NC0001422_Laboratory COCs - S7-Ele1FR_20150805

Duke Energy
Laboratory Services
13339 Hagers Ferry Road Bld. MG03A
Huntersville, NC 28078

Project ID: Ash Basin GW Assessment – S7

Metals, Mercury, Hexavalent Chromium, Chloride,
Sulfate, Sodium, Alkalinity, Bicarbonate, Carbonate,
Turbidity, Total Dissolved Solids, Total Suspended
Solids, Dissolved Oxygen, pH, Temperature and
Conductivity

Analytical Report
24127

Element One, Inc.
6319-D Carolina Beach Rd., Wilmington, NC 28412
910-793-0128 FAX: [phone] [e-mail]
el1
The following data for Analytical Report 24127
has been reviewed for completeness, accuracy,
adherence to method protocol,
and compliance with quality assurance guidelines.
Review by:
1
Katie Strickland, B.S. Chemist
March 3, 2015
Report Reviewed and Finalized By:
I � I /;� 0 �
Ken Smith, Laboratory Director
March 3, 2015
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SUMMARY OF RESULTS

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Summary of Analysis

Summary of Method 200.8 Metals Analysis
S7 212 Transcom Ct.
24127-1
Element mg/L
----------------- ---------------
Aluminum 0.157
Antimony < 0.001
Arsenic < 0.005
Barium 0.032
Beryllium < 0.001
Boron 0.021
Cadmium < 0.002
Calcium 11.6
Chromium < 0.005
Cobalt < 0.001
Copper < 0.003
Iron < 0.02
Lead < 0.003
Magnesium 1.45
Manganese 0.018
Molybdenum < 0.005
Nickel < 0.005
Potassium 1.40
Selenium < 0.005
Strontium 0.027
Thallium < 0.0002
Vanadium < 0.0003
Zinc 0.007

Summary of Method 245.1 Mercury Analysis
S7 212 Transcom Ct. S7 212 Transcom Ct.
24127-1 24127-1 dup
Element mg/L mg/L
----------------- ------ --------------- ---------------
Mercury #1 < 0.0002 < 0.0002
#2 < 0.0002 < 0.0002

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Summary of Analysis

Summary of Method 218.6 Hexavalent Chromium Analysis
S7 212 Transcom Ct.
24127-1
Element µg/L
----------------- ---------------
Chromium (VI) < 0.1

Summary of Method 300.0 Anions Analysis
S7 212 Transcom Ct.
24127-1
Element mg/L
----------------- ---------------
Chloride 4.41
Sulfate 11.9

Summary of Method ASTM D6919-03 Sodium Analysis
S7 212 Transcom Ct. S7 212 Transcom Ct.
24127-1 24127-1 dup
Element mg/L mg/L
----------------- --------------- ---------------
Sodium 2.90 2.93

Summary of Standard Method 2320B Alkalinity Analysis
S7 212 Transcom Ct. S7 212 Transcom Ct.
24127-1 24127-1 dup
Assay mg/L mg/L
----------------- --------------- ---------------
Alkalinity as CaCO3 9.95 9.95

Summary of Standard Method 4500 CO2 E Analysis
S7 212 Transcom Ct. S7 212 Transcom Ct.
24127-1 24127-1 dup
Assay mg/L mg/L
----------------- --------------- ---------------
Bicarbonate (HCO32- as CaCO3) 9.95 9.95
Carbonate (CO32- as CaCO3) < 1 < 1

Summary of Standard Method 2130 B Turbidity Analysis
S7 212 Transcom Ct.
24127-1
Assay NTU
----------------- ---------------
Turbidity < 1

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Summary of Analysis

Summary of Standard Method 2540 C TDS Analysis
S7 212 Transcom Ct. S7 212 Transcom Ct.
24127-1 24127-1
Assay mg/L mg/L
----------------- --------------- ---------------
Total Dissolved Solids 63.0 64.5

Summary of Standard Method 2540 D TSS Analysis
S7 212 Transcom Ct.
24127-1
Assay mg/L
----------------- ---------------
Total Suspended Solids < 2.5

Summary of Standard Method 4500O G DO Analysis
S7 212 Transcom Ct.
24127-1
Assay mg/L
----------------- ---------------
Dissolved Oxygen 4.52

Summary of Standard Method 4500H+ pH Analysis
S7 212 Transcom Ct.
24127-1
Assay SU
----------------- ---------------
pH 5.58

Summary of Standard Method 2500 B Temperature Analysis
S7 212 Transcom Ct.
24127-1
Assay °C
----------------- ---------------
Temperature 18.6

Summary of Standard Method 2510 B Conductivity Analysis
S7 212 Transcom Ct.
24127-1
Assay µmhos/cm
----------------- ---------------
Conductivity 96.0

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ANALYTICAL NARRATIVE

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Element One Analytical Narrative

Client: Duke Energy Element One #: 24127
Client ID: Ash Basin GW Assessment –S7 Analyst: DBW, DAM, KLS, PQT, KAM
Method: See table below Dates Received: 02/25/2015
Analytes: See table below Dates Analyzed: 02/25-03/03/15

Summary of Analysis
The samples were collected by Element One, Inc. on 02/25/2015 and were analyzed for
pH, temperature, conductivity and dissolved oxygen in the field immediately following
sampling. Samples were returned to Element One, Inc., prepared and analyzed for the
other parameters following method protocol. The samples were analyzed for metals
according to EPA Method 200.8 protocol on a PerkinElmer ELAN 6100 ICP-MS. The
samples were analyzed for mercury according to EPA method 245.1 on a PerkinElmer
FIMS-100 CVAA mercury analyzer. Samples were prepared and analyzed for chromium
(VI) according to SW-846 Method 0061 protocol on a Shimadzu 2010 HPLC unit and a
Timberline RDR-1 Reaction Module. Samples were analyzed for chloride, sulfate by
EPA 300.0 and sodium by ATSM D6919-03 on Metrohm 861/788 and 761/788 ion
chromatograph system.

Detection Limits
The following is a list of parameters, methods used and the associated reporting limit for
each:
Parameter DL, mg/L Method Parameter DL, mg/L Method
Beryllium 0.001 EPA 200.8 Antimony *0.001 EPA 200.8
Boron 0.005 EPA 200.8 Barium 0.005 EPA 200.8
Magnesium 0.02 EPA 200.8 Thallium *0.0002 EPA 200.8
Aluminum 0.005 EPA 200.8 Lead 0.003 EPA 200.8
Potassium 0.02 EPA 200.8 Mercury 0.0002 EPA 245.1
Calcium 0.05 EPA 200.8 Chloride 0.1 EPA 300.0
Vanadium *0.0003 EPA 200.8 Sulfate 0.1 EPA 300.0
Chromium 0.005 EPA 200.8 Sodium 0.05 ASTM D6919-03
Manganese 0.005 EPA 200.8 Alkalinity 1 SM 2320 B
Iron 0.02 EPA 200.8 Bicarbonate 1 SM 4500 CO2 D
Cobalt *0.001 EPA 200.8 Carbonate 1 SM 4500 CO2 D
Nickel 0.005 EPA 200.8 Turbidity 1.0 NTU SM 2130 B
Copper 0.003 EPA 200.8 TDS 10 SM 2540 C
Zinc 0.005 EPA 200.8 TSS 2.5 SM 2540 D
Arsenic 0.005 EPA 200.8 Dissolved Oxygen SM 4500O G
Selenium 0.005 EPA 200.8 pH 1.0 SU SM 4500-H+
Strontium 0.005 EPA 200.8 Temperature SM 2500 B
Molybdenum 0.005 EPA 200.8 Conductivity 10µmhos/cm SM2510B
Cadmium 0.002 EPA 200.8
*Detection Limit based on client request.

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Element One Analytical Narrative

Analysis QA/QC

Duplicate analyses relative percent difference (RPD), sample spike recovery and second
source calibration verification data are summarized in the Quality Control Section.
*The boron spike recovery was outside of laboratory guidelines of 75-125% recovery
with 141% recovery. Sample was reanalyzed at a ten-fold dilution resulting in 120%
recovery. Sample was non-detect for boron at the ten-fold dilution.
All other QA/QC data was within the criteria of the method.

Additional Comments

The reported results have not been corrected for any blank values or spike recovery
values. The reported results relate only to the items tested or calibrated.

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QUALITY CONTROL SUMMARY

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Summary of Quality Control Data

Metals Second Source Calibration Check Recoveries
(QC limits: ±10% for Second Source Continuing Check Standard*)
Element 1 ppb 50 ppb 100 ppb* 250 ppb
----------------- ----------------- ----------------- ----------------- -----------------
Aluminum 102% 100% 97% 99%
Antimony 106% 109% 108% 108%
Arsenic 127% 103% 102% 102%
Barium 102% 108% 108% 107%
Beryllium 101% 101% 100% 103%
Cadmium 105% 103% 103% 102%
Chromium 123% 109% 107% 104%
Cobalt 96% 107% 107% 102%
Copper 97% 107% 104% 107%
Lead 114% 110% 108% 102%
Manganese 104% 108% 108% 103%
Molybdenum 105% 107% 107% 107%
Nickel 102% 102% 103% 101%
Selenium 116% 102% 105% 104%
Strontium 103% --- 103% 102%
Thallium 103% 108% 105% 104%
Zinc 103% 104% 104% 103%

Element 21 ppb 250 ppb 1100 ppb* 2500 ppb
----------------- ----------------- ----------------- ----------------- -----------------
Calcium 117% 105% 102% 101%
Iron 104% 105% 103% 102%
Magnesium 106% 109% 105% 101%
Potassium 100% 104% 102% 100%

Element 5 ppb 100 ppb* 250 ppb
----------------- ----------------- ----------------- -----------------
Boron 117% 109% 106%

