NC0001422_ATT 5 - Water - J15020166report_20150805

13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Analytical Laboratory
Order Number:J15020166
Project Name:AB GW ASSESSMENT WATER
Lab Contact:Mary Ann Ogle
Date:2/23/2015
Customer Address:
Customer Name(s):Perry Waldrep, Tim Hunsucker, Kathy Webb, John Toepfer
Phone: [phone]
Report Authorized By:
(Signature)
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub-contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.
Mary Ann Ogle
Page 1 of 53
Sample ID's & Descriptions:
Sample ID Plant/Station
Collection
Date and Time Collected By Sample Description
2015003048 Sutton 05-Feb-15 9:20 AM ILLEGIBLE AW-4C
2015003049 Sutton 05-Feb-15 11:05 AM ILLEGIBLE AW-4B
2015003050 Sutton 05-Feb-15 12:15 PM ILLEGIBLE Source Water
2015003051 Sutton 05-Feb-15 1:10 PM ILLEGIBLE AW-6D
2015003052 Sutton 05-Feb-15 1:50 PM ILLEGIBLE AW-6B
2015003053 Sutton 05-Feb-15 3:20 PM ILLEGIBLE AW-3C
2015003054 Sutton 05-Feb-15 5:05 PM ILLEGIBLE AW-3B
2015003055 Sutton 05-Feb-15 4:55 PM ILLEGIBLE AW-2C
2015003056 Sutton 05-Feb-15 9:10 AM ILLEGIBLE Filter Blank
9 Total Samples
Page 2 of 53
COC and .pdf report are in agreement with sample totals
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits.
All laboratory QA/QC requirements are acceptable.
Yes No
Technical Validation Review
Checklist:
Yes No
Yes No
Report Sections Included:
Job Summary Report Sub-contracted Laboratory Results
Sample Identification Customer Specific Data Sheets, Reports, & Documentation
Technical Validation of Data Package Customer Database Entries
Analytical Laboratory Certificate of Analysis
Analytical Laboratory QC Report
Chain of Custody
Reviewed By:DBA Account Date:2/23/2015
Electronic Data Deliverable (EDD) Sent Separately
Page 3 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003048
Collection Date:05-Feb-15 9:20 AM
Site:AW-4C
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.030 mg-N/L EPA 353.2 02/14/2015 12:04 TLINN0.02 2
INORGANIC IONS BY IC
Chloride 37 mg/L EPA 300.0 02/09/2015 08:42 BGN90340.5 5
Sulfate 110 mg/L EPA 300.0 02/09/2015 08:42 BGN90342.5 25
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/12/2015 10:58 TLINN0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/18/2015 20:06 TLINN0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.026 mg/L EPA 200.7 02/09/2015 13:37 MHH71310.005 1
Barium (Ba)0.076 mg/L EPA 200.7 02/09/2015 13:37 MHH71310.005 1
Boron (B)1.15 mg/L EPA 200.7 02/09/2015 13:37 MHH71310.05 1
Iron (Fe)12.4 mg/L EPA 200.7 02/09/2015 13:37 MHH71310.01 1
Manganese (Mn)1.17 mg/L EPA 200.7 02/09/2015 13:37 MHH71310.005 1
Strontium (Sr)0.678 mg/L EPA 200.7 02/09/2015 13:37 MHH71310.005 1
Zinc (Zn)0.042 mg/L EPA 200.7 02/09/2015 13:37 MHH71310.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)48.4 mg/L EPA 200.7 02/11/2015 15:43 MHALL30.1 10
Magnesium (Mg)5.30 mg/L EPA 200.7 02/11/2015 15:43 MHALL30.005 1
Potassium (K)6.07 mg/L EPA 200.7 02/11/2015 15:43 MHALL30.1 1
Sodium (Na)32.7 mg/L EPA 200.7 02/11/2015 15:43 MHALL30.5 10
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.101 mg/L EPA 200.7 02/09/2015 12:13 MHH71310.005 1
Barium (Ba)0.080 mg/L EPA 200.7 02/09/2015 12:13 MHH71310.005 1
Boron (B)1.16 mg/L EPA 200.7 02/09/2015 12:13 MHH71310.05 1
Iron (Fe)15.1 mg/L EPA 200.7 02/09/2015 12:13 MHH71310.01 1
Manganese (Mn)1.27 mg/L EPA 200.7 02/09/2015 12:13 MHH71310.005 1
Strontium (Sr)0.672 mg/L EPA 200.7 02/09/2015 12:13 MHH71310.005 1
Zinc (Zn)0.064 mg/L EPA 200.7 02/09/2015 12:13B2 MHH71310.005 1
Page 4 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003048
Collection Date:05-Feb-15 9:20 AM
Site:AW-4C
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/11/2015 13:18 DJSULL111
Arsenic (As)< 1 ug/L EPA 200.8 02/11/2015 13:18 DJSULL111
Beryllium (Be)< 1 ug/L EPA 200.8 02/11/2015 13:18 DJSULL111
Cadmium (Cd)< 1 ug/L EPA 200.8 02/11/2015 13:18 DJSULL111
Chromium (Cr)< 1 ug/L EPA 200.8 02/11/2015 13:18 DJSULL111
Cobalt (Co)24.8 ug/L EPA 200.8 02/11/2015 13:18 DJSULL111
Copper (Cu)< 1 ug/L EPA 200.8 02/11/2015 13:18 DJSULL111
Lead (Pb)< 1 ug/L EPA 200.8 02/11/2015 13:18 DJSULL111
Molybdenum (Mo)2.19 ug/L EPA 200.8 02/11/2015 13:18 DJSULL111
Nickel (Ni)< 1 ug/L EPA 200.8 02/11/2015 13:18 DJSULL111
Selenium (Se)< 1 ug/L EPA 200.8 02/11/2015 13:18 DJSULL111
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/11/2015 13:18 DJSULL10.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/11/2015 13:18 DJSULL10.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/14/2015 15:05 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 02/14/2015 15:05 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 02/14/2015 15:05 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 02/14/2015 15:05 JAHERMA11
Chromium (Cr)1.16 ug/L EPA 200.8 02/14/2015 15:05 JAHERMA11
Cobalt (Co)24.5 ug/L EPA 200.8 02/14/2015 15:05 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 02/14/2015 15:05 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 02/14/2015 15:05 JAHERMA11
Molybdenum (Mo)2.30 ug/L EPA 200.8 02/14/2015 15:05 JAHERMA11
Nickel (Ni)1.47 ug/L EPA 200.8 02/14/2015 15:05 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 02/14/2015 15:05 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/14/2015 15:05 JAHERMA0.2 1
Vanadium (V) Low Level 0.850 ug/L EPA 200.8 02/14/2015 15:05 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 300 mg/L SM2540C 02/11/2015 16:38 GHUTCHI251
Total Carbon
TOC 3.9 mg/L SM5310C/EPA9060A 02/12/2015 15:45 TJA70670.1 1
TOTAL SUSPENDED SOLIDS
TSS 26 mg/L SM2540D 02/10/2015 13:42 GHUTCHI51
Page 5 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003049
Collection Date:05-Feb-15 11:05 AM
Site:AW-4B
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.016 mg-N/L EPA 353.2 02/14/2015 11:56 TLINN0.01 1
