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Home My WebLink AboutNC0001422_Laboratory COCs - S17-Microbac-FR_20150805Fayetteville Division Certificate of Analysis Project: GW Sample - Coal Ash Date Reported: 05/29/15Division of Water Well Testing 1636 Mail Service Center Duke Energy Raleigh NC, 27709 Date Sampled: 04/30/15 Sampled By: Dermer Date Received: 05/01/15 ResultAnalyte Analyzed Method QualifierUnits K5E0015-01 Analyzed By S17 Field Data 5.1 pHpH Units 04/30/15 12:00 DermerpH Conductivity 92 mho 04/30/15 12:00 Dermer SM2510 Dissolved Oxygen 9.6 mg/L 04/30/15 12:00 Dermer SM4500 O Turbidity NTU 04/30/15 12:00 Dermer SM2130B0.34 Analyzed by: Microbac Laboratories, Inc. - Chicagoland Antimony mg/L EPA 200.8 Rev 5.405/22/15 17:47 RPL<0.0010 Arsenic mg/L EPA 200.8 Rev 5.405/22/15 17:47 RPL<0.0010 Cobalt mg/L EPA 200.8 Rev 5.405/22/15 17:47 RPL<0.0010 Thallium mg/L EPA 200.8 Rev 5.405/22/15 17:47 RPL<0.0010 Vanadium mg/L EPA 200.8 Rev 5.405/22/15 17:47 RPL<0.0050 Mercury mg/L EPA 245.1 Rev 3.005/27/15 10:09 SA<0.00020 Analyzed by: Microbac Laboratories, Inc. - Fayetteville Bicarbonate Alkalinity mg CaCO3/L SM 2320 B-199705/11/15 13:18 NCH1.23 Carbonate Alkalinity mg CaCO3/L SM 2320 B-199705/11/15 13:18 NCH0.00 Hydroxyl Alkalinity mg CaCO3/L SM 2320 B-199705/11/15 13:18 NCH0.00 Aluminum mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW0.129 Barium mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW0.0420 Beryllium mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW<0.000250 Boron mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW0.0620 Cadmium mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW<0.00100 Calcium mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW10.3 Chloride Bmg/L EPA 300.0, Rev. 2.1 (1993)05/04/15 14:53 NCH15.2 Chromium mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW<0.00100 Copper mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW0.0330 Dissolved Oxygen mg/L SM 4500-O G-200105/01/15 14:15 DSK8.40 Iron mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW0.0330 Lead mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW<0.00300 Magnesium mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW1.34 Manganese mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW0.0690 Microbac Laboratories, Inc. 2592 Hope Mills Road | Fayetteville, NC 28306 | 910.864.1920 p | 910.864.8774 f | www.microbac.com Page 1 of 7 Fayetteville Division Certificate of Analysis Project: GW Sample - Coal Ash Date Reported: 05/29/15Division of Water Well Testing 1636 Mail Service Center Duke Energy Raleigh NC, 27709 Date Sampled: 04/30/15 Sampled By: Dermer Date Received: 05/01/15 ResultAnalyte Analyzed Method QualifierUnits K5E0015-01 Analyzed By S17 Analyzed by: Microbac Laboratories, Inc. - Fayetteville Molybdenum mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW<0.00100 Nickel mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW<0.00100 Oxidation Reduction Potential mV SM 2580B05/29/15 15:23 JMO227.0 Potassium mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW1.41 Selenium mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW<0.0100 Sodium mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW6.35 Total Dissolved Solids Bmg/L SM 2540 