NC0001422_DRAFT_GA140483_ADD01_LVSutton_Data Report_20150805

Prepared for
Duke Energy
526 South Church Street
Charlotte, North Carolina 28202
PRELIMINARY SITE
INVESTIGATION DATA REPORT
ADDENDUM NO. 1
CONCEPTUAL CLOSURE PLAN
L.V. SUTTON PLANT
Prepared by
Geosyntec Consultants of NC, PC
1300 South Mint Street, Suite 110
Charlotte, North Carolina 28203
Project Number GC5592
July 2014

GC5592/GA140483_ADD01_LVSutton_Data Report.docx i 07.29.14
TABLE OF CONTENTS

1. INTRODUCTION ................................................................................................ 1
2. FADA INVESTIGATION .................................................................................... 2
2.1 Overview and Background .......................................................................... 2
2.1.1 Previous Investigation .................................................................... 2
2.1.2 Data Gaps ....................................................................................... 2
2.2 Field Investigation ....................................................................................... 3
2.2.1 Groundwater Monitoring ................................................................ 3
2.2.2 Soil and CCR Investigation ............................................................ 4
2.3 Summary ...................................................................................................... 5
3. ADDITIONAL INVESTIGATION IN THE 1971 POND ................................... 6
3.1 Overview ..................................................................................................... 6
3.2 Geoprobe Borings and Sampling ................................................................. 6
3.3 Laboratory Tests .......................................................................................... 6
3.3.1 Geotechnical Tests ......................................................................... 6
3.3.2 Analytical Tests .............................................................................. 7
3.4 Summary ...................................................................................................... 7
4. REFERENCES ..................................................................................................... 8

TABLE OF CONTENTS (Continued)

GC5592/GA140483_ADD01_LVSutton_Data Report.docx ii 07.29.14
LIST OF TABLES

Table 2.T1: FADA Investigation- Groundwater Elevation Data
Table 2.T2: FADA Investigation - Groundwater Field Parameters
Table 2.T3: FADA Investigation - Groundwater Analytical Data
Table 2.T4: FADA Investigation - Soil and CCR Analytical Data
Table 2.T5: FADA Investigation - SPLP Analytical Data
Table 3.T1: Summary of Index Test Results
Table 3.T2: 1971 Pond Investigation – CCR Analytical Data
Table 3.T3: 1971 Pond Investigation – SPLP Analytical Data

LIST OF FIGURES

Figure 2.F1: Hydrogeological Investigation Soil, CCR, and Groundwater Sampling
Locations
Figure 3.F1: L.V. Sutton Plant Historical and Conceptual Closure Geotechnical
Investigation

LIST OF APPENDICES

Appendix 2.A1: Field Forms
Appendix 2.A2: Laboratory Analytical Results
Appendix 2.A3: Geosyntec DPT Boring Logs
Appendix 3.A1: Boring Logs
Appendix 3.A2: Geotechnical Laboratory Test Results
Appendix 3.A3: Photographic Record

GC5592/GA140483_ADD01_LVSutton_Data Report.docx 1 07.29.14
1. INTRODUCTION
Geosyntec Consultants of North Carolina, P.C. (Geosyntec) has been evaluating
conceptual closure options for the CCR ponds located at the L.V. Sutton Plant using: (i)
available information from historical documents and drawings; (ii) data obtained from
the field investigations conducted by Geosyntec in May 2014; and (iii) laboratory
testing results for the samples collected from the referenced Geosyntec investigations.
Several preliminary conceptual closure options were developed and were discussed with
Duke Energy Corporation (DEC) during a meeting held on 4 June 2014. During the
meeting, two additional field tasks were identified to enhance the conceptual closure
plan development based on new findings from the field investigation related to
subsurface conditions.
The two additional field tasks are:
• Former Ash Disposal Area (FADA) Investigation: This investigation serves to
supplement the historical investigation data to delineate the vertical boundaries
of coal combustion residual (CCR) materials and collect groundwater quality
information in the area.
• Additional Investigation in the 1971 Pond: This investigation serves to refine the
horizontal and vertical delineation of CCR materials located deeper in the 1971
Pond and address the new information gathered from the Geosyntec field
investigation conducted in May 2014.
This report includes the findings from these two additional field tasks and is provided as
an addendum to the Preliminary Site Investigation Data Report [Geosyntec, 2014]
submitted to DEC on 24 June 2014.
The remaining sections of this report are organized as follows:
• Section 2 presents the data from the FADA investigation;
• Section 3 presents the data from the additional investigation in the 1971 Pond;
and
• Section 4 presents the cited references.

GC5592/GA140483_ADD01_LVSutton_Data Report.docx 2 07.29.14
2. FADA INVESTIGATION
2.1 Overview and Background
The FADA is located between the discharge canal and the coal pile. It is believed that
CCR may have been disposed of in this area between approximately 1954 and 1972.
Geosyntec understands that the FADA may be on the North Carolina Inactive
Hazardous Waste Sites Priority List and may, at some point, have been under the North
Carolina Department of Environment and Natural Resources (NCDENR) Department of
Waste Management (DWM) Inactive Hazardous Sites Branch’s voluntary program.
As pointed out in Section 1, DEC and Geosyntec agreed during a meeting held on 4
June 2014 to conduct an additional investigation in the FADA Area. Between 30 June
and 2 July 2014 Geosyntec performed an environmental investigation of the FADA to
supplement the historical investigation data, delineate the vertical boundaries of CCR
materials and collect groundwater quality information in the area.
2.1.1 Previous Investigation
Environmental assessments were conducted in the FADA Area from 2001 through 2009
to assess potential CCR impacts. Soil borings using hand augers and larger test pits
were used to delineate the extent of CCRs in soil in the FADA area to determine the soil
impacts in accordance with requirements under the Inactive Hazardous Sites Branch of
the NCDENR. Groundwater monitoring wells were also installed as part of this
investigation to assess groundwater quality in the FADA. In many cases, the test pits
and soil borings were terminated near the top of the water table, before reaching native
soil.
2.1.2 Data Gaps
A review of the logs for the borings and test pits conducted in previous assessments
indicated that the majority of borings may have been terminated at the top of the water
table, even if the soil boring(s) still had CCRs present at the bottom of the boring. As
such, the vertical delineation of CCRs in soil was not complete. Further, the last time
groundwater samples were collected from all wells within the FADA was in 2005.
Only well pairs MW-13/13D and MW-16/16D were sampled more recently. Therefore,
a current round of more comprehensive groundwater sampling was needed within the
FADA.

GC5592/GA140483_ADD01_LVSutton_Data Report.docx 3 07.29.14
2.2 Field Investigation
2.2.1 Groundwater Monitoring
An electronic water level indicator was used to measure the depth-to-water in a total of
nine shallow and deep monitoring wells previously installed in the FADA. The depth-
to-water measurements were collected on 30 June and 1 July 2014 from a reference
point or survey mark on the top of the well casing to the nearest 0.01 ft. Survey data
collected by WSP Sells as part of this event were used to convert the depth-to-water
measurements to groundwater elevations. Table 2.T1 presents the depth-to-water
measurements and groundwater elevations for each location.
Unfiltered water samples were collected from the nine existing wells using low-flow
sampling methods as described in EPA Region 4 Groundwater Sampling Standard
Operating Procedure (SOP) [EPA, 2011a]. Wells were purged using a low-flow
peristaltic pump with the tubing intake located at the midpoint of the water within the
screened interval of the wells. To the extent practical, the purge rate was set to
minimize drawdown and avoid agitation of the sample. The water was purged through
a flow-through cell equipped with temperature, pH, conductivity, oxidation-reduction
potential (ORP) and dissolved oxygen (DO) sensors to monitor variations in these
parameters. Turbidity was measured using a separate turbidity meter.
The wells were considered sufficiently purged when the following water quality
parameters had stabilized for three consecutive readings as follows:
• pH: ±0.2 SU;
• Specific Conductance: ±5%; and
• Turbidity: <10 NTUs or stable within 10%
If the designated water quality parameters had not stabilized after five well volumes had
been purged, then purging stopped at that time and a note of explanation was recorded
in the field log forms. Table 2.T2 presents the final measured field parameters. The
groundwater sampling logs are included in Appendix 2.A1.
Samples were sent under chain-of-custody protocol to Lancaster Laboratories located in
Lancaster, PA, for analysis of:

GC5592/GA140483_ADD01_LVSutton_Data Report.docx 4 07.29.14
• the NC Hazardous Substance List metals (antimony, arsenic, beryllium,
cadmium, chromium, copper, lead, manganese, mercury, nickel, selenium,
silver, thallium, zinc);
• major cations (calcium [Ca], magnesium [Mg], sodium [Na], and potassium
[K]);
• major anions (chloride [Cl], bromide [Br], sulfate [SO4] and alkalinity);
• strontium [Sr], boron [B], barium [Ba], molybdenum [Mo], iron [Fe], vanadium
[V] nitrate/nitrite [NO3/NO2]; and
• total dissolved solids [TDS].
The samples were properly preserved, labeled, logged onto a chain-of-custody form,
and placed into an iced cooler prior to shipment.
The analytical results are presented in Table 2.T3. Hardcopies of the laboratory
analytical reports are included in Appendix 2.A2.
Upon initial evaluation of the analytical results and the associated quality control data,
the data are considered usable for meeting the data quality objectives.
2.2.2 Soil and CCR Investigation
A preliminary, screening-level assessment of the soils and CCR materials in the FADA
was conducted using Geoprobe investigation techniques to (i) visually assess materials
to evaluate composition as either soil, CCR materials, or a mixture, (ii) verify native
soil had been reached, and (iii) collect soil and/or CCR samples from impacted
locations. Geosyntec subcontracted SAEDACCO of Fort Mill, SC, to provide direct
push technology (DPT) boring services. The sample locations are shown on Figure
2.F1. The boring logs for each location are included in Appendix 2.A3.
A subset of soil and/or CCR samples was collected from the borings. When CCR
materials were present above the groundwater table, a sample was collected from the
unsaturated zone approximately 1 ft above the water table. When CCR materials were
present below the groundwater table, a sample was collected from an area of the
saturated zone with the greatest visual impacts. In cases where the transition to native
soil was not visually evident, samples were collected in order to verify that native soil

GC5592/GA140483_ADD01_LVSutton_Data Report.docx 5 07.29.14
had been reached. The solid samples were mixed manually using a stainless steel spoon
in a stainless steel bowl and packed into laboratory-supplied containers and ziplock
bags. Following the assessment, 12 soil samples from six locations that were judged to
be representative of CCR materials and CCR/soil mixtures were selected along with two
additional samples for native soil verification and transferred to laboratory-supplied
containers. The selected samples were sent under chain-of-custody protocol to
Lancaster Laboratories located in Lancaster, PA, for analysis of:
• NC Hazardous Substance List metals (antimony, arsenic, beryllium, cadmium,
chromium, copper, lead, manganese, mercury, nickel, selenium, silver, thallium,
zinc);
• Strontium, boron, barium, molybdenum and iron;
• pH; and
• Leachability of metals using the Synthetic Precipitation Leaching Procedure
(SPLP).
The samples were properly preserved, labeled, logged onto a chain-of-custody form,
and placed into an iced cooler prior to shipment.
The analytical results are presented in Table 2.T4 (total metals, pH, and % moisture)
and Table 2.T5 (SPLP). Hardcopies of the laboratory analytical reports are included in
Appendix 2.A2.
Upon initial review of the analytical results and the associated quality control data, the
results are considered usable for meeting the data quality objectives.
2.3 Summary
The data from the FADA investigation presented herein will be evaluated and
interpreted in an Addendum 2 to the “Data Interpretation and Analysis Report (I & A
Report)” to be submitted to DEC.

GC5592/GA140483_ADD01_LVSutton_Data Report.docx 6 07.29.14
3. ADDITIONAL INVESTIGATION IN THE 1971 POND
3.1 Overview
Geosyntec conducted a subsurface investigation in the 1971 Pond in May 2014. The
investigation consisted of two soil test borings, two Cone Penetration Tests (CPTs), one
seismic CPT (SCPT), and six geoprobes. With the results from the Geosyntec May
2014 investigation, the bottom of CCR within the 1971 Pond was not clearly delineated
since the bottom of CCR varied to a large extent from one location to another.
From 25 June to 2 July 2014 Geosyntec performed an additional investigation in the
1971 Pond. The additional investigation consisted of geoprobe borings and laboratory
tests to delineate the horizontal and vertical extent of CCR within the pond. Samples
were continuously collected during the geoprobe borings. Selected samples were
transported for laboratory testing to characterize geotechnical and environmental
properties. These laboratory testing results were used to verify the bottom of CCR
estimated based on visual assessment in the field.
3.2 Geoprobe Borings and Sampling
Fourteen geoprobes were advanced within the 1971 Pond and on the pond dike. Two
borings were located in a soft ground area covered by vegetation. Access to those two
locations was facilitated by DEC by building an access road. Mid-Atlantic Drilling of
Wilmington, NC was subcontracted to conduct the geoprobe borings using a track-
mounted 6600 rig [ASTM D 6282]. The boring logs are presented in Appendix 3.A1.
The locations of those borings are presented in Figure 3.F1. In the geoprobe borings, a
hollow rod interior lined with a clear plastic sleeve was pushed into the ground. During
the borings, samples were continuously collected in 4-ft-long increments. The collected
samples were visually classified and logged. Selected samples were then bagged or
stored in laboratory-supplied containers, and sent under chain-of-custody protocol for
laboratory testing.
3.3 Laboratory Tests
3.3.1 Geotechnical Tests
Geosyntec subcontracted Excel Geotechnical Testing, Inc., to conduct a geotechnical
laboratory testing program for samples collected during the geoprobe borings. The
testing program included two grain size distribution tests [ASTM D 422] (both of which

GC5592/GA140483_ADD01_LVSutton_Data Report.docx 7 07.29.14
included a hydrometer test [ASTM D 422]) and 13 Atterberg Limit tests [ASTM D
4318]. The test results are summarized in Table 3.T1. The data report prepared by
Excel Geotechnical Testing is presented in Appendix 3.A2.
3.3.2 Analytical Tests
Geosyntec subcontracted Lancaster Laboratories located in Lancaster, PA to conduct an
analytical laboratory testing program for samples collected during the geoprobe borings.
The selected samples were sent under chain-of-custody protocol for analysis of:
• NC Hazardous Substance List metals (antimony, arsenic, beryllium, cadmium,
chromium, copper, lead, manganese, mercury, nickel, selenium, silver, thallium,
zinc);
• Strontium, boron, barium, molybdenum and iron;
• pH; and
• Leachability of metals using the Synthetic Precipitation Leaching Procedure
(SPLP).
The samples were properly preserved, labeled, logged onto a chain-of-custody form,
and placed into an iced cooler prior to shipment. The CCR analytical results and SPLP
results are presented in Table 3.T2 and Table 3.T3, respectively. The data report
prepared by Lancaster Laboratories is presented in Appendix 2.A2.
3.4 Summary
The results from the additional investigation in the 1971 Pond are presented above.
These results along with those from the Geosyntec May 2014 investigation and the
available historical data will be used by Geosyntec to evaluate the geotechnical
performance of the CCR ponds during and after closure. The interpretation of the
Geosyntec investigation results presented herein will be included in an Addendum 2 to
the “Data Interpretation and Analysis Report (I & A Report)” to be submitted to DEC.

GC5592/GA140483_ADD01_LVSutton_Data Report.docx 8 07.29.14
4. REFERENCES
ASTM Standard D 422 (2007), "Standard Test Method for Particle-Size Analysis of
Soils," ASTM International, West Conshohocken, PA, DOI: 10.1520/D0422-
63R07, www.astm.org.
ASTM Standard D 4318 (2010), "Standard Test Methods for Liquid Limit, Plastic
Limit, and Plasticity Index of Soils," ASTM International, West Conshohocken,
PA, DOI: 10.1520/D4318-10, www.astm.org.
ASTM Standard D 6282 (1998), "Standard Guide for Direct Push Soil Sampling for
Environmental Site Characterizations," ASTM International, West
Conshohocken, PA, DOI: 10.1520/ D6282-98R05, www.astm.org.
Geosyntec Consultants, Inc. (2014), "Data Interpretation and Analysis Report.
Conceptual Closure Plan, L.V. Sutton Plant”.

TABLES
Table 2.T1. FADA Investigation- Groundwater Elevation Data
L.V. Sutton Hydrogeologic Site Assessment
July 2014 1 of 1 Geosyntec
Location ID Date
Relative TOC
Elevation
(ft)
Depth to Water
(ft BTOC)
Relative Groundwater
Elevation
(ft)
MW-13 7/1/2014 16.39 7.87 8.52
MW-13D 7/1/2014 16.89 8.38 8.51
MW-14 6/30/2014 12.97 4.75 8.22
MW-15 7/1/2014 10.19 3.91 6.28
MW-15D 7/1/2014 10.00 3.71 6.29
MW-16 7/1/2014 15.81 7.34 8.47
MW-16D 7/1/2014 15.45 7.01 8.44
MW-20 7/1/2014 12.46 9.73 2.73
MW-20D 7/1/2014 12.49 9.27 3.22
Notes:
1. ft BTOC indicates feet below top of casing.
2. TOC indicates top of casing (elevations referenced to NAVD88).
3. ft indicates feet.
4. TOC and relative groundwater elevations are relative to NAVD88.
5. TOC of was surveyed by WSP on July 7-8, 2014.
6. MW-14 was sampled using low-flow sampling on 6/30/2014 following water level collection.
Ta
b
l
e

2
.
T
2
.

F
A
D
A

I
n
v
e
s
t
i
g
a
t
i
o
n

-

G
r
o
u
n
d
w
a
t
e
r

F
i
e
l
d

P
a
r
a
m
e
t
e
r
s
L.
V
.

S
u
t
t
o
n

H
y
d
r
o
g
e
o
l
o
g
i
c

S
i
t
e

A
s
s
e
s
s
m
e
n
t
Dr
a
w
d
o
w
n

p
H

C
o
n
d
u
c
t
i
v
i
t
y

T
e
m
p
e
r
a
t
u
r
e

T
u
r
b
i
d
i
t
y

O
R
P

D
O
(f
t
)

(
S
.
U
.
)

(
µ
S
/
c
m
)

(
˚C)

(
N
T
U
)

(
m
V
)

(
m
g
/
L
)
MW
-
1
3

8
-
1
8

7
/
2
/
2
0
1
4

0
.
0
2

6
.
8
5

5
1
0
.
5

2
1
.
3

9
.
9
5

-
7
5
.
4

0
.
6
9
MW
-
1
3
D

3
3
.
5
-
3
8
.
5

7
/
2
/
2
0
1
4

0
.
2
0

7
.
0
4

7
7
3

2
1
.
9

6
.
9
8

-
1
0
6
.
2

1
.
5
1
MW
-
1
4

1
-
1
1

6
/
3
0
/
2
0
1
4

0
.
0
5

6
.
5
0

1
5
1
.
4

2
6
.
8

1
6
.
1

4
.
4

1
.
8
5
MW
-
1
5

1
-
1
1

7
/
2
/
2
0
1
4

0
.
0
1

6
.
7
3

5
8
3

2
1
.
5

2
.
3
8

-
8
3
.
8

1
.
3
5
MW
-
1
5
D

4
0
-
4
5

7
/
2
/
2
0
1
4

0
.
1
0

6
.
4
3

6
2
6

2
3
.
0

8
.
1
8

5
2
.
8

1
.
2
6
MW
-
1
6

2
-
1
2

7
/
1
/
2
0
1
4

0
.
0
1

6
.
3
0

1
9
3

2
3
.
3

2
8
.
4

-
1
8
.
9

1
.
6
7
MW
-
1
6
D

4
2
-
4
7

7
/
1
/
2
0
1
4

0
.
1
5

4
.
8
2

5
3
9

2
2
.
3

7
.
3
0

9
5
.
4

1
.
0
4
MW
-
2
0

4
-
1
4

7
/
1
/
2
0
1
4

-
0
.
0
2

6
.
3
2

4
7
1
.
2

2
1
.
7

1
.
5
4

-
6
0
.
5

2
.
3
8
MW
-
2
0
D

4
3
-
4
8

7
/
1
/
2
0
1
4

0
.
3
2

7
.
0
8

5
4
4

2
2
.
0

1
2
.
5

-
4
8
.
5

0
.
8
4
No
t
e
s
:
1.

f
t

i
n
d
i
c
a
t
e
s

f
e
e
t
.
2.

f
t

B
G
S

i
n
d
i
c
a
t
e
s

f
e
e
t

b
e
l
o
w

g
r
o
u
n
d

s
u
r
f
a
c
e
.
3.

S
.
U
.

i
n
d
i
c
a
t
e
s

s
t
a
n
d
a
r
d

u
n
i
t
s
.
4.

µS/
c
m

i
n
d
i
c
a
t
e
s

m
i
c
r
o
s
i
e
m
e
n
s

p
e
r

c
e
n
t
i
m
e
t
e
r
.
5.

˚C
i
n
d
i
c
a
t
e
s

d
e
g
r
e
e
s

C
e
l
s
i
u
s
.
6.

N
T
U

i
n
d
i
c
a
t
e
s

N
e
p
h
e
l
o
m
e
t
r
i
c

t
u
r
b
i
d
i
t
y

u
n
i
t
s
.
7.

O
R
P

i
n
d
i
c
a
t
e
s

o
x
i
d
a
t
i
o
n

r
e
d
u
c
t
i
o
n

p
o
t
e
n
t
i
a
l
.
8.

m
V

i
n
d
i
c
a
t
e
s

m
i
l
l
i
v
o
l
t
s
.
9.

D
O

i
n
d
i
c
a
t
e
s

d
i
s
s
o
l
v
e
d

o
x
y
g
e
n
.
10
.

m
g
/
L

i
n
d
i
c
a
t
e
s

m
i
l
l
i
g
r
a
m
s

p
e
r

l
i
t
e
r
.
Lo
c
a
t
i
o
n
Sc
r
e
e
n

In
t
e
r
v
a
l

(f
t

B
G
S
)
Sa
m
p
l
e

D
a
t
e
Ju
l
y

2
0
1
4

1

o
f

1

G
e
o
s
y
n
t
e
c
Table 2.T3. FADA Investigation - Groundwater Analytical Data
L.V. Sutton Hydrogeologic Site Assessment
July 2014 1 of 2 Geosyntec
Antimony Arsenic Barium Beryllium Boron Cadmium Calcium Total Chromium Copper Iron Lead Magnesium Manganese Mercury Molybdenum Nickel Potassium
NC 10 700 NC 700 2 NC 10 1,000 300 15 NC 50 1 NC 100 NC
1 NC NC 4 NC NC NC NC NC NC NC NC NC NC NC NC NC
MW-13 8-18 7/2/2014 5.1 U 218 367 0.67 U 935 0.33 U 45,300 < 30 2.8 U 5,500 4.7 U 15,700 145 0.06 U 140 1.6 U 13,000
MW-13D 33.5-38.5 7/2/2014 5.1 U < 40 144 0.67 U 2,350 0.33 U 89,400 < 30 2.8 U 4,720 4.7 U 25,100 459 0.06 U 319 1.6 U 14,700
MW-14 1-11 6/30/2014 5.1 U < 40 441 0.67 U 104 0.33 U 47,300 < 30 2.8 U 1,170 4.7 U 3,030 27.5 0.06 U < 20 1.6 U 5,360
MW-15 1-11 7/2/2014 5.1 U < 40 36.5 0.67 U < 100 0.33 U 114,000 < 30 2.8 U 5,720 4.7 U 5,200 109 0.06 U < 20 1.6 U 3,500
MW-15D 40-45 7/2/2014 5.1 U 7.2 U 53.3 0.67 U 550 0.33 U 61,500 < 30 2.8 U 724 4.7 U 8,180 1,620 0.06 U 1.7 U 1.6 U 7,610
MW-16 2-12 7/1/2014 5.1 U < 40 26.3 0.67 U 143 0.33 U 8,660 < 30 2.8 U 781 4.7 U 3,860 20.4 0.06 U < 20 1.6 U 5,460
MW-16D 42-47 7/1/2014 5.1 U < 40 34.3 0.67 U 432 0.33 U 24,500 1.3 U 2.8 U 1,820 4.7 U 5,970 269 0.06 U 1.7 U < 20 4,820
MW-20 4-14 7/1/2014 5.1 U 7.2 U 126 0.67 U 129 0.33 U 85,500 < 30 2.8 U 2,610 4.7 U 8,940 413 0.06 U 1.7 U < 20 6,710
MW-20D 43-48 7/1/2014 5.1 U 7.2 U 58.7 0.67 U 227 0.33 U 69,900 < 30 2.8 U 2,310 4.7 U 5,620 190 0.06 U < 20 1.6 U 2,720
Notes:
1. U indicates results below the method
detection limit (MDL) and < indicates results
below the practical quantitation limit (PQL).
2. µg/L indicates micrograms per liter.
3. IMAC indicates Interim Maximum Allowable
Concentrations.
4. Groundwater Standards and IMAC values
are from Classifications and Water Quality
Applicable to the Groundwaters of
North Carolina (NCDENR, Division of Water
Quality, April 2013).
5. NC indicates no criteria.
6. TDS indicates total dissolved solids.
7. ft BGS indicates feet below ground surface.
8. Sample IDs for these locations were a
combination of location and sampling
date, i.e. GW-MW-16-20140701 or
20140630 - MW14.
Groundwater Standards
IMAC
Location Sample Date
Screen
Interval
(ft BGS)
Concentration (µg/L)
Table 2.T3. FADA Investigation - Groundwater Analytical Data
L.V. Sutton Hydrogeologic Site Assessment
July 2014 2 of 2 Geosyntec
MW-13 8-18 7/2/2014
MW-13D 33.5-38.5 7/2/2014
MW-14 1-11 6/30/2014
MW-15 1-11 7/2/2014
MW-15D 40-45 7/2/2014
MW-16 2-12 7/1/2014
MW-16D 42-47 7/1/2014
MW-20 4-14 7/1/2014
MW-20D 43-48 7/1/2014
Notes:
1. U indicates results below the method
detection limit (MDL) and < indicates results
below the practical quantitation limit (PQL).
2. µg/L indicates micrograms per liter.
3. IMAC indicates Interim Maximum Allowable
Concentrations.
4. Groundwater Standards and IMAC values
are from Classifications and Water Quality
Applicable to the Groundwaters of
North Carolina (NCDENR, Division of Water
Quality, April 2013).
5. NC indicates no criteria.
6. TDS indicates total dissolved solids.
7. ft BGS indicates feet below ground surface.
8. Sample IDs for these locations were a
combination of location and sampling
date, i.e. GW-MW-16-20140701 or
20140630 - MW14.
Groundwater Standards
IMAC
Location Sample Date
Screen
Interval
(ft BGS)Selenium Silver Sodium Strontium Thallium Vanadium Zinc Bromide Chloride Nitrate (as N)Nitrite (as NO2-)Sulfate Alkalinity (as CaCO3)TDS
20 20 NC NC NC NC 1,000 NC 250,000 10,000 1,000 250,000 NC 500,000
NC NC NC NC 0.2 0.3 NC NC NC NC NC NC NC NC
4.8 U 1.8 U 44,800 1,400 5.1 U 1.9 U < 40 2,000U 47,200 250 U 400 U 128,000 86,900 370,000
4.8 U 1.8 U 52,100 3,200 5.1 U 1.9 U < 40 2,000U 59,600 250 U 400 U 96,900 235,000 516,000
4.8 U 1.8 U 19,200 398 5.1 U 11.4 < 40 2,000U 22,700 < 500 400 U 6,500 125,000 200,000
4.8 U 1.8 U 18,300 553 5.1 U 1.9 U < 40 2,000U 45,100 250 U 400 U 42,000 211,000 398,000
4.8 U 1.8 U 66,500 615 5.1 U 1.9 U < 40 2,000U 131,000 250 U 400 U 75,700 70,100 435,000
4.8 U 1.8 U 26,900 105 5.1 U < 10 < 40 2,000U 28,000 250 U 400 U 31,800 23,800 140,000
4.8 U 1.8 U 80,700 154 5.1 U < 10 < 40 2,000U 114,000 250 U 400 U 89,000 2,700 345,000
4.8 U 1.8 U 16,300 785 5.1 U 41.3 < 40 2,000U 18,800 250 U 400 U 53,700 207,000 334,000
4.8 U 1.8 U 51,700 186 5.1 U 1.9 U < 40 2,000U 83,500 250 U 400 U 69,600 118,000 365,000
Concentration (µg/L)
Table 2.T4. FADA Investigation - Soil and CCR Analytical Data
L.V. Sutton Hydrogeologic Site Assessment
July 2014 1 of 2 Geosyntec
Antimony Arsenic Barium Beryllium Boron Cadmium Total Chromium Copper Iron Lead Manganese Mercury Molybdenum Nickel
3-4 0.317 U < 3.84 3.28 0.0643 U < 9.59 0.0317 U < 2.88 < 1.92 348 < 2.88 3.12 0.0096 U < 1.92 < 1.92
7-8 0.47 U 26.5 452 3.54 24.6 0.047 U 18.8 42.8 12,600 13.9 44.9 < 0.296 < 2.85 54.8
1.5-2.5 0.337 U < 4.09 5.57 0.0685 U < 10.2 0.0337 U < 3.07 < 2.04 833 < 3.07 7.45 0.0103 U 0.174 U 2.1
5-6 0.567 U 28.1 314 2.73 22.8 0.0567 U 20.4 34.8 11,700 9.56 58.6 < 0.341 < 3.43 17.4
F-DPT4 18-20*7/1/2014 < 8.47 < 8.47 34.2 0.142 U < 21.2 < 2.12 6.51 < 4.24 1,610 < 6.36 15.6 0.0209 U < 4.24 < 4.24
2-4 0.41 U 18.5 340 2.76 < 12.4 0.041 U 11.8 27 11,400 8.63 81.1 < 0.251 < 2.48 18.6
6-8 0.517 U 42.2 708 7.84 19 0.0517 U 25.4 66.4 13,500 18.8 85.7 < 0.311 < 3.13 34.9
3-4 0.394 U < 4.78 31.8 < 1.19 < 11.9 0.0394 U < 3.58 5.03 2,180 < 3.58 8.22 0.0117 U < 2.39 3.27
7-8 0.546 U 31.1 543 5.79 < 16.5 0.0546 U 22.2 58.2 8,130 17.7 43.5 < 0.315 < 3.31 27
15-16*0.377 U < 4.57 7.41 0.0766 U < 11.4 0.0377 U < 3.43 0.377 U 267 < 3.43 2.52 0.0118 U 0.194 U < 2.29
7-8 0.345 U 6.44 38.8 < 1.04 < 10.4 0.0345 U 4.16 7.55 2,080 3.52 10.9 0.0108 U < 2.09 3.93
11-12 0.383 U 7.54 261 1.59 < 11.6 0.0383 U 6.59 14.7 9,420 3.6 46.9 0.0117 U < 2.32 8.38
3-4 0.537 U 35.1 447 5.15 < 16.3 0.0537 U 21.1 56.1 13,400 14.6 152 < 0.312 < 3.25 29.9
7-8 0.526 U 39 443 2.64 < 15.9 0.0526 U 17.1 34.9 16,200 9.93 72.7 < 0.308 < 3.19 16.6
Notes:
1. DPT locations were surveyed by WSP on July 7-8, 2014.
2. U indicates results below the method detection
limit (MDL) and < indicates results below the
practical quantitation limit (PQL).
3. mg/kg indicates milligrams per kilogram.
4. ft BGS indicates feet below ground surface.
5. Sample IDs for these locations were a
combination of location, depth, and sampling
date, i.e. SS-F-DPT-1(3-4)-20140630.
6. * indicates sample was collected to verify that native
soil had been reached.
7. S.U. indicates standard units.
F-DPT3 6/30/2014
F-DPT5 7/1/2014
F-DPT11 7/2/2014
F-DPT14 7/2/2014
Location
Sample
Interval
(ft BGS)
Sample Date Concentration (mg/kg)
F-DPT7 7/1/2014
F-DPT1 6/30/2014
Table 2.T4. FADA Investigation - Soil and CCR Analytical Data
L.V. Sutton Hydrogeologic Site Assessment
July 2014 2 of 2 Geosyntec
3-4
7-8
1.5-2.5
5-6
F-DPT4 18-20*7/1/2014
2-4
6-8
3-4
7-8
15-16*
7-8
11-12
3-4
7-8
Notes:
1. DPT locations were surveyed by WSP on July 7-8, 2014.
2. U indicates results below the method detection
limit (MDL) and < indicates results below the
practical quantitation limit (PQL).
3. mg/kg indicates milligrams per kilogram.
4. ft BGS indicates feet below ground surface.
5. Sample IDs for these locations were a
combination of location, depth, and sampling
date, i.e. SS-F-DPT-1(3-4)-20140630.
6. * indicates sample was collected to verify that native
soil had been reached.
7. S.U. indicates standard units.
F-DPT3 6/30/2014
F-DPT5 7/1/2014
F-DPT11 7/2/2014
F-DPT14 7/2/2014
Location
Sample
Interval
(ft BGS)
Sample Date
F-DPT7 7/1/2014
F-DPT1 6/30/2014
Selenium Silver Strontium Thallium Zinc
0.422 U 0.182 U 1.74 0.767 U < 3.84 0.7 6.65
< 5.7 0.271 U 337 1.14 U 31.3 33.2 6.55
0.45 U 0.194 U 11.4 0.818 U < 4.09 5 8.28
< 6.87 0.326 U 201 1.37 U 14 44 7.71
0.932 U 0.403 U 21 1.69 U 9.63 52.8 5.54
< 4.96 0.236 U 184 0.993 U 16.6 21 7.53
6.86 0.298 U 475 1.25 U 28 37.4 7.8
0.525 U 0.227 U 11.8 0.955 U 5.99 18.7 6.1
< 6.61 0.314 U 336 1.32 U 22.4 40.7 7.21
0.503 U 0.217 U 3.43 0.915 U < 4.57 16.7 7.16
0.459 U 0.198 U 21.3 0.835 U < 4.18 8.8 6.43
< 4.65 0.221 U 83.7 0.929 U 6.3 16.4 6.69
< 6.5 0.309 U 235 1.3 U 20.5 38.5 6.32
< 6.38 0.303 U 195 1.28 U 15 39.1 5.9
Moisture
(%)
pH (Lab)
(S.U.)
Concentration (mg/kg)
Ta
b
l
e

2
.
T
5
.

F
A
D
A

I
n
v
e
s
t
i
g
a
t
i
o
n

-

S
P
L
P

A
n
a
l
y
t
i
c
a
l

D
a
t
a
L.
V
.

S
u
t
t
o
n

H
y
d
r
o
g
e
o
l
o
g
i
c

S
i
t
e

A
s
s
e
s
s
m
e
n
t
An
t
i
m
o
n
y

A
r
s
e
n
i
c

B
a
r
i
u
m

B
e
r
y
l
l
i
u
m

B
o
r
o
n

C
a
d
m
i
u
m

C
a
l
c
i
u
m

T
o
t
a
l

C
h
r
o
m
i
u
m

C
o
p
p
e
r

I
r
o
n

L
e
a
d

M
a
g
n
e
s
i
u
m

M
a
n
g
a
n
e
s
e
NC

1
0

7
0
0

N
C

7
0
0

2

N
C

1
0

1
,
0
0
0

3
0
0

1
5

N
C

5
0
1

N
C

N
C

4

N
C

N
C

N
C

N
C

N
C

N
C

N
C

N
C

N
C
3-
4
5.
1

U

7
.
2

U

2
9
.
9

0
.
6
7

U

<

1
0
0

0
.
3
3

U

1
,
8
4
0

1
.
3

U

2
.
8

U

<

4
0
0

4
.
7

U

2
5
9

<

1
0
7-
8
5.
1

U

<

4
0

1
0
4

0
.
6
7

U

<

1
0
0

0
.
3
3

U

1
,
5
5
0

<

3
0

2
.
8

U

<

4
0
0

4
.
7

U

<

2
0
0

<

1
0
1.
5
-
2
.
5
5.
1

U

7
.
2

U

6
1
.
2

0
.
6
7

U

<

1
0
0

0
.
3
3

U

1
0
,
2
0
0

<

3
0

2
.
8

U

4
7
3

4
.
7

U

3
9
1

<

1
0
5-
6
5.
1

U

<

4
0

2
2
.
3

0
.
6
7

U

<

1
0
0

0
.
3
3

U

4
,
3
4
0

1
.
3

U

2
.
8

U

3
3
.
4

U

4
.
7

U

2
0
4

<

1
0
F-
D
P
T
4
18
-
2
0
*

7
/
1
/
2
0
1
4
5.
1

U

7
.
2

U

4
2
.
4

0
.
6
7

U

<

1
0
0

0
.
3
3

U

1
,
0
8
0

1
.
3

U

<

2
0

<

4
0
0

4
.
7

U

<

2
0
0

<

1
0
2-
4
<
4
0

<

4
0

1
0
5

0
.
6
7

U

<

1
0
0

0
.
3
3

U

5
,
4
0
0

<

3
0

<

2
0

<

4
0
0

4
.
7

U

3
2
3

<

1
0
6-
8
<
4
0

4
1
.
5

2
2
1

0
.
6
7

U

<

1
0
0

0
.
3
3

U

1
2
,
0
0
0

1
.
3

U

2
.
8

U

3
3
.
4

U

4
.
7

U

2
1
4

<

1
0
3-
4
5.
1

U

7
.
2

U

1
7
.
3

0
.
6
7

U

<

1
0
0

0
.
3
3

U

1
,
4
7
0

1
.
3

U

2
.
8

U

<

4
0
0

4
.
7

U

2
1
1

<

1
0
7-
8
<
4
0

<

4
0

2
9
5

0
.
6
7

U

<

1
0
0

0
.
3
3

U

5
,
6
0
0

1
.
3

U

2
.
8

U

3
3
.
4

U

4
.
7

U

3
0
6

<

1
0
15
-
1
6
*
5.
1

U

7
.
2

U

4
4
.
7

0
.
6
7

U

<

1
0
0

0
.
3
3

U

1
,
8
6
0

<

3
0

2
.
8

U

8
2
1

4
.
7

U

3
6
4

<

1
0
7-
8
5.
1

U

7
.
2

U

<

1
0

0
.
6
7

U

<

1
0
0

0
.
3
3

U

7
9
1

1
.
3

U

2
.
8

U

<

4
0
0

4
.
7

U

2
7
8

0
.
8
3

U
11
-
1
2
5.
1

U

7
.
2

U

5
7
.
1

0
.
6
7

U

<

1
0
0

0
.
3
3

U

1
,
3
0
0

<

3
0

2
.
8

U

4
2
6

4
.
7

U

5
0
0

<

1
0
3-
4
5.
1

U

7
.
2

U

3
5
.
2

0
.
6
7

U

<

1
0
0

0
.
3
3

U

1
,
1
1
0

1
.
3

U

2
.
8

U

<

4
0
0

4
.
7

U

5
1
5

<

1
0
7-
8
5.
1

U

7
.
2

U

8
7

0
.
6
7

U

<

1
0
0

0
.
3
3

U

1
,
7
1
0

1
.
3

U

2
.
8

U

3
3
.
4

U
4.7 U 320 0.83 U
No
t
e
s
:
1.

U

i
n
d
i
c
a
t
e
s

r
e
s
u
l
t
s

b
e
l
o
w

t
h
e

m
e
t
h
o
d

d
e
t
e
c
t
i
o
n

l
i
m
i
t

(
M
D
L
)

a
n
d

<

i
n
d
i
c
a
t
e
s

r
e
s
u
l
t
s

b
e
l
o
w

t
h
e

p
r
a
c
t
i
c
a
l

q
u
a
n
t
i
t
a
t
i
o
n

l
i
m
i
t

(
P
Q
L
)
.
2.

µ
g
/
L

i
n
d
i
c
a
t
e
s

m
i
c
r
o
g
r
a
m
s

p
e
r

l
i
t
e
r
.
3.

S
P
L
P

i
n
d
i
c
a
t
e
s

s
y
n
t
h
e
t
i
c

p
r
e
c
i
p
i
t
a
t
i
o
n

l
e
a
c
h
i
n
g

p
r
o
c
e
d
u
r
e
.
4.

f
t

B
G
S

i
n
d
i
c
a
t
e
s

f
e
e
t

b
e
l
o
w

g
r
o
u
n
d

s
u
r
f
a
c
e
.
5.

S
a
m
p
l
e

I
D
s

f
o
r

t
h
e
s
e

l
o
c
a
t
i
o
n
s

w
e
r
e

a

c
o
m
b
i
n
a
t
i
o
n

o
f

l
o
c
a
t
i
o
n
,

d
e
p
t
h
,

a
n
d

s
a
m
p
l
i
n
g

d
a
t
e
,

i
.
e
.

S
S
-
F
-
D
P
T
-
1
(
3
-
4
)
-
2
0
1
4
0
6
3
0
.
5.

*

i
n
d
i
c
a
t
e
s

s
a
m
p
l
e

w
a
s

c
o
l
l
e
c
t
e
d

t
o

v
e
r
i
f
y

t
h
a
t

n
a
t
i
v
e

s
o
i
l

h
a
d

b
e
e
n

r
e
a
c
h
e
d
.
Sa
m
p
l
e

In
t
e
r
v
a
l

(f
t

B
G
S
)
Sa
m
p
l
e

D
a
t
e
F-
D
P
T
1

6
/
3
0
/
2
0
1
4
Co
n
c
e
n
t
r
a
t
i
o
n

(
µ
g
/
L
)
Lo
c
a
t
i
o
n
F-
D
P
T
3

6
/
3
0
/
2
0
1
4
F-
D
P
T
1
4

7
/
2
/
2
0
1
4
Gr
o
u
n
d
w
a
t
e
r

S
t
a
n
d
a
r
d
s
IM
A
C
F-
D
P
T
5

7
/
1
/
2
0
1
4
F-
D
P
T
7

7
/
1
/
2
0
1
4
F-
D
P
T
1
1

7
/
2
/
2
0
1
4
Ju
l
y

2
0
1
4
1
o
f

2
Geosyntec
Ta
b
l
e

2
.
T
5
.

F
A
D
A

I
n
v
e
s
t
i
g
a
t
i
o
n

-

S
P
L
P

A
n
a
l
y
t
i
c
a
l

D
a
t
a
L.
V
.

S
u
t
t
o
n

H
y
d
r
o
g
e
o
l
o
g
i
c

S
i
t
e

A
s
s
e
s
s
m
e
n
t
3-
4
7-
8
1.
5
-
2
.
5
5-
6
F-
D
P
T
4
18
-
2
0
*

7
/
1
/
2
0
1
4
2-
4
6-
8
3-
4
7-
8
15
-
1
6
*
7-
8
11
-
1
2
3-
4
7-
8
No
t
e
s
:
1.

U

i
n
d
i
c
a
t
e
s

r
e
s
u
l
t
s

b
e
l
o
w

t
h
e

m
e
t
h
o
d

d
e
t
e
c
t
i
o
n

l
i
m
i
t

(
M
D
L
)

a
n
d

<

i
n
d
i
c
a
t
e
s

r
e
s
u
l
t
s

b
e
l
o
w

t
h
e

p
r
a
c
t
i
c
a
l

q
u
a
n
t
i
t
a
t
i
o
n

l
i
m
i
t

(
P
Q
L
)
.
2.

µ
g
/
L

i
n
d
i
c
a
t
e
s

m
i
c
r
o
g
r
a
m
s

p
e
r

l
i
t
e
r
.
3.

S
P
L
P

i
n
d
i
c
a
t
e
s

s
y
n
t
h
e
t
i
c

p
r
e
c
i
p
i
t
a
t
i
o
n

l
e
a
c
h
i
n
g

p
r
o
c
e
d
u
r
e
.
4.

f
t

B
G
S

i
n
d
i
c
a
t
e
s

f
e
e
t

b
e
l
o
w

g
r
o
u
n
d

s
u
r
f
a
c
e
.
5.

S
a
m
p
l
e

I
D
s

f
o
r

t
h
e
s
e

l
o
c
a
t
i
o
n
s

w
e
r
e

a

c
o
m
b
i
n
a
t
i
o
n

o
f

l
o
c
a
t
i
o
n
,

d
e
p
t
h
,

a
n
d

s
a
m
p
l
i
n
g

d
a
t
e
,

i
.
e
.

S
S
-
F
-
D
P
T
-
1
(
3
-
4
)
-
2
0
1
4
0
6
3
0
.
5.

*

i
n
d
i
c
a
t
e
s

s
a
m
p
l
e

w
a
s

c
o
l
l
e
c
t
e
d

t
o

v
e
r
i
f
y

t
h
a
t

n
a
t
i
v
e

s
o
i
l

h
a
d

b
e
e
n

r
e
a
c
h
e
d
.
Sa
m
p
l
e

In
t
e
r
v
a
l

(f
t

B
G
S
)
Sa
m
p
l
e

D
a
t
e
F-
D
P
T
1

6
/
3
0
/
2
0
1
4
Lo
c
a
t
i
o
n
F-
D
P
T
3

6
/
3
0
/
2
0
1
4
F-
D
P
T
1
4

7
/
2
/
2
0
1
4
Gr
o
u
n
d
w
a
t
e
r

S
t
a
n
d
a
r
d
s
IM
A
C
F-
D
P
T
5

7
/
1
/
2
0
1
4
F-
D
P
T
7

7
/
1
/
2
0
1
4
F-
D
P
T
1
1

7
/
2
/
2
0
1
4
Me
r
c
u
r
y

M
o
l
y
b
d
e
n
u
m

N
i
c
k
e
l

P
o
t
a
s
s
i
u
m

S
e
l
e
n
i
u
m

S
i
l
v
e
r

S
o
d
i
u
m

S
t
r
o
n
t
i
u
m

T
h
a
l
l
i
u
m

Z
i
n
c
1

N
C

1
0
0

N
C

2
0

2
0

N
C

N
C

N
C

1
,
0
0
0
NC

N
C

N
C

N
C

N
C

N
C

N
C

N
C

0
.
2

N
C
0.
0
6

U

<

2
0

<

2
0

1
3
3

U

4
.
8

U

1
.
8

U

4
,
8
1
0

<

1
0

5
.
1

U

<

4
0
0.
0
6

U

<

2
0

<

2
0

<
1
,
0
0
0

<

4
0

1
.
8

U

<
2
,
0
0
0

7
9
.
4

5
.
1

U

<

4
0
0.
0
6

U

1
.
7

U

<

2
0

1
3
3

U

4
.
8

U

1
.
8

U

6
,
2
2
0

2
0
.
1

5
.
1

U

<

4
0
0.
0
6

U

<

2
0

1
.
6

U

1
3
3

U

<

4
0

1
.
8

U

2
,
7
6
0

4
3
.
6

5
.
1

U

2

U
0.
0
6

U

1
.
7

U

1
.
6

U

1
3
3

U

4
.
8

U

1
.
8

U

1
2
,
6
0
0

<

1
0

5
.
1

U

<

4
0
0.
0
6

U

<

2
0

1
.
6

U

1
3
3

U

4
.
8

U

1
.
8

U

3
,
5
8
0

1
2
2

5
.
1

U

<

4
0
0.
0
6

U

<

2
0

1
.
6

U

<
1
,
0
0
0

<

4
0

1
.
8

U

<
2
,
0
0
0

2
4
7

5
.
1

U

<

4
0
0.
0
6

U

1
.
7

U

1
.
6

U

1
3
3

U

4
.
8

U

1
.
8

U

6
,
0
9
0

1
0
.
1

5
.
1

U

<

4
0
0.
0
6

U

2
6
.
1

1
.
6

U

1
3
3

U

<

4
0

1
.
8

U

2
,
7
1
0

1
3
9

5
.
1

U

2

U
0.
0
6

U

<

2
0

1
.
6

U

<
1
,
0
0
0

4
.
8

U

1
.
8

U

5
,
7
4
0

2
5

5
.
1

U

<

4
0
0.
0
6

U

1
.
7

U

1
.
6

U

1
3
3

U

4
.
8

U

1
.
8

U

2
,
5
5
0

2
0
.
2

5
.
1

U

2

U
0.
0
6

U

<

2
0

1
.
6

U

1
3
3

U

4
.
8

U

1
.
8

U

4
,
4
1
0

3
7
.
5

5
.
1

U

<

4
0
0.
0
6

U

<

2
0

1
.
6

U

1
3
3

U

4
.
8

U

1
.
8

U

5
,
5
3
0

2
1

5
.
1

U

<

4
0
0.
0
6

U

<

2
0

<

2
0

<
1
,
0
0
0

<

4
0

1
.
8

U

2
,
7
6
0

1
2
9

5
.
1

U

2

U
Co
n
c
e
n
t
r
a
t
i
o
n

(
µ
g
/
L
)
Ju
l
y

2
0
1
4
2
o
f

2
Geosyntec
Table 3.T1 Summary of Index Test Results
Sample ID Sample
Type [1]
GSE
(ft)[1]
Depth [2]
(ft, bgs)
Materi
al
LL
(%)
PL
(%)
PI
(%)
Grave
l (%)
Sand
(%)
Silt
(%)
Clay
(%)
Fines
Content
(%)
U.S.C.S [3]
GP-13-S-17 GP 40.0 66.0 Ash NP NP NP - - - - - ML
GP-13-S-18 GP 40.0 70.0 Ash NP NP NP - - - - - ML
GP-14-S-18 GP 45.2 70.0 Ash NP NP NP - - - - - ML
GP-14-S-19 GP 45.2 75.0 Ash NP NP NP - - - - - ML
GP-15-S-16 GP 43.9 62.0 Ash NP NP NP - - - - - ML
GP-17-S-11 GP 32.5 43.7 Soil 85 40 45 - - - - - OH
GP -17-S-12A GP 32.5 44.9 Soil 126 60 66 - - - - - OH
GP -17-S-12B GP 32.5 46.2 Soil 67 31 36 - - - - - CH
GP-17-S-13 GP 32.5 50.0 Soil 50 24 26 - - - - - CH
GP-17-S-14 GP 32.5 54.0 Soil NP NP NP 0.1 58.8 24.7 16.4 41.1 SM
GP-17-S-15 GP 32.5 58.0 Soil 26 22 4 - 44.4 33.8 21.8 55.6 CL-ML
MB-2-S-14 GP 35.6 66.0 Ash NP NP NP - - - - - ML
MB-2-S-17 GP 44.6 78.0 Ash NP NP NP - - - - - ML

Notes:
[1] GP: Geoprobe, GSE: Ground Surface Elevation.
[2] Mid-depth of the sample.
[3] USCS classification is determined based on a combination of visual-manual classification and laboratory data.
[4] Elevations are referenced to the North American Vertical Datum of 1988 (NAVD88).

