field pH
6.0
Std. Units
Field Temperature
14.5
deg C
Static Water Level
15.24
feet
Total Well Depth
7.5 Gallons
feet
Turbidity
519
NTU
Odor
Muddy
11/16/16 20:57 71-43-2
Appearance
No Odor
11/16/16 20:57 108-86-1
6200B MSV
Analytical Method: SM 6200B
Benzene
ND
ug/L
Bromobenzene
ND
ug/L
Bromochloromethane
ND
ug/L
Bromodichloromethane
ND
ug/L
Bromoform
ND
ug/L
Bromomethane
ND
ug/L
n-Butylbenzene
ND
ug/L
sec-Butylbenzene
ND
ug/L
tert-Butylbenzene
ND
ug/L
Carbon tetrachloride
ND
ug/L
Chlorobenzene
ND
ug/L
Chloroethane _
_.. _ _ _ , • 'ND
ug/L
Chloroform
ND
ug/L
Chloromethane
ND
ug/L
2-Chlorotoluene
ND
ug/L
4-Chlorotoluene
ND
ug/L
1,2-Dibromo-3-chloropropane
ND
ug/L
Dibromochloromethane
ND
ug/L
1,2-Dibromoethane (EDB)
ND
ug/L
Dibromomethane
ND
ug/L
1,2 -Dichlorobenzene
ND
ug/L
1,3 -Dichlorobenzene
ND
ug/L
1,4 -Dichlorobenzene
ND
ug/L
Dichlorodifluoromethane
ND
ug/L
1,1-Dichloroethane
ND
ug/L
1,2-Dichloroethane
ND
ug/L
1,1-Dichloroethene
ND
ug/L
cis-1,2-Dichloroethene
ND
ug/L
trans- l,2-Dichloroethene
ND
ug/L
1,2-Dichloropropane
ND
ug/L
1,3-Dichloropropane
ND
ug/L
2,2-Dichloropropane
ND
ug/L
1,1-Dichloropropene
ND
ug/L
cis-1,3-Dichloropropene
ND
ug/L
Date: 12/03/2016 12:15 AM
1 11/18/16 08:58
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
1
11/18/16 08:58
1
11/18/16 08:58
0.10
1
11/18/16 08:58
0.50
1
11/18/16 08:58
1
11/18/16 08:58
1
11/18/16 08:58
1.0
1
11/18/16 08:58
1
11/18/16 08:58
1
11/18/16 08:58
0.50
1
11/16/16 20:57 71-43-2
0.50
1
11/16/16 20:57 108-86-1
0.50
1
11/16/16 20:57 74-97-5
0.50
1
11/16/16 20:57 75-27-4
0.50
1
11/16/16 20:57 75-25-2
5.0
1
11/16/16 20:57 74-83-9
0.50
1
11/16/16 20:57 104-51-8
0.50
1
11/16/16 20:57 135-98-8
0.50
1
11/16/16 20:57 98-06-6
0.50
1
11/16/16 20:57 56-23-5
0.50
1
11/16/16 20:57 108-90-7
1.0
i
11/16/16 20:57 75-00-3
0.50
1
11/16/16 20:57 67-66-3
1.0
1
11/16/16 20:57 74-87-3
0.50
1
11/16/16 20:57 95-49-8
0.50
1
11/16/16 20:57 106-43-4
1.0
1
11/16/16 20:57 96-12-8
0.50
1
11/16/16 20:57 124-48-1
0.50
1
11/16/16 20:57 106-93-4
0.50
1
11/16/16 20:57 74-95-3
0.50
1
11/16/16 20:57 95-50-1
0.50
1
11/16/16 20:57 541-73-1
0.50
1
11/16/16 20:57 106-46-7
0.50
1
11/16/1620:57 75-71-8
0.50
1
11/16/16 20:57 75-34-3
0.50
1
11/16/16 20:57 107-06-2
0.50
1
11/16/16 20:57 75-35-4
0.50
1
11/16/16 20:57 156-59-2
0.50
1
11/16/16 20:57 156-60-5
0.50
1
11/16/16 20:57 78-87-5
0.50
1
11/16/16 20:57 142-28-9
0.50
1
11/16/16 20:57 594-20-7
0.50
1
11/16/16 20:57 563-58-6
0.50
1
11/16/16 20:57 10061-01-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