C-199705/05/15 13:30 MLW75.0 Total Suspended Solids mg/L SM 2540 D-199705/04/15 10:29 NCH<1.00 Strontium mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW0.0450 Sulfate as SO4 mg/L EPA 300.0, Rev. 2.1 (1993)05/04/15 14:53 NCH23 Turbidity NTU SM 2130 B-200105/01/15 14:10 DSK<1.0 Zinc mg/L EPA 200.7 Rev 4.4 199405/29/15 08:20 JAW<0.0100 QC Batch Run - (Microbac Laboratories, Inc. - Chicagoland ) SourceResultUnits LimitRPDAnalyte Calcium 1.53 20mg/L41.6 15E0986 Copper 0.626 20mg/L0.0290 15E0973 Cobalt 1.24 20mg/L0.0196 15E0986 Cobalt 0.626 20mg/L0.0199 15E0973 Chromium 0.337 20mg/L0.186 15E0973 Calcium 1.67 20mg/L7.75 15E0973 Magnesium 2.78 20mg/L8.73 15E0973 Chromium 1.06 20mg/L0.190 15E0986 Magnesium 1.44 20mg/L15.2 15E0986 Lead 0.181 20mg/L0.194 15E0973 Lead 1.55 20mg/L0.190 15E0986 Cadmium 0.291 20mg/L0.0198 15E0973 Iron 0.121 20mg/L0.367 15E0986 Iron 0.974 20mg/L0.473 15E0973 Microbac Laboratories, Inc. 2592 Hope Mills Road | Fayetteville, NC 28306 | 910.864.1920 p | 910.864.8774 f | www.microbac.com Page 2 of 7 Fayetteville Division Certificate of Analysis Project: GW Sample - Coal Ash Date Reported: 05/29/15Division of Water Well Testing 1636 Mail Service Center Duke Energy Raleigh NC, 27709 Date Sampled: 04/30/15 Sampled By: Dermer Date Received: 05/01/15 QC Batch Run - (Microbac Laboratories, Inc. - Chicagoland ) SourceResultUnits LimitRPDAnalyte Copper 1.09 20mg/L0.0198 15E0986 Arsenic 0.992 20mg/L0.197 15E0973 Arsenic 0.461 20mg/L0.201 15E0986 Antimony 0.587 20mg/L0.201 15E0973 Antimony 1.87 20mg/L0.204 15E0986 Aluminum 1.47 20mg/L0.197 15E0973 Aluminum 0.601 20mg/L0.241 15E0986 Cadmium 3.21 20mg/L0.0201 15E0986 Boron 0.818 20mg/L0.299 15E0973 Barium 0.191 20mg/L0.222 15E0973 Beryllium 0.244 20mg/L0.0235 15E0973 Beryllium 0.290 20mg/L0.0236 15E0986 Barium 0.939 20mg/L0.230 15E0986 Boron 2.56 20mg/L0.363 15E0986 Thallium 0.549 20mg/L0.199 15E0973 Strontium 1.36 20mg/L0.163 15E0986 Titanium 0.718 20mg/L0.204 15E0986 Tin 0.0244 20mg/L0.0969 15E0973 Thallium 2.06 20mg/L0.197 15E0986 Tin 2.11 20mg/L0.109 15E0986 Mercury 12.1 20mg/L0.000882 15E0978 Mercury 5.69 20mg/L0.00193 15E1032 Zinc 0.298 20mg/L0.232 15E0973 Zinc 0.934 20mg/L0.199 15E0986 Vanadium 4.97 20mg/L0.205 15E0986 Titanium 0.735 20mg/L0.205 15E0973 Potassium 0.788 20mg/L4.81 15E0986 Nickel 0.0273 20mg/L0.197 15E0986 Molybdenum 0.00736 20mg/L0.231 15E0986 Microbac Laboratories, Inc. 2592 Hope Mills Road | Fayetteville, NC 28306 | 910.864.1920 p | 910.864.8774 f | www.microbac.com Page 3 of 7 Fayetteville Division Certificate of Analysis Project: GW Sample - Coal Ash Date Reported: 05/29/15Division of Water Well Testing 1636 Mail Service Center Duke Energy Raleigh NC, 27709 Date Sampled: 04/30/15 Sampled By: Dermer Date Received: 05/01/15 QC Batch Run - (Microbac Laboratories, Inc. - Chicagoland ) SourceResultUnits LimitRPDAnalyte Molybdenum 1.09 20mg/L0.225 15E0973 Manganese 2.10 20mg/L0.100 15E0986 Strontium 0.685 20mg/L0.0281 15E0973 Vanadium 0.470 20mg/L0.196 15E0973 Manganese 1.35 20mg/L0.0435 15E0973 Nickel 0.360 20mg/L0.200 15E0973 Silver 0.493 20mg/L0.0182 15E0973 Sodium 1.31 20mg/L46.7 15E0973 Sodium 1.27 20mg/L45.5 15E0986 Silver 2.44 20mg/L0.0181 15E0986 Potassium 1.29 20mg/L4.07 15E0973 Selenium 0.502 20mg/L0.194 15E0986 