NC0001422_Laboratory COCs - S8R1-S8R2-S8R-Post Ele1-FR_20150805

Duke Energy
Laboratory Services
13339 Hagers Ferry Road Bld. MG03A
Huntersville, NC 28078

Project ID: Ash Basin GW Assessment – S8R

Metals, Mercury, Hexavalent Chromium, Chloride,
Sulfate, Sodium, Alkalinity, Bicarbonate, Carbonate,
Turbidity, Total Dissolved Solids, Total Suspended
Solids, Dissolved Oxygen, pH, Temperature and
Conductivity

Analytical Report
24842

Element One, Inc.
6319-D Carolina Beach Rd., Wilmington, NC 28412
910-793-0128 FAX: [phone] [e-mail]
el1
The following data for Analytical Report 24842
has been reviewed for completeness, accuracy,
adherence to method protocol,
and compliance with quality assurance guidelines.
Review by:
Katie Strickland, B.S. Chemist
June 10, 2015
Report Reviewed and Finalized By:
%�O
Ken Smith, Laboratory Director
June 10, 2015
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SUMMARY OF RESULTS

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Summary of Analysis

Summary of Method 200.8 Metals Analysis
S8R Well 1 Well
Head
S8R Well 2 Well
Head
S8R Well 2 Well
Head
S8R Well 1
Post
24842-1 24842-2 24842-2 dup 24842-3
Element mg/L mg/L mg/L mg/L
----------------- --------------- --------------- --------------- ---------------
Aluminum 0.039 0.068 0.067 0.018
Antimony < 0.001 < 0.001 < 0.001 < 0.001
Arsenic < 0.005 < 0.005 < 0.005 < 0.005
Barium 0.016 0.045 0.047 0.017
Beryllium < 0.001 < 0.001 < 0.001 < 0.001
Boron 0.017 0.210 0.211 0.019
Cadmium < 0.002 < 0.002 < 0.002 < 0.002
Calcium 3.84 10.1 10.3 3.73
Chromium < 0.005 < 0.005 < 0.005 < 0.005
Cobalt 0.003 0.004 0.004 0.003
Copper < 0.003 < 0.003 < 0.003 < 0.003
Iron 1.95 0.094 0.095 2.07
Lead < 0.003 < 0.003 < 0.003 < 0.003
Magnesium 0.443 2.50 2.51 0.435
Manganese 0.068 0.159 0.162 0.068
Molybdenum < 0.005 < 0.005 < 0.005 < 0.005
Nickel < 0.005 < 0.005 < 0.005 < 0.005
Potassium 0.536 2.13 2.21 0.553
Selenium < 0.005 < 0.005 < 0.005 < 0.005
Strontium 0.014 0.141 0.147 0.014
Thallium < 0.0002 < 0.0002 < 0.0002 < 0.0002
Vanadium < 0.0003 < 0.0003 < 0.0003 < 0.0003
Zinc 0.006 0.008 0.009 0.005

Summary of Method 245.1 Mercury Analysis
S8R Well 1 Well
Head
S8R Well 2 Well
Head
S8R Well 2 Well
Head
S8R Well 1
Post
24842-1 24842-2 24842-2 dup 24842-3
Element mg/L mg/L mg/L mg/L
----------------- ------ --------------- --------------- --------------- ---------------
Mercury #1 < 0.0002 < 0.0002 < 0.0002 < 0.0002
#2 < 0.0002 < 0.0002 < 0.0002 < 0.0002

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Summary of Analysis

Summary of Method 218.7 Hexavalent Chromium Analysis
S8R Well 1 Well
Head
S8R Well 2 Well
Head
S8R Well 2 Well
Head
S8R Well 1
Post
24842-1 24842-2 24842-2 dup 24842-3
Element µg/L µg/L µg/L µg/L
----------------- --------------- --------------- --------------- ---------------
Chromium (VI) < 0.02 < 0.02 < 0.02 < 0.02

Summary of Method 300.0 Anions Analysis
S8R Well 1 Well Head S8R Well 2 Well Head S8R Well 1 Post
24842-1 24842-2 24842-3
Element mg/L mg/L mg/L
----------------- --------------- --------------- ---------------
Chloride 3.39 18.2 3.31
Sulfate 5.84 34.6 5.33

Summary of Method ASTM D6919-03 Sodium Analysis
S8R Well 1 Well Head S8R Well 2 Well Head S8R Well 1 Post
24842-1 24842-2 24842-3
Element mg/L mg/L mg/L
----------------- --------------- --------------- ---------------
Sodium 2.13 11.5 2.09

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Summary of Analysis

Summary of Standard Method 2320B Alkalinity Analysis
S8R Well 1 Well
Head
S8R Well 1 Well
Head
S8R Well 2 Well
Head
S8R Well 1
Post
24842-1 24842-1 dup 24842-2 24842-3
Assay mg/L mg/L mg/L mg/L
----------------- --------------- --------------- --------------- ---------------
Alkalinity as CaCO3 8.96 8.96 10.5 7.96

Summary of Standard Method 4500 CO2 E Analysis
S8R Well 1 Well
Head
S8R Well 2 Well
Head
S8R Well 1
Post
24842-1 24842-2 24842-3
Assay mg/L mg/L mg/L
----------------- --------------- --------------- ---------------
Bicarbonate (HCO32- as CaCO3) 8.96 10.45 7.96
Carbonate (CO32- as CaCO3) < 1 < 1 < 1

Summary of Standard Method 2130 B Turbidity Analysis
S8R Well 1 Well Head S8R Well 2 Well Head S8R Well 1 Post
24842-1 24842-2 24842-3
Assay NTU NTU NTU
----------------- --------------- --------------- ---------------
Turbidity < 1.0 < 1.0 < 1.0

Summary of Standard Method 2540 C TDS Analysis
S8R Well 1 Well
Head
S8R Well 1 Well
Head
S8R Well 2 Well
Head
S8R Well 1
Post
24842-1 24842-1 dup 24842-2 24842-3
Assay mg/L mg/L mg/L mg/L
----------------- --------------- --------------- --------------- ---------------
Total Dissolved Solids 21.3 20.7 77.3 24.0

Summary of Standard Method 2540 D TSS Analysis
S8R Well 1 Well Head S8R Well 2 Well Head S8R Well 1 Post
24842-1 24842-2 24842-3
Assay mg/L mg/L mg/L
----------------- --------------- --------------- ---------------
Total Suspended Solids < 2.5 < 2.5 < 2.5

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Summary of Analysis

Summary of Standard Method 4500O G DO Analysis
S8R Well 1 Well Head S8R Well 2 Well Head S8R Well 1 Post
24842-1 24842-2 24842-3
Assay mg/L mg/L mg/L
----------------- --------------- --------------- ---------------
Dissolved Oxygen 5.73 7.85 6.98

Summary of Standard Method 4500H+ pH Analysis
S8R Well 1 Well Head S8R Well 2 Well Head S8R Well 1 Post
24842-1 24842-2 24842-3
Assay SU SU SU
----------------- --------------- --------------- ---------------
pH 5.89 5.29 5.75

Summary of Standard Method 2500 B Temperature Analysis
S8R Well 1 Well Head S8R Well 2 Well Head S8R Well 1 Post
24842-1 24842-2 24842-3
Assay °C °C °C
----------------- --------------- --------------- ---------------
Temperature 22.2 22.1 28.3

Summary of Standard Method 2510 B Conductivity Analysis
S8R Well 1 Well Head S8R Well 2 Well Head S8R Well 1 Post
24842-1 24842-2 24842-3
Assay µmhos/cm µmhos/cm µmhos/cm
----------------- --------------- --------------- ---------------
Conductivity 54.5 155.7 60.6

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ANALYTICAL NARRATIVE

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Element One Analytical Narrative

Client: Duke Energy Element One #: 24842
Client ID: Ash Basin GW Assessment –S8R Analyst: DBW, DAM, KLS, LAW, PQT, KAM, DMR
Method: See table below Dates Received: 05/27/2015
Analytes: See table below Dates Analyzed: 05/27-29/15

Summary of Analysis
The samples were collected by Element One, Inc. on 05/27/2015 and were analyzed for
pH, temperature, conductivity and dissolved oxygen in the f ield immediately following
sampling. Samples were returned to Element One, Inc., prepared and analyzed for the
other parameters following method protocol. The samples were analyzed for metals
according to EPA Method 200.8 protocol on a PerkinElmer ELAN 6100 ICP-MS. The
samples were analyzed for mercury according to EPA method 245.1 on a PerkinElmer
FIMS-100 CVAA mercury analyzer. Samples were prepared and analyzed for chromium
(VI) according to EPA 218.7 protocol on a Shimadzu 2010 HPLC unit and a Timberline
RDR-1 Reaction Module. Samples were analyzed for chloride, sulfate by EPA 300.0
and sodium by ATSM D6919-03 on Metrohm 861/788 and 761/788 ion chromatograph
system.

Detection Limits
The following is a list of parameters, methods used and the associated reporting limit for
each:
Parameter DL, mg/L Method Parameter DL, mg/L Method
Beryllium 0.001 EPA 200.8 Antimony *0.001 EPA 200.8
Boron 0.005 EPA 200.8 Barium 0.005 EPA 200.8
Magnesium 0.02 EPA 200.8 Thallium *0.0002 EPA 200.8
Aluminum 0.005 EPA 200.8 Lead 0.003 EPA 200.8
Potassium 0.02 EPA 200.8 Mercury 0.0002 EPA 245.1
Calcium 0.05 EPA 200.8 Chromium (VI) 0.02µg/L EPA 218.7
Vanadium *0.0003 EPA 200.8 Chloride 0.1 EPA 300.0
Chromium 0.005 EPA 200.8 Sulfate 0.1 EPA 300.0
Manganese 0.005 EPA 200.8 Sodium 0.05 ASTM D6919-03
Iron 0.02 EPA 200.8 Alkalinity 1 SM 2320 B
Cobalt *0.001 EPA 200.8 Bicarbonate 1 SM 4500 CO2 D
Nickel 0.005 EPA 200.8 Carbonate 1 SM 4500 CO2 D
Copper 0.003 EPA 200.8 Turbidity 1.0 NTU SM 2130 B
Zinc 0.005 EPA 200.8 TDS 10 SM 2540 C
Arsenic 0.005 EPA 200.8 TSS 2.5 SM 2540 D
Selenium 0.005 EPA 200.8 Dissolved Oxygen SM 4500O G
Strontium 0.005 EPA 200.8 pH 1.0 SU SM 4500-H+
Molybdenum 0.005 EPA 200.8 Temperature SM 2500 B
Cadmium 0.002 EPA 200.8 Conductivity 10µmhos/cm SM2510B
*Detection Limit based on client request.

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Element One Analytical Narrative

Analysis QA/QC

Duplicate analyses relative percent difference (RPD), sample spike recovery and second
source calibration verification data are summarized in the Quality Control Section. All
QA/QC data was within the criteria of the method.

Additional Comments

The reported results have not been corrected for any blank values or spike recovery
values. The reported results relate only to the items tested or calibrated.

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QUALITY CONTROL SUMMARY

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Summary of Quality Control Data

200.8 Duplicate Analysis RPD
(QC limits: < 20% for RPD.)
S8R Well 2 Well Head
Element RPD
----------------- ---------------
Aluminum 2.1%
Antimony NA
Arsenic NA
Barium 3.6%
Beryllium NA
Boron 0.5%
Cadmium NA
Calcium 1.7%
Chromium NA
Cobalt 5.0%
Copper NA
Iron 1.0%
Lead NA
Magnesium 0.2%
Manganese 1.3%
Molybdenum NA
Nickel NA
Potassium 3.6%
Selenium NA
Strontium 3.7%
Thallium NA
Vanadium NA
Zinc 15.3%
*See Analytical Narrative page 10.