INORGANIC IONS BY IC
Chloride 4.4 mg/L EPA 300.0 02/06/2015 20:52 BGN90340.1 1
Sulfate 4.7 mg/L EPA 300.0 02/06/2015 20:52 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/12/2015 11:00 TLINN0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/18/2015 20:08 TLINN0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.006 mg/L EPA 200.7 02/09/2015 14:00 MHH71310.005 1
Barium (Ba)0.019 mg/L EPA 200.7 02/09/2015 14:00 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 02/09/2015 14:00 MHH71310.05 1
Iron (Fe)2.28 mg/L EPA 200.7 02/09/2015 14:00 MHH71310.01 1
Manganese (Mn)0.223 mg/L EPA 200.7 02/09/2015 14:00 MHH71310.005 1
Strontium (Sr)0.022 mg/L EPA 200.7 02/09/2015 14:00 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 02/09/2015 14:00 MHH71310.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)7.15 mg/L EPA 200.7 02/11/2015 15:56 MHALL30.01 1
Magnesium (Mg)0.656 mg/L EPA 200.7 02/11/2015 15:56 MHALL30.005 1
Potassium (K)1.09 mg/L EPA 200.7 02/11/2015 15:56 MHALL30.1 1
Sodium (Na)2.86 mg/L EPA 200.7 02/11/2015 15:56 MHALL30.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.036 mg/L EPA 200.7 02/09/2015 12:01 MHH71310.005 1
Barium (Ba)0.021 mg/L EPA 200.7 02/09/2015 12:01 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 02/09/2015 12:01 MHH71310.05 1
Iron (Fe)2.60 mg/L EPA 200.7 02/09/2015 12:01 MHH71310.01 1
Manganese (Mn)0.232 mg/L EPA 200.7 02/09/2015 12:01 MHH71310.005 1
Strontium (Sr)0.023 mg/L EPA 200.7 02/09/2015 12:01 MHH71310.005 1
Zinc (Zn)0.008 mg/L EPA 200.7 02/09/2015 12:01B2 MHH71310.005 1
Page 6 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003049
Collection Date:05-Feb-15 11:05 AM
Site:AW-4B
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/11/2015 13:33 DJSULL111
Arsenic (As)< 1 ug/L EPA 200.8 02/11/2015 13:33 DJSULL111
Beryllium (Be)< 1 ug/L EPA 200.8 02/11/2015 13:33 DJSULL111
Cadmium (Cd)< 1 ug/L EPA 200.8 02/11/2015 13:33 DJSULL111
Chromium (Cr)< 1 ug/L EPA 200.8 02/11/2015 13:33 DJSULL111
Cobalt (Co)1.48 ug/L EPA 200.8 02/11/2015 13:33 DJSULL111
Copper (Cu)< 1 ug/L EPA 200.8 02/11/2015 13:33 DJSULL111
Lead (Pb)< 1 ug/L EPA 200.8 02/11/2015 13:33 DJSULL111
Molybdenum (Mo)4.37 ug/L EPA 200.8 02/11/2015 13:33 DJSULL111
Nickel (Ni)< 1 ug/L EPA 200.8 02/11/2015 13:33 DJSULL111
Selenium (Se)< 1 ug/L EPA 200.8 02/11/2015 13:33 DJSULL111
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/11/2015 13:33 DJSULL10.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/11/2015 13:33 DJSULL10.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/14/2015 15:16 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 02/14/2015 15:16 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 02/14/2015 15:16 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 02/14/2015 15:16 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 02/14/2015 15:16 JAHERMA11
Cobalt (Co)1.39 ug/L EPA 200.8 02/14/2015 15:16 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 02/14/2015 15:16 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 02/14/2015 15:16 JAHERMA11
Molybdenum (Mo)4.01 ug/L EPA 200.8 02/14/2015 15:16 JAHERMA11
Nickel (Ni)1.29 ug/L EPA 200.8 02/14/2015 15:16 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 02/14/2015 15:16 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/14/2015 15:16 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/14/2015 15:16 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 43 mg/L SM2540C 02/11/2015 16:38 GHUTCHI251
Total Carbon
TOC 1.1 mg/L SM5310C/EPA9060A 02/12/2015 15:45 TJA70670.1 1
TOTAL SUSPENDED SOLIDS
TSS 8.0 mg/L SM2540D 02/10/2015 13:42 GHUTCHI51
Page 7 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003050
Collection Date:05-Feb-15 12:15 PM
Site:Source Water
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 02/14/2015 11:59 TLINN0.01 1
INORGANIC IONS BY IC
Chloride 8.8 mg/L EPA 300.0 02/06/2015 21:08 BGN90340.1 1
Sulfate 1.1 mg/L EPA 300.0 02/06/2015 21:08 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/12/2015 11:02 TLINN0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/18/2015 20:11 TLINN0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.007 mg/L EPA 200.7 02/09/2015 14:09 MHH71310.005 1
Barium (Ba)< 0.005 mg/L EPA 200.7 02/09/2015 14:09 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 02/09/2015 14:09 MHH71310.05 1
Iron (Fe)0.150 mg/L EPA 200.7 02/09/2015 14:09 MHH71310.01 1
Manganese (Mn)0.008 mg/L EPA 200.7 02/09/2015 14:09 MHH71310.005 1
Strontium (Sr)0.046 mg/L EPA 200.7 02/09/2015 14:09 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 02/09/2015 14:09 MHH71310.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)15.3 mg/L EPA 200.7 02/11/2015 16:00 MHALL30.01 1
Magnesium (Mg)1.23 mg/L EPA 200.7 02/11/2015 16:00 MHALL30.005 1
Potassium (K)0.853 mg/L EPA 200.7 02/11/2015 16:00 MHALL30.1 1
Sodium (Na)9.44 mg/L EPA 200.7 02/11/2015 16:00 MHALL30.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.020 mg/L EPA 200.7 02/09/2015 12:17 MHH71310.005 1
Barium (Ba)< 0.005 mg/L EPA 200.7 02/09/2015 12:17 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 02/09/2015 12:17 MHH71310.05 1
Iron (Fe)0.963 mg/L EPA 200.7 02/09/2015 12:17 MHH71310.01 1
Manganese (Mn)0.013 mg/L EPA 200.7 02/09/2015 12:17 MHH71310.005 1
Strontium (Sr)0.047 mg/L EPA 200.7 02/09/2015 12:17 MHH71310.005 1
Zinc (Zn)0.008 mg/L EPA 200.7 02/09/2015 12:17B2 MHH71310.005 1
Page 8 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003050
Collection Date:05-Feb-15 12:15 PM
Site:Source Water
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/11/2015 13:38 DJSULL111
Arsenic (As)< 1 ug/L EPA 200.8 02/11/2015 13:38 DJSULL111
Beryllium (Be)< 1 ug/L EPA 200.8 02/11/2015 13:38 DJSULL111
Cadmium (Cd)< 1 ug/L EPA 200.8 02/11/2015 13:38 DJSULL111
