NC0001422_Laboratory COCs - S8Well #2-Envirochem-FR_20150805

Environmental Chemists, Inc.
envirochem 6602 Windmill Way • Wilmington, NC 25405
[phone] (Lab) • [phone] (Fax)
SM
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Duke Energy -Laboratory
Date of Report: Apr 20, 2015
1339 Hagers Ferry Road/Bld 7405 MG03A2
Customer PO #:
Huntersville NC 28078
Customer ID: 15030001
Attention: Peggy Kendall
Report #: 2015-02737
Project ID: Ash Pond Investigation
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
15-06244 Site: Reg # 4055 Well # 2
3/5/2015
10:45 AM DW Ray Porter/Cindy McDonald
Test
Method
Results Date Analyzed
Bicarbonate as CaCO3
Bicarbonate as CaCO3
1 mg/L
03/19/2015
Carbonate as CaCO3
Carbonate as CaCO3
<1 mg/L
03/19/2015
Aluminum
EPA200.7
0.070mg/L
03/11/2015
Boron
EPA200.7
0.25 mg/L
03/11/2015
Calcium
EPA200.7
9.50 mg/L
03/12/2015
Iron
EPA200.7
0.120mg/L
03/11/2015
Magnesium
EPA200.7
2.19mg/L
03/12/2015
Potassium
EPA200.7
1.79mg/L
03/12/2015
Sodium
EPA200.7
11.8mg/L
03/12/2015
Strontium
EPA200.7
0.133mg/L
03/11/2015
Zinc
EPA200.7
0.015mg/L
03/1112015
Antimony
EPA200.8
<0.000099mg/L
03/1012015
Arsenic
EPA200.8
0.000293J mg/L
03/10/2015
J: Estimated. Between Method Detection Limit and Reporting Limit.
Barium
EPA200.8
0.045mg/L
03/10/2015
Beryllium
EPA200.8
<0.000146mg/L
03/10/2015
Cadmium
EPA200.8
<0.0000827mg/L
03/10/2015
Chromium
EPA200.8
<0.000148mg/L
03/10/2015
Cobalt
EPA200.8
0.004mg/L
03/11/2015
Copper
EPA200.8
0.008mg/L
03/10/2015
Lead
EPA200.8
0.000520 J mg/L
03/10/2015
J: Estimated. Between Method Detection Limit and Reporting Limit.
Manganese
EPA200.8
0.142mg/L
03/11/2015
Molybdenum
EPA200.8
<0.0001 15 mg/L
03/10/2015
Nickel
EPA200.8
< 0.100 mg/L
03/10/2015
Selenium
EPA200.8
0.00059408 J mg/L
03/27/2015
J: Estimated. Between Method Detection Limit and Reporting Limit.
Report #:: 2015-02737 Page 1 of 2

00 7 1
gn:v7irochem'
ANALYTICAL & CONSULTING
CHEMISTS
Environmental Chemists, Inc.
Duke Energy -Laboratory
1339 Hagers Ferry Road/Bid 7405 MG03A2
Huntersville NC 28078
Attention: Peggy Kendall
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Date of Report: Apr 20, 2015
Customer PO #:
Customer ID: 15030001
Report #: 2015-02737
Project ID: Ash Pond Investigation
Thallium
EPA200.8
<0.0001 mg/L
03/10/2015
Vanadium
EPA200.8
0.000236 J mg/L
03/11/2015
J: Estimated. Between Method Detection Limit and Reporting Limit.
Hexavalent Chromium
EPA218-7
<0.02 pg/L
03/09/2015
Mercury
EPA 245.1
<0.0004 mg/L
03/09/2015
Sulfate
EPA300.0
33mg/L
03/11/2015
Turbidity
SM2130B
0.2NTU
03/06/2015
Field Turbidity 0.2 NTU.
Alkalinity
SM2320B
1 mg/L
03/13/2015
Conductivity
SM 2510 B
156 umho/cm
03/12/2015
Total Dissolved Solids (TDS)
SM 2540 C
85 mg/L
03/06/2015
Residue Suspended (TSS)
SM2540D
<2.5 mg/L
03/09/2015
Temperature
SM 2550 B
18.7 C
03/05/2015
Chloride
SM4500 CI B
19 mg/L
03/12/2015
pH
SM4500H8
5.21 units
03/05/2015
Dissolved Oxygen
SM45000G
4.10mg/L
03/05/2015
Comment: Turbidity, temperature, pH and dissolved oxygen measured in field at sample collection. All non -
detects for metals
reported to MDL.
Reviewed by
Report #:: 2015-02737 Page 2 of 2