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Summary of Quality Control Data

200.8 Sample Spike Recovery
(QC limits: 75-125% for Recovery.)
S8R Well 1 Post
Element Recovery
----------------- ---------------
Aluminum 104%
Antimony 98%
Arsenic 97%
Barium 95%
Beryllium 93%
Boron 92%
Cadmium 94%
Calcium 120%
Chromium 105%
Cobalt 100%
Copper 101%
Iron 86%
Lead 109%
Magnesium 94%
Manganese 91%
Molybdenum 108%
Nickel 105%
Potassium 89%
Selenium 89%
Strontium 95%
Thallium 102%
Vanadium 109%
Zinc 91%
*See Analytical Narrative page 10.

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Summary of Quality Control Data

Metals Second Source Calibration Check Recoveries
(QC limits: ±10% for Second Source Continuing Check Standard*)
Element 1 ppb 50 ppb 100 ppb* 250 ppb
----------------- ----------------- ----------------- ----------------- -----------------
Aluminum 109% 102% 109% 111%
Antimony 106% 102% 97% 93%
Arsenic 91% 103% 107% 103%
Barium 79% 100% 97% 93%
Beryllium 104% 103% 105% 102%
Cadmium 106% 101% 105% 103%
Chromium 91% 93% 98% 103%
Cobalt 101% 99% 96% 93%
Copper 112% 102% 98% 93%
Lead 116% 101% 110% 113%
Manganese 108% 103% 107% 110%
Molybdenum 103% 100% 110% 110%
Nickel 101% 103% 108% 106%
Selenium 107% 103% 108% 104%
Strontium 100% ---- 100% 92%
Zinc 96% 101% 100% 93%

Element 21 ppb 250 ppb 1100 ppb* 2500 ppb
----------------- ----------------- ----------------- ----------------- -----------------
Calcium 93% 93% 100% 93%
Iron 89% 103% 95% 90%
Magnesium 107% 100% 103% 107%
Potassium 98% 100% 99% 92%

Element 5 ppb 50 ppb 100 ppb* 250 ppb
----------------- ----------------- ----------------- ----------------- -----------------
Boron 131% 104% 108% 117%

Element 0.3 ppb 1 ppb 10 ppb* 25 ppb
----------------- ----------------- ----------------- ----------------- -----------------
Thallium 99% 102% 101% 101%
Vanadium 92% 105% 103% 99%

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Summary of Quality Control Data

Mercury 245.1 Duplicate Analysis RPD
(QC limits: < 20% for RPD)
S8R Well 2 Well Head
Element RPD
----------------- ---------------
Mercury NA

Mercury 245.1 Sample Spike Recovery
(QC limits: 75-125% for Recovery)
S8R Well 1 Post
Element Recovery
----------------- ---------------
Mercury 101%

Chromium (VI) 218.6 Duplicate Analysis RPD
(QC limits: < 10% for RPD)
S8R Well 2 Well Head
Element RPD
----------------- ---------------
Chromium (VI) NA

Chromium (VI) 218.6 Sample Spike Recovery
(QC limits: 90-110% for Recovery)
S8R Well 1 Post
Element Recovery
----------------- ---------------
Chromium (VI) 100%

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Summary of Quality Control Data

300.0 Sample Spike Recovery
(QC limits: 90-110% for Recovery.)
S8R Well 1 Well Head
Element Recovery
----------------- ---------------
Chloride 99%
Sulfate 96%

Sodium ASTM D6919-03 Sample Spike Recovery
(QC limits: 90-110% for Recovery)
S8R Well 1 Well Head
Element Recovery
----------------- ---------------
Sodium 103%

Alkalinity SM 2320B Duplicate Analysis RPD
(QC limits: < 10% for RPD)
S8R Well 1 Well Head
Element RPD
----------------- ---------------
Alkalinity 0.0%

TDS SM 2540 C Duplicate Analysis RPD
(QC limits: < 10% for RPD)
S8R Well 1 Well Head
Element RPD
----------------- ---------------
Total Dissolved Solids 3.17%

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SAMPLE CUSTODY

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ANALYTICAL DATA

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Analytical Calculations

Metals, Mercury-

Metals (mg/L) = ICP Results (µg/L)*Dilution
1000
Where-

ICP-Hg Results = Raw sample concentration (ppb)—ICP-Hg -Data Sheet

Dilution= Diluted Volume--ICP-MS Run Sheet/ Hg Run Sheet
Aliquot

Chromium (VI)-

Chromium (VI) (µg/L) = HPLC Results (µg/L)*Dilution
Where-

HPLC Results = Raw sample concentration (ppb)—HPLC -Data Sheet

Dilution= Diluted Volume--HPLC Run Sheet
Aliquot

Anions-

Anions (mg/L) = IC Results (mg/L)*Dilution
Where-

IC Results = Raw sample concentration (ppm)—IC-Data Sheet

Dilution= Diluted Volume-- IC-Data Sheet
Aliquot

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Analytical Calculations

Spike Recovery-

Spike (%) = (Spiked Result (µg/L) – Sample Result (µg/L)) X100
Spike Amount (µg/L)

Where-

Spike Result = Raw sample concentration (ppb)--ICP-Data Sheet

Sample Result = Raw sample concentration (ppb)--ICP-Data Sheet

Spike Amount--ICP-MS Spike Table

Duplicate Analysis RPD-

RPD (%) = (Duplicate Result (µg/L) - Sample Result (µg/L)) X100
Average (µg/L)

Where-

Sample Result and Duplicate Results=Raw sample concentration (ppb)--ICP-Data
Sheet