Element 0.3 ppb 1 ppb 10 ppb* 25 ppb
----------------- ----------------- ----------------- ----------------- -----------------
Vanadium 98% 94% 99% 98%

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Summary of Quality Control Data

Mercury 245.1 Duplicate Analysis RPD
(QC limits: < 20% for RPD)
Sample ID RPD
------------------------- -------------
S7 212 Transcom Ct. NA

Mercury 245.1 Sample Spike Recovery
(QC limits: 75-125% for Recovery)
Sample ID Recovery
------------------------- -------------
S7 212 Transcom Ct. 98%

218.6 Sample Spike Recovery
(QC limits: 90-110% for Recovery)
S7 212 Transcom Ct.
Element Recovery
----------------- ---------------
Chromium (VI) 98%

300.0 Sample Spike Recovery
(QC limits: 90-110% for Recovery)
S7 212 Transcom Ct.
Element Recovery
----------------- ---------------
Chloride 99%
Sulfate 99%

Sodium ASTM D6919-03 Duplicate Analysis RPD
(QC limits: < 10% for RPD)
Sample ID RPD
------------------------- -------------
S7 212 Transcom Ct. 1.1%

Sodium ASTM D6919-03 Sample Spike Recovery
(QC limits: 90-110% for Recovery)
Sample ID Recovery
------------------------- -------------
S7 212 Transcom Ct. 98%

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Summary of Quality Control Data

Alkalinity SM 2320 B Duplicate Analysis RPD
(QC limits: < 10% for RPD)
Sample ID RPD
------------------------- -------------
S7 212 Transcom Ct. 0.0%

SM 4500 CO2 D Duplicate Analysis RPD
(QC limits: < 10% for RPD)
S7 212 Transcom Ct.
Element RPD
----------------- ---------------
Bicarbonate 0.0%
Carbonate NA

Turbidity SM 2130 B Duplicate Analysis RPD
(QC limits: < 10% for RPD)
Sample ID RPD
------------------------- -------------
S7 212 Transcom Ct. NA

Total Dissolved Solids SM 2540 C Duplicate Analysis RPD
(QC limits: < 5% for RPD)
Sample ID RPD
------------------------- -------------
S7 212 Transcom Ct. 2.35%

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SAMPLE CUSTODY

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ANALYTICAL DATA

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Analytical Calculations

Metals, Mercury-

Metals (mg/L) = ICP Results (µg/L)*Dilution
1000
Where-

ICP-Hg Results = Raw sample concentration (ppb)—ICP-Hg -Data Sheet

Dilution= Diluted Volume--ICP-MS Run Sheet/ Hg Run Sheet
Aliquot

Chromium (VI)-

Chromium (VI) (µg/L) = HPLC Results (µg/L)*Dilution
Where-

HPLC Results = Raw sample concentration (ppb)—HPLC -Data Sheet

Dilution= Diluted Volume--HPLC Run Sheet
Aliquot

Anions-

Anions (mg/L) = IC Results (mg/L)*Dilution
Where-

IC Results = Raw sample concentration (ppm)—IC-Data Sheet

Dilution= Diluted Volume-- IC-Data Sheet
Aliquot

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Analytical Calculations

Spike Recovery-

Spike (%) = (Spiked Result (µg/L) – Sample Result (µg/L)) X100
Spike Amount (µg/L)

Where-

Spike Result = Raw sample concentration (ppb)--ICP-Data Sheet

Sample Result = Raw sample concentration (ppb)--ICP-Data Sheet

Spike Amount--ICP-MS Spike Table

Duplicate Analysis RPD-

RPD (%) = (Duplicate Result (µg/L) - Sample Result (µg/L)) X100
Average (µg/L)

Where-

Sample Result and Duplicate Results=Raw sample concentration (ppb)--ICP-Data
Sheet