1`�aceAnalXical-
www.pacelabs.com
ANALYTICAL RESULTS
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW -2 Lab ID: 92319771002 Collected: 11/15/16 14:15 Received: 11/15/16 15:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
trans-1,3-Dichloropropene
Diisopropyl ether
Ethylbenzene
Hexachloro-1,3-butadiene
Isopropylbenzene (Cumene)
Methylene Chloride
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2 -Tetrachloroethane
1,1,2,2 -Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlo robe nzene
1,2,4-Trichlo robe nzene
1,1,1 -Trichloroethane
1,1,2 -Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl chloride
m&p-Xylene
o -Xylene
Surrogates
1,2-Dichloroethane-d4 (S)
4-Bromofluorobenzene (S)
Toluene -d8 (S)
2540C Total Dissolved Solids
Total Dissolved Solids
MBIO 9222D Fecal Coliform AVL
Fecal Coliforms
350.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
4500 Chloride
Chloride
Date: 12/03/2016 12:15 AM
Analytical Method: SM 6200B
ND
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
2.0
1
ND
ug/L
0.50
1
ND
ug/L
2.0
1
ND
ug/L
0.50
1
ND
ug/L
2.0
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
2.0
1
ND
ug/L
2.0
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
1.0
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
0.50
1
ND
ug/L
1.0
1
ND
ug/L
f.0
_ _1. ._.
ND
ug/L
0.50
1
89
%
70-130
1
96
%
70-130
1
96
%
70-130
1
Analytical Method: SM 2540C
79.0 mg/L 25.0 1
Analytical Method: SM 9222D
ND CFU/100 mL 10.0 10
Analytical Method: EPA 350.1 1993 Rev 2.0
ND mg/L 0.10 1
Analytical Method: EPA 353.2
0.091 mg/L 0.020 1
Analytical Method: SM 4500 -CI -E
2.1 mg/L 1.0 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
11/16/16 20:57 10061-02-6
11/16/16 20:57 108-20-3
11/16/16 20:57 100-41-4
11/16/16 20:57 87-68-3
11/16/1620:57 98-82-8
11/16/1620:57 75-09-2
11/16/16 20:57 1634-04-4
11/16/16 20:57 91-20-3
11/16/16 20:57 103-65-1
11/16/16 20:57 100-42-5
11/16/16 20:57 630-20-6
11/16/16 20:57 79-34-5
11/16/16 20:57 127-18-4
11/16/16 20:57 108-88-3
11/16/16 20:57 87-61-6
11/16/16 20:57 120-82-1
11/16/16 20:57 71-55-6
11/16/16 20:57 79-00-5
11/16/16 20:57 79-01-6
11/16/16 20:57 75-69-4
11/16/16 20:57 96-18-4
11/16/16 20:57 95-63-6
11/16/16 20:57 108-67-8
11/16/1620:57 75-01-4
11/16/16 20:57 179601-23-1
11/16/16 20:57 95-47-6
11/16/1620:57 17060-07-0
11/16/1620:57 460-00-4
11/16/1620:57 2037-26-5
11/17/1617:39 D6
11/15/16 16:00
12/02/16 16:46 7664-41-7
11/15/16 22:12
11/21/16 22:50 16887-00-6

aceAnalXical
www.pactwabs.com
ANALYTICAL RESULTS
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW -2 Lab ID: 92319771002 Collected: 11/15/16 14:15 Received: 11/15/16 15:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 5310B
Total Organic Carbon ND mg/L 1.0 1 12/02/16 00:01 7440-44-0
REPORT OF LABORATORY ANALYSIS
. This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.

aceAnalXical o
/ www.paretabs.com
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
Sample: MW -313
Parameters
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Lab ID: 92319771003 Collected: 11/15/16 14:05 Received: 11/15/16 15:15 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Monitoring Well Data Analytical Method
Collected By
Mark
1
11/18/16 08:59
Swann
Collected Date
11/15/2016
1
11/18/16 08:59
Collected Time
14:05
1
11/18/16 08:59
Field pH
6.5
Std. Units
0.10
1
11/18/16 08:59
Field Temperature
15.5
deg C
0.50
1
11/18/16 08:59
Static Water Level
5.15
feet
1
11/18/16 08:59
Total Well Depth
4.75
feet
1
11/18/16 08:59
Gallons
Turbidity
46.13
NTU
1.0
1
11/18/16 08:59
Odor
No odor
1
11/18/16 08:59
Appearance
cloudy
1
11/18/16 08:59
62008 MSV
Analytical Method:
SM 6200B
Benzene
ND
ug/L
0.50
1
11/16/16 21:14 71-43-2
Bromobenzene
ND
ug/L
0.50
1
11/16/16 21:14 108-86-1
Bromochloromethane
ND
ug/L
0.50
1
11/16/16 21:14 74-97-5
Bromod ichloromethane
ND
ug/L
0.50
1
11/16/16 21:14 75-27-4
Bromoform
ND
ug/L
0.50
1
11/16/16 21:14 75-25-2
Bromomethane
ND
ug/L
5.0
1
11/16/16 21:14 74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
11/16/1621:14 104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
11/16/16 21:14 135-98-8
tert-Butylbenzene
ND
ug/L
0.50
1
11/16/16 21:14 98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
11/16/16 21:14 56-23-5
Chlorobenzene
• �.. -•ND
ug/L
0.50
1
11/16/16 21:14 108-90-7
Chloroethane
ND
ug/L
1.0
1
11/16/1621:14 75-00-3
Chloroform
ND
ug/L
0.50
1
11/16/16 21:14 67-66-3
Chloromethane
ND
ug/L
1.0
1
11/16/16 21:14 74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
11/16/16 21:14 95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
11/16/16 21:14 106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
11/16/1621:14 96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
11/16/16 21:14 124-48-1
1,2-Dibromoethane(EDB)
ND
ug/L
0.50
1
11/16/1621:14 106-93-4
Dibromomethane
ND
ug/L
0.50
1
11/16/1621:14 74-95-3
1,2 -Dichlorobenzene
ND
ug/L
0.50
1
11/16/1621:14 95-50-1
1,3 -Dichlorobenzene
ND
ug/L
0.50
1
11/16/1621:14 541-73-1
1,4 -Dichlorobenzene
ND
ug/L
0.50
1
11/16/1621:14 106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
11/16/16 21:14 75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
11/16/1621:14 75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
11/16/1621:14 107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
11/16/1621:14 75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
11/16/1621:14 156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
11/16/1621:14 156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
11/16/1621:14 78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
11/16/1621:14 142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
11/16/16 21:14 594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
11/16/1621:14 563-58-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.

