NC0001422_ATT 5 - Water - J15050565report_20150805

13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number: J15050565
Project Name:SUTTON - AB GW ASSESSMENT WATER
Lab Contact:Mary Ann Ogle
Date:6/8/2015
Customer Address:
Customer Name(s): Perry Waldrep, Tim Hunsucker, Kathy Webb, John Toepfer
Phone: [phone]
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.
Mary Ann Ogle
Analytical Lab
Page 1 of 56
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection
Date and Time Collected By Sample Description
2015015484 Sutton 18-May-15 3:00 PM ILLEGIBLE AW-2D
2015015485 Sutton 18-May-15 1:03 PM ILLEGIBLE AW-5D
2015015486 Sutton 19-May-15 11:25 AM ILLEGIBLE AW-5E
2015015487 Sutton 19-May-15 8:40 AM ILLEGIBLE AW-9D
2015015488 Sutton 18-May-15 10:45 AM ILLEGIBLE Equipment Blank
2015015489 Sutton 19-May-15 8:40 AM ILLEGIBLE Equipment Blank
2015015490 Sutton 18-May-15 10:45 AM ILLEGIBLE Filter Blank
2015015491 Sutton 19-May-15 8:40 AM ILLEGIBLE Filter Blank
8 Total Samples
Analytical Lab
Page 2 of 56
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:Mary Ann Ogle Date:6/8/2015
Electronic Data Deliverable (EDD) Sent Separately
Analytical Lab
Page 3 of 56
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050565
2015015484
Collection Date: 18-May-15 3:00 PM
Site: AW-2D
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.012 mg-N/L EPA 353.2 05/27/2015 13:01 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 140 mg/L EPA 300.0 05/26/2015 15:19 BGN90342.5 25
Sulfate 34 mg/L EPA 300.0 05/26/2015 15:19 BGN9034110
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 05/28/2015 12:21 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 05/29/2015 13:48 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.021 mg/L EPA 200.7 05/21/2015 09:33 MHALL30.005 1
Barium (Ba)0.010 mg/L EPA 200.7 05/21/2015 09:33 MHALL30.005 1
Boron (B)0.657 mg/L EPA 200.7 05/21/2015 09:33 MHALL30.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 05/21/2015 09:33 MHALL30.01 1
Manganese (Mn)0.027 mg/L EPA 200.7 05/21/2015 09:33 MHALL30.005 1
Strontium (Sr)0.105 mg/L EPA 200.7 05/21/2015 09:33 MHALL30.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 05/21/2015 09:33 MHALL30.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)13.4 mg/L EPA 200.7 05/21/2015 10:37 MHALL30.01 1
Magnesium (Mg)7.42 mg/L EPA 200.7 05/21/2015 10:37 MHALL30.005 1
Potassium (K)8.07 mg/L EPA 200.7 05/21/2015 10:37 MHALL30.1 1
Sodium (Na)166 mg/L EPA 200.7 05/21/2015 10:37 MHALL30.5 10
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.239 mg/L EPA 200.7 05/22/2015 11:39 MHALL30.005 1
Barium (Ba)0.009 mg/L EPA 200.7 05/22/2015 11:39 MHALL30.005 1
Boron (B)0.652 mg/L EPA 200.7 05/22/2015 11:39 MHALL30.05 1
Iron (Fe)0.316 mg/L EPA 200.7 05/22/2015 11:39 MHALL30.01 1
Manganese (Mn)0.027 mg/L EPA 200.7 05/22/2015 11:39 MHALL30.005 1
Strontium (Sr)0.101 mg/L EPA 200.7 05/22/2015 11:39 MHALL30.005 1
Zinc (Zn)0.013 mg/L EPA 200.7 05/22/2015 11:39 MHALL30.005 1
Analytical Lab
Page 4 of 56
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050565
2015015484
Collection Date: 18-May-15 3:00 PM
Site: AW-2D
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 06/04/2015 15:29 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 06/04/2015 15:29 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 06/04/2015 15:29 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 06/04/2015 15:29 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 06/04/2015 15:29 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 06/04/2015 15:29 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 06/04/2015 15:29 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 06/04/2015 15:29 JAHERMA11
Molybdenum (Mo)1.82 ug/L EPA 200.8 06/04/2015 15:29 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 06/04/2015 15:29 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 06/04/2015 15:29 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 06/04/2015 15:29 JAHERMA0.2 1
Vanadium (V) Low Level 0.522 ug/L EPA 200.8 06/04/2015 15:29 JAHERMA0.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 06/05/2015 12:41 SLS256011
Arsenic (As)< 1 ug/L EPA 200.8 06/05/2015 12:41 SLS256011