Average= (Duplicate + Sample Results)
2

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PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: Blank
Sample DatFriday, February 27, 2015 09:14:23
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 38024.9 ppb
|- Sc 45 243822.6 ppb
| V-1 51 55730.8 ppb
| V 51 56210.8 ppb
|> Rh 103 559336.2 ppb
Ho 165 897420.7 ppb
Kr 83 53 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 1
Sample DatFriday, February 27, 2015 09:15:35
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 36623.2 ppb
|- Sc 45 243566.7 ppb
| V-1 51 58014.9 0.38943 ppb
| V 51 69253.5 0.69019 ppb
|> Rh 103 543090 ppb
Ho 165 862574 ppb
Kr 83 -137 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 2
Sample DatFriday, February 27, 2015 09:16:47
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 35997.1 ppb
|- Sc 45 246887.3 ppb
| V-1 51 150548.5 9.3325 ppb
| V 51 257840.8 9.63993 ppb
|> Rh 103 533537 ppb
Ho 165 854987.5 ppb
Kr 83 -1857.9 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 3
Sample DatFriday, February 27, 2015 09:17:59
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 35168.5 ppb
|- Sc 45 239575 ppb
| V-1 51 353123.4 30.24285 ppb
| V 51 662362.8 30.13035 ppb
|> Rh 103 510988.7 ppb
Ho 165 824413.3 ppb
Kr 83 -5457 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatFriday, February 27, 2015 09:19:10
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 37849.6 ppb
|- Sc 45 241041.3 ppb
| V-1 51 38900.2 ppb
| V 51 40376.2 ppb
|> Rh 103 562493.6 ppb
Ho 165 898319.3 ppb
Kr 83 44.1 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 2
Sample DatFriday, February 27, 2015 09:20:22
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 37191.1 ppb
|- Sc 45 243815.8 ppb
| V-1 51 41258.7 0.31183 ppb
| V 51 45759.3 0.29334 ppb
|> Rh 103 550263 ppb
Ho 165 875309.5 ppb
Kr 83 58.3 mg/L
ICP-Data 1 of 23
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e 24127-Metals 46.1
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 3
Sample DatFriday, February 27, 2015 09:21:34
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 37341.2 ppb
|- Sc 45 246117.3 ppb
| V-1 51 48360.9 0.95629 ppb
| V 51 60116.5 0.94079 ppb
|> Rh 103 551880 ppb
Ho 165 876460.6 ppb
Kr 83 54.8 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatFriday, February 27, 2015 09:22:46
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 36398.1 ppb
|- Sc 45 244950.7 ppb
| V-1 51 143004.9 10.1753 ppb
| V 51 248690.3 9.93583 ppb
|> Rh 103 533147.6 ppb
Ho 165 851850.3 ppb
Kr 83 -1847.7 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 5
Sample DatFriday, February 27, 2015 09:23:58
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 37062.3 ppb
|- Sc 45 246660.3 ppb
| V-1 51 301859.6 25.14334 ppb
| V 51 564586.5 24.62238 ppb
|> Rh 103 537941.7 ppb
Ho 165 857801.6 ppb
Kr 83 47.5 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 9
Sample DatFriday, February 27, 2015 09:25:11
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 37773.7 ppb
|- Sc 45 245958.6 ppb
| V-1 51 35888.7 -0.22031 ppb
| V 51 37521.3 -0.10106 ppb
|> Rh 103 555836.7 ppb
Ho 165 896372.2 ppb
Kr 83 46.4 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 10
Sample DatFriday, February 27, 2015 09:26:23
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 37997.3 ppb
|- Sc 45 252477.9 ppb
| V-1 51 91579.3 4.85382 ppb
| V 51 148267.4 4.88155 ppb
|> Rh 103 558337.6 ppb
Ho 165 894139.7 ppb
Kr 83 -948 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24127-1.1
Sample DatFriday, February 27, 2015 09:28:49
Sample DesDuke
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 37861.7 ppb
|- Sc 45 257935.8 ppb
| V-1 51 38951.8 0.03498 ppb
| V 51 42817.4 0.12406 ppb
|> Rh 103 559634.6 ppb
Ho 165 921358.5 ppb
Kr 83 -4879.3 mg/L
ICP-Data 2 of 23
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e 24127-Metals 46.2
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24127-1.1
Sample DatFriday, February 27, 2015 09:30:00
Sample DesDuke
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 37368 ppb
|- Sc 45 260548.7 ppb
| V-1 51 95878 5.39125 ppb
| V 51 155378.5 5.31619 ppb
|> Rh 103 549274 ppb
Ho 165 905517.4 ppb
Kr 83 -5844.6 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatFriday, February 27, 2015 09:31:14
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 36982.3 ppb
|- Sc 45 238646.2 ppb
| V-1 51 37749.9 -0.13412 ppb
| V 51 39534.4 -0.05373 ppb
|> Rh 103 569726.2 ppb
Ho 165 895915.8 ppb
Kr 83 56.4 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatFriday, February 27, 2015 09:32:26
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
Li 6 35402.3 ppb
|- Sc 45 242539.8 ppb
| V-1 51 142551 9.93876 ppb
| V 51 247406.9 9.71288 ppb
|> Rh 103 540724.8 ppb
Ho 165 850827.4 ppb
Kr 83 -1866 mg/L
Method 6020 & 200.8 Metals Summary Report
Sample ID: Blank
Sample DatFriday, February 27, 2015 09:44:02
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 38603 ppb
| Be 9 4.3 ppb
| B 10 47.3 ppb
|- B 11 191 ppb
|- Mg 24 822.7 ppb
| Mg 25 117.3 ppb
| Al 27 1089.1 ppb
| K 39 444024.3 ppb
| Ca 44 26990.7 ppb
| Sc 45 243364.5 ppb
| Cr 52 9513 ppb
| Cr 53 46611.3 ppb
| Fe 54 28442.4 ppb
| Mn 55 1151.1 ppb
| Fe 57 4737.9 ppb
| Co 59 99 ppb
| Ni 60 97 ppb
| Cu 63 682.4 ppb
| Cu 65 418.7 ppb
| Zn 66 611 ppb
| Zn 67 4409.4 ppb
| Zn 68 1819.5 ppb
| As 75 -871.1 ppb
| Se 77 4325 ppb
| Se 82 21.2 ppb
| Sr 88 217 ppb
| Mo 95 95.3 ppb
| Mo 97 70.3 ppb
| Mo 98 139.8 ppb
|> Rh 103 555654.3 ppb
| Cd 111 14.9 ppb
|- Cd 114 28.1 ppb
|- Sb 121 260.3 ppb
| Sb 123 202.8 ppb
| Ba 135 125.7 ppb
| Ba 137 225.3 ppb
|> Ho 165 891039.1 ppb
| Tl 205 141.3 ppb
| Pb 206 180 ppb
| Pb 207 162.3 ppb
|- Pb 208 726 ppb
Kr 83 51.2 ppb
ICP-Data 3 of 23
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e 24127-Metals 46.3
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 1
Sample DatFriday, February 27, 2015 09:47:15
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 38533.8 ppb
| Be 9 310.3 1 ppb
| B 10 371.3 5.79551 ppb
|- B 11 1577.5 5.57964 ppb
|- Mg 24 64306.9 21 ppb
| Mg 25 9335.8 21 ppb
| Al 27 5816.2 1 ppb
| K 39 627107.1 21 ppb
| Ca 44 33949.6 21 ppb
| Sc 45 247610.4 ppb
| Cr 52 18969.8 1 ppb
| Cr 53 52858.4 1 ppb
| Fe 54 44379.1 21 ppb
| Mn 55 15823.8 1 ppb
| Fe 57 11396.1 21 ppb
| Co 59 12180.8 1 ppb
| Ni 60 2667.1 1 ppb
| Cu 63 6681.8 1 ppb
| Cu 65 3301.6 1 ppb
| Zn 66 2261.9 1 ppb
| Zn 67 5284.5 1 ppb
| Zn 68 3119.9 1 ppb
| As 75 978 1 ppb
| Se 77 4607.5 1 ppb
| Se 82 228.1 1 ppb
| Sr 88 29660 1.04828 ppb
| Mo 95 4426.4 1 ppb
| Mo 97 2731.1 1 ppb
| Mo 98 6978.8 1 ppb
|> Rh 103 558646.6 ppb
| Cd 111 2669.8 1 ppb
|- Cd 114 6114.6 1 ppb
|- Sb 121 9631.1 1 ppb
| Sb 123 7220.9 1 ppb
| Ba 135 2816.4 1 ppb
| Ba 137 4925.7 1 ppb
|> Ho 165 891720.1 ppb
| Tl 205 26553.4 1 ppb
| Pb 206 8731.2 1.05792 ppb
| Pb 207 7739.6 1.0769 ppb
|- Pb 208 35094.9 1.07128 ppb
Kr 83 -139.5 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 2
Sample DatFriday, February 27, 2015 09:50:27
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 37510.4 ppb
| Be 9 28112.8 99.9994 ppb
| B 10 6116.4 111.2785 ppb
|- B 11 27302.9 111.8951 ppb
|- Mg 24 3100899.3 1099.973 ppb
| Mg 25 474443 1099.994 ppb
| Al 27 470181.1 99.99997 ppb
| K 39 9670812 1099.991 ppb
| Ca 44 371549.2 1099.986 ppb
| Sc 45 248490.9 ppb
| Cr 52 922945.3 99.99974 ppb
| Cr 53 161663.4 99.95757 ppb
| Fe 54 864126.3 1100.005 ppb
| Mn 55 1486951.6 100.0002 ppb
| Fe 57 339687.1 1099.986 ppb
| Co 59 1183391.9 99.99983 ppb
| Ni 60 257661.7 100.0001 ppb
| Cu 63 597455.7 99.99999 ppb
| Cu 65 296602 100.0003 ppb
| Zn 66 170097.7 100.0003 ppb
| Zn 67 33795 99.98098 ppb
| Zn 68 128855.2 99.99986 ppb
| As 75 208588 100.0012 ppb
| Se 77 19987 99.99337 ppb
| Se 82 21650.4 100.0005 ppb
| Sr 88 2754472.7 98.50381 ppb
| Mo 95 432762.2 100 ppb
| Mo 97 268237.3 100.0001 ppb
| Mo 98 691161.6 100.0001 ppb
|> Rh 103 556612.1 ppb
| Cd 111 263260.2 99.99995 ppb
|- Cd 114 617311.4 100.0002 ppb