Average= (Duplicate + Sample Results)
2

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PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: Blank
Sample DatThursday, May 28, 2015 14:15:33
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 63924.7 ppb
|- Sc 45 335290.3 ppb
| V-1 51 16873.5 ppb
| V 51 19248.7 ppb
|> Rh 103 664552.9 ppb
|> Ho 165 1243361.4 ppb
|- Tl 205 584.4 ppb
Kr 83 59.5 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 1
Sample DatThursday, May 28, 2015 14:16:48
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 63765.2 ppb
|- Sc 45 327105.1 ppb
| V-1 51 29352.9 0.8873 ppb
| V 51 46137.9 0.94468 ppb
|> Rh 103 664722.1 ppb
|> Ho 165 1250080.7 ppb
|- Tl 205 37172.2 0.97411 ppb
Kr 83 52.4 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 2
Sample DatThursday, May 28, 2015 14:18:03
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 64977.9 ppb
|- Sc 45 329272.5 ppb
| V-1 51 163691.5 10.32057 ppb
| V 51 315495.4 10.32153 ppb
|> Rh 103 668126.5 ppb
|> Ho 165 1267437.4 ppb
|- Tl 205 380221.9 9.97404 ppb
Kr 83 50 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 3
Sample DatThursday, May 28, 2015 14:19:18
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 62692.9 ppb
|- Sc 45 317719.8 ppb
| V-1 51 432072.3 29.8969 ppb
| V 51 857196 29.89467 ppb
|> Rh 103 651681.3 ppb
|> Ho 165 1242308.6 ppb
|- Tl 205 1120552.4 30.00952 ppb
Kr 83 49.8 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatThursday, May 28, 2015 14:20:32
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 63431.7 ppb
|- Sc 45 331058.9 ppb
| V-1 51 8068.2 ppb
| V 51 10520.6 ppb
|> Rh 103 675831.4 ppb
|> Ho 165 1263828.4 ppb
|- Tl 205 713.4 ppb
Kr 83 47 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 2
Sample DatThursday, May 28, 2015 14:21:48
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 64807.6 ppb
|- Sc 45 327670.1 ppb
| V-1 51 11527 0.2402 ppb
| V 51 18558.3 0.27615 ppb
|> Rh 103 676193.9 ppb
|> Ho 165 1251827.3 ppb
|- Tl 205 11814 0.29544 ppb
Kr 83 47.8 mg/L
ICP-Data 1 of 22
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PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 3
Sample DatThursday, May 28, 2015 14:23:03
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 65064.1 ppb
|- Sc 45 331535 ppb
| V-1 51 21091.4 0.93829 ppb
| V 51 38333.8 0.98785 ppb
|> Rh 103 661392.6 ppb
|> Ho 165 1248343 ppb
|- Tl 205 38711.3 1.0138 ppb
Kr 83 43.6 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatThursday, May 28, 2015 14:24:18
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 68617.9 ppb
|- Sc 45 346736.6 ppb
| V-1 51 162168.2 10.33021 ppb
| V 51 320990.6 10.3215 ppb
|> Rh 103 700001.2 ppb
|> Ho 165 1308678.1 ppb
|- Tl 205 395757.2 10.05852 ppb
Kr 83 40.6 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 5
Sample DatThursday, May 28, 2015 14:25:34
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 63973.6 ppb
|- Sc 45 323456.4 ppb
| V-1 51 374310.8 26.38226 ppb
| V 51 745726.1 26.24153 ppb
|> Rh 103 653078 ppb
|> Ho 165 1222178.9 ppb
|- Tl 205 932492.5 25.38756 ppb
Kr 83 48.6 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 9
Sample DatThursday, May 28, 2015 14:26:50
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 68421.1 ppb
|- Sc 45 349176.5 ppb
| V-1 51 5498.3 -0.19928 ppb
| V 51 8365.7 -0.08988 ppb
|> Rh 103 715055.6 ppb
|> Ho 165 1322968.5 ppb
|- Tl 205 749.7 0.00011 ppb
Kr 83 30.7 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 10
Sample DatThursday, May 28, 2015 14:28:05
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 64704.3 ppb
|- Sc 45 344231 ppb
| V-1 51 811326 56.18959 ppb
| V 51 1609490.9 55.44304 ppb
|> Rh 103 672557.2 ppb
|> Ho 165 1247714.4 ppb
|- Tl 205 1832493.6 48.97999 ppb
Kr 83 49.1 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 2
Sample DatThursday, May 28, 2015 14:29:21
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 66950.2 ppb
|- Sc 45 346299.6 ppb
| V-1 51 5346.2 -0.20082 ppb
| V 51 8190.7 -0.0891 ppb
|> Rh 103 698945.6 ppb
|> Ho 165 1298549.2 ppb
|- Tl 205 726.4 -0.00013 ppb
Kr 83 50.4 mg/L
ICP-Data 2 of 22
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PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-1.1
Sample DatThursday, May 28, 2015 14:30:38
Sample DesDUKE
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 67000.3 ppb
|- Sc 45 357326.8 ppb
| V-1 51 9771.9 0.09565 ppb
| V 51 17330.7 0.21446 ppb
|> Rh 103 699351.7 ppb
|> Ho 165 1302747.8 ppb
|- Tl 205 1833.3 0.028 ppb
Kr 83 -3356.9 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-2.1
Sample DatThursday, May 28, 2015 14:31:52
Sample DesDUKE
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 65459.5 ppb
|- Sc 45 355307.8 ppb
| V-1 51 7207.2 -0.05523 ppb
| V 51 11879.1 0.05017 ppb
|> Rh 103 669764.5 ppb
|> Ho 165 1288687.4 ppb
|- Tl 205 1365.8 0.01638 ppb
Kr 83 -27957.7 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-2.1
Sample DatThursday, May 28, 2015 14:33:07
Sample DesDUKE
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 66988.1 ppb
|- Sc 45 355968.2 ppb
| V-1 51 7524.1 -0.04163 ppb
| V 51 12179.3 0.05396 ppb
|> Rh 103 680722.5 ppb
|> Ho 165 1312990.5 ppb
|- Tl 205 1115.1 0.00949 ppb
Kr 83 -27744.2 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-3.1
Sample DatThursday, May 28, 2015 14:34:22
Sample DesDUKE
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 64114.2 ppb
|- Sc 45 343267.4 ppb
| V-1 51 8991.1 0.06429 ppb
| V 51 15884.7 0.18472 ppb
|> Rh 103 675748.8 ppb
|> Ho 165 1249985.7 ppb
|- Tl 205 754.7 0.0013 ppb
Kr 83 -3177.1 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-3.1
Sample DatThursday, May 28, 2015 14:35:37
Sample DesDUKE
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 66016.3 ppb
|- Sc 45 354887.1 ppb
| V-1 51 792427.4 54.97318 ppb
| V 51 1572678.9 54.26559 ppb
|> Rh 103 670524.2 ppb
|> Ho 165 1260432.1 ppb
|- Tl 205 1933291.5 51.07152 ppb
Kr 83 -3018.2 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatThursday, May 28, 2015 14:36:54
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 63645.8 ppb
|- Sc 45 328248.7 ppb
| V-1 51 4948 -0.2102 ppb
| V 51 7602.1 -0.0955 ppb
|> Rh 103 663668.4 ppb
|> Ho 165 1233380.5 ppb
|- Tl 205 459.3 -0.00638 ppb
Kr 83 38.4 mg/L
ICP-Data 3 of 22
elementOne
e 24842-Metals 63.3
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatThursday, May 28, 2015 14:38:09
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 65146.6 ppb
|- Sc 45 331562.7 ppb
| V-1 51 153490.6 10.14559 ppb
| V 51 304795.4 10.17459 ppb
|> Rh 103 672694.7 ppb
|> Ho 165 1258541 ppb
|- Tl 205 375635.1 9.9184 ppb
Kr 83 44.4 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC 50ppb
Sample DatThursday, May 28, 2015 14:42:30
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 66365.3 ppb
|- Sc 45 336434.4 ppb
| V-1 51 820365.9 56.93538 ppb
| V 51 1544878.9 53.29866 ppb
|> Rh 103 669598.6 ppb
|> Ho 165 1230155.2 ppb
|- Tl 205 1805026.1 48.80854 ppb
Kr 83 50.9 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatThursday, May 28, 2015 14:43:47
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 67250.5 ppb
|- Sc 45 348248 ppb
| V-1 51 8607.4 0.02759 ppb
| V 51 11189.6 0.01651 ppb
|> Rh 103 689161.9 ppb
|> Ho 165 1277204.3 ppb
|- Tl 205 585.7 -0.00349 ppb
Kr 83 42.1 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatThursday, May 28, 2015 14:45:02
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 70061.3 ppb
|- Sc 45 351423.6 ppb
| V-1 51 163571.7 10.3412 ppb
| V 51 323821.8 10.33439 ppb
|> Rh 103 705482.8 ppb
|> Ho 165 1293398.4 ppb
|- Tl 205 391458.7 10.05831 ppb
Kr 83 36.6 mg/L
ICP-Data 4 of 22
elementOne
e 24842-Metals 63.4
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: Blank
Sample DatThursday, May 28, 2015 17:14:43
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 125623.7 ppb
| Be 9 13.7 ppb
| B 10 1489.8 ppb
|- B 11 6742.2 ppb
|- Mg 24 9072 ppb
| Mg 25 1323.4 ppb
| Al 27 14156.5 ppb
| K 39 469609.6 ppb
| Ca 44 32521.4 ppb
| Sc 45 413151.9 ppb
| Cr 52 16471.2 ppb
| Cr 53 38790.6 ppb
| Fe 54 53351.5 ppb
| Mn 55 3791.5 ppb
| Fe 57 7943.8 ppb
| Co 59 692 ppb
| Ni 60 620.4 ppb
| Cu 63 1636.8 ppb
| Cu 65 995.7 ppb
| Zn 66 2197.6 ppb
| Zn 67 4341.4 ppb
| Zn 68 2561.4 ppb
| As 75 -878.2 ppb
| Se 77 4926 ppb
| Se 82 22.4 ppb
| Sr 88 1397.4 ppb
| Mo 95 2241 ppb
| Mo 97 1365.8 ppb
| Mo 98 3565.7 ppb
|> Rh 103 736879.1 ppb
| Cd 111 157.1 ppb
| Cd 114 317 ppb
| Sb 121 340.3 ppb
| Sb 123 275.1 ppb
| Ba 135 661.7 ppb
| Ba 137 1141.4 ppb
| Ho 165 1376706.8 ppb
| Pb 206 1235.8 ppb
| Pb 207 1023.7 ppb
|- Pb 208 4737.2 ppb
Kr 83 55.5 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 1