Table 3.T2. 1971 Pond Investigation - CCR Analytical Data
L.V. Sutton Hydrogeologic Site Assessment
Antimony Arsenic Barium Beryllium Boron Cadmium Total Chromium Copper Iron Lead Manganese Mercury Molybdenum Nickel
GP12 28-32 7/2/2014 < 6.17 67.6 467 5.99 41.2 < 1.54 46.8 76.8 13200 30.8 64.1 < 0.31 4.39 35.9
64-68 0.464 U 129 865 6.56 52.2 < 1.41 49 64 19,600 32.9 95.1 < 0.274 < 2.81 34.3
68-72 0.45 U 127 591 5.1 52.3 < 1.36 47.4 64.8 19,500 31.4 101 < 0.269 2.91 40.8
60-62 0.502 U 137 562 3.82 34.3 < 1.52 31.9 58.8 13,500 24.2 72.8 < 0.289 < 3.04 26.5
68-72 0.459 U 144 661 5.45 45.5 < 1.39 55.8 66.5 29,500 29.6 114 < 0.269 < 2.78 41
60-64 0.432 U 125 493 4.89 66.7 0.0432 U 65.1 64.5 43,400 24.6 160 < 0.249 2.68 47.3
68.7-70.7 0.453 U 35.6 265 3 30.2 0.0453 U 22.3 28.9 22,400 15.2 63.4 < 0.28 < 2.75 112
64-68 0.452 U 87.3 502 3.92 42.3 0.0452 U 43.8 59.1 14,500 26.1 87.6 < 0.255 < 2.74 29.8
76-80 0.457 U 155 735 5.7 55.3 0.0457 U 54.5 83.8 31,500 28.9 128 < 0.275 3.01 43.6
Notes:
1. 'U' indicates results below the method detection limit (MDL)
2. '<' indicates results below the practical quantitation limit (PQL).
3. mg/kg represents milligrams per kilogram.
4. ft BGS represents feet below ground surface.
5. S.U. represents standard units.
GP13
GP14
7/1/2014
7/2/2014
GP15 7/1/2014
MB2 6/25/2014
Location
Sample
Interval
(ft BGS)
Sample Date Concentration (mg/kg)
July 2014 1 of 2 Geosyntec
Table 3.T2. 1971 Pond Investigation - CCR Analytical Data
L.V. Sutton Hydrogeologic Site Assessment
GP12 28-32 7/2/2014
64-68
68-72
60-62
68-72
60-64
68.7-70.7
64-68
76-80
Notes:
1. 'U' indicates results below the method detection limit (MDL)
2. '<' indicates results below the practical quantitation limit (PQL).
3. mg/kg represents milligrams per kilogram.
4. ft BGS represents feet below ground surface.
5. S.U. represents standard units.
GP13
GP14
7/1/2014
7/2/2014
GP15 7/1/2014
MB2 6/25/2014
Location
Sample
Interval
(ft BGS)
Sample Date
Selenium Silver Strontium Thallium Zinc
< 6.17 0.293 U 322 < 9.26 51.4 37.7 7.62
6.68 0.267 U 491 < 8.44 53.3 32.3 8.69
5.71 0.259 U 388 < 8.17 53.4 30.1 8.61
< 6.08 0.289 U 295 < 9.12 36.3 34.2 8.65
6.04 0.264 U 598 < 8.34 55.4 29.5 8.63
< 5.24 0.249 U 561 9.28 55.8 25.9 8.28
< 5.49 0.261 U 237 62.5 27.5 29.3 7.89
< 5.48 0.26 U 318 1.1 U 43.6 27 8.23
6.74 0.263 U 587 1.11 U 57.6 27.8 8.41
Moisture
(%)
pH (Lab)
(S.U.)
Concentration (mg/kg)
July 2014 2 of 2 Geosyntec
Table 3.T3. 1971 Pond Investigation - SPLP Analytical Data
L.V. Sutton Hydrogeologic Site Assessment
Antimony Arsenic Barium Beryllium Boron Cadmium Calcium Total Chromium Copper Iron Lead Magnesium Manganese
NC 10 700 NC 700 2 NC 10 1,000 300 15 NC 50
1 NC NC 4 NC NC NC NC NC NC NC NC NC
GP12 28-32 7/2/2014 < 40 71.6 135 0.67 U < 100 0.33 U 3,240 1.3 U 28.1 33.4 U 4.7 U 529 < 10
64-68 5.1 U 251 67.6 0.67 U 137 0.33 U 4,420 < 30 2.8 U < 400 4.7 U 1230 < 10
68-72 < 40 254 32.1 0.67 U 177 0.33 U 3,730 < 30 2.8 U < 400 4.7 U 1180 < 10
60-62 5.1 U 247 90.1 0.67 U < 100 0.33 U 2,990 < 30 2.8 U < 400 4.7 U 603 < 10
68-72 < 40 263 28.1 0.67 U < 100 0.33 U 4,830 < 30 2.8 U < 400 4.7 U 560 < 10
60-64 5.1 U 208 17.8 0.67 U 100 0.33 U 6,350 < 30 2.8 U < 400 4.7 U 678 < 10
68.7-70.7 5.1 U 91.4 33.2 0.67 U < 100 0.33 U 6,440 1.3 U 2.8 U < 400 4.7 U 960 < 10
64-68 5.1 U 184 124 0.67 U < 100 0.33 U 4,320 < 30 2.8 U < 400 4.7 U 751 < 10
76-80 5.1 U 316 54.3 0.67 U 105 0.33 U 4,900 < 30 2.8 U < 400 4.7 U 849 < 10
Notes:
1. 'U' indicates results below the method detection limit (MDL)
2. '<' indicates results below the practical quantitation limit (PQL).
3. µg/L represents micrograms per liter.
4. SPLP represents synthetic precipitation leaching procedure.
5. ft BGS indicates feet below ground surface.
7/2/2014
MB2 6/25/2014
IMAC
GP15 7/1/2014
GP13 7/1/2014
GP14
Groundwater Standards
Location
Sample
Interval
(ft BGS)
Sample
Date
Concentration (µg/L)
July 2014 1 of 2 Geosyntec
Table 3.T3. 1971 Pond Investigation - SPLP Analytical Data
L.V. Sutton Hydrogeologic Site Assessment
GP12 28-32 7/2/2014
64-68
68-72
60-62
68-72
60-64
68.7-70.7
64-68
76-80
Notes:
1. 'U' indicates results below the method detection limit (MDL)
2. '<' indicates results below the practical quantitation limit (PQL).
3. µg/L represents micrograms per liter.
4. SPLP represents synthetic precipitation leaching procedure.
5. ft BGS indicates feet below ground surface.
7/2/2014
MB2 6/25/2014
IMAC
GP15 7/1/2014
GP13 7/1/2014
GP14
Groundwater Standards
Location
Sample
Interval
(ft BGS)
Sample
Date Mercury Molybdenum Nickel Potassium Selenium Silver Sodium Strontium Thallium Zinc
1 NC 100 NC 20 20 NC NC NC 1,000
NC NC NC NC NC NC NC NC 0.2 NC
0.06 U 141 < 20 <1,000 < 40 18 U 2,200 191 5.1 U < 40
0.06 U < 20 1.6 U <1,000 < 40 18 U 3060 249 5.1 U < 40
0.06 U < 20 1.6 U 133 U < 40 < 100 3,950 183 5.1 U < 40
0.06 U < 20 < 20 <1,000 < 40 18 U 3,870 102 5.1 U < 40
0.06 U < 20 1.6 U 133 U < 40 18 U 3,240 163 5.1 U < 40
0.06 U < 20 1.6 U 133 U < 40 18 U 9,010 197 5.1 U < 40
0.06 U < 20 < 20 <1,000 < 40 18 U 3450 240 5.1 U < 40
0.06 U < 20 1.6 U <1,000 < 40 1.8 U <2,000 281 5.1 U 2 U
0.06 U < 20 1.6 U <1,000 < 40 1.8 U 2,060 185 5.1 U < 40
Concentration (µg/L)
July 2014 2 of 2 Geosyntec

FIGURES
&>&>&>
&>
&>
&>
&>
&>
&>
&>
&>
&>
&>
&>
&>
@ A
@ A
@ A @ A
@ A @ A
@ A @ A
@ A
MW-16
MW
-
1
5
MW
-
2
0
MW
-
1
3
MW-16D
MW
-
1
5
D
MW
-
2
0
D
MW
-
1
3
D
MW

-

1
4
FDPT-9
FD
P
T
-
8
FD
P
T
-
7
FD
P
T
-
6
FD
P
T
-
5
FD
P
T
-
4
FDPT-3FDPT-2 FDPT-1
FD
P
T
-
1
5
FD
P
T
-
1
4
FDPT-13FDPT-12
FD
P
T
-
1
1
FD
P
T
-
1
0
So
u
r
c
e
:

E
s
r
i
,

D
i
g
i
t
a
l
G
l
o
b
e
,

G
e
o
E
y
e
,

i
-
c
u
b
e
d
,

E
a
r
t
h
s
t
a
r Geographics, CNES/Airbus DS, USDA, USGS, AEX, Getmappin g, Aerogrid, IGN, IGP, swisstopo, and
th
e

G
I
S

U
s
e
r

C
o
m
m
u
n
i
t
y
DPT Investigation and Groundwater Monitoring Well Locations L.V. Sutton Plant Figure 2.F1
P
a
t
h
:

(
\
\
c
h
a
r
l
o
t
t
e
-
0
1
\
d
a
t
a
)

M
:
\
G
I
S
\
D
u
k
e

S
u
t
t
o
n
\
M
X
D
s
\
R
e
p
o
r
t

N
o
.

1

A
d
d
e
n
d
u
m
\
F
i
g
u
r
e

A
.
F
1

-

F
A
D
A

I
n
v
e
s
t
i
g
a
t
i
o
n

L
o
c
a
t
i
o
n
s
.
m
x
d

2
9

J
u
l
y

2
0
1
4
;

R
D
o
n
a
h
u
e
Raleigh, NC July 2014³
Le
g
e
n
d
&>
DP
T

L
o
c
a
t
i
o
n
@ A
Mo
n
i
t
o
r
i
n
g

W
e
l
l
CC
R
CC
R

w
i
t
h

C
C
R
-
s
a
n
d

m
i
x
t
u
r
e
CC
R
-
s
a
n
d

m
i
x
t
u
r
e
0

4
0
0

8
0
0
Feet
No
t
e
s
:
1.

S
a
m
p
l
e
s

c
o
l
l
e
c
t
e
d

3
0

J
u
n
e

2
0
1
4

t
o

3

J
u
l
y

2
0
1
4
.
2.

D
e
p
t
h
s

p
r
e
s
e
n
t
e
d

a
r
e

i
n

f
e
e
t

b
e
l
o
w

g
r
o
u
n
d

s
u
r
f
a
c
e.
3.

F
A
D
A

i
m
p
a
c
t

b
o
u
n
d
a
r
i
e
s

d
e
t
e
r
m
i
n
e
d

f
r
o
m

f
i
g
u
r
e
s

p
ro
v
i
d
e
d

b
y

B
B
&
L
.
5.

C
C
R

i
n
d
i
c
a
t
e
s

c
o
a
l

c
o
m
b
u
s
t
i
o
n

r
e
s
i
d
u
a
l
s
.
6.

L
o
c
a
t
i
o
n
s

w
e
r
e

s
u
r
v
e
y
e
d

b
y

W
S
P

o
n

J
u
l
y

7
-
8
,

2
0
1
4
.
7.

H
o
r
i
z
o
n
t
a
l

c
o
o
r
d
i
n
a
t
e

s
y
s
t
e
m

U
S

S
t
a
t
e

P
l
a
n
e

1
9
8
3
N
o
r
t
h

C
a
r
o
l
i
n
a
,

U
S

s
u
r
v
e
y

f
e
e
t
.
8.

2
0
1
1

W
o
r
l
d

I
m
a
g
e
r
y

-

S
o
u
r
c
e
:

E
s
r
i
,

D
i
g
i
t
a
l
G
l
o
b
e
,
G
e
o
E
y
e
,

i
-
c
u
b
e
d
,

U
S
D
A
,

U
S
G
S
,
AE
X
,

G
e
t
m
a
p
p
i
n
g
,

A
e
r
o
g
r
i
d
,

I
G
N
,

I
G
P
,

s
w
i
s
s
t
o
p
o
,

a
n
d
t
h
e

G
I
S

U
s
e
r

C
o
m
m
u
n
i
t
y
.
PZ-5B
PZ-4B
PZ-3B
PZ-2B
CPT-1
CPT-2
CPT-3
CPT-4
CPT-5 CPT-6A
CPT-7A
CPT-8
GP-1
GP-2
GP-3
GP-4
GP-5
GP-6
SCPT-1
SCPT-2
SCPT-3A
SCPT-4
SCPT-5A
SCPT-6
SPT-1
SPT-2
SPT-3
SPT-4
SPT-5
SPT-6
SPT-7
SPT-8
SPT-10
SPT-11
PZ-1B
PZ-6B
B-1
B-2
B-3
HA-1-1
HA-1-2
HA-2-2 HA-2-1
HA-3-1
HA-3-2
L.V. SUTTON PLANT
HISTORICAL AND CONCEPTUAL
CLOSURE GEOTECHNICAL INVESTIGATION
PROJECT NO:
FIGURE
JULY 2014
3.F1
GC5592
0 600'1200'
SCALE IN FEET
N
LEGEND
GEOSYNTEC CONE PENETRATION TEST
GEOSYNTEC GEOPROBE (MAY 2014)
GEOSYNTEC GEOPROBE (JUNE-JULY 2014)
GEOSYNTEC MARSH BORINGS (JUNE-JULY 2014)
GEOSYNTEC PIEZOMETER
GEOSYNTEC SEISMIC CONE PENETRATION TEST
GEOSYNTEC STANDARD PENETRATION TEST
HISTORICAL HAND-AUGER
HISTORICAL PIEZOMETER
HISTORICAL STANDARD PENETRATION TEST
NOTES:
1.B-SERIES, HA-SERIES, AND PZ-B-SERIES POINTS ARE
SHOWN AT APPROXIMATE LOCATIONS.
2.POST-FIX 'A' FOR GEOSYNTEC INVESTIGATION POINTS
INDICATES A POINT ON THE DIKE OF 2006 INTERIOR
CONTAINMENT AREA.
3.THE LOCATIONS OF THE GEOSYNTEC BORINGS WERE
SURVEYED BY WSP SELLS, INC., IN MAY AND JULY 2014.
COOLING
POND
CANAL
CPT-1
GP-1
SPT-1
SCPT-1
2006 INTERIOR
CONTAINMENT AREA
1971
ASH POND AREA
1984 ASH
POND AREA
HA-1-1
B-1
PZ-1
PZ-1971
GP-7
MB-1

APPENDIX 2.A1

Field Forms
/4, !
Briefing Conducted By., 5igna ure:
� 'h� l
VVVVYII%% %W
Tailgate Safety Briefing Sign -In Log
a e:Time:
role name:
Sutton Steam Plant (Duke)
roe u er:
GN5616
This sign -in log documents the topics of the tailgate safety briefing and individual attendance at the briefing. Personnel who perform work operations onsite are required to attend
each safety briefing and acknowledge receipt of such briefings daily. Please provide a brief narrative of the following topics as applicable to the Project
Scope of Work
Soil (DPT) and GW MW sampling
HASP I THA review
SOP Review
PPE Requirements
C� hat
,
It'd r hr17)U �6>1 fnn r i -
�
Incident Revi•- N
Safety Alerts
Other:
Personnel Si
n-In List
Printed Name and Company
Signature p
Printed Name and Company
Signature
1
1. 1 �
i
7.
2. fll8.
4. JC�A �Pcj4c
10.
5.
11.
6.
12.
EHS 202 - Safety Meetings

Vi�U��` iliL�r:
Tailgate Safe BriefSign.-in Log
Brief mg on uc a y: grra ur®:
a e:
me:
Proiegt name:
Fromm Number:
Sutton Steam Plant (Duke)
GN5616
This sign -in log documents the topics of the tailgate safety briefing and individual attendance at the briefing. Personnel who perform work operations onsite are required to attend
each safety briefing and acknowledge receipt of such briefings daily. Please provide a brief narrative of the following topics as applicable
to the Pro ect
Scope of Work
Soil (DPT) and GW MW sampling
HASP ! THA review
SOP Review
PPE Requirementslp
l (1 U C�
may. r, �,� c, d t- �-c�f ru �j t
r-�t
" -
Incident Review
Safety Alerts
Other:
Personnel Sign
-in List
Prin d Name and Com an
Si ' pure
Printed Name and Company
Signature
1. rt+G'C ; ,
L.r
7.
i
2. ' U. 60
8.
3. M l r1-MEL- PAr'nlVk)N �f65YAtTf C.
9.
4 44 JeAAi Gear4 c
10.
5.
11.
6.
12.
EHS 202 - Safety Meetings

Vi'iV�iyIILW%,
Tailgate Safety Briefing Sign -in Log
Orteling ConducW
q y: Sigrta re: Date, ime:
Frolect name:
Sutton Steam Plant (Duke)
GN5616
This sign -in log documents the topics of the tailgate safety briefing and individual attendance at the briefing. Personnel who perform work operations onsite are required to attend
each safety briefing and acknowledge receipt of such briefin s daily. Please rovide a brief narrative of the following topics as applicable to the Pro"ect
Scope of Work
Soil (DPT) and GW MW sampling
HASP I THA review
SOP Review
PPE Requirements
f c ( IC -VT 1 0-"` 5 }f [ t vyl V�Cu' G ham, a� r f 174
Incident Review
Safety Alerts
Other:
Personnel Sl
n4n list
Printed Name and Cornpany
Siggature
Printed Name and Company
Signature
1.IN -& "j SALAD A'(..CO
7.
2. kIl" Ni , vA
8.
3. M I `NAg PR7tN�1� 1 b5S'rJ�
_ _.r
9.
4, A14 JP411,1 � ✓1�ec
10.
5.
11.
6,
12.
EHS 202 - Safety Meetings

Geosyntec
Tailgate
SafetyBriefing L Sign -in o
r g an u y; Sign re:
'-
Date:
3[Time:
ro ec name:
its ec umber;
Sutton Steam Plant (Duke)
GN5616
This sign -in log documents the topics of the tailgate safety briefing and individual attendance at the briefing. Personnel who perform work operations onsite are required to attend
each safety briefing and acknowledge receipt of such briefin s daily,
Please provide a brief narrative of the following topics as applicable to the Project
Scope of Work
Soil (DPT) and GW MW sampling
HASP / THA review
SOP Review
PPE Requirements
{{
Incident Review
Safety Alerts
Other:
Personnel Sian -in List
Printed Name and Company
Signature
Printed Name and Company
Signature
1�� ,� ff��
1. ��� ES ��C.W W
Lam-
7.
2. fi - r ors
Lill f1.
8
3,
g,
4.
10.
5.
11.
6
12.
EHS 202 - Safety Meetings

RECORD OF BOREHOLE ` � _ ' I Sheet I of
PROJECT: 7 V f Vn d %` bel I ►-1 ir�J P 4 6t P � rI DRILING VV COMPANY: S O C,,b rr (()o
C P�
PROJECT #: CSSGI �J DRILLER:
I.I �
LOCATION: !1 m I h t-an C� GEOSYNT 5ONNEL: ' 0
DRILL RIG: �
DATE'
fQ -3/1 1 �I
z
H
a
w
c
SOIL PROFILE
DESCRIPTION
)'y Yh P c(,, V rn + a,n -�/vp , VW 11
VV lya cp— ✓0,)ts
y
C 3S , 1lQj v�j
Sa hi(,y-zd J '
sC�
Sdt-V'u t7U, vu
0 f
cc
U
w WELL CONSTRUCTION
C DETAILS
U
W
a
VIELL CASING
f U Interval:
JoingType:
W V t.
Diamet
Slot Siz
q01
End Cap:
FILTER P C
Interval:
Type:
FILTER PAC SEAL
` Interval:
Type:
ANNULUS SEA
Interval:
Type: <
WELL COMPLETI
Pad:
Protective Casing:
DRILLING METHOE
Soil Drill:
Rock Drill:
1U we 1
1z

RECORD OF BOREHOLE E- -. Z Sheet 1 of
PROJECT: 5,) hC () -C'A t)fJ DRILING COMPANY: aeq- (m
PROJECT #: U 61&S Gf 7i DRILLER: W.
/ll ` GEOSYNTEC PERSONNEL: � l� On a,h �
LOCATION: Kr ) ('VI ; n �n
DRILL RIG: G�f h �� � -� m Z D r
DATE t 1
L� SOIL PROFILE
x a WELL CONSTRUCTION
wDESCRIPTION C DETAILS
A A U
W
rYl Cc� 1 Nm I b(� y�f �D (G��q 'ELL CASING
9 J ��' 1 I erval:
(a r' e S A !U p W7 G M terial:
a_ Di eter:
tau
J r Q a u Join Type:
�aSSlY�1e �C�1 , WEL S.
Intern
Ma eria
Diwnete
,, V r r- / Slot Size,
Jl (l End Cap:
�r '� J �, V C 6( t"rC� FILTER P
Interval:
FILTER PAC
Interval:
Type:
ANNULUS SE
Interval:
Type:
WELL COMPLE ION,
Pad: fG
Protective Casing:
DRILLING METH DS'
36 Soil Drill:
Rock Drill:

RECORD OF BOREHOLE - i —
Sheet i of
PROJECT: 5u it ry - �� DRILING COMPANY j ` , f7'1-� Cl/ 6
PROJECT #: C-1C -�-Y P- DRILLER:
W ► VA
. r /
LOCATION: W i I' r-t n GEOSYNTEC
DRILL RIG:
PERSONNEL:
`^P
C-5,."
DATE
ILA
SOIL PROFILE
A
wDESCRIPTION
C
WELL CONSTRUCTION
DETAILS
A
�
U
W
C4
a
(1(1 e ,Urn rv" S� N D,
ELL CASING
t
tervai:
VGt a S� C ��f
Meter:
2�Join
Di
Type:
31
61.10
r ,J
s o ��LU
WEL
Inte
Ma
Material
l�ubS
Diameter.
—�
e
C—( l� 5 , —sa
Slot Size:
End Cap:
o
d 1 ✓fir. fir`
J
+
��0 1
FILTER PA
Interval:
� o� � � 1 olc� S� c-!�l
s
Type:
,S
_
7 S
FILTER PACK EAL
Interval:
/
Type:
ANNULUS SEAL
Interval:
Type:
WELL COMPLETI
Pad:
Protective Casing:
Q I I eG ,Z .} J
DRILLING METHOD
Soil Drill:
l
Rock Drill:
2 D► � D 630 � I c�o'�
�
(F 'DP�'t C5-(�'

Mr-k-UKU Ut tSUKtHULE { _j-)p I -Lj Sheet 1 of
PROJECT: S L) fV f1 — 'F/10�Y DRILING COMPANY: G L�
PROJECT #: G�'q2 / DRILLER: Vv1 1�
LOCATION: N j^)C GEOSYNTEC PERSONNEL" 1
DRILL RIG:
DATE
SOIL PROFILE
x WELL CONSTRUCTION
WDESCRIPTION C DETAILS
A U
l ` SA r V b WELL CASING
r ' �j Interval:
OT 3 Ma rial:
Di eter:
�( dry- 0 Joint ype:
WELL CREEN
(V-W) Vi Interval:
sMaterial: p �
S� l S r ( f Diameter:
O Slot Size:
C O L'T V t (Q S End Cap: �—
FILTER PA
Interval:
sI�V U 1�� Type:
FILTER PAC EAL
S C /1 LS r�.t �[ Interval:
f ,.{ � Type:
ANNULUS SE L
S\ 1 S16C Nb S C.10 rcL--# d, Interval:
Type:
1 WELL COMPL
S� 1 C D r� r� ` G h teY .4) f Pad:
Protective Casin
DRILLING METH DS
C C L I V M �`1►� Soil Drill:
q 1VV 4�r , Rock Drill:
.-
ra� Ca, .
s �- C
zo 1 10-7 ,1 co,

RECORD OF BOREHOLE -F—Sheet 1 of
PROJECT: S\7wr) - p1Am DRILING COMPANY: -SPK7c r�fi(.Co
PROJECT #: �� 5� 2 DRILLER: Wk 4l tA�/ f
'" GEOSYNTEC PERSONN[4L
LOCATION: v V li rti , � �„ Al G
DRILL RIG: "1 fp (2-'
DATE
SOIL PROFILE
w WELL CONSTRUCTION
wDESCRIPTION C DETAILS
A � U
W
O-q v / b � { u b' qL WELL CASING
1 ` l Interval:
Material:
t ! ► (� 0 SS , �� iameter:
Jo' t Type:
S WE SCREEN
lntery 1:
tvi_G� _t U Materi
-_Diamnete
)&) % Slot Size..
Q I End Cap:
/ n v Cq ry C0 FILTER PA K
` Interval:
Type:
�Z�Ip Sfs O j p f C �, h FILTER PAC SEAL
Interval:
Type:
flu-- � ANNULUS SEA
Interval:
Type:
Cne / ( V Pad:
CC3MPLETi N:
Protective Casing:
DRILLING METHOD
SAWD Soil Drill:
Rock Drill:
SS'lp jS
a)
2d)
,-i D * /),

RECORD OF BOREHOLE r a Sheet I of
PROJECT: So Vbv-% - F Q R DRILUNG COMPANY: :3^ f-0-� CC0
PROJECT #: EjC �Z DRILLER: VV r I I 1GL I (1
GEOSYNTEC PERSONNEL:.
LOCATION: W jklt, ]'?l � po r, tj
DRILL RIG:
DATE -1 1 `
SOIL PROFILE
wDESCRIPTION
A
0-1 S.KN 0 Ali
jDrmc �Isr S�� SSbl Lc��
g4'
�lvAA1,
"f 9A
(61�6tad SS+—b6— 'S—
�a UA
W WELL CONSTRUCTION
C DETAILS
� U
W
WELL CASING
jot terva]_
Y
.loin Type:
WEL SCREEN
Interva ;
Nlateria :
Diamete :�
R1nt S67P
End Cap:
FILTER P K
Interval: .
Type:
_
FILTER PA
Interval:
{�Nr
Type:
ANNULUS SE k
Interval:
"Type:
�-
WELL COMPLEX
Pad:
Protective Casing:
DRILLING MET]
Soil Drill:
Rock Drill:

RECORD OF BOREHOLE - & T-, `-A- Sheet l of
PROJECT: , )Cjlvh ' F16�DM DRILING COMPANY -
PROJECT DRILLER: r } r g
1 r G GEOSYNTE P RS�j L:' i
LOCATION: W � 1 YYl �r � n 1 V �
</`J►l
DRILL RIG: L�Z��
DATE
SOIL PROFILE
WELL CONSTRUCTION
W
WDESCRIPTION
�
U
DETAILS
q
W
a
�n,II I
iUw� Joidv�M S-t lV P LV 1 oIV,�
WELL CASING
serval:
gS u �t { Y ►` f� �Lf 1� ,
JJ
�o r'
aterial:
D eser:
�^
Joi t Type:
E SCREEN
Irate 1: �
Mate 1:
(Q11n.r Oxf SIB V6� 1�
Diame r:
Slot Six :
End Cap
FILTER. ACK
-`
ly-�.�
'
7.� l
Interval:
Type:
-
rrx, ✓J�}Y1
FILTER P CK SEAL
Interval:
bf b
,V
Type:
ANNULUS EAL
Interval:
h ` 1
I I
WELL COMP ETION:
J
Pad:
Protective Casi g:
r h
�1" v 1✓ 012-4 t\j C1
'DRILLING ME HODS
r lIl s.�'�'
Soil Drill:
Rock aril I:

RECORD OF BOREHOLE —1 Sheet 1 of
PROJECT: ' 0 itv r� T 4 0 DRILING COMPANY: -
PROJECT #: �s DRILLERW-. ,
GEOSYNTEC PERSONNEL.
LOCATION:"
DRILL RIG: L a ���► `^C
[SATE
F
A.
w
A
SOIL PROFILE
DESCRIPTION
U
m� d IU � � h r 5 / � 5,4 (� v✓�
r1 �1 (p6 ff,b6y `�I
J
q raj s Mir a w 0,81- -
S '
fm
- l ► tir" bf0 err WP.
Trkh S, n Gl G.f a-
lo' 1
ltifi% �J�-V s�n6p� Sri Iww�d,
faDu Sfle
F X
q�n
WELL CONSTRUCTION
DETAILS
CASING
eter:
Type:
SCREEN C
End Cap:
FILTER P
Interval:
Type:
FILTER PAC S At
Interval:
- Tti pe:
ANNULUS SEA
ffl Interval:
Type:
WELL COMPLETI N`;
�f
Protective Casing:
DRILLING MET]
Soil Drill:
Rock Drill:

W-4
3i5
RECORD OF BOREHOLE — cf Sheet I of
PROJECT: S,; rb h ` FflO fi DRILING COMPANY: , fy-- tnrLC6
PROJECT #: 6-)a5l // DRILLER: We I
r� GEOSYNTEC PERSONNEL:
LOCATION: U11 = � (Y1 � �� � � 1 v
DRILL RIG: 17 ?j%/ �`—c—
DATE
SOIL PROFILE
x w WELL CONSTRUCTION
WDESCRIPTION DETAILS
A U
W
ar h JAW f 'r� ✓ J ry
nLL
CASING
I Ial:
Ma erial: , „ n
�Ja Ssl�j 4 (��J Di eter: N�} U��
Joint ype:
WELL CREEK
s
n� Interval 0, `�I Material.
I �Vv 6,,v, SAW
� %�j V „ b , Diameter.
Slot Size:
End Cap:
FILTER PA
Interval:
Type:
(A 1 d A, � JJY� V FILTER PAC AL
Interval: /.
Type:
c
ANNULUS SE
1 f 'fir a +' C� Interval:
1 f 0 W^ .l AN P , t, a tr J Type:
�6 � ' S►1} � � � � � � l � � C ���1 WELL COMPLE ON:
Pad:
_ tective Casing:
DRILLING METH S
Soil Drill:
— Rock Dri It:
o I,�
)A

RECORD OF BOREHOLE - � — Sheet I of
PROJECT: L! tr[x1 - FA JA DRILING `COMPANY:
PROJECT #: (,ss Q DRILLER; VV, i I K4 t j
GEOSYNTEC PERSONNEL:
n
LOCATION: W I � M i n G( �r i v% �� ,p� �� L
'y
DRILL RIG: L'f� U�'�
DATE -1 , I
SOIL PROFILE
WELL CONSTRUCTION
a
WDESCRIPTION
C
U
DETAILS
C
W
—�
V(,� �► C Ot l� S i I t �—S at I-�t
9
Ida /
WELT. CASING
terval:
(�
aerial:
Di eter:
Jain Type:
WELL EN
(
Interval:
Material:
Diameter:
Slot Size:
I C O 0-r
End Cap:
PAC
Salti ^l c 1 �� � �
FILTER
Interval:
�'i'I �
Type:
AT�
� ►� � � � � �F�i � �� S� h
�,�
to h S
FILTER PACKS
Interval:
Type: �
ANNULUS SEAL S
e- CI t ,V M
" 1 f iy i i. S}�-�
'Interval:
Type:
WELL COMPLETIO
ad:
CLh1 O %�a2 ! IVC,
Protective Casing:
_OoT-OPT-qJ
DRILLING METHODSCv
Soil Drill:
`tiO-ToZLe Q(j
Rock Drill:
ss -� -ba -1 o CZ
Vv t 1 1

RECORD OF BOREHOLE —L)p—j—jj Sheet l of
PROJECT:U "l1 -V�A-bA DRILMG COMPANY:&I cc-
PROJECT #: G us- g2 DRILLER: Vv, w 4 �
1_I �,.iz GEOSYNTEC PERSONNEf
LOCATION: Yv I rVA n q - , C
DRILL RIG: 1 & y�G�-
DATE
F
a
W
A
SOIL PROFILE
DESCRIPTION
SA M 0
JL 1 V T
�-►'� AA, ,Eh)re
SN R
ISO yr c d wf\,, DI
ti:� { a+0
SoJu-o-mod , - -ra c-A- �L a-A
Sf -c CJ-1
wNp dr- �of-\Nq
IWO- S-S- F - () p T I t ( 7 - �)
-Zu F�-" q
SE- F---�)a`f 11 (Ii
-i�
_2a1u0`40'i-@ tad
U
O
W
WELL CONSTRUCTION
DETAILS
O
U
W
a
11jiJELL CASING
V i I`�iterval-
4uI Joint
WELLS REEN
Interval:
3
Material:
Diameter:
Slot Size:
End Cap:
/
FILTER PACK
Interval:
Type:
FILTER PACK S
Interval: i
J,
Type:
ANNULUS SEAL C
Interval:
WELL COMPLETIO :
Pad:
Protective Casing:
DRILLING METHODS
Soil Drill:
Rock Drill:
ND We)"]

RECORD OF BOREHOLE LjD.—jj Sheet 1 of
PROJECT:s(J VtJh - A 1) A DRILING COMPANY:S�(�� C�v
PROJECT #: bus-S-(j`Z DRILLER: V/
��/ GEOSYNTECPERSONNEL)
.
LOCATION: Y � OLV 'r` NJ Z W 198 n C��► �-2
DRILL RIG: �% ZZ ► Q
DATE -7 _ -7 _ILA
SOIL PROFILE
x
WDESCRIPTION
A
6-fSo�I J
(rx ., C iA I,jrP
�1 �hv o r o-4-o�, S NNb
�I- �n
'5a--tuf6--V-j JO-OL
SA/V
S�
tiC�
�/p s Uv,�p�s ca fl-ec�col
W WELL CONSTRUCTION
C DETAILS
� U
w
WELL CASING
Join\Tppe:
?j9s�
Diameter:
Slot Size:
--End Cap:
FILTER PA
J� Interval:
Type:
FILTER PACK E
Interval:
Type:
�JI ANNULUS SEAL
Interval:
WELL COMPLE1
Pad:
Protective Casing:
DRILLING MET[
Soil Drill:
Rock Drill:

RECORD OF BOREHOLE -t j -r3 Sheet 1 of
PROJECT: S (f-}ids —040iff DRILING COMPANY:
PROJECT #: GIGS-Tq2 DRILLER: IN, I I
GEOSYNTEC
,A� PERSO' NEIS►
LOCATION: V r I ►'►'1 i Y' � I v
DRILL RIG: Z4"1
DATE ^ ,2 " ` .
l
SOIL PROFILE
WELL CONSTRUCTION
F
W
W
DESCRIPTION
A
G
DETAILS
A
_
w
c4
I-fPf / / 12S
if l/l/� T h
WELT. CASING
/
nter""
Vh c d IVY a h �- ��a v✓r• S�
aterite
'ameter:
Y� I fd" -� l�" `i 1 Q l ��'
Jo ntType:
WE L SCREEN
�Inte at:
Mate
Diann er:
Slot Si e:
V"
End Ca
Q
O n-
l�J
Vrj�l�O ) G��
FILTER ACK
nterval:
Type:
FILTER PA K SEAL
Interval:
Type:
ANNULUS SE L
{
b \av)n:]
Interval:
Type:
WELL ION:
P
Protective Casino:
DRILLING METH DS
Soil Drill:
Rack Drill:

RECORD OF BOREHOLE - — Lj Sheet l of
PROJECT:, j {'Wp DRILING COMPANY: fp C
PROJECT C'S DRILLER: 1 i
`_ GEOSYNTEC PERSONNEL"-
�1v \1�M ��`� �l �� +�
DRILL RIG: ' 7 f
DATE 7,
i
x
F
a
w
A
SOIL PROFILE
DESCRIPTION
C�,PvA
i s u w S J, S M p r PCs
�AA
rnr d N w aW C to, owh %ANb
S te'C1,+c.0
SRC
V P wv, S 1ktQ C t
C —tid c� 0102
1-0 `LI °1a1e(r`6
W WELL CONSTRUCTION
C DETAILS
�7 U
(,,hy WELL CASING
serval:
a mete Ma 1 tI n
i meter: V V
Jai Type:
1 l _ SC EEN
rn. Intery l-
J_ rR .
slot Size
End Cap:
FILTER
Interval:
• Type:
ILTER PAC Sl
Interval:
Type:
ANNULUS SEA
Interval:
Type:.
WELL COMPLE'
ad:
Protective Casin:
DRILLING MET]
Soil .Drill:
Rock Drill:

RECORD OF
PROJECT:(]
PROJECT #:
LOCATION: V ` ;'rn I F+ , �,m
DRILL RIG:
DATE —1
SOIL PROFILE
F
W DESCRIPTION
Y W
( S-, kA- � , C C PC5
V`
S ot"IU �
DRILING CO,'vIPANY: � CLDM CC)
DRILLER: UA.t j
GEOSYNTE PE ONNE :
I s C (fir b�pv� b I ac�c
C A TW u t
Swo
�n -S:A Nr��
(�e tv\ratLP
?NIP 6 p- 10(-/��
�)o VLVVVIO L's rouecfi�
Sheet 1
W WELL CONSTRUCTION
C DETAILS
r7 U
( WELL CASING
U�t terval;
terial: A 'd
Di eter: !V
Joi Type: J
7S WEL SCREEN
Intery
Materi
Diarnef e
Slot Size:
/ End Cap:
7i t FILTER PA
Interval:
Type:
FILTER PAC SEAL
Interval:
Type:
v!
ANNULUS SEA
m
Interval:
Type:
WELL COMPLE
O
Pad:
Protective Casing:
DRILLING METH
D5
Soil Drill:
Rock Drill:
�)
/

�
Cir
GeosConsultants of NC, PC
V O S� `^G c
4601 Six Forks Rd
4601 Six
consulturi is
Suite 340
Raleigh, NC 27609
GROUNDWATER SAMPLING LOG
Project Name Duke -Sutton
Date —4
Project Number GC5592 Phase/Task
Location Wilmington, NC
Personnel .
Well ID ll lr1 l' (, Screen Interval (ft) 1K — 1
DTW (ft), 93
Pump/Tubing Setting (ft) 1 2S I Jilt,
Well Diameter (in) ", I
DTB (ft)
Tubing Diameter (in) , it
Depth Measurement Location TOC
Specific
Purge Rate pH Conductance Temp.
Turbidity ORP DO
Time (mUmin) DTW (ft) (S.U.) (µS/cm) CC)
(NTU) (mV) (mg/L�X)y
/
7�
// e 120D i
l fp 3 1 �.J t/L1 I I A 31. � 1
1 6v �� A
' I 1
1 , I 'Ten'a, i I
1 s Q.
1 QC10 j ,014
1 I a v ,3 I
_69 3 ,
iaoo I a Y 9
21,3
qN3 I 1 (�.
1 I
1 1 '
, s Gq
1 f
1 i1
1 1
1
111
f 1 1 1
1 1
I1
1
1 1
I
1 1
1
I
! 1
! ! 1
1 I
1 7
1 1 ! 1
1 1
i 1
1 I
1 I 1 1
1 1 1
1 1
Y
D 6771-
Criteria EPA Region 4 102
pH 0.1 0.2
Cond. / Sr). Cond. 1 5% 3%
10% or <10 NTU none
10% or 0.2 mg/L 10% or 0.2
none 20 mV
54MPI-e CUU cT5D AT 12: I1
WELL VOLUME _ (TOTAL WELL DEPTH - STATIC DEPTH TO WATER) X WELL CAPACITY
_ ( feet - feet) X gallons/foot = gallons
WELL CAPACITY (gallons/foot): 0.75'= 0.02: V= 0.04; 1.25"= 0.06; 2"=0.16; 3"= 0.37; 4"= 0.65; 5"= 1.02; 6"= 1.47; 12"= 5.88
EQUIPMENT VOLUME = (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
_( gal/ft X feet) + gallons = gallons
TUBING INSIDE DIA. CAPACITY (gal/ft): 1/8"=0.0006; 3/16"=0.0014; 1/4"=0.0026; 5/16"=0.004; 3/8"0.006; 1/2" = 0.010

C_JF-eC3SyU1teC ® Geosyntec Consultants ofNC, PC
Suit Six Forks Rd
Suite 340
C orzs ultarit s Raleigh, NC 27609
GROUNDWATER SAMPLING LOG
Project Name OUXf VTT04 Date_ �7- l b2_ l 1
Project Number CRSFq', Phase/Task _
Location L- I S oTlrk �'i�DcM P L 1C Personnel to e 0f\Sa I &'
Well ID —m—W -1 %0 Screen Interval (ft) DTW (ft) . , 9 '2—
Pump/Tubing Setting (ft)
Well Diameter (in) DTB (ft) Zf
Tubing Diameter (in) j
Depth Measurement Location To
Specific
Purge Rate T pH Conductance Temp. Turbidity ORP DO
Time (mUmin) DTW (ft) S.U.) (µS/cm) (°C) (NTU) (mV) (mg/L)
L1, 1 X_ 6 3 , 4 Z i � �2. 2. 0
e 7 _ r I
1 �.' i �• • 1 i 1 S-w/�w{
LY I 1 r Y-2— -' —_. I
1
5 1 22_.� 1 , . 2l�j
'L I %�t, 1>r�
119
1 I e
1 1 e i
r e r r 1
1 1 I I f I I
1 1 1
Stabilization
ASTM D 6771-
NOTES
Criteria
EPA Region 4
02
pH
0.1
0.2
us'
Cond. / Sp. Cond_
5%
3%
r 5p ✓ry �' L� � �t
Turbidity
10% or <10 NTUI
none
DO
10% or 0 2 mg/L
10% or 0.2 mg1L
ORP
none 1
20 mV
VOLUME = (TOTAL WELL DEPTH -STATIC DEPTH TO WATER) X WELL CAPACITY
_ feet - feet) X allons/foot gallc
CAPACITY (gallonsifoot): 0.75"= 0.02; 1"= 0.04; 1.25"= 0.06; 2"=0.16; 3"= 0.37; 4"= 0.65: 5"= 1.02: 6"= 1.47; 12"= 5.88
'MENT VOLUME = (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
�( gal/ft X feet) + gallons = gallons
0 INSIDE DIA. CAPACITY (gal/ft): 1/8"=0.0006; 3/16"=0.0014; 1/4"=0.0026; 5/16"=0.004; 3/8"0.006; 112" = 0.010
3(1

Geo
Cxec3syrl tVC 460syntecConsultantsofNC,PC
Six Forks Rd
Suit Suite 340
C"ri S -ul tula t S Raleigh, NC 27609
Gs ROUNDWATER SAMPLING LOG
Project Name {ZXIV : U f-roj Date t `• 1 !
Project Number 6165 V �Z_ Phase/Task 02_13
M. Location 44+6*r L -Y , 5 ryoO 51-60n F1-,Jr K Personnel M C 1S' IIt
Well ID _ .r Screen Interval (ft) I - I I DTW (ft) �! d
Pump/Tubing Setting (ft) 6 141) 70
Well Diameter (in) rrvl DTB (ft) 4
Tubing Diameter (in)/
Depth Measurement Location $.
Specific
Purge Rate
pH
Conductance
Temp.
Turbidity
ORP
DO
Time
(mL/min)
DTW A
(S.U.)
(PS/cm)
CC)
(NTU)
(mV)
(mg/L)
2
if r
I
6.13
;35.
� 2 X>
� 3 ,b
I 6f y
� ?.•G
33.3
iJLL
i
/f+�—�%
t✓
a
- �01 �'
I r r
i T 1 1
I .� ,
i {� ,
i e
M
I
.�
d
�ZA
ZI40
I
6{qo
I ' 1,
I
1
I
{
t
1
r
1
1
r
t
{
t
1
1
i
I
i
i
1
r
n
_
i
I
1
e
1 Reg
ion
D 6771-
EPA Rion 4
)H 0-1 02
Cond. / Sp. Cond. 5% 3%
Turbidity 10% or <10 NTU none
)O 10% or 0. 2 mg/L 10% or 0.2
)RP none 120 mV
6 piM pC ir CPLI
WELL. VOLUME = (TOTAL WELL DEPTH -STATIC DEPTH TO WATER) X WELL CAPACITY
_ ( feet - feet) X allons/foot gallons
WELL CAPACITY (gallonslfooty 0.75"= 0.02; 1"= 0.04; 1.25"= 0-06; 2"=0-16; 3"= 0-37; 4"= 0.65; 5"= 1,02; 6"= 1.47; 12"= 5.88
EQUIPMENT VOLUME = (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
_( gallft X feet) + gallons = 2allons
TUBING INSIDE DIA. CAPACITY (gala: 1/8"=0.0006; 3/16"=0.0014; 1/4"=0.0026; 5/16"=0.004; 3/8"0.006; 1/2" = 0.010
I� 14 q y,g

Geo
C-xe"syritc!cco* 4601 Sixc Consultants ofNC, PC
4601 Six Forks Rd
Suite 340
consul taints Raleigh, NC 27609
GROUNDWATER SAMPLING LOG
Project Name -A ("'If sui 7 f;*J
Date /ice l r32 / j '9
Project Number
Phase/Task
Location
Personnel /4
Well ID 41AW Jn
Screen Interval (ft)
DTW (ft)
PumpfTubing Setting (ft)
Well Diameter (in)
DTB (ft)�
Tubing Diameter (in).
Depth Measurement Location Z4F'
Specific
Purge Rate
pH Conductance Temp.
Turbidity ORP DO
Time
(mL/min)
DTW (ft) (S.U.) (VS/cm) CC)
(NTU) (mV) (mg/L)
-
,
�-�A try
Stabilization
i i i i i
°
1 1
f 1 l i 1 1
1
1
1 I i 1 i 1
ASTM D 6771- NOTES
i i
i i
1 1
1 f
Criteria
EPA Region 4 02 5
H
Cond. / Sp. Cond.
0.1
5%
02 %aftelnTE' M1a/l�Y
3/0
Turbidity
DO
10% or <10 NTLJJ
10%or0.2mg/L
none
4 rf
10%or0.2mg/L � /: �i-/l �~M �1el
�! Y�' W 7
— M,F�c
ORP
none
20 mV
VOLUME = (TOTAL WELL DEPTH - STATIC DEPTH TO WATER) X WELL CAPACITY
_ ( feet - feet) X gallons/Foot =
CAPACITY (gallons/foot): 0.75"= 0.02; 1"= 0.04; 1.25"= 0.06; 2"=0.16; 3"= 0.37; 4"= 0.65; 5"= 1.02; 6"= 1.47; 12"= 5.88
'MENT VOLUME = (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
_( alfft X feet) + gallons = aal
3 INSIDE DIA. CAPACITY (gal/ft): 1/8"=0.0006; 3/16"=0 0014; 1/4"=0.0026; 5/16"=0.004; 3/8"0.006; 112" = 0.010
?" v 3,-3 �-r : e- Pr 9
o,Fr —

Consultants of NC, PC
4601 Six
4601 S Forks Rd
t
C On.S ulta_n i s
Suite 340
Raleigh, NC 27609
GROUNDWATER SAMPLING LOG
Project Name Duke -Sutton
Date 1 )L
Project Number GC5592
Phase/Task
Q a nj
Location Wilmington, NC
Personnel JC'v?��
Well ID �S Screen Interval (ft)
40' "
DTW (ft) 3,q 3
Pump/Tubing Setting (ft)
Well Diameter (in)
"'
DTB (ft) LO--,Sy
Tubing Diameter (in)
n
Depth Measurement Location TOC
Specific
Purge Rate pH
Conductancq
Temp.
Turbidity ORP DO
Time (mL/min) DTW A (S. U.)
(µS/cm)
(°C)
(NTU) (mV) (mg/L)
iC anti L d411
0 / ;
9/� I F I �(to
7S
I aa.3
I a I q
I 9 I G % S 1
�.cR/.��_
J
Ir E 0i
R AX
I I I
1 I I 1
!
f 1 I
1 I I 1
I 1 1 t
1
1
[ I I
1 1 1
I 1 I t
I 1 1 I
1
1
I 1 1
1 1 1
1 I t 1
1 I 1 1
!
r
f 1 1
r 1 1
t 1 1
1
1 I
1
1 1 I
I
r1
I 1 i
Stabilization ASTM D 6771-
Criteria EPA Region 4 02
pH 04 0.2
Cond. / Sp. Cond, 5% 3%
Turbidity 10% or <10 NTU none
DO 10% or 0.2 mg/L 10% or 0.2 mg/
ORP none 20 mV
r-
JA M PLt:
WELL VOLUME _ (TOTAL WELL DEPTH - STATIC DEPTH TO WATER) X WELL CAPACITY
_ ( feet - feet) X gallons/foot = gallons
WELL CAPACITY (gallons/foot): 0.75"= 0.02; 1"= 0.04; 1.25"= 0.06; 2"=0.16; 3"= 0.37; 4"= 0.65; 5"= 1.02; 6"= 1.47; 12"= 5.88
EQUIPMENT VOLUME _ (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
_( gal/ft X feet) + gallons = gallons
TUEING INSIDE DIA. CAPACITY (galit); 1/8-0.0006; 3/16"=0.0014; 1l4"=0.0026; 5/16"=0.004; 3/8"0.006; 1/2" = 0.010
i1

Gec)syiritec
Geosyntec Consultants of NC, PC
4601 Six Forks Rd
c on S ulta rit s
Suite 340
Raleigh, NC 27609
GROUNDWATER SAMPLING LOG
Project Name Duke -Sutton
Date
Project Number GC5592 Phase/Task
Location Wilmington, NC
Personnel III.
Well ID �Q Screen Interval (ft) — /
DTW (ft)
Pump/Tubing Setting (ft)
Well Diameter (in)
DTB (ft)
Tubing Diameter (in).
Depth Measurement Location TOC
Specific
Purge Rate pH Conductance . Temp.
Turbidity ORP DO
Time
(mUmin) DTW A (S.U.) (µS/qm) (°C)
(NTU) (mV) (mg/L)
sr
I I a I •,L
Ira.
: p
jz
I
I I I o!• s Ze.r
1
1
1.
171
,.
srto 3.I I
I
1 t I
J
1
1
1 A 1 I
1 • 1 1 1
1
1
1 1
1 1
or
1
1
1
•
i
i • i i • I •
i
i (�f/ i
,
1
1
1 r
I I L13, (a1
1
IV.
r r 1
I -140. i
y
I
1 1 I I 1 •
1
(�
j 1
1 1 i 1 ,
X
Z�•� I i
1
1
i 1 1 A
r 1 f 1
1
1
1 1
1 1
1
i i 1 1
1
1 1
Stabilization ASTM D 6771-
Criteria EPA Region 4 02
pH 0.1 0.2
Cond. / Sp. Cond, 5% 3%
Turbidity 10% or <10 NTU none
DO 10% or 0.2 mg1L 10% or 0.2 mg/
ORP I none 1 20 mV
JAMPLIr dOWZY& L40 P3TO
WELL VOLUME _ (TOTAL WELL DEPTH - STATIC DEPTH TO WATER) X WELL CAPACITY
_ ( feet - feet) X gallons/foot = gallons
WELL CAPACITY (gallons/foot): 0.75"= 0.02; 1"= 0.04; 1.25"= 0.06; 2"=0.16; 3"= 0.37; 4"= 0.65; 5"= 1.02; 6"= 1.47; 12"= 5.88
EQUIPMENT VOLUME = (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
_( gal/ft X feet) + gallons = gallons
TUBING INSIDE DIA. CAPACITY (gal/ft): 1/8"=0.0006; 3/16"=0.0014; 1/4"=0.0026; 5/16"=0.004; 3/8"0.006; 1/2" = 0.010
Scr&. ^ L--I f
12' AAal I r 3•f�i'
e i
Tt'�
�• 11.tic ►z 15•,�,I