|- Sb 121 953970.8 100.0001 ppb
| Sb 123 725338.6 100.0002 ppb
| Ba 135 271480 100 ppb
| Ba 137 472845.7 99.99997 ppb
|> Ho 165 898833.1 ppb
| Tl 205 2379702.9 99.99881 ppb
| Pb 206 860651.6 105.6901 ppb
| Pb 207 754382 106.4026 ppb
|- Pb 208 3434130.8 106.1985 ppb
Kr 83 -18614.7 ppb
ICP-Data 4 of 23
elementOne
e 24127-Metals 46.4
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 3
Sample DatFriday, February 27, 2015 09:53:40
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 36508.6 ppb
| Be 9 134836.6 499.7192 ppb
| B 10 26589.5 497.8238 ppb
|- B 11 120292.3 498.0995 ppb
|- Mg 24 14856017 5493.549 ppb
| Mg 25 2145286.5 5480.644 ppb
| Al 27 2141791.1 498.4217 ppb
| K 39 45756432 5498.869 ppb
| Ca 44 1683206.2 5494.217 ppb
| Sc 45 246044.4 ppb
| Cr 52 4169384.9 498.3815 ppb
| Cr 53 572652.8 498.4816 ppb
| Fe 54 3761328.1 5477.735 ppb
| Mn 55 6801884.2 498.4856 ppb
| Fe 57 1608419.9 5493.291 ppb
| Co 59 5471193.5 498.6907 ppb
| Ni 60 1233383.2 499.3912 ppb
| Cu 63 2722386.2 498.4066 ppb
| Cu 65 1414812 499.3384 ppb
| Zn 66 804628.5 499.2107 ppb
| Zn 67 140670.5 498.758 ppb
| Zn 68 613376.4 499.499 ppb
| As 75 1017069.1 499.6855 ppb
| Se 77 80189.5 499.6421 ppb
| Se 82 102580.3 499.1984 ppb
| Sr 88 13661563 500.0805 ppb
| Mo 95 2049538.9 499.1813 ppb
| Mo 97 1316732 499.8857 ppb
| Mo 98 3232886.8 498.929 ppb
|> Rh 103 549976 ppb
| Cd 111 1268283 499.5164 ppb
|- Cd 114 2803137.2 498.326 ppb
|- Sb 121 4467581.5 498.6918 ppb
| Sb 123 3388302.7 498.6411 ppb
| Ba 135 1325148.1 499.5223 ppb
| Ba 137 2192254 498.4865 ppb
|> Ho 165 899628.9 ppb
| Tl 205 11725108 499.7023 ppb
| Pb 206 3883580.4 497.9214 ppb
| Pb 207 3397159.8 497.8777 ppb
|- Pb 208 15436799 497.8359 ppb
Kr 83 -92557.1 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatFriday, February 27, 2015 09:56:52
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 36735.9 ppb
| Be 9 11 0.02565 ppb
| B 10 563 9.66973 ppb
|- B 11 2471 9.44676 ppb
|- Mg 24 1773.6 0.36304 ppb
| Mg 25 255.3 0.36388 ppb
| Al 27 997.7 -0.01634 ppb
| K 39 449216.3 1.67276 ppb
| Ca 44 29491.8 10.08869 ppb
| Sc 45 237812.1 ppb
| Cr 52 9498 0.02033 ppb
| Cr 53 54586.6 8.44992 ppb
| Fe 54 28161.2 0.39194 ppb
| Mn 55 1641.8 0.03814 ppb
| Fe 57 5198.2 1.90686 ppb
| Co 59 492.7 0.03659 ppb
| Ni 60 148 0.0218 ppb
| Cu 63 1046.7 0.07001 ppb
| Cu 65 588.4 0.0636 ppb
| Zn 66 459.7 -0.08711 ppb
| Zn 67 5538.7 4.47405 ppb
| Zn 68 1726.2 -0.04819 ppb
| As 75 -713 0.06997 ppb
| Se 77 3805.1 -2.90614 ppb
| Se 82 38.5 0.08675 ppb
| Sr 88 1032.1 0.03043 ppb
| Mo 95 1225.4 0.27876 ppb
| Mo 97 749 0.26116 ppb
| Mo 98 1888.5 0.27335 ppb
|> Rh 103 545100.5 ppb
| Cd 111 96.7 0.03275 ppb
|- Cd 114 216.1 0.03403 ppb
|- Sb 121 481.3 0.0262 ppb
| Sb 123 370.6 0.02626 ppb
| Ba 135 198.7 0.02966 ppb
| Ba 137 343.3 0.02902 ppb
|> Ho 165 867821.5 ppb
| Tl 205 833.4 0.0306 ppb
| Pb 206 440.7 0.0351 ppb
| Pb 207 383.3 0.03404 ppb
|- Pb 208 1708.7 0.03333 ppb
Kr 83 50.3 ppb
ICP-Data 5 of 23
elementOne
e 24127-Metals 46.5
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 2
Sample DatFriday, February 27, 2015 10:00:05
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 38630.4 ppb
| Be 9 404.3 1.40166 ppb
| B 10 329.3 4.99879 ppb
|- B 11 1460.1 4.97202 ppb
|- Mg 24 63367.8 22.34062 ppb
| Mg 25 9211.3 22.44303 ppb
| Al 27 7683.2 1.47776 ppb
| K 39 632855.8 20.89645 ppb
| Ca 44 35384.7 24.8583 ppb
| Sc 45 254347.6 ppb
| Cr 52 22356.1 1.46047 ppb
| Cr 53 56547.2 8.08801 ppb
| Fe 54 44271.9 21.48834 ppb
| Mn 55 21929.4 1.46975 ppb
| Fe 57 11420.2 21.74135 ppb
| Co 59 17199.6 1.50625 ppb
| Ni 60 3675.1 1.39929 ppb
| Cu 63 9323.8 1.52666 ppb
| Cu 65 4748.6 1.47387 ppb
| Zn 66 3023.2 1.43842 ppb
| Zn 67 6044 5.40993 ppb
| Zn 68 3668.7 1.42647 ppb
| As 75 1937.2 1.3418 ppb
| Se 77 4117.3 -1.96796 ppb
| Se 82 267.7 1.15769 ppb
| Sr 88 43682.1 1.53694 ppb
| Mo 95 6177.4 1.43108 ppb
| Mo 97 3907.8 1.40771 ppb
| Mo 98 9966.1 1.46482 ppb
|> Rh 103 569017 ppb
| Cd 111 3853.8 1.46139 ppb
|- Cd 114 8954.1 1.53295 ppb
|- Sb 121 12121.4 1.31302 ppb
| Sb 123 9212.9 1.31509 ppb
| Ba 135 3752.1 1.35603 ppb
| Ba 137 6717.5 1.46415 ppb
|> Ho 165 906961.7 ppb
| Tl 205 35924.6 1.51226 ppb
| Pb 206 11940.2 1.49521 ppb
| Pb 207 10306.2 1.47439 ppb
|- Pb 208 47244 1.48813 ppb
Kr 83 -228.2 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 3
Sample DatFriday, February 27, 2015 10:03:17
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 37344.9 ppb
| Be 9 68665.4 248.7564 ppb
| B 10 15045.8 274.9918 ppb
|- B 11 67177.9 271.4862 ppb
|- Mg 24 6712270.8 2515.51 ppb
| Mg 25 1001756.4 2593.642 ppb
| Al 27 1116459.4 263.1652 ppb
| K 39 20798534 2504.338 ppb
| Ca 44 773591.1 2512.407 ppb
| Sc 45 245669.8 ppb
| Cr 52 2147030.5 259.5708 ppb
| Cr 53 315389.4 259.0709 ppb
| Fe 54 1838804.5 2694.163 ppb
| Mn 55 3449700.5 256.2446 ppb
| Fe 57 736554.3 2541.579 ppb
| Co 59 2771115.5 256.0633 ppb
| Ni 60 615772.3 252.7661 ppb
| Cu 63 1497931.7 277.9648 ppb
| Cu 65 745986.5 266.7913 ppb
| Zn 66 409896.7 257.51 ppb
| Zn 67 73576.7 256.9225 ppb
| Zn 68 309776.8 255.0324 ppb
| As 75 513198 255.8064 ppb
| Se 77 42897 258.151 ppb
| Se 82 52475.3 258.8264 ppb
| Sr 88 6902487.8 256.0937 ppb
| Mo 95 1055742.6 260.5974 ppb
| Mo 97 660727.3 254.2401 ppb
| Mo 98 1704049.3 266.4993 ppb
|> Rh 103 542606.2 ppb
| Cd 111 635499.2 253.6926 ppb
|- Cd 114 1484093 267.3346 ppb
|- Sb 121 2241734 255.9305 ppb
| Sb 123 1792863.3 269.8082 ppb
| Ba 135 659383.7 254.2553 ppb
| Ba 137 1148264.5 267.0458 ppb
|> Ho 165 879293.4 ppb
| Tl 205 5965063.9 260.0401 ppb
| Pb 206 1990862.1 261.208 ppb
| Pb 207 1803943.7 270.4054 ppb
|- Pb 208 7891857.1 260.3781 ppb
Kr 83 -46733.4 ppb
ICP-Data 6 of 23
elementOne
e 24127-Metals 46.6
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatFriday, February 27, 2015 10:06:30
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 37278.1 ppb
| Be 9 28053.6 101.8052 ppb
| B 10 6388.6 116.4617 ppb
|- B 11 28881.8 116.5112 ppb
|- Mg 24 3119619.6 1149.233 ppb
| Mg 25 461349.8 1174.517 ppb
| Al 27 456474.8 105.687 ppb
| K 39 9732087.9 1123.383 ppb
| Ca 44 365648.7 1120.49 ppb
| Sc 45 242763.5 ppb
| Cr 52 907681.9 107.2815 ppb
| Cr 53 161388.8 108.7109 ppb
| Fe 54 857502.6 1212.934 ppb
| Mn 55 1479948.4 108.0429 ppb
| Fe 57 336913.1 1134.421 ppb
| Co 59 1180648.7 107.2464 ppb
| Ni 60 255139.8 102.9355 ppb
| Cu 63 594657.1 108.433 ppb
| Cu 65 295776.1 103.949 ppb
| Zn 66 168786.3 104.0639 ppb
| Zn 67 33731.5 107.0809 ppb
| Zn 68 128282.6 102.9861 ppb
| As 75 206901.2 101.6779 ppb
| Se 77 19862.4 102.1362 ppb
| Se 82 21696.1 105.1798 ppb
| Sr 88 2829782 103.2365 ppb
| Mo 95 433721 105.2628 ppb
| Mo 97 268214.8 101.4688 ppb
| Mo 98 692118.3 106.4569 ppb
|> Rh 103 551684.1 ppb
| Cd 111 262875.3 103.1944 ppb
|- Cd 114 615085.1 108.9558 ppb
|- Sb 121 949835.6 107.4019 ppb
| Sb 123 724999.5 108.0741 ppb
| Ba 135 270632 103.3416 ppb
| Ba 137 470725.1 108.4228 ppb
|> Ho 165 887586.7 ppb
| Tl 205 2441109.6 105.4188 ppb
| Pb 206 849455.1 110.343 ppb
| Pb 207 744727.6 110.5735 ppb
|- Pb 208 3394773.8 110.9194 ppb
Kr 83 -19123.1 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 5
Sample DatFriday, February 27, 2015 10:09:43
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 38459.9 ppb
| Be 9 14132.3 49.70422 ppb
| B 10 4255.3 74.88962 ppb
|- B 11 19019.9 74.11134 ppb
|- Mg 24 737707.2 271.2665 ppb
| Mg 25 104937.4 266.5338 ppb
| Al 27 252162.3 58.20178 ppb
| K 39 2171139.7 208.9708 ppb
| Ca 44 105931.7 261.2625 ppb
| Sc 45 247017.5 ppb
| Cr 52 468455.9 54.74039 ppb
| Cr 53 109280 59.35241 ppb
| Fe 54 227532.8 290.9911 ppb
| Mn 55 744028.4 54.19175 ppb
| Fe 57 81512 261.914 ppb
| Co 59 589656 53.49522 ppb
| Ni 60 127082.1 51.1925 ppb
| Cu 63 306840.6 55.81357 ppb
| Cu 65 152336.7 53.39492 ppb
| Zn 66 84825.5 52.04341 ppb
| Zn 67 19817.9 56.22623 ppb
| Zn 68 65294.7 51.6217 ppb
| As 75 104413 51.45282 ppb
| Se 77 11824.4 49.32288 ppb
| Se 82 10566.7 51.09324 ppb
| Sr 88 634.7 0.01523 ppb
| Mo 95 216146.5 52.38768 ppb