Sample DatThursday, May 28, 2015 17:17:55
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 126542 ppb
| Be 9 787.7 1.04804 ppb
| B 10 2556.4 4.53285 ppb
|- B 11 11552 4.62281 ppb
|- Mg 24 168845.4 24.33462 ppb
| Mg 25 24193.2 24.68832 ppb
| Al 27 27888.5 1.34797 ppb
| K 39 781799.1 21.96734 ppb
| Ca 44 44709.7 23.76096 ppb
| Sc 45 421730.7 ppb
| Cr 52 32963.7 1.2068 ppb
| Cr 53 43020.2 2.3672 ppb
| Fe 54 83317.5 25.65392 ppb
| Mn 55 29100.2 1.13612 ppb
| Fe 57 18828.8 24.02535 ppb
| Co 59 19426.1 1.14848 ppb
| Ni 60 4449.8 1.03454 ppb
| Cu 63 10610.2 1.14642 ppb
| Cu 65 5540.7 1.19958 ppb
| Zn 66 4538.8 0.87575 ppb
| Zn 67 4741.9 0.86627 ppb
| Zn 68 4207.3 0.81839 ppb
| As 75 2186.9 1.06841 ppb
| Se 77 5556 2.41037 ppb
| Se 82 358.1 1.05519 ppb
| Sr 88 40458.2 0.56997 ppb
| Mo 95 6574.4 0.846 ppb
| Mo 97 4115.3 0.80995 ppb
| Mo 98 10513.7 0.84621 ppb
|> Rh 103 740930.7 ppb
| Cd 111 4167.9 1.0834 ppb
| Cd 114 9549.9 1.16267 ppb
| Sb 121 12771.3 1.14123 ppb
| Sb 123 9894.2 1.15533 ppb
| Ba 135 4059.6 0.93419 ppb
| Ba 137 7099.1 1.0137 ppb
| Ho 165 1382626.1 ppb
| Pb 206 16141.3 1.20619 ppb
| Pb 207 14360.7 1.22592 ppb
|- Pb 208 64912.1 1.21664 ppb
Kr 83 -206.7 ppb
ICP-Data 5 of 22
elementOne
e 24842-Metals 63.5
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 2
Sample DatThursday, May 28, 2015 17:21:08
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 122755.6 ppb
| Be 9 74684 104.2113 ppb
| B 10 24761 103.1509 ppb
|- B 11 110054.6 103.5882 ppb
|- Mg 24 7671534.6 1183.049 ppb
| Mg 25 1158336.9 1265.945 ppb
| Al 27 1170431.5 115.0569 ppb
| K 39 17176028 1200.527 ppb
| Ca 44 650438.4 1237.696 ppb
| Sc 45 413996.5 ppb
| Cr 52 1518446.8 111.9793 ppb
| Cr 53 213965.2 104.5044 ppb
| Fe 54 1458142.8 1229.82 ppb
| Mn 55 2307003.3 104.8328 ppb
| Fe 57 560139.7 1239.416 ppb
| Co 59 1837465 114.1206 ppb
| Ni 60 395607.8 108.2111 ppb
| Cu 63 895888.9 115.8559 ppb
| Cu 65 443839 118.5625 ppb
| Zn 66 306437.5 115.8488 ppb
| Zn 67 53654.9 114.3048 ppb
| Zn 68 228237.5 114.6307 ppb
| As 75 300197.7 106.2817 ppb
| Se 77 31716.2 108.4125 ppb
| Se 82 33966.6 108.1441 ppb
| Sr 88 6697539.5 99.04268 ppb
| Mo 95 550005.6 108.6323 ppb
| Mo 97 343424.5 102.3815 ppb
| Mo 98 883899.9 108.9435 ppb
|> Rh 103 730807 ppb
| Cd 111 383255.7 104.8629 ppb
| Cd 114 900592.7 114.9075 ppb
| Sb 121 1222253.7 113.7017 ppb
| Sb 123 929294.9 113.0995 ppb
| Ba 135 375126.7 104.4569 ppb
| Ba 137 659326.2 113.628 ppb
| Ho 165 1357190.9 ppb
| Pb 206 1443051.7 118.27 ppb
| Pb 207 1276526.5 118.8253 ppb
|- Pb 208 5459528.5 111.7792 ppb
Kr 83 -45326 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 3
Sample DatThursday, May 28, 2015 17:24:20
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 123340.8 ppb
| Be 9 359379.5 499.1576 ppb
| B 10 114854.7 499.3628 ppb
|- B 11 507831.8 499.2751 ppb
|- Mg 24 37807372 5483.377 ppb
| Mg 25 5318441.4 5466.797 ppb
| Al 27 5330544.8 496.9879 ppb
| K 39 81665175 5479.891 ppb
| Ca 44 2942986.1 5472.45 ppb
| Sc 45 446402.9 ppb
| Cr 52 7121305.6 497.6037 ppb
| Cr 53 932869 499.0964 ppb
| Fe 54 6713229.1 5474.018 ppb
| Mn 55 11672411 499.0332 ppb
| Fe 57 2603174.3 5472.105 ppb
| Co 59 8516797.3 497.1756 ppb
| Ni 60 1936457 498.3577 ppb
| Cu 63 4082991.6 496.8285 ppb
| Cu 65 1973884.3 496.2871 ppb
| Zn 66 1390920.2 496.8305 ppb
| Zn 67 232982 497.1393 ppb
| Zn 68 1044211.9 497.0742 ppb
| As 75 1502595.4 498.7435 ppb
| Se 77 136442.2 498.3147 ppb
| Se 82 166494.1 498.3711 ppb
| Sr 88 35990976 500.1923 ppb
| Mo 95 2676516.5 498.2739 ppb
| Mo 97 1777629.9 499.5241 ppb
| Mo 98 4288302.2 498.2116 ppb
|> Rh 103 777748.5 ppb
| Cd 111 1940334.4 499.0273 ppb
| Cd 114 4144365.4 497.0182 ppb
| Sb 121 5687461.5 497.2594 ppb
| Sb 123 4348366 497.3798 ppb
| Ba 135 1904769.9 499.1088 ppb
| Ba 137 3066833.3 497.2744 ppb
| Ho 165 1446318 ppb
| Pb 206 6441029.3 496.3456 ppb
| Pb 207 5670253.2 496.2345 ppb
|- Pb 208 25850497 497.6437 ppb
Kr 83 -243897.1 ppb
ICP-Data 6 of 22
elementOne
e 24842-Metals 63.6
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatThursday, May 28, 2015 17:27:33
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 123253.4 ppb
| Be 9 35.3 0.03069 ppb
| B 10 2754.1 5.71138 ppb
|- B 11 12334.8 5.71965 ppb
|- Mg 24 8182.8 -0.17789 ppb
| Mg 25 1143.1 -0.23782 ppb
| Al 27 8083.6 -0.6275 ppb
| K 39 502033 1.03756 ppb
| Ca 44 30353.3 -6.45311 ppb
| Sc 45 432087.2 ppb
| Cr 52 19222.6 0.15261 ppb
| Cr 53 41138.2 0.51862 ppb
| Fe 54 55865.2 0.4553 ppb
| Mn 55 4189.6 0.01138 ppb
| Fe 57 8672.1 0.93251 ppb
| Co 59 1179.7 0.02763 ppb
| Ni 60 645 0.00051 ppb
| Cu 63 2255.9 0.06948 ppb
| Cu 65 1220.7 0.04851 ppb
| Zn 66 2253.9 -0.009 ppb
| Zn 67 4723.6 0.49045 ppb
| Zn 68 2671.4 0.00777 ppb
| As 75 -969.1 -0.02013 ppb
| Se 77 5486 1.45875 ppb
| Se 82 28.3 0.01577 ppb
| Sr 88 4222.4 0.03944 ppb
| Mo 95 11347.4 1.71914 ppb
| Mo 97 7085.7 1.63048 ppb
| Mo 98 17983 1.69871 ppb
|> Rh 103 764297.3 ppb
| Cd 111 234.6 0.01885 ppb
| Cd 114 511.4 0.02246 ppb
| Sb 121 586.4 0.02087 ppb
| Sb 123 489.5 0.02384 ppb
| Ba 135 826 0.03746 ppb
| Ba 137 1409.4 0.03753 ppb
| Ho 165 1404008.7 ppb
| Pb 206 1323.4 0.00353 ppb
| Pb 207 1234.8 0.01569 ppb
|- Pb 208 5506.7 0.01193 ppb
Kr 83 51 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 2
Sample DatThursday, May 28, 2015 17:30:45
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 127703.5 ppb
| Be 9 789.4 1.04046 ppb
| B 10 3554 8.6782 ppb
|- B 11 15663.2 8.47792 ppb
|- Mg 24 168613.7 23.282 ppb
| Mg 25 23852.9 23.29592 ppb
| Al 27 20773.4 0.56177 ppb
| K 39 796152.5 20.74523 ppb
| Ca 44 41380 13.93676 ppb
| Sc 45 441825.6 ppb
| Cr 52 35884.7 1.3176 ppb
| Cr 53 45146.2 2.56911 ppb
| Fe 54 84074 23.42332 ppb
| Mn 55 28918.9 1.07626 ppb
| Fe 57 19236.3 23.23232 ppb
| Co 59 20883 1.18702 ppb
| Ni 60 4523.8 1.00588 ppb
| Cu 63 11627.4 1.21725 ppb
| Cu 65 5874.2 1.22589 ppb
| Zn 66 4513.1 0.79848 ppb
| Zn 67 5252.5 1.5566 ppb
| Zn 68 4276.7 0.76844 ppb
| As 75 1790 0.90629 ppb
| Se 77 6045.3 3.40867 ppb
| Se 82 378.4 1.07193 ppb
| Sr 88 42792.5 0.57935 ppb
| Mo 95 9983.5 1.43598 ppb
| Mo 97 6162.4 1.34284 ppb
| Mo 98 15814 1.41726 ppb
|> Rh 103 771178.2 ppb
| Cd 111 4255.3 1.06118 ppb
| Cd 114 10014.5 1.17123 ppb
| Sb 121 13351.5 1.14604 ppb
| Sb 123 10252.3 1.14953 ppb
| Ba 135 4173.6 0.92028 ppb
| Ba 137 7359.3 1.00858 ppb
| Ho 165 1413348.3 ppb
| Pb 206 15924.3 1.13738 ppb
| Pb 207 14270.2 1.16526 ppb
|- Pb 208 64665 1.1595 ppb
Kr 83 -219.8 ppb
ICP-Data 7 of 22
elementOne
e 24842-Metals 63.7
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 3
Sample DatThursday, May 28, 2015 17:33:58
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 123857.3 ppb
| Be 9 185328.6 256.3373 ppb
| B 10 60366.8 258.338 ppb
|- B 11 269152 260.4552 ppb
|- Mg 24 17237652 2508.531 ppb
| Mg 25 2481324.5 2559.267 ppb
| Al 27 2719464.2 253.8147 ppb
| K 39 37983358 2540.311 ppb
| Ca 44 1419453.8 2615.836 ppb
| Sc 45 444714.3 ppb
| Cr 52 3729355.8 260.9812 ppb
| Cr 53 501830.3 258.9244 ppb
| Fe 54 3097070 2509.793 ppb
| Mn 55 5981903 256.6069 ppb
| Fe 57 1279810.6 2691.546 ppb
| Co 59 4406468.9 258.1679 ppb
| Ni 60 1000237.8 258.2697 ppb
| Cu 63 2195653.2 268.0533 ppb
| Cu 65 1166119.6 294.1668 ppb
| Zn 66 725224.1 259.5932 ppb
| Zn 67 123138.4 259.04 ppb
| Zn 68 546232.3 260.3774 ppb
| As 75 774477.6 258.1579 ppb
| Se 77 73101.8 258.843 ppb
| Se 82 86037 258.4541 ppb
| Sr 88 9278114.2 129.4147 ppb
| Mo 95 1422036 265.5301 ppb
| Mo 97 886717.1 249.9007 ppb
| Mo 98 2149079.8 250.3819 ppb
|> Rh 103 774890.8 ppb
| Cd 111 982475.5 253.5912 ppb
| Cd 114 2108624.3 253.7792 ppb
| Sb 121 2920058.2 256.2348 ppb
| Sb 123 2229112.5 255.9027 ppb
| Ba 135 965352.2 253.8031 ppb
| Ba 137 1690507.3 275.0667 ppb
| Ho 165 1423189.7 ppb
| Pb 206 3283497.7 253.9191 ppb
| Pb 207 2865855.1 251.6979 ppb
|- Pb 208 13076760 252.6306 ppb
Kr 83 -62806.6 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatThursday, May 28, 2015 17:37:11
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 117459.3 ppb
| Be 9 71875.7 104.8202 ppb
| B 10 24430.5 106.5569 ppb
|- B 11 109300.1 107.7596 ppb
|- Mg 24 7413153.7 1133.451 ppb
| Mg 25 1102177.4 1194.328 ppb
| Al 27 1116918.1 108.7975 ppb
| K 39 17339986 1201.838 ppb
| Ca 44 651516.2 1228.891 ppb
| Sc 45 412175 ppb
| Cr 52 1518342.7 111.0159 ppb
| Cr 53 218871.1 106.3249 ppb
| Fe 54 1461518.9 1221.921 ppb
| Mn 55 2365100.6 106.569 ppb
| Fe 57 562234.3 1233.518 ppb
| Co 59 1843243.6 113.5163 ppb
| Ni 60 397904.7 107.9249 ppb
| Cu 63 902948.7 115.7782 ppb
| Cu 65 447817.3 118.6124 ppb
| Zn 66 309137.8 115.881 ppb
| Zn 67 54434.5 115.0456 ppb
| Zn 68 227607.9 113.3367 ppb