C;e"Syritec Q 460[Sitec Consultants ofNC, PC
Suit Six Forks Rd
Suite 340
COn_Sul tuylt S Raleigh, NC 27609
GROUNDWATER SAMPLING LOG
Project Name �yyy is s i,s'ry tj Date OR: l D)
-r
Project Numbet y4C'559! _ Phase/Task CIV-1-113
Location (.. V SvT-rd,,. S Tf,4M L,AAIX Personnel 1)4. R/Vp LLB )
Well ID M W 1(;-V Screen Interval (ft) l DTW (ft)
Pump/Tubing Setting (ft)
Well Diameter (in) DTB (ft)
Tubing Diameter (in) % e
Depth Measurement Location rd[�
Time
Purge Rate
(mUmin)
DTW (ft)
pH
(S.U.)
Specific
Conductance
(µS/cm)
Temp.
(°C)
Turbidity
(NTU)
ORP
(MVV)
DO
(mg1L)
157
23.E
1�1
1 2-7u
i ✓�
C
1 V
r l
1
1-2
53;
212,
3140
; r ,
r a
Q
0.
(17
�,�
; /��..
; r
i ✓� i
; 2
_
zz
,16
;
zq
;
; 5-
,o
r
1
"
i
Stabilization
Criteria
EPA Region 4
ASTM D 6771-
02
NOTES
pH 0.1
02
Cond. / Sp. Cond. 5%
3%
Turbidity 10% or <10 NTUI
none
DO 10% or 0.2 mg1L
10% or 0.2 mg1L
ORP none
20 mV
LL VOLUME = (TOTAL WELL DEPTH -STATIC DEPTH TO WATER) X WELL CAPACITY
feet) X gallons/foot = gallons
_L CAPACITY (gallons/foot): 0.75"= 0.02; 1"= 0.04; 1.25"= 0.06; 2"=0,16; 3"= 0.37; 4"= 0.65; 5"= 1.02; 6"= 1.47; 12"= 5.88
JIPMENT VOLUME = (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
_( gal/ft X feet) + gallons = gallons
SING INSIDE DIA. CAPACITY (gal/ft): 1/8"=0.0006; 3/16"=0.0014; 1/4"=0.0026; 5/16"=0.004; 3/8" 0.006; 1/2" = 0 010 -

Cxec3syiritec C:*
c"ri stllta irit s
- GROUNDWATER SAMPLING LOG
Geosyntec Consultants of NC, PC
4601 Six Forks Rd
Suite 340
Raleigh, NC 27609
Project Name 0l/ K c VTTVADate 0
Project Number 4e-S 3 g'Z Phase/Task ® 23
Nt 1)IE '�
Location L. ✓, SOTT bk% 5TC4M PLpo4 Personnel M /oil-r11*IN
Well Ib / VL UO Screen Interval (ft)
Pump/Tubing Setting (ft) M .-
Well Diameter (in) 2
Tubing Diameter (in)
DTW (ft)
DTB (ft) j ;L , d
Depth Measurement Location TO
Specific
Purge Rate
pH
Conductance
Temp.
Turbidity
ORP
DO
Time
(mL/min)
DTW (ft)
(S.U.)
(µS/cm)
CC)
(NTU)
(mV)
(mg/L)
z-7-
1 q.
610
5,v,
1 z
„ 6
rti
5 r
7-29,
►�a
—11
e
r
r
r
5-113
1
1 2
d /, g
2 !
'`
r
3
f /
i i
r
r
i
1
1
1
1
r
1
1
i
1
1
!
r
1
1
1
1
1
1
r
I
1
1
r
1
1
r
r
I
i
i
i
r
1
i
1
r
i
1
i
1
i
i
i
i
i
i
i
i
r
1
r
1
1
1
1
1
i
i
Y
i
1
!
1
1
1
I
!
r
!
I 1
r
I
1
I
1
I
1
F
k
1
Stabilization
ASTM D 6771-
NOTES
Criteria
EPA Region 4
02
`,��
�J /
j rj
pH
01
0.2
Cond- / Sp. Cond.
5%
3%
Turbidity
10% or <10 NTUJ
none
DO
10%or02mg/L
10%or02mg1L
ORP
none
20 mV
WELL VOLUME = (TOTAL WELL DEPTH - STATIC DEPTH TO WATER) X WELL CAPACITY
( feet - feet) Xgallons/foot - gallons
WELL CAPACITY (gallons/foot): 0.75"= 0.02: 1"= 0-04; 1.25"= 0.06; 2"=0.16; 3"= 0-3T 4"= 0.65; 5"= 1.62; 6"= 1.47; 12"= 5.88
EQUIPMENT VOLUME = (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
_( al/ft X feet) + gallons = gallons
TUBING INSIDE DIA. CAPACITY (gal/ft): 1/8"=0.0006; 3/16"=0.0014; 1/4"=0.0026; 5/16"=0.004; 3/8"0-006; 1/2" = 0.010
14
�'� 6"5 '

tec Consultants of NC, PC
4601 Si
4601 Six Forks Rd
7
C Qn.S ultc��-� S
Suite 340
Raleigh, NC 27609
GROUNDWATER SAMPLING LOG
Project Name Duke -Sutton
Date i fiq
Project Number GC5592
�f
Phase/Task CS�q
Location Wilmington, NC
Personnel iM SLAW fA "Pak
Well ID MW 01) Screen Interval (ft) 14 3- 411
DTW (ft) I.q
Pump/Tubing Setting (ft)
w 4s"
Well Diameter (in) '"
DTB (ft) . b
Tubing Diameter (in)
11
Depth Measurement Location TOC
Specific
Purge Rate pH
Conductance
Temp-
Turbidity ORP DO
Time
(mUmin) DTW (ft) (S.U.)
(µS/cm)
(°C)
(NTU) (mV) .(mg/L)
i
1 A.
710€iis
i
&•,
IR%
;Z €
I
€ V.1 lads
:Z a
S33
€ 0
IS •
•:
€
1.04
€ .► I € o.
1
i
((
3 E i
1 €
I
i
r 1 6
�rJ i � €
1
i
1 I 1
! 1 I
•nD
l
1
I
.L
1
I
1 r
I y
•#
I
1
€ - 1
1 1 1
1
•
,
1 � , ,
•.
1
VM
1
F US i 1
IN1� €
F
a
11
€
I o$ I
y €
.o
I - .s
e
i _.1_
- 1
TM D 6771- INOTES
"riteria EPA Region 4 02
)H 0.1 0.2
Cond. / Sp. Cond. 5% 3%
rurbidity 10% or <10 NTU none
:)O 10% or 0.2 mg1L 10% or 0.2 ,
DRP I none 1 20 mV
SA IMP L6 c bzc,C61 hT /6 : 3 S-
WELL VOLUME _ (TOTAL WELL DEPTH - STATIC DEPTH TO WATER) X WELL CAPACITY
_ ( feet - feet) X gallons/foot = gallons
WELL CAPACITY (gallons/foot): 0.75"= 0.02; 1"= 0.04; 1.25"= 0.06; 2"=0.16; 3"= 0.37; 4"= 0.65; 5"= 1.02; 6"= 1.47; 12"= 5.88
EQUIPMENT VOLUME = (TUBING CAPACITY X TUBING LENGTH) + FLOW CELL VOLUME
_( gal/ft X feet) + gallons = gallons
TUBING INSIDE DIA. CAPACITY (gal/ft): 1/8"=0.0006; 3/16"=0-0014; 1/4"=0.0026; 6/16"=0.004; 3/8"0.006; 1/2" = 0.010

Geosyntec Consultants
Water Quality Instrument Calibration Form
Project/Site: JM j,f�JJ! Project#: h ,S�'L Field Personnel:
Water Quality Meter - Model/Serial #• 'I ; �1 r; ,._� Fi �. `` _1)
Turbidimeter - Model/Serial # i` AC' l Alm) (1 I'),,,r r)r r✓)-/t`,
Dissolved
DEP SOP
Date
Time
Temp Saturation
Reading
Reading
Pass
Oxygen
FT 1500
(oC) (mg/L)'
(mg/L)
N
or Fail
CAL ICV
Acceptance
A)q�.
�^
Criteria: +/-0
Q
3nigIL
F
CAL ICV CCV
P F
CAL ICV CCV
P F
Specific
DEP SOP
Date
Time
Standard Standard
Standard
Reading
Pass
Conductance
FT 1200
(mS/cm) Lot #
Exp. Date
(MS/CM)
or Fail
AL IC CCV3�Lj�
CAL IC c
tl
:; To-
��
,� 31o{
' iiLo
4.4Zi
+
P Ui
CAL ICV CCV
P F
CAL CCV CCV
P F
CAL ICV CCV
P F
CAL ICV CCV
P F
pH
DEP SOP
Date
Time
Standard Standard
Standard
Reading
Pass
FT 1100
(SU) Lot #
Exp. Date
(SU)
or Fail
CAL CCV
Acceptance
U. i':
,�'� V,f
F
CAL IC CCV
C C
w+^ ! I' l
,awl!
T 7 '
1, �Q �,®F
•.
F
CAL ICV
00
F
CAL ICV
NCC
�:Z'
.�
�L,(}'f
F
CAL ICV
,, �,t+
F
ORP
SOP N/A
Date
Time
Std. mV @ Standard
Standard
Reading
Pass
Temp °C Lot #
Exp. Date
(mV)
or Fail
ca�CCV
CAL ICV QC �
fl3
�
1 Its
99 �36C 4Ab 3,'�
r
9IK, �
^fR+y_
Q) F
%F
`--per
CAL ICV CCV
—sue--
F
CAL ICV CCV
p F
5 ecific Conductance Probe Cleaned?7YYNS
No
Disolved Oxygen membrane Changed? Yes ti
1. see able hs l200-2 on the back of this form
CAL - Initial Calibration Comments,
ICV - Initial Calibration Verification
CCV - Continuing Calibration Verification
Allow adequate time for the dissolved oxygen sensor to equilibrate during air calibration
Calibrate specific conductance using at least two standards that bracket the range of expected sample readings (unless readings < 0 1 mS/cm then one standard of 0 1 mS/an is acceptable)
Calibrate pH using at least two standards (typ pH 4 and 7) that bracket the range of expected sample readings; always start with pH 7; add a third calibration point if needed (i.e pH > 7)
If parameter fails to calibrate within SOP acceptance criteria then append sample results with a "J" qualifier
0.1 - 10 NTU
Date
Reading
Pass or
Std LLNTU
(NTU)
Fail
rF
IC CCV
IV
S7,b�
CAL
ICV CCV
!
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
11404TU
Reading
Pass or
Std :NTU
Date
(NTU)
Fail
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
41-100 NTU
Reading
Pass or
Std�•SNTU
Date
(NTU)
Fail
L
I CCV
G�
F
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
>100 NTU
Reading
Pass or
Std ! ,'NTU
Date
(NTU)
Fail
CAL
ICV CCV
/ cL q-)Di
P, F
CAL
ICV CCV
�P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
Geosyntec
consultants
WQ Cal Form (Version 1) 6/23/2009

4
Geosyntec Consultants
Water Quality Instrument Calibration Form
Project/Site: ® 3-4Project*: CS,G'Z Field Personnel:
to/.for nA o 14u Anotc. - KAn 4.1JQ ;aI a. '7_ L—.14 _ _l C11_ . s Vt Y / J"I1 t*-A F.^t�1
M.
Model/Serial It S f Mib I, -I Him A ['_ mu -el. 10
Dissolved
DEP SOP
Date
Time
"Temp Saturation
_ YReading
y Reading
Pass
Oxygen
FT 1500
(OC) (mg/L)1
(mg/L)
M)
or Fail
CAL
IC CCV
s
a�z -
�
..
P F
CAL
ICV
O2 I
!2L.1
,
."
R iP
CAL
ICV CCV
p F
CAL
ICV CCV
p F
Specific
DEP SOP Date
Time
Standard Standard
Standard
Reading
Pass
Conductance
FT 1200
(MS/CM) Lot #
Exp. Date
(MS/cm)
or Fail
��,CCC
tt
Q' 'V_M13
OEM
P P
CAL
ICV CCV
P F
CAL
ICV CCV
p F
CAL
ICV CCV
p F
CAL
ICV CCV
p F
pH
DEP SOP
Date
Time
Standard Standard
Standard
Reading
Pass
FT 1100
(SU) Lot #
Exp. Date
(SU)
or Fail,
CAL
IC CCV
S�
I
S
{ F
CCV
.
F
CAI_
CAL
CAL
I C
ICV CC
ICV
•�
6 b
t,/
F
F
F
CAL
ICV
A
a
7-rr�►►q
F
ORP
SOP N/A Date*
-rime
Std. mV @ ' Standard
Standard
Reading
Pass
Temp 'C Lot #
Exp. Date
(mV)
or Fail
AL
q;05
CAL
ICV
�r
CAL
ICV CCV
p F
CAL
ICV CCV
p F
Specific Conductance Probe Cleaned? es
No
Disolved Oxy2en membrane Changed? Yes
- TUDate
ading
Pass or
— TU(NTU)
Fail
V
F
CAL ICV CCV
P F
CAL ICV CCV
P F
11 -40 NTU
Reading
Pass or
Std NT
Date
(NTU)
Fail
CAL i V CV
P F
CAL CC CCV
P F
CAL IC CCV
P F
CAL IC CCV
P F
CAL I CV
P F
CAL V CV
P F
41 - 10 TU
Reading
Pass or
Std -TU
Date
(NTU)
Fail
CAL I CC
*
F
CAL !C
P F
CAL ICV CCV
P F
CAL ICV CCV
P F
CAL ICV CCV
P F
CAL ICV CCV
P F
>1 0 NTU
Reading
Pass or
StdjjWTU
Date
(NTU)
Fail
ICV CCV
{)
F
cAL
cc
�.
P
CAL ICV CCV
P F
CAL ICV CCV
P F
CAL - Initial Calibration Comments:
ICV - Initial Calibration Verification
CCV - Continuing Calibration Verification
Now adequate time for the dissolved oxygen sensor to equilibrate during air calibration
Calibrate specific conductance using at least two standards that bracket the range of expected sample readings (unless readings < 0.1 mS/cm then one standard of 0 1 mS/cm is acceptable)
Calibrate pH using at least two standards (typ. pH 4 and 7) that bracket the range of expected sample readings; always start with pH 7; add a third calibration point if needed (i e. pH > 7)
If parameter fails to calibrate within SOP acceptance criteria then append sample results with a "J" qualifier
Geosyntec
7
9
WQ Cal Form (Version 1) 6/23/2009

Geosyntec Consultants
Water Quality instrument Calibration Form
Fro)eetlStte; Project #: Field Personnel.
Water Quality Meter - Model/Serial #: Turbidmeter - Made!/Seri
lDissolved DEP SOP Date Time Temp Saturation Reading Reading Pass.,
Oxygen FT 1500 (°C) (mg/L)t (mg/L) (%) or •L Fail
CAL JCV ��Acceptancer
CAL ICV CCV
O,7I 04 ((,A„�i g_ 371 _ • = P g�� P F
P F
CAL ICV CCV P F
CAL ICV CCV P F
Specific DEP SOP Date Time Standard Standard Standard Reading Pass
Conductance FT 1200 (ms/cm) Lot # Exp. Date (MS/CM) or Fail
n ?:'Acceptance Criteria: +/- 5%
CAL ICV
CAL ICV CCV
CAL ICV CCV P F
CAL ICV CCV P F
CAL ICV CCV P F
CAL ICV CCV P F
pH DEP SOP Date Time Standard Standard Standard Reading Pass
FT 1100 (SU) Lot # Exp. Date (SU) or Fail
CAL ICV%EI/(I j� {✓ i�l7 (x.9 G- F
CAL ICV 0?11 "� I
F
cAL Icv ( b 'L i f��00 �q"'�~`yF
CAL ICV CCV F
CAL ICV CCV P F
CAL ICV CCV P F
ORP SOP N/A Date Time Std. mV @ Standard Standard Reading Pass
Temp °C Lot # Exp. Date (mv) or Fail
CAL ICV ( O� /q 1)7V P F
CAL ICV CCV p F
CAL ICV CCV P F
CAL ICV CCV p F
1. See Table FS 2200-2 on the back of this form
CAL.- Initial Calibration Comments: f`
ICV - lnllial Calibration Verification
CCV - Untbuing Calibration Verification
Allow adequate tithe for, the dissolved oxygen sensor to equilibrate during air calibration
Calibrate specific conductance s`6TaS standards that bracket the range of expected sample readings (unless readings a 0 1 mS/cm then one.,standaTd of 0 1 mS/cm is acceptable)
Calibrate pH using at least two standards (typ. pH 4 always-slart-wnt"H-7, -add a third calibration point if needed (i e. pH > 7)
If parameter fails to calibrate within SOP acceptance criteria then append sample results with a "J" qualifier
WQ Cal Form (Version 1)
0.11NTU
Date
Reading
Pass or
Stcl
NTU
(NTU)
Fail
CAL
ICV
P F
CAL
fCV
CCTV
P F
CAL
IPV
CC
P F
CAL
lov
CC'
1
P F
11 -40 NTU
Readijig
Pass or
Std
_NTU
Date
(NT.U)
Fail
CAL
ICV
CCV
!
P F
CAL
ICV
CCV
l
i
P F
CAL
ICV
CCV
��
P F
CAL
ICV
CCV
/
P F
CAL
ICV
CCV
P F
CAL
ICV
CCV
Ir
r
P F
i
41 - 100 NTU
Ir
ra /
Reading
Pass or
Std
_NTU
a
//
(NTU)
Fail
CAL
ICV
P F
CAL
ICV
CCV
77-
P F
CAL
ICV
CCV
P F
CAL
ICV
CCV
P F
CAL
ICV
'CCV
P F
CAL
ICV
CCV/EE�
P F
>100 NTU
Reading
Pass or
Std --N
Date
ae
(NTU)
Fail
CAL
ICV
C
P F
CAL
ICV
CCV
P F
CAL
I
CCV
CAL
V
CCV
j
P F
Geosyntec
consultants
6/23/2009

Geosyntec Consultants
Water Quality Instrument Calibration Form
i
Project/Site: ]�uy-1 b 1 T �b✓�/
Pro'eet #: U:-_21Field
Person1IL`T
Jrj � O�'v
aal .r�, >ON
Water Qualit Meter - ModelfSerial #: }'� 4 ar . P'L „f = % i , r•^ }�
.nel:
L
Dissolved
bidimeter - ModellSer
Oxygen
DEP SOP
FT 1500 Date Time
Temp Saturation
Reading
9
Reading
g
Pass
(°C) (mg/L)t
(mg/L)
(%)
or Fail
A;�CcCV
% ICASCV — �-
A,
Acceptance
Criteria: +1-0,3rn71L
��se-?�i'7� -
F F
2
9
7 !
P F
CAL ICV CCV--��r,
CAL ICV CCV
P FP
F
Specific
Conductance
DEP SOP Date Time
FT 1200
Standard Standard
Standard
Reading
Pass
(MS/CM) Lot #
Exp. Date
(MS/CM)
or Fail
!CALCCV'
�-
E03
+. `tfF03
—^4R?'l
,Accet.
P F
CAL ICV CCV
CAL ICV CCV
-
P F
CAL. ICV CCV
P F
CAL ICV CCV
P F
P F
DEP SOP Date Time Standard Standard Standard Reading Pass
FT 1100 (SU) Lot # Exp. Date
p (SU) or Fail
Acceptance Criteria: +/-0 27U
CCV fl{ i7&rZ a?j� �7 +.� f I p / F
c`
G'i
CCV 3G — 1 t J +'lLa� F
CCV ri A F
CCV i F
CCV` 3 t
F
CCV t 1 x ? F
SOP N/A Date Time Std. mV @ Standard Standard Reading Pass
°C
Temp
Lot #
Exp. Date
(mV) or Fail
1C CCV '
CID l>.
ZA2.S
gal
VZM�Mllll
I CCV
ICV CCV
4 W I to
+ t
P F
P F
0.1 -10 NTU
Std MNTU
Date
Reading Pass or
(NTU) Fail
CA 1 CCV
t1 :y�;'
! r' F
CAL ICV CV
c"�;
) F
CAL IC CCV
LED"
pF
dK ICV CCV
P F
11 - 40 NTU
Date
Reading Pass or
Std NTU
—
(NTU) Fail
..41
CV
p F
CAL ICV CCV
p F
CAI. ICV CCV
p F
CAL ICV CCV
p F
CAL ICV CCV
p F
CAL ICV CCV
P F
41 - 100 NTU
Std Y&NTU
Date
e
Reading Pass or
Fail
(NTU)
CAL I CCV
CAL I (4q—CgZ>
4-.o
,p F
F
ICV) CCV
;
F
CAL ICV CCV
L'
p F
CAI. ICV CCV
p F
CAL ICV CCV
p F
>100 NTU
Stcll LNTU
Date
Reading Pass or
(NTU) Fail
CA�CV,',/
r� F
C ICV 4
F
AL ICV CV
r p F
CAL ICV CCV
F
1. See Table FS 2200-2 on the back of this form 11
CAL -Initial Calibration Comments: OuT or- PA4,4f j T-1 0IJ JSfD f'pZl�Cl+tf!f:3`
ICV - Initial Calibration Verification ay N1�
CCV - Continuing Calibration Verification
Allow adequate time for the dissolved oxygen sensor to equilibrate during air calibration
Calibrate specific conductance using at least two standards that bracket the range of expected sample readings (unless readings < 0 1 mS/cm then one standard of 0 1 mS/cm is acceptable) CreOS tee D
Calibrate pH using at least two standards (typ pH 4 and 7) that bracket the range of expected sample readings; always start with pH 7; add a third calibration point if needed (i a pH > 7) j ' `
If parameter fails to calibrate within SOP acceptance criteria then append sample results with a "J" qualifier Consultants
WQ Cal Form (Version 1)
6/23/2009

Geosyntec Consultants
Water Quality Instrument Calibration Form
Project/Site: Pt)a SVTTA) Project#: � -✓5r Field Personnel: {'1 i, ll
Wafor r]„aliN KA.fcr _ *. V L , (X, n i i s / 1 ! ,-. ?
Model/Serial * elAC4 24(I A
Dissolved
DEP SOP
Date
Time
Temp Saturation
Reading
Reading
Pass
Oxygen
FT 1500
(°C) (mg/L)'
(mg/L)
M)
or Fail
CAL
L'
ICV
0 GCV
G^
d
t9 !
Dqb
2�..'Z-+ 1, -3 0
_
Acceptance
.. r
I
b
F
P F
AL
ICV
/
iG�
�s Ja
P
CAL
ICV CCV
P F
Specific
DEP SOP
Date
Time
Standard Standard
Standard
Reading
Pass
Conductance
FT 1200
(mS/cm) Lot #
Exp. Date
(mS/cm)
or Fail
CAL
C
ICV 4 GC
CCV0
f% Z
i z Sv, 2rl�(, �I 1✓d3�3
( 'I,AL*16
+
of
Acceptance Criteria:
lei ]
t"76
+/- 5%
F
P F
CAL
ICV
��!C j`i"
i.3S
.2
f. .S
P
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
pH
DEP SOP
Date
Time
Standard Standard
Standard
Reading
Pass
FT 1100
(SU) Lot #
Exp. Date
(Sul
or Fail
CAL
CAL
ICVncc
ICV
?.lam
,�% °2
b
j�= ..�' Tf /? CG}. G!
G
!41 lE-'
tr WOW
} 9 .,
�*JIKAfffj
F
At
I
C CCV
1
y._
r• G
i3 P.
'.
—
r ,Fj %�1
r
F
G✓15
t7
P F
CAL
ICV CV
-?
w" _ !r i�f (r :
M1J � "
3•
F
CA
CCV
ifth
!�7FA
F
ORP
SOP N/A
Date
Time
Std. mV @ Standard
Standard
Reading
Pass
Temp °C Lot #
Exp. Date
(mv)
or Fail
VICV
AL
CV
27?�
'/ / r9i�
2� t.
?^J(I'
c ll/hl�i
-7F
>�`z
.
(F'3 F
ICVrC
0
0.'2N,7
_
r, U
P F
CAL
ICV CCV
P F
S eclfic Conductance Probe CleanedMY s
No
Disolved Oxygen membrane Changed? Yes
o
0.1 - 10 NTU
Std 5 NTU
Date
Reading
Pass or
'
(NTU)
Fail
CAL I
rr/i
f' F
CCV
F
CAL ICV CC
j'
�. a
F
CAL ICV CCV
P F
11 - 40 NTU
Date
Reading
Pass or
Std NTU
(NTU)
Fail
CAL ICV;CCV
P F
CAL ICV - CCV
P F
CAL ICV: CCV
P F
CAL ICV CCV
P F
CAL ICV CCV
P F
CAL ICV; CCV
P F
41 - 100 NTU
Std NTU
Date
Reading
Pass or
Fail
(NTU)
CAL ICV CC
CCV
Acce
c :- •fi,
YAj y
7
(P F
p
CV ,;�
—M.
=. i
F
CAL ICV CCV
P F
CAL ICV CCV
P F
CAL ICV CCV
P F
>100 NTU
Std 4aNTU
Date
Reading
Pass or
Fail
(NTU)
CAL XV
Acceptance
'c.
Criteria:
GrG "
+/- 5%
i;p F
CAL ICV CCv
CAL ICV
F
,i.f
F
CAL ICV CCV
P F
,. — i ao,e ro ccoo-A on me uacK or mm corm
CAL - Initial Calibration Comments:
ICV- Initial Calibration Verification
CCV - Continuing Calibration Verification
Allow adequate time for the dissolved oxygen sensor to equilibrate during air calibration
Calibrate specific conductance using at least two standards that bracket the range of expected sample readings (unless readings < 0 1 mS/cm then one standard of 0.1 mS/cm is acceptable)
Calibrate pH using at least two standards (typ pH 4 and 7) that bracket the range of expected sample readings; always start with pH 7; add a third calibration point if needed (i.e pH > 7)
If parameter fails to calibrate within SOP acceptance criteria then append sample results with a "J" qualifier
Geosyntec
consultants
WQ Cal Form (Version 1) 6/23/2009

Geosyntec Consultants
jjjj
Water Quality Instrument Calibration Form
((��
Project/Site: f. V6 S,40., Project #: � �� i �
1 Field Personnel „A �• A.
Water Quality Meter - Modet/Serial #: �S� G� ,- ; ' 4,;, 1 lid (� Turbidimeter - Model/Seria
❑tSSiTIWed DEP SOP /Temp Saturation Reading Reading Pass
Oxygen FT 1500 Date Time (°C) (mg/L)t (mg/L) (%) or Fail
CAL
ICV
CCV
Acceptance
Criferia:
P ,F
CAL
ICV
CCV
P F
CAL
ICV
CCV
P F
CAL
ICV
CCV
P F
Specific
DEP SOP
Date
Time
Standard
Standard
Standard
Reading
Pass
Conductance
FT 1200
(MS/CM)
Lot #
Exp. Date
(MS/CM)
or Fail
CAL
ICV
CCV
P F
CAL
ICV
CCV
P F
CAL
ICV
CCV
P F
CAL
ICV
CCV
P F
CAL
ICV
CCV
P F
CAL
ICV
CCV
P F
pH
DEP SOP
Date
Time
Standard
Standard
Standard
Reading
Pass
FT 1100
(SU)
Lot #
Exp. Date
(SU)
or Fail
CAL
CAL
Icv
ICV
J�C
/g;Z2..fJ�(a�c%
`/
3
`l @aY
�
�)^ li*
�.t'1=�
: , F
CAL
ICV
tEP
3
3
L
f o uO t'�.�3�(4�q
62 20
n g
f .» �'
r
t!� Ci i
i 1�,. !� y_
F
F
CAL
ICV
CCV
p F
CAL
ICV
CCV
p F
CAL
ICV
CCV
P F
O€iP
SOP N/A
Date
Time
Std. mV @
Standard
Standard
Reading
Pass
Temp °C
Lot #
Exp. Date
(mV)
or Fail
P,¢
0.1 - 10 NTU
Date
Reading
Pass or
Std NTU
(NTU)
Fail
r•.
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
11 -40 NTU
Reading
Pass or
Std _NTU
Date
(NTU)
Fail
CAL
ICV CCV
.
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
41 - 100 NTU
Reading
Pass or
Std _NTU
Date
(NTU)
Fail
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
CAL
ICV CCV
P F
>100 NTU
Date
Reading
Pass or
Std NTU
(NTU)
Fail
CAL ICV CCV
P
F
CAL
ICV
CCV
P
F
CAL ICV CCV
P
F
CAL
ICV
CCV
P
F
CAL ICV CCV
P
F
CAL
ICV
CCV
P
F
CAL ICV CCV
P
F
CAL
ICV
CCV
P
F
S ecific Conductance Probe Cleaned? Yes No Disolved Oxygen membrane Changed? Yes No
1 S T bl F 220 '
. ee a e S 0-2 on the back of this form
CAL - Initial Calibration Comments:
ICV - Initial Calibration Verification
CCV - Continuing Calibration Verification
Allow adequate time for the dissolved oxygen sensor to equilibrate during air calibration
Calibrate specific conductance using at least two standards that bracket the range of expected sample readings (unless readings < 0 1 mS/cm then one standard of 0 1 mS/cm is acceptable)
Calibrate pH using at least two standards (typ. pH 4 and 7) that bracket the range of expected sample readings; always start with pH 7; add a third calibration point if needed (i a pH > 7)
If parameter fails to calibrate within SOP acceptance criteria then append sample results with a "J" qualifier
WQ Cal Form (Version 1)
Geosyntec
6/23/2009

Geosyntec Consultants
Water Quality Instrument Calibration Form
Project/Site:
to W� S�tC,�1
Project #: G C S S�Z- Field Personnel: 4 ..; .
tt
-.¢ t n
Water Quality
Meter - Model/Serial #:
.^ l �! ' ��S I { "y i OL7 ,', Turbidimeter_-
ModeflSerial # O N C'N Ic Lx/�
Dissolved
Oxygen
DEP SOP
FT 1500 Date
Temp Saturation Reading Reading
Time
Pass
0.1 - 10 NTU Reading Pass or
Date g
VC) (mg/L)' (mg/L) M
or Fail
Std BTU S� 9q (NTU) Fail
C9 !GV:Ccv
CAL ICV %C}�2
�
_
DsiIk5l
9, 'L3
5( .- ,
�6 j
CAL ICV CCV
CAL ICV CCV
Specific
DEP SOP
Date
Time
Standard
Standard
Standard
Conductance
FT 1200
(MS/CM)
Lot #
Exp. Date
o y` c
L{ A E03�
CAL ICV
3 IL{
. {�
!, fs I
CAL ICV CCV
CAL ICV CCV
CAL ICV CCV
CAL ICV CCV
pH
DEP SOP Date
Time
Standard
Standard
Standard
FT 1100
(SU)
Lot #
Exp. Date
CCV Ij C1 ti01 t r 00
CCV L 4 C1=1t� i1Gt{AtO
CCV
ICV
ICV C / rt lv.Oo P Aq",
SOP N/A Date Time Std. mV @ Standard
Temp °C Lot #
r
r.
Pi F
L I CCV
to
F
© F
CAL ICV CG 9
1. Ora
Pj F
P F
CAL ICV CCV
P F
P F
CAL ICV CCV
P F
Reading
(MS/CM)
Pass
or Fail
11-40 TU Date
Std NTU `
Reading
/(NTU)
Pass o
Fail
"P' F
CAL
ICV I
P F
G Pj
F
CAL
ICV G`, V +
P F
P
F
CAL
ICV V
P F
P
F
CAL
I
V
IC�Vcc
P F
P
F
CAL
ICV
P F
Reading Pass
(SU) or Fail
F
F
F
F
F
F
41 -100 NTU Date Reading Pass
Std -'7- _?� (NTU) Fail
!Pxx-v,
:2(a Pi- -r'� ,,_ F
IC ...3
F
ICV CCV
P F
ICV CCV
P F
ICV CCV
P F
ICV CCV
P F
Standard Reading Pass >100 NTU Reading Pass o
Exp. Date (mv) or Fail Std iNTU c/q/ Date (NTU) Fail
ig> �v'2�1.� H A'G3l �i � ccv Z 14
. .
P F AL
ICV CG 3 J '�: a�1 19'.,7 P/' F - AL CCV ;jam-- (pr' F
ICV CCV P F CAL ICV � � i F
ICV CCV P F CAL ICV CCV P F
1. See Table FS 2200-2 on the back of this form
CAL -Initial Calibration Comments: I yf -f� ✓ ; f• o
ICV - Initial Calibration Verification
CCV - Continuing Calibration Verification
Allow adequate time for the dissolved oxygen sensor to equilibrate during air calibration
Calibrate specific conductance using at least two standards that bracket the range of expected sample readings (unless readings < 0.1 mS/cm then one standard of 0 1 mS/cm is acceptable)
Calibrate pH using at least two standards (typ pH 4 and 7) that bracket the range of expected sample readings; always start with pH 7; add a third calibration point if needed (i e. pH > 7)
If parameter fails to calibrate within SOP acceptance criteria then append sample results with a "J" qualifier
Geosyntec °
consultants
WQ Cal Form (Version 1) 6/23/2009

APPENDIX 2.A2

Laboratory Analytical Results

ANALYTICAL RESULTS

Prepared by:

Eurofins Lancaster Laboratories Environmental
2425 New Holland Pike
Lancaster, PA 17601
Prepared for:

GeoSyntec Consultants
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607

July 16, 2014

Project: Duke Sutton, NC

Submittal Date: 07/01/2014
Group Number: 1485674
SDG: DUK34
PO Number: GC5592
State of Sample Origin: NC

Client Sample Description Lancaster Labs (LL) #
20140630-MW14 Grab Groundwater Sample 7516890

The specific methodologies used in obtaining the enclosed analytical results are indicated on the
Laboratory Sample Analysis Record.

ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Lauren Wellborn
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Beau Hodge
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Rachel Donahue
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Herwig Goldemund

Respectfully Submitted,

[phone]

Page 1 of 8

Page 2 of 8

LL Sample # WW 7516890
LL Group # 1485674
Account # 10634
Sample Description: 20140630-MW14 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 17:00 by MP
Submitted: 07/01/2014 09:30
GeoSyntec Consultants
Reported: 07/16/2014 13:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DSMT4 SDG#: DUK34-01*
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.0097 J 17440-38-2 07035 0.0072 0.0400 Arsenic
0.441 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.104 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
47.3 17440-70-2 01750 0.0334 0.400 Calcium
0.0016 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
1.17 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
3.03 17439-95-4 01757 0.0167 0.200 Magnesium
0.0275 17439-96-5 07058 0.00083 0.0100 Manganese
0.0064 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
5.36 17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
19.2 17440-23-5 01767 0.167 2.00 Sodium
0.398 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0114 17440-62-2 07071 0.0019 0.0100 Vanadium
0.0021 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
mg/l mg/lmg/lWet Chemistry EPA 300.0
N.D.524959-67-901505 2.0 2.5 Bromide
22.7 516887-00-600224 1.0 2.0 Chloride
0.27 J 514797-55-800368 0.25 0.50 Nitrate Nitrogen
N.D.514797-65-001506 0.40 0.50 Nitrite Nitrogen
6.5 514808-79-800228 1.5 5.0 Sulfate
mg/l as CaCO3mg/l as CaCO3mg/l as CaCO3EPA 310.1
125 1n.a. 12150 0.70 2.0 Total Alkalinity
mg/l mg/lmg/lSM 2540 C-1997
200 1n.a. 00212 9.7 30.0 Total Dissolved Solids
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
*=This limit was used in the evaluation of the final result
Page 3 of 8

LL Sample # WW 7516890
LL Group # 1485674
Account # 10634
Sample Description: 20140630-MW14 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 17:00 by MP
Submitted: 07/01/2014 09:30
GeoSyntec Consultants
Reported: 07/16/2014 13:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DSMT4 SDG#: DUK34-01*
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 04:09 1418806350011SW-846 6010C Barium 07046
1Tara L Snyder07/09/2014 04:09 1418806350011SW-846 6010C Beryllium 07047
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Boron 08014
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Cadmium 07049
1Tara L Snyder07/09/2014 04:09 1418806350011SW-846 6010C Calcium 01750
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Copper 07053
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Iron 01754
1Joanne M Gates07/09/2014 13:35 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Magnesium 01757
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Molybdenum 07060
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Nickel 07061
1Tara L Snyder07/09/2014 04:09 1418806350011SW-846 6010C Potassium 01762
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Silver 07066
1Tara L Snyder07/09/2014 04:09 1418806350011SW-846 6010C Sodium 01767
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Strontium 08068
1Tara L Snyder07/09/2014 04:09 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 22:05 1418806350011SW-846 6010C Zinc 07072
1Damary Valentin07/16/2014 07:36 1419557130041SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/08/2014 11:00 1418857130011SW-846 7470A WW SW846 Hg Digest 05713
1Micaela L Dishong07/11/2014 09:34 1419157130022SW-846 7470A WW SW846 Hg Digest 05713
1James L Mertz07/15/2014 09:08 1419557130043SW-846 7470A WW SW846 Hg Digest 05713
5Clinton M Wilson07/01/2014 14:15 14182347901B1EPA 300.0 Bromide 01505
5Clinton M Wilson07/01/2014 14:15 14182347901B1EPA 300.0 Chloride 00224
5Clinton M Wilson07/01/2014 14:15 14182347901B1EPA 300.0 Nitrate Nitrogen 00368
5Clinton M Wilson07/01/2014 14:15 14182347901B1EPA 300.0 Nitrite Nitrogen 01506
5Clinton M Wilson07/01/2014 14:15 14182347901B1EPA 300.0 Sulfate 00228
1Yolunder Y Bunch07/02/2014 20:38 14183011102A1EPA 310.1 Total Alkalinity 12150
1Sarah E Thompson07/01/2014 11:40 14182021201A1SM 2540 C-1997 Total Dissolved Solids 00212
*=This limit was used in the evaluation of the final result
Page 4 of 8

Page 1 of 2

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1485674
Reported: 07/16/14 at 01:40 PM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these
situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD was performed, unless otherwise
specified in the method.

All Inorganic Initial Calibration and Continuing Calibration Blanks met acceptable method criteria unless
otherwise noted on the Analysis Report.

Laboratory Compliance Quality Control

Blank Blank Blank Report LCS LCSD LCS/LCSD
Analysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max

Batch number: 141880635001 Sample number(s): 7516890
Antimony N.D. 0.0051 0.0400 mg/l 109 88-111
Arsenic N.D. 0.0072 0.0400 mg/l 111 90-113
Barium N.D. 0.00033 0.0100 mg/l 108 90-110
Beryllium N.D. 0.00067 0.0100 mg/l 106 90-111
Boron N.D. 0.0046 0.100 mg/l 100 90-110
Cadmium N.D. 0.00033 0.0100 mg/l 105 90-112
Calcium N.D. 0.0334 0.400 mg/l 109 90-112
Chromium N.D. 0.0013 0.0300 mg/l 102 90-110
Copper N.D. 0.0028 0.0200 mg/l 108 90-112
Iron N.D. 0.0334 0.400 mg/l 112 90-112
Lead N.D. 0.0047 0.0300 mg/l 114 88-116
Magnesium N.D. 0.0167 0.200 mg/l 107 89-110
Manganese 0.0013 J 0.00083 0.0100 mg/l 108 90-110
Molybdenum N.D. 0.0017 0.0200 mg/l 106 90-110
Nickel N.D. 0.0016 0.0200 mg/l 111 90-117
Potassium N.D. 0.133 1.00 mg/l 104 90-110
Selenium N.D. 0.0048 0.0400 mg/l 103 89-113
Silver N.D. 0.0018 0.0100 mg/l 94 80-120
Sodium N.D. 0.167 2.00 mg/l 106 87-114
Strontium N.D. 0.00033 0.0100 mg/l 108 90-110
Thallium N.D. 0.0051 0.0600 mg/l 101 90-118
Vanadium N.D. 0.0019 0.0100 mg/l 102 90-110
Zinc N.D. 0.0020 0.0400 mg/l 104 90-110

Batch number: 141955713004 Sample number(s): 7516890
Mercury N.D. 0.00006
0
0.00020 mg/l 100 80-120

Batch number: 14182347901B Sample number(s): 7516890
Bromide N.D. 0.40 0.50 mg/l 99 90-110
Chloride N.D. 0.20 0.40 mg/l 98 90-110
Nitrate Nitrogen N.D. 0.050 0.10 mg/l 102 90-110
Nitrite Nitrogen N.D. 0.080 0.10 mg/l 101 90-110
Sulfate N.D. 0.30 1.0 mg/l 101 90-110

Batch number: 14182021201A Sample number(s): 7516890
Total Dissolved Solids N.D. 9.7 30.0 mg/l 105 80-120

Batch number: 14183011102A Sample number(s): 7516890
Total Alkalinity N.D. 0.70 2.0 mg/l as
CaCO3
97 90-110

Page 5 of 8

Page 2 of 2

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1485674
Reported: 07/16/14 at 01:40 PM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Sample Matrix Quality Control
Unspiked (UNSPK) = the sample used in conjunction with the matrix spike
Background (BKG) = the sample used in conjunction with the duplicate

MS MSD MS/MSD RPD BKG DUP DUP Dup RPD
Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___

Batch number: 141880635001 Sample number(s): 7516890 UNSPK: P520777 BKG: P520777
Antimony 108 106 76-122 2 20 N.D. N.D. 0 (1) 20
Arsenic 104 108 81-123 3 20 0.0199 J 0.0133 J 39* (1) 20
Barium 102 101 78-125 1 20 0.144 0.136 6 20
Beryllium 102 101 87-114 1 20 N.D. N.D. 0 (1) 20
Boron 74* 87 87-111 6 20 2.35 2.10 11 (1) 20
Cadmium 99 99 75-122 0 20 N.D. N.D. 0 (1) 20
Calcium 7 (2) -1 (2) 75-125 0 20 89.4 84.3 6 20
Chromium 98 95 76-120 2 20 0.0017 J 0.0019 J 11 (1) 20
Copper 106 106 86-122 0 20 N.D. N.D. 0 (1) 20
Iron 72 (2) 112 (2) 75-125 7 20 4.72 4.44 6 20
Lead 101 100 75-125 1 20 N.D. N.D. 0 (1) 20
Magnesium 20 (2) 10 (2) 81-118 1 20 25.1 23.6 6 20
Manganese 98 94 75-125 2 20 0.459 0.430 7 20
Molybdenum 102 102 89-117 0 20 0.319 0.293 9 20
Nickel 104 103 79-123 1 20 N.D. N.D. 0 (1) 20
Potassium 100 98 77-128 1 20 14.7 13.8 6 20
Selenium 100 101 75-125 1 20 N.D. N.D. 0 (1) 20
Silver 93 91 75-125 2 20 N.D. N.D. 0 (1) 20
Sodium 21 (2) 51 (2) 84-117 3 20 52.1 47.3 10 (1) 20
Strontium 49* 72* 88-117 6 20 3.20 2.88 11 20
Thallium 95 94 75-125 0 20 N.D. N.D. 0 (1) 20
Vanadium 97 97 90-117 0 20 N.D. N.D. 0 (1) 20
Zinc 100 99 85-117 0 20 0.0041 J 0.0038 J 8 (1) 20

Batch number: 141955713004 Sample number(s): 7516890 UNSPK: P514111 BKG: P514111
Mercury 94 97 80-120 2 20 N.D. N.D. 0 (1) 20

Batch number: 14182347901B Sample number(s): 7516890 UNSPK: 7516890 BKG: 7516890
Bromide 99 90-110 N.D. N.D. 0 (1) 20
Chloride 102 90-110 22.7 23.0 1 20
Nitrate Nitrogen 102 90-110 0.27 J 0.28 J 5 (1) 20
Nitrite Nitrogen 99 90-110 N.D. N.D. 0 (1) 20
Sulfate 104 90-110 6.5 6.6 3 (1) 20

Batch number: 14182021201A Sample number(s): 7516890 UNSPK: P515584 BKG: P515584
Total Dissolved Solids 384* 66-131 4,080 4,080 0 5

Batch number: 14183011102A Sample number(s): 7516890 UNSPK: P518803 BKG: P518803
Total Alkalinity 39 17-146 199 200 1 5

Page 6 of 8
Page 7 of 8
Explanation of Symbols and Abbreviations

3768 0713
The following defines common symbols and abbreviations used in reporting technical data:
RL Reporting Limit BMQL Below Minimum Quantitation Level
N.D. none detected MPN Most Probable Number
TNTC Too Numerous To Count CP Units cobalt-chloroplatinate units
IU International Units NTU nephelometric turbidity units
umhos/cm micromhos/cm ng nanogram(s)
C degrees Celsius F degrees Fahrenheit
meq milliequivalents lb. pound(s)
g gram(s) kg kilogram(s)
µg microgram(s) mg milligram(s)
mL milliliter(s) L liter(s)
m3 cubic meter(s) µL microliter(s)
pg/L picogram/liter
< less than - The number following the sign is the limit of quantitation, the smallest amount of analyte which can be
reliably determined using this specific test.
> greater than
ppm parts per million - One ppm is equivalent to one milligram per kilogram (mg/kg), or one gram per million grams. For
aqueous liquids, ppm is usually taken to be equivalent to milligrams per liter (mg/l), because one liter of water has a
weight very close to a kilogram. For gases or vapors, one ppm is equivalent to one microliter per liter of gas.
ppb parts per billion
Dry weight Results printed under this heading have been adjusted for moisture content. This increases the analyte weight
basis concentration to approximate the value present in a similar sample without moisture. All other results are reported
on an as-received basis.
Data Qualifiers:
C – result confirmed by reanalysis.
J - estimated value – The result is ≥ the Method Detection Limit (MDL) and < the Limit of Quantitation (LOQ).
U.S. EPA CLP Data Qualifiers:
Organic Qualifiers Inorganic Qualifiers
A TIC is a possible aldol-condensation product B Value is <CRDL, but ≥IDL
B Analyte was also detected in the blank E Estimated due to interference
C Pesticide result confirmed by GC/MS M Duplicate injection precision not met
D Compound quantitated on a diluted sample N Spike sample not within control limits
E Concentration exceeds the calibration range of S Method of standard additions (MSA) used
the instrument for calculation
N Presumptive evidence of a compound (TICs only) U Compound was not detected
P Concentration difference between primary and W Post digestion spike out of control limits
confirmation columns >25% * Duplicate analysis not within control limits
U Compound was not detected + Correlation coefficient for MSA <0.995
X,Y,Z Defined in case narrative
Analytical test results meet all requirements of NELAC unless otherwise noted under the individual analysis.
Measurement uncertainty values, as applicable, are available upon request.
Tests results relate only to the sample tested. Clients should be aware that a critical step in a chemical or microbiological
analysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of material involved, the
test results will be meaningless. If you have questions regarding the proper techniques of collecting samples, please contact
us. We cannot be held responsible for sample integrity, however, unless sampling has been performed by a member of our
staff. This report shall not be reproduced except in full, without the written approval of the laboratory.
Times are local to the area of activity. Parameters listed in the 40 CFR part 136 Table II as “analyze immediately” are not
performed within 15 minutes.

WARRANTY AND LIMITS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results for the sample as submitted. THE
FOREGOING EXPRESS WARRANTY IS EXCLUSIVE AND IS GIVEN IN LIEU OF ALL OTHER WARRANTIES, EXPRESSED OR IMPLIED. WE DISCLAIM
ANY OTHER WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING A WARRANTY OF FITNESS FOR PARTICULAR PURPOSE AND WARRANTY OF
MERCHANTABILITY. IN NO EVENT SHALL EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL, LLC BE LIABLE FOR INDIRECT, SPECIAL,
CONSEQUENTIAL, OR INCIDENTAL DAMAGES INCLUDING, BUT NOT LIMITED TO, DAMAGES FOR LOSS OF PROFIT OR GOODWILL REGARDLESS
OF (A) THE NEGLIGENCE (EITHER SOLE OR CONCURRENT) OF EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL AND (B) WHETHER
EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL HAS BEEN INFORMED OF THE POSSIBILITY OF SUCH DAMAGES. We accept no legal
responsibility for the purposes for which the client uses the test results. No purchase order or other order for work shall be accepted by Eurofins Lancaster
Laboratories Environmental which includes any conditions that vary from the Standard Terms and Conditions, and Eurofins Lancaster Laboratories
Environmental hereby objects to any conflicting terms contained in any acceptance or order submitted by client.
Page 8 of 8

ANALYTICAL RESULTS

Prepared by:

Eurofins Lancaster Laboratories Environmental
2425 New Holland Pike
Lancaster, PA 17601
Prepared for:

GeoSyntec Consultants
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607

July 16, 2014

Project: Duke Sutton, NC

Submittal Date: 07/02/2014
Group Number: 1486078
SDG: DUK35
PO Number: GC5592
State of Sample Origin: NC

Client Sample Description Lancaster Labs (LL) #
SS-MB2(64.0-68.0)-20140625 Grab Soil Sample 7519007
SS-MB2(64.0-68.0)-20140625 Grab Soil Sample 7519008
SS-MB2(76.0-80.0)-20140625 Grab Soil Sample 7519009
SS-MB2(76.0-80.0)-20140625 Grab Soil Sample 7519010
GW-MW16-20140701 Grab Groundwater Sample 7519011
GW-MW16D-20140701 Grab Groundwater Sample 7519012
EB-02-20140701 Grab Water Sample 7519013
SB-02-20140701 Grab Water Sample 7519014
GW-MW20-20140701 Grab Groundwater Sample 7519015
GW-MW20D-20140701 Grab Groundwater Sample 7519016

The specific methodologies used in obtaining the enclosed analytical results are indicated on the
Laboratory Sample Analysis Record.

ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Lauren Wellborn
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Beau Hodge
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Rachel Donahue
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Herwig Goldemund

Page 1 of 28

ANALYTICAL RESULTS

Prepared by:

Eurofins Lancaster Laboratories Environmental
2425 New Holland Pike
Lancaster, PA 17601
Prepared for:

GeoSyntec Consultants
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607

July 14, 2014

Project: Duke Sutton, NC

Submittal Date: 07/03/2014
Group Number: 1486445
SDG: DUK36
PO Number: GC5592
State of Sample Origin: NC

Client Sample Description Lancaster Labs (LL) #
SS-F-DPT-1(3-4)-20140630 Solid Sample 7520693
SS-F-DPT-1(3-4)-20140630 Solid Sample 7520694
SS-F-DPT-1(7-8)-20140630 Solid Sample 7520695
SS-F-DPT-1(7-8)-20140630 Solid Sample 7520696
SS-F-DPT-3(1.5-2.5)-20140630 Solid Sample 7520697
SS-F-DPT-3(1.5-2.5)-20140630 Solid Sample 7520698
SS-F-DPT-3(5-6)-20140630 Solid Sample 7520699
SS-F-DPT-3(5-6)-20140630 Solid Sample 7520700
SS-F-DPT-5(2-4)-20140701 Solid Sample 7520701
SS-F-DPT-5(2-4)-20140701 MS Solid Sample 7520702
SS-F-DPT-5(2-4)-20140701 MSD Solid Sample 7520703
SS-F-DPT-5(2-4)-20140701 DUP Solid Sample 7520704
SS-F-DPT-5(2-4)-20140701 Solid Sample 7520705
SS-F-DPT-5(2-4)-20140701 MS Solid Sample 7520706
SS-F-DPT-5(2-4)-20140701 MSD Solid Sample 7520707
SS-F-DPT-5(2-4)-20140701 DUP Solid Sample 7520708
SS-F-DPT-5(6-8)-20140701 Solid Sample 7520709
SS-F-DPT-5(6-8)-20140701 Solid Sample 7520710
SS-F-DPT-95(7-8)-20140701 Solid Sample 7520711
SS-F-DPT-95(7-8)-20140701 Solid Sample 7520712
SS-F-DPT-7(3-4)-20140701 Solid Sample 7520713
SS-F-DPT-7(3-4)-20140701 Solid Sample 7520714
SS-F-DPT-7(7-8)-20140701 Solid Sample 7520715
SS-F-DPT-7(7-8)-20140701 Solid Sample 7520716
SS-F-DPT-4(18-20)-20140701 Solid Sample 7520717
SS-F-DPT-4(18-20)-20140701 Solid Sample 7520718
SS-F-DPT-11(7-8)-20140702 Solid Sample 7520719
SS-F-DPT-11(7-8)-20140702 Solid Sample 7520720
SS-F-DPT-11(11-12)-20140702 Solid Sample 7520721
SS-F-DPT-11(11-12)-20140702 Solid Sample 7520722
SS-F-DPT-7(15-16)-20140701 Solid Sample 7520723
Page 1 of 81

SS-F-DPT-7(15-16)-20140701 Solid Sample 7520724
SS-F-DPT-14(3-4)-20140702 Solid Sample 7520725
SS-F-DPT-14(3-4)-20140702 Solid Sample 7520726
SS-F-DPT-14(7-8)-20140702 Solid Sample 7520727
SS-F-DPT-14(7-8)-20140702 Solid Sample 7520728

The specific methodologies used in obtaining the enclosed analytical results are indicated on the
Laboratory Sample Analysis Record.

ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Lauren Wellborn
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Beau Hodge
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Rachel Donahue
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Herwig Goldemund

Respectfully Submitted,

[phone]

Page 2 of 81

LL Sample # SW 7520693
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-1(3-4)-20140630 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 14:15 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS13T SDG#: DUK36-01
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.317 3.84 Antimony
0.715 J 17440-38-2 06935 0.614 3.84 Arsenic
3.28 17440-39-3 06946 0.0317 0.959 Barium
N.D.17440-41-7 06947 0.0643 0.959 Beryllium
3.98 J 17440-42-8 07914 0.806 9.59 Boron
N.D.17440-43-9 06949 0.0317 0.959 Cadmium
0.815 J 17440-47-3 06951 0.106 2.88 Chromium
0.598 J 17440-50-8 06953 0.317 1.92 Copper
348 17439-89-6 01654 3.20 38.4 Iron
1.52 J 17439-92-1 06955 0.480 2.88 Lead
3.12 17439-96-5 06958 0.0796 0.959 Manganese
0.164 J 17439-98-7 06960 0.163 1.92 Molybdenum
0.516 J 17440-02-0 06961 0.144 1.92 Nickel
N.D.17782-49-2 06936 0.422 3.84 Selenium
N.D.17440-22-4 06966 0.182 0.959 Silver
1.74 17440-24-6 07968 0.0317 0.959 Strontium
N.D.17440-28-0 06925 0.767 5.75 Thallium
1.69 J 17440-66-6 06972 0.249 3.84 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
N.D.17439-97-6 00159 0.0096 0.191 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
6.65 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 22.8 C.
% %%Wet Chemistry SM 2540 G-1997
0.70 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Arsenic 06935
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 3 of 81

LL Sample # SW 7520693
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-1(3-4)-20140630 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 14:15 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS13T SDG#: DUK36-01
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Iron 01654
1John P Hook07/09/2014 19:46 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Silver 06966
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 15:09 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:02 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002A1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 4 of 81

LL Sample # TL 7520694
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-1(3-4)-20140630 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 14:15 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS13S SDG#: DUK36-02
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
N.D.17440-38-2 07035 0.0072 0.0400 Arsenic
0.0299 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0295 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
1.84 17440-70-2 01750 0.0334 0.400 Calcium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.345 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.259 17439-95-4 01757 0.0167 0.200 Magnesium
0.0026 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0032 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
0.0117 J 17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
4.81 17440-23-5 01767 0.167 2.00 Sodium
0.0052 J 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0066 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Beryllium 07047
1Joanne M Gates07/11/2014 08:15 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 5 of 81

LL Sample # TL 7520694
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-1(3-4)-20140630 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 14:15 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS13S SDG#: DUK36-02
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 02:34 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:16 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 6 of 81

LL Sample # SW 7520695
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-1(7-8)-20140630 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 14:20 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS17T SDG#: DUK36-03
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.470 5.70 Antimony
26.5 17440-38-2 06935 0.912 5.70 Arsenic
452 57440-39-3 06946 0.235 7.13 Barium
3.54 17440-41-7 06947 0.0955 1.43 Beryllium
24.6 17440-42-8 07914 1.20 14.3 Boron
N.D.17440-43-9 06949 0.0470 1.43 Cadmium
18.8 17440-47-3 06951 0.157 4.28 Chromium
42.8 17440-50-8 06953 0.470 2.85 Copper
12,600 17439-89-6 01654 4.76 57.0 Iron
13.9 17439-92-1 06955 0.713 4.28 Lead
44.9 17439-96-5 06958 0.118 1.43 Manganese
1.06 J 17439-98-7 06960 0.242 2.85 Molybdenum
54.8 17440-02-0 06961 0.214 2.85 Nickel
5.23 J 17782-49-2 06936 0.627 5.70 Selenium
N.D.17440-22-4 06966 0.271 1.43 Silver
337 57440-24-6 07968 0.235 7.13 Strontium
N.D.17440-28-0 06925 1.14 8.55 Thallium
31.3 17440-66-6 06972 0.371 5.70 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.154 J 17439-97-6 00159 0.0148 0.296 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
6.55 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23.1 C.
% %%Wet Chemistry SM 2540 G-1997
33.2 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Arsenic 06935
5John P Hook07/09/2014 19:54 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 7 of 81

LL Sample # SW 7520695
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-1(7-8)-20140630 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 14:20 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS17T SDG#: DUK36-03
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Iron 01654
1John P Hook07/09/2014 19:50 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Silver 06966
5John P Hook07/09/2014 19:54 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 15:13 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:04 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002A1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 8 of 81

LL Sample # TL 7520696
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-1(7-8)-20140630 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 14:20 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS17S SDG#: DUK36-04
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.0109 J 17440-38-2 07035 0.0072 0.0400 Arsenic
0.104 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0195 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
1.55 17440-70-2 01750 0.0334 0.400 Calcium
0.0016 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.197 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.151 J 17439-95-4 01757 0.0167 0.200 Magnesium
0.0030 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0019 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
0.0075 J 17440-02-0 07061 0.0016 0.0200 Nickel
0.151 J 17440-09-7 01762 0.133 1.00 Potassium
0.0108 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
1.97 J 17440-23-5 01767 0.167 2.00 Sodium
0.0794 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0060 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Beryllium 07047
1Joanne M Gates07/11/2014 08:19 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 9 of 81

LL Sample # TL 7520696
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-1(7-8)-20140630 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 14:20 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS17S SDG#: DUK36-04
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 02:37 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:18 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 10 of 81

LL Sample # SW 7520697
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-3(1.5-2.5)-20140630 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 16:02 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS31T SDG#: DUK36-05
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.337 4.09 Antimony
1.28 J 17440-38-2 06935 0.654 4.09 Arsenic
5.57 17440-39-3 06946 0.0337 1.02 Barium
N.D.17440-41-7 06947 0.0685 1.02 Beryllium
2.68 J 17440-42-8 07914 0.858 10.2 Boron
N.D.17440-43-9 06949 0.0337 1.02 Cadmium
2.34 J 17440-47-3 06951 0.112 3.07 Chromium
1.83 J 17440-50-8 06953 0.337 2.04 Copper
833 17439-89-6 01654 3.41 40.9 Iron
2.31 J 17439-92-1 06955 0.511 3.07 Lead
7.45 17439-96-5 06958 0.0848 1.02 Manganese
N.D.17439-98-7 06960 0.174 2.04 Molybdenum
2.10 17440-02-0 06961 0.153 2.04 Nickel
N.D.17782-49-2 06936 0.450 4.09 Selenium
N.D.17440-22-4 06966 0.194 1.02 Silver
11.4 17440-24-6 07968 0.0337 1.02 Strontium
N.D.17440-28-0 06925 0.818 6.13 Thallium
3.06 J 17440-66-6 06972 0.266 4.09 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
N.D.17439-97-6 00159 0.0103 0.207 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
8.28 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23.3 C.
% %%Wet Chemistry SM 2540 G-1997
5.0 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Arsenic 06935
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 11 of 81

LL Sample # SW 7520697
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-3(1.5-2.5)-20140630 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 16:02 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS31T SDG#: DUK36-05
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Iron 01654
1John P Hook07/09/2014 19:58 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Silver 06966
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 15:17 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:06 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002A1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 12 of 81

LL Sample # TL 7520698
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-3(1.5-2.5)-20140630 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 16:02 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS31S SDG#: DUK36-06
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
N.D.17440-38-2 07035 0.0072 0.0400 Arsenic
0.0612 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0438 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
10.2 17440-70-2 01750 0.0334 0.400 Calcium
0.0019 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.473 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.391 17439-95-4 01757 0.0167 0.200 Magnesium
0.0044 J 17439-96-5 07058 0.00083 0.0100 Manganese
N.D.17439-98-7 07060 0.0017 0.0200 Molybdenum
0.0020 J 17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
6.22 17440-23-5 01767 0.167 2.00 Sodium
0.0201 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0099 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Beryllium 07047
1Joanne M Gates07/11/2014 08:23 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 13 of 81

LL Sample # TL 7520698
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-3(1.5-2.5)-20140630 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 16:02 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS31S SDG#: DUK36-06
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 02:41 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:20 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 14 of 81

LL Sample # SW 7520699
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-3(5-6)-20140630 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 16:12 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS35T SDG#: DUK36-07
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.567 6.87 Antimony
28.1 17440-38-2 06935 1.10 6.87 Arsenic
314 57440-39-3 06946 0.283 8.59 Barium
2.73 17440-41-7 06947 0.115 1.72 Beryllium
22.8 17440-42-8 07914 1.44 17.2 Boron
N.D.17440-43-9 06949 0.0567 1.72 Cadmium
20.4 17440-47-3 06951 0.189 5.15 Chromium
34.8 17440-50-8 06953 0.567 3.43 Copper
11,700 17439-89-6 01654 5.73 68.7 Iron
9.56 17439-92-1 06955 0.859 5.15 Lead
58.6 17439-96-5 06958 0.143 1.72 Manganese
1.21 J 17439-98-7 06960 0.292 3.43 Molybdenum
17.4 17440-02-0 06961 0.258 3.43 Nickel
5.33 J 17782-49-2 06936 0.755 6.87 Selenium
N.D.17440-22-4 06966 0.326 1.72 Silver
201 57440-24-6 07968 0.283 8.59 Strontium
N.D.17440-28-0 06925 1.37 10.3 Thallium
14.0 17440-66-6 06972 0.446 6.87 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.228 J 17439-97-6 00159 0.0171 0.341 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
7.71 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23.1 C.
% %%Wet Chemistry SM 2540 G-1997
44.0 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Arsenic 06935
5John P Hook07/09/2014 20:14 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 15 of 81

LL Sample # SW 7520699
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-3(5-6)-20140630 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 16:12 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS35T SDG#: DUK36-07
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Iron 01654
1John P Hook07/09/2014 20:10 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Silver 06966
5John P Hook07/09/2014 20:14 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 15:20 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:08 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002A1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 16 of 81

LL Sample # TL 7520700
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-3(5-6)-20140630 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 16:12 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS35S SDG#: DUK36-08
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.0229 J 17440-38-2 07035 0.0072 0.0400 Arsenic
0.0223 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0278 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
4.34 17440-70-2 01750 0.0334 0.400 Calcium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
N.D.17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.204 17439-95-4 01757 0.0167 0.200 Magnesium
0.0099 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0071 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17440-09-7 01762 0.133 1.00 Potassium
0.0051 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
2.76 17440-23-5 01767 0.167 2.00 Sodium
0.0436 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Beryllium 07047
1Joanne M Gates07/11/2014 08:26 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 17 of 81

LL Sample # TL 7520700
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-3(5-6)-20140630 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/30/2014 16:12 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS35S SDG#: DUK36-08
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 02:45 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:22 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 18 of 81

LL Sample # SW 7520701
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52T SDG#: DUK36-09BKG
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.410 4.96 Antimony
18.5 17440-38-2 06935 0.794 4.96 Arsenic
340 57440-39-3 06946 0.205 6.21 Barium
2.76 17440-41-7 06947 0.0831 1.24 Beryllium
8.38 J 17440-42-8 07914 1.04 12.4 Boron
N.D.17440-43-9 06949 0.0410 1.24 Cadmium
11.8 17440-47-3 06951 0.137 3.72 Chromium
27.0 17440-50-8 06953 0.410 2.48 Copper
11,400 17439-89-6 01654 4.14 49.6 Iron
8.63 17439-92-1 06955 0.621 3.72 Lead
81.1 17439-96-5 06958 0.103 1.24 Manganese
1.79 J 17439-98-7 06960 0.211 2.48 Molybdenum
18.6 17440-02-0 06961 0.186 2.48 Nickel
3.39 J 17782-49-2 06936 0.546 4.96 Selenium
N.D.17440-22-4 06966 0.236 1.24 Silver
184 57440-24-6 07968 0.205 6.21 Strontium
N.D.17440-28-0 06925 0.993 7.45 Thallium
16.6 17440-66-6 06972 0.323 4.96 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.0339 J 17439-97-6 00159 0.0126 0.251 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
7.53 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23.2 C.
% %%Wet Chemistry SM 2540 G-1997
21.0 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Arsenic 06935
5John P Hook07/09/2014 19:07 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 19 of 81

LL Sample # SW 7520701
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52T SDG#: DUK36-09BKG
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Iron 01654
1John P Hook07/09/2014 18:43 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Silver 06966
5John P Hook07/09/2014 19:07 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 14:32 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:11 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 20 of 81

LL Sample # SW 7520702
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 MS Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52T SDG#: DUK36-09MS
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
49.9 17440-36-0 06944 0.398 4.82 Antimony
35.8 17440-38-2 06935 0.772 4.82 Arsenic
571 57440-39-3 06946 0.199 6.03 Barium
8.80 17440-41-7 06947 0.0808 1.21 Beryllium
242 17440-42-8 07914 1.01 12.1 Boron
5.70 17440-43-9 06949 0.0398 1.21 Cadmium
39.7 17440-47-3 06951 0.133 3.62 Chromium
57.9 17440-50-8 06953 0.398 2.41 Copper
12,600 17439-89-6 01654 4.03 48.2 Iron
25.9 17439-92-1 06955 0.603 3.62 Lead
123 17439-96-5 06958 0.100 1.21 Manganese
235 17439-98-7 06960 0.205 2.41 Molybdenum
80.0 17440-02-0 06961 0.181 2.41 Nickel
20.7 17782-49-2 06936 0.530 4.82 Selenium
4.49 17440-22-4 06966 0.229 1.21 Silver
296 57440-24-6 07968 0.199 6.03 Strontium
13.5 17440-28-0 06925 0.964 7.23 Thallium
72.1 17440-66-6 06972 0.313 4.82 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.226 J 17439-97-6 00159 0.0118 0.237 Mercury
% %%Wet Chemistry SM 2540 G-1997
21.0 1n.a. 00118 0.50 0.50 Moisture
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Arsenic 06935
5John P Hook07/09/2014 19:26 1418806370023SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Beryllium 06947
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Iron 01654
1John P Hook07/09/2014 18:55 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Nickel 06961
*=This limit was used in the evaluation of the final result
Page 21 of 81

LL Sample # SW 7520702
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 MS Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52T SDG#: DUK36-09MS
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Silver 06966
5John P Hook07/09/2014 19:26 1418806370023SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 14:43 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:21 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture 00118
*=This limit was used in the evaluation of the final result
Page 22 of 81

LL Sample # SW 7520703
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 MSD Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52T SDG#: DUK36-09MSD
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
51.3 17440-36-0 06944 0.402 4.87 Antimony
36.5 17440-38-2 06935 0.779 4.87 Arsenic
604 57440-39-3 06946 0.201 6.09 Barium
9.06 17440-41-7 06947 0.0815 1.22 Beryllium
243 17440-42-8 07914 1.02 12.2 Boron
5.78 17440-43-9 06949 0.0402 1.22 Cadmium
40.5 17440-47-3 06951 0.134 3.65 Chromium
59.6 17440-50-8 06953 0.402 2.43 Copper
12,300 17439-89-6 01654 4.07 48.7 Iron
27.0 17439-92-1 06955 0.609 3.65 Lead
122 17439-96-5 06958 0.101 1.22 Manganese
240 17439-98-7 06960 0.207 2.43 Molybdenum
81.1 17440-02-0 06961 0.183 2.43 Nickel
21.1 17782-49-2 06936 0.536 4.87 Selenium
4.49 17440-22-4 06966 0.231 1.22 Silver
318 57440-24-6 07968 0.201 6.09 Strontium
13.6 17440-28-0 06925 0.974 7.30 Thallium
73.3 17440-66-6 06972 0.316 4.87 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.282 17439-97-6 00159 0.0122 0.244 Mercury
% %%Wet Chemistry SM 2540 G-1997
21.0 1n.a. 00118 0.50 0.50 Moisture
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Arsenic 06935
5John P Hook07/09/2014 19:30 1418806370023SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Beryllium 06947
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Iron 01654
1John P Hook07/09/2014 18:59 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Nickel 06961
*=This limit was used in the evaluation of the final result
Page 23 of 81

LL Sample # SW 7520703
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 MSD Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52T SDG#: DUK36-09MSD
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Silver 06966
5John P Hook07/09/2014 19:30 1418806370023SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 14:47 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:23 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture 00118
*=This limit was used in the evaluation of the final result
Page 24 of 81

LL Sample # SW 7520704
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 DUP Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52T SDG#: DUK36-09DUP
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.402 4.87 Antimony
20.8 17440-38-2 06935 0.779 4.87 Arsenic
389 57440-39-3 06946 0.201 6.09 Barium
3.42 17440-41-7 06947 0.0815 1.22 Beryllium
9.31 J 17440-42-8 07914 1.02 12.2 Boron
N.D.17440-43-9 06949 0.0402 1.22 Cadmium
13.7 17440-47-3 06951 0.134 3.65 Chromium
32.7 17440-50-8 06953 0.402 2.43 Copper
11,500 17439-89-6 01654 4.07 48.7 Iron
10.2 17439-92-1 06955 0.609 3.65 Lead
55.3 17439-96-5 06958 0.101 1.22 Manganese
1.51 J 17439-98-7 06960 0.207 2.43 Molybdenum
20.2 17440-02-0 06961 0.183 2.43 Nickel
4.68 J 17782-49-2 06936 0.536 4.87 Selenium
N.D.17440-22-4 06966 0.231 1.22 Silver
213 57440-24-6 07968 0.201 6.09 Strontium
N.D.17440-28-0 06925 0.974 7.30 Thallium
14.3 17440-66-6 06972 0.316 4.87 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.0395 J 17439-97-6 00159 0.0118 0.237 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
7.51 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23 C.
% %%Wet Chemistry SM 2540 G-1997
21.0 1n.a. 00118 0.50 0.50 Moisture
23.1 1n.a. 00121 0.50 0.50 Moisture Duplicate
The duplicate moisture value is provided to assess the precision of the
moisture test. For comparability purposes, the initial moisture
determination is the value used to perform dry weight calculations.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Arsenic 06935
5John P Hook07/09/2014 19:22 1418806370021SW-846 6010C Barium 06946
*=This limit was used in the evaluation of the final result
Page 25 of 81

LL Sample # SW 7520704
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 DUP Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52T SDG#: DUK36-09DUP
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Beryllium 06947
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Iron 01654
1John P Hook07/09/2014 18:51 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Silver 06966
5John P Hook07/09/2014 19:22 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 14:39 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:19 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture 00118
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture Duplicate 00121
*=This limit was used in the evaluation of the final result
Page 26 of 81

LL Sample # TL 7520705
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52S SDG#: DUK36-10BKG
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
0.0055 J 17440-36-0 07044 0.0051 0.0400 Antimony
0.0197 J 17440-38-2 07035 0.0072 0.0400 Arsenic
0.105 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0284 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
5.40 17440-70-2 01750 0.0334 0.400 Calcium
0.0021 J 17440-47-3 07051 0.0013 0.0300 Chromium
0.0085 J 17440-50-8 07053 0.0028 0.0200 Copper
0.370 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.323 17439-95-4 01757 0.0167 0.200 Magnesium
0.0031 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0172 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
3.58 17440-23-5 01767 0.167 2.00 Sodium
0.122 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0059 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Beryllium 07047
1Joanne M Gates07/11/2014 08:01 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 27 of 81

LL Sample # TL 7520705
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52S SDG#: DUK36-10BKG
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 01:56 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:24 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 28 of 81

LL Sample # TL 7520706
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 MS Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52S SDG#: DUK36-10MS
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
4.82 17440-36-0 07044 0.0051 0.0400 Antimony
4.90 17440-38-2 07035 0.0072 0.0400 Arsenic
94.6 257440-39-3 07046 0.0083 0.250 Barium
4.86 27440-41-7 07047 0.0013 0.0200 Beryllium
4.49 17440-42-8 08014 0.0046 0.100 Boron
0.914 17440-43-9 07049 0.00033 0.0100 Cadmium
52.6 17440-70-2 01750 0.0334 0.400 Calcium
4.58 17440-47-3 07051 0.0013 0.0300 Chromium
4.72 17440-50-8 07053 0.0028 0.0200 Copper
5.25 17439-89-6 01754 0.0334 0.400 Iron
4.53 17439-92-1 07055 0.0047 0.0300 Lead
47.4 17439-95-4 01757 0.0167 0.200 Magnesium
4.51 17439-96-5 07058 0.00083 0.0100 Manganese
9.40 17439-98-7 07060 0.0017 0.0200 Molybdenum
4.50 17440-02-0 07061 0.0016 0.0200 Nickel
48.9 17440-09-7 01762 0.133 1.00 Potassium
0.965 17782-49-2 07036 0.0048 0.0400 Selenium
3.53 17440-22-4 07066 0.0018 0.0100 Silver
49.0 17440-23-5 01767 0.167 2.00 Sodium
5.06 27440-24-6 08068 0.00066 0.0200 Strontium
4.35 17440-28-0 07022 0.0051 0.0600 Thallium
4.62 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
0.0193 17439-97-6 00259 0.00060 0.0020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Arsenic 07035
25Tara L Snyder07/11/2014 02:11 1419006360011SW-846 6010C Barium 07046
2Joanne M Gates07/11/2014 08:56 1419006360012SW-846 6010C Beryllium 07047
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 29 of 81

LL Sample # TL 7520706
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 MS Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52S SDG#: DUK36-10MS
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Sodium 01767
2Joanne M Gates07/11/2014 08:56 1419006360012SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 02:07 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:26 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 30 of 81

LL Sample # TL 7520707
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 MSD Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52S SDG#: DUK36-10MSD
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
4.65 17440-36-0 07044 0.0051 0.0400 Antimony
4.72 17440-38-2 07035 0.0072 0.0400 Arsenic
90.7 257440-39-3 07046 0.0083 0.250 Barium
4.77 27440-41-7 07047 0.0013 0.0200 Beryllium
4.40 17440-42-8 08014 0.0046 0.100 Boron
0.880 17440-43-9 07049 0.00033 0.0100 Cadmium
50.6 17440-70-2 01750 0.0334 0.400 Calcium
4.51 17440-47-3 07051 0.0013 0.0300 Chromium
4.58 17440-50-8 07053 0.0028 0.0200 Copper
5.31 17439-89-6 01754 0.0334 0.400 Iron
4.38 17439-92-1 07055 0.0047 0.0300 Lead
46.3 17439-95-4 01757 0.0167 0.200 Magnesium
4.45 17439-96-5 07058 0.00083 0.0100 Manganese
9.15 17439-98-7 07060 0.0017 0.0200 Molybdenum
4.37 17440-02-0 07061 0.0016 0.0200 Nickel
47.8 17440-09-7 01762 0.133 1.00 Potassium
0.933 17782-49-2 07036 0.0048 0.0400 Selenium
4.03 17440-22-4 07066 0.0018 0.0100 Silver
48.7 17440-23-5 01767 0.167 2.00 Sodium
4.90 27440-24-6 08068 0.00066 0.0200 Strontium
4.19 17440-28-0 07022 0.0051 0.0600 Thallium
4.46 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
0.0182 17439-97-6 00259 0.00060 0.0020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Arsenic 07035
25Tara L Snyder07/11/2014 02:19 1419006360011SW-846 6010C Barium 07046
2Joanne M Gates07/11/2014 09:00 1419006360012SW-846 6010C Beryllium 07047
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 31 of 81

LL Sample # TL 7520707
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 MSD Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52S SDG#: DUK36-10MSD
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Sodium 01767
2Joanne M Gates07/11/2014 09:00 1419006360012SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 02:15 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:28 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 32 of 81

LL Sample # TL 7520708
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 DUP Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52S SDG#: DUK36-10DUP
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
0.0066 J 17440-36-0 07044 0.0051 0.0400 Antimony
0.0183 J 17440-38-2 07035 0.0072 0.0400 Arsenic
0.115 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0285 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
5.30 17440-70-2 01750 0.0334 0.400 Calcium
0.0019 J 17440-47-3 07051 0.0013 0.0300 Chromium
0.0091 J 17440-50-8 07053 0.0028 0.0200 Copper
0.362 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.314 17439-95-4 01757 0.0167 0.200 Magnesium
0.0032 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0149 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17440-09-7 01762 0.133 1.00 Potassium
0.0051 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
3.43 17440-23-5 01767 0.167 2.00 Sodium
0.120 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0069 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Beryllium 07047
1Joanne M Gates07/11/2014 08:08 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 33 of 81

LL Sample # TL 7520708
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(2-4)-20140701 DUP Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS52S SDG#: DUK36-10DUP
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 02:03 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:31 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 34 of 81

LL Sample # SW 7520709
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(6-8)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:10 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS56T SDG#: DUK36-11
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.517 6.26 Antimony
42.2 17440-38-2 06935 1.00 6.26 Arsenic
708 57440-39-3 06946 0.258 7.83 Barium
7.84 17440-41-7 06947 0.105 1.57 Beryllium
19.0 17440-42-8 07914 1.32 15.7 Boron
N.D.17440-43-9 06949 0.0517 1.57 Cadmium
25.4 17440-47-3 06951 0.172 4.70 Chromium
66.4 17440-50-8 06953 0.517 3.13 Copper
13,500 17439-89-6 01654 5.23 62.6 Iron
18.8 17439-92-1 06955 0.783 4.70 Lead
85.7 17439-96-5 06958 0.130 1.57 Manganese
0.985 J 17439-98-7 06960 0.266 3.13 Molybdenum
34.9 17440-02-0 06961 0.235 3.13 Nickel
6.86 17782-49-2 06936 0.689 6.26 Selenium
N.D.17440-22-4 06966 0.298 1.57 Silver
475 57440-24-6 07968 0.258 7.83 Strontium
N.D.17440-28-0 06925 1.25 9.40 Thallium
28.0 17440-66-6 06972 0.407 6.26 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.0875 J 17439-97-6 00159 0.0156 0.311 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
7.80 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23.3 C.
% %%Wet Chemistry SM 2540 G-1997
37.4 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Arsenic 06935
5John P Hook07/09/2014 20:22 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 35 of 81

LL Sample # SW 7520709
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(6-8)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:10 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS56T SDG#: DUK36-11
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Iron 01654
1John P Hook07/09/2014 20:18 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Silver 06966
5John P Hook07/09/2014 20:22 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 15:24 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:25 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 36 of 81

LL Sample # TL 7520710
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(6-8)-20140701 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:10 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS56S SDG#: DUK36-12
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
0.0132 J 17440-36-0 07044 0.0051 0.0400 Antimony
0.0415 17440-38-2 07035 0.0072 0.0400 Arsenic
0.221 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0183 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
12.0 17440-70-2 01750 0.0334 0.400 Calcium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
N.D.17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.214 17439-95-4 01757 0.0167 0.200 Magnesium
0.0019 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0112 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
0.300 J 17440-09-7 01762 0.133 1.00 Potassium
0.0284 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
1.35 J 17440-23-5 01767 0.167 2.00 Sodium
0.247 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0023 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Beryllium 07047
1Joanne M Gates07/11/2014 08:30 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 37 of 81

LL Sample # TL 7520710
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-5(6-8)-20140701 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:10 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS56S SDG#: DUK36-12
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 02:48 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:33 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 38 of 81

LL Sample # SW 7520711
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-95(7-8)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:10 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS95T SDG#: DUK36-13
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.488 5.92 Antimony
42.3 17440-38-2 06935 0.947 5.92 Arsenic
686 57440-39-3 06946 0.244 7.40 Barium
7.41 17440-41-7 06947 0.0991 1.48 Beryllium
17.5 17440-42-8 07914 1.24 14.8 Boron
N.D.17440-43-9 06949 0.0488 1.48 Cadmium
25.3 17440-47-3 06951 0.163 4.44 Chromium
62.7 17440-50-8 06953 0.488 2.96 Copper
13,000 17439-89-6 01654 4.94 59.2 Iron
17.8 17439-92-1 06955 0.740 4.44 Lead
79.8 17439-96-5 06958 0.123 1.48 Manganese
0.975 J 17439-98-7 06960 0.251 2.96 Molybdenum
33.3 17440-02-0 06961 0.222 2.96 Nickel
6.74 17782-49-2 06936 0.651 5.92 Selenium
N.D.17440-22-4 06966 0.281 1.48 Silver
449 57440-24-6 07968 0.244 7.40 Strontium
N.D.17440-28-0 06925 1.18 8.88 Thallium
27.8 17440-66-6 06972 0.385 5.92 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.0955 J 17439-97-6 00159 0.0145 0.290 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
7.79 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 22.9 C.
% %%Wet Chemistry SM 2540 G-1997
35.0 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Arsenic 06935
5John P Hook07/09/2014 20:30 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 39 of 81

LL Sample # SW 7520711
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-95(7-8)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:10 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS95T SDG#: DUK36-13
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Iron 01654
1John P Hook07/09/2014 20:26 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Silver 06966
5John P Hook07/09/2014 20:30 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 15:28 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:27 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 40 of 81

LL Sample # TL 7520712
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-95(7-8)-20140701 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:10 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS95S SDG#: DUK36-14
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
0.0141 J 17440-36-0 07044 0.0051 0.0400 Antimony
0.0426 17440-38-2 07035 0.0072 0.0400 Arsenic
0.213 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0184 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
11.7 17440-70-2 01750 0.0334 0.400 Calcium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
N.D.17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.220 17439-95-4 01757 0.0167 0.200 Magnesium
0.0028 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0150 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
0.283 J 17440-09-7 01762 0.133 1.00 Potassium
0.0280 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
1.35 J 17440-23-5 01767 0.167 2.00 Sodium
0.243 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Beryllium 07047
1Joanne M Gates07/11/2014 08:34 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 41 of 81

LL Sample # TL 7520712
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-95(7-8)-20140701 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:10 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS95S SDG#: DUK36-14
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 02:52 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:35 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 42 of 81

LL Sample # SW 7520713
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-7(3-4)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:30 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS73T SDG#: DUK36-15
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.394 4.78 Antimony
4.27 J 17440-38-2 06935 0.764 4.78 Arsenic
31.8 17440-39-3 06946 0.0394 1.19 Barium
0.383 J 17440-41-7 06947 0.0800 1.19 Beryllium
1.96 J 17440-42-8 07914 1.00 11.9 Boron
N.D.17440-43-9 06949 0.0394 1.19 Cadmium
3.39 J 17440-47-3 06951 0.131 3.58 Chromium
5.03 17440-50-8 06953 0.394 2.39 Copper
2,180 17439-89-6 01654 3.99 47.8 Iron
2.51 J 17439-92-1 06955 0.597 3.58 Lead
8.22 17439-96-5 06958 0.0991 1.19 Manganese
0.294 J 17439-98-7 06960 0.203 2.39 Molybdenum
3.27 17440-02-0 06961 0.179 2.39 Nickel
N.D.17782-49-2 06936 0.525 4.78 Selenium
N.D.17440-22-4 06966 0.227 1.19 Silver
11.8 17440-24-6 07968 0.0394 1.19 Strontium
N.D.17440-28-0 06925 0.955 7.17 Thallium
5.99 17440-66-6 06972 0.310 4.78 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
N.D.17439-97-6 00159 0.0117 0.233 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
6.10 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23.2 C.
% %%Wet Chemistry SM 2540 G-1997
18.7 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Arsenic 06935
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 43 of 81

LL Sample # SW 7520713
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-7(3-4)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:30 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS73T SDG#: DUK36-15
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Iron 01654
1Tara L Snyder07/10/2014 04:41 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Silver 06966
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 15:32 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:29 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 44 of 81

LL Sample # TL 7520714
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-7(3-4)-20140701 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:30 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS73S SDG#: DUK36-16
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
N.D.17440-38-2 07035 0.0072 0.0400 Arsenic
0.0173 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0397 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
1.47 17440-70-2 01750 0.0334 0.400 Calcium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.281 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.211 17439-95-4 01757 0.0167 0.200 Magnesium
0.0014 J 17439-96-5 07058 0.00083 0.0100 Manganese
N.D.17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
6.09 17440-23-5 01767 0.167 2.00 Sodium
0.0101 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0060 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Beryllium 07047
1Joanne M Gates07/11/2014 08:45 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 45 of 81

LL Sample # TL 7520714
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-7(3-4)-20140701 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:30 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS73S SDG#: DUK36-16
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 02:56 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:41 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 46 of 81

LL Sample # SW 7520715
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-7(7-8)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:32 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS77T SDG#: DUK36-17
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.546 6.61 Antimony
31.1 17440-38-2 06935 1.06 6.61 Arsenic
543 57440-39-3 06946 0.273 8.27 Barium
5.79 17440-41-7 06947 0.111 1.65 Beryllium
15.6 J 17440-42-8 07914 1.39 16.5 Boron
N.D.17440-43-9 06949 0.0546 1.65 Cadmium
22.2 17440-47-3 06951 0.182 4.96 Chromium
58.2 17440-50-8 06953 0.546 3.31 Copper
8,130 17439-89-6 01654 5.52 66.1 Iron
17.7 17439-92-1 06955 0.827 4.96 Lead
43.5 17439-96-5 06958 0.137 1.65 Manganese
1.62 J 17439-98-7 06960 0.281 3.31 Molybdenum
27.0 17440-02-0 06961 0.248 3.31 Nickel
6.29 J 17782-49-2 06936 0.727 6.61 Selenium
N.D.17440-22-4 06966 0.314 1.65 Silver
336 57440-24-6 07968 0.273 8.27 Strontium
N.D.17440-28-0 06925 1.32 9.92 Thallium
22.4 17440-66-6 06972 0.430 6.61 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.0915 J 17439-97-6 00159 0.0157 0.315 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
7.21 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23.3 C.
% %%Wet Chemistry SM 2540 G-1997
40.7 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Arsenic 06935
5Tara L Snyder07/10/2014 04:48 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 47 of 81

LL Sample # SW 7520715
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-7(7-8)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:32 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS77T SDG#: DUK36-17
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Iron 01654
1Tara L Snyder07/10/2014 04:44 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Silver 06966
5Tara L Snyder07/10/2014 04:48 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 15:36 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:31 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 48 of 81

LL Sample # TL 7520716
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-7(7-8)-20140701 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:32 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS77S SDG#: DUK36-18
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
0.010 J 17440-36-0 07044 0.0051 0.0400 Antimony
0.0182 J 17440-38-2 07035 0.0072 0.0400 Arsenic
0.295 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0278 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
5.60 17440-70-2 01750 0.0334 0.400 Calcium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
N.D.17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.306 17439-95-4 01757 0.0167 0.200 Magnesium
0.0054 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0261 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17440-09-7 01762 0.133 1.00 Potassium
0.0053 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
2.71 17440-23-5 01767 0.167 2.00 Sodium
0.139 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Beryllium 07047
1Joanne M Gates07/11/2014 08:48 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 49 of 81

LL Sample # TL 7520716
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-7(7-8)-20140701 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:32 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS77S SDG#: DUK36-18
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 02:59 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:43 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 50 of 81

LL Sample # SW 7520717
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-4(18-20)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 12:48 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D418T SDG#: DUK36-19
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
0.839 J 17440-36-0 06944 0.699 8.47 Antimony
3.02 J 17440-38-2 06935 1.36 8.47 Arsenic
34.2 17440-39-3 06946 0.0699 2.12 Barium
N.D.17440-41-7 06947 0.142 2.12 Beryllium
7.03 J 17440-42-8 07914 1.78 21.2 Boron
0.0826 J 17440-43-9 06949 0.0699 2.12 Cadmium
6.51 17440-47-3 06951 0.233 6.36 Chromium
3.15 J 17440-50-8 06953 0.699 4.24 Copper
1,610 17439-89-6 01654 7.08 84.7 Iron
2.32 J 17439-92-1 06955 1.06 6.36 Lead
15.6 17439-96-5 06958 0.176 2.12 Manganese
0.428 J 17439-98-7 06960 0.360 4.24 Molybdenum
3.23 J 17440-02-0 06961 0.318 4.24 Nickel
N.D.17782-49-2 06936 0.932 8.47 Selenium
N.D.17440-22-4 06966 0.403 2.12 Silver
21.0 17440-24-6 07968 0.0699 2.12 Strontium
N.D.17440-28-0 06925 1.69 12.7 Thallium
9.63 17440-66-6 06972 0.551 8.47 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
N.D.17439-97-6 00159 0.0209 0.418 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
5.54 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23.1 C.
% %%Wet Chemistry SM 2540 G-1997
52.8 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Arsenic 06935
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 51 of 81

LL Sample # SW 7520717
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-4(18-20)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 12:48 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D418T SDG#: DUK36-19
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Iron 01654
1Tara L Snyder07/10/2014 04:53 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Silver 06966
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 15:40 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:33 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402B1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 52 of 81

LL Sample # TL 7520718
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-4(18-20)-20140701 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 12:48 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D418S SDG#: DUK36-20
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
N.D.17440-38-2 07035 0.0072 0.0400 Arsenic
0.0424 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0994 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
1.08 17440-70-2 01750 0.0334 0.400 Calcium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
0.0037 J 17440-50-8 07053 0.0028 0.0200 Copper
0.0850 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.190 J 17439-95-4 01757 0.0167 0.200 Magnesium
0.0020 J 17439-96-5 07058 0.00083 0.0100 Manganese
N.D.17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
12.6 17440-23-5 01767 0.167 2.00 Sodium
0.0033 J 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0091 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Beryllium 07047
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 53 of 81

LL Sample # TL 7520718
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-4(18-20)-20140701 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 12:48 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D418S SDG#: DUK36-20
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 03:03 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:45 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 54 of 81

LL Sample # SW 7520719
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-11(7-8)-20140702 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 09:58 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D117T SDG#: DUK36-21
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.345 4.18 Antimony
6.44 17440-38-2 06935 0.668 4.18 Arsenic
38.8 17440-39-3 06946 0.0345 1.04 Barium
0.845 J 17440-41-7 06947 0.0700 1.04 Beryllium
2.62 J 17440-42-8 07914 0.877 10.4 Boron
N.D.17440-43-9 06949 0.0345 1.04 Cadmium
4.16 17440-47-3 06951 0.115 3.13 Chromium
7.55 17440-50-8 06953 0.345 2.09 Copper
2,080 17439-89-6 01654 3.49 41.8 Iron
3.52 17439-92-1 06955 0.522 3.13 Lead
10.9 17439-96-5 06958 0.0867 1.04 Manganese
0.378 J 17439-98-7 06960 0.178 2.09 Molybdenum
3.93 17440-02-0 06961 0.157 2.09 Nickel
N.D.17782-49-2 06936 0.459 4.18 Selenium
N.D.17440-22-4 06966 0.198 1.04 Silver
21.3 17440-24-6 07968 0.0345 1.04 Strontium
N.D.17440-28-0 06925 0.835 6.27 Thallium
3.99 J 17440-66-6 06972 0.272 4.18 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
N.D.17439-97-6 00159 0.0108 0.216 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
6.43 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23.2 C.
% %%Wet Chemistry SM 2540 G-1997
8.8 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Arsenic 06935
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 55 of 81

LL Sample # SW 7520719
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-11(7-8)-20140702 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 09:58 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D117T SDG#: DUK36-21
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Iron 01654
1Tara L Snyder07/10/2014 04:56 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Silver 06966
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 15:43 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:35 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402B1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 56 of 81

LL Sample # TL 7520720
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-11(7-8)-20140702 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 09:58 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D117S SDG#: DUK36-22
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
N.D.17440-38-2 07035 0.0072 0.0400 Arsenic
0.0038 J 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0321 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
0.791 17440-70-2 01750 0.0334 0.400 Calcium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.0362 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.278 17439-95-4 01757 0.0167 0.200 Magnesium
N.D.17439-96-5 07058 0.00083 0.0100 Manganese
N.D.17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
2.55 17440-23-5 01767 0.167 2.00 Sodium
0.0202 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Beryllium 07047
1Joanne M Gates07/11/2014 08:52 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 57 of 81

LL Sample # TL 7520720
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-11(7-8)-20140702 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 09:58 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D117S SDG#: DUK36-22
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 03:07 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:47 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 58 of 81

LL Sample # SW 7520721
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-11(11-12)-20140702 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 10:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D111T SDG#: DUK36-23
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.383 4.65 Antimony
7.54 17440-38-2 06935 0.743 4.65 Arsenic
261 57440-39-3 06946 0.192 5.81 Barium
1.59 17440-41-7 06947 0.0778 1.16 Beryllium
4.89 J 17440-42-8 07914 0.976 11.6 Boron
N.D.17440-43-9 06949 0.0383 1.16 Cadmium
6.59 17440-47-3 06951 0.128 3.48 Chromium
14.7 17440-50-8 06953 0.383 2.32 Copper
9,420 17439-89-6 01654 3.88 46.5 Iron
3.60 17439-92-1 06955 0.581 3.48 Lead
46.9 17439-96-5 06958 0.0964 1.16 Manganese
0.441 J 17439-98-7 06960 0.197 2.32 Molybdenum
8.38 17440-02-0 06961 0.174 2.32 Nickel
0.555 J 17782-49-2 06936 0.511 4.65 Selenium
N.D.17440-22-4 06966 0.221 1.16 Silver
83.7 17440-24-6 07968 0.0383 1.16 Strontium
N.D.17440-28-0 06925 0.929 6.97 Thallium
6.30 17440-66-6 06972 0.302 4.65 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
N.D.17439-97-6 00159 0.0117 0.233 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
6.69 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23.1 C.
% %%Wet Chemistry SM 2540 G-1997
16.4 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Arsenic 06935
5Tara L Snyder07/10/2014 05:04 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 59 of 81

LL Sample # SW 7520721
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-11(11-12)-20140702 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 10:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D111T SDG#: DUK36-23
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Iron 01654
1Tara L Snyder07/10/2014 05:00 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Silver 06966
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 15:54 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:37 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402B1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 60 of 81

LL Sample # TL 7520722
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-11(11-12)-20140702 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 10:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D111S SDG#: DUK36-24
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
N.D.17440-38-2 07035 0.0072 0.0400 Arsenic
0.0571 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0535 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
1.30 17440-70-2 01750 0.0334 0.400 Calcium
0.0021 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.426 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.500 17439-95-4 01757 0.0167 0.200 Magnesium
0.0054 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0024 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
4.41 17440-23-5 01767 0.167 2.00 Sodium
0.0375 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0060 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Beryllium 07047
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 61 of 81

LL Sample # TL 7520722
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-11(11-12)-20140702 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 10:00 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D111S SDG#: DUK36-24
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 03:18 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:49 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 62 of 81

LL Sample # SW 7520723
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-7(15-16)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:35 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D715T SDG#: DUK36-25
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.377 4.57 Antimony
1.07 J 17440-38-2 06935 0.732 4.57 Arsenic
7.41 17440-39-3 06946 0.0377 1.14 Barium
N.D.17440-41-7 06947 0.0766 1.14 Beryllium
2.75 J 17440-42-8 07914 0.960 11.4 Boron
N.D.17440-43-9 06949 0.0377 1.14 Cadmium
1.12 J 17440-47-3 06951 0.126 3.43 Chromium
N.D.17440-50-8 06953 0.377 2.29 Copper
267 17439-89-6 01654 3.82 45.7 Iron
1.12 J 17439-92-1 06955 0.572 3.43 Lead
2.52 17439-96-5 06958 0.0949 1.14 Manganese
N.D.17439-98-7 06960 0.194 2.29 Molybdenum
0.252 J 17440-02-0 06961 0.171 2.29 Nickel
N.D.17782-49-2 06936 0.503 4.57 Selenium
N.D.17440-22-4 06966 0.217 1.14 Silver
3.43 17440-24-6 07968 0.0377 1.14 Strontium
N.D.17440-28-0 06925 0.915 6.86 Thallium
0.935 J 17440-66-6 06972 0.297 4.57 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
N.D.17439-97-6 00159 0.0118 0.237 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
7.16 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23.1 C.
% %%Wet Chemistry SM 2540 G-1997
16.7 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Arsenic 06935
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 63 of 81

LL Sample # SW 7520723
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-7(15-16)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:35 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D715T SDG#: DUK36-25
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Iron 01654
1Tara L Snyder07/10/2014 05:08 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Silver 06966
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 15:58 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:43 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402B1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 64 of 81

LL Sample # TL 7520724
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-7(15-16)-20140701 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:35 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D715S SDG#: DUK36-26
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
N.D.17440-38-2 07035 0.0072 0.0400 Arsenic
0.0447 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0527 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
1.86 17440-70-2 01750 0.0334 0.400 Calcium
0.0045 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.821 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.364 17439-95-4 01757 0.0167 0.200 Magnesium
0.0079 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0063 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
0.217 J 17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
5.74 17440-23-5 01767 0.167 2.00 Sodium
0.0250 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0099 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Beryllium 07047
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 65 of 81

LL Sample # TL 7520724
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-7(15-16)-20140701 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:35 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D715S SDG#: DUK36-26
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 03:22 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:51 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 66 of 81

LL Sample # SW 7520725
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-14(3-4)-20140702 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:30 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D143T SDG#: DUK36-27
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.537 6.50 Antimony
35.1 17440-38-2 06935 1.04 6.50 Arsenic
447 57440-39-3 06946 0.268 8.13 Barium
5.15 17440-41-7 06947 0.109 1.63 Beryllium
9.87 J 17440-42-8 07914 1.37 16.3 Boron
N.D.17440-43-9 06949 0.0537 1.63 Cadmium
21.1 17440-47-3 06951 0.179 4.88 Chromium
56.1 17440-50-8 06953 0.537 3.25 Copper
13,400 17439-89-6 01654 5.43 65.0 Iron
14.6 17439-92-1 06955 0.813 4.88 Lead
152 17439-96-5 06958 0.135 1.63 Manganese
3.02 J 17439-98-7 06960 0.276 3.25 Molybdenum
29.9 17440-02-0 06961 0.244 3.25 Nickel
2.77 J 17782-49-2 06936 0.715 6.50 Selenium
N.D.17440-22-4 06966 0.309 1.63 Silver
235 57440-24-6 07968 0.268 8.13 Strontium
N.D.17440-28-0 06925 1.30 9.76 Thallium
20.5 17440-66-6 06972 0.423 6.50 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.106 J 17439-97-6 00159 0.0156 0.312 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
6.32 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23.1 C.
% %%Wet Chemistry SM 2540 G-1997
38.5 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Arsenic 06935
5Tara L Snyder07/10/2014 05:16 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 67 of 81

LL Sample # SW 7520725
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-14(3-4)-20140702 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:30 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D143T SDG#: DUK36-27
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Iron 01654
1Tara L Snyder07/10/2014 05:12 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Silver 06966
5Tara L Snyder07/10/2014 05:16 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 16:02 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:45 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402B1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 68 of 81

LL Sample # TL 7520726
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-14(3-4)-20140702 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:30 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D143S SDG#: DUK36-28
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
N.D.17440-38-2 07035 0.0072 0.0400 Arsenic
0.0352 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0466 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
1.11 17440-70-2 01750 0.0334 0.400 Calcium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.139 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.515 17439-95-4 01757 0.0167 0.200 Magnesium
0.0021 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0073 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
5.53 17440-23-5 01767 0.167 2.00 Sodium
0.0210 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0079 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Beryllium 07047
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 69 of 81

LL Sample # TL 7520726
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-14(3-4)-20140702 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:30 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D143S SDG#: DUK36-28
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 03:25 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:53 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 70 of 81

LL Sample # SW 7520727
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-14(7-8)-20140702 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:40 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D147T SDG#: DUK36-29
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.526 6.38 Antimony
39.0 17440-38-2 06935 1.02 6.38 Arsenic
443 57440-39-3 06946 0.263 7.97 Barium
2.64 17440-41-7 06947 0.107 1.59 Beryllium
12.4 J 17440-42-8 07914 1.34 15.9 Boron
N.D.17440-43-9 06949 0.0526 1.59 Cadmium
17.1 17440-47-3 06951 0.175 4.78 Chromium
34.9 17440-50-8 06953 0.526 3.19 Copper
16,200 17439-89-6 01654 5.32 63.8 Iron
9.93 17439-92-1 06955 0.797 4.78 Lead
72.7 17439-96-5 06958 0.132 1.59 Manganese
2.19 J 17439-98-7 06960 0.271 3.19 Molybdenum
16.6 17440-02-0 06961 0.239 3.19 Nickel
4.83 J 17782-49-2 06936 0.701 6.38 Selenium
N.D.17440-22-4 06966 0.303 1.59 Silver
195 57440-24-6 07968 0.263 7.97 Strontium
N.D.17440-28-0 06925 1.28 9.57 Thallium
15.0 17440-66-6 06972 0.414 6.38 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.131 J 17439-97-6 00159 0.0154 0.308 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
5.90 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23 C.
% %%Wet Chemistry SM 2540 G-1997
39.1 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Arsenic 06935
5Tara L Snyder07/10/2014 05:32 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 71 of 81

LL Sample # SW 7520727
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-14(7-8)-20140702 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:40 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D147T SDG#: DUK36-29
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Iron 01654
1Tara L Snyder07/10/2014 05:28 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Silver 06966
5Tara L Snyder07/10/2014 05:32 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 16:06 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:47 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 20:15 14184039402B1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 19:40 14189820002B1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 72 of 81

LL Sample # TL 7520728
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-14(7-8)-20140702 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:40 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D147S SDG#: DUK36-30*
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
N.D.17440-38-2 07035 0.0072 0.0400 Arsenic
0.0870 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0250 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
1.71 17440-70-2 01750 0.0334 0.400 Calcium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
N.D.17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.320 17439-95-4 01757 0.0167 0.200 Magnesium
N.D.17439-96-5 07058 0.00083 0.0100 Manganese
0.0089 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
0.0021 J 17440-02-0 07061 0.0016 0.0200 Nickel
0.409 J 17440-09-7 01762 0.133 1.00 Potassium
0.0065 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
2.76 17440-23-5 01767 0.167 2.00 Sodium
0.129 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Antimony 07044
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Barium 07046
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Beryllium 07047
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Boron 08014
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Cadmium 07049
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Calcium 01750
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 73 of 81

LL Sample # TL 7520728
LL Group # 1486445
Account # 10634
Sample Description: SS-F-DPT-14(7-8)-20140702 Solid Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:40 by RD
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:29
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
D147S SDG#: DUK36-30*
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Copper 07053
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Iron 01754
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Lead 07055
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Magnesium 01757
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Manganese 07058
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Molybdenum 07060
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Nickel 07061
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Potassium 01762
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Selenium 07036
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Silver 07066
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Sodium 01767
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Strontium 08068
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Thallium 07022
1Tara L Snyder07/11/2014 03:29 1419006360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 21:55 1419057130031SW-846 7470A Mercury 00259
1James L Mertz07/10/2014 06:33 1419006360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/10/2014 07:34 1419057130031SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/08/2014 12:00 14189-2486-
1567
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 74 of 81

Page 1 of 4

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1486445
Reported: 07/14/14 at 11:29 AM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these
situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD was performed, unless otherwise
specified in the method.