_ WaneAnalXical"
www.pacelabs.com
I
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
Sample: MW -3B Lab ID: 92319771003 Collected: 11/15/16 14:05 Received: 11/15/16 15:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV Analytical Method: SM 6200B
cis-1,3-Dichloropropene
NO
ug/L
0.50
1
11/16/1621:14 10061-01-5
trans- l,3-Dich loropropene
NO
ug/L
0.50
1
11/16/1621:14 10061-02-6
Diisopropyl ether
NO
ug/L
0.50
1
11/16/16 21:14 108-20-3
Ethylbenzene
NO
ug/L
0.50
1
11/16/1621:14 100-41-4
Hexachloro-1,3-butadiene
NO
ug/L
2.0
1
11/16/1621:14 87-68-3
Isopropylbenzene (Cumene)
NO
ug/L
0.50
1
11/16/1621:14 98-82-8
Methylene Chloride
NO
ug/L
2.0
1
11/16/16 21:14 75-09-2
Methyl-tert-butyl ether
NO
ug/L
0.50
1
11/16/16 21:14 1634-04-4
Naphthalene
NO
ug/L
2.0
1
11/16/16 21:14 91-20-3
n-Propylbenzene
NO
ug/L
0.50
1
11/16/16 21:14 103-65-1
Styrene
NO
ug/L
0.50
1
11/16/1621:14 100-42-5
1,1,1,2 -Tetrachloroethane
NO
ug/L
0.50
1
11/16/1621:14 630-20-6
1,1,2,2 -Tetrachloroethane
NO
ug/L
0.50
1
11/16/1621:14 79-34-5
Tetrachloroethene
NO
ug/L
0.50
1
11/16/16 21:14 127-18-4
Toluene
NO
ug/L
0.50
1
11/16/1621:14 108-88-3
1,2,3-Trichlo robe nzene
NO
ug/L
2.0
1
11/16/1621:14 87-61-6
1,2,4-Trichlo robe nzene
NO
ug/L
2.0
1
11/16/1621:14 120-82-1
1,1,1 -Trichloroethane
NO
ug/L
0.50
1
11/16/1621:14 71-55-6
1,1,2 -Trichloroethane
NO
ug/L
0.50
1
11/16/1621:14 79-00-5
Trichloroethene
NO
ug/L
0.50
1
11/16/16 21:14 79-01-6
Trichlorofluoromethane
NO
ug/L
1.0
1
11/16/16 21:14 75-69-4
1,2,3-Trichloropropane
NO
ug/L
0.50
1
11/16/1621:14 96-18-4
1,2,4-Trimethylbenzene
NO
ug/L
0.50
1
11/16/1621:14 95-63-6
1,3,5-Trimethylbenzene
NO
ug/L
0.50
1
11/16/1621:14 108-67-8
Vinyl chloride
Nb
ug/L
1.0
1"'
11/16/16 21:14'76-0l .4
m&p-Xylene
NO
ug/L
1.0
1
11/16/1621:14 179601-23-1
o -Xylene
NO
ug/L
0.50
1
11/16/16 21:14 95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
91
%
70-130
1
11/16/16 21:14 17060-07-0
4-Bromofluorobenzene (S)
94
%
70-130
1
11/16/16 21:14 460-00-4
Toluene -d8 (S)
99
%
70-130
1
11/16/16 21:14 2037-26-5
2540C Total Dissolved Solids
Analytical Method: SM 2540C
Total Dissolved Solids
72.0
mg/L
25.0
1
11/17/16 17:40
MBIO 9222D Fecal Coliform AVL
Analytical Method: SM 9222D
Fecal Coliforms
NO
CFU/100 mL
2.0
2
11/15/16 16:00
350.1 Ammonia
Analytical Method: EPA 350.1 1993
Rev 2.0
Nitrogen, Ammonia
NO
mg/L
0.10
1
12/02/16 16:47 7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2
Nitrogen, Nitrate
NO
mg/L
0.020
1
11/15/16 22:11
4500 Chloride
Analytical Method: SM 4500 -CI -E
Chloride
2.8
mg/L
1.0
1
11/21/1622:51 16887-00-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM
without the written consent of
Pace Analytical Services, LLC.