Beryllium (Be)< 1 ug/L EPA 200.8 06/05/2015 12:41 SLS256011
Cadmium (Cd)< 1 ug/L EPA 200.8 06/05/2015 12:41 SLS256011
Chromium (Cr)1.07 ug/L EPA 200.8 06/05/2015 12:41 SLS256011
Cobalt (Co)< 1 ug/L EPA 200.8 06/05/2015 12:41 SLS256011
Copper (Cu)< 1 ug/L EPA 200.8 06/05/2015 12:41 SLS256011
Lead (Pb)< 1 ug/L EPA 200.8 06/05/2015 12:41 SLS256011
Molybdenum (Mo)2.01 ug/L EPA 200.8 06/05/2015 12:41 SLS256011
Nickel (Ni)< 1 ug/L EPA 200.8 06/05/2015 12:41 SLS256011
Selenium (Se)< 1 ug/L EPA 200.8 06/05/2015 12:41 SLS256011
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 06/05/2015 12:41 SLS25600.2 1
Vanadium (V) Low Level 0.908 ug/L EPA 200.8 06/05/2015 12:41 SLS25600.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 500 mg/L SM2540C 05/21/2015 10:10 AGIBBS5251
Total Carbon
TOC 2.4 mg/L SM5310C/EPA9060A 05/27/2015 11:59 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 6.0 mg/L SM2540D 05/21/2015 09:09 AGIBBS551
Analytical Lab
Page 5 of 56
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050565
2015015485
Collection Date: 18-May-15 1:03 PM
Site: AW-5D
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 05/27/2015 13:02 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 90 mg/L EPA 300.0 05/22/2015 16:23 BGN9034110
Sulfate 24 mg/L EPA 300.0 05/22/2015 16:23 BGN9034110
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 05/28/2015 12:28 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 05/29/2015 13:55 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.022 mg/L EPA 200.7 05/21/2015 09:44 MHALL30.005 1
Barium (Ba)0.008 mg/L EPA 200.7 05/21/2015 09:44 MHALL30.005 1
Boron (B)0.282 mg/L EPA 200.7 05/21/2015 09:44 MHALL30.05 1
Iron (Fe)0.013 mg/L EPA 200.7 05/21/2015 09:44 MHALL30.01 1
Manganese (Mn)0.026 mg/L EPA 200.7 05/21/2015 09:44 MHALL30.005 1
Strontium (Sr)0.079 mg/L EPA 200.7 05/21/2015 09:44 MHALL30.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 05/21/2015 09:44 MHALL30.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)13.9 mg/L EPA 200.7 05/21/2015 10:34 MHALL30.01 1
Magnesium (Mg)5.93 mg/L EPA 200.7 05/21/2015 10:34 MHALL30.005 1
Potassium (K)6.65 mg/L EPA 200.7 05/21/2015 10:34 MHALL30.1 1
Sodium (Na)96.9 mg/L EPA 200.7 05/21/2015 10:34 MHALL30.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.413 mg/L EPA 200.7 05/22/2015 11:51 MHALL30.005 1
Barium (Ba)0.008 mg/L EPA 200.7 05/22/2015 11:51 MHALL30.005 1
Boron (B)0.296 mg/L EPA 200.7 05/22/2015 11:51 MHALL30.05 1
Iron (Fe)0.454 mg/L EPA 200.7 05/22/2015 11:51 MHALL30.01 1
Manganese (Mn)0.030 mg/L EPA 200.7 05/22/2015 11:51 MHALL30.005 1
Strontium (Sr)0.088 mg/L EPA 200.7 05/22/2015 11:51 MHALL30.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 05/22/2015 11:51 MHALL30.005 1
Analytical Lab
Page 6 of 56
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050565
2015015485
Collection Date: 18-May-15 1:03 PM
Site: AW-5D
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 06/04/2015 15:43 JAHERMA11
Arsenic (As)1.28 ug/L EPA 200.8 06/04/2015 15:43 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 06/04/2015 15:43 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 06/04/2015 15:43 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 06/04/2015 15:43 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 06/04/2015 15:43 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 06/04/2015 15:43 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 06/04/2015 15:43 JAHERMA11
Molybdenum (Mo)24.5 ug/L EPA 200.8 06/04/2015 15:43 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 06/04/2015 15:43 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 06/04/2015 15:43 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 06/04/2015 15:43 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 06/04/2015 15:43 JAHERMA0.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 06/05/2015 12:27 SLS256011
Arsenic (As)1.66 ug/L EPA 200.8 06/05/2015 12:27 SLS256011
Beryllium (Be)< 1 ug/L EPA 200.8 06/05/2015 12:27 SLS256011
Cadmium (Cd)< 1 ug/L EPA 200.8 06/05/2015 12:27 SLS256011
Chromium (Cr)1.24 ug/L EPA 200.8 06/05/2015 12:27 SLS256011
Cobalt (Co)< 1 ug/L EPA 200.8 06/05/2015 12:27 SLS256011
Copper (Cu)< 1 ug/L EPA 200.8 06/05/2015 12:27 SLS256011