All Inorganic Initial Calibration and Continuing Calibration Blanks met acceptable method criteria unless
otherwise noted on the Analysis Report.

Laboratory Compliance Quality Control

Blank Blank Blank Report LCS LCSD LCS/LCSD
Analysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max

Batch number: 141880637002 Sample number(s): 7520693,7520695,7520697,7520699,7520701-
7520704,7520709,7520711,7520713,7520715,7520717,7520719,7520721,7520723,752072
5,7520727

Antimony N.D. 0.330 4.00 mg/kg 104 80-120
Arsenic N.D. 0.640 4.00 mg/kg 106 80-120
Barium 0.0340 J 0.0330 1.00 mg/kg 100 80-120
Beryllium N.D. 0.0670 1.00 mg/kg 100 80-120
Boron 2.54 J 0.840 10.0 mg/kg 98 80-120
Cadmium N.D. 0.0330 1.00 mg/kg 102 80-120
Chromium N.D. 0.110 3.00 mg/kg 100 80-120
Copper N.D. 0.330 2.00 mg/kg 102 80-120
Iron N.D. 3.34 40.0 mg/kg 105 80-120
Lead N.D. 0.500 3.00 mg/kg 104 80-120
Manganese N.D. 0.0830 1.00 mg/kg 103 80-120
Molybdenum N.D. 0.170 2.00 mg/kg 101 80-120
Nickel N.D. 0.150 2.00 mg/kg 106 80-120
Selenium N.D. 0.440 4.00 mg/kg 97 80-120
Silver N.D. 0.190 1.00 mg/kg 82 80-120
Strontium 0.179 J 0.0330 1.00 mg/kg 101 80-120
Thallium N.D. 0.800 6.00 mg/kg 92 80-120
Zinc 1.06 J 0.260 4.00 mg/kg 100 80-120

Batch number: 141880638001 Sample number(s): 7520693,7520695,7520697,7520699,7520701-
7520704,7520709,7520711,7520713,7520715,7520717,7520719,7520721,7520723,752072
5,7520727

Mercury N.D. 0.0100 0.200 mg/kg 85 80-120

Batch number: 141900636001 Sample number(s): 7520694,7520696,7520698,7520700,7520705-
7520708,7520710,7520712,7520714,7520716,7520718,7520720,7520722,7520724,752072
6,7520728

Antimony N.D. 0.0051 0.0400 mg/l 108 80-120
Arsenic N.D. 0.0072 0.0400 mg/l 106 80-120
Barium N.D. 0.00033 0.0100 mg/l 103 80-120
Beryllium N.D. 0.00067 0.0100 mg/l 102 80-120
Boron N.D. 0.0046 0.100 mg/l 95 80-120
Cadmium N.D. 0.00033 0.0100 mg/l 104 80-120
Calcium N.D. 0.0334 0.400 mg/l 103 80-120
Chromium N.D. 0.0013 0.0300 mg/l 103 80-120
Copper N.D. 0.0028 0.0200 mg/l 105 80-120
Iron N.D. 0.0334 0.400 mg/l 105 80-120
Lead N.D. 0.0047 0.0300 mg/l 110 80-120
Magnesium N.D. 0.0167 0.200 mg/l 102 80-120
Manganese N.D. 0.00083 0.0100 mg/l 104 80-120
Molybdenum N.D. 0.0017 0.0200 mg/l 107 80-120
Page 75 of 81

Page 2 of 4

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1486445
Reported: 07/14/14 at 11:29 AM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Blank Blank Blank Report LCS LCSD LCS/LCSD
Analysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max
Nickel N.D. 0.0016 0.0200 mg/l 109 80-120
Potassium N.D. 0.133 1.00 mg/l 100 80-120
Selenium N.D. 0.0048 0.0400 mg/l 104 80-120
Silver N.D. 0.0018 0.0100 mg/l 111 80-120
Sodium N.D. 0.167 2.00 mg/l 103 80-120
Strontium N.D. 0.00033 0.0100 mg/l 104 80-120
Thallium N.D. 0.0051 0.0600 mg/l 98 80-120
Zinc N.D. 0.0020 0.0400 mg/l 103 80-120

Batch number: 141905713003 Sample number(s): 7520694,7520696,7520698,7520700,7520705-
7520708,7520710,7520712,7520714,7520716,7520718,7520720,7520722,7520724,752072
6,7520728

Mercury N.D. 0.00006
0
0.00020 mg/l 107 80-120

Batch number: 14184039402A Sample number(s):
7520693,7520695,7520697,7520699,7520701,7520704,7520709,7520711,7520713,752071
5

pH 100 90-110

Batch number: 14184039402B Sample number(s): 7520717,7520719,7520721,7520723,7520725,7520727
pH 100 90-110

Batch number: 14189820002A Sample number(s): 7520693,7520695,7520697,7520699
Moisture 100 99-101

Batch number: 14189820002B Sample number(s): 7520701-
7520704,7520709,7520711,7520713,7520715,7520717,7520719,7520721,7520723,752072
5,7520727

Moisture 100 99-101
Moisture 100 99-101
Moisture Duplicate 100 99-101

Sample Matrix Quality Control
Unspiked (UNSPK) = the sample used in conjunction with the matrix spike
Background (BKG) = the sample used in conjunction with the duplicate

MS MSD MS/MSD RPD BKG DUP DUP Dup RPD
Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___

Batch number: 141880637002 Sample number(s): 7520693,7520695,7520697,7520699,7520701-
7520704,7520709,7520711,7520713,7520715,7520717,7520719,7520721,7520723,7520725,
7520727 UNSPK: 7520701 BKG: 7520701
Antimony 83 84 75-125 3 20 N.D. N.D. 0 (1) 20
Arsenic 96 98 75-125 2 20 14.6 16.5 12 (1) 20
Barium 96 108 75-125 6 20 269 307 13 20
Beryllium 100 104 83-119 3 20 2.18 2.70 22* (1) 20
Boron 97 96 84-110 1 20 6.62 J 7.35 J 10 (1) 20
Cadmium 95 95 75-120 1 20 N.D. N.D. 0 (1) 20
Chromium 116 118 75-125 2 20 9.34 10.9 15 (1) 20
Copper 102 107 75-125 3 20 21.3 25.8 19 20
Iron 965 (2) 741 (2) 75-125 2 20 9,010 9,100 1 20
Lead 96 100 75-125 4 20 6.81 8.09 17 (1) 20
Page 76 of 81

Page 3 of 4

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1486445
Reported: 07/14/14 at 11:29 AM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Sample Matrix Quality Control
Unspiked (UNSPK) = the sample used in conjunction with the matrix spike
Background (BKG) = the sample used in conjunction with the duplicate

MS MSD MS/MSD RPD BKG DUP DUP Dup RPD
Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___
Manganese 70* 67* 75-125 1 20 64.1 43.7 38* 20
Molybdenum 97 98 82-110 2 20 1.42 J 1.19 J 17 (1) 20
Nickel 102 103 75-125 1 20 14.7 16.0 9 20
Selenium 96 97 75-125 2 20 2.68 J 3.70 J 32* (1) 20
Silver 75 74* 75-125 0 20 N.D. N.D. 0 (1) 20
Strontium 93 111 81-125 7 20 145 168 15 20
Thallium 75* 75* 78-119 1 20 N.D. N.D. 0 (1) 20
Zinc 92 93 75-125 2 20 13.1 11.3 15 (1) 20

Batch number: 141880638001 Sample number(s): 7520693,7520695,7520697,7520699,7520701-
7520704,7520709,7520711,7520713,7520715,7520717,7520719,7520721,7520723,7520725,
7520727 UNSPK: 7520701 BKG: 7520701
Mercury 97 122* 80-120 22* 20 0.0268 J 0.0312 J 15 (1) 20

Batch number: 141900636001 Sample number(s): 7520694,7520696,7520698,7520700,7520705-
7520708,7520710,7520712,7520714,7520716,7520718,7520720,7520722,7520724,7520726,
7520728 UNSPK: 7520705 BKG: 7520705
Antimony 96 93 75-125 4 20 0.0055 J 0.0066 J 18 (1) 20
Arsenic 98 94 75-125 4 20 0.0197 J 0.0183 J 7 (1) 20
Barium 94 91 75-125 4 20 0.105 0.115 10 20
Beryllium 97 95 75-125 2 20 N.D. N.D. 0 (1) 20
Boron 89 87 75-125 2 20 0.0284 J 0.0285 J 0 (1) 20
Cadmium 91 88 75-125 4 20 N.D. N.D. 0 (1) 20
Calcium 94 90 75-125 4 20 5.40 5.30 2 20
Chromium 91 90 75-125 1 20 0.0021 J 0.0019 J 12 (1) 20
Copper 94 91 75-125 3 20 0.0085 J 0.0091 J 8 (1) 20
Iron 98 99 75-125 1 20 0.370 J 0.362 J 2 (1) 20
Lead 91 88 75-125 3 20 N.D. N.D. 0 (1) 20
Magnesium 94 92 75-125 2 20 0.323 0.314 3 (1) 20
Manganese 90 89 75-125 1 20 0.0031 J 0.0032 J 4 (1) 20
Molybdenum 94 91 75-125 3 20 0.0172 J 0.0149 J 14 (1) 20
Nickel 90 87 75-125 3 20 N.D. N.D. 0 (1) 20
Potassium 98 96 75-125 2 20 N.D. N.D. 0 (1) 20
Selenium 96 93 75-125 3 20 N.D. 0.0051 J 200* (1) 20
Silver 71* 81 75-125 13 20 N.D. N.D. 0 (1) 20
Sodium 91 90 75-125 1 20 3.58 3.43 4 (1) 20
Strontium 99 96 75-125 3 20 0.122 0.120 1 20
Thallium 87 84 75-125 4 20 N.D. N.D. 0 (1) 20
Zinc 92 89 75-125 3 20 0.0059 J 0.0069 J 16 (1) 20

Batch number: 141905713003 Sample number(s): 7520694,7520696,7520698,7520700,7520705-
7520708,7520710,7520712,7520714,7520716,7520718,7520720,7520722,7520724,7520726,
7520728 UNSPK: 7520705 BKG: 7520705
Mercury 96 91 80-120 6 20 N.D. N.D. 0 (1) 20

Batch number: 14184039402A Sample number(s):
7520693,7520695,7520697,7520699,7520701,7520704,7520709,7520711,7520713,7520715
BKG: 7520701
pH 7.53 7.51 0 3

Batch number: 14184039402B Sample number(s): 7520717,7520719,7520721,7520723,7520725,7520727 BKG: 7520727
pH 5.90 5.86 1 3
Page 77 of 81

Page 4 of 4

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1486445
Reported: 07/14/14 at 11:29 AM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Sample Matrix Quality Control
Unspiked (UNSPK) = the sample used in conjunction with the matrix spike
Background (BKG) = the sample used in conjunction with the duplicate

MS MSD MS/MSD RPD BKG DUP DUP Dup RPD
Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___

Batch number: 14189820002A Sample number(s): 7520693,7520695,7520697,7520699 BKG: 7520697
Moisture 5.0 5.4 8* 5

Batch number: 14189820002B Sample number(s): 7520701-
7520704,7520709,7520711,7520713,7520715,7520717,7520719,7520721,7520723,7520725,
7520727 BKG: 7520701
Moisture 21.0 23.1 10* 5
Moisture 21.0 23.1 10* 5
Moisture Duplicate 21.0 23.1 10* 5

Page 78 of 81
Page 79 of 81
Page 80 of 81
Explanation of Symbols and Abbreviations

3768 0713
The following defines common symbols and abbreviations used in reporting technical data:
RL Reporting Limit BMQL Below Minimum Quantitation Level
N.D. none detected MPN Most Probable Number
TNTC Too Numerous To Count CP Units cobalt-chloroplatinate units
IU International Units NTU nephelometric turbidity units
umhos/cm micromhos/cm ng nanogram(s)
C degrees Celsius F degrees Fahrenheit
meq milliequivalents lb. pound(s)
g gram(s) kg kilogram(s)
µg microgram(s) mg milligram(s)
mL milliliter(s) L liter(s)
m3 cubic meter(s) µL microliter(s)
pg/L picogram/liter
< less than - The number following the sign is the limit of quantitation, the smallest amount of analyte which can be
reliably determined using this specific test.
> greater than
ppm parts per million - One ppm is equivalent to one milligram per kilogram (mg/kg), or one gram per million grams. For
aqueous liquids, ppm is usually taken to be equivalent to milligrams per liter (mg/l), because one liter of water has a
weight very close to a kilogram. For gases or vapors, one ppm is equivalent to one microliter per liter of gas.
ppb parts per billion
Dry weight Results printed under this heading have been adjusted for moisture content. This increases the analyte weight
basis concentration to approximate the value present in a similar sample without moisture. All other results are reported
on an as-received basis.
Data Qualifiers:
C – result confirmed by reanalysis.
J - estimated value – The result is ≥ the Method Detection Limit (MDL) and < the Limit of Quantitation (LOQ).
U.S. EPA CLP Data Qualifiers:
Organic Qualifiers Inorganic Qualifiers
A TIC is a possible aldol-condensation product B Value is <CRDL, but ≥IDL
B Analyte was also detected in the blank E Estimated due to interference
C Pesticide result confirmed by GC/MS M Duplicate injection precision not met
D Compound quantitated on a diluted sample N Spike sample not within control limits
E Concentration exceeds the calibration range of S Method of standard additions (MSA) used
the instrument for calculation
N Presumptive evidence of a compound (TICs only) U Compound was not detected
P Concentration difference between primary and W Post digestion spike out of control limits
confirmation columns >25% * Duplicate analysis not within control limits
U Compound was not detected + Correlation coefficient for MSA <0.995
X,Y,Z Defined in case narrative
Analytical test results meet all requirements of NELAC unless otherwise noted under the individual analysis.
Measurement uncertainty values, as applicable, are available upon request.
Tests results relate only to the sample tested. Clients should be aware that a critical step in a chemical or microbiological
analysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of material involved, the
test results will be meaningless. If you have questions regarding the proper techniques of collecting samples, please contact
us. We cannot be held responsible for sample integrity, however, unless sampling has been performed by a member of our
staff. This report shall not be reproduced except in full, without the written approval of the laboratory.
Times are local to the area of activity. Parameters listed in the 40 CFR part 136 Table II as “analyze immediately” are not
performed within 15 minutes.

WARRANTY AND LIMITS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results for the sample as submitted. THE
FOREGOING EXPRESS WARRANTY IS EXCLUSIVE AND IS GIVEN IN LIEU OF ALL OTHER WARRANTIES, EXPRESSED OR IMPLIED. WE DISCLAIM
ANY OTHER WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING A WARRANTY OF FITNESS FOR PARTICULAR PURPOSE AND WARRANTY OF
MERCHANTABILITY. IN NO EVENT SHALL EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL, LLC BE LIABLE FOR INDIRECT, SPECIAL,
CONSEQUENTIAL, OR INCIDENTAL DAMAGES INCLUDING, BUT NOT LIMITED TO, DAMAGES FOR LOSS OF PROFIT OR GOODWILL REGARDLESS
OF (A) THE NEGLIGENCE (EITHER SOLE OR CONCURRENT) OF EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL AND (B) WHETHER
EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL HAS BEEN INFORMED OF THE POSSIBILITY OF SUCH DAMAGES. We accept no legal
responsibility for the purposes for which the client uses the test results. No purchase order or other order for work shall be accepted by Eurofins Lancaster
Laboratories Environmental which includes any conditions that vary from the Standard Terms and Conditions, and Eurofins Lancaster Laboratories
Environmental hereby objects to any conflicting terms contained in any acceptance or order submitted by client.
Page 81 of 81

Respectfully Submitted,

[phone]

Page 2 of 28

LL Sample # SW 7519007
LL Group # 1486078
Account # 10634
Sample Description: SS-MB2(64.0-68.0)-20140625 Grab Soil Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/25/2014 14:45 by WS
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
MB264 SDG#: DUK35-01
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.452 5.48 Antimony
87.3 17440-38-2 06935 0.877 5.48 Arsenic
502 57440-39-3 06946 0.226 6.85 Barium
3.92 17440-41-7 06947 0.0918 1.37 Beryllium
42.3 17440-42-8 07914 1.15 13.7 Boron
N.D.17440-43-9 06949 0.0452 1.37 Cadmium
43.8 17440-47-3 06951 0.151 4.11 Chromium
59.1 17440-50-8 06953 0.452 2.74 Copper
14,500 17439-89-6 01654 4.58 54.8 Iron
26.1 17439-92-1 06955 0.685 4.11 Lead
87.6 17439-96-5 06958 0.114 1.37 Manganese
2.09 J 17439-98-7 06960 0.233 2.74 Molybdenum
29.8 17440-02-0 06961 0.205 2.74 Nickel
4.59 J 17782-49-2 06936 0.603 5.48 Selenium
N.D.17440-22-4 06966 0.260 1.37 Silver
318 57440-24-6 07968 0.226 6.85 Strontium
N.D.17440-28-0 06925 1.10 8.22 Thallium
43.6 17440-66-6 06972 0.356 5.48 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.140 J 17439-97-6 00159 0.0127 0.255 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
8.23 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23.6 C.
% %%Wet Chemistry SM 2540 G-1997
27.0 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Antimony 06944
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Arsenic 06935
5John P Hook07/09/2014 20:34 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 3 of 28

LL Sample # SW 7519007
LL Group # 1486078
Account # 10634
Sample Description: SS-MB2(64.0-68.0)-20140625 Grab Soil Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/25/2014 14:45 by WS
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
MB264 SDG#: DUK35-01
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Copper 06953
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Iron 01654
1John P Hook07/09/2014 19:38 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Silver 06966
5John P Hook07/09/2014 20:34 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 14:54 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 14:59 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 18:40 14184039401B1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 18:12 14189820001B1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 4 of 28

LL Sample # TL 7519008
LL Group # 1486078
Account # 10634
Sample Description: SS-MB2(64.0-68.0)-20140625 Grab Soil Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/25/2014 14:45 by WS
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
M264S SDG#: DUK35-02
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.184 17440-38-2 07035 0.0072 0.0400 Arsenic
0.124 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0517 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
4.32 17440-70-2 01750 0.0334 0.400 Calcium
0.0024 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.0602 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.751 17439-95-4 01757 0.0167 0.200 Magnesium
0.0038 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0036 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
0.654 J 17440-09-7 01762 0.133 1.00 Potassium
0.0102 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
1.39 J 17440-23-5 01767 0.167 2.00 Sodium
0.281 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Antimony 07044
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/10/2014 05:39 1418906360011SW-846 6010C Barium 07046
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Beryllium 07047
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Boron 08014
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Cadmium 07049
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Calcium 01750
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 5 of 28

LL Sample # TL 7519008
LL Group # 1486078
Account # 10634
Sample Description: SS-MB2(64.0-68.0)-20140625 Grab Soil Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/25/2014 14:45 by WS
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
M264S SDG#: DUK35-02
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Copper 07053
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Iron 01754
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Lead 07055
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Magnesium 01757
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Manganese 07058
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Molybdenum 07060
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Nickel 07061
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Potassium 01762
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Selenium 07036
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Silver 07066
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Sodium 01767
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Strontium 08068
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Thallium 07022
1Katlin N Cataldi07/09/2014 21:31 1418906360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/10/2014 13:38 1418957130021SW-846 7470A Mercury 00259
1Micaela L Dishong07/09/2014 09:10 1418906360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/09/2014 09:25 1418957130021SW-846 7470A WW SW846 Hg Digest 05713
n.a.Darin P Wagner07/07/2014 12:15 14188-482-15671SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 6 of 28

LL Sample # SW 7519009
LL Group # 1486078
Account # 10634
Sample Description: SS-MB2(76.0-80.0)-20140625 Grab Soil Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/25/2014 15:20 by WS
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
MB276 SDG#: DUK35-03
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.457 5.54 Antimony
155 57440-38-2 06935 4.43 27.7 Arsenic
735 107440-39-3 06946 0.457 13.9 Barium
5.70 17440-41-7 06947 0.0928 1.39 Beryllium
55.3 17440-42-8 07914 1.16 13.9 Boron
N.D.17440-43-9 06949 0.0457 1.39 Cadmium
54.5 17440-47-3 06951 0.152 4.16 Chromium
83.8 17440-50-8 06953 0.457 2.77 Copper
31,500 57439-89-6 01654 23.1 277 Iron
28.9 17439-92-1 06955 0.693 4.16 Lead
128 17439-96-5 06958 0.115 1.39 Manganese
3.01 17439-98-7 06960 0.235 2.77 Molybdenum
43.6 17440-02-0 06961 0.208 2.77 Nickel
6.74 17782-49-2 06936 0.609 5.54 Selenium
N.D.17440-22-4 06966 0.263 1.39 Silver
587 57440-24-6 07968 0.229 6.93 Strontium
N.D.17440-28-0 06925 1.11 8.31 Thallium
57.6 17440-66-6 06972 0.360 5.54 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.128 J 17439-97-6 00159 0.0137 0.275 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
8.41 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 23.5 C.
% %%Wet Chemistry SM 2540 G-1997
27.8 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 14:58 1418806370021SW-846 6010C Antimony 06944
5John P Hook07/09/2014 20:39 1418806370021SW-846 6010C Arsenic 06935
10John P Hook07/09/2014 20:43 1418806370021SW-846 6010C Barium 06946
1Eric L Eby07/08/2014 14:58 1418806370021SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 7 of 28

LL Sample # SW 7519009
LL Group # 1486078
Account # 10634
Sample Description: SS-MB2(76.0-80.0)-20140625 Grab Soil Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/25/2014 15:20 by WS
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
MB276 SDG#: DUK35-03
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Eric L Eby07/08/2014 14:58 1418806370021SW-846 6010C Boron 07914
1Eric L Eby07/08/2014 14:58 1418806370021SW-846 6010C Cadmium 06949
1Eric L Eby07/08/2014 14:58 1418806370021SW-846 6010C Chromium 06951
1Eric L Eby07/08/2014 14:58 1418806370021SW-846 6010C Copper 06953
5John P Hook07/09/2014 20:39 1418806370021SW-846 6010C Iron 01654
1John P Hook07/09/2014 19:42 1418806370021SW-846 6010C Lead 06955
1Eric L Eby07/08/2014 14:58 1418806370021SW-846 6010C Manganese 06958
1Eric L Eby07/08/2014 14:58 1418806370021SW-846 6010C Molybdenum 06960
1Eric L Eby07/08/2014 14:58 1418806370021SW-846 6010C Nickel 06961
1Eric L Eby07/08/2014 14:58 1418806370021SW-846 6010C Selenium 06936
1Eric L Eby07/08/2014 14:58 1418806370021SW-846 6010C Silver 06966
5John P Hook07/09/2014 20:39 1418806370021SW-846 6010C Strontium 07968
1Eric L Eby07/08/2014 14:58 1418806370021SW-846 6010C Thallium 06925
1Eric L Eby07/08/2014 14:58 1418806370021SW-846 6010C Zinc 06972
1Parker D Lindstrom07/11/2014 15:01 1418806380011SW-846 7471B Mercury 00159
1James L Mertz07/08/2014 05:19 1418806370021SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/08/2014 07:27 1418806380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/03/2014 18:40 14184039401B1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/08/2014 18:12 14189820001B1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 8 of 28

LL Sample # TL 7519010
LL Group # 1486078
Account # 10634
Sample Description: SS-MB2(76.0-80.0)-20140625 Grab Soil Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/25/2014 15:20 by WS
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
M276S SDG#: DUK35-04
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.316 17440-38-2 07035 0.0072 0.0400 Arsenic
0.0543 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.105 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
4.90 17440-70-2 01750 0.0334 0.400 Calcium
0.0023 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.125 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.849 17439-95-4 01757 0.0167 0.200 Magnesium
0.0034 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0043 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
0.437 J 17440-09-7 01762 0.133 1.00 Potassium
0.0235 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
2.06 17440-23-5 01767 0.167 2.00 Sodium
0.185 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0025 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Antimony 07044
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Arsenic 07035
1Tara L Snyder07/10/2014 06:01 1418906360011SW-846 6010C Barium 07046
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Beryllium 07047
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Boron 08014
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Cadmium 07049
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Calcium 01750
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Chromium 07051
*=This limit was used in the evaluation of the final result
Page 9 of 28

LL Sample # TL 7519010
LL Group # 1486078
Account # 10634
Sample Description: SS-MB2(76.0-80.0)-20140625 Grab Soil Sample
Non-Volatile Extraction
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 06/25/2014 15:20 by WS
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
M276S SDG#: DUK35-04
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Copper 07053
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Iron 01754
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Lead 07055
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Magnesium 01757
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Manganese 07058
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Molybdenum 07060
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Nickel 07061
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Potassium 01762
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Selenium 07036
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Silver 07066
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Sodium 01767
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Strontium 08068
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Thallium 07022
1Katlin N Cataldi07/09/2014 22:07 1418906360011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/10/2014 13:46 1418957130021SW-846 7470A Mercury 00259
1Micaela L Dishong07/09/2014 09:10 1418906360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1James L Mertz07/09/2014 09:25 1418957130021SW-846 7470A WW SW846 Hg Digest 05713
n.a.Darin P Wagner07/07/2014 12:15 14188-482-15671SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 10 of 28

LL Sample # WW 7519011
LL Group # 1486078
Account # 10634
Sample Description: GW-MW16-20140701 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:40 by MP
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DSM16 SDG#: DUK35-05
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.0081 J 17440-38-2 07035 0.0072 0.0400 Arsenic
0.0263 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.143 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
8.66 17440-70-2 01750 0.0334 0.400 Calcium
0.0020 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.781 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
3.86 17439-95-4 01757 0.0167 0.200 Magnesium
0.0204 17439-96-5 07058 0.00083 0.0100 Manganese
0.0118 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
5.46 17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
26.9 17440-23-5 01767 0.167 2.00 Sodium
0.105 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0029 J 17440-62-2 07071 0.0019 0.0100 Vanadium
0.0041 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
mg/l mg/lmg/lWet Chemistry EPA 300.0
N.D.524959-67-901505 2.0 2.5 Bromide
28.0 516887-00-600224 1.0 2.0 Chloride
N.D.514797-55-800368 0.25 0.50 Nitrate Nitrogen
N.D.514797-65-001506 0.40 0.50 Nitrite Nitrogen
31.8 514808-79-800228 1.5 5.0 Sulfate
mg/l as CaCO3mg/l as CaCO3mg/l as CaCO3EPA 310.1
23.8 1n.a. 12150 0.70 2.0 Total Alkalinity
mg/l mg/lmg/lSM 2540 C-1997
140 1n.a. 00212 9.7 30.0 Total Dissolved Solids
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
*=This limit was used in the evaluation of the final result
Page 11 of 28

LL Sample # WW 7519011
LL Group # 1486078
Account # 10634
Sample Description: GW-MW16-20140701 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:40 by MP
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DSM16 SDG#: DUK35-05
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 04:13 1418806350011SW-846 6010C Barium 07046
1Tara L Snyder07/09/2014 04:13 1418806350011SW-846 6010C Beryllium 07047
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Boron 08014
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Cadmium 07049
1Tara L Snyder07/09/2014 04:13 1418806350011SW-846 6010C Calcium 01750
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Copper 07053
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Iron 01754
1Tara L Snyder07/09/2014 04:13 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Magnesium 01757
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Molybdenum 07060
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Nickel 07061
1Tara L Snyder07/09/2014 04:13 1418806350011SW-846 6010C Potassium 01762
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Silver 07066
1Tara L Snyder07/09/2014 04:13 1418806350011SW-846 6010C Sodium 01767
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Strontium 08068
1Tara L Snyder07/09/2014 04:13 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 22:09 1418806350011SW-846 6010C Zinc 07072
1Damary Valentin07/16/2014 07:51 1419557130041SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/08/2014 11:00 1418857130011SW-846 7470A WW SW846 Hg Digest 05713
1Micaela L Dishong07/11/2014 09:34 1419157130022SW-846 7470A WW SW846 Hg Digest 05713
1James L Mertz07/15/2014 09:08 1419557130043SW-846 7470A WW SW846 Hg Digest 05713
5Clinton M Wilson07/02/2014 19:08 14183987601A1EPA 300.0 Bromide 01505
5Clinton M Wilson07/02/2014 19:08 14183987601A1EPA 300.0 Chloride 00224
5Clinton M Wilson07/02/2014 19:08 14183987601A1EPA 300.0 Nitrate Nitrogen 00368
5Clinton M Wilson07/02/2014 19:08 14183987601A1EPA 300.0 Nitrite Nitrogen 01506
5Clinton M Wilson07/02/2014 19:08 14183987601A1EPA 300.0 Sulfate 00228
1Michele L Graham07/07/2014 18:04 14188002103A1EPA 310.1 Total Alkalinity 12150
1Sarah E Thompson07/02/2014 12:20 14183021202A1SM 2540 C-1997 Total Dissolved Solids 00212
*=This limit was used in the evaluation of the final result
Page 12 of 28

LL Sample # WW 7519012
LL Group # 1486078
Account # 10634
Sample Description: GW-MW16D-20140701 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:20 by MP
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS16D SDG#: DUK35-06FD
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.0083 J 17440-38-2 07035 0.0072 0.0400 Arsenic
0.0343 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.432 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
24.5 17440-70-2 01750 0.0334 0.400 Calcium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
1.82 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
5.97 17439-95-4 01757 0.0167 0.200 Magnesium
0.269 17439-96-5 07058 0.00083 0.0100 Manganese
N.D.17439-98-7 07060 0.0017 0.0200 Molybdenum
0.0022 J 17440-02-0 07061 0.0016 0.0200 Nickel
4.82 17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
80.7 57440-23-5 01767 0.835 10.0 Sodium
0.154 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0043 J 17440-62-2 07071 0.0019 0.0100 Vanadium
0.0378 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
mg/l mg/lmg/lWet Chemistry EPA 300.0
N.D.524959-67-901505 2.0 2.5 Bromide
114 5016887-00-600224 10.0 20.0 Chloride
N.D.514797-55-800368 0.25 0.50 Nitrate Nitrogen
N.D.514797-65-001506 0.40 0.50 Nitrite Nitrogen
89.0 1014808-79-800228 3.0 10.0 Sulfate
mg/l as CaCO3mg/l as CaCO3mg/l as CaCO3EPA 310.1
2.7 1n.a. 12150 0.70 2.0 Total Alkalinity
mg/l mg/lmg/lSM 2540 C-1997
345 1n.a. 00212 9.7 30.0 Total Dissolved Solids
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
*=This limit was used in the evaluation of the final result
Page 13 of 28

LL Sample # WW 7519012
LL Group # 1486078
Account # 10634
Sample Description: GW-MW16D-20140701 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 13:20 by MP
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS16D SDG#: DUK35-06FD
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 04:16 1418806350011SW-846 6010C Barium 07046
1Tara L Snyder07/09/2014 04:16 1418806350011SW-846 6010C Beryllium 07047
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Boron 08014
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Cadmium 07049
1Tara L Snyder07/09/2014 04:16 1418806350011SW-846 6010C Calcium 01750
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Copper 07053
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Iron 01754
1Tara L Snyder07/09/2014 04:16 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Magnesium 01757
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Molybdenum 07060
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Nickel 07061
1Tara L Snyder07/09/2014 04:16 1418806350011SW-846 6010C Potassium 01762
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Silver 07066
5Tara L Snyder07/09/2014 04:20 1418806350011SW-846 6010C Sodium 01767
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Strontium 08068
1Tara L Snyder07/09/2014 04:16 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 22:20 1418806350011SW-846 6010C Zinc 07072
1Damary Valentin07/16/2014 07:53 1419557130041SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/08/2014 11:00 1418857130011SW-846 7470A WW SW846 Hg Digest 05713
1Micaela L Dishong07/11/2014 09:34 1419157130022SW-846 7470A WW SW846 Hg Digest 05713
1James L Mertz07/15/2014 09:08 1419557130043SW-846 7470A WW SW846 Hg Digest 05713
5Clinton M Wilson07/02/2014 19:56 14183987601A1EPA 300.0 Bromide 01505
50Clinton M Wilson07/03/2014 13:05 14183987601A1EPA 300.0 Chloride 00224
5Clinton M Wilson07/02/2014 19:56 14183987601A1EPA 300.0 Nitrate Nitrogen 00368
5Clinton M Wilson07/02/2014 19:56 14183987601A1EPA 300.0 Nitrite Nitrogen 01506
10Clinton M Wilson07/03/2014 12:46 14183987601A1EPA 300.0 Sulfate 00228
1Michele L Graham07/07/2014 14:55 14188002102A1EPA 310.1 Total Alkalinity 12150
1Sarah E Thompson07/02/2014 12:20 14183021202A1SM 2540 C-1997 Total Dissolved Solids 00212
*=This limit was used in the evaluation of the final result
Page 14 of 28

LL Sample # WW 7519013
LL Group # 1486078
Account # 10634
Sample Description: EB-02-20140701 Grab Water Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 12:20 by MP
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DSEB2 SDG#: DUK35-07EB
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
N.D.17440-38-2 07035 0.0072 0.0400 Arsenic
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.00094 J 17439-96-5 07058 0.00083 0.0100 Manganese
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-62-2 07071 0.0019 0.0100 Vanadium
N.D.17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 22:23 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 22:23 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 04:24 1418806350011SW-846 6010C Beryllium 07047
1John P Hook07/08/2014 22:23 1418806350011SW-846 6010C Cadmium 07049
1John P Hook07/08/2014 22:23 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 22:23 1418806350011SW-846 6010C Copper 07053
1Tara L Snyder07/09/2014 04:24 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 22:23 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 22:23 1418806350011SW-846 6010C Nickel 07061
1John P Hook07/08/2014 22:23 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 22:23 1418806350011SW-846 6010C Silver 07066
1Tara L Snyder07/09/2014 04:24 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 22:23 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 22:23 1418806350011SW-846 6010C Zinc 07072
1Damary Valentin07/16/2014 07:55 1419557130041SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/08/2014 11:00 1418857130011SW-846 7470A WW SW846 Hg Digest 05713
1Micaela L Dishong07/11/2014 09:34 1419157130022SW-846 7470A WW SW846 Hg Digest 05713
1James L Mertz07/15/2014 09:08 1419557130043SW-846 7470A WW SW846 Hg Digest 05713
*=This limit was used in the evaluation of the final result
Page 15 of 28

LL Sample # WW 7519014
LL Group # 1486078
Account # 10634
Sample Description: SB-02-20140701 Grab Water Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 12:10 by MP
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DSSB2 SDG#: DUK35-08
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
N.D.17440-38-2 07035 0.0072 0.0400 Arsenic
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
N.D.17439-92-1 07055 0.0047 0.0300 Lead
N.D.17439-96-5 07058 0.00083 0.0100 Manganese
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-62-2 07071 0.0019 0.0100 Vanadium
N.D.17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 22:27 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 22:27 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 04:27 1418806350011SW-846 6010C Beryllium 07047
1John P Hook07/08/2014 22:27 1418806350011SW-846 6010C Cadmium 07049
1John P Hook07/08/2014 22:27 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 22:27 1418806350011SW-846 6010C Copper 07053
1Tara L Snyder07/09/2014 04:27 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 22:27 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 22:27 1418806350011SW-846 6010C Nickel 07061
1John P Hook07/08/2014 22:27 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 22:27 1418806350011SW-846 6010C Silver 07066
1Tara L Snyder07/09/2014 04:27 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 22:27 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 22:27 1418806350011SW-846 6010C Zinc 07072
1Damary Valentin07/16/2014 07:57 1419557130041SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/08/2014 11:00 1418857130011SW-846 7470A WW SW846 Hg Digest 05713
1Micaela L Dishong07/11/2014 09:34 1419157130022SW-846 7470A WW SW846 Hg Digest 05713
1James L Mertz07/15/2014 09:08 1419557130043SW-846 7470A WW SW846 Hg Digest 05713
*=This limit was used in the evaluation of the final result
Page 16 of 28

LL Sample # WW 7519015
LL Group # 1486078
Account # 10634
Sample Description: GW-MW20-20140701 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 15:40 by MP
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DSM20 SDG#: DUK35-09
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
N.D.17440-38-2 07035 0.0072 0.0400 Arsenic
0.126 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.129 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
85.5 17440-70-2 01750 0.0334 0.400 Calcium
0.0019 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
2.61 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
8.94 17439-95-4 01757 0.0167 0.200 Magnesium
0.413 17439-96-5 07058 0.00083 0.0100 Manganese
N.D.17439-98-7 07060 0.0017 0.0200 Molybdenum
0.0134 J 17440-02-0 07061 0.0016 0.0200 Nickel
6.71 17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
16.3 17440-23-5 01767 0.167 2.00 Sodium
0.785 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0413 17440-62-2 07071 0.0019 0.0100 Vanadium
0.0054 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
mg/l mg/lmg/lWet Chemistry EPA 300.0
N.D.524959-67-901505 2.0 2.5 Bromide
18.8 516887-00-600224 1.0 2.0 Chloride
N.D.514797-55-800368 0.25 0.50 Nitrate Nitrogen
N.D.514797-65-001506 0.40 0.50 Nitrite Nitrogen
53.7 514808-79-800228 1.5 5.0 Sulfate
mg/l as CaCO3mg/l as CaCO3mg/l as CaCO3EPA 310.1
207 1n.a. 12150 0.70 2.0 Total Alkalinity
mg/l mg/lmg/lSM 2540 C-1997
334 1n.a. 00212 9.7 30.0 Total Dissolved Solids
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
*=This limit was used in the evaluation of the final result
Page 17 of 28

LL Sample # WW 7519015
LL Group # 1486078
Account # 10634
Sample Description: GW-MW20-20140701 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 15:40 by MP
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DSM20 SDG#: DUK35-09
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 04:38 1418806350011SW-846 6010C Barium 07046
1Tara L Snyder07/09/2014 04:38 1418806350011SW-846 6010C Beryllium 07047
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Boron 08014
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Cadmium 07049
1Tara L Snyder07/09/2014 04:38 1418806350011SW-846 6010C Calcium 01750
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Copper 07053
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Iron 01754
1Tara L Snyder07/09/2014 04:38 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Magnesium 01757
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Molybdenum 07060
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Nickel 07061
1Tara L Snyder07/09/2014 04:38 1418806350011SW-846 6010C Potassium 01762
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Silver 07066
1Tara L Snyder07/09/2014 04:38 1418806350011SW-846 6010C Sodium 01767
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Strontium 08068
1Tara L Snyder07/09/2014 04:38 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 22:31 1418806350011SW-846 6010C Zinc 07072
1Damary Valentin07/16/2014 07:59 1419557130041SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/08/2014 11:00 1418857130011SW-846 7470A WW SW846 Hg Digest 05713
1Micaela L Dishong07/11/2014 09:34 1419157130022SW-846 7470A WW SW846 Hg Digest 05713
1James L Mertz07/15/2014 09:08 1419557130043SW-846 7470A WW SW846 Hg Digest 05713
5Clinton M Wilson07/02/2014 23:59 14183987601B1EPA 300.0 Bromide 01505
5Clinton M Wilson07/02/2014 23:59 14183987601B1EPA 300.0 Chloride 00224
5Clinton M Wilson07/02/2014 23:59 14183987601B1EPA 300.0 Nitrate Nitrogen 00368
5Clinton M Wilson07/02/2014 23:59 14183987601B1EPA 300.0 Nitrite Nitrogen 01506
5Clinton M Wilson07/02/2014 23:59 14183987601B1EPA 300.0 Sulfate 00228
1Michele L Graham07/07/2014 14:28 14188002102A1EPA 310.1 Total Alkalinity 12150
1Sarah E Thompson07/03/2014 07:43 14184021201A1SM 2540 C-1997 Total Dissolved Solids 00212
*=This limit was used in the evaluation of the final result
Page 18 of 28

LL Sample # WW 7519016
LL Group # 1486078
Account # 10634
Sample Description: GW-MW20D-20140701 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 16:35 by MP
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS20D SDG#: DUK35-10FD*
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
N.D.17440-38-2 07035 0.0072 0.0400 Arsenic
0.0587 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.227 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
69.9 17440-70-2 01750 0.0334 0.400 Calcium
0.0014 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
2.31 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
5.62 17439-95-4 01757 0.0167 0.200 Magnesium
0.190 17439-96-5 07058 0.00083 0.0100 Manganese
0.0072 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
2.72 17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
51.7 27440-23-5 01767 0.334 4.00 Sodium
0.186 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-62-2 07071 0.0019 0.0100 Vanadium
0.0020 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
mg/l mg/lmg/lWet Chemistry EPA 300.0
N.D.524959-67-901505 2.0 2.5 Bromide
83.5 2016887-00-600224 4.0 8.0 Chloride
N.D.514797-55-800368 0.25 0.50 Nitrate Nitrogen
N.D.514797-65-001506 0.40 0.50 Nitrite Nitrogen
69.6 514808-79-800228 1.5 5.0 Sulfate
mg/l as CaCO3mg/l as CaCO3mg/l as CaCO3EPA 310.1
118 1n.a. 12150 0.70 2.0 Total Alkalinity
mg/l mg/lmg/lSM 2540 C-1997
365 1n.a. 00212 9.7 30.0 Total Dissolved Solids
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
*=This limit was used in the evaluation of the final result
Page 19 of 28

LL Sample # WW 7519016
LL Group # 1486078
Account # 10634
Sample Description: GW-MW20D-20140701 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 16:35 by MP
Submitted: 07/02/2014 09:20
GeoSyntec Consultants
Reported: 07/16/2014 13:58
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS20D SDG#: DUK35-10FD*
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 04:46 1418806350011SW-846 6010C Barium 07046
1Tara L Snyder07/09/2014 04:46 1418806350011SW-846 6010C Beryllium 07047
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Boron 08014
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Cadmium 07049
1Tara L Snyder07/09/2014 04:46 1418806350011SW-846 6010C Calcium 01750
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Copper 07053
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Iron 01754
1Tara L Snyder07/09/2014 04:46 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Magnesium 01757
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Molybdenum 07060
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Nickel 07061
1Tara L Snyder07/09/2014 04:46 1418806350011SW-846 6010C Potassium 01762
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Silver 07066
2Tara L Snyder07/09/2014 04:50 1418806350011SW-846 6010C Sodium 01767
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Strontium 08068
1Tara L Snyder07/09/2014 04:46 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 22:35 1418806350011SW-846 6010C Zinc 07072
1Damary Valentin07/16/2014 08:01 1419557130041SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/08/2014 11:00 1418857130011SW-846 7470A WW SW846 Hg Digest 05713
1Micaela L Dishong07/11/2014 09:34 1419157130022SW-846 7470A WW SW846 Hg Digest 05713
1James L Mertz07/15/2014 09:08 1419557130043SW-846 7470A WW SW846 Hg Digest 05713
5Clinton M Wilson07/03/2014 01:20 14183987601B1EPA 300.0 Bromide 01505
20Clinton M Wilson07/03/2014 13:21 14183987601B1EPA 300.0 Chloride 00224
5Clinton M Wilson07/03/2014 01:20 14183987601B1EPA 300.0 Nitrate Nitrogen 00368
5Clinton M Wilson07/03/2014 01:20 14183987601B1EPA 300.0 Nitrite Nitrogen 01506
5Clinton M Wilson07/03/2014 01:20 14183987601B1EPA 300.0 Sulfate 00228
1Michele L Graham07/07/2014 14:09 14188002102A1EPA 310.1 Total Alkalinity 12150
1Sarah E Thompson07/03/2014 07:43 14184021201A1SM 2540 C-1997 Total Dissolved Solids 00212
*=This limit was used in the evaluation of the final result
Page 20 of 28

Page 1 of 5

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1486078
Reported: 07/16/14 at 01:58 PM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these
situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD was performed, unless otherwise
specified in the method.

All Inorganic Initial Calibration and Continuing Calibration Blanks met acceptable method criteria unless
otherwise noted on the Analysis Report.