| Mo 97 134690.6 50.87537 ppb
| Mo 98 347648.1 53.38894 ppb
|> Rh 103 552347.1 ppb
| Cd 111 130986.1 51.34845 ppb
|- Cd 114 308323.4 54.54214 ppb
|- Sb 121 483880.6 54.4894 ppb
| Sb 123 367576.9 54.56393 ppb
| Ba 135 134420.4 51.1057 ppb
| Ba 137 234462.5 53.77109 ppb
|> Ho 165 891369.3 ppb
| Tl 205 1258355.8 54.12524 ppb
| Pb 206 430584.3 55.69398 ppb
| Pb 207 373404.6 55.20251 ppb
|- Pb 208 1706571 55.52059 ppb
Kr 83 57.4 ppb
ICP-Data 7 of 23
elementOne
e 24127-Metals 46.7
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 9
Sample DatFriday, February 27, 2015 10:12:56
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 38736.8 ppb
| Be 9 3.7 -0.00238 ppb
| B 10 352.7 5.38817 ppb
|- B 11 1636.8 5.64338 ppb
|- Mg 24 6226.8 2.10283 ppb
| Mg 25 908.4 2.12954 ppb
| Al 27 16100.3 3.66449 ppb
| K 39 458820.8 4.8799 ppb
| Ca 44 42411.7 58.46305 ppb
| Sc 45 238477.4 ppb
| Cr 52 13426.9 0.55511 ppb
| Cr 53 106266.2 61.69352 ppb
| Fe 54 34081.4 10.99609 ppb
| Mn 55 3086.2 0.15298 ppb
| Fe 57 5686.1 4.303 ppb
| Co 59 2966.2 0.27343 ppb
| Ni 60 220.7 0.05446 ppb
| Cu 63 2050.9 0.26876 ppb
| Cu 65 1093.7 0.25705 ppb
| Zn 66 7706.3 4.62534 ppb
| Zn 67 12244 30.96058 ppb
| Zn 68 7351.6 4.80685 ppb
| As 75 -1543.8 -0.36665 ppb
| Se 77 9070.9 34.29206 ppb
| Se 82 23.1 0.0143 ppb
| Sr 88 1744.8 0.05887 ppb
| Mo 95 322.7 0.0589 ppb
| Mo 97 212.7 0.05802 ppb
| Mo 98 565.8 0.06977 ppb
|> Rh 103 526432.4 ppb
| Cd 111 20.1 0.00243 ppb
|- Cd 114 48.9 0.00408 ppb
|- Sb 121 737 0.0577 ppb
| Sb 123 549.9 0.0554 ppb
| Ba 135 189.7 0.0277 ppb
| Ba 137 359.7 0.03464 ppb
|> Ho 165 851313 ppb
| Tl 205 210.7 0.00337 ppb
| Pb 206 368.3 0.02656 ppb
| Pb 207 322.3 0.02583 ppb
|- Pb 208 1417.7 0.02462 ppb
Kr 83 55.5 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 10
Sample DatFriday, February 27, 2015 10:16:09
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 38013.2 ppb
| Be 9 14371 51.13453 ppb
| B 10 4055.2 72.18928 ppb
|- B 11 18286.4 72.0704 ppb
|- Mg 24 1603098.1 624.7912 ppb
| Mg 25 232711.2 626.6101 ppb
| Al 27 353016.8 86.42942 ppb
| K 39 4726918.8 551.4936 ppb
| Ca 44 216545 668.9965 ppb
| Sc 45 241927.6 ppb
| Cr 52 476088.1 59.02786 ppb
| Cr 53 170932.3 127.1665 ppb
| Fe 54 451465.8 657.3549 ppb
| Mn 55 751157.3 57.97678 ppb
| Fe 57 174054.8 612.8307 ppb
| Co 59 605907.6 58.23841 ppb
| Ni 60 128921.5 55.02323 ppb
| Cu 63 313356.9 60.40227 ppb
| Cu 65 156369.2 58.08516 ppb
| Zn 66 104605.4 68.11271 ppb
| Zn 67 29755 98.90394 ppb
| Zn 68 80726.6 68.07228 ppb
| As 75 105064.9 54.82624 ppb
| Se 77 17462.1 93.0736 ppb
| Se 82 10725.4 54.97472 ppb
| Sr 88 1453646.2 56.1078 ppb
| Mo 95 217310.2 55.78607 ppb
| Mo 97 136324.8 54.54212 ppb
| Mo 98 351213.3 57.14721 ppb
|> Rh 103 521383.6 ppb
| Cd 111 129027.9 53.58932 ppb
|- Cd 114 302836.8 56.75922 ppb
|- Sb 121 478250.9 55.52056 ppb
| Sb 123 362761.1 55.51813 ppb
| Ba 135 133851.4 52.4557 ppb
| Ba 137 234454.3 55.4418 ppb
|> Ho 165 864651.1 ppb
| Tl 205 1273418.2 56.4692 ppb
| Pb 206 437689 58.37349 ppb
| Pb 207 376144 57.34289 ppb
|- Pb 208 1725767.9 57.89761 ppb
Kr 83 -9779.2 ppb
ICP-Data 8 of 23
elementOne
e 24127-Metals 46.8
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC STD 2
Sample DatFriday, February 27, 2015 10:19:22
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 39262.6 ppb
| Be 9 413 1.40826 ppb
| B 10 285.7 4.14253 ppb
|- B 11 1234.8 4.01139 ppb
|- Mg 24 62584.8 22.38435 ppb
| Mg 25 8997.8 22.23878 ppb
| Al 27 7863.4 1.54372 ppb
| K 39 625302.9 21.09099 ppb
| Ca 44 34779.1 24.53828 ppb
| Sc 45 249341.7 ppb
| Cr 52 22510.2 1.51665 ppb
| Cr 53 66802.7 18.34156 ppb
| Fe 54 44543.5 22.79687 ppb
| Mn 55 22130.6 1.50717 ppb
| Fe 57 11541.7 22.71133 ppb
| Co 59 16977.8 1.50833 ppb
| Ni 60 3728.4 1.44167 ppb
| Cu 63 9249.4 1.5371 ppb
| Cu 65 4681.2 1.47417 ppb
| Zn 66 2990.8 1.44539 ppb
| Zn 67 7235.5 9.98669 ppb
| Zn 68 3702.1 1.49509 ppb
| As 75 1752 1.26523 ppb
| Se 77 4378.1 0.08154 ppb
| Se 82 274.1 1.20666 ppb
| Sr 88 42999.1 1.53552 ppb
| Mo 95 6113.1 1.43677 ppb
| Mo 97 3859.8 1.41056 ppb
| Mo 98 9808 1.46293 ppb
|> Rh 103 560762.5 ppb
| Cd 111 3750 1.44282 ppb
|- Cd 114 8940.3 1.55299 ppb
|- Sb 121 12049.3 1.31563 ppb
| Sb 123 9123.8 1.31232 ppb
| Ba 135 3879.2 1.41471 ppb
| Ba 137 6521.7 1.43093 ppb
|> Ho 165 899743.9 ppb
| Tl 205 35889.7 1.52318 ppb
| Pb 206 11787.6 1.48788 ppb
| Pb 207 10255.8 1.47906 ppb
|- Pb 208 47107.9 1.49556 ppb
Kr 83 -223.2 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24127-1.1
Sample DatFriday, February 27, 2015 10:22:35
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 37064.2 ppb
| Be 9 13.3 0.03344 ppb
| B 10 1253.1 22.30678 ppb
|- B 11 5803.5 22.95861 ppb
|- Mg 24 4153919.6 1446.247 ppb
| Mg 25 620335.5 1492.393 ppb
| Al 27 842405.5 184.506 ppb
| K 39 12676461 1395.439 ppb
| Ca 44 3328723.3 10311.38 ppb
| Sc 45 273051.7 ppb
| Cr 52 10322.9 0.03722 ppb
| Cr 53 25447.3 -21.04 ppb
| Fe 54 44560.6 20.30181 ppb
| Mn 55 267745.3 18.39955 ppb
| Fe 57 10528.8 17.91388 ppb
| Co 59 2971.5 0.2462 ppb
| Ni 60 515.7 0.15768 ppb
| Cu 63 8214 1.29352 ppb
| Cu 65 4086.6 1.21296 ppb
| Zn 66 11758.6 6.5004 ppb
| Zn 67 5413 2.66374 ppb
| Zn 68 11252 7.18515 ppb
| As 75 18.2 0.43127 ppb
| Se 77 821 -23.09153 ppb
| Se 82 63.4 0.18751 ppb
| Sr 88 775267.6 26.72031 ppb
| Mo 95 960.1 0.19738 ppb
| Mo 97 576.7 0.17977 ppb
| Mo 98 1514.9 0.19887 ppb
|> Rh 103 583737.5 ppb
| Cd 111 147 0.04872 ppb
|- Cd 114 232.3 0.03394 ppb
|- Sb 121 796 0.0542 ppb
| Sb 123 593.3 0.05214 ppb
| Ba 135 84298.7 29.85321 ppb
| Ba 137 147552.7 31.51714 ppb
|> Ho 165 956157.7 ppb
| Tl 205 450 0.01196 ppb
| Pb 206 1239.8 0.12622 ppb
| Pb 207 1042.7 0.11984 ppb
|- Pb 208 4854.5 0.12374 ppb
Kr 83 -5185.8 ppb
ICP-Data 9 of 23
elementOne
e 24127-Metals 46.9
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24127-1.1
Sample DatFriday, February 27, 2015 10:25:47
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 37814.1 ppb
| Be 9 14702.5 52.59929 ppb
| B 10 5101.1 91.52392 ppb
|- B 11 23348.3 92.72501 ppb
|- Mg 24 5983277.1 2078.403 ppb
| Mg 25 877421.9 2105.246 ppb
| Al 27 1116060.1 243.9194 ppb
| K 39 17707483 1965.119 ppb
| Ca 44 3580037.8 11068.81 ppb
| Sc 45 273256.1 ppb
| Cr 52 509389.5 56.20021 ppb
| Cr 53 75959.7 23.8796 ppb
| Fe 54 498484.1 646.0465 ppb
| Mn 55 1095228.6 75.33989 ppb
| Fe 57 190406.6 596.8888 ppb
| Co 59 648792.2 55.55912 ppb
| Ni 60 141249.6 53.69699 ppb
| Cu 63 332525 57.08935 ppb
| Cu 65 164017.9 54.26528 ppb
| Zn 66 94673.2 54.85423 ppb
| Zn 67 18470.8 47.51142 ppb
| Zn 68 74296.6 55.53915 ppb
| As 75 112446.1 52.27974 ppb
| Se 77 8914.4 26.96565 ppb
| Se 82 11179.8 51.02274 ppb
| Sr 88 2302831.1 79.20871 ppb
| Mo 95 243449.2 55.68963 ppb
| Mo 97 150292.8 53.58867 ppb
| Mo 98 387947.4 56.23523 ppb
|> Rh 103 585285.8 ppb
| Cd 111 139077 51.46341 ppb
|- Cd 114 327268.2 54.64639 ppb
|- Sb 121 519444.6 54.11583 ppb
| Sb 123 395790.9 54.3566 ppb
| Ba 135 232393.1 81.78713 ppb
| Ba 137 405009.9 85.95188 ppb
|> Ho 165 963578.4 ppb
| Tl 205 1322463 52.63714 ppb
| Pb 206 451356.2 54.02546 ppb
| Pb 207 389379.5 53.26867 ppb
|- Pb 208 1787759 53.82193 ppb
Kr 83 -15563.8 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24127-1.1
Sample DatFriday, February 27, 2015 10:45:16
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 36542 ppb
| Be 9 5.3 0.00461 ppb
| B 10 511.7 8.74257 ppb
|- B 11 2373 9.08448 ppb
|- Mg 24 864989.6 308.192 ppb
| Mg 25 121791 299.7879 ppb
| Al 27 168146.1 37.51125 ppb
| K 39 2954967.5 292.4893 ppb
| Ca 44 749852.8 2310.357 ppb
| Sc 45 238512.9 ppb
| Cr 52 10446.3 0.07943 ppb
| Cr 53 32838.2 -13.73887 ppb
| Fe 54 38121.4 12.6775 ppb
| Mn 55 57027.6 3.94882 ppb
| Fe 57 6051.7 3.94592 ppb
| Co 59 2306 0.19386 ppb
| Ni 60 283 0.07173 ppb
| Cu 63 2296.3 0.28192 ppb
| Cu 65 1210.1 0.26582 ppb
| Zn 66 3753.1 1.87258 ppb
| Zn 67 4339 -0.6683 ppb
| Zn 68 4460.1 2.04318 ppb
| As 75 -161.6 0.34656 ppb
| Se 77 1112.7 -21.11729 ppb
| Se 82 29.1 0.0349 ppb
| Sr 88 155923.3 5.49754 ppb