aceAnaljftal
www.pecelgbs.com
ANALYTICAL RESULTS
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample: MW -3B Lab ID: 92319771003 Collected: 11/15/16 14:05 Received: 11/15/16 15:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5310B TOC Analytical Method: SM 53108
Total Organic Carbon 1.5 mg/L 1.0 1 12/02/16 00:37 7440-44-0
Date: 12/03/2016 1 2:15 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

aceAnaljftal o
/ www.pacelabs.com
I
QUALITY CONTROL DATA
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
QC Batch: 337240 Analysis Method: SM 62008
QC Batch Method: SM 6200B Analysis Description: 6200B MSV
Associated Lab Samples: 92319771001, 92319771002, 92319771003
METHOD BLANK: 1870247 Matrix: Water
Associated Lab Samples: 92319771001, 92319771002, 92319771003
Blank Reporting
Parameter Units Result Limit
Analyzed
1,1,1,2 -Tetrachloroethane
ug/L
ND
0.50
11/16/1619:33
1,1,1 -Trichloroethane
ug/L
ND
0.50
11/16/1619:33
1,1,2,2 -Tetrachloroethane
ug/L
ND
0.50
11/16/1619:33
1,1,2 -Trichloroethane
ug/L
ND
0.50
11/16/1619:33
1,1-Dichloroethane
ug/L
ND
0.50
11/16/1619:33
1,1-Dichloroethene
ug/L
ND
0.50
11/16/1619:33
1,1-Dichloropropene
ug/L
ND
0.50
11/16/1619:33
1,2,3-Trichlorobenzene
ug/L
ND
2.0
11/16/1619:33
1,2,3-Trichloropropane
ug/L
ND
0.50
11/16/1619:33
1,2,4-Trichlorobenzene
ug/L
ND
2.0
11/16/1619:33
1,2,4 -Trim ethyl benzene
ug/L
ND
0.50
11/16/1619:33
1,2- Dib romo-3-chloropropane
ug/L
ND
1.0
11/16/1619:33
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
11/16/16 19:33
1,2 -Dichlorobenzene
ug/L
ND
0.50
11/16/1619:33
1,2-Dichloroethane
ug/L
ND
0.50
11/16/1619:33
1,2-Dichloropropane
ug/L
ND
0.50
11/16/1619:33
1,3,5 -Trim ethyl benzene
ug/L
ND
0.50
11/16/1619:33
1,3 -Dichlorobenzene
ug/L
ND
0.50
11/16/1619:33
1,3-Dichloropropane
ug/L
ND
0.50
11/16/1619:33
1,4 -Dichlorobenzene
ug/L
ND
0.50
11/16/1619:33
2,2-Dichloropropane
ug/L
ND
0.50
11/16/1619:33
2-Chlorotoluene
ug/L
ND
0.50
11/16/1619:33
4-Chlorotoluene
ug/L
ND
0.50
11/16/1619:33
Benzene
ug/L
ND
0.50
11/16/1619:33
Bromobenzene
ug/L
ND
0.50
11/16/1619:33
Bromochloromethane
ug/L
ND
0.50
11/16/1619:33
Bromodichloromethane
ug/L
ND
0.50
11/16/1619:33
Bromoform
ug/L
ND
0.50
11/16/1619:33
Bromomethane
ug/L
ND
5.0
11/16/1619:33
Carbon tetrachloride
ug/L
ND
0.50
11/16/16 19:33
Chlorobenzene
ug/L
ND
0.50
11/16/1619:33
Chloroethane
ug/L
ND
1.0
11/16/1619:33
Chloroform
ug/L
ND
0.50
11/16/1619:33
Chloromethane
ug/L
ND
1.0
11/16/1619:33
cis-1,2-Dichloroethene
ug/L
ND
0.50
11/16/1619:33
cis-1,3-Dichloropropene
ug/L
ND
0.50
11/16/1619:33
Dibromochloromethane
ug/L
ND
0.50
11/16/1619:33
Dibromomethane
ug/L
ND
0.50
11/16/1619:33
Dichlorodifluoromethane
ug/L
ND
0.50
11/16/1619:33
Diisopropyl ether
ug/L
ND
0.50
11/16/16 19:33
Ethylbenzene
ug/L
ND
0.50
11/16/1619:33
Qualifiers
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.