Laboratory Compliance Quality Control

Blank Blank Blank Report LCS LCSD LCS/LCSD
Analysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max

Batch number: 141880635001 Sample number(s): 7519011-7519016
Antimony N.D. 0.0051 0.0400 mg/l 109 88-111
Arsenic N.D. 0.0072 0.0400 mg/l 111 90-113
Barium N.D. 0.00033 0.0100 mg/l 108 90-110
Beryllium N.D. 0.00067 0.0100 mg/l 106 90-111
Boron N.D. 0.0046 0.100 mg/l 100 90-110
Cadmium N.D. 0.00033 0.0100 mg/l 105 90-112
Calcium N.D. 0.0334 0.400 mg/l 109 90-112
Chromium N.D. 0.0013 0.0300 mg/l 102 90-110
Copper N.D. 0.0028 0.0200 mg/l 108 90-112
Iron N.D. 0.0334 0.400 mg/l 112 90-112
Lead N.D. 0.0047 0.0300 mg/l 114 88-116
Magnesium N.D. 0.0167 0.200 mg/l 107 89-110
Manganese 0.0013 J 0.00083 0.0100 mg/l 108 90-110
Molybdenum N.D. 0.0017 0.0200 mg/l 106 90-110
Nickel N.D. 0.0016 0.0200 mg/l 111 90-117
Potassium N.D. 0.133 1.00 mg/l 104 90-110
Selenium N.D. 0.0048 0.0400 mg/l 103 89-113
Silver N.D. 0.0018 0.0100 mg/l 94 80-120
Sodium N.D. 0.167 2.00 mg/l 106 87-114
Strontium N.D. 0.00033 0.0100 mg/l 108 90-110
Thallium N.D. 0.0051 0.0600 mg/l 101 90-118
Vanadium N.D. 0.0019 0.0100 mg/l 102 90-110
Zinc N.D. 0.0020 0.0400 mg/l 104 90-110

Batch number: 141880637002 Sample number(s): 7519007,7519009
Antimony N.D. 0.330 4.00 mg/kg 104 80-120
Arsenic N.D. 0.640 4.00 mg/kg 106 80-120
Barium 0.0340 J 0.0330 1.00 mg/kg 100 80-120
Beryllium N.D. 0.0670 1.00 mg/kg 100 80-120
Boron 2.54 J 0.840 10.0 mg/kg 98 80-120
Cadmium N.D. 0.0330 1.00 mg/kg 102 80-120
Chromium N.D. 0.110 3.00 mg/kg 100 80-120
Copper N.D. 0.330 2.00 mg/kg 102 80-120
Iron N.D. 3.34 40.0 mg/kg 105 80-120
Lead N.D. 0.500 3.00 mg/kg 104 80-120
Manganese N.D. 0.0830 1.00 mg/kg 103 80-120
Molybdenum N.D. 0.170 2.00 mg/kg 101 80-120
Nickel N.D. 0.150 2.00 mg/kg 106 80-120
Selenium N.D. 0.440 4.00 mg/kg 97 80-120
Silver N.D. 0.190 1.00 mg/kg 82 80-120
Strontium 0.179 J 0.0330 1.00 mg/kg 101 80-120
Thallium N.D. 0.800 6.00 mg/kg 92 80-120
Zinc 1.06 J 0.260 4.00 mg/kg 100 80-120
Page 21 of 28

Page 2 of 5

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1486078
Reported: 07/16/14 at 01:58 PM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Blank Blank Blank Report LCS LCSD LCS/LCSD
Analysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max

Batch number: 141880638001 Sample number(s): 7519007,7519009
Mercury N.D. 0.0100 0.200 mg/kg 85 80-120

Batch number: 141890636001 Sample number(s): 7519008,7519010
Antimony N.D. 0.0051 0.0400 mg/l 102 80-120
Arsenic N.D. 0.0072 0.0400 mg/l 102 80-120
Barium N.D. 0.00033 0.0100 mg/l 101 80-120
Beryllium N.D. 0.00067 0.0100 mg/l 100 80-120
Boron N.D. 0.0046 0.100 mg/l 97 80-120
Cadmium N.D. 0.00033 0.0100 mg/l 102 80-120
Calcium N.D. 0.0334 0.400 mg/l 101 80-120
Chromium N.D. 0.0013 0.0300 mg/l 101 80-120
Copper N.D. 0.0028 0.0200 mg/l 97 80-120
Iron N.D. 0.0334 0.400 mg/l 102 80-120
Lead N.D. 0.0047 0.0300 mg/l 105 80-120
Magnesium N.D. 0.0167 0.200 mg/l 98 80-120
Manganese 0.0011 J 0.00083 0.0100 mg/l 102 80-120
Molybdenum N.D. 0.0017 0.0200 mg/l 101 80-120
Nickel N.D. 0.0016 0.0200 mg/l 105 80-120
Potassium N.D. 0.133 1.00 mg/l 97 80-120
Selenium N.D. 0.0048 0.0400 mg/l 97 80-120
Silver N.D. 0.0018 0.0100 mg/l 103 80-120
Sodium N.D. 0.167 2.00 mg/l 98 80-120
Strontium N.D. 0.00033 0.0100 mg/l 99 80-120
Thallium 0.0056 J 0.0051 0.0600 mg/l 91 80-120
Zinc 0.0036 J 0.0020 0.0400 mg/l 101 80-120

Batch number: 141895713002 Sample number(s): 7519008,7519010
Mercury N.D. 0.00006
0
0.00020 mg/l 112 80-120

Batch number: 141955713004 Sample number(s): 7519011-7519016
Mercury N.D. 0.00006
0
0.00020 mg/l 100 80-120

Batch number: 14183987601A Sample number(s): 7519011-7519012
Bromide N.D. 0.40 0.50 mg/l 91 91 90-110 0 20
Chloride N.D. 0.20 0.40 mg/l 93 92 90-110 0 20
Nitrate Nitrogen N.D. 0.050 0.10 mg/l 93 94 90-110 0 20
Nitrite Nitrogen N.D. 0.080 0.10 mg/l 93 93 90-110 0 20
Sulfate N.D. 0.30 1.0 mg/l 98 99 90-110 0 20

Batch number: 14183987601B Sample number(s): 7519015-7519016
Bromide N.D. 0.40 0.50 mg/l 91 91 90-110 0 20
Chloride N.D. 0.20 0.40 mg/l 93 92 90-110 0 20
Nitrate Nitrogen N.D. 0.050 0.10 mg/l 93 94 90-110 0 20
Nitrite Nitrogen N.D. 0.080 0.10 mg/l 93 93 90-110 0 20
Sulfate N.D. 0.30 1.0 mg/l 98 99 90-110 0 20

Batch number: 14183021202A Sample number(s): 7519011-7519012
Total Dissolved Solids N.D. 9.7 30.0 mg/l 98 80-120

Batch number: 14184021201A Sample number(s): 7519015-7519016
Total Dissolved Solids N.D. 9.7 30.0 mg/l 95 80-120

Page 22 of 28

Page 3 of 5

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1486078
Reported: 07/16/14 at 01:58 PM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Blank Blank Blank Report LCS LCSD LCS/LCSD
Analysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max
Batch number: 14184039401B Sample number(s): 7519007,7519009
pH 99 90-110

Batch number: 14188002102A Sample number(s): 7519012,7519015-7519016
Total Alkalinity N.D. 0.70 2.0 mg/l as
CaCO3
97 90-110

Batch number: 14188002103A Sample number(s): 7519011
Total Alkalinity N.D. 0.70 2.0 mg/l as
CaCO3
96 90-110

Batch number: 14189820001B Sample number(s): 7519007,7519009
Moisture 100 99-101

Sample Matrix Quality Control
Unspiked (UNSPK) = the sample used in conjunction with the matrix spike
Background (BKG) = the sample used in conjunction with the duplicate

MS MSD MS/MSD RPD BKG DUP DUP Dup RPD
Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___

Batch number: 141880635001 Sample number(s): 7519011-7519016 UNSPK: P520777 BKG: P520777
Antimony 108 106 76-122 2 20 N.D. N.D. 0 (1) 20
Arsenic 104 108 81-123 3 20 0.0199 J 0.0133 J 39* (1) 20
Barium 102 101 78-125 1 20 0.144 0.136 6 20
Beryllium 102 101 87-114 1 20 N.D. N.D. 0 (1) 20
Boron 74* 87 87-111 6 20 2.35 2.10 11 (1) 20
Cadmium 99 99 75-122 0 20 N.D. N.D. 0 (1) 20
Calcium 7 (2) -1 (2) 75-125 0 20 89.4 84.3 6 20
Chromium 98 95 76-120 2 20 0.0017 J 0.0019 J 11 (1) 20
Copper 106 106 86-122 0 20 N.D. N.D. 0 (1) 20
Iron 72 (2) 112 (2) 75-125 7 20 4.72 4.44 6 20
Lead 101 100 75-125 1 20 N.D. N.D. 0 (1) 20
Magnesium 20 (2) 10 (2) 81-118 1 20 25.1 23.6 6 20
Manganese 98 94 75-125 2 20 0.459 0.430 7 20
Molybdenum 102 102 89-117 0 20 0.319 0.293 9 20
Nickel 104 103 79-123 1 20 N.D. N.D. 0 (1) 20
Potassium 100 98 77-128 1 20 14.7 13.8 6 20
Selenium 100 101 75-125 1 20 N.D. N.D. 0 (1) 20
Silver 93 91 75-125 2 20 N.D. N.D. 0 (1) 20
Sodium 21 (2) 51 (2) 84-117 3 20 52.1 47.3 10 (1) 20
Strontium 49* 72* 88-117 6 20 3.20 2.88 11 20
Thallium 95 94 75-125 0 20 N.D. N.D. 0 (1) 20
Vanadium 97 97 90-117 0 20 N.D. N.D. 0 (1) 20
Zinc 100 99 85-117 0 20 0.0041 J 0.0038 J 8 (1) 20

Batch number: 141880637002 Sample number(s): 7519007,7519009 UNSPK: P520701 BKG: P520701
Antimony 83 84 75-125 3 20 N.D. N.D. 0 (1) 20
Arsenic 96 98 75-125 2 20 14.6 16.5 12 (1) 20
Barium 96 108 75-125 6 20 269 307 13 20
Beryllium 100 104 83-119 3 20 2.18 2.70 22* (1) 20
Boron 97 96 84-110 1 20 6.62 J 7.35 J 10 (1) 20
Cadmium 95 95 75-120 1 20 N.D. N.D. 0 (1) 20
Page 23 of 28

Page 4 of 5

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1486078
Reported: 07/16/14 at 01:58 PM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Sample Matrix Quality Control
Unspiked (UNSPK) = the sample used in conjunction with the matrix spike
Background (BKG) = the sample used in conjunction with the duplicate

MS MSD MS/MSD RPD BKG DUP DUP Dup RPD
Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___
Chromium 116 118 75-125 2 20 9.34 10.9 15 (1) 20
Copper 102 107 75-125 3 20 21.3 25.8 19 20
Iron 965 (2) 741 (2) 75-125 2 20 9,010 9,100 1 20
Lead 96 100 75-125 4 20 6.81 8.09 17 (1) 20
Manganese 70* 67* 75-125 1 20 64.1 43.7 38* 20
Molybdenum 97 98 82-110 2 20 1.42 J 1.19 J 17 (1) 20
Nickel 102 103 75-125 1 20 14.7 16.0 9 20
Selenium 96 97 75-125 2 20 2.68 J 3.70 J 32* (1) 20
Silver 75 74* 75-125 0 20 N.D. N.D. 0 (1) 20
Strontium 93 111 81-125 7 20 145 168 15 20
Thallium 75* 75* 78-119 1 20 N.D. N.D. 0 (1) 20
Zinc 92 93 75-125 2 20 13.1 11.3 15 (1) 20

Batch number: 141880638001 Sample number(s): 7519007,7519009 UNSPK: P520701 BKG: P520701
Mercury 97 122* 80-120 22* 20 0.0268 J 0.0312 J 15 (1) 20

Batch number: 141890636001 Sample number(s): 7519008,7519010 UNSPK: 7519008 BKG: 7519008
Antimony 88 87 75-125 1 20 N.D. N.D. 0 (1) 20
Arsenic 89 88 75-125 1 20 0.184 0.182 1 (1) 20
Barium 90 89 75-125 2 20 0.124 0.123 0 20
Beryllium 85 83 75-125 1 20 N.D. N.D. 0 (1) 20
Boron 86 86 75-125 1 20 0.0517 J 0.0473 J 9 (1) 20
Cadmium 89 88 75-125 1 20 N.D. N.D. 0 (1) 20
Calcium 89 89 75-125 0 20 4.32 4.36 1 20
Chromium 88 87 75-125 1 20 0.0024 J 0.0028 J 15 (1) 20
Copper 93 93 75-125 1 20 N.D. N.D. 0 (1) 20
Iron 87 87 75-125 0 20 0.0602 J 0.0572 J 5 (1) 20
Lead 89 88 75-125 1 20 N.D. N.D. 0 (1) 20
Magnesium 87 87 75-125 0 20 0.751 0.759 1 (1) 20
Manganese 88 87 75-125 1 20 0.0038 J 0.0037 J 2 (1) 20
Molybdenum 89 87 75-125 2 20 0.0036 J 0.0033 J 9 (1) 20
Nickel 89 89 75-125 1 20 N.D. N.D. 0 (1) 20
Potassium 92 92 75-125 0 20 0.654 J 0.663 J 1 (1) 20
Selenium 86 85 75-125 1 20 0.0102 J 0.0101 J 1 (1) 20
Silver 49* 48* 75-125 2 20 N.D. N.D. 0 (1) 20
Sodium 90 89 75-125 0 20 1.39 J 1.39 J 0 (1) 20
Strontium 90 89 75-125 1 20 0.281 0.282 0 20
Thallium 89 87 75-125 1 20 N.D. N.D. 0 (1) 20
Zinc 87 87 75-125 1 20 N.D. N.D. 0 (1) 20

Batch number: 141895713002 Sample number(s): 7519008,7519010 UNSPK: 7519008 BKG: 7519008
Mercury 99 93 80-120 7 20 N.D. N.D. 0 (1) 20

Batch number: 141955713004 Sample number(s): 7519011-7519016 UNSPK: P514111 BKG: P514111
Mercury 94 97 80-120 2 20 N.D. N.D. 0 (1) 20

Batch number: 14183987601A Sample number(s): 7519011-7519012 UNSPK: 7519011 BKG: 7519011
Bromide 89* 90-110 N.D. N.D. 0 (1) 20
Chloride 83* 90-110 28.0 27.8 0 20
Nitrate Nitrogen 92 90-110 N.D. N.D. 0 (1) 20
Nitrite Nitrogen 86* 90-110 N.D. N.D. 0 (1) 20
Sulfate 96 90-110 31.8 31.7 0 20
Page 24 of 28

Page 5 of 5

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1486078
Reported: 07/16/14 at 01:58 PM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Sample Matrix Quality Control
Unspiked (UNSPK) = the sample used in conjunction with the matrix spike
Background (BKG) = the sample used in conjunction with the duplicate

MS MSD MS/MSD RPD BKG DUP DUP Dup RPD
Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___

Batch number: 14183987601B Sample number(s): 7519015-7519016 UNSPK: 7519015 BKG: 7519015
Bromide 89* 90-110 N.D. N.D. 0 (1) 20
Chloride 85* 90-110 18.8 18.6 1 20
Nitrate Nitrogen 91 90-110 N.D. N.D. 0 (1) 20
Nitrite Nitrogen 88* 90-110 N.D. N.D. 0 (1) 20
Sulfate 97 90-110 53.7 53.7 0 20

Batch number: 14183021202A Sample number(s): 7519011-7519012 UNSPK: P518932 BKG: P518932
Total Dissolved Solids 102 66-131 1,620 1,880 15* 5

Batch number: 14184021201A Sample number(s): 7519015-7519016 UNSPK: P519692 BKG: P519692
Total Dissolved Solids 97 66-131 792 786 1 5

Batch number: 14184039401B Sample number(s): 7519007,7519009 BKG: 7519007
pH 8.23 8.20 0 3

Batch number: 14188002102A Sample number(s): 7519012,7519015-7519016 UNSPK: P520819 BKG: P520819
Total Alkalinity 89 85 17-146 2 5 296 296 0 5

Batch number: 14188002103A Sample number(s): 7519011 UNSPK: P520777 BKG: P520777
Total Alkalinity 47 48 17-146 1 5 235 235 0 5

Batch number: 14189820001B Sample number(s): 7519007,7519009 BKG: 7519009
Moisture 27.8 25.9 7* 5

Page 25 of 28
Page 26 of 28
Page 27 of 28
Explanation of Symbols and Abbreviations

3768 0713
The following defines common symbols and abbreviations used in reporting technical data:
RL Reporting Limit BMQL Below Minimum Quantitation Level
N.D. none detected MPN Most Probable Number
TNTC Too Numerous To Count CP Units cobalt-chloroplatinate units
IU International Units NTU nephelometric turbidity units
umhos/cm micromhos/cm ng nanogram(s)
C degrees Celsius F degrees Fahrenheit
meq milliequivalents lb. pound(s)
g gram(s) kg kilogram(s)
µg microgram(s) mg milligram(s)
mL milliliter(s) L liter(s)
m3 cubic meter(s) µL microliter(s)
pg/L picogram/liter
< less than - The number following the sign is the limit of quantitation, the smallest amount of analyte which can be
reliably determined using this specific test.
> greater than
ppm parts per million - One ppm is equivalent to one milligram per kilogram (mg/kg), or one gram per million grams. For
aqueous liquids, ppm is usually taken to be equivalent to milligrams per liter (mg/l), because one liter of water has a
weight very close to a kilogram. For gases or vapors, one ppm is equivalent to one microliter per liter of gas.
ppb parts per billion
Dry weight Results printed under this heading have been adjusted for moisture content. This increases the analyte weight
basis concentration to approximate the value present in a similar sample without moisture. All other results are reported
on an as-received basis.
Data Qualifiers:
C – result confirmed by reanalysis.
J - estimated value – The result is ≥ the Method Detection Limit (MDL) and < the Limit of Quantitation (LOQ).
U.S. EPA CLP Data Qualifiers:
Organic Qualifiers Inorganic Qualifiers
A TIC is a possible aldol-condensation product B Value is <CRDL, but ≥IDL
B Analyte was also detected in the blank E Estimated due to interference
C Pesticide result confirmed by GC/MS M Duplicate injection precision not met
D Compound quantitated on a diluted sample N Spike sample not within control limits
E Concentration exceeds the calibration range of S Method of standard additions (MSA) used
the instrument for calculation
N Presumptive evidence of a compound (TICs only) U Compound was not detected
P Concentration difference between primary and W Post digestion spike out of control limits
confirmation columns >25% * Duplicate analysis not within control limits
U Compound was not detected + Correlation coefficient for MSA <0.995
X,Y,Z Defined in case narrative
Analytical test results meet all requirements of NELAC unless otherwise noted under the individual analysis.
Measurement uncertainty values, as applicable, are available upon request.
Tests results relate only to the sample tested. Clients should be aware that a critical step in a chemical or microbiological
analysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of material involved, the
test results will be meaningless. If you have questions regarding the proper techniques of collecting samples, please contact
us. We cannot be held responsible for sample integrity, however, unless sampling has been performed by a member of our
staff. This report shall not be reproduced except in full, without the written approval of the laboratory.
Times are local to the area of activity. Parameters listed in the 40 CFR part 136 Table II as “analyze immediately” are not
performed within 15 minutes.

WARRANTY AND LIMITS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results for the sample as submitted. THE
FOREGOING EXPRESS WARRANTY IS EXCLUSIVE AND IS GIVEN IN LIEU OF ALL OTHER WARRANTIES, EXPRESSED OR IMPLIED. WE DISCLAIM
ANY OTHER WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING A WARRANTY OF FITNESS FOR PARTICULAR PURPOSE AND WARRANTY OF
MERCHANTABILITY. IN NO EVENT SHALL EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL, LLC BE LIABLE FOR INDIRECT, SPECIAL,
CONSEQUENTIAL, OR INCIDENTAL DAMAGES INCLUDING, BUT NOT LIMITED TO, DAMAGES FOR LOSS OF PROFIT OR GOODWILL REGARDLESS
OF (A) THE NEGLIGENCE (EITHER SOLE OR CONCURRENT) OF EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL AND (B) WHETHER
EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL HAS BEEN INFORMED OF THE POSSIBILITY OF SUCH DAMAGES. We accept no legal
responsibility for the purposes for which the client uses the test results. No purchase order or other order for work shall be accepted by Eurofins Lancaster
Laboratories Environmental which includes any conditions that vary from the Standard Terms and Conditions, and Eurofins Lancaster Laboratories
Environmental hereby objects to any conflicting terms contained in any acceptance or order submitted by client.
Page 28 of 28

ANALYTICAL RESULTS

Prepared by:

Eurofins Lancaster Laboratories Environmental
2425 New Holland Pike
Lancaster, PA 17601
Prepared for:

GeoSyntec Consultants
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607

July 14, 2014

Project: Duke Sutton, NC

Submittal Date: 07/03/2014
Group Number: 1486459
SDG: DUK37
PO Number: GC5592
State of Sample Origin: NC

Client Sample Description Lancaster Labs (LL) #
GW-MW13D-20140702 Grab Groundwater Sample 7520777
GW-MW13D-20140702 MS Grab Groundwater Sample 7520778
GW-MW13D-20140702 MSD Grab Groundwater Sample 7520779
GW-MW13D-20140702 DUP Grab Groundwater Sample 7520780
GW-MW13-20140702 Grab Groundwater Sample 7520781
GW-MW15-20140702 Grab Groundwater Sample 7520782
GW-MW159-20140702 Grab Groundwater Sample 7520783
GW-MW15D-20140702 Grab Groundwater Sample 7520784
GW-MW15-20140702-MBQC Grab Groundwater Sample 7520785

The specific methodologies used in obtaining the enclosed analytical results are indicated on the
Laboratory Sample Analysis Record.

ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Lauren Wellborn
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Beau Hodge
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Rachel Donahue
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Herwig Goldemund

Page 1 of 24

Respectfully Submitted,

[phone]

Page 2 of 24

LL Sample # WW 7520777
LL Group # 1486459
Account # 10634
Sample Description: GW-MW13D-20140702 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 12:10 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS13D SDG#: DUK37-01BKG
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.0199 J 17440-38-2 07035 0.0072 0.0400 Arsenic
0.144 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
2.35 57440-42-8 08014 0.0230 0.500 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
89.4 17440-70-2 01750 0.0334 0.400 Calcium
0.0017 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
4.72 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
25.1 17439-95-4 01757 0.0167 0.200 Magnesium
0.459 17439-96-5 07058 0.00083 0.0100 Manganese
0.319 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
14.7 17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
52.1 57440-23-5 01767 0.835 10.0 Sodium
3.20 57440-24-6 08068 0.0017 0.0500 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-62-2 07071 0.0019 0.0100 Vanadium
0.0041 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
mg/l mg/lmg/lWet Chemistry EPA 300.0
N.D.524959-67-901505 2.0 2.5 Bromide
59.6 2016887-00-600224 4.0 8.0 Chloride
N.D.514797-55-800368 0.25 0.50 Nitrate Nitrogen
N.D.514797-65-001506 0.40 0.50 Nitrite Nitrogen
96.9 2014808-79-800228 6.0 20.0 Sulfate
mg/l as CaCO3mg/l as CaCO3mg/l as CaCO3EPA 310.1
235 1n.a. 12150 0.70 2.0 Total Alkalinity
mg/l mg/lmg/lSM 2540 C-1997
516 1n.a. 00212 19.4 60.0 Total Dissolved Solids
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
*=This limit was used in the evaluation of the final result
Page 3 of 24

LL Sample # WW 7520777
LL Group # 1486459
Account # 10634
Sample Description: GW-MW13D-20140702 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 12:10 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS13D SDG#: DUK37-01BKG
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 21:43 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 21:43 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 03:16 1418806350011SW-846 6010C Barium 07046
1Tara L Snyder07/09/2014 03:16 1418806350011SW-846 6010C Beryllium 07047
5Tara L Snyder07/09/2014 03:39 1418806350011SW-846 6010C Boron 08014
1John P Hook07/08/2014 21:43 1418806350011SW-846 6010C Cadmium 07049
1Tara L Snyder07/09/2014 03:16 1418806350011SW-846 6010C Calcium 01750
1John P Hook07/08/2014 21:43 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 21:43 1418806350011SW-846 6010C Copper 07053
1John P Hook07/08/2014 21:43 1418806350011SW-846 6010C Iron 01754
1Joanne M Gates07/09/2014 12:59 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 21:43 1418806350011SW-846 6010C Magnesium 01757
1John P Hook07/08/2014 21:43 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 21:43 1418806350011SW-846 6010C Molybdenum 07060
1John P Hook07/08/2014 21:43 1418806350011SW-846 6010C Nickel 07061
1Tara L Snyder07/09/2014 03:16 1418806350011SW-846 6010C Potassium 01762
1John P Hook07/08/2014 21:43 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 21:43 1418806350011SW-846 6010C Silver 07066
5Tara L Snyder07/09/2014 03:39 1418806350011SW-846 6010C Sodium 01767
5Tara L Snyder07/09/2014 03:39 1418806350011SW-846 6010C Strontium 08068
1Tara L Snyder07/09/2014 03:16 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 21:43 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 21:43 1418806350011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 14:44 1418957130062SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/09/2014 09:23 1418957130061SW-846 7470A WW SW846 Hg Digest 05713
5Clinton M Wilson07/03/2014 19:51 14184987601B1EPA 300.0 Bromide 01505
20Sandra J Miller07/07/2014 07:21 14184987601B1EPA 300.0 Chloride 00224
5Clinton M Wilson07/03/2014 19:51 14184987601B1EPA 300.0 Nitrate Nitrogen 00368
5Clinton M Wilson07/03/2014 19:51 14184987601B1EPA 300.0 Nitrite Nitrogen 01506
20Clinton M Wilson07/05/2014 19:05 14184987601B1EPA 300.0 Sulfate 00228
1Michele L Graham07/07/2014 17:19 14188002103A1EPA 310.1 Total Alkalinity 12150
1Sarah E Thompson07/08/2014 10:13 14189021201A1SM 2540 C-1997 Total Dissolved Solids 00212
*=This limit was used in the evaluation of the final result
Page 4 of 24

LL Sample # WW 7520778
LL Group # 1486459
Account # 10634
Sample Description: GW-MW13D-20140702 MS Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 12:15 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS13D SDG#: DUK37-01MS
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
0.540 17440-36-0 07044 0.0051 0.0400 Antimony
0.177 17440-38-2 07035 0.0072 0.0400 Arsenic
2.18 17440-39-3 07046 0.00033 0.0100 Barium
0.0512 17440-41-7 07047 0.00067 0.0100 Beryllium
3.84 57440-42-8 08014 0.0230 0.500 Boron
0.0494 17440-43-9 07049 0.00033 0.0100 Cadmium
89.7 17440-70-2 01750 0.0334 0.400 Calcium
0.197 17440-47-3 07051 0.0013 0.0300 Chromium
0.266 17440-50-8 07053 0.0028 0.0200 Copper
5.45 17439-89-6 01754 0.0334 0.400 Iron
0.151 17439-92-1 07055 0.0047 0.0300 Lead
25.5 17439-95-4 01757 0.0167 0.200 Magnesium
0.950 17439-96-5 07058 0.00083 0.0100 Manganese
2.35 17439-98-7 07060 0.0017 0.0200 Molybdenum
0.519 17440-02-0 07061 0.0016 0.0200 Nickel
24.7 17440-09-7 01762 0.133 1.00 Potassium
0.150 17782-49-2 07036 0.0048 0.0400 Selenium
0.0467 17440-22-4 07066 0.0018 0.0100 Silver
54.2 57440-23-5 01767 0.835 10.0 Sodium
3.70 57440-24-6 08068 0.0017 0.0500 Strontium
0.142 17440-28-0 07022 0.0051 0.0600 Thallium
0.485 17440-62-2 07071 0.0019 0.0100 Vanadium
0.502 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
0.0010 17439-97-6 00259 0.000060 0.00020 Mercury
mg/l mg/lmg/lWet Chemistry EPA 300.0
45.3 1024959-67-901505 4.0 5.0 Bromide
127 4016887-00-600224 8.0 16.0 Chloride
9.3 1014797-55-800368 0.50 1.0 Nitrate Nitrogen
8.2 1014797-65-001506 0.80 1.0 Nitrite Nitrogen
288 4014808-79-800228 12.0 40.0 Sulfate
mg/l as CaCO3mg/l as CaCO3mg/l as CaCO3EPA 310.1
323 1n.a. 12150 0.70 2.0 Total Alkalinity
mg/l mg/lmg/lSM 2540 C-1997
895 1n.a. 00212 19.4 60.0 Total Dissolved Solids
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
*=This limit was used in the evaluation of the final result
Page 5 of 24

LL Sample # WW 7520778
LL Group # 1486459
Account # 10634
Sample Description: GW-MW13D-20140702 MS Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 12:15 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS13D SDG#: DUK37-01MS
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 21:54 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 21:54 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 03:28 1418806350011SW-846 6010C Barium 07046
1Tara L Snyder07/09/2014 03:28 1418806350011SW-846 6010C Beryllium 07047
5Tara L Snyder07/09/2014 03:58 1418806350012SW-846 6010C Boron 08014
1John P Hook07/08/2014 21:54 1418806350011SW-846 6010C Cadmium 07049
1Tara L Snyder07/09/2014 03:28 1418806350011SW-846 6010C Calcium 01750
1John P Hook07/08/2014 21:54 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 21:54 1418806350011SW-846 6010C Copper 07053
1John P Hook07/08/2014 21:54 1418806350011SW-846 6010C Iron 01754
1Joanne M Gates07/09/2014 13:59 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 21:54 1418806350011SW-846 6010C Magnesium 01757
1John P Hook07/08/2014 21:54 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 21:54 1418806350011SW-846 6010C Molybdenum 07060
1John P Hook07/08/2014 21:54 1418806350011SW-846 6010C Nickel 07061
1Tara L Snyder07/09/2014 03:28 1418806350011SW-846 6010C Potassium 01762
1John P Hook07/08/2014 21:54 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 21:54 1418806350011SW-846 6010C Silver 07066
5Tara L Snyder07/09/2014 03:58 1418806350012SW-846 6010C Sodium 01767
5Tara L Snyder07/09/2014 03:58 1418806350012SW-846 6010C Strontium 08068
1Tara L Snyder07/09/2014 03:28 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 21:54 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 21:54 1418806350011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 14:46 1418957130062SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/09/2014 09:23 1418957130061SW-846 7470A WW SW846 Hg Digest 05713
10Clinton M Wilson07/03/2014 20:23 14184987601B1EPA 300.0 Bromide 01505
40Sandra J Miller07/07/2014 07:53 14184987601B1EPA 300.0 Chloride 00224
10Clinton M Wilson07/03/2014 20:23 14184987601B1EPA 300.0 Nitrate Nitrogen 00368
10Clinton M Wilson07/03/2014 20:23 14184987601B1EPA 300.0 Nitrite Nitrogen 01506
40Clinton M Wilson07/05/2014 19:37 14184987601B2EPA 300.0 Sulfate 00228
1Michele L Graham07/07/2014 17:26 14188002103A1EPA 310.1 Total Alkalinity 12150
1Sarah E Thompson07/08/2014 10:13 14189021201A1SM 2540 C-1997 Total Dissolved Solids 00212
*=This limit was used in the evaluation of the final result
Page 6 of 24

LL Sample # WW 7520779
LL Group # 1486459
Account # 10634
Sample Description: GW-MW13D-20140702 MSD Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 12:20 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS13D SDG#: DUK37-01MSD
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
0.532 17440-36-0 07044 0.0051 0.0400 Antimony
0.181 17440-38-2 07035 0.0072 0.0400 Arsenic
2.17 17440-39-3 07046 0.00033 0.0100 Barium
0.0507 17440-41-7 07047 0.00067 0.0100 Beryllium
4.09 57440-42-8 08014 0.0230 0.500 Boron
0.0494 17440-43-9 07049 0.00033 0.0100 Cadmium
89.4 17440-70-2 01750 0.0334 0.400 Calcium
0.192 17440-47-3 07051 0.0013 0.0300 Chromium
0.265 17440-50-8 07053 0.0028 0.0200 Copper
5.85 17439-89-6 01754 0.0334 0.400 Iron
0.150 17439-92-1 07055 0.0047 0.0300 Lead
25.3 17439-95-4 01757 0.0167 0.200 Magnesium
0.930 17439-96-5 07058 0.00083 0.0100 Manganese
2.35 17439-98-7 07060 0.0017 0.0200 Molybdenum
0.513 17440-02-0 07061 0.0016 0.0200 Nickel
24.5 17440-09-7 01762 0.133 1.00 Potassium
0.151 17782-49-2 07036 0.0048 0.0400 Selenium
0.0455 17440-22-4 07066 0.0018 0.0100 Silver
57.2 57440-23-5 01767 0.835 10.0 Sodium
3.92 57440-24-6 08068 0.0017 0.0500 Strontium
0.142 17440-28-0 07022 0.0051 0.0600 Thallium
0.486 17440-62-2 07071 0.0019 0.0100 Vanadium
0.501 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
0.0010 17439-97-6 00259 0.000060 0.00020 Mercury
mg/l as CaCO3mg/l as CaCO3mg/l as CaCO3Wet Chemistry EPA 310.1
326 1n.a. 12150 0.70 2.0 Total Alkalinity
mg/l mg/lmg/lSM 2540 C-1997
890 1n.a. 00212 19.4 60.0 Total Dissolved Solids
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 21:58 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 21:58 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 03:31 1418806350011SW-846 6010C Barium 07046
1Tara L Snyder07/09/2014 03:31 1418806350011SW-846 6010C Beryllium 07047
*=This limit was used in the evaluation of the final result
Page 7 of 24

LL Sample # WW 7520779
LL Group # 1486459
Account # 10634
Sample Description: GW-MW13D-20140702 MSD Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 12:20 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS13D SDG#: DUK37-01MSD
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
5Tara L Snyder07/09/2014 04:01 1418806350012SW-846 6010C Boron 08014
1John P Hook07/08/2014 21:58 1418806350011SW-846 6010C Cadmium 07049
1Tara L Snyder07/09/2014 03:31 1418806350011SW-846 6010C Calcium 01750
1John P Hook07/08/2014 21:58 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 21:58 1418806350011SW-846 6010C Copper 07053
1John P Hook07/08/2014 21:58 1418806350011SW-846 6010C Iron 01754
1Joanne M Gates07/09/2014 14:03 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 21:58 1418806350011SW-846 6010C Magnesium 01757
1John P Hook07/08/2014 21:58 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 21:58 1418806350011SW-846 6010C Molybdenum 07060
1John P Hook07/08/2014 21:58 1418806350011SW-846 6010C Nickel 07061
1Tara L Snyder07/09/2014 03:31 1418806350011SW-846 6010C Potassium 01762
1John P Hook07/08/2014 21:58 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 21:58 1418806350011SW-846 6010C Silver 07066
5Tara L Snyder07/09/2014 04:01 1418806350011SW-846 6010C Sodium 01767
5Tara L Snyder07/09/2014 04:01 1418806350012SW-846 6010C Strontium 08068
1Tara L Snyder07/09/2014 03:31 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 21:58 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 21:58 1418806350011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 14:49 1418957130062SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/09/2014 09:23 1418957130061SW-846 7470A WW SW846 Hg Digest 05713
1Michele L Graham07/07/2014 17:32 14188002103A1EPA 310.1 Total Alkalinity 12150
1Sarah E Thompson07/08/2014 10:13 14189021201A1SM 2540 C-1997 Total Dissolved Solids 00212
*=This limit was used in the evaluation of the final result
Page 8 of 24

LL Sample # WW 7520780
LL Group # 1486459
Account # 10634
Sample Description: GW-MW13D-20140702 DUP Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 12:10 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS13D SDG#: DUK37-01DUP
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.0133 J 17440-38-2 07035 0.0072 0.0400 Arsenic
0.136 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
2.10 57440-42-8 08014 0.0230 0.500 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
84.3 17440-70-2 01750 0.0334 0.400 Calcium
0.0019 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
4.44 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
23.6 17439-95-4 01757 0.0167 0.200 Magnesium
0.430 17439-96-5 07058 0.00083 0.0100 Manganese
0.293 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
13.8 17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
47.3 57440-23-5 01767 0.835 10.0 Sodium
2.88 57440-24-6 08068 0.0017 0.0500 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-62-2 07071 0.0019 0.0100 Vanadium
0.0038 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
mg/l mg/lmg/lWet Chemistry EPA 300.0
N.D.524959-67-901505 2.0 2.5 Bromide
58.9 2016887-00-600224 4.0 8.0 Chloride
N.D.514797-55-800368 0.25 0.50 Nitrate Nitrogen
N.D.514797-65-001506 0.40 0.50 Nitrite Nitrogen
95.4 2014808-79-800228 6.0 20.0 Sulfate
mg/l as CaCO3mg/l as CaCO3mg/l as CaCO3EPA 310.1
235 1n.a. 12150 0.70 2.0 Total Alkalinity
mg/l mg/lmg/lSM 2540 C-1997
503 1n.a. 00212 19.4 60.0 Total Dissolved Solids
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
*=This limit was used in the evaluation of the final result
Page 9 of 24

LL Sample # WW 7520780
LL Group # 1486459
Account # 10634
Sample Description: GW-MW13D-20140702 DUP Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 12:10 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS13D SDG#: DUK37-01DUP
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 21:50 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 21:50 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 03:24 1418806350011SW-846 6010C Barium 07046
1Tara L Snyder07/09/2014 03:24 1418806350011SW-846 6010C Beryllium 07047
5Tara L Snyder07/09/2014 03:54 1418806350011SW-846 6010C Boron 08014
1John P Hook07/08/2014 21:50 1418806350011SW-846 6010C Cadmium 07049
1Tara L Snyder07/09/2014 03:24 1418806350011SW-846 6010C Calcium 01750
1John P Hook07/08/2014 21:50 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 21:50 1418806350011SW-846 6010C Copper 07053
1John P Hook07/08/2014 21:50 1418806350011SW-846 6010C Iron 01754
1Tara L Snyder07/09/2014 03:24 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 21:50 1418806350011SW-846 6010C Magnesium 01757
1John P Hook07/08/2014 21:50 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 21:50 1418806350011SW-846 6010C Molybdenum 07060
1John P Hook07/08/2014 21:50 1418806350011SW-846 6010C Nickel 07061
1Tara L Snyder07/09/2014 03:24 1418806350011SW-846 6010C Potassium 01762
1John P Hook07/08/2014 21:50 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 21:50 1418806350011SW-846 6010C Silver 07066
5Tara L Snyder07/09/2014 03:54 1418806350011SW-846 6010C Sodium 01767
5Tara L Snyder07/09/2014 03:54 1418806350011SW-846 6010C Strontium 08068
1Tara L Snyder07/09/2014 03:24 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 21:50 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 21:50 1418806350011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 14:51 1418957130062SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/09/2014 09:23 1418957130061SW-846 7470A WW SW846 Hg Digest 05713
5Clinton M Wilson07/03/2014 20:07 14184987601B1EPA 300.0 Bromide 01505
20Sandra J Miller07/07/2014 07:37 14184987601B1EPA 300.0 Chloride 00224
5Clinton M Wilson07/03/2014 20:07 14184987601B1EPA 300.0 Nitrate Nitrogen 00368
5Clinton M Wilson07/03/2014 20:07 14184987601B1EPA 300.0 Nitrite Nitrogen 01506
20Clinton M Wilson07/05/2014 19:21 14184987601B1EPA 300.0 Sulfate 00228
1Michele L Graham07/07/2014 17:39 14188002103A1EPA 310.1 Total Alkalinity 12150
1Sarah E Thompson07/08/2014 10:13 14189021201A1SM 2540 C-1997 Total Dissolved Solids 00212
*=This limit was used in the evaluation of the final result
Page 10 of 24

LL Sample # WW 7520781
LL Group # 1486459
Account # 10634
Sample Description: GW-MW13-20140702 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 12:11 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS-13 SDG#: DUK37-02
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.218 17440-38-2 07035 0.0072 0.0400 Arsenic
0.367 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.935 27440-42-8 08014 0.0092 0.200 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
45.3 17440-70-2 01750 0.0334 0.400 Calcium
0.0013 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
5.50 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
15.7 17439-95-4 01757 0.0167 0.200 Magnesium
0.145 17439-96-5 07058 0.00083 0.0100 Manganese
0.140 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
13.0 17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
44.8 27440-23-5 01767 0.334 4.00 Sodium
1.40 27440-24-6 08068 0.00066 0.0200 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-62-2 07071 0.0019 0.0100 Vanadium
0.0022 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
mg/l mg/lmg/lWet Chemistry EPA 300.0
N.D.524959-67-901505 2.0 2.5 Bromide
47.2 2016887-00-600224 4.0 8.0 Chloride
N.D.514797-55-800368 0.25 0.50 Nitrate Nitrogen
N.D.514797-65-001506 0.40 0.50 Nitrite Nitrogen
128 2014808-79-800228 6.0 20.0 Sulfate
mg/l as CaCO3mg/l as CaCO3mg/l as CaCO3EPA 310.1
86.9 1n.a. 12150 0.70 2.0 Total Alkalinity
mg/l mg/lmg/lSM 2540 C-1997
370 1n.a. 00212 9.7 30.0 Total Dissolved Solids
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
*=This limit was used in the evaluation of the final result
Page 11 of 24

LL Sample # WW 7520781
LL Group # 1486459
Account # 10634
Sample Description: GW-MW13-20140702 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 12:11 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS-13 SDG#: DUK37-02
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 22:38 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 22:38 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 04:53 1418806350011SW-846 6010C Barium 07046
1Tara L Snyder07/09/2014 04:53 1418806350011SW-846 6010C Beryllium 07047
2Tara L Snyder07/09/2014 04:57 1418806350011SW-846 6010C Boron 08014
1John P Hook07/08/2014 22:38 1418806350011SW-846 6010C Cadmium 07049
1Tara L Snyder07/09/2014 04:53 1418806350011SW-846 6010C Calcium 01750
1John P Hook07/08/2014 22:38 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 22:38 1418806350011SW-846 6010C Copper 07053
1John P Hook07/08/2014 22:38 1418806350011SW-846 6010C Iron 01754
1Joanne M Gates07/09/2014 13:39 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 22:38 1418806350011SW-846 6010C Magnesium 01757
1John P Hook07/08/2014 22:38 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 22:38 1418806350011SW-846 6010C Molybdenum 07060
1John P Hook07/08/2014 22:38 1418806350011SW-846 6010C Nickel 07061
1Tara L Snyder07/09/2014 04:53 1418806350011SW-846 6010C Potassium 01762
1John P Hook07/08/2014 22:38 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 22:38 1418806350011SW-846 6010C Silver 07066
2Tara L Snyder07/09/2014 04:57 1418806350011SW-846 6010C Sodium 01767
2Tara L Snyder07/09/2014 04:57 1418806350011SW-846 6010C Strontium 08068
1Tara L Snyder07/09/2014 04:53 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 22:38 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 22:38 1418806350011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 14:53 1418957130061SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/09/2014 09:23 1418957130061SW-846 7470A WW SW846 Hg Digest 05713
5Clinton M Wilson07/03/2014 21:12 14184987601B1EPA 300.0 Bromide 01505
20Sandra J Miller07/07/2014 08:09 14184987601B1EPA 300.0 Chloride 00224
5Clinton M Wilson07/03/2014 21:12 14184987601B1EPA 300.0 Nitrate Nitrogen 00368
5Clinton M Wilson07/03/2014 21:12 14184987601B1EPA 300.0 Nitrite Nitrogen 01506
20Clinton M Wilson07/05/2014 19:54 14184987601B1EPA 300.0 Sulfate 00228
1Michele L Graham07/07/2014 17:45 14188002103A1EPA 310.1 Total Alkalinity 12150
1Sarah E Thompson07/08/2014 10:13 14189021201A1SM 2540 C-1997 Total Dissolved Solids 00212
*=This limit was used in the evaluation of the final result
Page 12 of 24

LL Sample # WW 7520782
LL Group # 1486459
Account # 10634
Sample Description: GW-MW15-20140702 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:35 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS-15 SDG#: DUK37-03
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.0383 J 17440-38-2 07035 0.0072 0.0400 Arsenic
0.0365 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0592 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
114 17440-70-2 01750 0.0334 0.400 Calcium
0.0014 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
5.72 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
5.20 17439-95-4 01757 0.0167 0.200 Magnesium
0.109 17439-96-5 07058 0.00083 0.0100 Manganese
0.0076 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
3.50 17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
18.3 17440-23-5 01767 0.167 2.00 Sodium
0.553 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-62-2 07071 0.0019 0.0100 Vanadium
0.0022 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
mg/l mg/lmg/lWet Chemistry EPA 300.0
N.D.524959-67-901505 2.0 2.5 Bromide
45.1 1016887-00-600224 2.0 4.0 Chloride
N.D.514797-55-800368 0.25 0.50 Nitrate Nitrogen
N.D.514797-65-001506 0.40 0.50 Nitrite Nitrogen
42.0 514808-79-800228 1.5 5.0 Sulfate
mg/l as CaCO3mg/l as CaCO3mg/l as CaCO3EPA 310.1
211 1n.a. 12150 0.70 2.0 Total Alkalinity
mg/l mg/lmg/lSM 2540 C-1997
398 1n.a. 00212 9.7 30.0 Total Dissolved Solids
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
*=This limit was used in the evaluation of the final result
Page 13 of 24

LL Sample # WW 7520782
LL Group # 1486459
Account # 10634
Sample Description: GW-MW15-20140702 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:35 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS-15 SDG#: DUK37-03
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 05:01 1418806350011SW-846 6010C Barium 07046
1Tara L Snyder07/09/2014 05:01 1418806350011SW-846 6010C Beryllium 07047
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Boron 08014
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Cadmium 07049
1Tara L Snyder07/09/2014 05:01 1418806350011SW-846 6010C Calcium 01750
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Copper 07053
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Iron 01754
1Joanne M Gates07/09/2014 13:51 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Magnesium 01757
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Molybdenum 07060
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Nickel 07061
1Tara L Snyder07/09/2014 05:01 1418806350011SW-846 6010C Potassium 01762
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Silver 07066
1Tara L Snyder07/09/2014 05:01 1418806350011SW-846 6010C Sodium 01767
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Strontium 08068
1Tara L Snyder07/09/2014 05:01 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 22:42 1418806350011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 14:59 1418957130061SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/09/2014 09:23 1418957130061SW-846 7470A WW SW846 Hg Digest 05713
5Clinton M Wilson07/03/2014 21:28 14184987601B1EPA 300.0 Bromide 01505
10Sandra J Miller07/07/2014 08:25 14184987601B1EPA 300.0 Chloride 00224
5Clinton M Wilson07/03/2014 21:28 14184987601B1EPA 300.0 Nitrate Nitrogen 00368
5Clinton M Wilson07/03/2014 21:28 14184987601B1EPA 300.0 Nitrite Nitrogen 01506
5Clinton M Wilson07/03/2014 21:28 14184987601B1EPA 300.0 Sulfate 00228
1Michele L Graham07/07/2014 16:45 14188002103A1EPA 310.1 Total Alkalinity 12150
1Sarah E Thompson07/08/2014 10:13 14189021201A1SM 2540 C-1997 Total Dissolved Solids 00212
*=This limit was used in the evaluation of the final result
Page 14 of 24

LL Sample # WW 7520783
LL Group # 1486459
Account # 10634
Sample Description: GW-MW159-20140702 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:30 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS159 SDG#: DUK37-04
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.0377 J 17440-38-2 07035 0.0072 0.0400 Arsenic
0.0343 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0583 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
110 17440-70-2 01750 0.0334 0.400 Calcium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
5.41 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
5.12 17439-95-4 01757 0.0167 0.200 Magnesium
0.105 17439-96-5 07058 0.00083 0.0100 Manganese
0.0069 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
3.38 17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
17.5 17440-23-5 01767 0.167 2.00 Sodium
0.548 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-62-2 07071 0.0019 0.0100 Vanadium
0.0021 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
mg/l mg/lmg/lWet Chemistry EPA 300.0
N.D.524959-67-901505 2.0 2.5 Bromide
43.6 1016887-00-600224 2.0 4.0 Chloride
N.D.514797-55-800368 0.25 0.50 Nitrate Nitrogen
N.D.514797-65-001506 0.40 0.50 Nitrite Nitrogen
41.9 514808-79-800228 1.5 5.0 Sulfate
mg/l as CaCO3mg/l as CaCO3mg/l as CaCO3EPA 310.1
221 1n.a. 12150 0.70 2.0 Total Alkalinity
mg/l mg/lmg/lSM 2540 C-1997
410 1n.a. 00212 9.7 30.0 Total Dissolved Solids
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
*=This limit was used in the evaluation of the final result
Page 15 of 24

LL Sample # WW 7520783
LL Group # 1486459
Account # 10634
Sample Description: GW-MW159-20140702 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:30 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS159 SDG#: DUK37-04
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 05:08 1418806350011SW-846 6010C Barium 07046
1Tara L Snyder07/09/2014 05:08 1418806350011SW-846 6010C Beryllium 07047
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Boron 08014
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Cadmium 07049
1Tara L Snyder07/09/2014 05:08 1418806350011SW-846 6010C Calcium 01750
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Copper 07053
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Iron 01754
1Joanne M Gates07/09/2014 13:55 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Magnesium 01757
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Molybdenum 07060
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Nickel 07061
1Tara L Snyder07/09/2014 05:08 1418806350011SW-846 6010C Potassium 01762
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Silver 07066
1Tara L Snyder07/09/2014 05:08 1418806350011SW-846 6010C Sodium 01767
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Strontium 08068
1Tara L Snyder07/09/2014 05:08 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 22:46 1418806350011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 15:01 1418957130061SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/09/2014 09:23 1418957130061SW-846 7470A WW SW846 Hg Digest 05713
5Clinton M Wilson07/03/2014 21:44 14184987601B1EPA 300.0 Bromide 01505
10Sandra J Miller07/07/2014 08:42 14184987601B1EPA 300.0 Chloride 00224
5Clinton M Wilson07/03/2014 21:44 14184987601B1EPA 300.0 Nitrate Nitrogen 00368
5Clinton M Wilson07/03/2014 21:44 14184987601B1EPA 300.0 Nitrite Nitrogen 01506
5Clinton M Wilson07/03/2014 21:44 14184987601B1EPA 300.0 Sulfate 00228
1Michele L Graham07/07/2014 14:22 14188002102A1EPA 310.1 Total Alkalinity 12150
1Sarah E Thompson07/08/2014 10:13 14189021201A1SM 2540 C-1997 Total Dissolved Solids 00212
*=This limit was used in the evaluation of the final result
Page 16 of 24

LL Sample # WW 7520784
LL Group # 1486459
Account # 10634
Sample Description: GW-MW15D-20140702 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:43 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS15D SDG#: DUK37-05
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
N.D.17440-38-2 07035 0.0072 0.0400 Arsenic
0.0533 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.550 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
61.5 17440-70-2 01750 0.0334 0.400 Calcium
0.0019 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.724 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
8.18 17439-95-4 01757 0.0167 0.200 Magnesium
1.62 27439-96-5 07058 0.0017 0.0200 Manganese
N.D.17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
7.61 17440-09-7 01762 0.133 1.00 Potassium
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
66.5 27440-23-5 01767 0.334 4.00 Sodium
0.615 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-62-2 07071 0.0019 0.0100 Vanadium
0.0062 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
mg/l mg/lmg/lWet Chemistry EPA 300.0
N.D.524959-67-901505 2.0 2.5 Bromide
131 5016887-00-600224 10.0 20.0 Chloride
N.D.514797-55-800368 0.25 0.50 Nitrate Nitrogen
N.D.514797-65-001506 0.40 0.50 Nitrite Nitrogen
75.7 1014808-79-800228 3.0 10.0 Sulfate
mg/l as CaCO3mg/l as CaCO3mg/l as CaCO3EPA 310.1
70.1 1n.a. 12150 0.70 2.0 Total Alkalinity
mg/l mg/lmg/lSM 2540 C-1997
435 1n.a. 00212 9.7 30.0 Total Dissolved Solids
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
*=This limit was used in the evaluation of the final result
Page 17 of 24

LL Sample # WW 7520784
LL Group # 1486459
Account # 10634
Sample Description: GW-MW15D-20140702 Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:43 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS15D SDG#: DUK37-05
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 05:23 1418806350011SW-846 6010C Barium 07046
1Tara L Snyder07/09/2014 05:23 1418806350011SW-846 6010C Beryllium 07047
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Boron 08014
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Cadmium 07049
1Tara L Snyder07/09/2014 05:23 1418806350011SW-846 6010C Calcium 01750
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Copper 07053
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Iron 01754
1Tara L Snyder07/09/2014 05:23 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Magnesium 01757
2Tara L Snyder07/09/2014 05:27 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Molybdenum 07060
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Nickel 07061
1Tara L Snyder07/09/2014 05:23 1418806350011SW-846 6010C Potassium 01762
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Silver 07066
2Tara L Snyder07/09/2014 05:27 1418806350011SW-846 6010C Sodium 01767
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Strontium 08068
1Tara L Snyder07/09/2014 05:23 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 22:49 1418806350011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 15:03 1418957130061SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/09/2014 09:23 1418957130061SW-846 7470A WW SW846 Hg Digest 05713
5Clinton M Wilson07/03/2014 22:00 14184987601B1EPA 300.0 Bromide 01505
50Sandra J Miller07/07/2014 08:58 14184987601B1EPA 300.0 Chloride 00224
5Clinton M Wilson07/03/2014 22:00 14184987601B1EPA 300.0 Nitrate Nitrogen 00368
5Clinton M Wilson07/03/2014 22:00 14184987601B1EPA 300.0 Nitrite Nitrogen 01506
10Clinton M Wilson07/05/2014 20:42 14184987601B1EPA 300.0 Sulfate 00228
1Michele L Graham07/07/2014 21:07 14188002104A1EPA 310.1 Total Alkalinity 12150
1Sarah E Thompson07/08/2014 10:13 14189021201A1SM 2540 C-1997 Total Dissolved Solids 00212
*=This limit was used in the evaluation of the final result
Page 18 of 24

LL Sample # WW 7520785
LL Group # 1486459
Account # 10634
Sample Description: GW-MW15-20140702-MBQC Grab Groundwater Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 15:45 by MP
Submitted: 07/03/2014 09:15
GeoSyntec Consultants
Reported: 07/14/2014 11:33
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
DS15Q SDG#: DUK37-06*
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.0354 J 17440-38-2 07035 0.0072 0.0400 Arsenic
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
0.0015 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.105 17439-96-5 07058 0.00083 0.0100 Manganese
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17782-49-2 07036 0.0048 0.0400 Selenium
N.D.17440-22-4 07066 0.0018 0.0100 Silver
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
N.D.17440-62-2 07071 0.0019 0.0100 Vanadium
0.0022 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/08/2014 22:53 1418806350011SW-846 6010C Antimony 07044
1John P Hook07/08/2014 22:53 1418806350011SW-846 6010C Arsenic 07035
1Tara L Snyder07/09/2014 05:31 1418806350011SW-846 6010C Beryllium 07047
1John P Hook07/08/2014 22:53 1418806350011SW-846 6010C Cadmium 07049
1John P Hook07/08/2014 22:53 1418806350011SW-846 6010C Chromium 07051
1John P Hook07/08/2014 22:53 1418806350011SW-846 6010C Copper 07053
1Tara L Snyder07/09/2014 05:31 1418806350011SW-846 6010C Lead 07055
1John P Hook07/08/2014 22:53 1418806350011SW-846 6010C Manganese 07058
1John P Hook07/08/2014 22:53 1418806350011SW-846 6010C Nickel 07061
1John P Hook07/08/2014 22:53 1418806350011SW-846 6010C Selenium 07036
1John P Hook07/08/2014 22:53 1418806350011SW-846 6010C Silver 07066
1Tara L Snyder07/09/2014 05:31 1418806350011SW-846 6010C Thallium 07022
1John P Hook07/08/2014 22:53 1418806350011SW-846 6010C Vanadium 07071
1John P Hook07/08/2014 22:53 1418806350011SW-846 6010C Zinc 07072
1Parker D Lindstrom07/12/2014 15:05 1418957130061SW-846 7470A Mercury 00259
1Micaela L Dishong07/08/2014 11:13 1418806350011SW-846 3005A WW SW846(IV) ICP Dig (tot
rec)
10635
1James L Mertz07/09/2014 09:23 1418957130061SW-846 7470A WW SW846 Hg Digest 05713
*=This limit was used in the evaluation of the final result
Page 19 of 24

Page 1 of 3

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1486459
Reported: 07/14/14 at 11:33 AM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these
situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD was performed, unless otherwise
specified in the method.