| Mo 95 247 0.03505 ppb
| Mo 97 172.3 0.03667 ppb
| Mo 98 377.4 0.03488 ppb
|> Rh 103 570036 ppb
| Cd 111 38.7 0.00886 ppb
|- Cd 114 66.1 0.00643 ppb
|- Sb 121 3897.8 0.38681 ppb
| Sb 123 2965.7 0.38711 ppb
| Ba 135 17322.5 6.20613 ppb
| Ba 137 29966 6.47413 ppb
|> Ho 165 939597.2 ppb
| Tl 205 158 0.00038 ppb
| Pb 206 488.3 0.03662 ppb
| Pb 207 408.7 0.03335 ppb
|- Pb 208 1905.7 0.03522 ppb
Kr 83 -996.6 ppb
ICP-Data 10 of 23
elementOne
e 24127-Metals 46.10
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24127-1.1
Sample DatFriday, February 27, 2015 10:48:29
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 36152.8 ppb
| Be 9 13979.4 52.29989 ppb
| B 10 4314 80.84378 ppb
|- B 11 19512.6 80.94798 ppb
|- Mg 24 1680081.1 597.6893 ppb
| Mg 25 244143.5 599.9765 ppb
| Al 27 446051 99.72053 ppb
| K 39 4910096.3 520.2993 ppb
| Ca 44 827516.2 2553.93 ppb
| Sc 45 258290.4 ppb
| Cr 52 500720.6 56.6174 ppb
| Cr 53 79044.7 28.35064 ppb
| Fe 54 252898 315.9745 ppb
| Mn 55 862200.6 60.75188 ppb
| Fe 57 88959.5 277.3021 ppb
| Co 59 632803.1 55.51551 ppb
| Ni 60 134443.3 52.3778 ppb
| Cu 63 318803.7 56.08543 ppb
| Cu 65 158894.8 53.85739 ppb
| Zn 66 89827.9 53.31239 ppb
| Zn 67 17734 46.47911 ppb
| Zn 68 70032.5 53.60492 ppb
| As 75 110370.6 52.58501 ppb
| Se 77 8971.4 28.6613 ppb
| Se 82 10990.2 51.41285 ppb
| Sr 88 154819.2 5.44737 ppb
| Mo 95 233156.2 54.63924 ppb
| Mo 97 144939.7 52.9338 ppb
| Mo 98 375171.4 55.70667 ppb
|> Rh 103 571287.7 ppb
| Cd 111 136003.4 51.57402 ppb
|- Cd 114 322272.7 55.14125 ppb
|- Sb 121 506351.5 54.09351 ppb
| Sb 123 388533.7 54.70477 ppb
| Ba 135 160368.9 57.83066 ppb
| Ba 137 278201.3 60.5248 ppb
|> Ho 165 939645.9 ppb
| Tl 205 1312373.3 53.53996 ppb
| Pb 206 452050 55.46143 ppb
| Pb 207 387021.6 54.27796 ppb
|- Pb 208 1781486.9 54.98073 ppb
Kr 83 -989.8 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatFriday, February 27, 2015 10:51:42
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 39193.2 ppb
| Be 9 5.7 0.00435 ppb
| B 10 271.7 3.89923 ppb
|- B 11 1205.7 3.90374 ppb
|- Mg 24 1582.8 0.28917 ppb
| Mg 25 236 0.31196 ppb
| Al 27 1567.1 0.11729 ppb
| K 39 423345.9 -1.44315 ppb
| Ca 44 29357.7 9.75351 ppb
| Sc 45 236542.8 ppb
| Cr 52 11536.3 0.26785 ppb
| Cr 53 51862.5 5.96107 ppb
| Fe 54 29265.7 2.05909 ppb
| Mn 55 1432.8 0.02247 ppb
| Fe 57 4667.5 0.08298 ppb
| Co 59 241 0.01323 ppb
| Ni 60 93 -0.00084 ppb
| Cu 63 485.3 -0.03397 ppb
| Cu 65 295.7 -0.04081 ppb
| Zn 66 465.3 -0.08372 ppb
| Zn 67 4257.3 -0.2141 ppb
| Zn 68 1707.2 -0.0621 ppb
| As 75 -912.8 -0.03274 ppb
| Se 77 6271.2 13.51558 ppb
| Se 82 22.5 0.00828 ppb
| Sr 88 609.4 0.01466 ppb
| Mo 95 209.7 0.02853 ppb
| Mo 97 133.3 0.02457 ppb
| Mo 98 323.5 0.02898 ppb
|> Rh 103 544783.8 ppb
| Cd 111 54 0.01568 ppb
|- Cd 114 105.2 0.01399 ppb
|- Sb 121 1638.8 0.15436 ppb
| Sb 123 1285.9 0.16 ppb
| Ba 135 155.7 0.01095 ppb
| Ba 137 256 0.00663 ppb
|> Ho 165 896848.4 ppb
| Tl 205 426.3 0.01208 ppb
| Pb 206 266.7 0.01088 ppb
| Pb 207 232 0.00996 ppb
|- Pb 208 1082.7 0.0113 ppb
Kr 83 49.2 ppb
ICP-Data 11 of 23
elementOne
e 24127-Metals 46.11
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatFriday, February 27, 2015 10:54:55
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 39176.9 ppb
| Be 9 27568.4 95.19391 ppb
| B 10 6073 105.2855 ppb
|- B 11 27591.1 105.8635 ppb
|- Mg 24 3023255.5 1122.157 ppb
| Mg 25 451009.2 1156.623 ppb
| Al 27 449452.6 104.8447 ppb
| K 39 9714576.6 1130.376 ppb
| Ca 44 369314.8 1141.606 ppb
| Sc 45 241784.9 ppb
| Cr 52 903945.6 107.6324 ppb
| Cr 53 164248.6 112.5593 ppb
| Fe 54 852512.5 1215.06 ppb
| Mn 55 1489807.5 109.5472 ppb
| Fe 57 338282.7 1147.538 ppb
| Co 59 1157667.4 105.9578 ppb
| Ni 60 251665.8 102.2867 ppb
| Cu 63 581713.9 106.8598 ppb
| Cu 65 288545.5 102.1537 ppb
| Zn 66 164789.9 102.3729 ppb
| Zn 67 32559.5 103.705 ppb
| Zn 68 125567.7 101.5297 ppb
| As 75 204859.3 101.4 ppb
| Se 77 20964.2 110.3462 ppb
| Se 82 21233.7 103.7073 ppb
| Sr 88 2789789.3 102.5708 ppb
| Mo 95 424826.5 103.8945 ppb
| Mo 97 265973.2 101.3732 ppb
| Mo 98 682091.9 105.6837 ppb
|> Rh 103 547586.3 ppb
| Cd 111 261236.6 103.3198 ppb
|- Cd 114 613613.7 109.5279 ppb
|- Sb 121 955605.5 105.733 ppb
| Sb 123 729143.9 106.3377 ppb
| Ba 135 270150.7 100.9167 ppb
| Ba 137 470645.1 106.0553 ppb
|> Ho 165 907519.1 ppb
| Tl 205 2515978.3 106.2665 ppb
| Pb 206 891849.4 113.2873 ppb
| Pb 207 783796.3 113.8252 ppb
|- Pb 208 3563950.2 113.9036 ppb
Kr 83 -18846.2 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: Blank
Sample DatFriday, February 27, 2015 11:28:45
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 39808.5 ppb
| Be 9 ppb
| B 10 182.3 ppb
|- B 11 819.4 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 210150.8 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 313.3 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 538507 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 893034.8 ppb
| Tl 205 ppb
| Pb 206 166.3 ppb
| Pb 207 148 ppb
|- Pb 208 665.7 ppb
Kr 83 59.2 ppb
ICP-Data 12 of 23
elementOne
e 24127-Metals 46.12
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 1
Sample DatFriday, February 27, 2015 11:30:02
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 40767.4 ppb
| Be 9 ppb
| B 10 480.7 4.94031 ppb
|- B 11 2056.6 4.53199 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 237756.3 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 29062.1 1.05357 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 549122.3 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 910997.2 ppb
| Tl 205 ppb
| Pb 206 9201 1.14299 ppb
| Pb 207 8103.6 1.15043 ppb
|- Pb 208 36891.4 1.1529 ppb
Kr 83 -141.1 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 2
Sample DatFriday, February 27, 2015 11:31:20
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 40066.3 ppb
| Be 9 ppb
| B 10 6291.5 104.6431 ppb
|- B 11 28365.6 104.3575 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 232174.2 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 2754343 101.425 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 546125.3 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 922235.9 ppb
| Tl 205 ppb
| Pb 206 909102.3 113.4927 ppb
| Pb 207 788784.5 112.5961 ppb
|- Pb 208 3571205 112.2336 ppb
Kr 83 -18612.9 ppb
ICP-Data 13 of 23
elementOne
e 24127-Metals 46.13
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 3
Sample DatFriday, February 27, 2015 11:32:38
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 39885.5 ppb
| Be 9 ppb
| B 10 29076.6 498.9892 ppb
|- B 11 129103.9 498.6707 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 247885.5 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 13547983 499.9374 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 539069 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 930401 ppb
| Tl 205 ppb
| Pb 206 4204017.6 498.2669 ppb
| Pb 207 3660070.4 498.3366 ppb
|- Pb 208 16697024 498.4886 ppb
Kr 83 -91759.2 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatFriday, February 27, 2015 11:33:56
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 39985.8 ppb
| Be 9 ppb
| B 10 380.7 3.4099 ppb
|- B 11 1705.2 3.43608 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 215389.6 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 2561.8 0.08295 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 546312.7 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 912296 ppb
| Tl 205 ppb
| Pb 206 888 0.08821 ppb
| Pb 207 756 0.08539 ppb
|- Pb 208 3464.3 0.08618 ppb
Kr 83 53.3 ppb
ICP-Data 14 of 23
elementOne
e 24127-Metals 46.14
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 2
Sample DatFriday, February 27, 2015 11:35:15
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 41447.6 ppb
| Be 9 ppb
| B 10 289 1.65011 ppb
|- B 11 1258.8 1.52612 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 250949.7 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 43750.6 1.5109 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 571704.1 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 950864.1 ppb