Selenium 0.995 20mg/L0.190 15E0973 QC Batch Run - (Microbac Laboratories, Inc. - Fayetteville) SourceResultUnits LimitRPDAnalyte Copper 27 200mg/L0.0510 K5E0760 Chloride 0.4 10mg/L15.8 K5D1006 Chromium 24 200mg/L0.0190 K5E0760 Chloride 1 10mg/L8.06 K5D1011 Chromium 0.4 200mg/L0.253 K5E0760 Copper 1 200mg/L0.269 K5E0760 Dissolved Oxygen 18mg/LND K5D0939 Dissolved Oxygen 0 18mg/L8.40 K5E0015 Iron 4 200mg/L4.63 K5E0760 Iron 6 200mg/L9.99 K5E0760 Barium 0.8 200mg/L0.242 K5E0760 Lead 200mg/LND K5E0760 Lead 2 200mg/L0.232 K5E0760 Boron 7 200mg/L0.0150 K5E0760 Microbac Laboratories, Inc. 2592 Hope Mills Road | Fayetteville, NC 28306 | 910.864.1920 p | 910.864.8774 f | www.microbac.com Page 4 of 7 Fayetteville Division Certificate of Analysis Project: GW Sample - Coal Ash Date Reported: 05/29/15Division of Water Well Testing 1636 Mail Service Center Duke Energy Raleigh NC, 27709 Date Sampled: 04/30/15 Sampled By: Dermer Date Received: 05/01/15 QC Batch Run - (Microbac Laboratories, Inc. - Fayetteville) SourceResultUnits LimitRPDAnalyte Aluminum 8 200mg/L7.26 K5E0760 Aluminum 8 10mg/L2.01 K5E0760 Barium 4 200mg/L0.0250 K5E0760 Beryllium 200mg/LND K5E0760 Boron 5 200mg/L0.263 K5E0760 Cadmium 200mg/LND K5E0760 Cadmium 1 200mg/L0.248 K5E0760 Calcium 9 200mg/L8.36 K5E0760 Calcium 6 200mg/L14.3 K5E0760 Beryllium 0 200mg/L0.246 K5E0760 Total Dissolved Solids 4 5mg/L72.0 K5E0015 Total Suspended Solids 2 5mg/L14.5 K5E0010 Total Suspended Solids 33 5mg/L1.75 K5E0007 Total Suspended Solids 0 5mg/L7.25 K5D1002 Strontium 0 200mg/L0.0350 K5E0760 Strontium 3 200mg/L0.275 K5E0760 Sodium 6 200mg/L107 K5E0760 Sulfate as SO4 0.6 10mg/L4.12 K5D1011 Sulfate as SO4 0.9 10mg/L8.46 K5D1006 Turbidity 5NTUNDK5E0015 Zinc 0.2 200mg/L0.843 K5E0760 Zinc 5 15mg/L0.602 K5E0760 Nickel 1 200mg/L0.262 K5E0760 Magnesium 10 200mg/L1.73 K5E0760 Magnesium 3 200mg/L6.87 K5E0760 Manganese 4 200mg/L0.290 K5E0760 Manganese 0 200mg/L0.0560 K5E0760 Molybdenum 15mg/LND K5E0760 Sodium 9 200mg/L93.4 K5E0760 Microbac Laboratories, Inc. 2592 Hope Mills Road | Fayetteville, NC 28306 | 910.864.1920 p | 910.864.8774 f | www.microbac.com Page 5 of 7 Fayetteville Division Certificate of Analysis Project: GW Sample - Coal Ash Date Reported: 05/29/15Division of Water Well Testing 1636 Mail Service Center Duke Energy Raleigh NC, 27709 Date Sampled: 04/30/15 Sampled By: Dermer Date Received: 05/01/15 QC Batch Run - (Microbac Laboratories, Inc. - Fayetteville) SourceResultUnits LimitRPDAnalyte Nickel 14 15mg/L0.0150 K5E0760 Potassium 8 200mg/L7.65 K5E0760 Potassium 6 200mg/L13.2 K5E0760 Selenium 3 200mg/L0.260 K5E0760 Selenium 15mg/LND K5E0760 Molybdenum 0.8 200mg/L0.254 K5E0760 Notes and Definitions E Value above quantitation range B Detected in the associated Method Blank State Certifications: NCDNR #11 NCDOH #37714 Respectfully Submitted Jeanne Overstreet, Project Manager Thank you for your business. We invite your feedback on our level of service to you. Please contact the Division Manager, Rob Dermer at 910-864-1920 with any questions. You may also contact J. Trevor Boyce, President at president@microbac.com Microbac Laboratories, Inc. 2592 Hope Mills Road | Fayetteville, NC 28306 | 910.864.1920 p | 910.864.8774 f | www.microbac.com Page 6 of 7 Page 7 of 7