All Inorganic Initial Calibration and Continuing Calibration Blanks met acceptable method criteria unless
otherwise noted on the Analysis Report.

Laboratory Compliance Quality Control

Blank Blank Blank Report LCS LCSD LCS/LCSD
Analysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max

Batch number: 141880635001 Sample number(s): 7520777-7520785
Antimony N.D. 0.0051 0.0400 mg/l 109 88-111
Arsenic N.D. 0.0072 0.0400 mg/l 111 90-113
Barium N.D. 0.00033 0.0100 mg/l 108 90-110
Beryllium N.D. 0.00067 0.0100 mg/l 106 90-111
Boron N.D. 0.0046 0.100 mg/l 100 90-110
Cadmium N.D. 0.00033 0.0100 mg/l 105 90-112
Calcium N.D. 0.0334 0.400 mg/l 109 90-112
Chromium N.D. 0.0013 0.0300 mg/l 102 90-110
Copper N.D. 0.0028 0.0200 mg/l 108 90-112
Iron N.D. 0.0334 0.400 mg/l 112 90-112
Lead N.D. 0.0047 0.0300 mg/l 114 88-116
Magnesium N.D. 0.0167 0.200 mg/l 107 89-110
Manganese 0.0013 J 0.00083 0.0100 mg/l 108 90-110
Molybdenum N.D. 0.0017 0.0200 mg/l 106 90-110
Nickel N.D. 0.0016 0.0200 mg/l 111 90-117
Potassium N.D. 0.133 1.00 mg/l 104 90-110
Selenium N.D. 0.0048 0.0400 mg/l 103 89-113
Silver N.D. 0.0018 0.0100 mg/l 94 80-120
Sodium N.D. 0.167 2.00 mg/l 106 87-114
Strontium N.D. 0.00033 0.0100 mg/l 108 90-110
Thallium N.D. 0.0051 0.0600 mg/l 101 90-118
Vanadium N.D. 0.0019 0.0100 mg/l 102 90-110
Zinc N.D. 0.0020 0.0400 mg/l 104 90-110

Batch number: 141895713006 Sample number(s): 7520777-7520785
Mercury N.D. 0.00006
0
0.00020 mg/l 103 80-120

Batch number: 14184987601B Sample number(s): 7520777-7520778,7520780-7520784
Bromide N.D. 0.40 0.50 mg/l 91 91 90-110 0 20
Chloride N.D. 0.20 0.40 mg/l 91 92 90-110 1 20
Nitrate Nitrogen N.D. 0.050 0.10 mg/l 92 92 90-110 0 20
Nitrite Nitrogen N.D. 0.080 0.10 mg/l 91 91 90-110 0 20
Sulfate N.D. 0.30 1.0 mg/l 98 98 90-110 0 20

Batch number: 14188002102A Sample number(s): 7520783
Total Alkalinity N.D. 0.70 2.0 mg/l as
CaCO3
97 90-110

Batch number: 14188002103A Sample number(s): 7520777-7520782
Total Alkalinity N.D. 0.70 2.0 mg/l as
CaCO3
96 90-110

Page 20 of 24

Page 2 of 3

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1486459
Reported: 07/14/14 at 11:33 AM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Blank Blank Blank Report LCS LCSD LCS/LCSD
Analysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max
Batch number: 14188002104A Sample number(s): 7520784
Total Alkalinity N.D. 0.70 2.0 mg/l as
CaCO3
96 90-110

Batch number: 14189021201A Sample number(s): 7520777-7520784
Total Dissolved Solids N.D. 9.7 30.0 mg/l 89 80-120

Sample Matrix Quality Control
Unspiked (UNSPK) = the sample used in conjunction with the matrix spike
Background (BKG) = the sample used in conjunction with the duplicate

MS MSD MS/MSD RPD BKG DUP DUP Dup RPD
Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___

Batch number: 141880635001 Sample number(s): 7520777-7520785 UNSPK: 7520777 BKG: 7520777
Antimony 108 106 76-122 2 20 N.D. N.D. 0 (1) 20
Arsenic 104 108 81-123 3 20 0.0199 J 0.0133 J 39* (1) 20
Barium 102 101 78-125 1 20 0.144 0.136 6 20
Beryllium 102 101 87-114 1 20 N.D. N.D. 0 (1) 20
Boron 74* 87 87-111 6 20 2.35 2.10 11 (1) 20
Cadmium 99 99 75-122 0 20 N.D. N.D. 0 (1) 20
Calcium 7 (2) -1 (2) 75-125 0 20 89.4 84.3 6 20
Chromium 98 95 76-120 2 20 0.0017 J 0.0019 J 11 (1) 20
Copper 106 106 86-122 0 20 N.D. N.D. 0 (1) 20
Iron 72 (2) 112 (2) 75-125 7 20 4.72 4.44 6 20
Lead 101 100 75-125 1 20 N.D. N.D. 0 (1) 20
Magnesium 20 (2) 10 (2) 81-118 1 20 25.1 23.6 6 20
Manganese 98 94 75-125 2 20 0.459 0.430 7 20
Molybdenum 102 102 89-117 0 20 0.319 0.293 9 20
Nickel 104 103 79-123 1 20 N.D. N.D. 0 (1) 20
Potassium 100 98 77-128 1 20 14.7 13.8 6 20
Selenium 100 101 75-125 1 20 N.D. N.D. 0 (1) 20
Silver 93 91 75-125 2 20 N.D. N.D. 0 (1) 20
Sodium 21 (2) 51 (2) 84-117 3 20 52.1 47.3 10 (1) 20
Strontium 49* 72* 88-117 6 20 3.20 2.88 11 20
Thallium 95 94 75-125 0 20 N.D. N.D. 0 (1) 20
Vanadium 97 97 90-117 0 20 N.D. N.D. 0 (1) 20
Zinc 100 99 85-117 0 20 0.0041 J 0.0038 J 8 (1) 20

Batch number: 141895713006 Sample number(s): 7520777-7520785 UNSPK: 7520777 BKG: 7520777
Mercury 102 102 80-120 0 20 N.D. N.D. 0 (1) 20

Batch number: 14184987601B Sample number(s): 7520777-7520778,7520780-7520784 UNSPK: 7520777 BKG: 7520777
Bromide 91 90-110 N.D. N.D. 0 (1) 20
Chloride 85* 90-110 59.6 58.9 1 20
Nitrate Nitrogen 93 90-110 N.D. N.D. 0 (1) 20
Nitrite Nitrogen 82* 90-110 N.D. N.D. 0 (1) 20
Sulfate 95 90-110 96.9 95.4 2 (1) 20

Batch number: 14188002102A Sample number(s): 7520783 UNSPK: P520819 BKG: P520819
Total Alkalinity 89 85 17-146 2 5 296 296 0 5

Batch number: 14188002103A Sample number(s): 7520777-7520782 UNSPK: 7520777 BKG: 7520777
Page 21 of 24

Page 3 of 3

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1486459
Reported: 07/14/14 at 11:33 AM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Sample Matrix Quality Control
Unspiked (UNSPK) = the sample used in conjunction with the matrix spike
Background (BKG) = the sample used in conjunction with the duplicate

MS MSD MS/MSD RPD BKG DUP DUP Dup RPD
Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___
Total Alkalinity 47 48 17-146 1 5 235 235 0 5

Batch number: 14188002104A Sample number(s): 7520784 UNSPK: P520624 BKG: P520624
Total Alkalinity 90 17-146 61.9 63.8 3 5

Batch number: 14189021201A Sample number(s): 7520777-7520784 UNSPK: 7520777 BKG: 7520777
Total Dissolved Solids 95 94 66-131 1 23 516 503 3 5

Page 22 of 24
Page 23 of 24
Explanation of Symbols and Abbreviations

3768 0713
The following defines common symbols and abbreviations used in reporting technical data:
RL Reporting Limit BMQL Below Minimum Quantitation Level
N.D. none detected MPN Most Probable Number
TNTC Too Numerous To Count CP Units cobalt-chloroplatinate units
IU International Units NTU nephelometric turbidity units
umhos/cm micromhos/cm ng nanogram(s)
C degrees Celsius F degrees Fahrenheit
meq milliequivalents lb. pound(s)
g gram(s) kg kilogram(s)
µg microgram(s) mg milligram(s)
mL milliliter(s) L liter(s)
m3 cubic meter(s) µL microliter(s)
pg/L picogram/liter
< less than - The number following the sign is the limit of quantitation, the smallest amount of analyte which can be
reliably determined using this specific test.
> greater than
ppm parts per million - One ppm is equivalent to one milligram per kilogram (mg/kg), or one gram per million grams. For
aqueous liquids, ppm is usually taken to be equivalent to milligrams per liter (mg/l), because one liter of water has a
weight very close to a kilogram. For gases or vapors, one ppm is equivalent to one microliter per liter of gas.
ppb parts per billion
Dry weight Results printed under this heading have been adjusted for moisture content. This increases the analyte weight
basis concentration to approximate the value present in a similar sample without moisture. All other results are reported
on an as-received basis.
Data Qualifiers:
C – result confirmed by reanalysis.
J - estimated value – The result is ≥ the Method Detection Limit (MDL) and < the Limit of Quantitation (LOQ).
U.S. EPA CLP Data Qualifiers:
Organic Qualifiers Inorganic Qualifiers
A TIC is a possible aldol-condensation product B Value is <CRDL, but ≥IDL
B Analyte was also detected in the blank E Estimated due to interference
C Pesticide result confirmed by GC/MS M Duplicate injection precision not met
D Compound quantitated on a diluted sample N Spike sample not within control limits
E Concentration exceeds the calibration range of S Method of standard additions (MSA) used
the instrument for calculation
N Presumptive evidence of a compound (TICs only) U Compound was not detected
P Concentration difference between primary and W Post digestion spike out of control limits
confirmation columns >25% * Duplicate analysis not within control limits
U Compound was not detected + Correlation coefficient for MSA <0.995
X,Y,Z Defined in case narrative
Analytical test results meet all requirements of NELAC unless otherwise noted under the individual analysis.
Measurement uncertainty values, as applicable, are available upon request.
Tests results relate only to the sample tested. Clients should be aware that a critical step in a chemical or microbiological
analysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of material involved, the
test results will be meaningless. If you have questions regarding the proper techniques of collecting samples, please contact
us. We cannot be held responsible for sample integrity, however, unless sampling has been performed by a member of our
staff. This report shall not be reproduced except in full, without the written approval of the laboratory.
Times are local to the area of activity. Parameters listed in the 40 CFR part 136 Table II as “analyze immediately” are not
performed within 15 minutes.

WARRANTY AND LIMITS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results for the sample as submitted. THE
FOREGOING EXPRESS WARRANTY IS EXCLUSIVE AND IS GIVEN IN LIEU OF ALL OTHER WARRANTIES, EXPRESSED OR IMPLIED. WE DISCLAIM
ANY OTHER WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING A WARRANTY OF FITNESS FOR PARTICULAR PURPOSE AND WARRANTY OF
MERCHANTABILITY. IN NO EVENT SHALL EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL, LLC BE LIABLE FOR INDIRECT, SPECIAL,
CONSEQUENTIAL, OR INCIDENTAL DAMAGES INCLUDING, BUT NOT LIMITED TO, DAMAGES FOR LOSS OF PROFIT OR GOODWILL REGARDLESS
OF (A) THE NEGLIGENCE (EITHER SOLE OR CONCURRENT) OF EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL AND (B) WHETHER
EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL HAS BEEN INFORMED OF THE POSSIBILITY OF SUCH DAMAGES. We accept no legal
responsibility for the purposes for which the client uses the test results. No purchase order or other order for work shall be accepted by Eurofins Lancaster
Laboratories Environmental which includes any conditions that vary from the Standard Terms and Conditions, and Eurofins Lancaster Laboratories
Environmental hereby objects to any conflicting terms contained in any acceptance or order submitted by client.
Page 24 of 24

ANALYTICAL RESULTS

Prepared by:

Eurofins Lancaster Laboratories Environmental
2425 New Holland Pike
Lancaster, PA 17601
Prepared for:

GeoSyntec Consultants
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607

July 15, 2014

Project: Duke Sutton, NC

Submittal Date: 07/08/2014
Group Number: 1487148
SDG: DUK38
PO Number: GC5592
State of Sample Origin: NC

Client Sample Description Lancaster Labs (LL) #
SS-GP12(28-32)-20140702 Solid Sample 7525095
SS-GP12(28-32)-20140702 Solid Sample 7525096
SS-GP13(64-68)-20140701 Solid Sample 7525097
SS-GP13(64-68)-20140701 Solid Sample 7525098
SS-GP13(68-72)-20140701 Solid Sample 7525099
SS-GP13(68-72)-20140701 Solid Sample 7525100
SS-GP14(60-62)-20140702 Solid Sample 7525101
SS-GP14(60-62)-20140702 Solid Sample 7525102
SS-GP14(68-72)-20140702 Solid Sample 7525103
SS-GP14(68-72)-20140702 Solid Sample 7525104
SS-GP15(60-64)-20140701 Solid Sample 7525105
SS-GP15(60-64)-20140701 Solid Sample 7525106
SS-GP15(68.7-70.7)-20140701 Solid Sample 7525107
SS-GP15(68.7-70.7)-20140701 Solid Sample 7525108

The specific methodologies used in obtaining the enclosed analytical results are indicated on the
Laboratory Sample Analysis Record.

ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Lauren Wellborn
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Beau Hodge
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Rachel Donahue
ELECTRONIC
COPY TO
GeoSyntec Consultants Attn: Herwig Goldemund

Page 1 of 35

Respectfully Submitted,

[phone]

Page 2 of 35

LL Sample # SW 7525095
LL Group # 1487148
Account # 10634
Sample Description: SS-GP12(28-32)-20140702 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 12:20 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
12-28 SDG#: DUK38-01
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
0.758 J 17440-36-0 06944 0.509 6.17 Antimony
67.6 17440-38-2 06935 0.988 6.17 Arsenic
467 57440-39-3 06946 0.255 7.72 Barium
5.99 17440-41-7 06947 0.103 1.54 Beryllium
41.2 17440-42-8 07914 1.30 15.4 Boron
0.230 J 17440-43-9 06949 0.0509 1.54 Cadmium
46.8 17440-47-3 06951 0.170 4.63 Chromium
76.8 17440-50-8 06953 0.509 3.09 Copper
13,200 17439-89-6 01654 5.15 61.7 Iron
30.8 17439-92-1 06955 0.772 4.63 Lead
64.1 17439-96-5 06958 0.128 1.54 Manganese
4.39 17439-98-7 06960 0.262 3.09 Molybdenum
35.9 17440-02-0 06961 0.232 3.09 Nickel
5.43 J 17782-49-2 06936 0.679 6.17 Selenium
N.D.17440-22-4 06966 0.293 1.54 Silver
322 57440-24-6 07968 0.255 7.72 Strontium
5.45 J 17440-28-0 06925 1.23 9.26 Thallium
51.4 17440-66-6 06972 0.401 6.17 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.0871 J 17439-97-6 00159 0.0155 0.310 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
7.62 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 22 C.
% %%Wet Chemistry SM 2540 G-1997
37.7 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Antimony 06944
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Arsenic 06935
5Eric L Eby07/14/2014 16:39 1419206370011SW-846 6010C Barium 06946
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 3 of 35

LL Sample # SW 7525095
LL Group # 1487148
Account # 10634
Sample Description: SS-GP12(28-32)-20140702 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 12:20 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
12-28 SDG#: DUK38-01
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Boron 07914
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Cadmium 06949
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Chromium 06951
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Copper 06953
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Iron 01654
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Lead 06955
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Manganese 06958
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Molybdenum 06960
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Nickel 06961
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Selenium 06936
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Silver 06966
5Eric L Eby07/14/2014 16:39 1419206370011SW-846 6010C Strontium 07968
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Thallium 06925
1Joanne M Gates07/14/2014 09:52 1419206370011SW-846 6010C Zinc 06972
1Damary Valentin07/14/2014 15:33 1419206380011SW-846 7471B Mercury 00159
1James L Mertz07/13/2014 08:55 1419206370011SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/13/2014 10:58 1419206380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/11/2014 21:30 14192039401A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/10/2014 18:44 14191820003A1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 4 of 35

LL Sample # TL 7525096
LL Group # 1487148
Account # 10634
Sample Description: SS-GP12(28-32)-20140702 Solid Sample
SPLP NON-VOLATILE EXTRACTION
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 12:20 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1228S SDG#: DUK38-02
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
0.0222 J 17440-36-0 07044 0.0051 0.0400 Antimony
0.0716 17440-38-2 07035 0.0072 0.0400 Arsenic
0.135 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0463 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
3.24 17440-70-2 01750 0.0334 0.400 Calcium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
0.0281 17440-50-8 07053 0.0028 0.0200 Copper
N.D.17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.529 17439-95-4 01757 0.0167 0.200 Magnesium
0.0080 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.141 17439-98-7 07060 0.0017 0.0200 Molybdenum
0.0046 J 17440-02-0 07061 0.0016 0.0200 Nickel
0.600 J 17440-09-7 01762 0.133 1.00 Potassium
0.0090 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.107440-22-4 07066 0.0180 0.100 Silver
The silver result was performed by the Method of Standard Addition.
Reporting limits were raised due to interference from the sample matrix.
2.20 17440-23-5 01767 0.167 2.00 Sodium
0.191 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0027 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Antimony 07044
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Arsenic 07035
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Barium 07046
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Beryllium 07047
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Boron 08014
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Cadmium 07049
*=This limit was used in the evaluation of the final result
Page 5 of 35

LL Sample # TL 7525096
LL Group # 1487148
Account # 10634
Sample Description: SS-GP12(28-32)-20140702 Solid Sample
SPLP NON-VOLATILE EXTRACTION
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 12:20 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1228S SDG#: DUK38-02
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Calcium 01750
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Chromium 07051
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Copper 07053
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Iron 01754
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Lead 07055
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Magnesium 01757
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Manganese 07058
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Molybdenum 07060
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Nickel 07061
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Potassium 01762
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Selenium 07036
10Joanne M Gates07/15/2014 08:37 1419106360012SW-846 6010C Silver 07066
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Sodium 01767
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Strontium 08068
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Thallium 07022
1John P Hook07/14/2014 19:37 1419106360011SW-846 6010C Zinc 07072
1Damary Valentin07/14/2014 11:46 1419157130011SW-846 7470A Mercury 00259
1Micaela L Dishong07/14/2014 10:10 1419106360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1Micaela L Dishong07/11/2014 09:00 1419157130011SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/09/2014 14:00 14190-2486-
1567A
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 6 of 35

LL Sample # SW 7525097
LL Group # 1487148
Account # 10634
Sample Description: SS-GP13(64-68)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 10:00 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
13-64 SDG#: DUK38-03
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.464 5.63 Antimony
129 17440-38-2 06935 0.900 5.63 Arsenic
865 107440-39-3 06946 0.464 14.1 Barium
6.56 17440-41-7 06947 0.0943 1.41 Beryllium
52.2 17440-42-8 07914 1.18 14.1 Boron
0.245 J 17440-43-9 06949 0.0464 1.41 Cadmium
49.0 17440-47-3 06951 0.155 4.22 Chromium
64.0 17440-50-8 06953 0.464 2.81 Copper
19,600 17439-89-6 01654 4.70 56.3 Iron
32.9 17439-92-1 06955 0.703 4.22 Lead
95.1 17439-96-5 06958 0.117 1.41 Manganese
2.01 J 17439-98-7 06960 0.239 2.81 Molybdenum
34.3 17440-02-0 06961 0.211 2.81 Nickel
6.68 17782-49-2 06936 0.619 5.63 Selenium
N.D.17440-22-4 06966 0.267 1.41 Silver
491 57440-24-6 07968 0.232 7.03 Strontium
6.25 J 17440-28-0 06925 1.13 8.44 Thallium
53.3 17440-66-6 06972 0.366 5.63 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.156 J 17439-97-6 00159 0.0137 0.274 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
8.69 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 21.6 C.
% %%Wet Chemistry SM 2540 G-1997
32.3 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Antimony 06944
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Arsenic 06935
10Eric L Eby07/14/2014 16:47 1419206370011SW-846 6010C Barium 06946
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 7 of 35

LL Sample # SW 7525097
LL Group # 1487148
Account # 10634
Sample Description: SS-GP13(64-68)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 10:00 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
13-64 SDG#: DUK38-03
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Boron 07914
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Cadmium 06949
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Chromium 06951
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Copper 06953
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Iron 01654
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Lead 06955
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Manganese 06958
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Molybdenum 06960
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Nickel 06961
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Selenium 06936
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Silver 06966
5Eric L Eby07/14/2014 16:43 1419206370011SW-846 6010C Strontium 07968
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Thallium 06925
1Joanne M Gates07/14/2014 09:56 1419206370011SW-846 6010C Zinc 06972
1Damary Valentin07/14/2014 15:43 1419206380011SW-846 7471B Mercury 00159
1James L Mertz07/13/2014 08:55 1419206370011SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/13/2014 10:58 1419206380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/11/2014 21:30 14192039401A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/10/2014 18:44 14191820003A1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 8 of 35

LL Sample # TL 7525098
LL Group # 1487148
Account # 10634
Sample Description: SS-GP13(64-68)-20140701 Solid Sample
SPLP NON-VOLATILE EXTRACTION
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 10:00 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1364S SDG#: DUK38-04
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.251 17440-38-2 07035 0.0072 0.0400 Arsenic
0.0676 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.137 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
4.42 17440-70-2 01750 0.0334 0.400 Calcium
0.0024 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.0523 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
1.23 17439-95-4 01757 0.0167 0.200 Magnesium
0.0013 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0045 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
0.168 J 17440-09-7 01762 0.133 1.00 Potassium
0.0344 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.107440-22-4 07066 0.0180 0.100 Silver
The silver result was performed by the Method of Standard Addition.
Reporting limits were raised due to interference from the sample matrix.
3.06 17440-23-5 01767 0.167 2.00 Sodium
0.249 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0036 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Antimony 07044
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Arsenic 07035
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Barium 07046
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Beryllium 07047
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Boron 08014
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Cadmium 07049
*=This limit was used in the evaluation of the final result
Page 9 of 35

LL Sample # TL 7525098
LL Group # 1487148
Account # 10634
Sample Description: SS-GP13(64-68)-20140701 Solid Sample
SPLP NON-VOLATILE EXTRACTION
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 10:00 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1364S SDG#: DUK38-04
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Calcium 01750
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Chromium 07051
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Copper 07053
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Iron 01754
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Lead 07055
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Magnesium 01757
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Manganese 07058
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Molybdenum 07060
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Nickel 07061
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Potassium 01762
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Selenium 07036
10Joanne M Gates07/15/2014 08:52 1419106360012SW-846 6010C Silver 07066
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Sodium 01767
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Strontium 08068
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Thallium 07022
1John P Hook07/14/2014 20:14 1419106360011SW-846 6010C Zinc 07072
1Damary Valentin07/14/2014 11:58 1419157130011SW-846 7470A Mercury 00259
1Micaela L Dishong07/14/2014 10:10 1419106360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1Micaela L Dishong07/11/2014 09:00 1419157130011SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/09/2014 14:00 14190-2486-
1567A
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 10 of 35

LL Sample # SW 7525099
LL Group # 1487148
Account # 10634
Sample Description: SS-GP13(68-72)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 10:10 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1368- SDG#: DUK38-05
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.450 5.45 Antimony
127 17440-38-2 06935 0.872 5.45 Arsenic
591 57440-39-3 06946 0.225 6.81 Barium
5.10 17440-41-7 06947 0.0913 1.36 Beryllium
52.3 17440-42-8 07914 1.14 13.6 Boron
0.285 J 17440-43-9 06949 0.0450 1.36 Cadmium
47.4 17440-47-3 06951 0.150 4.09 Chromium
64.8 17440-50-8 06953 0.450 2.72 Copper
19,500 17439-89-6 01654 4.55 54.5 Iron
31.4 17439-92-1 06955 0.681 4.09 Lead
101 17439-96-5 06958 0.113 1.36 Manganese
2.91 17439-98-7 06960 0.232 2.72 Molybdenum
40.8 17440-02-0 06961 0.204 2.72 Nickel
5.71 17782-49-2 06936 0.599 5.45 Selenium
N.D.17440-22-4 06966 0.259 1.36 Silver
388 57440-24-6 07968 0.225 6.81 Strontium
7.40 J 17440-28-0 06925 1.09 8.17 Thallium
53.4 17440-66-6 06972 0.354 5.45 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.186 J 17439-97-6 00159 0.0135 0.269 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
8.61 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 21.7 C.
% %%Wet Chemistry SM 2540 G-1997
30.1 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Antimony 06944
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Arsenic 06935
5Eric L Eby07/14/2014 16:59 1419206370011SW-846 6010C Barium 06946
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 11 of 35

LL Sample # SW 7525099
LL Group # 1487148
Account # 10634
Sample Description: SS-GP13(68-72)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 10:10 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1368- SDG#: DUK38-05
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Boron 07914
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Cadmium 06949
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Chromium 06951
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Copper 06953
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Iron 01654
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Lead 06955
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Manganese 06958
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Molybdenum 06960
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Nickel 06961
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Selenium 06936
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Silver 06966
5Eric L Eby07/14/2014 16:59 1419206370011SW-846 6010C Strontium 07968
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Thallium 06925
1Joanne M Gates07/14/2014 10:08 1419206370011SW-846 6010C Zinc 06972
1Damary Valentin07/14/2014 15:45 1419206380011SW-846 7471B Mercury 00159
1James L Mertz07/13/2014 08:55 1419206370011SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/13/2014 10:58 1419206380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/11/2014 21:30 14192039401A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/10/2014 18:44 14191820003A1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 12 of 35

LL Sample # TL 7525100
LL Group # 1487148
Account # 10634
Sample Description: SS-GP13(68-72)-20140701 Solid Sample
SPLP NON-VOLATILE EXTRACTION
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 10:10 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1368S SDG#: DUK38-06
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
0.0057 J 17440-36-0 07044 0.0051 0.0400 Antimony
0.254 17440-38-2 07035 0.0072 0.0400 Arsenic
0.0321 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.177 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
3.73 17440-70-2 01750 0.0334 0.400 Calcium
0.0024 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.119 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
1.18 17439-95-4 01757 0.0167 0.200 Magnesium
0.0022 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0064 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17440-09-7 01762 0.133 1.00 Potassium
0.0293 J 17782-49-2 07036 0.0048 0.0400 Selenium
0.0210 J 107440-22-4 07066 0.0180 0.100 Silver
The silver result was performed by the Method of Standard Addition.
Reporting limits were raised due to interference from the sample matrix.
3.95 17440-23-5 01767 0.167 2.00 Sodium
0.183 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0099 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Antimony 07044
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Arsenic 07035
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Barium 07046
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Beryllium 07047
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Boron 08014
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Cadmium 07049
*=This limit was used in the evaluation of the final result
Page 13 of 35

LL Sample # TL 7525100
LL Group # 1487148
Account # 10634
Sample Description: SS-GP13(68-72)-20140701 Solid Sample
SPLP NON-VOLATILE EXTRACTION
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 10:10 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1368S SDG#: DUK38-06
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Calcium 01750
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Chromium 07051
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Copper 07053
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Iron 01754
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Lead 07055
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Magnesium 01757
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Manganese 07058
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Molybdenum 07060
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Nickel 07061
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Potassium 01762
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Selenium 07036
10Joanne M Gates07/15/2014 09:14 1419106360012SW-846 6010C Silver 07066
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Sodium 01767
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Strontium 08068
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Thallium 07022
1John P Hook07/14/2014 20:18 1419106360011SW-846 6010C Zinc 07072
1Damary Valentin07/14/2014 12:00 1419157130011SW-846 7470A Mercury 00259
1Micaela L Dishong07/14/2014 10:10 1419106360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1Micaela L Dishong07/11/2014 09:00 1419157130011SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/09/2014 14:00 14190-2486-
1567A
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 14 of 35

LL Sample # SW 7525101
LL Group # 1487148
Account # 10634
Sample Description: SS-GP14(60-62)-20140702 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 10:00 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1460- SDG#: DUK38-07
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.502 6.08 Antimony
137 17440-38-2 06935 0.973 6.08 Arsenic
562 57440-39-3 06946 0.251 7.60 Barium
3.82 17440-41-7 06947 0.102 1.52 Beryllium
34.3 17440-42-8 07914 1.28 15.2 Boron
0.228 J 17440-43-9 06949 0.0502 1.52 Cadmium
31.9 17440-47-3 06951 0.167 4.56 Chromium
58.8 17440-50-8 06953 0.502 3.04 Copper
13,500 17439-89-6 01654 5.08 60.8 Iron
24.2 17439-92-1 06955 0.760 4.56 Lead
72.8 17439-96-5 06958 0.126 1.52 Manganese
2.33 J 17439-98-7 06960 0.258 3.04 Molybdenum
26.5 17440-02-0 06961 0.228 3.04 Nickel
3.97 J 17782-49-2 06936 0.669 6.08 Selenium
N.D.17440-22-4 06966 0.289 1.52 Silver
295 57440-24-6 07968 0.251 7.60 Strontium
4.62 J 17440-28-0 06925 1.22 9.12 Thallium
36.3 17440-66-6 06972 0.395 6.08 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.0850 J 17439-97-6 00159 0.0144 0.289 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
8.65 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 21.6 C.
% %%Wet Chemistry SM 2540 G-1997
34.2 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Antimony 06944
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Arsenic 06935
5Eric L Eby07/14/2014 17:03 1419206370011SW-846 6010C Barium 06946
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 15 of 35

LL Sample # SW 7525101
LL Group # 1487148
Account # 10634
Sample Description: SS-GP14(60-62)-20140702 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 10:00 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1460- SDG#: DUK38-07
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Boron 07914
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Cadmium 06949
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Chromium 06951
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Copper 06953
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Iron 01654
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Lead 06955
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Manganese 06958
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Molybdenum 06960
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Nickel 06961
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Selenium 06936
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Silver 06966
5Eric L Eby07/14/2014 17:03 1419206370011SW-846 6010C Strontium 07968
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Thallium 06925
1Joanne M Gates07/14/2014 10:12 1419206370011SW-846 6010C Zinc 06972
1Damary Valentin07/14/2014 15:47 1419206380011SW-846 7471B Mercury 00159
1James L Mertz07/13/2014 08:55 1419206370011SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/13/2014 10:58 1419206380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/11/2014 21:30 14192039401A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/10/2014 18:44 14191820003A1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 16 of 35

LL Sample # TL 7525102
LL Group # 1487148
Account # 10634
Sample Description: SS-GP14(60-62)-20140702 Solid Sample
SPLP NON-VOLATILE EXTRACTION
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 10:00 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1460S SDG#: DUK38-08
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.247 17440-38-2 07035 0.0072 0.0400 Arsenic
0.0901 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0547 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
2.99 17440-70-2 01750 0.0334 0.400 Calcium
0.0033 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.114 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.603 17439-95-4 01757 0.0167 0.200 Magnesium
0.0031 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0053 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
0.0020 J 17440-02-0 07061 0.0016 0.0200 Nickel
0.144 J 17440-09-7 01762 0.133 1.00 Potassium
0.0077 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.107440-22-4 07066 0.0180 0.100 Silver
The silver result was performed by the Method of Standard Addition.
Reporting limits were raised due to interference from the sample matrix.
3.87 17440-23-5 01767 0.167 2.00 Sodium
0.102 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0049 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Antimony 07044
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Arsenic 07035
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Barium 07046
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Beryllium 07047
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Boron 08014
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Cadmium 07049
*=This limit was used in the evaluation of the final result
Page 17 of 35

LL Sample # TL 7525102
LL Group # 1487148
Account # 10634
Sample Description: SS-GP14(60-62)-20140702 Solid Sample
SPLP NON-VOLATILE EXTRACTION
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 10:00 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1460S SDG#: DUK38-08
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Calcium 01750
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Chromium 07051
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Copper 07053
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Iron 01754
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Lead 07055
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Magnesium 01757
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Manganese 07058
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Molybdenum 07060
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Nickel 07061
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Potassium 01762
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Selenium 07036
10Joanne M Gates07/15/2014 09:29 1419106360012SW-846 6010C Silver 07066
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Sodium 01767
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Strontium 08068
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Thallium 07022
1John P Hook07/14/2014 20:22 1419106360011SW-846 6010C Zinc 07072
1Damary Valentin07/14/2014 12:02 1419157130011SW-846 7470A Mercury 00259
1Micaela L Dishong07/14/2014 10:10 1419106360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1Micaela L Dishong07/11/2014 09:00 1419157130011SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/09/2014 14:00 14190-2486-
1567A
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 18 of 35

LL Sample # SW 7525103
LL Group # 1487148
Account # 10634
Sample Description: SS-GP14(68-72)-20140702 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 10:15 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1468- SDG#: DUK38-09
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.459 5.56 Antimony
144 57440-38-2 06935 4.45 27.8 Arsenic
661 57440-39-3 06946 0.229 6.95 Barium
5.45 17440-41-7 06947 0.0932 1.39 Beryllium
45.5 17440-42-8 07914 1.17 13.9 Boron
0.163 J 17440-43-9 06949 0.0459 1.39 Cadmium
55.8 17440-47-3 06951 0.153 4.17 Chromium
66.5 17440-50-8 06953 0.459 2.78 Copper
29,500 57439-89-6 01654 23.2 278 Iron
29.6 17439-92-1 06955 0.695 4.17 Lead
114 17439-96-5 06958 0.115 1.39 Manganese
2.65 J 17439-98-7 06960 0.236 2.78 Molybdenum
41.0 17440-02-0 06961 0.209 2.78 Nickel
6.04 17782-49-2 06936 0.612 5.56 Selenium
N.D.17440-22-4 06966 0.264 1.39 Silver
598 57440-24-6 07968 0.229 6.95 Strontium
6.68 J 17440-28-0 06925 1.11 8.34 Thallium
55.4 17440-66-6 06972 0.362 5.56 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.124 J 17439-97-6 00159 0.0134 0.269 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
8.63 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 21.5 C.
% %%Wet Chemistry SM 2540 G-1997
29.5 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Joanne M Gates07/14/2014 10:16 1419206370011SW-846 6010C Antimony 06944
5Eric L Eby07/14/2014 17:07 1419206370011SW-846 6010C Arsenic 06935
5Eric L Eby07/14/2014 17:07 1419206370011SW-846 6010C Barium 06946
1Joanne M Gates07/14/2014 10:16 1419206370011SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 19 of 35

LL Sample # SW 7525103
LL Group # 1487148
Account # 10634
Sample Description: SS-GP14(68-72)-20140702 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 10:15 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1468- SDG#: DUK38-09
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Joanne M Gates07/14/2014 10:16 1419206370011SW-846 6010C Boron 07914
1Joanne M Gates07/14/2014 10:16 1419206370011SW-846 6010C Cadmium 06949
1Joanne M Gates07/14/2014 10:16 1419206370011SW-846 6010C Chromium 06951
1Joanne M Gates07/14/2014 10:16 1419206370011SW-846 6010C Copper 06953
5Eric L Eby07/14/2014 17:07 1419206370011SW-846 6010C Iron 01654
1Joanne M Gates07/14/2014 10:16 1419206370011SW-846 6010C Lead 06955
1Joanne M Gates07/14/2014 10:16 1419206370011SW-846 6010C Manganese 06958
1Joanne M Gates07/14/2014 10:16 1419206370011SW-846 6010C Molybdenum 06960
1Joanne M Gates07/14/2014 10:16 1419206370011SW-846 6010C Nickel 06961
1Joanne M Gates07/14/2014 10:16 1419206370011SW-846 6010C Selenium 06936
1Joanne M Gates07/14/2014 10:16 1419206370011SW-846 6010C Silver 06966
5Eric L Eby07/14/2014 17:07 1419206370011SW-846 6010C Strontium 07968
1Joanne M Gates07/14/2014 10:16 1419206370011SW-846 6010C Thallium 06925
1Joanne M Gates07/14/2014 10:16 1419206370011SW-846 6010C Zinc 06972
1Damary Valentin07/14/2014 15:53 1419206380011SW-846 7471B Mercury 00159
1James L Mertz07/13/2014 08:55 1419206370011SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/13/2014 10:58 1419206380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/11/2014 21:30 14192039401A1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/10/2014 18:44 14191820003A1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 20 of 35

LL Sample # TL 7525104
LL Group # 1487148
Account # 10634
Sample Description: SS-GP14(68-72)-20140702 Solid Sample
SPLP NON-VOLATILE EXTRACTION
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 10:15 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1468S SDG#: DUK38-10
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
0.0057 J 17440-36-0 07044 0.0051 0.0400 Antimony
0.263 17440-38-2 07035 0.0072 0.0400 Arsenic
0.0281 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0761 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
4.83 17440-70-2 01750 0.0334 0.400 Calcium
0.0050 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.101 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.560 17439-95-4 01757 0.0167 0.200 Magnesium
0.0044 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0046 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17440-09-7 01762 0.133 1.00 Potassium
0.0281 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.107440-22-4 07066 0.0180 0.100 Silver
The silver result was performed by the Method of Standard Addition.
Reporting limits were raised due to interference from the sample matrix.
3.24 17440-23-5 01767 0.167 2.00 Sodium
0.163 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0038 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Antimony 07044
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Arsenic 07035
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Barium 07046
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Beryllium 07047
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Boron 08014
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Cadmium 07049
*=This limit was used in the evaluation of the final result
Page 21 of 35

LL Sample # TL 7525104
LL Group # 1487148
Account # 10634
Sample Description: SS-GP14(68-72)-20140702 Solid Sample
SPLP NON-VOLATILE EXTRACTION
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/02/2014 10:15 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1468S SDG#: DUK38-10
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Calcium 01750
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Chromium 07051
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Copper 07053
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Iron 01754
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Lead 07055
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Magnesium 01757
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Manganese 07058
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Molybdenum 07060
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Nickel 07061
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Potassium 01762
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Selenium 07036
10Joanne M Gates07/15/2014 09:44 1419106360012SW-846 6010C Silver 07066
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Sodium 01767
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Strontium 08068
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Thallium 07022
1John P Hook07/14/2014 20:25 1419106360011SW-846 6010C Zinc 07072
1Damary Valentin07/14/2014 12:04 1419157130011SW-846 7470A Mercury 00259
1Micaela L Dishong07/14/2014 10:10 1419106360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1Micaela L Dishong07/11/2014 09:00 1419157130011SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/09/2014 14:00 14190-2486-
1567A
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 22 of 35

LL Sample # SW 7525105
LL Group # 1487148
Account # 10634
Sample Description: SS-GP15(60-64)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:30 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1560- SDG#: DUK38-11
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.432 5.24 Antimony
125 17440-38-2 06935 0.839 5.24 Arsenic
493 57440-39-3 06946 0.216 6.55 Barium
4.89 17440-41-7 06947 0.0878 1.31 Beryllium
66.7 17440-42-8 07914 1.10 13.1 Boron
N.D.17440-43-9 06949 0.0432 1.31 Cadmium
65.1 17440-47-3 06951 0.144 3.93 Chromium
64.5 17440-50-8 06953 0.432 2.62 Copper
43,400 57439-89-6 01654 21.9 262 Iron
24.6 17439-92-1 06955 0.655 3.93 Lead
160 57439-96-5 06958 0.544 6.55 Manganese
2.68 17439-98-7 06960 0.223 2.62 Molybdenum
47.3 17440-02-0 06961 0.197 2.62 Nickel
4.54 J 17782-49-2 06936 0.576 5.24 Selenium
N.D.17440-22-4 06966 0.249 1.31 Silver
561 57440-24-6 07968 0.216 6.55 Strontium
9.28 17440-28-0 06925 1.05 7.86 Thallium
55.8 17440-66-6 06972 0.341 5.24 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.0778 J 17439-97-6 00159 0.0125 0.249 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
8.28 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 22.2 C.
% %%Wet Chemistry SM 2540 G-1997
25.9 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Joanne M Gates07/14/2014 10:20 1419206370011SW-846 6010C Antimony 06944
1Joanne M Gates07/14/2014 10:20 1419206370011SW-846 6010C Arsenic 06935
5Eric L Eby07/14/2014 17:11 1419206370011SW-846 6010C Barium 06946
1Joanne M Gates07/14/2014 10:20 1419206370011SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 23 of 35

LL Sample # SW 7525105
LL Group # 1487148
Account # 10634
Sample Description: SS-GP15(60-64)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:30 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1560- SDG#: DUK38-11
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Joanne M Gates07/14/2014 10:20 1419206370011SW-846 6010C Boron 07914
1Joanne M Gates07/14/2014 10:20 1419206370011SW-846 6010C Cadmium 06949
1Joanne M Gates07/14/2014 10:20 1419206370011SW-846 6010C Chromium 06951
1Joanne M Gates07/14/2014 10:20 1419206370011SW-846 6010C Copper 06953
5Eric L Eby07/14/2014 17:11 1419206370011SW-846 6010C Iron 01654
1Joanne M Gates07/14/2014 10:20 1419206370011SW-846 6010C Lead 06955
5Eric L Eby07/14/2014 17:11 1419206370011SW-846 6010C Manganese 06958
1Joanne M Gates07/14/2014 10:20 1419206370011SW-846 6010C Molybdenum 06960
1Joanne M Gates07/14/2014 10:20 1419206370011SW-846 6010C Nickel 06961
1Joanne M Gates07/14/2014 10:20 1419206370011SW-846 6010C Selenium 06936
1Joanne M Gates07/14/2014 10:20 1419206370011SW-846 6010C Silver 06966
5Eric L Eby07/14/2014 17:11 1419206370011SW-846 6010C Strontium 07968
1Joanne M Gates07/14/2014 10:20 1419206370011SW-846 6010C Thallium 06925
1Joanne M Gates07/14/2014 10:20 1419206370011SW-846 6010C Zinc 06972
1Damary Valentin07/14/2014 15:55 1419206380011SW-846 7471B Mercury 00159
1James L Mertz07/13/2014 08:55 1419206370011SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/13/2014 10:58 1419206380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/11/2014 21:30 14192039401B1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/10/2014 18:44 14191820003A1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 24 of 35

LL Sample # TL 7525106
LL Group # 1487148
Account # 10634
Sample Description: SS-GP15(60-64)-20140701 Solid Sample
SPLP NON-VOLATILE EXTRACTION
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:30 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1560S SDG#: DUK38-12
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.208 17440-38-2 07035 0.0072 0.0400 Arsenic
0.0178 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.100 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
6.35 17440-70-2 01750 0.0334 0.400 Calcium
0.0036 J 17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.0561 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.678 17439-95-4 01757 0.0167 0.200 Magnesium
0.0021 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0042 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
N.D.17440-02-0 07061 0.0016 0.0200 Nickel
N.D.17440-09-7 01762 0.133 1.00 Potassium
0.0278 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.107440-22-4 07066 0.0180 0.100 Silver
The silver result was performed by the Method of Standard Addition.
Reporting limits were raised due to interference from the sample matrix.
9.01 17440-23-5 01767 0.167 2.00 Sodium
0.197 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0030 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Antimony 07044
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Arsenic 07035
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Barium 07046
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Beryllium 07047
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Boron 08014
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Cadmium 07049
*=This limit was used in the evaluation of the final result
Page 25 of 35

LL Sample # TL 7525106
LL Group # 1487148
Account # 10634
Sample Description: SS-GP15(60-64)-20140701 Solid Sample
SPLP NON-VOLATILE EXTRACTION
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 14:30 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1560S SDG#: DUK38-12
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Calcium 01750
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Chromium 07051
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Copper 07053
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Iron 01754
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Lead 07055
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Magnesium 01757
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Manganese 07058
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Molybdenum 07060
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Nickel 07061
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Potassium 01762
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Selenium 07036
10Joanne M Gates07/15/2014 10:07 1419106360012SW-846 6010C Silver 07066
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Sodium 01767
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Strontium 08068
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Thallium 07022
1John P Hook07/14/2014 20:29 1419106360011SW-846 6010C Zinc 07072
1Damary Valentin07/14/2014 12:06 1419157130011SW-846 7470A Mercury 00259
1Micaela L Dishong07/14/2014 10:10 1419106360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1Micaela L Dishong07/11/2014 09:00 1419157130011SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/09/2014 14:00 14190-2486-
1567A
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 26 of 35

LL Sample # SW 7525107
LL Group # 1487148
Account # 10634
Sample Description: SS-GP15(68.7-70.7)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 15:00 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1568- SDG#: DUK38-13
Dry
Limit of
Quantitation
Dry
Method
Detection Limit* Dry
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/kg mg/kgmg/kgMetals SW-846 6010C
N.D.17440-36-0 06944 0.453 5.49 Antimony
35.6 17440-38-2 06935 0.879 5.49 Arsenic
265 57440-39-3 06946 0.227 6.87 Barium
3.00 17440-41-7 06947 0.0920 1.37 Beryllium
30.2 17440-42-8 07914 1.15 13.7 Boron
N.D.17440-43-9 06949 0.0453 1.37 Cadmium
22.3 17440-47-3 06951 0.151 4.12 Chromium
28.9 17440-50-8 06953 0.453 2.75 Copper
22,400 17439-89-6 01654 4.59 54.9 Iron
15.2 17439-92-1 06955 0.687 4.12 Lead
63.4 17439-96-5 06958 0.114 1.37 Manganese
2.38 J 17439-98-7 06960 0.233 2.75 Molybdenum
112 17440-02-0 06961 0.206 2.75 Nickel
1.82 J 17782-49-2 06936 0.604 5.49 Selenium
N.D.17440-22-4 06966 0.261 1.37 Silver
237 57440-24-6 07968 0.227 6.87 Strontium
62.5 17440-28-0 06925 1.10 8.24 Thallium
27.5 17440-66-6 06972 0.357 5.49 Zinc
mg/kg mg/kgmg/kgSW-846 7471B
0.0272 J 17439-97-6 00159 0.0140 0.280 Mercury
Std. Units Std. UnitsStd. UnitsWet Chemistry SW-846 9045D modified
7.89 1n.a. 00394 0.0100 0.0100 pH
The pH was measured in water at 21.6 C.
% %%Wet Chemistry SM 2540 G-1997
29.3 1n.a. 00111 0.50 0.50 Moisture
Moisture represents the loss in weight of the sample after oven drying at
103 - 105 degrees Celsius. The moisture result reported is on an
as-received basis.
General Sample Comments
State of North Carolina Lab Certification No. 521

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Antimony 06944
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Arsenic 06935
5Eric L Eby07/14/2014 17:15 1419206370011SW-846 6010C Barium 06946
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Beryllium 06947
*=This limit was used in the evaluation of the final result
Page 27 of 35

LL Sample # SW 7525107
LL Group # 1487148
Account # 10634
Sample Description: SS-GP15(68.7-70.7)-20140701 Solid Sample
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 15:00 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1568- SDG#: DUK38-13
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Boron 07914
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Cadmium 06949
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Chromium 06951
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Copper 06953
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Iron 01654
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Lead 06955
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Manganese 06958
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Molybdenum 06960
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Nickel 06961
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Selenium 06936
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Silver 06966
5Eric L Eby07/14/2014 17:15 1419206370011SW-846 6010C Strontium 07968
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Thallium 06925
1Joanne M Gates07/14/2014 10:24 1419206370011SW-846 6010C Zinc 06972
1Damary Valentin07/14/2014 15:57 1419206380011SW-846 7471B Mercury 00159
1James L Mertz07/13/2014 08:55 1419206370011SW-846 3050B SW SW846 (IV)ICP/ICPMS
Digest
10637
1James L Mertz07/13/2014 10:58 1419206380011SW-846 7471B SW SW846 (IV) Hg Digest 10638
1Luz M Groff07/11/2014 21:30 14192039401B1SW-846 9045D
modified
pH 00394
1Scott W Freisher07/10/2014 18:44 14191820003A1SM 2540 G-1997 Moisture 00111
*=This limit was used in the evaluation of the final result
Page 28 of 35

LL Sample # TL 7525108
LL Group # 1487148
Account # 10634
Sample Description: SS-GP15(68.7-70.7)-20140701 Solid Sample
SPLP NON-VOLATILE EXTRACTION
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 15:00 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1568S SDG#: DUK38-14*
As Received
Limit of
Quantitation
As Received
Method
Detection Limit* As Received
ResultAnalysis Name CAS Number
Dilution
Factor
CAT
No.
mg/l mg/lmg/lMetals SW-846 6010C
N.D.17440-36-0 07044 0.0051 0.0400 Antimony
0.0914 17440-38-2 07035 0.0072 0.0400 Arsenic
0.0332 17440-39-3 07046 0.00033 0.0100 Barium
N.D.17440-41-7 07047 0.00067 0.0100 Beryllium
0.0763 J 17440-42-8 08014 0.0046 0.100 Boron
N.D.17440-43-9 07049 0.00033 0.0100 Cadmium
6.44 17440-70-2 01750 0.0334 0.400 Calcium
N.D.17440-47-3 07051 0.0013 0.0300 Chromium
N.D.17440-50-8 07053 0.0028 0.0200 Copper
0.0698 J 17439-89-6 01754 0.0334 0.400 Iron
N.D.17439-92-1 07055 0.0047 0.0300 Lead
0.960 17439-95-4 01757 0.0167 0.200 Magnesium
0.0033 J 17439-96-5 07058 0.00083 0.0100 Manganese
0.0026 J 17439-98-7 07060 0.0017 0.0200 Molybdenum
0.0021 J 17440-02-0 07061 0.0016 0.0200 Nickel
0.209 J 17440-09-7 01762 0.133 1.00 Potassium
0.0152 J 17782-49-2 07036 0.0048 0.0400 Selenium
N.D.107440-22-4 07066 0.0180 0.100 Silver
The silver result was performed by the Method of Standard Addition.
Reporting limits were raised due to interference from the sample matrix.
3.45 17440-23-5 01767 0.167 2.00 Sodium
0.240 17440-24-6 08068 0.00033 0.0100 Strontium
N.D.17440-28-0 07022 0.0051 0.0600 Thallium
0.0077 J 17440-66-6 07072 0.0020 0.0400 Zinc
mg/l mg/lmg/lSW-846 7470A
N.D.17439-97-6 00259 0.000060 0.00020 Mercury
General Sample Comments
State of North Carolina Lab Certification No. 521

If the analysis is for determination of Hazardous Waste Characteristics,
see Table 1 in EPA Code of Federal Regulations 40 CFR 261.24.