Environmental Chemists, Inc.
envirochem 6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
SM
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
QC for Duke Energy - 2015-02737
LCS
Parameter
True Value
m 2
Result
m
%True Value
Limits
Alkalinity
12.5
13
104
90-110
Aluminum
0.05
0.05
100
90-110
Antimony
0.01
0.01
100
90-110
Arsenic
0.01
0.01
100
90-110
Barium
0.01
0.01
100
90-110
Beryllium
0.01
0.01
100
90-110
Boron
0.05
0.05
100
90-110
Cadmium
0.01
0.01
100
90-110
Calcium
0.5
0.5
100
90-110
Chloride
50
48
96
90-110
Chromium
0.01
0.01
100
90-110
Cobalt
0.01
0.01
100
90-110
Conductivity
10000
99900
99.9
90/110
Copper
0.01
0.01
100
90-110
Iron
0.05
0.05
100
90-110
Lead
0.01
0.01
100
90-110
Magnesium
0.5
0.5
100
90-110
Manganese
0.01
0.01
100
90-110
Mercury
0.0040
0.0037
92
90-110
Molybdenum
0.01
0.01
100
90-110
Nickel
0.0050
0.0048
96
90-110
Potassium
0.5
0.5
100
90-110
TSS
248.8
274.4
110
90-110
Selenium
0.01
0.01
100
90-110
Sodium
0.5
0.5
100
90-110
Strontium
0.05
0.05
100
90-110
Sulfate
50
50
100
90-110
Thallium
0.0050
0.0048
96
90-110
TDS
600
601
100
f 10
Turbidity
N/A
N/A
N/A
N/A

Vanadium
0.01
0.01
100
90-110
Zinc
0.05
0.05
100
90-110
1/M. XYM
Parameter
True Value
mg/L
Result
mg/L
%
Recovery
%
Difference
Limits %
Recovery
Limits %
Difference
Alkalinity
N/A
N/A
N/A
N/A
N/A
N/A
Aluminum
0.100
0.099/0.100
99/100
1
80-120
<_ 20
Antimony
0.025
0.028/0.028
112/112
0
80-120
<_ 20
Arsenic
0.025
0.030/0.030
120/120
0
80-120
< 20
Barium
0.025
0.025/0.025
100/100
0
80-120
<_ 20
Beryllium
0.025
0.029/0.029
116/116
0
80-120
< 20
Boron
0.100
0.097/0.095
97/95
2
80-120
<_ 20
Cadmium
0.025
0.028/0.028
112/112
0
80-120
<_ 20
Calcium
1.0
0.98/0.99
98/99
1
80-120
< 20
Chloride
N/A
N/A
N/A
N/A
N/A
N/A
Chromium
0.025
0.024/0.025
96/100
4
80-120
<_ 20
Cobalt
0.025
0.024/0.025
96/100
4
80-120
<_ 20
Conductivity
N/A
N/A
N/A
N/A
N/A
N/A
Copper
0.025
0.027/0.028
108/112
4
80-120
<_ 20
Iron
0.100
0.098/100
98/100
2
80-120
<_ 20
Lead
0.025
0.023/0.023
92/92
0
80-120
<_ 20
Magnesium
1.0
0.98/1.0
98/100
2
80-120
<_ 20
Manganese
0.025
0.024/0.025
96/100
4
80-120
<_ 20
Mercury
0.0020
0.0022/0.0019
110/95
15
80-120
<_ 20
Molybdenum
0.025
0.028/0.028
112/112
0
80-120
<_ 20
Nickel
0.0100
0.0099/0,0103
99/103
4
80-120
<_ 20
Potassium
1.0
1.0/1.0
100/100
0
80-120
<_ 20
TSS
N/A
N/A
N/A
N/A
N/A
N/A
Selenium
0.025
0.030/0.030
120/120
0
80-120
<_ 20
Sodium
1.0
1.0/1.0
100/100
0
80-120
<_ 20
Strontium
0.100
0.098/0.105
98/105
7
80-120
<_ 20

10.0
10.5/10.6
105/106
1
80-120
<_ 20
0.0100
0.0102/0.0105
102/105
3
80-120
<_ 20
N/A
N/A
N/A
N/A
N/A
N/A
MVanadium
N/A
N/A
N/A
N/A
N/A
N/A
0.025
0.024/0.025
96/100
4
80-120
<_20
0.100
0.099/0.102
99/102
3
80-120
20
71TTVT WA'TV 4ZA1% PT.Ti.0
Parameter
Results mg/L
% Difference
Limits
Alkalinity
36
36
0
<_ 10
Aluminum
N/A
N/A
N/A
N/A
Antimony
N/A
N/A
N/A
N/A
Arsenic
N/A
N/A
N/A
N/A
Barium
N/A
N/A
N/A
N/A
Beryllium
N/A
N/A
N/A
N/A
Boron
N/A
N/A
N/A
N/A
Cadmium
N/A
N/A
N/A
N/A
Calcium
N/A
N/A
N/A
N/A
Chloride
467
462
1
< 10
Chromium
N/A
N/A
N/A
N/A
Cobalt
N/A
N/A
N/A
N/A
Conductivity
156
156
0
<_ 10
Copper
N/A
N/A
N/A
N/A
Iron
N/A
N/A
N/A
N/A
Lead
N/A
N/A
N/A
N/A
Magnesium
N/A
N/A
N/A
N/A
Manganese
N/A
N/A
N/A
N/A
Mercury
N/A
N/A
N/A
N/A
Molybdenum
N/A
N/A
N/A
N/A
Nickel
N/A
N/A
N/A
N/A
Potassium
N/A
N/A
N/A
N/A
TSS
313.3
303.3
3
<_ 10
Selenium
N/A
N/A
N/A
N/A
Sodium
N/A
N/A
N/A
N/A