Chromium (Cr)< 1 ug/L EPA 200.8 02/11/2015 13:38 DJSULL111
Cobalt (Co)< 1 ug/L EPA 200.8 02/11/2015 13:38 DJSULL111
Copper (Cu)< 1 ug/L EPA 200.8 02/11/2015 13:38 DJSULL111
Lead (Pb)< 1 ug/L EPA 200.8 02/11/2015 13:38 DJSULL111
Molybdenum (Mo)< 1 ug/L EPA 200.8 02/11/2015 13:38 DJSULL111
Nickel (Ni)< 1 ug/L EPA 200.8 02/11/2015 13:38 DJSULL111
Selenium (Se)< 1 ug/L EPA 200.8 02/11/2015 13:38 DJSULL111
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/11/2015 13:38 DJSULL10.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/11/2015 13:38 DJSULL10.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/14/2015 15:32 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 02/14/2015 15:32 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 02/14/2015 15:32 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 02/14/2015 15:32 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 02/14/2015 15:32 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 02/14/2015 15:32 JAHERMA11
Copper (Cu)1.58 ug/L EPA 200.8 02/14/2015 15:32 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 02/14/2015 15:32 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 02/14/2015 15:32 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 02/14/2015 15:32 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 02/14/2015 15:32 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/14/2015 15:32 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/14/2015 15:32 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 75 mg/L SM2540C 02/11/2015 16:38 GHUTCHI251
Total Carbon
TOC 0.794 mg/L SM5310C/EPA9060A 02/12/2015 15:45 TJA70670.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 02/10/2015 13:42 GHUTCHI51
Page 9 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003051
Collection Date:05-Feb-15 1:10 PM
Site:AW-6D
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)< 0.01 mg-N/L EPA 353.2 02/14/2015 12:00 TLINN0.01 1
INORGANIC IONS BY IC
Chloride 170 mg/L EPA 300.0 02/09/2015 08:58 BGN9034550
Sulfate 43 mg/L EPA 300.0 02/09/2015 08:58 BGN90340.5 5
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/12/2015 11:05 TLINN0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/18/2015 20:13 TLINN0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.025 mg/L EPA 200.7 02/09/2015 14:17 MHH71310.005 1
Barium (Ba)0.015 mg/L EPA 200.7 02/09/2015 14:17 MHH71310.005 1
Boron (B)0.890 mg/L EPA 200.7 02/09/2015 14:17 MHH71310.05 1
Iron (Fe)0.065 mg/L EPA 200.7 02/09/2015 14:17 MHH71310.01 1
Manganese (Mn)0.015 mg/L EPA 200.7 02/09/2015 14:17 MHH71310.005 1
Strontium (Sr)0.070 mg/L EPA 200.7 02/09/2015 14:17 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 02/09/2015 14:17 MHH71310.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)6.77 mg/L EPA 200.7 02/11/2015 16:04 MHALL30.01 1
Magnesium (Mg)3.68 mg/L EPA 200.7 02/11/2015 16:04 MHALL30.005 1
Potassium (K)7.01 mg/L EPA 200.7 02/11/2015 16:04 MHALL30.1 1
Sodium (Na)248 mg/L EPA 200.7 02/11/2015 16:04 MHALL32.5 50
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.189 mg/L EPA 200.7 02/09/2015 12:21 MHH71310.005 1
Barium (Ba)0.017 mg/L EPA 200.7 02/09/2015 12:21 MHH71310.005 1
Boron (B)0.930 mg/L EPA 200.7 02/09/2015 12:21 MHH71310.05 1
Iron (Fe)0.329 mg/L EPA 200.7 02/09/2015 12:21 MHH71310.01 1
Manganese (Mn)0.017 mg/L EPA 200.7 02/09/2015 12:21 MHH71310.005 1
Strontium (Sr)0.074 mg/L EPA 200.7 02/09/2015 12:21 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 02/09/2015 12:21B2 MHH71310.005 1
Page 10 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003051
Collection Date:05-Feb-15 1:10 PM
Site:AW-6D
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/11/2015 13:44 DJSULL111
Arsenic (As)3.01 ug/L EPA 200.8 02/11/2015 13:44 DJSULL111
Beryllium (Be)< 1 ug/L EPA 200.8 02/11/2015 13:44 DJSULL111
Cadmium (Cd)< 1 ug/L EPA 200.8 02/11/2015 13:44 DJSULL111
Chromium (Cr)< 1 ug/L EPA 200.8 02/11/2015 13:44 DJSULL111
Cobalt (Co)< 1 ug/L EPA 200.8 02/11/2015 13:44 DJSULL111
Copper (Cu)< 1 ug/L EPA 200.8 02/11/2015 13:44 DJSULL111
Lead (Pb)< 1 ug/L EPA 200.8 02/11/2015 13:44 DJSULL111
Molybdenum (Mo)9.45 ug/L EPA 200.8 02/11/2015 13:44 DJSULL111
Nickel (Ni)< 1 ug/L EPA 200.8 02/11/2015 13:44 DJSULL111
Selenium (Se)< 1 ug/L EPA 200.8 02/11/2015 13:44 DJSULL111
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/11/2015 13:44 DJSULL10.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/11/2015 13:44 DJSULL10.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/14/2015 15:43 JAHERMA11
Arsenic (As)3.27 ug/L EPA 200.8 02/14/2015 15:43 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 02/14/2015 15:43 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 02/14/2015 15:43 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 02/14/2015 15:43 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 02/14/2015 15:43 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 02/14/2015 15:43 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 02/14/2015 15:43 JAHERMA11
Molybdenum (Mo)9.68 ug/L EPA 200.8 02/14/2015 15:43 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 02/14/2015 15:43 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 02/14/2015 15:43 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/14/2015 15:43 JAHERMA0.2 1
Vanadium (V) Low Level 0.580 ug/L EPA 200.8 02/14/2015 15:43 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 660 mg/L SM2540C 02/11/2015 16:38 GHUTCHI251
Total Carbon
TOC 21 mg/L SM5310C/EPA9060A 02/12/2015 15:45 TJA7067110
TOTAL SUSPENDED SOLIDS
TSS 7.0 mg/L SM2540D 02/10/2015 13:42 GHUTCHI51
Page 11 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003052
Collection Date:05-Feb-15 1:50 PM
Site:AW-6B
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.015 mg-N/L EPA 353.2 02/14/2015 12:02 TLINN0.01 1