| Tl 205 ppb
| Pb 206 12767.3 1.46245 ppb
| Pb 207 11259.6 1.48174 ppb
|- Pb 208 50914.3 1.46954 ppb
Kr 83 -238.3 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 3
Sample DatFriday, February 27, 2015 11:36:32
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 39092.2 ppb
| Be 9 ppb
| B 10 15251.4 265.7429 ppb
|- B 11 67853.6 266.0193 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 245768.3 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 6710868.2 251.194 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 531532.6 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 911950.9 ppb
| Tl 205 ppb
| Pb 206 2058006.7 248.9765 ppb
| Pb 207 1912720.3 266.0454 ppb
|- Pb 208 8322275.9 253.8473 ppb
Kr 83 -45427.7 ppb
ICP-Data 15 of 23
elementOne
e 24127-Metals 46.15
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatFriday, February 27, 2015 11:37:51
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 39935 ppb
| Be 9 ppb
| B 10 6479.3 108.617 ppb
|- B 11 28902 109.0115 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 220621.5 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 2756791.3 100.6025 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 545066.2 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 925443.6 ppb
| Tl 205 ppb
| Pb 206 911282 108.564 ppb
| Pb 207 790341.9 108.1715 ppb
|- Pb 208 3586061.6 107.6411 ppb
Kr 83 -18618.1 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 5
Sample DatFriday, February 27, 2015 11:39:10
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 40243.3 ppb
| Be 9 ppb
| B 10 4234.7 69.3746 ppb
|- B 11 19427.5 71.71077 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 233398.1 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 976.1 0.02424 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 547955.3 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 920973.5 ppb
| Tl 205 ppb
| Pb 206 459120.6 54.9918 ppb
| Pb 207 395167.4 54.40765 ppb
|- Pb 208 1818558.9 54.9064 ppb
Kr 83 57 ppb
ICP-Data 16 of 23
elementOne
e 24127-Metals 46.16
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 9
Sample DatFriday, February 27, 2015 11:40:28
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 40089.2 ppb
| Be 9 ppb
| B 10 310.7 2.22332 ppb
|- B 11 1415.1 2.30647 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 229256.4 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 1803.2 0.05724 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 521407.5 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 876083.4 ppb
| Tl 205 ppb
| Pb 206 455 0.03694 ppb
| Pb 207 372.3 0.03299 ppb
|- Pb 208 1751.1 0.03497 ppb
Kr 83 52.4 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 10
Sample DatFriday, February 27, 2015 11:41:46
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 39581.8 ppb
| Be 9 ppb
| B 10 4148.6 69.07214 ppb
|- B 11 18597.4 69.6799 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 232644.4 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 1438230 54.91243 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 520881.7 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 878226.2 ppb
| Tl 205 ppb
| Pb 206 458055 57.4992 ppb
| Pb 207 395460.8 57.03028 ppb
|- Pb 208 1807818 57.16224 ppb
Kr 83 -9683 ppb
ICP-Data 17 of 23
elementOne
e 24127-Metals 46.17
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC STD 2
Sample DatFriday, February 27, 2015 11:43:05
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 40310.3 ppb
| Be 9 ppb
| B 10 260.7 1.29872 ppb
|- B 11 1133.1 1.16817 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 234165.7 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 42368.4 1.49988 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 557398.7 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 924149.4 ppb
| Tl 205 ppb
| Pb 206 12325.4 1.45095 ppb
| Pb 207 10823.4 1.46424 ppb
|- Pb 208 49510 1.46928 ppb
Kr 83 -236.3 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24127-1.1
Sample DatFriday, February 27, 2015 11:44:23
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 36733 ppb
| Be 9 ppb
| B 10 1192.4 19.19934 ppb
|- B 11 5662.8 20.70622 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 251342.3 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 743207.3 26.15488 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 564871.4 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 948162.3 ppb
| Tl 205 ppb
| Pb 206 1207.1 0.11983 ppb
| Pb 207 1055.4 0.12005 ppb
|- Pb 208 4923.9 0.12359 ppb
Kr 83 -4978.4 ppb
ICP-Data 18 of 23
elementOne
e 24127-Metals 46.18
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24127-1.1
Sample DatFriday, February 27, 2015 11:45:41
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 37020.3 ppb
| Be 9 ppb
| B 10 4936.7 88.66552 ppb
|- B 11 22581.1 91.38619 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 260052 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 2189698.6 76.87549 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 566477 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 954111.5 ppb
| Tl 205 ppb
| Pb 206 455221.2 52.59299 ppb
| Pb 207 390039.4 51.78339 ppb
|- Pb 208 1794376.3 52.2327 ppb
Kr 83 -14770 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24127-1.1
Sample DatFriday, February 27, 2015 11:53:55
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 36408.2 ppb
| Be 9 ppb
| B 10 263 1.8242 ppb
|- B 11 1170.4 1.78894 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 231456.1 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 78109 2.72536 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 567372.4 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 928604.6 ppb
| Tl 205 ppb
| Pb 206 352.3 0.02131 ppb
| Pb 207 314.7 0.02194 ppb
|- Pb 208 1419.4 0.02179 ppb
Kr 83 -478.3 ppb
ICP-Data 19 of 23
elementOne
e 24127-Metals 46.19
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24127-1.1
Sample DatFriday, February 27, 2015 11:55:13
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 36723.3 ppb
| Be 9 ppb
| B 10 3401 60.62418 ppb
|- B 11 15341 61.53011 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 244081.3 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 77369.1 2.68597 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 570316.4 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 940796.8 ppb
| Tl 205 ppb
| Pb 206 440.3 0.03111 ppb
| Pb 207 380.7 0.03025 ppb
|- Pb 208 1704.7 0.02963 ppb
Kr 83 -467.6 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatFriday, February 27, 2015 11:56:32
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 39185 ppb
| Be 9 ppb
| B 10 153.3 -0.46066 ppb
|- B 11 703.7 -0.404 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 227198.4 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 203 -0.00413 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 542500.5 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 900009.6 ppb
| Tl 205 ppb
| Pb 206 121.3 -0.00566 ppb
| Pb 207 104.7 -0.00629 ppb
|- Pb 208 474.3 -0.00606 ppb
Kr 83 48.3 ppb
ICP-Data 20 of 23
elementOne
e 24127-Metals 46.20
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatFriday, February 27, 2015 11:57:50
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 39800.4 ppb
| Be 9 ppb
| B 10 6461.6 108.6323 ppb
|- B 11 28306.4 107.1299 ppb
|- Mg 24 ppb
| Mg 25 ppb
| Al 27 ppb
| K 39 ppb
| Ca 44 ppb
| Sc 45 234978.4 ppb
| Cr 52 ppb
| Cr 53 ppb
| Fe 54 ppb
| Mn 55 ppb
| Fe 57 ppb
| Co 59 ppb
| Ni 60 ppb
| Cu 63 ppb
| Cu 65 ppb
| Zn 66 ppb
| Zn 67 ppb
| Zn 68 ppb
| As 75 ppb
| Se 77 ppb
| Se 82 ppb
| Sr 88 2730385.7 99.66686 ppb
| Mo 95 ppb
| Mo 97 ppb
| Mo 98 ppb
|> Rh 103 544961.7 ppb
| Cd 111 ppb
|- Cd 114 ppb
|- Sb 121 ppb
| Sb 123 ppb
| Ba 135 ppb
| Ba 137 ppb
|> Ho 165 914403.5 ppb
| Tl 205 ppb
| Pb 206 909154.3 109.6008 ppb