Strontium
N/A
N/A
N/A
N/A
Sulfate
28
29
4
< 10
Thallium
N/A
N/A
N/A
N/A
TDS
403
404
0
<_ 10
Turbidity
0.37
0.37
0
< 10
Vanadium
N/A
N/A
N/A
N/A
Zinc
N/A
N/A
N/A
N/A
BLANKS
Parameter
Rmg�'
Limit, mg/L
Alkalinity
1
1
Aluminum
<0.005
0.005
Antimony
<0.0005
0.0005
Arsenic
<0.0005
0.0005
Barium
<0.0005
0.0005
Beryllium
<0.0005
0.0005
Boron
<0.005
0.005
Cadmium
<0.0005
0.0005
Calcium
<0.5
0.5
Chloride
<2.5
2.5
Chromium
<0.0005
0.0005
Cobalt
<0.0005
0.0005
Conductivity
<5
5
Copper
<0.0005
0.0005
Iron
<0.005
0.005
Lead
<0.0005
0.0005
Magnesium
<0.5
0.5
Manganese
<0.0005
0.0005
Mercury
<0.0002
0.0002
Molybdenum
<0.0005
0.0005
Nickel
<0.00005
0.00005
Potassium
<0.5
0.5
TSS
<2.5
2.5

Selenium
<0.0005
0.0005
Sodium
<0.5
0.5
Strontium
<0.005
0.005
Sulfate
<2.5
2.5
Thallium
<0.00005
0.00005
TDS
<2.5
2.5
Turbidity
N/A
N/A
Vanadium
<0.0005
0.0005
Zinc
<0.005
0.005

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elementOne
Ray Porter
Environmental Chemists, Inc.
66002 Windmill Way
Wilmington, NC 28405
Sample #
Sample Matrix DW
Date Sampled 03/05/2015
Delivered by Client
Parameter
Chromium VI
Element One Inc.
6319-D Carolina Beach Rd.
Wilmington, NC 28412
Phone: [phone]
Fax: [phone]
[e-mail]
FINAL REPORT OF ANALYSES
March 09, 2015
Client Project Name:
Client Project Number:
E1 Project Number e24189
Sample ID 15-06244
Sample Type Date Received 03/06/2015
Time Sampled 1045 Time Received 0810
Sampler Received by KMS
E1 Sample # 24189-5
Result Unit Dilution DL Method Date
< 0.02 pg/L 1 0.02 EPA 218.7 03/09/2015
Ken mith, Laboratory Director
24189 Envirochem Cr6+Report Compiled by �'w
NC Certifications: DW 37788 and DWQ DENR 604

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Meter Id: 11277 Meter Id: 11250 Meter Id: 09996 - Meter Id: NYI-11373 ---
Analyst:
pH Analysis
neoe.e..... McPoed• SM dGnn R R SM ?.e
Cal. Time
Calibration Buffer 4.0
Calibration Buffer 10.0 "Check Buffer 7.0
Comments
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/740 2--
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Slope: 919- c) _
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"pH buffer checks are to be within ±0.1 pH units of the standards true value
Facility/Sample location
Time Sampled*
Time Analyzed+•
Temp ('C) ■ I
pH Result
Buffer Check value
Comment
9.
's-2,1
+If sample is measured in directly in the stream only time analyzed would be recorded.
►Indicates a recommended drift check (Use Buffer 7.0) Should be within � 0.1 units of the buffees true value)
a Document the temperature of the sample at the time of analysis. Note: This temperature is not to be used for reporting on the monthly monitoring report
Calibration drift check is recommended when performing analysis at multiple sampling locations,
*All pH results in pH units (i.e., s.u.).
. _Total Residual Chlorine (PRC)
D.f<... Mr/hndr Rarh TTIU f LR37n..
Facility/Sample Location
Time Sampled
I Time Analyzed
TRC Result
uglL
Daily check standard
obtained value ug/L
Comment
11LC check standard obtained true value 210 (acceptance range 190-220 ug/L) (Should recover within �10% of the
check standard's obtained true value)
Dissolved Oxygen (DO)
Reference Method: SM 4500 O G, 20th Edition, —YSI DO 550 A Model—YSI PRO 20
Temperature
.0
Adjusted An
Calibration♦
Saturation
%
Calibration
Time
Facility/Sample Location
DO reading
mg/L
`Time
AnalyzedTime
Sampled
Sample Temperature
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- - - -- ♦ When performing analysis at multiple sampling locations, re-calibration(s) should he performed every four hours.
`Analysis time and sampling time the same. (Ideally the sample should be analyzed m-situ):.
Temperature Sensor Annual Check Date(550 A): INPROCESS Temperature Sensor Annual Check Date (PRO 20):IN PROCESS
Temperature .. ..._ .
Reference Method: SM 2550 B 20- Edition
Facility/Sample Location
Tenn/Dent.-C
`Timle Analy=nime Sampled
.- Comments
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