INORGANIC IONS BY IC
Chloride 5.1 mg/L EPA 300.0 02/06/2015 21:41 BGN90340.1 1
Sulfate 9.4 mg/L EPA 300.0 02/06/2015 21:41 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/12/2015 11:12 TLINN0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/18/2015 20:20 TLINN0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.111 mg/L EPA 200.7 02/09/2015 14:21 MHH71310.005 1
Barium (Ba)0.030 mg/L EPA 200.7 02/09/2015 14:21 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 02/09/2015 14:21 MHH71310.05 1
Iron (Fe)0.526 mg/L EPA 200.7 02/09/2015 14:21 MHH71310.01 1
Manganese (Mn)0.090 mg/L EPA 200.7 02/09/2015 14:21 MHH71310.005 1
Strontium (Sr)0.016 mg/L EPA 200.7 02/09/2015 14:21 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 02/09/2015 14:21 MHH71310.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)3.64 mg/L EPA 200.7 02/11/2015 16:08 MHALL30.01 1
Magnesium (Mg)0.610 mg/L EPA 200.7 02/11/2015 16:08 MHALL30.005 1
Potassium (K)1.42 mg/L EPA 200.7 02/11/2015 16:08 MHALL30.1 1
Sodium (Na)3.77 mg/L EPA 200.7 02/11/2015 16:08 MHALL30.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.283 mg/L EPA 200.7 02/09/2015 12:26 MHH71310.005 1
Barium (Ba)0.031 mg/L EPA 200.7 02/09/2015 12:26 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 02/09/2015 12:26 MHH71310.05 1
Iron (Fe)0.597 mg/L EPA 200.7 02/09/2015 12:26 MHH71310.01 1
Manganese (Mn)0.090 mg/L EPA 200.7 02/09/2015 12:26 MHH71310.005 1
Strontium (Sr)0.016 mg/L EPA 200.7 02/09/2015 12:26 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 02/09/2015 12:26B2 MHH71310.005 1
Page 12 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003052
Collection Date:05-Feb-15 1:50 PM
Site:AW-6B
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/11/2015 13:49 DJSULL111
Arsenic (As)< 1 ug/L EPA 200.8 02/11/2015 13:49 DJSULL111
Beryllium (Be)< 1 ug/L EPA 200.8 02/11/2015 13:49 DJSULL111
Cadmium (Cd)< 1 ug/L EPA 200.8 02/11/2015 13:49 DJSULL111
Chromium (Cr)< 1 ug/L EPA 200.8 02/11/2015 13:49 DJSULL111
Cobalt (Co)< 1 ug/L EPA 200.8 02/11/2015 13:49 DJSULL111
Copper (Cu)< 1 ug/L EPA 200.8 02/11/2015 13:49 DJSULL111
Lead (Pb)< 1 ug/L EPA 200.8 02/11/2015 13:49 DJSULL111
Molybdenum (Mo)< 1 ug/L EPA 200.8 02/11/2015 13:49 DJSULL111
Nickel (Ni)1.04 ug/L EPA 200.8 02/11/2015 13:49 DJSULL111
Selenium (Se)< 1 ug/L EPA 200.8 02/11/2015 13:49 DJSULL111
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/11/2015 13:49 DJSULL10.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/11/2015 13:49 DJSULL10.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/14/2015 15:49 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 02/14/2015 15:49 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 02/14/2015 15:49 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 02/14/2015 15:49 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 02/14/2015 15:49 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 02/14/2015 15:49 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 02/14/2015 15:49 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 02/14/2015 15:49 JAHERMA11
Molybdenum (Mo)< 1 ug/L EPA 200.8 02/14/2015 15:49 JAHERMA11
Nickel (Ni)1.59 ug/L EPA 200.8 02/14/2015 15:49 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 02/14/2015 15:49 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/14/2015 15:49 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/14/2015 15:49 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 27 mg/L SM2540C 02/12/2015 15:21 GHUTCHI251
Total Carbon
TOC 3.1 mg/L SM5310C/EPA9060A 02/12/2015 15:45 TJA70670.1 1
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L SM2540D 02/10/2015 13:42 GHUTCHI51
Page 13 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003053
Collection Date:05-Feb-15 3:20 PM
Site:AW-3C
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.032 mg-N/L EPA 353.2 02/14/2015 12:09 TLINN0.02 2
INORGANIC IONS BY IC
Chloride 130 mg/L EPA 300.0 02/09/2015 09:15 BGN90342.5 25
Sulfate 110 mg/L EPA 300.0 02/09/2015 09:15 BGN90342.5 25
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/12/2015 11:19 TLINN0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/18/2015 20:27 TLINN0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.042 mg/L EPA 200.7 02/09/2015 14:35 MHH71310.005 1
Barium (Ba)0.086 mg/L EPA 200.7 02/09/2015 14:35 MHH71310.005 1
Boron (B)1.08 mg/L EPA 200.7 02/09/2015 14:35 MHH71310.05 1
Iron (Fe)24.9 mg/L EPA 200.7 02/09/2015 14:35 MHH71310.05 5
Manganese (Mn)2.08 mg/L EPA 200.7 02/09/2015 14:35 MHH71310.005 1
Strontium (Sr)0.528 mg/L EPA 200.7 02/09/2015 14:35 MHH71310.005 1
Zinc (Zn)0.123 mg/L EPA 200.7 02/09/2015 14:35 MHH71310.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)47.3 mg/L EPA 200.7 02/11/2015 16:12 MHALL30.1 10
Magnesium (Mg)10.3 mg/L EPA 200.7 02/11/2015 16:12 MHALL30.005 1
Potassium (K)6.20 mg/L EPA 200.7 02/11/2015 16:12 MHALL30.1 1
Sodium (Na)75.3 mg/L EPA 200.7 02/11/2015 16:12 MHALL30.5 10
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.129 mg/L EPA 200.7 02/09/2015 12:30 MHH71310.005 1
Barium (Ba)0.087 mg/L EPA 200.7 02/09/2015 12:30 MHH71310.005 1
Boron (B)1.09 mg/L EPA 200.7 02/09/2015 12:30 MHH71310.05 1
Iron (Fe)26.6 mg/L EPA 200.7 02/09/2015 12:30 MHH71310.1 10
Manganese (Mn)2.12 mg/L EPA 200.7 02/09/2015 12:30 MHH71310.005 1
Strontium (Sr)0.537 mg/L EPA 200.7 02/09/2015 12:30 MHH71310.005 1
Zinc (Zn)0.126 mg/L EPA 200.7 02/09/2015 12:30B2 MHH71310.005 1
Page 14 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003053
Collection Date:05-Feb-15 3:20 PM
Site:AW-3C
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/11/2015 13:54 DJSULL111
Arsenic (As)< 1 ug/L EPA 200.8 02/11/2015 13:54 DJSULL111
Beryllium (Be)< 1 ug/L EPA 200.8 02/11/2015 13:54 DJSULL111