aceAnalXical m
i www.pacelabs.com
QUALITY CONTROL DATA
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
METHOD BLANK: 1870247 Matrix: Water
Associated Lab Samples: 92319771001, 92319771002, 92319771003
Blank Reporting
Parameter Units Result Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
11/16/1619:33
Isopropylbenzene (Cumene)
ug/L
ND
0.50
11/16/16 19:33
m&p-Xylene
ug/L
ND
1.0
11/16/1619:33
Methyl-tert-butyl ether
ug/L
ND
0.50
11/16/16 19:33
Methylene Chloride
ug/L
ND
2.0
11/16/16 19:33
n-Butylbenzene
ug/L
ND
0.50
11/16/1619:33
n-Propylbenzene
ug/L
ND
0.50
11/16/1619:33
Naphthalene
ug/L
ND
2.0
11/16/1619:33
o -Xylene
ug/L
ND
0.50
11/16/1619:33
sec-Butylbenzene
ug/L
ND
0.50
11/16/1619:33
Styrene
ug/L
ND
0.50
11/16/1619:33
tert-Butylbenzene
ug/L
ND
0.50
11/16/1619:33
Tetrachloroethene
ug/L
ND
0.50
11/16/1619:33
Toluene
ug/L
ND
0.50
11/16/1619:33
trans-1,2-Dichloroethene
ug/L
ND
0.50
11/16/1619:33
trans-1,3-Dichloropropene
ug/L
ND
0.50
11/16/1619:33
Trichloroethene
ug/L
ND
0.50
11/16/1619:33
Trichlorofluoromethane
ug/L
ND
1.0
11/16/1619:33
Vinyl chloride
ug/L
ND
1.0
11/16/16 19:33
1,2-Dichloroethane-d4 (S)
%
91
70-130
11/16/16 19:33
4-Bromofluorobenzene (S)
%
98
70-130
11/16/16 19:33
Toluene -d8 (S)
%
97
70-130
11/16/16 19:33
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1870248
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2 -Tetrachloroethane
ug/L
50
46.9
94
60-140
1,1,1 -Trichloroethane
ug/L
50
46.5
93
60-140
1,1,2,2 -Tetrachloroethane
ug/L
50
44.2
88
60-140
1,1,2 -Trichloroethane
ug/L
50
46.3
93
60-140
1,1-Dichloroethane
ug/L
50
47.5
95
60-140
1,1-Dichloroethene
ug/L
50
53.0
106
60-140
1,1-Dichloropropene
ug/L
50
47.9
96
60-140
1,2,3-Trichlorobenzene
ug/L
50
48.2
96
60-140
1,2,3-Trichloropropane
ug/L
50
41.5
83
60-140
1,2,4-Trichlorobenzene
ug/L
50
50.8
102
60-140
1,2,4-Trimethylbenzene
ug/L
50
49.3
99
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
43.2
86
60-140
1,2-Dibromoethane (EDB)
ug/L
50
46.3
93
60-140
1,2 -Dichlorobenzene
ug/L
50
50.0
100
60-140
1,2-Dichloroethane
ug/L
50
40.0
80
60-140
1,2-Dichloropropane
ug/L
50
45.5
91
60-140
1,3,5-Trimethylbenzene
ug/L
50
48.6
97
60-140
1,3 -Dichlorobenzene
ug/L
50
49.4
99
60-140
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.

a ce Analytical
/ www.pacelabs.com
QUALITY CONTROL DATA
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
LABORATORY CONTROL SAMPLE:
Parameter
1870248
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,3-Dichloropropane
ug/L
50
43.6
87
60-140
1,4 -Dichlorobenzene
ug/L
50
47.4
95
60-140
2,2-Dichloropropane
ug/L
50
49.0
98
60-140
2-Chlorotoluene
ug/L
50
46.8
94
60-140
4-Chlorotoluene
ug/L
50
46.7
93
60-140
Benzene
ug/L
50
49.3
99
60-140
Bromobenzene
ug/L
50
45.2
90
60-140
Bromochloromethane
ug/L
50
47.8
96
60-140
Bromodichloromethane
ug/L
50
47.2
94
60-140
Bromoform
ug/L
50
43.6
87
60-140
Bromomethane
ug/L
50
41.6
83
60-140
Carbon tetrachloride
ug/L
50
50.7
101
60-140
Chlorobenzene
ug/L
50
45.9
92
60-140
Chloroethane
ug/L
50
42.0
84
60-140
Chloroform
ug/L
50
45.2
90
60-140
Chloromethane
ug/L
50
48.1
96
60-140
cis-1,2-Dichloroethene
ug/L
50
46.0
92
60-140
cis-1,3-Dichloropropene
ug/L
50
46.8
94
60-140
Dibromochloromethane
ug/L
50
46.9
94
60-140
Dibromomethane
ug/L
50
45.4
91
60-140
Dichlorodifluoromethane
ug/L
50
43.7
87
60-140
Diisopropyl ether
ug/L
50
50.8
102
60-140
Ethylbenzene
ug/L
50
47.5
95
60-140
Hexachloro-1,3-butadiene
ug/L
50
51.4
103
60-140
Isopropylbenzene (Cumene)
ug/L
50
47.7
95
60-140
m&p-Xylene• •
ug/L
100
94.7
95
60-140
Methyl-tert-butyl ether
ug/L
50
48.2
96
60-140
Methylene Chloride
ug/L
50
56.2
112
60-140
n-Butylbenzene
ug/L
50
49.8
100
60-140
n-Propylbenzene
ug/L
50
48.4
97
60-140
Naphthalene
ug/L
50
46.2
92
60-140
o -Xylene
ug/L
50
45.9
92
60-140
sec-Butylbenzene
ug/L
50
49.8
100
60-140
Styrene
ug/L
50
47.2
94
60-140
tert-Butylbenzene
ug/L
50
42.6
85
60-140
Tetrachloroethene
ug/L
50
40.5
81
60-140
Toluene
ug/L
50
47.7
95
60-140
trans-1,2-Dichloroethene
ug/L
50
50.1
100
60-140
trans-1,3-Dichloropropene
ug/L
50
46.5
93
60-140
Trichloroethene
ug/L
50
46.7
93
60-140
Trichlorofluoromethane
ug/L
50
48.0
96
60-140
Vinyl chloride
ug/L
50
42.0
84
60-140
1,2-Dichloroethane-d4 (S)
%
92
70-130
4-Bromofluorobenzene (S)
%
96
70-130
Toluene -d8 (S)
%
102
70-130
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2016 1 2:15 AM without the written consent of Pace Analytical Services, LLC.