Lead (Pb)< 1 ug/L EPA 200.8 06/05/2015 12:27 SLS256011
Molybdenum (Mo)28.1 ug/L EPA 200.8 06/05/2015 12:27 SLS256011
Nickel (Ni)< 1 ug/L EPA 200.8 06/05/2015 12:27 SLS256011
Selenium (Se)< 1 ug/L EPA 200.8 06/05/2015 12:27 SLS256011
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 06/05/2015 12:27 SLS25600.2 1
Vanadium (V) Low Level 0.910 ug/L EPA 200.8 06/05/2015 12:27 SLS25600.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 340 mg/L SM2540C 05/21/2015 10:10 AGIBBS5251
Total Carbon
TOC 1.7 mg/L SM5310C/EPA9060A 05/27/2015 11:59 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 8.0 mg/L SM2540D 05/21/2015 09:09 AGIBBS551
Analytical Lab
Page 7 of 56
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050565
2015015486
Collection Date: 19-May-15 11:25 AM
Site: AW-5E
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 05/27/2015 13:08 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 520 mg/L EPA 300.0 05/26/2015 12:59 BGN903410100
Sulfate 110 mg/L EPA 300.0 05/26/2015 12:59 BGN90342.5 25
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 05/28/2015 12:31 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 05/29/2015 14:04 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.007 mg/L EPA 200.7 05/21/2015 09:48 MHALL30.005 1
Barium (Ba)0.009 mg/L EPA 200.7 05/21/2015 09:48 MHALL30.005 1
Boron (B)1.97 mg/L EPA 200.7 05/21/2015 09:48 MHALL30.05 1
Iron (Fe)0.022 mg/L EPA 200.7 05/21/2015 09:48 MHALL30.01 1
Manganese (Mn)0.016 mg/L EPA 200.7 05/21/2015 09:48 MHALL30.005 1
Strontium (Sr)0.212 mg/L EPA 200.7 05/21/2015 09:48 MHALL30.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 05/21/2015 09:48 MHALL30.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)17.3 mg/L EPA 200.7 05/21/2015 10:41 MHALL30.01 1
Magnesium (Mg)13.4 mg/L EPA 200.7 05/21/2015 10:41 MHALL30.005 1
Potassium (K)28.9 mg/L EPA 200.7 05/21/2015 10:41 MHALL30.1 1
Sodium (Na)561 mg/L EPA 200.7 05/21/2015 10:41 MHALL30.5 10
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.362 mg/L EPA 200.7 05/22/2015 11:55 MHALL30.005 1
Barium (Ba)0.008 mg/L EPA 200.7 05/22/2015 11:55 MHALL30.005 1
Boron (B)1.90 mg/L EPA 200.7 05/22/2015 11:55 MHALL30.05 1
Iron (Fe)0.652 mg/L EPA 200.7 05/22/2015 11:55 MHALL30.01 1
Manganese (Mn)0.022 mg/L EPA 200.7 05/22/2015 11:55 MHALL30.005 1
Strontium (Sr)0.221 mg/L EPA 200.7 05/22/2015 11:55 MHALL30.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 05/22/2015 11:55 MHALL30.005 1
Analytical Lab
Page 8 of 56
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050565
2015015486
Collection Date: 19-May-15 11:25 AM
Site: AW-5E
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 06/04/2015 15:48 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 06/04/2015 15:48 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 06/04/2015 15:48 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 06/04/2015 15:48 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 06/04/2015 15:48 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 06/04/2015 15:48 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 06/04/2015 15:48 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 06/04/2015 15:48 JAHERMA11
Molybdenum (Mo)16.0 ug/L EPA 200.8 06/04/2015 15:48 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 06/04/2015 15:48 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 06/04/2015 15:48 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 06/04/2015 15:48 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 06/04/2015 15:48 JAHERMA0.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 06/05/2015 12:45 SLS256011
Arsenic (As)1.25 ug/L EPA 200.8 06/05/2015 12:45 SLS256011
Beryllium (Be)< 1 ug/L EPA 200.8 06/05/2015 12:45 SLS256011
Cadmium (Cd)< 1 ug/L EPA 200.8 06/05/2015 12:45 SLS256011
Chromium (Cr)1.61 ug/L EPA 200.8 06/05/2015 12:45 SLS256011
Cobalt (Co)< 1 ug/L EPA 200.8 06/05/2015 12:45 SLS256011
Copper (Cu)< 1 ug/L EPA 200.8 06/05/2015 12:45 SLS256011
Lead (Pb)< 1 ug/L EPA 200.8 06/05/2015 12:45 SLS256011
Molybdenum (Mo)15.9 ug/L EPA 200.8 06/05/2015 12:45 SLS256011
Nickel (Ni)< 1 ug/L EPA 200.8 06/05/2015 12:45 SLS256011
Selenium (Se)< 1 ug/L EPA 200.8 06/05/2015 12:45 SLS256011