Cadmium (Cd)< 1 ug/L EPA 200.8 02/11/2015 13:54 DJSULL111
Chromium (Cr)< 1 ug/L EPA 200.8 02/11/2015 13:54 DJSULL111
Cobalt (Co)24.9 ug/L EPA 200.8 02/11/2015 13:54 DJSULL111
Copper (Cu)< 1 ug/L EPA 200.8 02/11/2015 13:54 DJSULL111
Lead (Pb)< 1 ug/L EPA 200.8 02/11/2015 13:54 DJSULL111
Molybdenum (Mo)2.04 ug/L EPA 200.8 02/11/2015 13:54 DJSULL111
Nickel (Ni)3.78 ug/L EPA 200.8 02/11/2015 13:54 DJSULL111
Selenium (Se)< 1 ug/L EPA 200.8 02/11/2015 13:54 DJSULL111
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/11/2015 13:54 DJSULL10.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/11/2015 13:54 DJSULL10.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/14/2015 15:54 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 02/14/2015 15:54 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 02/14/2015 15:54 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 02/14/2015 15:54 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 02/14/2015 15:54 JAHERMA11
Cobalt (Co)23.8 ug/L EPA 200.8 02/14/2015 15:54 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 02/14/2015 15:54 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 02/14/2015 15:54 JAHERMA11
Molybdenum (Mo)1.85 ug/L EPA 200.8 02/14/2015 15:54 JAHERMA11
Nickel (Ni)4.37 ug/L EPA 200.8 02/14/2015 15:54 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 02/14/2015 15:54 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/14/2015 15:54 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/14/2015 15:54 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 450 mg/L SM2540C 02/12/2015 15:21 GHUTCHI251
Total Carbon
TOC 3.5 mg/L SM5310C/EPA9060A 02/12/2015 15:45 TJA70670.1 1
TOTAL SUSPENDED SOLIDS
TSS 19 mg/L SM2540D 02/10/2015 13:42 GHUTCHI51
Page 15 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003054
Collection Date:05-Feb-15 5:05 PM
Site:AW-3B
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.011 mg-N/L EPA 353.2 02/14/2015 12:29 TLINN0.01 1
INORGANIC IONS BY IC
Chloride 5.2 mg/L EPA 300.0 02/06/2015 22:14 BGN90340.1 1
Sulfate 4.0 mg/L EPA 300.0 02/06/2015 22:14 BGN90340.1 1
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/12/2015 11:21 TLINN0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/18/2015 20:30 TLINN0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.012 mg/L EPA 200.7 02/09/2015 14:39 MHH71310.005 1
Barium (Ba)0.009 mg/L EPA 200.7 02/09/2015 14:39 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 02/09/2015 14:39 MHH71310.05 1
Iron (Fe)5.47 mg/L EPA 200.7 02/09/2015 14:39 MHH71310.01 1
Manganese (Mn)0.167 mg/L EPA 200.7 02/09/2015 14:39 MHH71310.005 1
Strontium (Sr)0.022 mg/L EPA 200.7 02/09/2015 14:39 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 02/09/2015 14:39 MHH71310.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)7.06 mg/L EPA 200.7 02/11/2015 16:16 MHALL30.01 1
Magnesium (Mg)0.880 mg/L EPA 200.7 02/11/2015 16:16 MHALL30.005 1
Potassium (K)1.27 mg/L EPA 200.7 02/11/2015 16:16 MHALL30.1 1
Sodium (Na)3.62 mg/L EPA 200.7 02/11/2015 16:16 MHALL30.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.112 mg/L EPA 200.7 02/09/2015 12:34 MHH71310.005 1
Barium (Ba)0.009 mg/L EPA 200.7 02/09/2015 12:34 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 02/09/2015 12:34 MHH71310.05 1
Iron (Fe)6.61 mg/L EPA 200.7 02/09/2015 12:34 MHH71310.01 1
Manganese (Mn)0.161 mg/L EPA 200.7 02/09/2015 12:34 MHH71310.005 1
Strontium (Sr)0.020 mg/L EPA 200.7 02/09/2015 12:34 MHH71310.005 1
Zinc (Zn)0.016 mg/L EPA 200.7 02/09/2015 12:34B2 MHH71310.005 1
Page 16 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003054
Collection Date:05-Feb-15 5:05 PM
Site:AW-3B
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/11/2015 13:59 DJSULL111
Arsenic (As)< 1 ug/L EPA 200.8 02/11/2015 13:59 DJSULL111
Beryllium (Be)< 1 ug/L EPA 200.8 02/11/2015 13:59 DJSULL111
Cadmium (Cd)< 1 ug/L EPA 200.8 02/11/2015 13:59 DJSULL111
Chromium (Cr)< 1 ug/L EPA 200.8 02/11/2015 13:59 DJSULL111
Cobalt (Co)< 1 ug/L EPA 200.8 02/11/2015 13:59 DJSULL111
Copper (Cu)< 1 ug/L EPA 200.8 02/11/2015 13:59 DJSULL111
Lead (Pb)< 1 ug/L EPA 200.8 02/11/2015 13:59 DJSULL111
Molybdenum (Mo)2.06 ug/L EPA 200.8 02/11/2015 13:59 DJSULL111
Nickel (Ni)< 1 ug/L EPA 200.8 02/11/2015 13:59 DJSULL111
Selenium (Se)< 1 ug/L EPA 200.8 02/11/2015 13:59 DJSULL111
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/11/2015 13:59 DJSULL10.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/11/2015 13:59 DJSULL10.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/14/2015 15:59 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 02/14/2015 15:59 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 02/14/2015 15:59 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 02/14/2015 15:59 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 02/14/2015 15:59 JAHERMA11
Cobalt (Co)< 1 ug/L EPA 200.8 02/14/2015 15:59 JAHERMA11
Copper (Cu)< 1 ug/L EPA 200.8 02/14/2015 15:59 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 02/14/2015 15:59 JAHERMA11
Molybdenum (Mo)2.25 ug/L EPA 200.8 02/14/2015 15:59 JAHERMA11
Nickel (Ni)< 1 ug/L EPA 200.8 02/14/2015 15:59 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 02/14/2015 15:59 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/14/2015 15:59 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/14/2015 15:59 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 46 mg/L SM2540C 02/12/2015 15:21 GHUTCHI251
Total Carbon
TOC 2.4 mg/L SM5310C/EPA9060A 02/12/2015 15:45 TJA70670.1 1
TOTAL SUSPENDED SOLIDS
TSS 9.0 mg/L SM2540D 02/10/2015 13:42 GHUTCHI51
Page 17 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003055
Collection Date:05-Feb-15 4:55 PM
Site:AW-2C
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