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ac�AnalXical
www.parWabe.com
QUALITY CONTROL DATA
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1870249
1870250
MS
MSD
92319771003
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
n-Butylbenzene
ug/L
ND
20
20
22.1
22.1
111
111
60-140
0
n-Propylbenzene
ug/L
ND
20
20
22.6
22.3
113
112
60-140
1
Naphthalene
ug/L
ND
20
20
21.0
21.1
105
106
60-140
1
o -Xylene
ug/L
ND
20
20
20.3
20.2
102
101
60-140
1
sec-Butylbenzene
ug/L
ND
20
20
22.3
22.4
112
112
60-140
0
Styrene
ug/L
ND
20
20
20.8
20.4
104
102
60-140
2
tert-Butylbenzene
ug/L
ND
20
20
19.2
18.8
96
94
60-140
2
Tetrachloroethene
ug/L
ND
20
20
18.3
18.4
91
92
60-140
1
Toluene
ug/L
ND
20
20
21.1
20.9
105
105
60-140
1
trans- l,2-Dichloroethene
ug/L
ND
20
20
24.0
22.7
120
114
60-140
5
trans- 1,3-Dich loropropene
ug/L
ND
20
20
20.0
19.7
100
98
60-140
2
Trichloroethene
ug/L
ND
20
20
21.2
21.3
106
107
60-140
1
Trichlorofluoromethane
ug/L
ND
20
20
24.0
22.8
120
114
60-140
5
Vinyl chloride
ug/L
ND
20
20
21.1
19.7
- 106
98
60-140
7
1,2-Dichloroethane-d4 (S)
%
91
91
70-130
4-Bromofluorobenzene (S)
%
98
98
70-130
Toluene -d8 (S)
%
98
98
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.
Qual

2eAnalXical'
wwwpacelabs.ccm
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
QC Batch: 337402
Analysis Method: SM 2540C
QC Batch Method: SM 2540C
Analysis Description: 2540C Total Dissolved Solids
Associated Lab Samples: 92319771001
METHOD BLANK: 1871211
Matrix: Water
Associated Lab Samples: 92319771001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Dissolved Solids
mg/L
ND 25.0 11/17/16 17:14
LABORATORY CONTROL SAMPLE: 1871212
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Dissolved Solids
mg/L
250 226 90 90-110
SAMPLE DUPLICATE: 1871213
92319606017 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Dissolved Solids
mg/L
146 157 7 D6
SAMPLE DUPLICATE: 1871214
92319627002 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Dissolved Solids
mg/L
1870 2620 33 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
• This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.

ace Analytical"
/ www.pacelabs.com
I ,
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
QC Batch: 337404
Analysis Method: SM 2540C
QC Batch Method: SM 2540C
Analysis Description: 2540C Total Dissolved Solids
Associated Lab Samples: 92319771002,
92319771003
METHOD BLANK: 1871218
Matrix: Water
Associated Lab Samples: 92319771002,
92319771003
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Dissolved Solids
mg/L
ND 25.0 11/17/16 17:38
LABORATORY CONTROL SAMPLE: 1871219
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Dissolved Solids
mg/L
250 240 96 90-110
SAMPLE DUPLICATE: 1871220
92319771002 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Dissolved Solids
mg/L
79.0 68.0 15 D6
SAMPLE DUPLICATE: 1871221
92319815009 Dup
Parameter
Units
Result Result RPD Qualifiers
-Total Dissolved Solids
mg/L
- 1090 1160 -- 7 DS
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.