| As 75 303380.7 106.4984 ppb
| Se 77 32324.4 109.7692 ppb
| Se 82 34348.6 108.4374 ppb
| Sr 88 6921816.4 101.5021 ppb
| Mo 95 564335.2 110.5294 ppb
| Mo 97 349952.6 103.4518 ppb
| Mo 98 901959.8 110.234 ppb
|> Rh 103 737061.7 ppb
| Cd 111 386954.9 104.9769 ppb
| Cd 114 906195 114.6414 ppb
| Sb 121 1227498 113.2239 ppb
| Sb 123 939957.7 113.4276 ppb
| Ba 135 376520.4 103.9588 ppb
| Ba 137 660379.6 112.8469 ppb
| Ho 165 1340600.8 ppb
| Pb 206 1414911 114.9824 ppb
| Pb 207 1247140.7 115.1012 ppb
|- Pb 208 5400032.4 109.6257 ppb
Kr 83 -46841.5 ppb
ICP-Data 8 of 22
elementOne
e 24842-Metals 63.8
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 5
Sample DatThursday, May 28, 2015 17:40:24
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 121581.1 ppb
| Be 9 36258.5 51.08164 ppb
| B 10 14420.8 58.02905 ppb
|- B 11 64530.6 58.63705 ppb
|- Mg 24 1781814.6 267.002 ppb
| Mg 25 257698.9 273.6522 ppb
| Al 27 586613.6 55.54373 ppb
| K 39 3489558.5 211.1361 ppb
| Ca 44 164723 257.1874 ppb
| Sc 45 418059.3 ppb
| Cr 52 776171.4 55.23779 ppb
| Cr 53 132741.2 54.21785 ppb
| Fe 54 398009.3 293.5244 ppb
| Mn 55 1245979.8 55.16386 ppb
| Fe 57 133535.8 274.7139 ppb
| Co 59 921525.9 55.82534 ppb
| Ni 60 198174.3 52.80842 ppb
| Cu 63 460320.2 57.98016 ppb
| Cu 65 228372.1 59.39165 ppb
| Zn 66 146821.2 53.71709 ppb
| Zn 67 28643.4 54.76507 ppb
| Zn 68 109380.9 52.91692 ppb
| As 75 148992.4 51.62628 ppb
| Se 77 18860.2 54.61689 ppb
| Se 82 16687.9 51.8074 ppb
| Sr 88 11091.3 0.13916 ppb
| Mo 95 281321.9 53.99697 ppb
| Mo 97 176357.6 51.10185 ppb
| Mo 98 457413.6 54.7956 ppb
|> Rh 103 748980.6 ppb
| Cd 111 192382.1 51.3392 ppb
| Cd 114 450531.8 56.06984 ppb
| Sb 121 613070.5 55.63383 ppb
| Sb 123 467354.3 55.48283 ppb
| Ba 135 183739.6 49.82871 ppb
| Ba 137 320092.1 53.72364 ppb
| Ho 165 1348476.2 ppb
| Pb 206 712300.6 56.91087 ppb
| Pb 207 620307.4 56.28771 ppb
|- Pb 208 2833569.1 56.56053 ppb
Kr 83 27.8 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 9
Sample DatThursday, May 28, 2015 17:43:37
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 124764.9 ppb
| Be 9 14 0.0006 ppb
| B 10 2407.7 4.04757 ppb
|- B 11 10619.2 3.8717 ppb
|- Mg 24 23679.1 2.11255 ppb
| Mg 25 3359 2.08326 ppb
| Al 27 63656.2 4.66938 ppb
| Sc 45 434408.6 ppb
| Mn 55 6872.9 0.12843 ppb
| Ni 60 323 -0.08383 ppb
| As 75 -1671.4 -0.2569 ppb
| Se 77 11039.7 22.98842 ppb
| Se 82 1.6 -0.06643 ppb
| Mo 95 3306.6 0.18909 ppb
| Mo 97 2109.9 0.20105 ppb
| Mo 98 5349.3 0.19812 ppb
|> Rh 103 763064.2 ppb
| Cd 111 97.3 -0.0171 ppb
| Cd 114 195 -0.01624 ppb
| Ho 165 1366695.7 ppb
| Pb 206 694.4 -0.04592 ppb
| Pb 207 612 -0.03992 ppb
|- Pb 208 2728.2 -0.04267 ppb
Kr 83 73.9 ppb
ICP-Data 9 of 22
elementOne
e 24842-Metals 63.9
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 10
Sample DatThursday, May 28, 2015 17:46:49
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 124079.1 ppb
| Be 9 37921.6 52.3443 ppb
| B 10 14734.6 58.07142 ppb
|- B 11 65103.7 57.88289 ppb
|- Mg 24 4085838.5 605.0481 ppb
| Mg 25 604328.8 634.2535 ppb
| Al 27 665912.9 62.29188 ppb
| Sc 45 440512.3 ppb
| Mn 55 1335194 58.25349 ppb
| Ni 60 210599.3 55.30239 ppb
| As 75 154119.5 52.61134 ppb
| Se 77 23859.6 72.94393 ppb
| Se 82 16453.2 50.324 ppb
| Mo 95 301332.8 57.01011 ppb
| Mo 97 188264.1 53.76561 ppb
| Mo 98 485986 57.38143 ppb
|> Rh 103 760179.9 ppb
| Cd 111 198869.2 52.29052 ppb
| Cd 114 461874.4 56.6346 ppb
| Ho 165 1397429.2 ppb
| Pb 206 758120 59.68324 ppb
| Pb 207 656667.6 58.71377 ppb
|- Pb 208 3023846.8 59.47348 ppb
Kr 83 -12932.5 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: Sample
Sample DatThursday, May 28, 2015 17:50:03
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 125972.5 ppb
| Be 9 818.4 1.09397 ppb
| B 10 3036.5 6.66036 ppb
|- B 11 13462 6.54163 ppb
|- Mg 24 164801.2 22.47347 ppb
| Mg 25 23647.7 22.83071 ppb
| Al 27 20827.5 0.5464 ppb
| Sc 45 439898.9 ppb
| Mn 55 30335.3 1.12359 ppb
| Ni 60 4644.9 1.02487 ppb
| As 75 2308.6 1.07187 ppb
| Se 77 6480.6 4.81795 ppb
| Se 82 387.4 1.0865 ppb
| Mo 95 7909.4 1.03082 ppb
| Mo 97 4926.7 0.97824 ppb
| Mo 98 12654.7 1.03187 ppb
|> Rh 103 779211.5 ppb
| Cd 111 4236.8 1.04517 ppb
| Cd 114 9949 1.15096 ppb
| Ho 165 1393846.9 ppb
| Pb 206 15864.2 1.11989 ppb
| Pb 207 13786.5 1.10984 ppb
|- Pb 208 63208.8 1.11852 ppb
Kr 83 -215.1 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-1.1
Sample DatThursday, May 28, 2015 17:53:16
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 131397.4 ppb
| Be 9 32.3 0.02357 ppb
| B 10 5705.8 17.15195 ppb
|- B 11 25206.6 16.98194 ppb
|- Mg 24 3129319.5 442.9841 ppb
| Mg 25 471275.3 472.7893 ppb
| Al 27 444271.6 39.25992 ppb
| Sc 45 479831.4 ppb
| Mn 55 1620411.9 67.65675 ppb
| Ni 60 2015.2 0.33923 ppb
| As 75 2020.5 0.96327 ppb
| Se 77 12452.2 26.53782 ppb
| Se 82 40.9 0.04916 ppb
| Mo 95 1985.6 -0.07866 ppb
| Mo 97 1260.8 -0.05842 ppb
| Mo 98 3145.3 -0.07973 ppb
|> Rh 103 794670.6 ppb
| Cd 111 116.5 -0.01332 ppb
| Cd 114 230 -0.01313 ppb
| Ho 165 1469235.3 ppb
| Pb 206 1567.8 0.01774 ppb
| Pb 207 1356.4 0.02162 ppb
|- Pb 208 6209.2 0.02073 ppb
Kr 83 -3855.2 ppb
ICP-Data 10 of 22
elementOne
e 24842-Metals 63.10
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-2.1
Sample DatThursday, May 28, 2015 17:56:29
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 134185.7 ppb
| Be 9 92.3 0.09915 ppb
| B 10 53981.5 212.1339 ppb
|- B 11 236363.6 209.8673 ppb
|- Mg 24 17820062 2504.343 ppb
| Mg 25 2563815.5 2553.382 ppb
| Al 27 767202.5 68.12577 ppb
| Sc 45 491329 ppb
| Mn 55 3850237.8 159.4266 ppb
| Ni 60 1640.5 0.24072 ppb
| As 75 -2648.5 -0.54338 ppb
| Se 77 17630.9 45.11968 ppb
| Se 82 232.2 0.60265 ppb
| Mo 95 1190.7 -0.22564 ppb
| Mo 97 772.7 -0.19475 ppb
| Mo 98 1853.7 -0.22869 ppb
|> Rh 103 802441.3 ppb
| Cd 111 231.2 0.01497 ppb
| Cd 114 441.2 0.01117 ppb
| Ho 165 1491053.9 ppb
| Pb 206 4042.2 0.20142 ppb
| Pb 207 3435.6 0.19692 ppb
|- Pb 208 16091.3 0.20404 ppb
Kr 83 -37040.6 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-2.1
Sample DatThursday, May 28, 2015 17:59:41
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 128931.2 ppb
| Be 9 99.7 0.11361 ppb
| B 10 50928.4 208.1541 ppb
|- B 11 228318.4 211.0038 ppb
|- Mg 24 17344101 2508.861 ppb
| Mg 25 2474267.3 2536.806 ppb
| Al 27 729728.9 66.67997 ppb
| Sc 45 483805.4 ppb
| Mn 55 3790326.8 161.5714 ppb
| Ni 60 1625.1 0.24867 ppb
| As 75 -1767.1 -0.27881 ppb
| Se 77 18182.8 49.15144 ppb
| Se 82 244.8 0.6596 ppb
| Mo 95 1273.8 -0.2041 ppb
| Mo 97 811.4 -0.1778 ppb
| Mo 98 2036.1 -0.20157 ppb
|> Rh 103 779682.5 ppb
| Cd 111 414.5 0.06353 ppb
| Cd 114 885.8 0.06567 ppb
| Ho 165 1438115.1 ppb
| Pb 206 4758.7 0.26519 ppb
| Pb 207 4079 0.26149 ppb
|- Pb 208 19098.6 0.2704 ppb
Kr 83 -37271.8 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-3.1
Sample DatThursday, May 28, 2015 18:02:53
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 129395.5 ppb
| Be 9 34 0.02647 ppb
| B 10 6058.4 19.00554 ppb
|- B 11 27105.7 19.15795 ppb
|- Mg 24 3056401.3 435.3902 ppb
| Mg 25 455128.6 459.5333 ppb
| Al 27 214101.2 18.32459 ppb
| Sc 45 466455.1 ppb
| Mn 55 1610721.4 67.6854 ppb
| Ni 60 1845.5 0.29957 ppb
| As 75 1334.5 0.74442 ppb
| Se 77 16356 41.44289 ppb
| Se 82 70.4 0.13676 ppb
| Mo 95 1395.4 -0.1846 ppb
| Mo 97 862.7 -0.16639 ppb
| Mo 98 2171.8 -0.18879 ppb
|> Rh 103 789545.8 ppb
| Cd 111 132 -0.00915 ppb
| Cd 114 236.6 -0.01211 ppb
| Ho 165 1415078.8 ppb
| Pb 206 1962.9 0.04857 ppb
| Pb 207 1636.8 0.04665 ppb
|- Pb 208 7666.3 0.04922 ppb
Kr 83 -3859.4 ppb
ICP-Data 11 of 22
elementOne
e 24842-Metals 63.11
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-3.1
Sample DatThursday, May 28, 2015 18:06:06
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 129818.4 ppb
| Be 9 35231.8 46.47189 ppb
| B 10 17204.3 65.55507 ppb
|- B 11 75806.9 65.16273 ppb
|- Mg 24 6781185.1 954.2162 ppb
| Mg 25 1001576.4 998.816 ppb
| Al 27 787571.2 70.13432 ppb
| Sc 45 475855.3 ppb
| Mn 55 2727783.7 113.1569 ppb
| Ni 60 210453.8 52.46085 ppb
| As 75 149159.6 48.37149 ppb
| Se 77 27616.9 82.12927 ppb
| Se 82 15289.5 44.39405 ppb
| Mo 95 298877.9 53.66566 ppb
| Mo 97 186732.7 50.61258 ppb
| Mo 98 482747.8 54.09345 ppb
|> Rh 103 800632.7 ppb
| Cd 111 188807.5 47.1308 ppb
| Cd 114 438098.4 50.99913 ppb
| Ho 165 1441483.3 ppb
| Pb 206 727074.3 54.34112 ppb
| Pb 207 635615 53.95467 ppb
|- Pb 208 2908153.6 54.30222 ppb
Kr 83 -16545.2 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatThursday, May 28, 2015 18:09:20
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 126290.8 ppb
| Be 9 14.3 0.0008 ppb
| B 10 1575.1 0.34276 ppb
|- B 11 7127.1 0.34516 ppb