ALKALINITY - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete Vendor Method V_SHEALY
NITRITE + NITRATE (COLORIMETRIC)
Nitrite + Nitrate (Colorimetric)0.030 mg-N/L EPA 353.2 02/14/2015 12:30 TLINN0.01 1
INORGANIC IONS BY IC
Chloride 5.1 mg/L EPA 300.0 02/06/2015 22:30 BGN90340.1 1
Sulfate 15 mg/L EPA 300.0 02/06/2015 22:30 BGN90340.5 5
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/12/2015 11:24 TLINN0.05 1
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/18/2015 20:32 TLINN0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)0.025 mg/L EPA 200.7 02/09/2015 14:43 MHH71310.005 1
Barium (Ba)0.036 mg/L EPA 200.7 02/09/2015 14:43 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 02/09/2015 14:43 MHH71310.05 1
Iron (Fe)15.5 mg/L EPA 200.7 02/09/2015 14:43 MHH71310.01 1
Manganese (Mn)0.402 mg/L EPA 200.7 02/09/2015 14:43 MHH71310.005 1
Strontium (Sr)0.020 mg/L EPA 200.7 02/09/2015 14:43 MHH71310.005 1
Zinc (Zn)0.006 mg/L EPA 200.7 02/09/2015 14:43 MHH71310.005 1
UNDIGESTED METALS BY ICP
Calcium (Ca)5.25 mg/L EPA 200.7 02/11/2015 16:20 MHALL30.01 1
Magnesium (Mg)0.641 mg/L EPA 200.7 02/11/2015 16:20 MHALL30.005 1
Potassium (K)1.20 mg/L EPA 200.7 02/11/2015 16:20 MHALL30.1 1
Sodium (Na)3.26 mg/L EPA 200.7 02/11/2015 16:20 MHALL30.05 1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (Al)0.141 mg/L EPA 200.7 02/09/2015 12:38 MHH71310.005 1
Barium (Ba)0.037 mg/L EPA 200.7 02/09/2015 12:38 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 02/09/2015 12:38 MHH71310.05 1
Iron (Fe)16.2 mg/L EPA 200.7 02/09/2015 12:38 MHH71310.01 1
Manganese (Mn)0.401 mg/L EPA 200.7 02/09/2015 12:38 MHH71310.005 1
Strontium (Sr)0.020 mg/L EPA 200.7 02/09/2015 12:38 MHH71310.005 1
Zinc (Zn)0.008 mg/L EPA 200.7 02/09/2015 12:38B2 MHH71310.005 1
Page 18 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003055
Collection Date:05-Feb-15 4:55 PM
Site:AW-2C
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/11/2015 14:04 DJSULL111
Arsenic (As)< 1 ug/L EPA 200.8 02/11/2015 14:04 DJSULL111
Beryllium (Be)< 1 ug/L EPA 200.8 02/11/2015 14:04 DJSULL111
Cadmium (Cd)< 1 ug/L EPA 200.8 02/11/2015 14:04 DJSULL111
Chromium (Cr)< 1 ug/L EPA 200.8 02/11/2015 14:04 DJSULL111
Cobalt (Co)2.15 ug/L EPA 200.8 02/11/2015 14:04 DJSULL111
Copper (Cu)< 1 ug/L EPA 200.8 02/11/2015 14:04 DJSULL111
Lead (Pb)< 1 ug/L EPA 200.8 02/11/2015 14:04 DJSULL111
Molybdenum (Mo)1.16 ug/L EPA 200.8 02/11/2015 14:04 DJSULL111
Nickel (Ni)1.97 ug/L EPA 200.8 02/11/2015 14:04 DJSULL111
Selenium (Se)< 1 ug/L EPA 200.8 02/11/2015 14:04 DJSULL111
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/11/2015 14:04 DJSULL10.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/11/2015 14:04 DJSULL10.3 1
TOTAL RECOVERABLE METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/14/2015 16:05 JAHERMA11
Arsenic (As)< 1 ug/L EPA 200.8 02/14/2015 16:05 JAHERMA11
Beryllium (Be)< 1 ug/L EPA 200.8 02/14/2015 16:05 JAHERMA11
Cadmium (Cd)< 1 ug/L EPA 200.8 02/14/2015 16:05 JAHERMA11
Chromium (Cr)< 1 ug/L EPA 200.8 02/14/2015 16:05 JAHERMA11
Cobalt (Co)2.01 ug/L EPA 200.8 02/14/2015 16:05 JAHERMA11
Copper (Cu)3.84 ug/L EPA 200.8 02/14/2015 16:05 JAHERMA11
Lead (Pb)< 1 ug/L EPA 200.8 02/14/2015 16:05 JAHERMA11
Molybdenum (Mo)1.19 ug/L EPA 200.8 02/14/2015 16:05 JAHERMA11
Nickel (Ni)2.79 ug/L EPA 200.8 02/14/2015 16:05 JAHERMA11
Selenium (Se)< 1 ug/L EPA 200.8 02/14/2015 16:05 JAHERMA11
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/14/2015 16:05 JAHERMA0.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/14/2015 16:05 JAHERMA0.3 1
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4)Complete Vendor Method V_SHEALY
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete Vendor Method V_ELE1
TOTAL DISSOLVED SOLIDS
TDS 42 mg/L SM2540C 02/12/2015 15:21 GHUTCHI251
Total Carbon
TOC 1.1 mg/L SM5310C/EPA9060A 02/12/2015 15:45 TJA70670.1 1
TOTAL SUSPENDED SOLIDS
TSS 16 mg/L SM2540D 02/10/2015 13:42 GHUTCHI51
Page 19 of 53
Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020166
2015003056
Collection Date:05-Feb-15 9:10 AM
Site:Filter Blank
Matrix:GW_WW
Analyte Analysis Date/TimeMethodUnits Qualifiers RDLResult
Sample #:
AnalystDF
Mercury Dissolved (cold vapor) in Water (Filtered)
Mercury (Hg)< 0.05 ug/L EPA 245.1 02/18/2015 20:34 TLINN0.05 1
DISSOLVED METALS BY ICP
Aluminum (Al)< 0.005 mg/L EPA 200.7 02/09/2015 14:47 MHH71310.005 1
Barium (Ba)< 0.005 mg/L EPA 200.7 02/09/2015 14:47 MHH71310.005 1
Boron (B)< 0.05 mg/L EPA 200.7 02/09/2015 14:47 MHH71310.05 1
Iron (Fe)< 0.01 mg/L EPA 200.7 02/09/2015 14:47 MHH71310.01 1
Manganese (Mn)< 0.005 mg/L EPA 200.7 02/09/2015 14:47 MHH71310.005 1
Strontium (Sr)< 0.005 mg/L EPA 200.7 02/09/2015 14:47 MHH71310.005 1
Zinc (Zn)< 0.005 mg/L EPA 200.7 02/09/2015 14:47 MHH71310.005 1
DISSOLVED METALS BY ICP-MS
Antimony (Sb)< 1 ug/L EPA 200.8 02/11/2015 14:09 DJSULL111
Arsenic (As)< 1 ug/L EPA 200.8 02/11/2015 14:09 DJSULL111
Beryllium (Be)< 1 ug/L EPA 200.8 02/11/2015 14:09 DJSULL111
Cadmium (Cd)< 1 ug/L EPA 200.8 02/11/2015 14:09 DJSULL111
Chromium (Cr)< 1 ug/L EPA 200.8 02/11/2015 14:09 DJSULL111
Cobalt (Co)< 1 ug/L EPA 200.8 02/11/2015 14:09 DJSULL111
Copper (Cu)< 1 ug/L EPA 200.8 02/11/2015 14:09 DJSULL111
Lead (Pb)< 1 ug/L EPA 200.8 02/11/2015 14:09 DJSULL111
Molybdenum (Mo)< 1 ug/L EPA 200.8 02/11/2015 14:09 DJSULL111
Nickel (Ni)< 1 ug/L EPA 200.8 02/11/2015 14:09 DJSULL111
Selenium (Se)< 1 ug/L EPA 200.8 02/11/2015 14:09 DJSULL111
Thallium (Tl) Low Level < 0.2 ug/L EPA 200.8 02/11/2015 14:09 DJSULL10.2 1
Vanadium (V) Low Level < 0.3 ug/L EPA 200.8 02/11/2015 14:09 DJSULL10.3 1
Qualifiers:
B2 Target analyte was detected in blank(s) at a concentration greater than ½ the reporting limit but less than the
reporting limit. Analyte concentration in sample is valid and may be used for compliance purposes.
