NC0001422_Laboratory COCs - S2Well 1&2-Envirochem-FR_20150805

Environmental Chemists, Inc.
envirochem 6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
SM
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE 094. DLS CERTIFICATE #37729
Duke Energy -Laboratory Date of Report: Apr 20, 2015
1339 Hagers Ferry Road/Bld 7405 MG03A2 Customer PO #:
Huntersville NC 28078 Customer ID: 15030001
Attention: Peggy Kendall Report #: 2015-02734
Project ID: Ash Pond Investigation
Lab ID
Sample ID: St. Wooten - Combo Collect Date/Time
Matrix Sampled by
15-06241
Site: Well 1 & 2 Combined 3/5/2015 11:45 AM
DW Ray Porter/Cindy McDonald
Test
Method
Results
Date Analyzed
Bicarbonate as CaCO3 Bicarbonate as CaCC3
36.0 mg/L
03/19/2015
Carbonate asCaCO3 Carbonate asCaCO3
<1mg/L
03/19/2015
Aluminum
EPA200.7
0.045mg/L
03/11/2015
Boron
EPA200.7
0.16 mg/L
03/11/2015
Calcium
EPA200.7
60.7mg/L
03/12/2015
Iron
EPA200.7
0.635mg/L
03/11/2015
Magnesium
EPA200.7
5.46 mg/L
03/12/2015
Potassium
EPA200.7
9.98mg/L
03/12/2015
Sodium
EPA200.7
24.1 mg/L
03/12/2015
Strontium
EPA200.7
0.287 mg/L
03/11/2015
Zinc
EPA200.7
0.015 mg/L
03/11/2015
Antimony
EPA200.6
<0.000099mg/L
03/10/2015
Arsenic
EPA 200.8
0.000575Jmg/L
03/10/2015
J: Estimated. Between Method Detection Limit and Reporting Limit.
Barium EPA 200.8
Beryllium EPA 200.8
Cadmium EPA 200.8
Chromium EPA 200.8
J: Estimated. Between Method Detection Limit and Reporting Limit.
Cobalt
EPA 200.8
Copper
EPA 200.8
Lead
EPA 200.8
Manganese
EPA 200.8
Molybdenum
EPA 200.8
J: Estimated. Between Method Detection Limit and Reporting Limit.
Nickel EPA 200.8
Selenium EPA 200.8
0.047 mg/L 03/10/2015
<0.000146 mg/L 03/1012015
<0.0000827 mg/L 03/1012015
0.000176 J mg/L 03/10/2015
0.002 mg/L
03/1112015
0.004 mg/L
03/10/2015
<0.000126 mg/L
03/10/2016
0.278 mg/L
03/11/2015
0.000758 J mg/L
03/10/2015
< 0.100 mg/L 03/10/2015
0.001 mg/L 03/27/2015
Report #:: 2015-02734 Pagel of 2

Environmental Chemists, Inc.
envirochem 6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
$M
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Duke Energy -Laboratory
1339 Hagers Ferry Road/Bld 7405 MG03A2
Huntersville NC 28078
Attention: Peggy Kendall
Date of Report: Apr 20, 2015
Customer PO #:
Customer ID: 15030001
Report M 2015-02734
Project ID: Ash Pond Investigation
Thallium
EPA200.8
<0.0001 mg/L
03/10/2015
Vanadium
EPA200.8
0.000386 J mg/L
03/11/2015
J: Estimated. Between Method Detection Limit and Reporting Limit.
Hexavalent Chromium
EPA218.7
<0.02 pg/L
03/09/2015
Mercury
EPA 245.1
<0.0004 mg/L
03/09/2015
Sulfate
EPA300.0
160mg/L
03/11/2015
Turbidity
SM 2130 B
5.3 NTU
03/06/2016
Field Turbidity 4.1 NTU.
Alkalinity
SM2320B
36mg/L
03/13/2015
Conductivity
SM 2510 B
506 umho/cm
03/12/2015
Total Dissolved Solids (TDS)
SM 2540 C
326 mg/L
03/06/2015
Residue Suspended (TSS)
SM 2540 D
<2.5 mg/L
03/09/2015
Temperature
SM 2550 B
18.7 C
03/05/2015
Chloride
SM 4500 CI B
25 mg/L
03/12/2015
pH
SM4500 H B
6.02 units
03/06/2015
Dissolved Oxygen
SM 4500 o c
6.60 mg/L
03/05/2015
Comment: Turbidity, temperature, pH and dissolved oxygen measured in field at sample collection. All non -
detects for metals reported to MDL.
Reviewed by:
Report*: 2015-02734 Page 2 of 2