|- Mg 24 5747.5 -0.56328 ppb
| Mg 25 842 -0.57842 ppb
| Al 27 5825.9 -0.85772 ppb
| K 39 503361.4 0.18153 ppb
| Ca 44 31729.9 -5.47844 ppb
| Sc 45 440731.9 ppb
| Cr 52 25780.2 0.57014 ppb
| Cr 53 55185.7 7.66428 ppb
| Fe 54 58425.5 1.26068 ppb
| Mn 55 3246.6 -0.03364 ppb
| Fe 57 8909.4 0.92074 ppb
| Co 59 395.7 -0.01975 ppb
| Ni 60 517.7 -0.03657 ppb
| Cu 63 1506.5 -0.02872 ppb
| Cu 65 940 -0.03026 ppb
| Zn 66 2101.6 -0.08536 ppb
| Zn 67 5689.4 2.28765 ppb
| Zn 68 2619 -0.05281 ppb
| As 75 -1416.9 -0.15773 ppb
| Se 77 7515.1 8.50652 ppb
| Se 82 0.7 -0.06888 ppb
| Sr 88 1681.5 0.00265 ppb
| Mo 95 1248.4 -0.21016 ppb
| Mo 97 754.4 -0.1951 ppb
| Mo 98 2027.2 -0.20398 ppb
|> Rh 103 785616.9 ppb
| Cd 111 85.4 -0.02089 ppb
| Cd 114 149.3 -0.02239 ppb
| Sb 121 278.3 -0.0073 ppb
| Sb 123 233.7 -0.00674 ppb
| Ba 135 699.4 -0.00155 ppb
| Ba 137 1206.7 -0.00162 ppb
| Ho 165 1393086.3 ppb
| Pb 206 424.7 -0.06811 ppb
| Pb 207 362.3 -0.06317 ppb
|- Pb 208 1703.4 -0.06379 ppb
Kr 83 63.3 ppb
ICP-Data 12 of 22
elementOne
e 24842-Metals 63.12
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatThursday, May 28, 2015 18:12:32
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 121746.4 ppb
| Be 9 72504.3 102.0211 ppb
| B 10 23611.6 98.93131 ppb
|- B 11 105176.3 99.57494 ppb
|- Mg 24 7653613.3 1107.439 ppb
| Mg 25 1125232.7 1153.817 ppb
| Al 27 1150827.5 106.0489 ppb
| K 39 18591020 1219.934 ppb
| Ca 44 681822.1 1216.449 ppb
| Sc 45 435727.3 ppb
| Cr 52 1611230.2 111.493 ppb
| Cr 53 237940.1 110.0428 ppb
| Fe 54 1555226.1 1230.837 ppb
| Mn 55 2506132.5 106.8666 ppb
| Fe 57 598824.4 1243.467 ppb
| Co 59 1936749 112.8814 ppb
| Ni 60 423910.9 108.8142 ppb
| Cu 63 976717.2 118.5327 ppb
| Cu 65 482788.3 121.0224 ppb
| Zn 66 329298.3 116.8267 ppb
| Zn 67 58657.6 117.5164 ppb
| Zn 68 245260.2 115.6029 ppb
| As 75 327264.2 108.711 ppb
| Se 77 35378.4 114.3981 ppb
| Se 82 36556.6 109.2158 ppb
| Sr 88 7357143.9 102.0962 ppb
| Mo 95 592139.2 109.7493 ppb
| Mo 97 371983 104.0678 ppb
| Mo 98 951598.5 110.0669 ppb
|> Rh 103 778851.3 ppb
| Cd 111 406514.7 104.3697 ppb
| Cd 114 951735.3 113.9463 ppb
| Sb 121 1285101.8 112.1793 ppb
| Sb 123 982153.1 112.1633 ppb
| Ba 135 397714.7 103.9168 ppb
| Ba 137 701179.1 113.3895 ppb
| Ho 165 1398549.5 ppb
| Pb 206 1443163.8 110.9739 ppb
| Pb 207 1274976.9 111.3522 ppb
|- Pb 208 5536787.7 106.3649 ppb
Kr 83 -49806.1 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: Blank
Sample DatFriday, May 29, 2015 14:34:57
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 27533.4 ppb
|- P 31 2410.7 ppb
| K 39 349714 ppb
| Ca 44 27618.9 ppb
| Sc 45 176058.9 ppb
| Cr 52 11385.1 ppb
| Cr 53 59747.7 ppb
| Fe 54 29282.8 ppb
| Fe 57 4192.3 ppb
| Co 59 123.3 ppb
| Cu 63 579 ppb
| Cu 65 330 ppb
| Zn 66 873 ppb
| Zn 67 5810.5 ppb
| Zn 68 1746.8 ppb
| Sr 88 393.7 ppb
|> Rh 103 492253.1 ppb
|- Sb 121 235.7 ppb
| Sb 123 176 ppb
| Ba 135 785.4 ppb
| Ba 137 1372.8 ppb
|> Ho 165 962924.7 ppb
Kr 83 45.7 ppb
ICP-Data 13 of 22
elementOne
e 24842-Metals 63.13
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 1
Sample DatFriday, May 29, 2015 14:36:55
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 27357 ppb
|- P 31 8267.8 18.94144 ppb
| K 39 478884.6 20.26357 ppb
| Ca 44 31532.6 19.69135 ppb
| Sc 45 175415.7 ppb
| Cr 52 19067.6 1.05485 ppb
| Cr 53 62222.9 3.52089 ppb
| Fe 54 41323.7 20.6796 ppb
| Fe 57 8850 20.36494 ppb
| Co 59 9212 1.00307 ppb
| Cu 63 5065.7 1.00446 ppb
| Cu 65 2631.7 1.07089 ppb
| Zn 66 1813.5 0.76506 ppb
| Zn 67 6006.7 1.16708 ppb
| Zn 68 2432.3 0.7358 ppb
| Sr 88 22517.5 0.99547 ppb
|> Rh 103 487699.2 ppb
|- Sb 121 8732.9 1.02915 ppb
| Sb 123 6833.1 1.03768 ppb
| Ba 135 2994.8 0.81541 ppb
| Ba 137 5230.8 0.80254 ppb
|> Ho 165 957012.5 ppb
Kr 83 -99.7 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 2
Sample DatFriday, May 29, 2015 14:38:53
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 27781.5 ppb
|- P 31 304531.9 954.24 ppb
| K 39 7474247.4 1068.087 ppb
| Ca 44 263885.9 1091.41 ppb
| Sc 45 180898.1 ppb
| Cr 52 729369.7 95.3299 ppb
| Cr 53 144864.8 95.97359 ppb
| Fe 54 660414 1038.328 ppb
| Fe 57 249416.3 1042.575 ppb
| Co 59 883906.2 95.5907 ppb
| Cu 63 443190.6 97.05055 ppb
| Cu 65 217446.7 98.90864 ppb
| Zn 66 128179.7 100.7468 ppb
| Zn 67 28036.9 101.1692 ppb
| Zn 68 99657.6 100.6237 ppb
| Sr 88 2210279.9 97.50596 ppb
|> Rh 103 497523.5 ppb
|- Sb 121 838185.9 97.99379 ppb
| Sb 123 651707.7 98.02748 ppb
| Ba 135 279958.7 99.31652 ppb
| Ba 137 485510.8 97.03373 ppb
|> Ho 165 990915.7 ppb
Kr 83 -14925.2 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 3
Sample DatFriday, May 29, 2015 14:40:52
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 26266.3 ppb
|- P 31 1488447.4 5009.156 ppb
| K 39 34735446 5506.385 ppb
| Ca 44 1140917.3 5501.723 ppb
| Sc 45 169985.5 ppb
| Cr 52 3546807.1 500.9339 ppb
| Cr 53 469820.9 500.8002 ppb
| Fe 54 3166679.5 5512.336 ppb
| Fe 57 1218670.8 5511.487 ppb
| Co 59 4339694.8 500.8819 ppb
| Cu 63 2140335.8 500.5899 ppb
| Cu 65 1029550.3 500.2181 ppb
| Zn 66 592857.8 499.8511 ppb
| Zn 67 108094.7 499.7658 ppb
| Zn 68 457456.3 499.8758 ppb
| Sr 88 10633626 500.4988 ppb
|> Rh 103 466158.2 ppb
|- Sb 121 4113599.5 500.4012 ppb
| Sb 123 3197152.9 500.3944 ppb
| Ba 135 1352177 500.1371 ppb
| Ba 137 2402180.3 500.5937 ppb
|> Ho 165 952498.6 ppb
Kr 83 -72019 ppb
ICP-Data 14 of 22
elementOne
e 24842-Metals 63.14
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatFriday, May 29, 2015 14:42:50
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 26667.2 ppb
|- P 31 2564.7 0.65161 ppb
| K 39 352514.7 1.46852 ppb
| Ca 44 27615.2 2.5006 ppb
| Sc 45 171632 ppb
| Cr 52 10596.8 -0.07781 ppb
| Cr 53 58455 -0.17877 ppb
| Fe 54 28803.2 0.13593 ppb
| Fe 57 4379.4 1.16894 ppb
| Co 59 590.4 0.05256 ppb
| Cu 63 1174.7 0.13746 ppb
| Cu 65 635.4 0.14677 ppb
| Zn 66 930 0.06047 ppb
| Zn 67 6033.7 1.57589 ppb
| Zn 68 1785.2 0.07642 ppb
| Sr 88 1563.5 0.05372 ppb
|> Rh 103 482894.1 ppb
|- Sb 121 622 0.04762 ppb
| Sb 123 463 0.04553 ppb
| Ba 135 950.4 0.06503 ppb
| Ba 137 1641.1 0.05998 ppb
|> Ho 165 950626.1 ppb
Kr 83 46.4 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 2
Sample DatFriday, May 29, 2015 14:44:48
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 26490.6 ppb
|- P 31 8209.4 19.22941 ppb
| K 39 472456.9 20.58637 ppb
| Ca 44 30943.2 19.53888 ppb
| Sc 45 171982.7 ppb
| Cr 52 17673.8 0.90915 ppb
| Cr 53 60551.7 2.84733 ppb
| Fe 54 39469.2 18.76064 ppb
| Fe 57 8534 19.67018 ppb
| Co 59 9088.9 1.00743 ppb
| Cu 63 5496 1.12315 ppb
| Cu 65 2743.1 1.14582 ppb
| Zn 66 2012.9 0.95566 ppb
| Zn 67 6301.2 3.07065 ppb
| Zn 68 2636.7 1.00013 ppb
| Sr 88 22266.2 1.00244 ppb
|> Rh 103 479012.8 ppb
|- Sb 121 8975.1 1.07377 ppb
| Sb 123 6853.4 1.05548 ppb
| Ba 135 2978.2 0.82498 ppb
| Ba 137 5113.8 0.793 ppb
|> Ho 165 943663.7 ppb
Kr 83 -106.3 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 3
Sample DatFriday, May 29, 2015 14:46:46
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 28983.4 ppb
|- P 31 742598.3 2228.789 ppb
| K 39 16366970 2287.952 ppb
| Ca 44 558599.4 2334.153 ppb
| Sc 45 189446.9 ppb
| Cr 52 1840708.3 231.4995 ppb
| Cr 53 273083.3 227.1653 ppb
| Fe 54 1470619 2258.908 ppb
| Fe 57 558843.5 2247.459 ppb
| Co 59 2248398 231.8953 ppb
| Cu 63 1113760.3 232.7182 ppb
| Cu 65 552706 239.8602 ppb
| Zn 66 309444.1 232.7486 ppb
| Zn 67 59411.3 231.7969 ppb
| Zn 68 243462.2 236.7405 ppb
| Sr 88 5490660.9 230.9517 ppb
|> Rh 103 521739.6 ppb
|- Sb 121 2150664.9 239.5186 ppb
| Sb 123 1623503.9 232.6405 ppb
| Ba 135 705977.2 238.9242 ppb
| Ba 137 1219959.6 232.6357 ppb
|> Ho 165 1040284.9 ppb
Kr 83 -37162.2 ppb
ICP-Data 15 of 22
elementOne
e 24842-Metals 63.15
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatFriday, May 29, 2015 14:48:45
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 27985.2 ppb
|- P 31 311753 975.9971 ppb
| K 39 7627724.7 1089.789 ppb
| Ca 44 265908.7 1099.381 ppb
| Sc 45 180571.5 ppb
| Cr 52 748058.3 97.68658 ppb
| Cr 53 143109.4 93.78612 ppb
| Fe 54 663185 1041.627 ppb
| Fe 57 252750.3 1055.574 ppb
| Co 59 884736.1 95.58437 ppb
| Cu 63 445874.5 97.52712 ppb
| Cu 65 218639 99.32556 ppb
| Zn 66 127692.9 100.2302 ppb
| Zn 67 28380.6 102.6236 ppb
| Zn 68 101238.8 102.1239 ppb
| Sr 88 2260355.2 99.5901 ppb
|> Rh 103 497957.7 ppb
|- Sb 121 835089.3 97.14168 ppb
| Sb 123 650773.1 97.39199 ppb
| Ba 135 280543.7 99.01833 ppb
| Ba 137 488502.5 97.14805 ppb
|> Ho 165 995838.3 ppb
Kr 83 -15267.8 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 5
Sample DatFriday, May 29, 2015 14:50:44
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 27538.5 ppb