Page 20 of 53
Page 21 of 53
Page 22 of 53
Page 23 of 53
Page 24 of 53
SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
QB10026Lot Number:
J15020166Project Number:
Sutton - Groundwater AssessmentProject Name:
02/20/2015Date Completed:
Grant Wilton
Project Manager
*QB10026*

This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non-paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
Page: 1 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Case Narrative
Duke Energy
Lot Number: QB10026
SC DHEC No: 32010 NC Field Parameters No: 5639 NELAC No: E87653 NC DENR No: 329
Project Name: Sutton - Groundwater Assessment
Project Number: J15020166
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPs), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page.
Page: 2 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QB10026

Project Name: Sutton - Groundwater Assessment
Project Number: J15020166
Sample Number Sample ID Matrix Date Sampled Date Received
001 02/05/2015 09202015003048Aqueous 02/10/2015
002 02/05/2015 11052015003049Aqueous 02/10/2015
003 02/05/2015 12152015003050Aqueous 02/10/2015
004 02/05/2015 13102015003051Aqueous 02/10/2015
005 02/05/2015 13502015003052Aqueous 02/10/2015
006 02/05/2015 15202015003053Aqueous 02/10/2015
007 02/05/2015 17052015003054Aqueous 02/10/2015
008 02/05/2015 16552015003055Aqueous 02/10/2015
(8 samples)
Page: 3 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QB10026

Project Name: Sutton - Groundwater Assessment
Project Number: J15020166
Sample Sample ID Matrix Parameter Method Result Q Units Page
001 2015003048 Aqueous Alkalinity SM 2320B-48 mg/L 5
001 2015003048 Aqueous Bicarbonate Alkalinity SM 2320B-48 mg/L 5
001 2015003048 Aqueous Methane RSK - 175 21 ug/L 6
002 2015003049 Aqueous Alkalinity SM 2320B-17 mg/L 7
002 2015003049 Aqueous Bicarbonate Alkalinity SM 2320B-17 mg/L 7
003 2015003050 Aqueous Alkalinity SM 2320B-47 mg/L 9
003 2015003050 Aqueous Bicarbonate Alkalinity SM 2320B-47 mg/L 9
004 2015003051 Aqueous Alkalinity SM 2320B-250 mg/L 11
004 2015003051 Aqueous Bicarbonate Alkalinity SM 2320B-250 mg/L 11
004 2015003051 Aqueous Methane RSK - 175 11 ug/L 12
006 2015003053 Aqueous Alkalinity SM 2320B-52 mg/L 15
006 2015003053 Aqueous Bicarbonate Alkalinity SM 2320B-52 mg/L 15
006 2015003053 Aqueous Methane RSK - 175 11 ug/L 16
007 2015003054 Aqueous Alkalinity SM 2320B-21 mg/L 17
007 2015003054 Aqueous Bicarbonate Alkalinity SM 2320B-21 mg/L 17
008 2015003055 Aqueous Alkalinity SM 2320B-12 mg/L 19
008 2015003055 Aqueous Bicarbonate Alkalinity SM 2320B-12 mg/L 19
(17 detections)
Page: 4 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003048
QB10026-001
02/05/2015 0920
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 02/16/2015 1759 BWS 67878
1 (Bicarbonate ) SM 2320B-2011 1 02/16/2015 1759 BWS 02/16/2015 1759
1 (Carbonate Al) SM 2320B-2011 1 02/16/2015 1759 BWS 02/16/2015 1759
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 48 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 48 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 5 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003048
QB10026-001
02/05/2015 0920
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 02/16/2015 1451 DCS 67934
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 21 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 6 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003049
QB10026-002
02/05/2015 1105
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 02/16/2015 1804 BWS 67878
1 (Bicarbonate ) SM 2320B-2011 1 02/16/2015 1804 BWS 02/16/2015 1804
1 (Carbonate Al) SM 2320B-2011 1 02/16/2015 1804 BWS 02/16/2015 1804
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 17 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 17 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 7 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003049
QB10026-002
02/05/2015 1105
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 02/16/2015 1501 DCS 67934
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 8 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003050
QB10026-003
02/05/2015 1215
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 02/16/2015 1810 BWS 67878
1 (Bicarbonate ) SM 2320B-2011 1 02/16/2015 1810 BWS 02/16/2015 1810
1 (Carbonate Al) SM 2320B-2011 1 02/16/2015 1810 BWS 02/16/2015 1810
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 47 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 47 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 9 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003050
QB10026-003
02/05/2015 1215
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 02/16/2015 1520 DCS 67934
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 10 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003051
QB10026-004
02/05/2015 1310
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 02/16/2015 1817 BWS 67878
1 (Bicarbonate ) SM 2320B-2011 1 02/16/2015 1817 BWS 02/16/2015 1817
1 (Carbonate Al) SM 2320B-2011 1 02/16/2015 1817 BWS 02/16/2015 1817
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 250 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 250 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 11 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003051
QB10026-004
02/05/2015 1310
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 02/16/2015 1531 DCS 67934
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 11 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 12 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003052
QB10026-005
02/05/2015 1350
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 02/16/2015 1822 BWS 67878
1 (Bicarbonate ) SM 2320B-2011 1 02/16/2015 1822 BWS 02/16/2015 1822
1 (Carbonate Al) SM 2320B-2011 1 02/16/2015 1822 BWS 02/16/2015 1822
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 ND 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 ND 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 13 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003052
QB10026-005
02/05/2015 1350
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 02/16/2015 1543 DCS 67934
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 14 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003053
QB10026-006
02/05/2015 1520
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 02/16/2015 1827 BWS 67878
1 (Bicarbonate ) SM 2320B-2011 1 02/16/2015 1827 BWS 02/16/2015 1827
1 (Carbonate Al) SM 2320B-2011 1 02/16/2015 1827 BWS 02/16/2015 1827
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 52 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 52 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 15 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003053
QB10026-006
02/05/2015 1520
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 02/16/2015 1555 DCS 67934
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 11 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 16 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003054
QB10026-007
02/05/2015 1705
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 02/16/2015 1844 BWS 67878
1 (Bicarbonate ) SM 2320B-2011 1 02/16/2015 1844 BWS 02/16/2015 1844