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 06/05/2015 12:45 SLS25600.2 1
Vanadium (V) Low Level 0.630 ug/L EPA 200.8 06/05/2015 12:45 SLS25600.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 1500 mg/L SM2540C 05/21/2015 10:10 AGIBBS5251
Total Carbon
TOC 3.5 mg/L SM5310C/EPA9060A 05/27/2015 11:59 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 64 mg/L SM2540D 05/21/2015 09:09 AGIBBS551
Analytical Lab
Page 9 of 56
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050565
2015015487
Collection Date: 19-May-15 8:40 AM
Site: AW-9D
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 05/27/2015 13:12 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride 210 mg/L EPA 300.0 05/26/2015 13:15 BGN90342.5 25
Sulfate 50 mg/L EPA 300.0 05/26/2015 13:15 BGN9034110
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 05/28/2015 12:33 ACPAYNE0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 05/29/2015 14:06 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.009 mg/L EPA 200.7 05/21/2015 09:52 MHALL30.005 1
Barium (Ba)0.006 mg/L EPA 200.7 05/21/2015 09:52 MHALL30.005 1
Boron (B)0.539 mg/L EPA 200.7 05/21/2015 09:52 MHALL30.05 1
Iron (Fe)0.069 mg/L EPA 200.7 05/21/2015 09:52 MHALL30.01 1
Manganese (Mn)0.031 mg/L EPA 200.7 05/21/2015 09:52 MHALL30.005 1
Strontium (Sr)0.122 mg/L EPA 200.7 05/21/2015 09:52 MHALL30.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 05/21/2015 09:52 MHALL30.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)17.0 mg/L EPA 200.7 05/21/2015 10:45 MHALL30.01 1
Magnesium (Mg)9.36 mg/L EPA 200.7 05/21/2015 10:45 MHALL30.005 1
Potassium (K)10.2 mg/L EPA 200.7 05/21/2015 10:45 MHALL30.1 1
Sodium (Na)209 mg/L EPA 200.7 05/21/2015 10:45 MHALL30.5 10
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.212 mg/L EPA 200.7 05/22/2015 11:59 MHALL30.005 1
Barium (Ba)0.007 mg/L EPA 200.7 05/22/2015 11:59 MHALL30.005 1
Boron (B)0.577 mg/L EPA 200.7 05/22/2015 11:59 MHALL30.05 1
Iron (Fe)0.393 mg/L EPA 200.7 05/22/2015 11:59 MHALL30.01 1
Manganese (Mn)0.034 mg/L EPA 200.7 05/22/2015 11:59 MHALL30.005 1
Strontium (Sr)0.133 mg/L EPA 200.7 05/22/2015 11:59 MHALL30.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 05/22/2015 11:59 MHALL30.005 1
Analytical Lab
Page 10 of 56
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050565
2015015487
Collection Date: 19-May-15 8:40 AM
Site: AW-9D
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 06/04/2015 15:52 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 06/04/2015 15:52 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 06/04/2015 15:52 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 06/04/2015 15:52 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 06/04/2015 15:52 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 06/04/2015 15:52 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 06/04/2015 15:52 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 06/04/2015 15:52 JAHERMA11
Molybdenum (Mo)8.49 ug/L EPA 200.8 06/04/2015 15:52 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 06/04/2015 15:52 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 06/04/2015 15:52 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 06/04/2015 15:52 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 06/04/2015 15:52 JAHERMA0.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 06/05/2015 12:50 SLS256011
Arsenic (As)< 1 ug/L EPA 200.8 06/05/2015 12:50 SLS256011
Beryllium (Be)< 1 ug/L EPA 200.8 06/05/2015 12:50 SLS256011
Cadmium (Cd)< 1 ug/L EPA 200.8 06/05/2015 12:50 SLS256011
Chromium (Cr)< 1 ug/L EPA 200.8 06/05/2015 12:50 SLS256011
Cobalt (Co)< 1 ug/L EPA 200.8 06/05/2015 12:50 SLS256011
Copper (Cu)< 1 ug/L EPA 200.8 06/05/2015 12:50 SLS256011
Lead (Pb)< 1 ug/L EPA 200.8 06/05/2015 12:50 SLS256011
Molybdenum (Mo)8.54 ug/L EPA 200.8 06/05/2015 12:50 SLS256011
Nickel (Ni)< 1 ug/L EPA 200.8 06/05/2015 12:50 SLS256011
Selenium (Se)< 1 ug/L EPA 200.8 06/05/2015 12:50 SLS256011
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 06/05/2015 12:50 SLS25600.2 1
Vanadium (V) Low Level 0.362 ug/L EPA 200.8 06/05/2015 12:50 SLS25600.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 610 mg/L SM2540C 05/21/2015 10:10 AGIBBS5251
Total Carbon