|- P 31 64113 196.3796 ppb
| K 39 1675799.7 200.2968 ppb
| Ca 44 77723.2 233.1914 ppb
| Sc 45 181995.4 ppb
| Cr 52 394602.4 51.25486 ppb
| Cr 53 101936.4 48.07781 ppb
| Fe 54 184519.1 257.2675 ppb
| Fe 57 61051.1 243.5309 ppb
| Co 59 454161.7 49.47851 ppb
| Cu 63 230424.5 50.76756 ppb
| Cu 65 111904.1 51.18965 ppb
| Zn 66 64518.3 50.73195 ppb
| Zn 67 17290.1 52.73184 ppb
| Zn 68 51304.1 51.31227 ppb
| Sr 88 922.4 0.02355 ppb
|> Rh 103 493686 ppb
|- Sb 121 425345.7 51.03735 ppb
| Sb 123 328949.9 50.78578 ppb
| Ba 135 139166.5 50.53078 ppb
| Ba 137 244171.5 49.95547 ppb
|> Ho 165 965469.9 ppb
Kr 83 56.4 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 9
Sample DatFriday, May 29, 2015 14:52:43
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 30181.6 ppb
|- P 31 3568 3.00285 ppb
| K 39 403368.3 4.43812 ppb
| Ca 44 28757.1 -2.81472 ppb
| Sc 45 202769.5 ppb
| Cr 52 15382 0.40957 ppb
| Cr 53 86825.9 24.95588 ppb
| Fe 54 41639.8 16.36111 ppb
| Fe 57 4819.3 1.43934 ppb
| Co 59 293.3 0.01672 ppb
| Cu 63 1403.8 0.16409 ppb
| Cu 65 749.4 0.17234 ppb
| Zn 66 4292.7 2.52552 ppb
| Zn 67 9537 14.4847 ppb
| Zn 68 4465.8 2.5424 ppb
| Sr 88 863.7 0.01863 ppb
|> Rh 103 524158.3 ppb
|- Sb 121 645.4 0.04622 ppb
| Sb 123 508.6 0.04833 ppb
| Ba 135 192 -0.22003 ppb
| Ba 137 340 -0.2157 ppb
|> Ho 165 1003446.4 ppb
Kr 83 51.5 ppb
ICP-Data 16 of 22
elementOne
e 24842-Metals 63.16
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 10
Sample DatFriday, May 29, 2015 14:54:41
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 30070.9 ppb
|- P 31 178784.7 534.3765 ppb
| K 39 4251830.8 559.1179 ppb
| Ca 44 165196.4 604.2783 ppb
| Sc 45 199281.1 ppb
| Cr 52 437036.8 54.17258 ppb
| Cr 53 139870.4 83.9092 ppb
| Fe 54 410414.9 599.6916 ppb
| Fe 57 147918.4 585.7851 ppb
| Co 59 505089.8 52.43256 ppb
| Cu 63 254457.2 53.42815 ppb
| Cu 65 126150.5 55.00113 ppb
| Zn 66 73631.7 55.22667 ppb
| Zn 67 22118.6 70.11894 ppb
| Zn 68 58251.7 55.65292 ppb
| Sr 88 1201999.9 50.87918 ppb
|> Rh 103 518196.2 ppb
|- Sb 121 454425.6 52.465 ppb
| Sb 123 350442 52.05656 ppb
| Ba 135 149532.8 52.25723 ppb
| Ba 137 258057.8 50.80959 ppb
|> Ho 165 1003216.4 ppb
Kr 83 -8085.8 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 2
Sample DatFriday, May 29, 2015 14:56:40
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 28241.8 ppb
|- P 31 8797.3 19.6741 ppb
| K 39 482519.6 18.27664 ppb
| Ca 44 29599.8 5.75385 ppb
| Sc 45 180312.2 ppb
| Cr 52 19156.2 0.97756 ppb
| Cr 53 63390.3 2.33889 ppb
| Fe 54 41148.9 17.99926 ppb
| Fe 57 9040.5 19.84951 ppb
| Co 59 9804.6 1.0311 ppb
| Cu 63 5516.7 1.063 ppb
| Cu 65 2833.4 1.11924 ppb
| Zn 66 2087.6 0.9289 ppb
| Zn 67 6897.6 4.21165 ppb
| Zn 68 2746.1 0.96553 ppb
| Sr 88 23288.5 0.99434 ppb
|> Rh 103 505044.3 ppb
|- Sb 121 9372.8 1.08982 ppb
| Sb 123 7010 1.04902 ppb
| Ba 135 3124.5 0.84753 ppb
| Ba 137 5761.2 0.89724 ppb
|> Ho 165 971329.9 ppb
Kr 83 -114.6 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-1.1
Sample DatFriday, May 29, 2015 14:58:39
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 30698.7 ppb
|- P 31 4889.6 6.91086 ppb
| K 39 4150243.4 535.6622 ppb
| Ca 44 908493 3844.015 ppb
| Sc 45 211214.1 ppb
| Cr 52 15886.9 0.46691 ppb
| Cr 53 89049.2 27.04359 ppb
| Fe 54 1281556.1 1945.696 ppb
| Fe 57 504110 2009.018 ppb
| Co 59 24927.5 2.53615 ppb
| Cu 63 5457.3 1.00312 ppb
| Cu 65 2727.7 1.02286 ppb
| Zn 66 9406.9 6.34047 ppb
| Zn 67 10852.5 20.03063 ppb
| Zn 68 9111.2 7.04059 ppb
| Sr 88 336157.8 14.00605 ppb
|> Rh 103 526007.4 ppb
|- Sb 121 891.1 0.07113 ppb
| Sb 123 656.7 0.06712 ppb
| Ba 135 49948.2 16.70486 ppb
| Ba 137 87283 16.44744 ppb
|> Ho 165 1036134.5 ppb
Kr 83 -2216.8 ppb
ICP-Data 17 of 22
elementOne
e 24842-Metals 63.17
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-2.1
Sample DatFriday, May 29, 2015 15:00:37
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 30395.7 ppb
|- P 31 4687.9 6.43492 ppb
| K 39 15244108 2128.701 ppb
| Ca 44 2483676.5 10831.37 ppb
| Sc 45 218443.7 ppb
| Cr 52 16411.8 0.55219 ppb
| Cr 53 95334.9 34.76905 ppb
| Fe 54 90945 94.13234 ppb
| Fe 57 29481.7 101.6102 ppb
| Co 59 40489.6 4.16578 ppb
| Cu 63 10950.6 2.16291 ppb
| Cu 65 5569.7 2.2689 ppb
| Zn 66 10364.2 7.12736 ppb
| Zn 67 11994.2 25.45313 ppb
| Zn 68 11104.4 9.07568 ppb
| Sr 88 3355461.3 141.2263 ppb
|> Rh 103 521305.7 ppb
|- Sb 121 774.4 0.05818 ppb
| Sb 123 628.3 0.06312 ppb
| Ba 135 135107.1 45.68783 ppb
| Ba 137 235939.2 44.95512 ppb
|> Ho 165 1035917.3 ppb
Kr 83 -22671.7 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-2.1
Sample DatFriday, May 29, 2015 15:02:36
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 29899.7 ppb
|- P 31 4600.2 6.71604 ppb
| K 39 15196514 2206.767 ppb
| Ca 44 2523116.6 11437.16 ppb
| Sc 45 211338.4 ppb
| Cr 52 16430.8 0.63543 ppb
| Cr 53 95168.1 38.58234 ppb
| Fe 54 88096.3 95.04319 ppb
| Fe 57 28322.7 101.3619 ppb
| Co 59 40944.4 4.37792 ppb
| Cu 63 10788.4 2.21735 ppb
| Cu 65 5543 2.35145 ppb
| Zn 66 12571.7 9.16529 ppb
| Zn 67 12097.7 27.93974 ppb
| Zn 68 12460.9 10.88421 ppb
| Sr 88 3352614.2 146.5892 ppb
|> Rh 103 501786.2 ppb
|- Sb 121 559.7 0.03618 ppb
| Sb 123 487.7 0.0451 ppb
| Ba 135 136191 47.5047 ppb
| Ba 137 237038.6 46.58561 ppb
|> Ho 165 1004546.1 ppb
Kr 83 -22663.4 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-3.1
Sample DatFriday, May 29, 2015 15:04:34
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 29976.6 ppb
|- P 31 4980 7.62052 ppb
| K 39 4146904.3 552.594 ppb
| Ca 44 905548.2 3948.664 ppb
| Sc 45 205160 ppb
| Cr 52 16482.6 0.603 ppb
| Cr 53 96307.6 37.91532 ppb
| Fe 54 1323189.7 2071.551 ppb
| Fe 57 514849.3 2113.57 ppb
| Co 59 24403 2.55675 ppb
| Cu 63 2336 0.37023 ppb
| Cu 65 1224.1 0.39091 ppb
| Zn 66 7689.3 5.22501 ppb
| Zn 67 11361.1 23.68962 ppb
| Zn 68 7850.7 6.04268 ppb
| Sr 88 327913.2 14.06737 ppb
|> Rh 103 510905.3 ppb
|- Sb 121 475 0.02691 ppb
| Sb 123 376 0.02902 ppb
| Ba 135 49263.5 17.14107 ppb
| Ba 137 85527.1 16.76777 ppb
|> Ho 165 996359.3 ppb
Kr 83 -2160.9 ppb
ICP-Data 18 of 22
elementOne
e 24842-Metals 63.18
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-3.1
Sample DatFriday, May 29, 2015 15:06:32
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 29765.2 ppb
|- P 31 164223.2 498.6819 ppb
| K 39 7480694.5 1042.12 ppb
| Ca 44 980518.5 4297.486 ppb
| Sc 45 206949.9 ppb
| Cr 52 415913.6 52.3799 ppb
| Cr 53 144421.8 91.52701 ppb
| Fe 54 1613130.6 2542.669 ppb
| Fe 57 621399.1 2561.022 ppb
| Co 59 497397.3 52.50175 ppb
| Cu 63 236243.9 50.43638 ppb
| Cu 65 117786.2 52.23138 ppb
| Zn 66 66572 50.71993 ppb
| Zn 67 22165.3 71.96035 ppb
| Zn 68 54296.4 52.65112 ppb
| Sr 88 1432039.1 61.63495 ppb
|> Rh 103 509665.2 ppb
|- Sb 121 424612.2 49.19847 ppb
| Sb 123 329109.4 49.06181 ppb
| Ba 135 189737 66.63912 ppb
| Ba 137 323593.1 64.0226 ppb
|> Ho 165 999526.3 ppb
Kr 83 -9644.3 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-2.1
Sample DatFriday, May 29, 2015 15:08:38
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 27867.7 ppb
|- P 31 2757.8 1.18854 ppb
| K 39 3075215.4 417.292 ppb
| Ca 44 456652.5 2024.249 ppb
| Sc 45 181121.1 ppb
| Cr 52 11557 0.03756 ppb
| Cr 53 72257 15.12434 ppb
| Fe 54 38927.5 16.64239 ppb
| Fe 57 8569.4 19.14613 ppb
| Co 59 8023.9 0.87159 ppb
| Cu 63 2636.4 0.4611 ppb
| Cu 65 1422.4 0.50881 ppb
| Zn 66 2516.3 1.33196 ppb
| Zn 67 7970.5 10.30599 ppb
| Zn 68 3430 1.78029 ppb
| Sr 88 615589.6 27.6706 ppb
|> Rh 103 487838 ppb
|- Sb 121 306 0.00804 ppb
| Sb 123 274 0.01464 ppb
| Ba 135 26291.3 9.21601 ppb
| Ba 137 45680.2 9.02092 ppb
|> Ho 165 975153.1 ppb
Kr 83 -4123.6 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-2.1
Sample DatFriday, May 29, 2015 15:10:36
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 27705.6 ppb
|- P 31 2864.8 1.68401 ppb
| K 39 3024161.9 417.0369 ppb
| Ca 44 456475.9 2058.637 ppb
| Sc 45 181512.4 ppb
| Cr 52 11461.9 0.04941 ppb
| Cr 53 69207.5 12.87331 ppb
| Fe 54 38443.8 16.85954 ppb
| Fe 57 8464.9 19.28226 ppb
| Co 59 7525.8 0.83006 ppb
| Cu 63 2763.8 0.49965 ppb
| Cu 65 1453.1 0.53393 ppb
| Zn 66 2812.8 1.60817 ppb
| Zn 67 7562.1 8.96725 ppb
| Zn 68 3725.4 2.15348 ppb
| Sr 88 602698.9 27.53086 ppb
|> Rh 103 480109.5 ppb
|- Sb 121 179.3 -0.0068 ppb
| Sb 123 147.7 -0.00442 ppb
| Ba 135 26767.7 9.49823 ppb
| Ba 137 47086 9.41414 ppb
|> Ho 165 964355.4 ppb
Kr 83 -4029.9 ppb
ICP-Data 19 of 22
elementOne
e 24842-Metals 63.19
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatFriday, May 29, 2015 15:12:35
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 27031.4 ppb
|- P 31 2616.4 0.9399 ppb
| K 39 355294.7 2.6583 ppb
| Ca 44 24832.5 -9.09609 ppb