aCMnalytkal
,www.pacebbs.com
QUALITY CONTROL DATA
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
QC Batch: 337154 Analysis Method: SM 9222D
QC Batch Method: SM 9222D Analysis Description: 9222D MBIO Fecal Coliform - AVL
Associated Lab Samples: 92319771001, 92319771002, 92319771003
METHOD BLANK: 1869550 Matrix: Water
Associated Lab Samples: 92319771001,92319771002,923'19771003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 11/15/16 16:00
SAMPLE DUPLICATE: 1869551
Parameter
Fecal Coliforms
92319771003 Dup
Units Result Result RPD Qualifiers
CFU/100 mL ND ND
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
. [phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.

aceAnalytical
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QUALITY CONTROL DATA
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
QC Batch: 338752 Analysis Method: EPA 350.1 1993 Rev 2.0
QC Batch Method: EPA 350.1 1993 Rev 2.0 Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92319771001, 92319771002, 92319771003
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 1878260 Matrix: Water
Associated Lab Samples: 92319771001, 92319771002, 92319771003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Ammonia mg/L ND 0.10 12/02/16 16:28
LABORATORY CONTROL SAMPLE: 1878261
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Ammonia mg/L 5 4.8 97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1878262 1878263
MS MSD
92319735007 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L ND 5 5 4.9 5.0 97 98 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1878264 1878265
MS MSD
92319735008 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[
Nitrogen, Ammonia mg/L ND 5 5 4.8 4.7 94 94 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.

r 2ceAnalyfical'
www,pacelabs.com
QUALITY CONTROL DATA
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
QC Batch: 337063 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Associated Lab Samples: 92319771001, 92319771002, 92319771003
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 1869222
Matrix: Water
Associated Lab Samples: 92319771001,
92319771002, 92319771003
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/L
ND 0.020
11/15/16 21:56
LABORATORY CONTROL SAMPLE:
1869223
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mg/L
2.5 2.4
96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1869224 1869225
MS MSD
92319627001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L ND 2.5 2.5 2.6 2.6 103 103 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1'2/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.

Ar
ayticalceAnal
wwwpacalabs.com
QUALITY CONTROL DATA
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
QC Batch: 337877 Analysis Method: SM 4500 -CI -E
QC Batch Method: SM 4500 -CI -E Analysis Description: 4500 Chloride
Associated Lab Samples: 92319771001, 92319771002, 92319771003
METHOD BLANK: 1873973 Matrix: Water
Associated Lab Samples: 92319771001, 92319771002, 92319771003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chloride mg/L ND 1.0 11/21/16 22:16
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 1873974
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chloride mg/L 20 20.7 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1873975 1873976
MS MSD
92319593003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Chloride mg/L 4.0 10 10 15.0 15.1 110 111 90-110 0 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1873977 1873978
MS MSD
92319646001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 112 10 10 128 128 166 160 90-110 0 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
. This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.

aeeAnalytical-
www.pacelabs.com
F
i
QUALITY CONTROL DATA
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
QC Batch: 338960 Analysis Method: SM 5310B
QC Batch Method: SM 5310B Analysis Description: 5310B TOC
Associated Lab Samples: 92319771001, 92319771002, 92319771003
METHOD BLANK: 1879456 Matrix: Water
Associated Lab Samples: 92319771001, 92319771002, 92319771003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Organic Carbon mg/L ND 1.0 12/01/16 20:24
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
LABORATORY CONTROL SAMPLE: 1879457
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Organic Carbon mg/L 25 25.0 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1879458
MS
92320395021 Spike
Parameter Units Result Conc.
Total Organic Carbon mg/L ND 25
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1879460
MS
92319771002 Spike
Parameter Units Result Conc.
Total Organic Carbon mg/L ND 25
1879459
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits RPD
25 24.4 24.8 98 99 90-110 2
1879461
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits RPD
25 23.9 24.2 93 94 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.
Qua[
Qual

aceAnalytical
wwwpacelabsxam
QUALIFIERS
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
DEFINITIONS
Pace Analytical Services, LLC
2225 Riverside Dr.
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Asheville, NC 28804
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.

aC Analytical
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Rose Hill MW 11/15
Pace Project No.: 92319771
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Lab ID
Sample ID
QC Batch Method
Analytical
QC Batch Analytical Method Batch
92319771001
MW -1
92319771002
MW -2
92319771003
MW -3B
92319771001
MW -1
SM 6200B
337240
92319771002
MW -2
SM 6200B
337240
92319771003
MW -3B
SM 6200B
337240
92319771001
MW -1
SM 2540C
337402
92319771002
MW -2
SM 2540C
337404
92319771003
MW -3B
SM 2540C
337404
92319771001
MW -1
SM 9222D
337154
92319771002
MW -2
SM 9222D
337154
92319771003
MW -3B
SM 9222D
337154
92319771001
MW -1
EPA 350.1 1993 Rev 2.0
338752
92319771002
MW -2
EPA 350.1 1993 Rev 2.0
338752
92319771003
MW -3B
EPA 350.1 1993 Rev 2.0
338752
92319771001
MW -1
EPA 353.2
337063
92319771002
MW -2
EPA 353.2
337063
92319771003
MW -3B
EPA 353.2
337063
92319771001
MW -1
SM 4500 -CI -E
337877
92319771002
MW -2
SM 4500 -CI -E
337877
92319771003
MW -3B
SM 4500 -CI -E
337877
92319771001
MW -1
SM 5310B
338960
92319771002-
MW -2 _�
.__-,.—.-...._ _.Sri 53106
338960 ___._... .,.._._.._
92319771003
MW -3B
SM 5310B
338960
REPORT OF LABORATORY ANALYSIS
a
This report shall not be reproduced, except in full,
Date: 12/03/2016 12:15 AM without the written consent of Pace Analytical Services, LLC.

