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Home My WebLink AboutNC0001422_Laboratory COCs - S4-Envirochem-FR_201508057 0_�� Environmental Chemists, Inc. chem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) SM 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DI-5 CERTIFICATE #37729 Duke Energy -Laboratory Date of Report: Apr 22, 2015 1339 Hagers Ferry Road/Bld 7405 MG03A2 Customer PO #: Huntersville NC 28078 Customer ID: 15030001 Attention: Peggy Kendall Report #: 2015-02979 Project ID: Ash Pond Investigation Lab ID Sample ID: Duke Energy- Ash Pond Collect Date/Time Matrix Sampled by 15-06854 Site: LCH Holdings 3/11/2015 2:00 PM DW Ray Porter Test Method Results Date Analyzed Bicarbonate as CaCO3 Bicarbonate as CaCO3 18.0 mg1L 03/23/2015 Carbonate as CaCO3 Carbonate as CaCO3 <2 mg/L 03/23/2015 Aluminum EPA200.7 0.041 mg/L 03/17/2015 Boron EPA200.7 0.18mg/L 03/24/2015 Calcium EPA200.7 20.0mg/L 03/18/2015 Iron EPA200.7 0.318mg1L 03/17/2015 Magnesium EPA200.7 1.61 mg/L 03/18/2015 Potassium EPA200.7 2.35mg/L 03/26/2015 Sodium EPA200.7 10.4mg/L 03/18/2015 Strontium EPA200.7 0.093mg/L 03/30/2015 Zinc EPA200.7 < 1.000 mg/L 03/17/2015 Antimony EPA 200.8 <0.0000987mg/L 04/16/2015 Arsenic EPA 200.8 0.000204J mg/L 04/16/2015 J: Estimated. Between Method Detection Limit and Reporting Limit. Barium EPA 200.8 < 0.400 mg/L 04/16/2015 Beryllium EPA 200.8 <0.002mg/L 03/17/2015 Cadmium EPA 200.8 0.0000998Jmg/L 04/1612015 J: Estimated. Between Method Detection Limit and Reporting Limit. Chromium EPA 200.8 <0.000148mg/L 04/16/2015 Cobalt EPA 200.8 0.000105J mg1L 04/16/2015 J: Estimated. Between Method Detection Limit and Reporting Limit. Copper EPA 200.8 0.218mg/L 03/12/2015 Lead EPA 200.8 0.005mg/L 03/17/2015 Manganese EPA 200.8 0.023mg/L 03/1712015 Molybdenum EPA 200.8 <0.0001 15 mg/L 04/16/2015 Nickel EPA 200.8 < 0.100 mg1L 04/16/2015 Selenium EPA 200.8 < 0.010 mg/L 04/16/2015 Report #:: 2016-02979 Page 1 of 2 Environmental Chemists, Inc. envirochem 6602 Windmill Way • Wilmington, NC 28405 (910) 392-0223 (Lab) • (910) 392-4424 (Fax) sm 710 Bowsertown Road • Manteo, NC 27954 (252)473-5702 ANALYTICAL & CONSULTING CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729 Duke Energy -Laboratory Date of Report: Apr 22, 2015 1339 Hagers Ferry Road/Bid 7405 MG03A2 Customer PO #: Huntersville NC 28078 Customer ID: 15030001 Attention: Peggy Kendall Report #: 2015-02979 Project ID: Ash Pond Investigation Thallium EPA200.8 <0.0000878mg/L 04/16/2015 Vanadium EPA200.8 0.000352Jmg/L 04/16/2015 J: Estimated. Between Method Detection Limit and Reporting Limit. Hexavalent Chromium EPA 218.7 <0.02 pg/L 03/20/2015 Mercury EPA245.1 <0.0004 mg/L 03/18/2015 Sulfate EPA300.0 41 mg/L 03/11/2015 Turbidity SM 2130 B 1.3 NTU 03/12/2015 Field Turbidity 1.9 NTU. Alkalinity SM 2320E 18 mg/L 03/23/2015 Conductivity SM 2510 B 194 umho/cm 03/12/2015 Total Dissolved Solids (TDS) SM 2540 C 125 mg/L 03/11/2015 Residue Suspended (TSS) SM 2540 D <2.5 mg/L 03/13/2015 Temperature SM 2550 B 17.2 C 03/11/2015 Chloride SM 4500 CI B 13 mg/L 03/12/2015 pH SM 4500 H B 5.56 units 03/11/2015 Dissolved Oxygen SM45000G 5.00mg/L 03/11/2015 Comment: Turbidity, temperature, pH and dissolved oxygen measured in field at sample collection. All non - detects for metals reported to MDL. Reviewed by: Report #:: 2015-02979 Page 2 of 2 ample rotor nation Environmental Chemist, Wilmingtor NC If not at well head why and list treatment Well Owner ID Public If public If public Sample devices and well number Well well or what is how many Well Use Well Well Well Date Time taken at prior to if more than one Owner private PWS homes Well Site (drinking, installation Well Casing Screen Sample sample wellhead sample well at property Name well? name ID? served? Address irrigation) date Depth Interval Interval Taken taken (Y/N) location I \ 'A y s Le,lk Imo\ fr` _ � � atzi.ei g 10 mkt c�nl L NO \l � 3(uj(r 14`o N S L `�r Duke Sample Number Duke Job Number Test Analyte Method CAS Number < or > Bicarbonate as CaCO3 Bicarbonate as CaCO3 Bicarbonate as CaCO3 71523 Carbonate as CaCO3 Carbonate as CaCO3 Carbonate as CaCO3 3812326 < Aluminum Aluminum EPA 200.7 7429905 < Boron Boron EPA 200.7 7440428 Calcium Calcium EPA 200.7 7440702 Cobalt Cobalt EPA 200.7 7440484 < Iron Iron EPA 200.7 7439896 Magnesium Magnesium EPA 200.7 7439954 Mol bdenum Molybdenum EPA 200.7 7439987 < Potassium Potassium EPA 200.7 7440097 Sodium Sodium EPA 200.7 7440235 Strontium Strontium EPA 200.7 7440246 Zinc Zinc EPA 200.7 7440666 < Antimony Antimony EPA 200.8 7440360 < Arsenic Arsenic EPA 200.8 7440382 < Barium Barium EPA 200.8 7440393 < Beryllium Beryllium EPA 200.8 7440417 < Cadmium Cadmium EPA 200.8 7440439 < Chromium Chromium EPA 200.8 7440473 < Copper Copper EPA 200.8 7440508 Lead Lead EPA 200.8 7439921 Manganese Manganese EPA 200.8 7439965 Nickel Nickel EPA 200.8 7440020 < Selenium Selenium EPA 200.8 7782492 < Thallium Thallium EPA 200.8 7440280 < Vanadium Vanadium EPA 200.8 7440622 < Hexavalent Chromium Hexavalent Chromium EPA 218.6 18540299 < Mercury Mercury EPA 245.1 7439976 < Sulfate Sulfate EPA 300.0 18758723 Turbidity Turbidity SM 2130 B 75354 Alkalinity Alkalinity SM 2320B 471341-alk Conductivity Conductivity SM 2510 B n/a Total Dissolved Solids TDS) Total Dissolved Solids (TDS) SM 2540 C 67163 Residue Suspended (TSS)Residue Suspended (TSS) SM 2540 D 57117-44-9 < Temperature Temperature SM 2550 B 75343 Chloride lChloride SM 4500 Cl B 16887006 H (Field) H (Field) SM 4500 H B 13967141 Dissolved Oxygen IDissolved Oxygen ISM 4500 0 G 7782447 Result Result Units Reporting Limit Qualifiers 18.0 m L 1 m /L 2 m /L 1 m /L 0.05 m L 0.01 m /L 0.18 m /L 0.01 m L 20.0 m L 1 m L 0.01 m /L 0.01 m /L 0.318 m /L 0.06 m /L 1.61 m /L 1 m /L 0.01 m /L 0.01 m /L 2.35 m /L 1 m /L 10.4 m /L 1 m /L 0.093 m /L 0.01 m /L 1 I m /L 1 m /L 0.003 m /L 0.003 m /L 0.005 m /L 0.005 m /L 0.4 m /L 0.4 m /L 0.002 m /L 0.002 m /L 0.001 m /L 0.001 m /L 0.02 m /L 0.02 m /L 0.218 m /L 0.05 m /L 0.005 m /L 0.003 m /L 0.023 m /L 0.01 m /L 0.1 m /L 0.1 m /L 0.01 m /L 0.01 m /L 0.001 m /L 0.001 m /L 0.001 m /L 0.001 m /L 0.02 n /L 50 n /L 0.0004 m /L 0.0004 m /L 41 m /L 15 m /L 1.3 NTU 0.1 NTU 18 m /L 1 m /L 194 umho/cm 10 umho/cm 125 m L 2.5 m L 2.5 m /L n/a m L 17.2 c 1 c 13 m /L 5 m /L 5.56 units 4 units 5.00 m /L 0.5 m /L el, elementOne Ray Porter Environmental Chemists, Inc. 66002 Windmill Way Wilmington, NC 28405 Element One Inc. 6319-D Carolina Beach Rd. Wilmington, NC 28412 Phone: 910 793-0128 Fax: 910 792-6853 ellab@ellab.com FINAL REPORT OF ANALYSES March 23, 2015 Client Project Name: Client Project Number. E1 Project Number e24305 Sample # Sample ID 15-06854 Sample Matrix DW Sample Type Date Received 03/19/2015 Date Sampled 03/11/2015 Time Sampled 1400 Time Received 1050 Delivered by Client Sampler Received by LLB E1 Sample # 24305-1 Parameter Result Unit Dilution DL Method Date Chromium VI < 0.02 pg/L 1 0.02 EPA 218.7 03/20/2015 i VV Kerf Smith, Laboratory Director 24305 Envirochem M218.7 Report Compiled by —]All-) NC Certifications: DW 37788 and DWQ DENR 604 r ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way Wilmington, NC 28405 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CER+IFICATION # 37729 OFFICE: 910-392-0223 FAX 910-392-4424 Analytical &Consulting Chemists COLLECTION AND CHAIN OF CUSTODY CLIENT: Duke Energy- Lab PROJECT NAME: Ash Pond Investigation REPORT NO:—Q g ADDRESS: 1339 Ha ers Ferry Rd/ Bldg 7405 MG03A2 CONTACT NAME: PO NO: Huntersville, NC 28079 REPORT TO: PHONE/FAX: Attn: Peggy Kendall COPY TO: E-MAIL: Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection d m A F vJ 0 a E `o 0 eC7 `o i j �' �� _ m U E O w g E Z PRESERVATION ANALYSIS REQUESTED Date Time Temp i i s 'o s $ x <o< Y o_ w 0 LC-kA V\,A&wp aa\ 5. vt,. 0 1t L 3 I li t q 0O o \1 Z C C P �( Metals: Al, B, Ca, Co, Fe, Mg, Mo, Na, Sr, V, Zn,b, As Ba,Se TCd,Cr, Cu, G G C P Hexavalent Chromium G G C P Sulfate, Chloride, Alkalinity, Carbonate, Bicarbonate, Conductivity G G C P TSS, TDS G G C P pH, Dissolved Oxygen, Temperature, Turbidity (all field parameters) G G C P Note: Special reporting limits. QA/QC reports required with data: EDDs required. G G C P and NC DENR via US mail. See project G G C P G G NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.2 ppm or less) In the field at the time of collection. See reverse for Instructions Transfer Relinquished By: Date/Time Received By: Date/Time 2. Temperature when Received: II, �i. Accepted: r/ ejected; Kesampie Delivered By: - iu V-� at+N wl, 5 S (n Received By: Date:_ Comments: n�TU Iov oL �� G Flo ."LI", ivy �- snk rtwn..=n.mmmam..�•mwm.nu...nm.ae.q..i®mu.u.:�etw.u.xew�.e�owa).euw....emin iwi..n r,.wm ne. am.r vn��R n. wa o.... m �u.q w. rr..e e.... w e....as. n.r.ro sJw�a wa o....m wa v. Mew m..�I wa o.... wa �.m. m+.m wa o....are wa w..ve.. ne erwa..�ae nor ��