TOC 2.6 mg/L SM5310C/EPA9060A 05/27/2015 11:59 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS 7.0 mg/L SM2540D 05/21/2015 09:09 AGIBBS551
Analytical Lab
Page 11 of 56
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050565
2015015488
Collection Date: 18-May-15 10:45 AM
Site: Equipment Blank
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 05/27/2015 13:13 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride < 0.1 mg/L EPA 300.0 05/22/2015 14:59 BGN90340.1 1
Sulfate < 0.1 mg/L EPA 300.0 05/22/2015 14:59 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 05/28/2015 12:35 ACPAYNE0.05 1
UNDIGESTED METALS BY ICP
Calcium (Ca)0.011 mg/L EPA 200.7 05/21/2015 11:18 MHALL30.01 1
Magnesium (Mg)< 0.005 mg/L EPA 200.7 05/21/2015 11:18 MHALL30.005 1
Potassium (K)< 0.1 mg/L EPA 200.7 05/21/2015 11:18 MHALL30.1 1
Sodium (Na)< 0.05 mg/L EPA 200.7 05/21/2015 11:18 MHALL30.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 05/22/2015 12:03 MHALL30.005 1
Barium (Ba)< 0.005 mg/L EPA 200.7 05/22/2015 12:03 MHALL30.005 1
Boron (B)< 0.05 mg/L EPA 200.7 05/22/2015 12:03 MHALL30.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 05/22/2015 12:03 MHALL30.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 05/22/2015 12:03 MHALL30.005 1
Strontium (Sr)< 0.005 mg/L EPA 200.7 05/22/2015 12:03 MHALL30.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 05/22/2015 12:03 MHALL30.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 06/05/2015 12:54 SLS256011
Arsenic (As)< 1 ug/L EPA 200.8 06/05/2015 12:54 SLS256011
Beryllium (Be)< 1 ug/L EPA 200.8 06/05/2015 12:54 SLS256011
Cadmium (Cd)< 1 ug/L EPA 200.8 06/05/2015 12:54 SLS256011
Chromium (Cr)< 1 ug/L EPA 200.8 06/05/2015 12:54 SLS256011
Cobalt (Co)< 1 ug/L EPA 200.8 06/05/2015 12:54 SLS256011
Copper (Cu)< 1 ug/L EPA 200.8 06/05/2015 12:54 SLS256011
Lead (Pb)< 1 ug/L EPA 200.8 06/05/2015 12:54 SLS256011
Molybdenum (Mo)< 1 ug/L EPA 200.8 06/05/2015 12:54 SLS256011
Nickel (Ni)< 1 ug/L EPA 200.8 06/05/2015 12:54 SLS256011
Selenium (Se)< 1 ug/L EPA 200.8 06/05/2015 12:54 SLS256011
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 06/05/2015 12:54 SLS25600.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 06/05/2015 12:54 SLS25600.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
Analytical Lab
Page 12 of 56
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050565
2015015488
Collection Date: 18-May-15 10:45 AM
Site: Equipment Blank
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L SM2540C 05/21/2015 10:10 AGIBBS5251
Total Carbon
TOC 0.410 mg/L SM5310C/EPA9060A 05/27/2015 11:59 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 05/21/2015 09:09 AGIBBS551
Analytical Lab
Page 13 of 56
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050565
2015015489
Collection Date: 19-May-15 8:40 AM
Site: Equipment Blank
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 05/27/2015 13:14 LSTARL10.01 1
INORGANIC IONS BY IC
Chloride < 0.1 mg/L EPA 300.0 05/22/2015 15:15 BGN90340.1 1
Sulfate < 0.1 mg/L EPA 300.0 05/22/2015 15:15 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 05/28/2015 12:38 ACPAYNE0.05 1
UNDIGESTED METALS BY ICP
Calcium (Ca)0.021 mg/L EPA 200.7 05/21/2015 11:21 MHALL30.01 1
Magnesium (Mg)< 0.005 mg/L EPA 200.7 05/21/2015 11:21 MHALL30.005 1
Potassium (K)< 0.1 mg/L EPA 200.7 05/21/2015 11:21 MHALL30.1 1
Sodium (Na)< 0.05 mg/L EPA 200.7 05/21/2015 11:21 MHALL30.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 05/22/2015 12:07 MHALL30.005 1
Barium (Ba)< 0.005 mg/L EPA 200.7 05/22/2015 12:07 MHALL30.005 1
Boron (B)< 0.05 mg/L EPA 200.7 05/22/2015 12:07 MHALL30.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 05/22/2015 12:07 MHALL30.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 05/22/2015 12:07 MHALL30.005 1
Strontium (Sr)< 0.005 mg/L EPA 200.7 05/22/2015 12:07 MHALL30.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 05/22/2015 12:07 MHALL30.005 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 06/05/2015 13:12 SLS256011
Arsenic (As)< 1 ug/L EPA 200.8 06/05/2015 13:12 SLS256011
Beryllium (Be)< 1 ug/L EPA 200.8 06/05/2015 13:12 SLS256011
Cadmium (Cd)< 1 ug/L EPA 200.8 06/05/2015 13:12 SLS256011
Chromium (Cr)< 1 ug/L EPA 200.8 06/05/2015 13:12 SLS256011