| Pb 207 803037.3 111.224 ppb
|- Pb 208 3606574.5 109.5941 ppb
Kr 83 -18455.4 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: Blank
Sample DatTuesday, March 03, 2015 11:48:11
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 55071.9 ppb
|- Be 9 1 ppb
|- Al 27 1626.5 ppb
| Sc 45 266506.7 ppb
|> Rh 103 561357.6 ppb
Ho 165 1085838.5 ppb
Kr 83 37.1 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 1
Sample DatTuesday, March 03, 2015 11:49:20
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 59178.3 ppb
|- Be 9 376.7 0.94024 ppb
|- Al 27 9420.9 1.27053 ppb
| Sc 45 292147.1 ppb
|> Rh 103 594343.3 ppb
Ho 165 1153866 ppb
Kr 83 -151.4 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 2
Sample DatTuesday, March 03, 2015 11:50:28
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 57693.6 ppb
|- Be 9 38907.6 99.88563 ppb
|- Al 27 644316.1 107.0896 ppb
| Sc 45 293894.8 ppb
|> Rh 103 588050.3 ppb
Ho 165 1158254.5 ppb
Kr 83 -17871.7 ppb
ICP-Data 21 of 23
elementOne
e 24127-Metals 46.21
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: Standard 3
Sample DatTuesday, March 03, 2015 11:51:37
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 52941.8 ppb
|- Be 9 178626.2 500.023 ppb
|- Al 27 2833360.9 498.5815 ppb
| Sc 45 282065.5 ppb
|> Rh 103 556647.7 ppb
Ho 165 1106965.7 ppb
Kr 83 -86884.9 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatTuesday, March 03, 2015 11:52:46
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 54439 ppb
|- Be 9 38 0.1017 ppb
|- Al 27 2285.3 0.09692 ppb
| Sc 45 284080.5 ppb
|> Rh 103 590190.1 ppb
Ho 165 1135183.2 ppb
Kr 83 37.7 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 2
Sample DatTuesday, March 03, 2015 11:53:54
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 54250 ppb
|- Be 9 371.7 1.0118 ppb
|- Al 27 7873.1 1.02199 ppb
| Sc 45 288964.5 ppb
|> Rh 103 590931.9 ppb
Ho 165 1123393.7 ppb
Kr 83 -157.4 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 3
Sample DatTuesday, March 03, 2015 11:55:03
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 46612.1 ppb
|- Be 9 81014 257.47 ppb
|- Al 27 1319872.4 246.9139 ppb
| Sc 45 260317.8 ppb
|> Rh 103 523427.5 ppb
Ho 165 1012511.5 ppb
Kr 83 -40834.8 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatTuesday, March 03, 2015 11:56:12
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 49867.9 ppb
|- Be 9 33781.1 100.3332 ppb
|- Al 27 557379.7 96.72738 ppb
| Sc 45 270779.8 ppb
|> Rh 103 563011.7 ppb
Ho 165 1086152.5 ppb
Kr 83 -17314.8 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 5
Sample DatTuesday, March 03, 2015 11:57:22
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 48439.9 ppb
|- Be 9 16564.4 50.6599 ppb
|- Al 27 282565.2 49.89896 ppb
| Sc 45 265888.6 ppb
|> Rh 103 551858.1 ppb
Ho 165 1044118.6 ppb
Kr 83 46.9 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 9
Sample DatTuesday, March 03, 2015 11:58:31
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 47297.6 ppb
|- Be 9 5 0.01319 ppb
|- Al 27 15596.1 2.63374 ppb
| Sc 45 259727.3 ppb
|> Rh 103 523703.8 ppb
Ho 165 976871.3 ppb
Kr 83 39.9 ppb
ICP-Data 22 of 23
elementOne
e 24127-Metals 46.22
PerkinElmer ELAN 6100 ICP-MS
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 10
Sample DatTuesday, March 03, 2015 11:59:40
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 45159.2 ppb
|- Be 9 16545.7 54.26892 ppb
|- Al 27 302532.1 58.7005 ppb
| Sc 45 249915.6 ppb
|> Rh 103 502734.3 ppb
Ho 165 951734.8 ppb
Kr 83 -8723.2 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC STD2
Sample DatTuesday, March 03, 2015 12:00:50
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 46614 ppb
|- Be 9 342 1.08436 ppb
|- Al 27 7007.7 0.97104 ppb
| Sc 45 263080.4 ppb
|> Rh 103 547345.9 ppb
Ho 165 1011767.5 ppb
Kr 83 -142.9 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24127
Sample DatTuesday, March 03, 2015 12:01:59
Sample DesDuke
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 42314.9 ppb
|- Be 9 16.7 0.05571 ppb
|- Al 27 880513.3 157.3703 ppb
| Sc 45 267047.6 ppb
|> Rh 103 547764.2 ppb
Ho 165 1034202 ppb
Kr 83 -4389.6 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: 24127
Sample DatTuesday, March 03, 2015 12:03:08
Sample DesDuke
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 40393.5 ppb
|- Be 9 14561 53.40684 ppb
|- Al 27 1186767.5 214.4852 ppb
| Sc 45 267540 ppb
|> Rh 103 541412.1 ppb
Ho 165 1013022.8 ppb
Kr 83 -13268.5 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 1
Sample DatTuesday, March 03, 2015 12:04:18
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 42988 ppb
|- Be 9 7.7 0.02392 ppb
|- Al 27 1711.5 0.02193 ppb
| Sc 45 260861.9 ppb
|> Rh 103 549682.2 ppb
Ho 165 976195.7 ppb
Kr 83 47.5 ppb
Method 6020 & 200.8 Metals Summary Report
Sample ID: QC Std 4
Sample DatTuesday, March 03, 2015 12:05:27
Sample Description:
Concentration Results
Analyte Mass Meas. IntensConc. MeanReport Unit
|> Li 6 43044.9 ppb
|- Be 9 29281.5 100.7858 ppb
|- Al 27 508491.5 89.91741 ppb
| Sc 45 262903.5 ppb
|> Rh 103 552489.2 ppb
Ho 165 1004835.9 ppb
Kr 83 -16910.9 ppb
ICP-Data 23 of 23
elementOne
e 24127-Metals 46.23
PerkinElmer FIMS-100 CVAA Mercury Analyzer
Sample_ID Date Time Mean_Sig Mean_Rd Mean_Rt Units Alq.Vol. Sig 1 Reading-1 Result-1 Sig 2 Reading-2 Result-2
Calib Blank 2/26/2015 9:28:37 AM 0.0005093 µg 0.0006169 0.0004016
STD 1= .004 ug 2/26/2015 9:30:17 AM 0.0014587 µg 0.0014817 0.0014357
STD 2= .04 ug 2/26/2015 9:31:58 AM 0.0135508 µg 0.013617 0.0134846
STD 3= .08 ug 2/26/2015 9:33:51 AM 0.0267601 µg 0.026873 0.0266471
STD 4= .16 ug 2/26/2015 9:35:46 AM 0.0532 µg 0.0534953 0.0529046
STD 5= .20 ug 2/26/2015 9:37:41 AM 0.0669434 µg 0.0671184 0.0667684
Reagent Blank 2/26/2015 9:39:34 AM 1.99E-07 5.95E-07 5.95E-07 µg 2.81E-05 8.43E-05 8.43E-05 -2.77E-05 -8.31E-05 -8.31E-05
0.004ug = DL 2/26/2015 9:41:15 AM 0.0014469 0.0043316 0.0043316 µg 0.0014155 0.0042377 0.0042377 0.0014783 0.0044256 0.0044256
0.080ug = QC STD 2 2/26/2015 9:42:59 AM 0.0266173 0.079686 0.079686 µg 0.0267017 0.0799388 0.0799388 0.0265328 0.0794332 0.0794332
0.080ug = QC STD 3 2/26/2015 9:44:56 AM 0.0263789 0.0789723 0.0789723 µg 0.026499 0.0793319 0.0793319 0.0262588 0.0786126 0.0786126
Reagent Blank 2/26/2015 9:46:50 AM 6.19E-06 1.85E-05 1.85E-05 µg -9.02E-05 -0.00027 -0.00027 0.0001026 0.0003071 0.0003071
0.004ug = DL 2/26/2015 10:05:58 AM 0.0014669 0.0043914 0.0043914 µg 0.0014356 0.0042977 0.0042977 0.0014981 0.0044851 0.0044851
0.080ug = QC STD 2 2/26/2015 10:07:41 AM 0.0268421 0.0803592 0.0803592 µg 0.0270399 0.0809511 0.0809511 0.0266444 0.0797672 0.0797672
Reagent Blank 2/26/2015 10:09:35 AM -5.98E-05 -0.000179 -0.000179 µg -6.44E-05 -0.0001928 -0.0001928 -5.52E-05 -0.0001652 -0.0001652
24127- 1.1 2/26/2015 10:25:14 AM 0.0001507 0.0004506 1.13E-05 µg 40 1 0.0001528 0.0004568 1.14E-05 0.0001486 0.0004444 1.11E-05
24127- 1.1 DUP 2/26/2015 10:26:58 AM 9.31E-05 0.0002782 6.95E-06 µg 40 1 9.64E-05 0.000288 7.20E-06 8.98E-05 0.0002683 6.71E-06
0.004ug = DL 2/26/2015 10:28:41 AM 0.0013791 0.0041287 0.0041287 µg 0.0014142 0.0042338 0.0042338 0.001344 0.0040237 0.0040237
0.080ug = QC STD 2 2/26/2015 10:30:24 AM 0.0268122 0.0802695 0.0802695 µg 0.0267981 0.0802273 0.0802273 0.0268263 0.0803116 0.0803116
Reagent Blank 2/26/2015 10:32:18 AM -3.21E-05 -9.62E-05 -9.62E-05 µg -1.08E-05 -3.22E-05 -3.22E-05 -5.35E-05 -0.0001601 -0.0001601
24127- 1.1 SPK 2/26/2015 10:34:01 AM 0.0261034 0.0781471 0.0019537 µg 40 1 0.0260911 0.07811 0.0019528 0.0261158 0.0781842 0.0019546
0.004ug = DL 2/26/2015 10:35:54 AM 0.0014119 0.0042269 0.0042269 µg 0.0014337 0.0042923 0.0042923 0.0013901 0.0041615 0.0041615
0.080ug = QC STD 3 2/26/2015 10:37:38 AM 0.0263539 0.0788974 0.0788974 µg 0.0264938 0.0793163 0.0793163 0.0262139 0.0784784 0.0784784
Reagent Blank 2/26/2015 10:39:32 AM 1.35E-06 4.04E-06 4.04E-06 µg -1.13E-05 -3.37E-05 -3.37E-05 1.40E-05 4.18E-05 4.18E-05

Hg-Data 1 of 1
elementOne
e 24127-Hg 47.1