1 (Carbonate Al) SM 2320B-2011 1 02/16/2015 1844 BWS 02/16/2015 1844
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 21 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 21 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 17 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003054
QB10026-007
02/05/2015 1705
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 02/16/2015 1608 DCS 67934
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 18 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003055
QB10026-008
02/05/2015 1655
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 (Alkalinity) SM 2320B-2011 1 02/16/2015 1849 BWS 67878
1 (Bicarbonate ) SM 2320B-2011 1 02/16/2015 1849 BWS 02/16/2015 1849
1 (Carbonate Al) SM 2320B-2011 1 02/16/2015 1849 BWS 02/16/2015 1849
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Alkalinity SM 2320B-20 12 1mg/L10
Bicarbonate Alkalinity SM 2320B-20 12 1mg/L10
Carbonate Alkalinity SM 2320B-20 ND 1mg/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 19 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane
Description:Matrix:
Date Received:
Client:Laboratory ID:
Date Sampled:
Duke Energy
2015003055
QB10026-008
02/05/2015 1655
02/10/2015
Aqueous
Project Name: Sutton - Groundwater
Project Number: J15020166
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 02/16/2015 1625 DCS 67934
AnalyticalCAS
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 1ug/L10
J = Estimated result < PQL and > MDL
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range
P = The RPD between two GC columns exceeds 40%ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
N = Recovery is out of criteria_
H = Out of holding time
Page: 20 of 20
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
QC Summary
QC Data for Lot Number: QB10026
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - MB
Batch:
Sample ID:QQ67878-001
67878
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Alkalinity ND 02/16/2015 162410mg/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QB10026
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Inorganic non-metals - LCS
Batch:
Sample ID:QQ67878-002
67878
Analytical Method:SM 2320B-2011
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(mg/L)(mg/L)
Alkalinity 98 02/16/2015 16319810090-1101
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QB10026
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane - MB
Batch:
Sample ID:QQ67934-001
67934
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter Result Q PQL Units Analysis DateDil
Methane ND 02/16/2015 135310ug/L1
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QB10026
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane - LCS
Batch:
Sample ID:QQ67934-002
67934
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date
% Rec
LimitDil(ug/L)(ug/L)
Methane 120 02/16/2015 11317815070-1301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QB10026
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
Methane - LCSD
Batch:
Sample ID:QQ67934-003
67934
Analytical Method:RSK - 175
Matrix:Aqueous
Parameter
Result
Q % Rec
Spike
Amount
Analysis Date% RPD
% Rec
Limit
% RPD
LimitDil(ug/L)(ug/L)
Methane 120 02/16/2015 11118015070-1302.2 301
Note:Calculations are performed before rounding to avoid round-off errors in calculated results
PQL = Practical quantitation limit
ND = Not detected at or above the PQL
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
J = Estimated result < PQL and > MDL
N = Recovery is out of criteriaP = The RPD between two GC columns exceeds 40%
+ = RPD is out of criteria_
QC Data for Lot Number: QB10026
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.

106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
Shealy Environmental Services, Inc.
Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy FmVrrallircCntal scm. s. In:. Pale L off
[Y,K1vT Al hl umbu' F-A17.016 F ep: om Da¢. UT+I VJ4
RdVi tf?IlK-Lkrnb'.f. lb E:_Jti.nsee Mir: IW?A4
Sample Receipt Checklist (SR
Clien(: t} r Coulcr I,ispmled by1data: AarLat O:OP i (J i
Means of receipt; 2 SESI ❑Client ❑ UPS ❑ FedEx ❑ Airborne Exp Qlh+.7
`.r'es j Nor
1. crc ousxod scab resent on the cooler?
Yes No ❑ INA
2. if custody iculs were presem, were they intazt and unbroken?
Cooler 1131#0rfigin�ajl temperature: upon reeeiptV'�erived (corrected) temperature upon refceipt=
.. P 'n '
y a
' lc 1 F 21C f f 0C
-1.
Method; ❑ Temperatvre
tank Against 13oLtles R Guo Tl>: #4 lR Gun Carrection Factor: � o�
Method of coolant:
Wet lee ❑ Blue Ice ❑ Dry Icc ❑ 1� one
if temperature: of any cooler excoeded 6,0' , was Projert Manager notified"
Yes ❑ Na ❑
NA
PM notiN4 by SRC, phone, note (circle one), wher;
4
For coolers rwAved v is cowmen i al c ourier, PM s are to be notified
,ka
immediately.)
4. is tha cammercial ccltrier's skin : s]i niwohed to this fonta'�
Yes
7u
y—es
No ❑
ajS
. Were proper custody procedures �relin u3shed received) followed?
YES
NA.
5a Wore swn 11es resin uished by client to commercial courier?
Yes
o
❑
+6. Were sample IDs listed on the t~ ?
Yc5
O
❑
7. Were sam Ic Ids l I sted oil al I salts le cantalncrs'�
$, Was collection date & time listed an the CO-C?
Yes
0
ye-9
#
9- Was collection date & tune listesd on Al] sAm le contalnen?
Yes
cr
❑
10. Dill all container label infurrnation 1), , date, time) agree with the COC?
4' �
❑
l 1. Were tests to the perfurmW.lisled on the COC? s
'e:s
t7
12. Did .all samples arrive in the proper aantainers for eaeft test'•?
❑
ores
o
13. Did all enrltaulers a1TiVe in good wndition unbroken, lids on, cLo. ?
Yes
No
❑
14. Was adequatz sample volume AyailablO
15. Were all mnples received within`r'4 the holding time or 48 (Losers, vr�Ii h';Ver
Yes ❑
No
corucslfirsf?
yCS ❑
No _
I . were any saw lcs containers Assing?
res
[Yes
i~fo
17. Were there any O=e3S Sam les not listed 0" COC?
F1 I
l $. Werrr bubbles przscnt = ` ea-size:P 11,"or 6mm in O iWfleter) in any V0A vial"
14
No
NA ❑
Yes ❑
swag ❑
NA
l4_ Wcre All metalz^O&G(j4f. fJnntrient sam ]cs received at a E H of ?
❑
N' o ❑
201. Were All e-vanide audJor sulfde samples received A# a N>1'2?
N.4
21. W`�ere all applic able NH3frKN{cyaTridelphenol (<0.2mg/L) samples free of
Yes ❑
No
NA
vesidual chlorine.?
_W75
No ❑
NA
2. Were collection temperatuires documented on the COC for NC sarrl les?
23. Weltclient remarks/requests (i.e. requested dilutions, MSiMSD designations,
Yes 0 No ❑ NA
� etc...) colTvA tnn.cribed from the C into the 4--omlment section in LINIS`�
YcS ❑ l Po
U_ 1'+'v'as thu ilua,te number used taken froi1 the contaioer label?
San. ple Preservation (Must be cnmpletc- d for any sample(s) inrorrcctly pre rvvd or with hcadsparc.)
Sarnplc(s)
were reccised incorrectly preserves and were 24jl.15wd
rdingly in Sam to rc�eiving with �+7a�I f usin SR. �'
Stern le(S)
__�H�gDa.,T-ThTD�,HC]
were received with bubb]cs >6 mm in diameter -
Sam lc s
were received with TRt7 > 0.2 rt1 lL (3f 921 is No
SC Drinking Water Pr)jeat Samples) pH verifiiud to be > 2 by _ Datc:
Sarre l f`
were not received at pHat <2 atld were adjusted acoord i ngly using SRO
finro-nh-. lahcts anulicd by;
V Verified by-. r Date; _ o
QN131.119rL#s;
— -F rerrrueynt
4et = I
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Page 53 of 53