Cobalt (Co)< 1 ug/L EPA 200.8 06/05/2015 13:12 SLS256011
Copper (Cu)< 1 ug/L EPA 200.8 06/05/2015 13:12 SLS256011
Lead (Pb)< 1 ug/L EPA 200.8 06/05/2015 13:12 SLS256011
Molybdenum (Mo)< 1 ug/L EPA 200.8 06/05/2015 13:12 SLS256011
Nickel (Ni)< 1 ug/L EPA 200.8 06/05/2015 13:12 SLS256011
Selenium (Se)< 1 ug/L EPA 200.8 06/05/2015 13:12 SLS256011
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 06/05/2015 13:12 SLS25600.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 06/05/2015 13:12 SLS25600.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
Analytical Lab
Page 14 of 56
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050565
2015015489
Collection Date: 19-May-15 8:40 AM
Site: Equipment Blank
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L SM2540C 05/21/2015 10:10 AGIBBS5251
Total Carbon
TOC 0.414 mg/L SM5310C/EPA9060A 05/27/2015 11:59 GHUTCHI0.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 05/21/2015 09:09 AGIBBS551
Analytical Lab
Page 15 of 56
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050565
2015015490
Collection Date: 18-May-15 10:45 AM
Site: Filter Blank
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 05/29/2015 14:09 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 05/21/2015 09:57 MHALL30.005 1
Barium (Ba)< 0.005 mg/L EPA 200.7 05/21/2015 09:57 MHALL30.005 1
Boron (B)< 0.05 mg/L EPA 200.7 05/21/2015 09:57 MHALL30.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 05/21/2015 09:57 MHALL30.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 05/21/2015 09:57 MHALL30.005 1
Strontium (Sr)< 0.005 mg/L EPA 200.7 05/21/2015 09:57 MHALL30.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 05/21/2015 09:57 MHALL30.005 1
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 06/04/2015 12:57 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 06/04/2015 12:57 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 06/04/2015 12:57 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 06/04/2015 12:57 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 06/04/2015 12:57 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 06/04/2015 12:57 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 06/04/2015 12:57 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 06/04/2015 12:57 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 06/04/2015 12:57 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 06/04/2015 12:57 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 06/04/2015 12:57 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 06/04/2015 12:57 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 06/04/2015 12:57 JAHERMA0.3 1
Analytical Lab
Page 16 of 56
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050565
2015015491
Collection Date: 19-May-15 8:40 AM
Site: Filter Blank
Matrix: GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 05/29/2015 14:11 ACPAYNE0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 05/21/2015 10:01 MHALL30.005 1
Barium (Ba)< 0.005 mg/L EPA 200.7 05/21/2015 10:01 MHALL30.005 1
Boron (B)< 0.05 mg/L EPA 200.7 05/21/2015 10:01 MHALL30.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 05/21/2015 10:01 MHALL30.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 05/21/2015 10:01 MHALL30.005 1
Strontium (Sr)< 0.005 mg/L EPA 200.7 05/21/2015 10:01 MHALL30.005 1
Zinc (Zn)0.005 mg/L EPA 200.7 05/21/2015 10:01 MHALL30.005 1
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 06/04/2015 13:01 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 06/04/2015 13:01 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 06/04/2015 13:01 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 06/04/2015 13:01 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 06/04/2015 13:01 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 06/04/2015 13:01 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 06/04/2015 13:01 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 06/04/2015 13:01 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 06/04/2015 13:01 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 06/04/2015 13:01 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 06/04/2015 13:01 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 06/04/2015 13:01 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 06/04/2015 13:01 JAHERMA0.3 1