| Sc 45 173326.9 ppb
| Cr 52 10588.2 -0.05911 ppb
| Cr 53 61245.6 4.08559 ppb
| Fe 54 29159.4 1.43748 ppb
| Fe 57 4186.6 0.5812 ppb
| Co 59 50.7 -0.00775 ppb
| Cu 63 460.7 -0.02279 ppb
| Cu 65 310 -0.00441 ppb
| Zn 66 850.4 0.00434 ppb
| Zn 67 6462 4.00935 ppb
| Zn 68 1793.8 0.1113 ppb
| Sr 88 1292.6 0.04286 ppb
|> Rh 103 476314.3 ppb
|- Sb 121 153.3 -0.00936 ppb
| Sb 123 117.4 -0.00852 ppb
| Ba 135 763 0.00109 ppb
| Ba 137 1343.4 0.00315 ppb
|> Ho 165 931693 ppb
Kr 83 41.9 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatFriday, May 29, 2015 15:14:33
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 28437.3 ppb
|- P 31 315907.6 986.8545 ppb
| K 39 7596991.2 1082.742 ppb
| Ca 44 266084.2 1097.329 ppb
| Sc 45 182092.4 ppb
| Cr 52 748839.3 97.56108 ppb
| Cr 53 142386.2 92.60043 ppb
| Fe 54 670236.1 1050.612 ppb
| Fe 57 255679.4 1065.573 ppb
| Co 59 904507.4 97.49911 ppb
| Cu 63 452290.2 98.71698 ppb
| Cu 65 223848.2 101.473 ppb
| Zn 66 130867.6 102.5124 ppb
| Zn 67 28902.2 104.7221 ppb
| Zn 68 102171.7 102.8534 ppb
| Sr 88 2246081.5 98.74544 ppb
|> Rh 103 499094 ppb
|- Sb 121 829138 97.54556 ppb
| Sb 123 641122.6 97.04214 ppb
| Ba 135 280263 100.0535 ppb
| Ba 137 485958 97.74061 ppb
|> Ho 165 984639.2 ppb
Kr 83 -15174.3 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-2.1
Sample DatFriday, May 29, 2015 15:16:56
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 30906.4 ppb
|- P 31 4988.7 7.70981 ppb
| K 39 15588094 2232.655 ppb
| Ca 44 2584954.4 11556.39 ppb
| Sc 45 218406.1 ppb
| Cr 52 15979.7 0.54615 ppb
| Cr 53 86731.4 27.70436 ppb
| Fe 54 93856.5 102.3296 ppb
| Fe 57 30794.7 110.0193 ppb
| Co 59 41660 4.39226 ppb
| Cu 63 11255.6 2.28448 ppb
| Cu 65 5724.5 2.39716 ppb
| Zn 66 11008.7 7.81861 ppb
| Zn 67 11228.9 23.30125 ppb
| Zn 68 11663.8 9.90435 ppb
| Sr 88 3413520.7 147.2196 ppb
|> Rh 103 508761.5 ppb
|- Sb 121 614 0.04174 ppb
| Sb 123 555.8 0.0544 ppb
| Ba 135 135871 46.90667 ppb
| Ba 137 236554 46.01239 ppb
|> Ho 165 1014813 ppb
Kr 83 -23089.1 ppb
ICP-Data 20 of 22
elementOne
e 24842-Metals 63.20
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-2.1
Sample DatFriday, May 29, 2015 15:18:54
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 31268.7 ppb
|- P 31 5101.1 7.96451 ppb
| K 39 15946795 2271.558 ppb
| Ca 44 2651793.5 11789.47 ppb
| Sc 45 220117.8 ppb
| Cr 52 16225.5 0.56635 ppb
| Cr 53 89056.4 29.73007 ppb
| Fe 54 91430.2 97.54604 ppb
| Fe 57 30451.3 107.8226 ppb
| Co 59 41988.1 4.40031 ppb
| Cu 63 12438.5 2.52199 ppb
| Cu 65 6344.2 2.65661 ppb
| Zn 66 12764.6 9.11722 ppb
| Zn 67 11977.6 26.34325 ppb
| Zn 68 12816.4 10.98746 ppb
| Sr 88 3500546.4 150.0657 ppb
|> Rh 103 511824.5 ppb
|- Sb 121 428.3 0.02016 ppb
| Sb 123 392.1 0.02982 ppb
| Ba 135 136780.6 46.78497 ppb
| Ba 137 238720.6 46.00082 ppb
|> Ho 165 1024244.8 ppb
Kr 83 -23664.5 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-3.1
Sample DatFriday, May 29, 2015 15:20:54
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 30575.2 ppb
|- P 31 3016.8 1.54089 ppb
| K 39 1079652.1 103.9017 ppb
| Ca 44 195129.9 745.2592 ppb
| Sc 45 192567.9 ppb
| Cr 52 12328 0.05882 ppb
| Cr 53 69290.7 7.69193 ppb
| Fe 54 283945.6 404.0816 ppb
| Fe 57 104722 413.4845 ppb
| Co 59 5033.7 0.51416 ppb
| Cu 63 888.7 0.06049 ppb
| Cu 65 519 0.07707 ppb
| Zn 66 1926.5 0.77876 ppb
| Zn 67 7593.8 6.79093 ppb
| Zn 68 2830.8 1.005 ppb
| Sr 88 66060.6 2.80567 ppb
|> Rh 103 513415.9 ppb
|- Sb 121 151.7 -0.01087 ppb
| Sb 123 125.4 -0.00864 ppb
| Ba 135 10034.9 3.2341 ppb
| Ba 137 17163.2 3.11044 ppb
|> Ho 165 1004520.1 ppb
Kr 83 -386 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24842-3.1
Sample DatFriday, May 29, 2015 15:22:52
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 26233.4 ppb
|- P 31 65617.3 218.6789 ppb
| K 39 2417279.8 342.9948 ppb
| Ca 44 238446 1075.399 ppb
| Sc 45 170269.9 ppb
| Cr 52 11599.7 0.15478 ppb
| Cr 53 66227.7 13.58579 ppb
| Fe 54 417552.4 701.7606 ppb
| Fe 57 158082.9 716.0742 ppb
| Co 59 465501.5 54.97503 ppb
| Cu 63 4232.3 0.88525 ppb
| Cu 65 2198.3 0.94201 ppb
| Zn 66 1828.5 0.88144 ppb
| Zn 67 7995.2 13.05407 ppb
| Zn 68 2710.1 1.22835 ppb
| Sr 88 63271.1 3.03096 ppb
|> Rh 103 455494.5 ppb
|- Sb 121 205.7 -0.00142 ppb
| Sb 123 168 0.00107 ppb
| Ba 135 9795.9 3.61376 ppb
| Ba 137 17136.5 3.56206 ppb
|> Ho 165 885105.4 ppb
Kr 83 -370.7 ppb
ICP-Data 21 of 22
elementOne
e 24842-Metals 63.21
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatFriday, May 29, 2015 15:24:51
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 27137.8 ppb
|- P 31 2555.7 0.79809 ppb
| K 39 348496.2 1.98173 ppb
| Ca 44 23926.4 -12.67493 ppb
| Sc 45 170049 ppb
| Cr 52 10250.8 -0.09599 ppb
| Cr 53 60254 3.41297 ppb
| Fe 54 28036.2 -0.15697 ppb
| Fe 57 4099.9 0.32228 ppb
| Co 59 66.7 -0.00587 ppb
| Cu 63 465 -0.02105 ppb
| Cu 65 260.7 -0.02698 ppb
| Zn 66 787.4 -0.04289 ppb
| Zn 67 6383.2 3.84682 ppb
| Zn 68 1734.5 0.06141 ppb
| Sr 88 211 -0.00776 ppb
|> Rh 103 472958.6 ppb
|- Sb 121 97.7 -0.0162 ppb
| Sb 123 83 -0.01396 ppb
| Ba 135 761.4 0.00091 ppb
| Ba 137 1313.1 -0.00285 ppb
|> Ho 165 930415.3 ppb
Kr 83 52.9 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatFriday, May 29, 2015 15:26:49
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 27409.7 ppb
|- P 31 299088.7 968.744 ppb
| K 39 7265522.2 1073.28 ppb
| Ca 44 252302.1 1076.884 ppb
| Sc 45 172644.3 ppb
| Cr 52 712082.5 96.18739 ppb
| Cr 53 140878.6 96.78865 ppb
| Fe 54 641218.5 1041.941 ppb
| Fe 57 241081.8 1041.498 ppb
| Co 59 855583.2 95.63814 ppb
| Cu 63 430287.1 97.37632 ppb
| Cu 65 213232.3 100.2278 ppb
| Zn 66 122790.2 99.71245 ppb
| Zn 67 27861.6 104.6519 ppb
| Zn 68 98322.1 102.6188 ppb
| Sr 88 2155724.6 98.2688 ppb
|> Rh 103 481284.1 ppb
|- Sb 121 806892.6 97.84688 ppb
| Sb 123 624215.6 97.38059 ppb
| Ba 135 272004.1 100.0787 ppb
| Ba 137 472314.6 97.91803 ppb
|> Ho 165 955286.2 ppb
Kr 83 -14558 ppb
ICP-Data 22 of 22
elementOne
e 24842-Metals 63.22
PerkinElmer FIMS-100 CVAA Mercury Analyzer
Sample_ID Date Time Mean_Sig Mean_Rd Mean_Rt Units Alq.Vol. Sig 1 Reading-1 Result-1 Sig 2 Reading-2 Result-2
Calib Blank 5/28/2015 11:41:56 AM 0.0006606 µg 0.0006205 0.0007007
STD1 = .004ug 5/28/2015 11:43:37 AM 0.0012793 µg 0.001248 0.0013106
STD2 = .04ug 5/28/2015 11:45:19 AM 0.0124206 µg 0.0123651 0.0124761
STD3 = .08ug 5/28/2015 11:47:12 AM 0.0248472 µg 0.0248836 0.0248107
STD4 = .16ug 5/28/2015 11:49:05 AM 0.0498484 µg 0.049663 0.0500338
STD5 = .2ug 5/28/2015 11:51:00 AM 0.0609196 µg 0.0609555 0.0608837
Reagent Blank 5/28/2015 11:52:54 AM 7.13E-05 0.0002316 0.0002316 µg 4.97E-05 0.0001614 0.0001614 9.29E-05 0.0003018 0.0003018
0.004ug = DL 5/28/2015 11:54:35 AM 0.0012567 0.0040842 0.0040842 µg 0.0012154 0.0039499 0.0039499 0.0012981 0.0042185 0.0042185
0.080ug = QC STD 2 5/28/2015 11:56:17 AM 0.0253928 0.0825227 0.0825227 µg 0.0254205 0.0826128 0.0826128 0.025365 0.0824327 0.0824327
0.080ug = QC STD 3 5/28/2015 11:58:14 AM 0.0249839 0.081194 0.081194 µg 0.0248961 0.0809086 0.0809086 0.0250717 0.0814794 0.0814794
Reagent Blank 5/28/2015 12:00:09 PM 2.77E-05 9.01E-05 9.01E-05 µg 7.86E-07 2.55E-06 2.55E-06 5.47E-05 0.0001776 0.0001776
0.004ug = DL 5/28/2015 1:54:05 PM 0.0012932 0.0042028 0.0042028 µg 0.0012838 0.0041723 0.0041723 0.0013026 0.0042334 0.0042334
0.080ug = QC STD 2 5/28/2015 1:55:49 PM 0.0259068 0.0841932 0.0841932 µg 0.0258008 0.0838489 0.0838489 0.0260127 0.0845376 0.0845376
Reagent Blank 5/28/2015 1:57:42 PM 0.0001304 0.0004238 0.0004238 µg 0.000119 0.0003868 0.0003868 0.0001418 0.0004608 0.0004608
24842-1.1 5/28/2015 2:03:04 PM -3.15E-06 -0.0002418 -6.05E-06 µg 40 1 3.43E-05 -0.00012 -3.00E-06 -4.06E-05 -0.0003636 -9.09E-06
24842-2.1 5/28/2015 2:04:48 PM 2.79E-05 -0.0001409 -3.52E-06 µg 40 1 -1.66E-05 -0.0002856 -7.14E-06 7.24E-05 3.69E-06 9.22E-08
24842-2.1 DUP 5/28/2015 2:06:29 PM -3.75E-06 -0.0002438 -6.09E-06 µg 40 1 -4.56E-06 -0.0002464 -6.16E-06 -2.94E-06 -0.0002411 -6.03E-06
24842-3.1 5/28/2015 2:08:07 PM 4.70E-05 -7.89E-05 -1.97E-06 µg 40 1 -3.01E-05 -0.0003295 -8.24E-06 0.0001241 0.0001718 4.30E-06
24842-3.1 SPK 5/28/2015 2:09:45 PM 0.0248609 0.0805626 0.0020141 µg 40 1 0.0249061 0.0807097 0.0020177 0.0248156 0.0804155 0.0020104
0.004ug = DL 5/28/2015 2:16:37 PM 0.0012883 0.0041867 0.0041867 µg 0.0013172 0.0042807 0.0042807 0.0012593 0.0040927 0.0040927
0.080ug = QC STD 2 5/28/2015 2:18:20 PM 0.0260012 0.0845001 0.0845001 µg 0.0259271 0.0842594 0.0842594 0.0260753 0.0847409 0.0847409
Reagent Blank 5/28/2015 2:20:14 PM 2.88E-05 9.35E-05 9.35E-05 µg 3.07E-06 9.98E-06 9.98E-06 5.45E-05 0.000177 0.000177

Hg-Data 1 of 1
elementOne
e 24842-Hg 64.1