Environmental Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
sm 710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
QC for Duke Energy - 2015-02734
LCS
Parameter
True Value
Rest
% True Value
Limits
Alkalinity
50
52
104
90-110
Aluminum
0.05
0.05
100
90-110
Antimony
0.01
0.01
100
90-110
Arsenic
0.01
0.01
100
90-110
Barium
0.01
0.01
100
90-110
Beryllium
0.01
0.01
100
90-110
Boron
0.05
0.05
100
90-110
Cadmium
0.01
0.01
100
90-110
Calcium
0.5
0.5
100
90-110
Chloride
50
48
96
90-110
Chromium
0.01
0.01
100
90-110
Cobalt
0.01
0.01
100
90-110
Conductivity
10000
99900
99.9
90/110
Copper
0.01
0.01
100
90-110
Iron
0.05
0.05
100
90-110
Lead
0.01
0.01
100
90-110
Magnesium
0.5
0.5
100
90-110
Manganese
0.01
0.01
100
90-110
Mercury
0.0040
0.0037
92
90-110
Molybdenum
0.01
0.01
100
90-110
Nickel
0.0050
0.0048
96
90-110
Potassium
0.5
0.5
100
90-110
TSS
248.8
274.4
110
90-110
Selenium
0.01
0.01
100
90-110
Sodium
0.5
0.5
100
90-110
Strontium
0.05
0.05
100
90-110
Sulfate
50
50
100
90-110
Thallium
0.0050
0.0048
96
90-110
TDS
600
601
100
:1: 10
Turbidity
N/A
N/A
N/A
N/A

Vanadium
0.01
0.01
100
90-110
Zinc
0.05
0.05
100
1 90-110
MS/MSD
Parameter
True Value
mg/L
Result
mg/L
%
Recovery
%
Difference
Limits %
Recovery
Limits %
Difference
Alkalinity
N/A
N/A
N/A
N/A
N/A
N/A
Aluminum
0.100
0.099/0.100
99/100
1
80-120
<20
Antimony
0.025
0.028/0.028
112/112
0
80-120
:520
Arsenic
0.025
0.030/0.030
120/120
0
80-120
<20
Barium
0.025
0.025/0.025
100/100
0
80-120
<20
Beryllium
0.025
0.029/0.029
116/116
0
80-120
<_ 20
Boron
0.100
0.097/0.095
97/95
2
80-120
<20
Cadmium
0.025
0.028/0.028
112/112
0
80-120
<_ 20
Calcium
1.0
0.98/0.99
98/99
1
80-120
<20
Chloride
N/A
N/A
N/A
N/A
N/A
N/A
Chromium
0.025
0.024/0.025
96/100
4
80-120
<20
Cobalt
0.025
0.024/0.025
96/100
4
80-120
<_ 20
Conductivity
N/A
N/A
N/A
N/A
N/A
N/A
Copper
0.025
0.027/0.028
108/112
4
80-120
<_ 20
Iron
0.100
0.098/0.100
98/100
2
80-120
<20
Lead
0.025
0.023/0.023
92/92
0
80-120
<_ 20
Magnesium
1.0
0.98/1.0
98/100
2
80-120
<20
Manganese
0.025
0.024/0.025
96/100
4
80-120
<20
Mercury
0.0020
0.0022/0.0019
110/95
15
80-120
<20
Molybdenum
0.025
0.028/0.028
112/112
0
80-120
5 20
Nickel
0.0100
0.0099/0.0103
99/103
4
80-120
<20
Potassium
1.0
1.0/1.0
100/100
0
80-120
_<20
TSS
N/A
N/A
N/A
N/A
N/A
N/A
Selenium
0.025
0.030/0.030
120/120
0
80-120
<20
Sodium
1.0
1.0/1.0
100/100
0
80-120
<20
Strontium
0.100
0.098/0.105
98/105
7
80-120
<20