Analytical Lab
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SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
QE22017Lot Number:
J15050565Project Number:
AB GW Assessment Water - SuttonProject Name:
05/29/2015Date Completed:
Grant Wilton
Project Manager
*QE22017*

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Duke Energy
Lot Number: QE22017
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
Project Name: AB GW Assessment Water - Sutton
Project Number: J15050565
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Page: 2 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QE22017

Project Name: AB GW Assessment Water - Sutton
Project Number: J15050565
Sample Number Sample ID Matrix Date Sampled Date Received
001 05/18/2015 15002015015484Aqueous 05/22/2015
002 05/18/2015 13052015015485Aqueous 05/22/2015
003 05/19/2015 11252015015486Aqueous 05/22/2015
004 05/19/2015 08402015015487Aqueous 05/22/2015
005 05/18/2015 10452015015488Aqueous 05/22/2015
006 05/19/2015 08402015015489Aqueous 05/22/2015
(6 samples)
Page: 3 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QE22017

Project Name: AB GW Assessment Water - Sutton
Project Number: J15050565
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 2015015484 Aqueous Alkalinity SM 2320B-170 mg/L 5
001 2015015484 Aqueous Bicarbonate Alkalinity SM 2320B-170 mg/L 5
002 2015015485 Aqueous Alkalinity SM 2320B-110 mg/L 7
002 2015015485 Aqueous Bicarbonate Alkalinity SM 2320B-110 mg/L 7
003 2015015486 Aqueous Alkalinity SM 2320B-350 mg/L 9
003 2015015486 Aqueous Bicarbonate Alkalinity SM 2320B-350 mg/L 9
004 2015015487 Aqueous Alkalinity SM 2320B-160 mg/L 11
004 2015015487 Aqueous Bicarbonate Alkalinity SM 2320B-160 mg/L 11
(8 detections)
Page: 4 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015015484
QE22017-001
05/18/2015 1500
05/22/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15050565
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/27/2015 2209 HMA 75907
1 (Bicarbonate ) SM 2320B-2011 1 05/28/2015 2209 HMA
1 (Carbonate Al) SM 2320B-2011 1 05/28/2015 2209 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 170 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 170 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 5 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015015484
QE22017-001
05/18/2015 1500
05/22/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15050565
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/26/2015 2311 JJG 75816
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015015485
QE22017-002
05/18/2015 1305
05/22/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15050565
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/27/2015 2215 HMA 75907
1 (Bicarbonate ) SM 2320B-2011 1 05/28/2015 2215 HMA
1 (Carbonate Al) SM 2320B-2011 1 05/28/2015 2215 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 110 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 110 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015015485
QE22017-002
05/18/2015 1305
05/22/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15050565
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/26/2015 2327 JJG 75816
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015015486
QE22017-003
05/19/2015 1125
05/22/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15050565
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/27/2015 2223 HMA 75907
1 (Bicarbonate ) SM 2320B-2011 1 05/28/2015 2223 HMA
1 (Carbonate Al) SM 2320B-2011 1 05/28/2015 2223 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 350 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 350 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015015486
QE22017-003
05/19/2015 1125
05/22/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15050565
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/26/2015 2342 JJG 75816
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015015487
QE22017-004
05/19/2015 0840
05/22/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15050565
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/27/2015 2241 HMA 75907