,f
,FaceAnalytical
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CHAIN -OF -CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must'be completed accurately.
'Important Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invoices not paid within 30 days. F-ALL-Q-020reV.07, 15 -May -2007
Section A Section B Section C
Page: � of /
Required Client Information: Required. Project Information: Invoice Information:
Company: �� Report To: Attention:
pp,, /� p l!
b+a / 9 2
'LLII 2
f?r,
ws
Address: Copy To: Company Name:
REGULATORY AGENCY
Address:
r° NPDES r GROUND WATER F DRINKING WATER
(- UST r RCRA r- OTHER
Email To: Purchase Order No.: Pace Quote
Reference:
Phone: Fax: Project Name:/) Pace Project
Site Location
Manager.
STATE:
-
Requested Due Date/TAT: Project Number: Pace Profile #:
Requested
Analysis
Filtered
(Y/N)
"`
Section D Matrix Codes
a
y'
z
Required Client Information MATRIX / CODE
o
g
COLLECTED
Preservatives
j.
Drinking Water DW
z0
' Water WT
Waste Water WW
U
COMPOSITE
COMPOSITE
Product P
: m
m
START
END/GRAB
W
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SoiVSolid SL
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p
`
SAMPLE ID wipe OL
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Sample IDs MUST BE UNIQUE Tissue TS
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DATE
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DATE TIME
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Pa-ce Project No.1 Lab I.D.
3
4
5
6
7
8.
10
11
;• 7
121
1
ADDITIONAL COMMENTS
RELINQUISHED BY/AFFILIATION DATE
TIME ACCEPTED BY/ AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
/ ' 1- • f� �
�/ 1
'ice-� iii
- i � �
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SAMPLER NAME AND SIGNATURE
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PRINT Name of SAMPLER: '� ,•,� v _
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SIGNATURE of SAMPLER: /, • l `--�---._
DATE Signed _
/ •/ �
(MMIDDIYY):�! .1
'Important Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1.5% per month for any invoices not paid within 30 days. F-ALL-Q-020reV.07, 15 -May -2007

Instructions for completing Chain of Custody (COC)
1. Section A and B: Complete all Client information at top of sheet: company name, address, phone, fax, contact (the person to contact if there are
questions, and who will receive the final report.), e-mail address (if available), PO#, Project Name and/or Project Number as you would like to see it
appear on' the report.
2. Section C: Invoice Information: Billing information is included in this section. This information should include the name and address of the person
receiving the invoice.
3. Quote Reference should be completed if a quotation was provided by Pace Analytical. The Project Manager, and Profile No. will be completed by
Pace Analytical Services.
4. Site Location: A separate COC must be filled out for each day of sample collection. Record the two letter postal code for the US state in which the
samples were collected.
5. Regulatory Agency: List the program that is guiding the work to ensure proper regulations are followed.
h. Section D: Complete a Sample Description in the "SAMPLE ID' section as you would like it to appear on the laboratory report. The following
information should also be included: the sample matrix, sample type (G (grab) or C (composite). When collecting a composite, the start time and end
time should be documented in the respective boxes. The collection time for a grab (G) sample should be entered in the boxes marked `Composite
End/Grab'), Sample temp at collection (if required by state), the total number of containers, and preservative used.
7. Marls if the sample was filtered in the field by marking Y or N in `Filtered' row by the Analysis requested.
8. Requested Analysis: List the required analysis and methods on the lines provided and place a check in the column for the samples requiring the
analysis. Additional comments should be referenced in the bottom left hand comer or include attachments for extended lists of parameters.
9. The sampler should print their name in the space provided and sign their name followed by the date of the sampling event at the bottom of the COC in
the spaces designated for `SAMPLER NAME AND SIGNATURE'.
10. When relinquishing custody of the samples to a representative of the laboratory or other organization, indicate the Item Numbers of those samples
being transferred; sign relinquished by, date and time, and include your affiliation.
*Important Note:
Standard Turnaround Time is 2 Weeks/10 business days. Results will be delivered by end of business on the date due unless other arrangements
have been made with your project manager.
Special Project Requirements such as Low Level Detection Limits or level of QC reported must be included on the chain of custody in the Additional
Comments section.