Sulfate
10.0
10.5/10.6
105/106
1
80-120
5 20
Thallium
0.0100
0.0102/0.0105
102/105
3
80-120
<_ 20
TDS
N/A
N/A
N/A
N/A
N/A
N/A
Turbidity
N/A
N/A
N/A
N/A
N/A
N/A
Vanadium
0.025
0.024/0.025
96/100
4
80-120
<_ 20
Zinc
0.100
0.099/0.102
99/102
3
80-120
<_ 20
DUPLICATE SAMPLES
Parameter
Results mg/L
% Difference
Limits
Alkalinity
36
36
0
< 10
Aluminum
N/A
N/A
N/A
N/A
Antimony
N/A
N/A
N/A
NIA
Arsenic
N/A
N/A
N/A
N/A
Barium
N/A
N/A
N/A
N/A
Beryllium
N/A
N/A
N/A
N/A
Boron
N/A
N/A
N/A
N/A
Cadmium
N/A
N/A
N/A
N/A
Calcium
N/A
N/A
N/A
N/A
Chloride
467
462
1
< 10
Chromium
N/A
N/A
N/A
N/A
Cobalt
N/A
N/A
N/A
N/A
Conductivity
156
156
0
< 10
Copper
N/A
N/A
N/A
N/A
Iron
N/A
N/A
N/A
N/A
Lead
N/A
N/A
N/A
N/A
Magnesium
N/A
N/A
N/A
N/A
Manganese
N/A
N/A
N/A
N/A
Mercury
N/A
N/A
N/A
N/A
Molybdenum
N/A
N/A
N/A
N/A
Nickel
N/A
N/A
N/A
N/A
Potassium
N/A
N/A
N/A
N/A
TSS
313.3
303.3
3
<_ 10
Selenium
N/A
N/A
N/A
N/A
Sodium
N/A
N/A
N/A
N/A

Strontium
N/A
N/A
N/A
N/A
Sulfate
28
29
4
< 10
Thallium
N/A
N/A
N/A
N/A
TDS
403
404
0
< 10
Turbidity
0.37
0.37
0
<_ 10
Vanadium
N/A
N/A
N/A
N/A
Zinc
N/A
N/A
N/A
N/A
BLANKS
Parameter
Results,
Limit, mg/L
Alkalinity
1
1
Aluminum
<0.005
0.005
Antimony
<0.0005
0.0005
Arsenic
<0.0005
0.0005
Barium
<0.0005
0.0005
Beryllium
<0.0005
0.0005
Boron
<0.005
0.005
Cadmium
<0.0005
0.0005
Calcium
<0.5
0.5
Chloride
2.5
2.5
Chromium
<0.0005
0.0005
Cobalt
<0.0005
0.0005
Conductivity
<5
5
Copper
<0.0005
0.0005
Iron
<0.005
0.005
Lead
<0.0005
0.0005
Magnesium
<0.5
0.5
Manganese
<0.0005
0.0005
Mercury
<0.0002
0.0002
Molybdenum
<0.0005
0.0005
Nickel
<0.00005
0.00005
Potassium
<0.5
0.5
TSS
<2.5
2.5