1 (Bicarbonate ) SM 2320B-2011 1 05/28/2015 2241 HMA
1 (Carbonate Al) SM 2320B-2011 1 05/28/2015 2241 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 160 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 160 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015015487
QE22017-004
05/19/2015 0840
05/22/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15050565
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/26/2015 2352 JJG 75816
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015015488
QE22017-005
05/18/2015 1045
05/22/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15050565
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/27/2015 2245 HMA 75907
1 (Bicarbonate ) SM 2320B-2011 1 05/28/2015 2245 HMA
1 (Carbonate Al) SM 2320B-2011 1 05/28/2015 2245 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 ND 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 ND 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015015488
QE22017-005
05/18/2015 1045
05/22/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15050565
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/27/2015 1056 DCS 75869
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 14 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015015489
QE22017-006
05/19/2015 0840
05/22/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15050565
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 05/27/2015 2250 HMA 75907
1 (Bicarbonate ) SM 2320B-2011 1 05/28/2015 2250 HMA
1 (Carbonate Al) SM 2320B-2011 1 05/28/2015 2250 HMA
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 ND 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 ND 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 15 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015015489
QE22017-006
05/19/2015 0840
05/22/2015
Aqueous
Project Name: AB GW Assessment Water -
Project Number: J15050565
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 05/27/2015 1107 DCS 75869
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 16 of 16
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
QC Summary
QC Data for Lot Number: QE22017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - MB
Batch:
Sample ID:QQ75907-001
75907
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Alkalinity ND 05/27/2015 212410mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QE22017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - LCS
Batch:
Sample ID:QQ75907-002
75907
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Alkalinity 90 05/27/2015 21309010090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QE22017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane - MB
Batch:
Sample ID:QQ75816-001
75816
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Methane ND 05/26/2015 202110ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QE22017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane - LCS
Batch:
Sample ID:QQ75816-002
75816
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Methane 140 05/26/2015 19519415070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QE22017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane - LCSD
Batch:
Sample ID:QQ75816-003
75816
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Methane 140 05/26/2015 20049315070-1301.5 301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QE22017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane - MB
Batch:
Sample ID:QQ75869-001
75869
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Methane ND 05/27/2015 103810ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QE22017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane - LCS
Batch:
Sample ID:QQ75869-002
75869
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Methane 120 05/27/2015 10177715070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QE22017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane - LCSD
Batch:
Sample ID:QQ75869-003
75869
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Methane 130 05/27/2015 10278815070-13013 301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QE22017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Analytical Lab
Page 56 of 56