Selenium
<0.0005
0.0005
Sodium
<0.5
0.5
Strontium
<0.005
0.005
Sulfate
<2.5
2.5
Thallium
<0.00005
0.00005
TDS
<2.5
2.5
Turbidity
N/A
N/A
Vanadium
<0.0005
0.0005
Zinc
<0.005
0.005

Element One Inc.
6319-D Carolina Beach Rd.
eI 1 Wilmington, NC 28412
Phone: [phone]
Fax: [phone]
[e-mail]
e�ementOne
FINAL REPORT OF ANALYSES
Ray Porter
March 09, 2015
Environmental Chemists, Inc.
Client Project Name:
66002 Windmill Way
Client Project Number:
Wilmington, NC 28405
E1 Project Number e24189
Sample #
Sample ID
15-06241
Sample Matrix DW
Sample Type
Date Received
03106/2015
Date Sampled 03/05/2015
Time Sampled
1145 Time Received
0810
Delivered by Client
Sampler
Received by
KMS
E1 Sample #
24189-3
Parameter
Result Unit Dilution
DL Method
Date
Chromium VI
< 0.02 pg/L
1 0.02 EPA 218.7
03/09/2015
Ken Smith, Laboratory Director
24189 Envirochem Cr6+Report Compiled by —Lk -
NC Certifications: DW 37788 and DWO DENR 604

a; ST
'Ghent ID. -
Facility Name: Environmental Chemists,Inc Permit494'
—` PLEASE CIRCLE METER USED FOR IDENTIFICATION PURPOSES
Meter Id: 11277 Meter Id: 11280. . Meter Id: 09996 Meter Id: NYI-11373 --
Analyst: L1
PH Analysis r
( ' I.AA = R CM In* -
Cahbratiotnni Buffer lU.0 •Check Buffer 7.0 V Comments
CaL Time
CalibrationBuffer 4.0
/
(J.V' �.� Slope: / -. / -
"pH buffer checks are to be within± 0.1 pH units of the standards true value
Facility/Sample location 7
Time Sampled♦ I
Time Analyzed
Temp (°C) ■
pH Result
heckvalue
Comment
�041
b0 132
1, 5
�f5
.02-
+If sample is measured in directly in the stream only time analyzed woula oe recornea.
►Iudicates a. recommended drift cbeck. (Use Buffer 7.0) Should be within � 0.1 units of the buffer's true value)
• Document the temperature of the sample at the time of analysis. Note This temperature is not to be used for reporting on the monthly monitoring report.
Calibration drift check is recommended when performing analysis at multiple sampliug locations,
*All pH results in pH units (r.e., s.u.).
_Total Residual Chlorine
Facility/Sample Location
Time Sampled
Time Analyzed I
TRC Result Daily check standard
uu/L obtained value ug/L
Comment
'1'RC check standard obtained true value 210 (acceptance range 19U-22U ug/L) (611ould recover wrmm Giu i at rat
cheep standard's obtained true value)
Dissolved Oxygen (DO)
Refereace Method: SM 4500 O G, 201h Edition, —YSI DO 550 A Model—YSIPRO 20
Temperature
.0
Adjusted Air
Calibration♦
(mg/L)
Saturation
%
Cahbration Facility/Sample Location DO reading °Time Sample Temperature
Time mg/L Analyzed/Ilme
I Sampled
Ob%
q;OD IMOM I'5;L Il.bv1VTO
♦Based on appropriate altitude adjustment
-- -- 4 When performing analysis at multiple sampling locations, re-calibration(s) should be performed every four hooks:" -
.. 'Analysis time and sampling time the same. (Ideally the sample should be analywrl in-situ):..........z.
- " Temperat¢re Sensor Annual CheckDate(550 A): IN PROCESS Temperature Sensor Annual Cheek Date (PRO 20):IN PROCESS
Temperature - ... .. ........ _ .. ----
.._._ — Reference Method. SM 2550 B 2e Edition
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