All QC is compliant unless otherwise noted. Please refer to the Quality
Control Summary for overall QC performance data and associated samples.
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Antimony 07044
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Arsenic 07035
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Barium 07046
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Beryllium 07047
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Boron 08014
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Cadmium 07049
*=This limit was used in the evaluation of the final result
Page 29 of 35

LL Sample # TL 7525108
LL Group # 1487148
Account # 10634
Sample Description: SS-GP15(68.7-70.7)-20140701 Solid Sample
SPLP NON-VOLATILE EXTRACTION
Duke Sutton

Project Name: Duke Sutton, NC
Collected: 07/01/2014 15:00 by WS
Submitted: 07/08/2014 09:20
GeoSyntec Consultants
Reported: 07/15/2014 12:40
2501 Blue Ridge Road
Suite 430
Raleigh NC 27607
1568S SDG#: DUK38-14*
Method Analysis Name CAT
No.
Analysis
Date and Time
Batch#Trial#Dilution
Factor
Analyst
Laboratory Sample Analysis Record
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Calcium 01750
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Chromium 07051
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Copper 07053
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Iron 01754
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Lead 07055
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Magnesium 01757
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Manganese 07058
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Molybdenum 07060
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Nickel 07061
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Potassium 01762
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Selenium 07036
10Joanne M Gates07/15/2014 10:22 1419106360012SW-846 6010C Silver 07066
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Sodium 01767
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Strontium 08068
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Thallium 07022
1John P Hook07/14/2014 20:33 1419106360011SW-846 6010C Zinc 07072
1Damary Valentin07/14/2014 12:08 1419157130011SW-846 7470A Mercury 00259
1Micaela L Dishong07/14/2014 10:10 1419106360011SW-846 3010A WW/TL SW846 (IV) ICP Dig
(tot)
10636
1Micaela L Dishong07/11/2014 09:00 1419157130011SW-846 7470A WW SW846 Hg Digest 05713
n.a.Christina A Huber07/09/2014 14:00 14190-2486-
1567A
1SW-846 1312 Synthetic Precipitation
Leach
01567
*=This limit was used in the evaluation of the final result
Page 30 of 35

Page 1 of 3

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1487148
Reported: 07/15/14 at 12:40 PM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Matrix QC may not be reported if insufficient sample or site-specific QC samples were not submitted. In these
situations, to demonstrate precision and accuracy at a batch level, a LCS/LCSD was performed, unless otherwise
specified in the method.

All Inorganic Initial Calibration and Continuing Calibration Blanks met acceptable method criteria unless
otherwise noted on the Analysis Report.

Laboratory Compliance Quality Control

Blank Blank Blank Report LCS LCSD LCS/LCSD
Analysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max

Batch number: 141910636001 Sample number(s): 7525096,7525098,7525100,7525102,7525104,7525106,7525108
Antimony N.D. 0.0051 0.0400 mg/l 106 80-120
Arsenic N.D. 0.0072 0.0400 mg/l 107 80-120
Barium N.D. 0.00033 0.0100 mg/l 103 80-120
Beryllium N.D. 0.00067 0.0100 mg/l 103 80-120
Boron N.D. 0.0046 0.100 mg/l 100 80-120
Cadmium N.D. 0.00033 0.0100 mg/l 108 80-120
Calcium N.D. 0.0334 0.400 mg/l 106 80-120
Chromium N.D. 0.0013 0.0300 mg/l 104 80-120
Copper N.D. 0.0028 0.0200 mg/l 105 80-120
Iron N.D. 0.0334 0.400 mg/l 107 80-120
Lead N.D. 0.0047 0.0300 mg/l 112 80-120
Magnesium N.D. 0.0167 0.200 mg/l 101 80-120
Manganese N.D. 0.00083 0.0100 mg/l 106 80-120
Molybdenum N.D. 0.0017 0.0200 mg/l 103 80-120
Nickel N.D. 0.0016 0.0200 mg/l 112 80-120
Potassium N.D. 0.133 1.00 mg/l 102 80-120
Selenium N.D. 0.0048 0.0400 mg/l 106 80-120
Silver N.D. 0.0018 0.0100 mg/l 111 80-120
Sodium N.D. 0.167 2.00 mg/l 100 80-120
Strontium N.D. 0.00033 0.0100 mg/l 105 80-120
Thallium N.D. 0.0051 0.0600 mg/l 107 80-120
Zinc N.D. 0.0020 0.0400 mg/l 107 80-120

Batch number: 141915713001 Sample number(s): 7525096,7525098,7525100,7525102,7525104,7525106,7525108
Mercury N.D. 0.00006
0
0.00020 mg/l 97 80-120

Batch number: 141920637001 Sample number(s): 7525095,7525097,7525099,7525101,7525103,7525105,7525107
Antimony N.D. 0.330 4.00 mg/kg 113 80-120
Arsenic N.D. 0.640 4.00 mg/kg 106 80-120
Barium N.D. 0.0330 1.00 mg/kg 104 80-120
Beryllium N.D. 0.0670 1.00 mg/kg 102 80-120
Boron 1.31 J 0.840 10.0 mg/kg 100 80-120
Cadmium N.D. 0.0330 1.00 mg/kg 105 80-120
Chromium N.D. 0.110 3.00 mg/kg 103 80-120
Copper N.D. 0.330 2.00 mg/kg 104 80-120
Iron N.D. 3.34 40.0 mg/kg 106 80-120
Lead N.D. 0.500 3.00 mg/kg 105 80-120
Manganese 0.0860 J 0.0830 1.00 mg/kg 103 80-120
Molybdenum N.D. 0.170 2.00 mg/kg 106 80-120
Nickel N.D. 0.150 2.00 mg/kg 109 80-120
Selenium N.D. 0.440 4.00 mg/kg 103 80-120
Silver N.D. 0.190 1.00 mg/kg 104 80-120
Page 31 of 35

Page 2 of 3

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1487148
Reported: 07/15/14 at 12:40 PM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Blank Blank Blank Report LCS LCSD LCS/LCSD
Analysis Name Result MDL** LOQ Units %REC %REC Limits RPD RPD Max
Strontium 0.105 J 0.0330 1.00 mg/kg 106 80-120
Thallium N.D. 0.800 6.00 mg/kg 120 80-120
Zinc 0.517 J 0.260 4.00 mg/kg 103 80-120

Batch number: 141920638001 Sample number(s): 7525095,7525097,7525099,7525101,7525103,7525105,7525107
Mercury N.D. 0.0100 0.200 mg/kg 92 80-120

Batch number: 14192039401A Sample number(s): 7525095,7525097,7525099,7525101,7525103
pH 99 90-110

Batch number: 14192039401B Sample number(s): 7525105,7525107
pH 99 90-110

Batch number: 14191820003A Sample number(s): 7525095,7525097,7525099,7525101,7525103,7525105,7525107
Moisture 100 99-101

Sample Matrix Quality Control
Unspiked (UNSPK) = the sample used in conjunction with the matrix spike
Background (BKG) = the sample used in conjunction with the duplicate

MS MSD MS/MSD RPD BKG DUP DUP Dup RPD
Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___

Batch number: 141910636001 Sample number(s): 7525096,7525098,7525100,7525102,7525104,7525106,7525108 UNSPK:
7525096 BKG: 7525096
Antimony 89 87 75-125 1 20 0.0222 J 0.0207 J 7 (1) 20
Arsenic 94 93 75-125 2 20 0.0716 0.0748 4 (1) 20
Barium 89 89 75-125 1 20 0.135 0.137 1 20
Beryllium 86 85 75-125 2 20 N.D. N.D. 0 (1) 20
Boron 87 87 75-125 0 20 0.0463 J 0.0443 J 4 (1) 20
Cadmium 90 89 75-125 1 20 N.D. N.D. 0 (1) 20
Calcium 92 90 75-125 2 20 3.24 3.31 2 20
Chromium 87 87 75-125 1 20 N.D. N.D. 0 (1) 20
Copper 90 89 75-125 1 20 0.0281 0.0278 1 (1) 20
Iron 87 84 75-125 3 20 N.D. N.D. 0 (1) 20
Lead 86 84 75-125 2 20 N.D. N.D. 0 (1) 20
Magnesium 88 85 75-125 3 20 0.529 0.533 1 (1) 20
Manganese 89 89 75-125 1 20 0.0080 J 0.0083 J 4 (1) 20
Molybdenum 85 84 75-125 2 20 0.141 0.142 1 20
Nickel 88 86 75-125 1 20 0.0046 J 0.0048 J 4 (1) 20
Potassium 93 91 75-125 3 20 0.600 J 0.577 J 4 (1) 20
Selenium 89 89 75-125 0 20 0.0090 J 0.0117 J 25* (1) 20
Silver 7* 7* 75-125 3 20 N.D. N.D. 0 (1) 20
Sodium 90 87 75-125 3 20 2.20 2.22 1 (1) 20
Strontium 83 82 75-125 1 20 0.191 0.194 2 20
Thallium 85 83 75-125 2 20 N.D. N.D. 0 (1) 20
Zinc 91 90 75-125 1 20 0.0027 J 0.0024 J 12 (1) 20

Batch number: 141915713001 Sample number(s): 7525096,7525098,7525100,7525102,7525104,7525106,7525108 UNSPK:
7525096 BKG: 7525096
Mercury 73* 71* 80-120 2 20 N.D. N.D. 0 (1) 20

Batch number: 141920637001 Sample number(s): 7525095,7525097,7525099,7525101,7525103,7525105,7525107 UNSPK:
Page 32 of 35

Page 3 of 3

Quality Control Summary

Client Name: GeoSyntec Consultants Group Number: 1487148
Reported: 07/15/14 at 12:40 PM

*- Outside of specification
**-This limit was used in the evaluation of the final result for the blank
(1) The result for one or both determinations was less than five times the LOQ.
(2) The unspiked result was more than four times the spike added.

Sample Matrix Quality Control
Unspiked (UNSPK) = the sample used in conjunction with the matrix spike
Background (BKG) = the sample used in conjunction with the duplicate

MS MSD MS/MSD RPD BKG DUP DUP Dup RPD
Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max___
P526716 BKG: P526716
Antimony 65* 68* 75-125 3 20 0.453 J 0.324 J 33* (1) 20
Arsenic 103 104 75-125 1 20 2.38 J 2.77 J 15 (1) 20
Barium 105 112 75-125 3 20 121 116 4 20
Beryllium 102 101 83-119 2 20 0.574 J 0.473 J 19 (1) 20
Boron 103 102 84-110 3 20 17.4 14.5 18 (1) 20
Cadmium 98 96 75-120 4 20 N.D. 0.0510 J 200* (1) 20
Chromium 118 116 75-125 2 20 18.7 17.9 4 20
Copper 116 132* 75-125 7 20 17.9 21.5 18 20
Iron -269
(2)
-30 (2) 75-125 1 20 19,000 16,200 16 20
Lead -377
(2)
317 (2) 75-125 74* 20 144 67.0 73* 20
Manganese 29 (2) 880 (2) 75-125 65* 20 417 307 30* 20
Molybdenum 98 97 82-110 3 20 0.990 J 0.724 J 31* (1) 20
Nickel 98 96 75-125 3 20 17.7 16.3 8 20
Selenium 96 99 75-125 1 20 N.D. N.D. 0 (1) 20
Silver 98 100 75-125 0 20 N.D. N.D. 0 (1) 20
Strontium 97 100 81-125 0 20 27.8 24.0 14 20
Thallium 112 111 78-119 3 20 N.D. N.D. 0 (1) 20
Zinc 117 136* 75-125 6 20 66.8 72.5 8 20

Batch number: 141920638001 Sample number(s): 7525095,7525097,7525099,7525101,7525103,7525105,7525107 UNSPK:
7525095 BKG: 7525095
Mercury 104 104 80-120 4 20 0.0543 J 0.0666 J 20 (1) 20

Batch number: 14192039401A Sample number(s): 7525095,7525097,7525099,7525101,7525103 BKG: P526010
pH 10.3 10.3 0 3

Batch number: 14192039401B Sample number(s): 7525105,7525107 BKG: P522507
pH 7.89 7.85 1 3

Batch number: 14191820003A Sample number(s): 7525095,7525097,7525099,7525101,7525103,7525105,7525107 BKG:
P526737
Moisture 3.7 3.7 1 5

Page 33 of 35
Page 34 of 35
Explanation of Symbols and Abbreviations

3768 0713
The following defines common symbols and abbreviations used in reporting technical data:
RL Reporting Limit BMQL Below Minimum Quantitation Level
N.D. none detected MPN Most Probable Number
TNTC Too Numerous To Count CP Units cobalt-chloroplatinate units
IU International Units NTU nephelometric turbidity units
umhos/cm micromhos/cm ng nanogram(s)
C degrees Celsius F degrees Fahrenheit
meq milliequivalents lb. pound(s)
g gram(s) kg kilogram(s)
µg microgram(s) mg milligram(s)
mL milliliter(s) L liter(s)
m3 cubic meter(s) µL microliter(s)
pg/L picogram/liter
< less than - The number following the sign is the limit of quantitation, the smallest amount of analyte which can be
reliably determined using this specific test.
> greater than
ppm parts per million - One ppm is equivalent to one milligram per kilogram (mg/kg), or one gram per million grams. For
aqueous liquids, ppm is usually taken to be equivalent to milligrams per liter (mg/l), because one liter of water has a
weight very close to a kilogram. For gases or vapors, one ppm is equivalent to one microliter per liter of gas.
ppb parts per billion
Dry weight Results printed under this heading have been adjusted for moisture content. This increases the analyte weight
basis concentration to approximate the value present in a similar sample without moisture. All other results are reported
on an as-received basis.
Data Qualifiers:
C – result confirmed by reanalysis.
J - estimated value – The result is ≥ the Method Detection Limit (MDL) and < the Limit of Quantitation (LOQ).
U.S. EPA CLP Data Qualifiers:
Organic Qualifiers Inorganic Qualifiers
A TIC is a possible aldol-condensation product B Value is <CRDL, but ≥IDL
B Analyte was also detected in the blank E Estimated due to interference
C Pesticide result confirmed by GC/MS M Duplicate injection precision not met
D Compound quantitated on a diluted sample N Spike sample not within control limits
E Concentration exceeds the calibration range of S Method of standard additions (MSA) used
the instrument for calculation
N Presumptive evidence of a compound (TICs only) U Compound was not detected
P Concentration difference between primary and W Post digestion spike out of control limits
confirmation columns >25% * Duplicate analysis not within control limits
U Compound was not detected + Correlation coefficient for MSA <0.995
X,Y,Z Defined in case narrative
Analytical test results meet all requirements of NELAC unless otherwise noted under the individual analysis.
Measurement uncertainty values, as applicable, are available upon request.
Tests results relate only to the sample tested. Clients should be aware that a critical step in a chemical or microbiological
analysis is the collection of the sample. Unless the sample analyzed is truly representative of the bulk of material involved, the
test results will be meaningless. If you have questions regarding the proper techniques of collecting samples, please contact
us. We cannot be held responsible for sample integrity, however, unless sampling has been performed by a member of our
staff. This report shall not be reproduced except in full, without the written approval of the laboratory.
Times are local to the area of activity. Parameters listed in the 40 CFR part 136 Table II as “analyze immediately” are not
performed within 15 minutes.

WARRANTY AND LIMITS OF LIABILITY - In accepting analytical work, we warrant the accuracy of test results for the sample as submitted. THE
FOREGOING EXPRESS WARRANTY IS EXCLUSIVE AND IS GIVEN IN LIEU OF ALL OTHER WARRANTIES, EXPRESSED OR IMPLIED. WE DISCLAIM
ANY OTHER WARRANTIES, EXPRESSED OR IMPLIED, INCLUDING A WARRANTY OF FITNESS FOR PARTICULAR PURPOSE AND WARRANTY OF
MERCHANTABILITY. IN NO EVENT SHALL EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL, LLC BE LIABLE FOR INDIRECT, SPECIAL,
CONSEQUENTIAL, OR INCIDENTAL DAMAGES INCLUDING, BUT NOT LIMITED TO, DAMAGES FOR LOSS OF PROFIT OR GOODWILL REGARDLESS
OF (A) THE NEGLIGENCE (EITHER SOLE OR CONCURRENT) OF EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL AND (B) WHETHER
EUROFINS LANCASTER LABORATORIES ENVIRONMENTAL HAS BEEN INFORMED OF THE POSSIBILITY OF SUCH DAMAGES. We accept no legal
responsibility for the purposes for which the client uses the test results. No purchase order or other order for work shall be accepted by Eurofins Lancaster
Laboratories Environmental which includes any conditions that vary from the Standard Terms and Conditions, and Eurofins Lancaster Laboratories
Environmental hereby objects to any conflicting terms contained in any acceptance or order submitted by client.
Page 35 of 35

APPENDIX 2.A3

Geosyntec DPT Boring Logs
Legend for Soil Classification Symbols
Pattern Description

SP – poorly graded sands

SW – well graded sands

GP – poorly graded gravels
GW – well graded gravels
SM – silty sands

SP-SM – poorly graded sand with silty sand

SP-SC – poorly graded sand with clayey sand

MH – elastic silts

ML – inorganic silts with slight plasticity

SC – clayey sands

CL – lean clays

CH – fat clays

OH – organic clays

Sand and CCR Mixture

CCR

0
-5
-10
-15
10
5
0
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
Collected SS-F-DPT-1 (3-4)
20140630 (submitted)
Collected SS-F-DPT-1 (7-8)
20140630 (submitted)
60%
60%
90%
25%
Tan medium SAND (SP), with trace roots and
trace CCRs
Very fine gray CCRs, saturated
Very fine gray to tan CCRs, saturated
Fine to medium tan SAND (SP), saturated
06/30/14
Rachel Donahue
SAEDACCO
Will Keyes
16
196875.5
2306640.9
11.9
F-DPT-1
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"
0
-5
-10
10
5
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
Collected SS-F-DPT-2 (3-4)
20140630
Collected SS-F-DPT-2 (7-8)
20140630
30%
50%
25%
Medium to fine brown to gray and orange well
graded SAND (SW), trace black specks
Fine orange to tan SAND (SW), trace black
specks, saturated
06/30/14
Rachel Donahue
SAEDACCO
Will Keyes
12
197079.5
2306716.4
14.2
F-DPT-2
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"
0
-5
-10
10
5
0
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
Collected SS-F-DPT-3 (1.5-2.5)
20140630 (submitted)
Collected SS-F-DPT-3 (5-6)
20140630 (submitted)
75%
100%
75%
Medium brown to tan SAND (SP), dry, trace black
specks
Medium brown to tan SAND (SP), saturated, trace
black specks
CCRs, saturated
Medium tan SAND (SP), saturated, trace black
specks
06/30/14
Rachel Donahue
SAEDACCO
Will Keyes
12
197022.7
2306385.9
10.3
F-DPT-3
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"
0
-5
-10
-15
-20
5
0
-5
-10
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
Collected SS-F-DPT-4 (2-3)
20140701
Collected SS-F-DPT-4 (7-8)
20140701
Collected SS-F-DPT-4 (18-20)
20140701 (submitted)
70%
75%
75%
60%
75%
Dark gray medium silty SAND (SM) with a silt
layer at 3 ft bgs, some roots, damp
Medium to dark gray medium SAND and CCR
mixture, saturated, layer of hard silt at 6.5 ft bgs
Light gray medium SAND (SP), trace black specs,
saturated
Dark brown medium silty SAND (SM), saturated
Dark brown medium silty SAND (SM), saturated,
becoming lighter color with depth
Gray medium SAND (SP), saturated
Gray medium SAND (SP), saturated, transitions to
dark gray organic silt layer
07/01/14
Rachel Donahue
SAEDACCO
Will Keyes
20
196505.8
2305220.2
8.7
F-DPT-4
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"
0
-5
-10
-15
-20
5
0
-5
-10
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
Collected SS-F-DPT-5 (2-4)
20140701 and MS and MSD
(submitted)
Collected SS-F-DPT-5 (6-8)
20140701 and duplicate SS-
F-DPT-5 (6-8) 20140701
(submitted)
75%
100%
0%
50%
60%
Very fine gray black silty material, possibly CCR's,
some areas have a sheen
Very fine gray black silty material, possibly CCR's,
some areas have a sheen, saturated
No recovery
fine to medium gray SAND (SP) with staining of
core at top of core
Medium brown SAND (SP) with some silt
Fine to medium light tan SAND (SP)
07/01/14
Rachel Donahue
SAEDACCO
Will Keyes
20
197182.6
2305313.3
9.7
F-DPT-5
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"
0
-5
-10
-15
-20
10
5
0
-5
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
Collected SS-F-DPT-6 (3-4)
20140701
Collected SS-F-DPT-6 (8-9)
20140701
100%
40%
100%
100%
100%
Fine tan and orange SAND (SP) with some gray
silt (possibly CCRs) and trace organics (roots)
Gray CCRs, saturated
Dark brown medium SAND and CCR mixture
Medium to dark brown silty SAND (SM), saturated
07/01/14
Rachel Donahue
SAEDACCO
Will Keyes
20
197155.9
2305004.4
10.9
F-DPT-6
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"
0
-5
-10
-15
-20
5
0
-5
-10
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
Collected SS-F-DPT-7 (3-4)
20140701 (submitted)
Collected SS-F-DPT-7 (7-8)
20140701 (submitted)
Collected SS-F-DPT-7 (15-16)
20140701 (submitted)
100%
75%
75%
75%
60%
Medium brown SAND (SP) with some gray silty
material (possibly CCRs)
Light to dark gray CCRs, compact, saturated
Medium brown silty SAND (SM), trace black
specks
Dark brown silty SAND (SM)
Medium brown SAND (SP), some brown silt
07/01/14
Rachel Donahue
SAEDACCO
Will Keyes
20
197035.6
2305560.4
9.0
F-DPT-7
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"
0
-5
-10
-15
-20
5
0
-5
-10
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
Collected SS-F-DPT-8 (3-4)
20140701
Collected SS-F-DPT-8 (3-4)
20140701
Drill bit got stuck during drilling and
core between 16 and 20 ft bgs
was unable to be recovered.
50%
75%
80%
60%
0%
Fine to medium tan and gray SAND (SP) with
gray silty material (possibly CCRs)
Gray fine SAND (SP) with CCRs, saturated
Gray fine CCRs
Gray medium SAND (SP) with black staining
Medium brown SAND and CCR mixture,
transitioning to dark brown silty SAND (SM) at 10
ft bgs
Fine tan SAND (SP), saturated, trace black
specks
07/01/14
Rachel Donahue
SAEDACCO
Will Keyes
20
197251.1
2305892.6
9.9
F-DPT-8
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"
0
-5
-10
-15
-20
10
5
0
-5
-10
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
Collected SS-F-DPT-9 (1-2)
20140701
Collected SS-F-DPT-9 (3-4)
20140701
100%
75%
100%
50%
30%
75%
Dark brown SAND and CCR mixture
Dark brown SAND and CCR mixture, saturated
Fine to medium tan SAND (SP), saturated, some
black specks
Brown SAND and CCR mixture
Fine tan SAND (SP), saturated
07/01/14
Rachel Donahue
SAEDACCO
Will Keyes
20
197173.0
2306258.2
10.0
F-DPT-9
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"
0
-5
-10
-15
-20
10
5
0
-5
-10
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
Collected SS-F-DPT-10 (3-4)
20140702
Collected SS-F-DPT-10 (8-9)
20140702
100%
50%
100%
25%
50%
50%
Very fine gray sand and CCR mixture, dry
Very fine gray SAND and CCR mixture, saturated
Very fine gray SAND and CCR mixture, saturated
Gray coarse SAND and CCR mixture, saturated
Fine to medium tan SAND (SP) transitioning to
brown, saturated
Fine to medium tan SAND (SP), saturated
07/02/14
Rachel Donahue
SAEDACCO
Will Keyes
24
197915.9
2305065.0
13.2
F-DPT-10
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"
0
-5
-10
-15
-20
15
10
5
0
-5
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
Collected SS-F-DPT-11 (7-8)
20140702 (sumbitted)
Collected SS-F-DPT-11 (7-8)
20140702 (submitted)
100%
50%
50%
50%
50%
Fine orange to gray SAND and CCR mixture
fine orange SAND and CCR mixture, damp
fine orange SAND and CCR mixture, saturated
Medium brown SAND (SP), saturated
Medium brown SAND (SP), saturated, trace black
specks
07/02/14
Rachel Donahue
SAEDACCO
Will Keyes
20
197706.3
2305633.3
15.0
F-DPT-11
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"
0
-5
-10
-15
-20
10
5
0
-5
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
No samples collected during
drilling
100%
25%
50%
50%
75%
Dark brown silty SAND (SM), topsoil
Fine tan SAND (SP)
Fine orange SAND (SP)
Fine orange SAND (SP), moist
Fine tan SAND (SP), saturated, trace black
specks
07/02/14
Rachel Donahue
SAEDACCO
Will Keyes
20
197519.4
2305959.0
11.4
F-DPT-12
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"
0
-5
-10
5
0
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
No samples collected during
drilling
50%
50%
20%
Possible CCRsMedium tan and brown SAND (SP) with some
staining, moist
Medium brown SAND (SP) transitioning to tan
SAND (SP) with depth, saturated
Medium tan SAND (SP), saturated
07/02/14
Rachel Donahue
SAEDACCO
Will Keyes
12
196602.1
2306104.6
7.5
F-DPT-13
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"
0
-5
-10
-15
-20
10
5
0
-5
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
Collected SS-F-DPT-14 (3-4)
20140702 (submitted)
Collected SS-F-DPT-14 (7-8)
20140702 (submitted)
100%
50%
50%
50%
50%
CCRs
CCRs, saturated
Coarse gray SAND and CCR mixture, saturated
Medium dark brown SAND (SP), saturated
Medium gray SAND (SP), transitioning to dark
gray SAND (SP) with depth, saturated
07/02/14
Rachel Donahue
SAEDACCO
Will Keyes
20
197495.7
2305270.0
12.5
F-DPT-14
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"
0
-5
-10
-15
5
0
-5
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Plant
Well Construction Details
NAVD88)
No samples collected during
drilling
100%
75%
75%
75%
Fine gray SAND and CCR mixture
Coarse gray SAND and CCR mixture, saturated
Medium tan SAND (SP), saturated
Dark brown and black coarse SAND and CCR
mixture, iridescent sheen, saturated
Medium brown SAND (SP), transitioning to tan
SAND (SP), saturated
07/02/14
Rachel Donahue
SAEDACCO
Will Keyes
16
196723.8
2305805.9
7.3
F-DPT-15
Direct Push Technology
Geoprobe 7822DT
Direct Push Technology
2"

APPENDIX 3.A1

Boring Logs
Legend for Soil Classification Symbols
Pattern Description

SP – poorly graded sands

SW – well graded sands

GP – poorly graded gravels
GW – well graded gravels
SM – silty sands

SP-SM – poorly graded sand with silt

SP-SC – poorly graded sand with clay

MH – elastic silts

ML – inorganic silts with low plasticity

SC – clayey sands

CL – lean clays

CH – fat clays

OH – organic clays of high plasticity

OL – organic clays of low plasticity

Ash

30
25
20
15
10
5
0
-5
-10
-15
-20
-25
-30
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 1 of 2
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
sandy SILT (ML) (Ash); gray; moist
sandy SILT (ML) (Ash); gray; moist
SILT with sand (top 1.4' sandier) (ML) (Ash); gray
(occasional black); moist to wet
Top 0.3': SILT (ML) (Ash); gray; moist to wet
Middle 2.2': Sand with silt (SP-SM) (Possible
Ash); brown; moist
Bottom 0.4': SILT with sand (ML) (Ash & Possible
Soil); gray; moist
sandy SILT (ML) (Ash & Possible Soil);
gray/brown; moist
SILT with sand (ML) (Ash); gray/brown/black; wet
SILT with sand (ML) (Ash); gray/black; wet
Top 1.5': SILT with sand (ML) (Ash); gray/black;
wet
Bottom 2.5': fine to medium SAND with silt (SP-
SM) (Soil); brown; wet
3.5'
3.1'
3.2'
2.9'
3'
4'
0.8'
4'
Sample Collected (12.3' - 14.5')
Sample Collected (28' - 28.9')
7/2/2014
Michael Martin
36 ft
197980.6
2305972.0
33.3 ft (NAVD88)
GP-07 (within the 1971 Pond)
Dual Tube
0
-35
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 2 of 2
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
fine to medium SAND (SP) (Soil); brown; wet 4'
Boring Terminated at 36 ft
7/2/2014
Michael Martin
36 ft
197980.6
2305972.0
33.3 ft (NAVD88)
GP-07 (within the 1971 Pond)
Dual Tube
30
25
20
15
10
5
0
-5
-10
-15
-20
-25
-30
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
SILT (ML) (Ash); gray; moist; occasional organic
matter
SILT with fine sand (ML) (Ash); gray; moist;
occasional roots at top 0.3'
SILT with fine sand (ML) (Ash); gray (occasional
black); moist
SILT with fine sand (ML) (Ash); gray/black
(occasional dark tan); moist (wet at middle 0.3 ft)
SILT (ML) (Ash); gray; wet
SILT (ML) (Ash); gray/dark tan (occasional black);
wet
Top 2': SILT (ML) (Ash); gray (occasional black);
wet
Bottom 2': fine to medium SAND (SP) (Soil);
gray/brown/white; wet
fine to medium SAND (SP) (Soil); brown/white;
wet
2.5'
2.6'
4'
3'
4'
4'
4'
2.5'
Start using water
Boring Terminated at 32 ft
6/26/2014
Michael Patinkin
32 ft
198603.9
2304725.8
32.6 ft (NAVD88)
GP-08 (within the 1971 Pond)
Dual Tube
30
25
20
15
10
5
0
-5
-10
-15
-20
-25
-30
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 1 of 2
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
Top 1.0': Top Soil (SP) (Soil); brown; dry;
occasional gravels
Bottom 3.0': SILT (ML) (Ash); gray; moist
SILT (ML) (Ash); gray; moist
SILT (ML) (Ash); gray; moist
SILT (ML) (Ash); gray; moist
SILT (ML) (Ash); gray; moist to wet; occasional
wood chips and roots
sandy SILT (ML) (Ash); gray/black/dark tan; wet
Top 2.5': SILT (ML) (Ash); dark tan (occasional
black); wet
Bottom 1.5': sandy SILT (ML) (Ash); gray/black;
wet; occasional wood chips
SILT with sand (ML) (Ash); gray/dark tan/black;
wet
4'
3.5'
3.0'
3.3'
2.5'
4'
4'
3.3'
6/26/2014
Michael Patinkin
40 ft
198963.0
2304385.6
34.1 ft (NAVD88)
GP-09 (within the 1971 Pond)
Dual Tube
0
-5
-35
-40
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 2 of 2
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
Top 2.0': SILT (ML) (Ash); gray/black/dark tan;
wet
Middle 0.5': organic CLAY (OL) (Soil); gray to
black; moist
Bottom 1.5': fine to medium SAND (SP) (Soil);
brown; wet
fine to medium SAND with silt (SP-SM) (Soil);
white/brown; wet
4'
2.3'
Sample Collected
Start using water
Boring Terminated at 40 ft
6/26/2014
Michael Patinkin
40 ft
198963.0
2304385.6
34.1 ft (NAVD88)
GP-09 (within the 1971 Pond)
Dual Tube
20
15
10
5
0
0
-5
-10
-15
-20
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
SILT with fine sand (ML) (Ash); gray; moist to wet;
occasional organic matter at top 0.3'
SILT (ML) (Ash); trace fine sand; gray/tan; moist
to wet
SILT (ML) (Ash); trace fine sand; gray/dark tan;
wet (moist at top 1')
SILT with fine sand (ML) (Ash); gray/black/dark
tan; wet; occasional roots at bottom 0.3'
Top 2': silty SAND (SM) (Ash); gray; wet
Bottom 1.5': fine to medium SAND (SP) (Soil);
gray/white; wet
fine to medium SAND (SP) (Soil); white/brown;
wet
2.5'
3'
4'
4'
3.5'
3'
Start using water
Boring Terminated at 24 ft
6/26/2014
Michael Patinkin
24 ft
199091.6
2304846.3
23.4 ft (NAVD88)
GP-10 (within the 1971 Pond)
Dual Tube
20
15
10
5
0
-5
-10
-15
-20
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
Top 1.5': silty SAND (SM) (Ash); gray; moist;
occasional organic matter
Bottom 1.0': sandy SILT (ML) (Ash); gray; moist to
wet
Top 1.5': silty SAND (SM) (Ash); gray; moist to
wet
Bottom 1.0': SILT with fine sand (ML) (Ash);
gray/black; wet
SILT with fine sand (ML) (Ash); gray/dark
tan/black; wet
SILT with fine sand (sandier at bottom 1 ft) (ML)
(Ash); gray/dark tan/black; wet
Top 2.7': SILT (ML) (Ash); gray/dark tan; wet;
occasional organic matter
Bottom 0.6': fine to medium SAND (SP) (Soil);
white/gray; wet
fine to medium SAND (SP) (Soil);
white/gray/brown; wet
2.5'
2.5'
2.5'
3'
3.3'
2.5'
Sample Collected
Start using water
Boring Terminated at 24 ft
6/26/2014
Michael Patinkin
24 ft
199364.0
2304729.4
24.6 ft (NAVD88)
GP-11 (within the 1971 Pond)
Dual Tube
40
35
30
25
20
15
0
-5
-10
-15
-20
-25
-30
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 1 of 2
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
SILT with fine sand (ML) (Ash); gray; moist
SILT (ML) (Ash); trace fine sand; gray; moist
SILT (ML) (Ash); trace fine sand; gray; moist (top
1' wet)
SILT with sand (ML) (Ash); gray; moist;
occasional organic matter
SILT with sand (ML) (Ash); gray/tan; moist
(occasionally wet)
Top 1.0': SILT (ML) (Ash); gray; wet
Bottom 1.8': sandy SILT (ML) (Ash); gray; moist
(occasionally wet)
SILT (with fine sand at top 1.5') (ML) (Ash);
gray/dark tan; wet (top 1' moist); occasional
organic matter
SILT with fine sand (ML) (Ash); dark
tan/gray/black; wet
3.2'
2.7'
2.3'
3.1'
2.8'
2.8'
4'
4'Sample Collected
Environmental Sample: SS-GP12 (28-32)-20140702
7/2/2014
Michael Martin
40 ft
199302.5
2305001.6
41.5 ft (NAVD88)
GP-12 (within the 1971 Pond)
Dual Tube
10
5
-35
-40
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 2 of 2
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
Top 2.5': SILT (ML) (Ash); dark tan/gray/black;
wet
Bottom 1.0': fine to medium SAND (SP) (Soil);
gray/white; wet
fine to medium SAND (SP) (Soil); gray; wet
3.5'
1.8'
Boring Terminated at 40 ft
7/2/2014
Michael Martin
40 ft
199302.5
2305001.6
41.5 ft (NAVD88)
GP-12 (within the 1971 Pond)
Dual Tube
40
35
30
25
20
15
10
0
-5
-10
-15
-20
-25
-30
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 1 of 3
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
SILT (ML) (Ash); gray; moist
SILT (ML) (Ash); gray; moist
SILT with fine sand (top 1' sandier) (ML) (Ash);
gray/brown; moist
SILT (ML) (Ash); gray; moist to wet; occasional
organic matter
SILT with fine sand (ML) (Ash); black/gray; moist
(bottom 0.7' wet); occasional wood chips
sandy SILT (ML) (Ash); gray; moist (occasionally
wet); occasional organic matter
SILT with sand (ML) (Ash); dark tan; wet; 0.4' of
sand at 25' bgs
SILT with fine sand (ML) (Ash); dark
tan/black/gray; wet
3.5'
3.2'
2.5'
3.4'
3.1'
2.7'
4'
4'
6/30/2014 to 7/1/2014
Michael Martin
80 ft
199150.5
2305092.7
40.0 ft (NAVD88)
GP-13 (within the 1971 Pond)
Dual Tube
5
0
-5
-10
-15
-20
-35
-40
-45
-50
-55
-60
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 2 of 3
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
SILT with fine sand (ML) (Ash); dark tan/black;
wet
SILT with fine sand (ML) (Ash); dark tan/black;
wet
No Recovery
SILT (with fine sand at top 1') (ML) (Ash); dark
tan/black; wet
SILT with fine sand (ML) (Ash); dark
tan/black/gray; wet
No Recovery
SILT (ML) (Ash); dark tan; wet
No Recovery
4'
4'
NR
3.5'
2'
NR
3.7'
NR
Clean out the borehole with water
Resume boring on 7/1/2014
Sample Collected
6/30/2014 to 7/1/2014
Michael Martin
80 ft
199150.5
2305092.7
40.0 ft (NAVD88)
GP-13 (within the 1971 Pond)
Dual Tube
-25
-30
-35
-40
-65
-70
-75
-80
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 3 of 3
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
SILT with fine sand (ML) (Ash); dark tan; wet
SILT with fine sand (ML) (Ash); dark tan; wet
No Recovery
No Recovery
3.3'
4'
NR
NR
Sample Collected; NP
Environmental Sample: SS-GP13 (64-68)-20140701
Sample Collected; NP
Environmental Sample: SS-GP13 (68-72)-20140701
Trace sand (soil) is observed in the annulus between the sampler
and outer casing
Boring Terminated at 80 ft
6/30/2014 to 7/1/2014
Michael Martin
80 ft
199150.5
2305092.7
40.0 ft (NAVD88)
GP-13 (within the 1971 Pond)
Dual Tube
45
40
35
30
25
20
15
0
-5
-10
-15
-20
-25
-30
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 1 of 3
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
SILT with fine to medium sand (ML) (Ash); gray;
moist
SILT with fine sand (ML) (Ash); gray ; moist
sandy SILT (ML) (Ash); gray/brown; moist
SILT with fine to medium sand (ML) (Ash); gray
(occasionally brown); moist
SILT with fine sand (ML) (Ash); gray/brown/black;
moist
SILT with fine to medium sand (ML) (Ash);
gray/black; wet
SILT with fine sand (ML) (Ash); gray/black/dark
tan; wet
SILT with fine sand (ML) (Ash & Soil); dark
tan/gray/black; wet; soil mix at bottom 0.7'
3.4'
3'
3.5'
3.3'
3'
4'
4'
3.5'
7/2/2014
Michael Martin
84 ft
198621.2
2305747.4
45.2 ft (NAVD88)
GP-14 (within the 1971 Pond)
Dual Tube
10
5
0
-5
-10
-15
-35
-40
-45
-50
-55
-60
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 2 of 3
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
sandy SILT (ML) (Ash & Possible Soil);
gray/brown/black; wet; soil mix at middle 0.7'
sandy SILT (ML) (Ash & Possible Soil);
gray/black; wet
SILT with fine sand (ML) (Ash); dark
tan/gray/black; wet
sandy SILT (ML) (Ash); black/gray; wet
Top 1.0': medium SAND (SP) (Possible Soil);
brown/black; wet
Bottom 3.0': SILT with fine sand (ML) (Ash);
gray/black/dark tan; wet
sandy SILT (ML) (Ash); gray; wet
No Recovery
SILT (ML) (Ash); dark tan/black; wet
3.5'
3.6'
3.8'
3.7'
4'
0.6'
NR
4'
Sample Collected (48'-49')
Sample Collected (60'-62')
Environmental Sample: SS-GP14 (60-62)-20140702
7/2/2014
Michael Martin
84 ft
198621.2
2305747.4
45.2 ft (NAVD88)
GP-14 (within the 1971 Pond)
Dual Tube
-20
-25
-30
-35
-65
-70
-75
-80
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 3 of 3
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
No Recovery
SILT (ML) (Ash); dark tan/black; wet
SILT (ML) (Ash); dark tan; wet
Top 2.8': SILT (ML) (Ash); dark tan/black; wet
Bottom 1': sandy SILT (ML) (Soil); gray; wet
No Recovery
NR
4'
3.5'
3.8'
NR
Sample Collected; NP
Environmental Sample: SS-GP14 (68-72)-20140702
Sample Collected (74.5'-75.5'); NP
Clean out the borehole with water
Trace sand (soil) is observed in the annulus between the sampler
and outer casing
Boring Terminated at 84 ft
7/2/2014
Michael Martin
84 ft
198621.2
2305747.4
45.2 ft (NAVD88)
GP-14 (within the 1971 Pond)
Dual Tube
40
35
30
25
20
15
0
-5
-10
-15
-20
-25
-30
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 1 of 3
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
SILT with fine to medium sand (ML) (Ash); gray;
moist
SILT with fine to medium sand (ML) (Ash); gray;
moist
SILT with fine to medium sand (ML) (Ash); gray;
moist
SILT with fine to medium sand (ML) (Ash);
gray/black; moist
SILT with fine sand (ML) (Ash); gray/black; moist
SILT with fine sand (ML) (Ash); gray/black; moist
(bottom 0.9' wet)
SILT with fine sand (ML) (Ash); black/gray/dark
tan; wet
sandy SILT (ML) (Ash); black/gray/dark tan; wet
3'
0.5'
2.8'
2.8'
3.1'
3.9'
3.3'
4'
7/1/2014
Michael Martin
84 ft
198295.2
2305863.3
43.9 ft (NAVD88)
GP-15 (within the 1971 Pond)
Dual Tube
10
5
0
-5
-10
-15
-35
-40
-45
-50
-55
-60
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 2 of 3
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
Top 2.0': SILT (ML) (Ash); dark tan/black; wet
Bottom 1.5': fine to medium SAND (SP) (Possible
Soil); gray; wet
SILT with fine sand (ML) (Ash (possible soil mix at
bottom)); black/dark tan/gray; wet
sandy SILT (ML) (Ash); dark tan/black; wet
sandy SILT (ML) (Ash & Possible Soil); dark
tan/black/brown; wet
sandy SILT (ML) (Ash); dark tan/black; wet
SILT with fine sand (ML) (Ash); dark tan/black;
wet
SILT with fine sand (ML) (Ash); dark tan/black;
wet
SILT (ML) (Ash); dark tan; wet
3.5'
3.8'
3.5'
2.5'
3.6'
3.8'
1.5'
3.5'
Sample Collected
Sample Collected
Sample Collected; NP
Environmental Sample: SS-GP15 (60-64)-20140701
7/1/2014
Michael Martin
84 ft
198295.2
2305863.3
43.9 ft (NAVD88)
GP-15 (within the 1971 Pond)
Dual Tube
-20
-25
-30
-35
-40
-65
-70
-75
-80
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 3 of 3
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
SILT (ML) (Ash); dark tan (occasionally black);
wet
SILT with sand (ML) (Ash); gray/dark tan/black;
wet
SILT with sand (ML) (Ash); gray/black; wet
Top 3.6': SILT with sand (ML) (Ash); dark
tan/black; wet
Bottom 0.2': fine to medium SAND (SP) (Soil);
brown; wet
fine to medium SAND (SP) (Soil); brown; wet
3'
2.7'
1.7'
3.8'
1.1'
Sample Collected (68.7'-70.7')
Environmental Sample: SS-GP15 (68.7-70.7)-20140701
Boring Terminated at 84 ft
7/1/2014
Michael Martin
84 ft
198295.2
2305863.3
43.9 ft (NAVD88)
GP-15 (within the 1971 Pond)
Dual Tube
30
25
0
-5
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
Top 2.2': SILT (ML) (Ash); gray; moist
Bottom 1.3': fine to medium SAND (SP) (Soil);
brown; moist
fine to medium SAND (SP) (Soil); brown; moist
3.5'
2.5'
Boring Terminated at 8 ft
6/30/2014
Weston Shin
8 ft
199205.8
2305534.9
31.6 ft (NAVD88)
GP-16 (within the 1971 Pond)
Dual Tube
30
25
20
0
-5
-10
-15
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
SILT (ML) (Ash); trace fine sand; gray; moist
SILT with fine sand (ML) (Ash); gray; moist
Top 0.4': SILT (ML) (Ash); trace fine sand; gray;
moist
Bottom 2.4': fine to medium SAND (SP) (Soil);
brown; moist
fine to medium SAND (SP) (Soil); brown/white;
moist
2.5'
2.7'
2.8'
3.2'
Boring Terminated at 16 ft
6/30/2014
Weston Shin
16 ft
199203.7
2305516.8
31.6 ft (NAVD88)
GP-16A (within the 1971 Pond)
Dual Tube
30
25
20
15
10
5
0
-5
-10
-15
-20
-25
-30
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 1 of 2
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
Top 1': fine to medium SAND (SP) (Road Fill
Material); gray; dry
Bottom 3': fine to medium SAND (SP) (Soil);
brown; moist
fine to medium SAND (SP) (Soil); brown; moist
fine to medium SAND (SP) (Soil);
brown/white/black; moist
fine to medium SAND (SP) (Soil); brown/gray;
moist to wet
fine to medium SAND (SP) (Soil);
brown/white/gray; wet
fine to medium SAND (SP) (Soil); brown; wet
fine to medium SAND (SP) (Soil); white/brown;
wet
fine to medium SAND (SP) (Soil); white
(occasional orange); wet
4'
4'
4'
4'
4'
3.5'
4'
4'
6/27/2014, 6/30/2014
M. Patinkin, W. Shin
60 ft
199099.6
2305644.4
32.5 ft (NAVD88)
GP-17 (on the 1971 Pond Dike)
Dual Tube/Macro Core
0
-5
-10
-15
-20
-25
-35
-40
-45
-50
-55
-60
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 2 of 2
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
fine to medium SAND (SP) (Soil); white; wet
fine to medium SAND (SP) (Soil); white/brown;
wet
Top 0.3': fine to medium SAND (SP) (Soil); brown;
wet; occasional wood chips
Bottom 0.7': organic CLAY (OH) (Soil); gray; moist
Top 3': organic CLAY (OH) (Soil); dark brown;
moist; abundant wood chips; top 1.3' cave-in
Bottom 1': fat CLAY (CH) (Soil); gray; moist;
abundant wood chips
fat CLAY (CH) (Soil); gray; moist; occasional
wood chips
silty fine to medium SAND (SM) (Soil); gray; wet;
occasional wood chips
silty CLAY to clayey SILT (CL-ML) (Soil); gray;
wet
4'
2'
1'
2.7'
4'
4'
3.2'
Start using water
Switch to Macro Core
Sample Collected; Bottom - LL=85, PL=40, PI=45
Resume drilling on 6/30/14; Switch to Dual Tube
Sample Collected; Top - LL=126, PL=60, PI=66; Bottom - LL=67,
PL=31, PI=36
Sample Collected; LL=50, PL=24, PI=26
Sample Collected; 0.1% Gravel, 58.8% Sand, 24.7% Silt, 16.4 Clay;
NP
Sample Collected; 44.4% Sand, 33.8% Silt, 21.8% Clay; LL=26,
PL=22, PI=4
Boring Terminated at 60 ft
6/27/2014, 6/30/2014
M. Patinkin, W. Shin
60 ft
199099.6
2305644.4
32.5 ft (NAVD88)
GP-17 (on the 1971 Pond Dike)
Dual Tube/Macro Core
20
15
10
5
0
-15
-20
-25
-30
-35
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 1 of 1
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
SILT with fine sand (ML) (Ash); gray; moist (wet in
the middle 0.3')
SILT with fine sand (ML) (Ash); gray (occasional
black); wet
SILT (with fine sand at the bottom 0.3') (ML)
(Ash); dark tan (black/dark tan at the bottom); wet
SILT (with fine sand at the bottom 0.5') (ML)
(Ash); dark tan/gray/black; wet; scattered wood
chips
Top 1': sandy SILT (ML) (Ash); dark
tan/gray/black; wet
Bottom 1': fine to medium SAND (SP) (Soil);
white; wet
fine to medium SAND (SP) (Soil); gray/white; wet
2.6'
4'
4'
4'
2'
3'
Start drilling from access path and skip sampling top 12 ft
Sample Collected
Boring Terminated at 36 ft
6/25/2014
Weston Shin
36 ft
198663.1
2304987.5
35.6 ft (NAVD88)
MB-1 (within the 1971 Pond)
Dual Tube
30
25
20
15
10
5
-15
-20
-25
-30
-35
-40
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 1 of 3
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
SILT with fine sand (ML) (Ash); gray; moist
SILT with fine sand (ML) (Ash); black/gray; moist
SILT (with fine sand at top 1 ft) (ML) (Ash); gray;
wet (moist at top 1 ft)
SILT (with fine sand at bottom 0.2 ft) (ML) (Ash);
gray; wet
SILT with fine sand (ML) (Ash); dark
tan/black/gray; wet
SILT with fine sand (ML) (Ash); dark
tan/black/gray; wet
silty SAND (SM) (Ash); black/dark tan/gray; wet
Top 2.5 ft: silty SAND (SM) (Ash); black; wet
Bottom 1.5': SILT with fine sand (ML) (Ash); dark
tan/black; wet
2.5'
3'
4'
4'
4'
4'
4'
4'
Start drilling from access path and skip sampling top 12 ft
6/25/2014
Michael Patinkin
84 ft
198526.3
2305458.9
44.6 ft (NAVD88)
MB-2 (within the 1971 Pond)
Dual Tube
0
-5
-10
-15
-20
-25
-45
-50
-55
-60
-65
-70
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 2 of 3
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
SILT (ML) (Ash); dark tan (occasional black); wet
No Recovery
SILT (ML) (Ash); dark tan (occasional black/gray);
wet; occasional gravel
No Recovery
SILT with fine sand (ML) (Ash); dark tan
(occasional black/gray); wet
SILT (ML) (Ash); dark tan (occasional black/gray);
wet
No Recovery
No Recovery
4'
NR
4'
NR
4'
4'
NR
NR
Sample Collected; NP
Environmental Sample: SS-MB2 (64.0-68.0)-20140625
6/25/2014
Michael Patinkin
84 ft
198526.3
2305458.9
44.6 ft (NAVD88)
MB-2 (within the 1971 Pond)
Dual Tube
-30
-35
-75
-80
SAMPLING METHOD:
All depths referenced to ground surface.
1300 South Mint Street
Charlotte, NC 28203
BORING LOG
GENERAL INFORMATION TECHNICAL INFORMATION
PROJECT NAME:
PROJECT NO:
BORING DATE:
GEOSYNTEC REPRESENTATIVE:
DRILLING CONTRACTOR:
DRILLER NAME:
DRILLING METHOD:
RIG TYPE:
BOREHOLE DIA:
Elev.Lithologic Description
SITE LOCATION:
Total Depth:
Pa
t
t
e
r
n
(ft)
Page 3 of 3
GC5592
Wilmington, North Carolina
BOREHOLE ID:
NORTHING:
EASTING:
GROUND ELEVATION:
Depth
(ft)
Re
c
o
v
e
r
y
Comments
Suite 110
L.V. Sutton Steam Electric Plant
Mid-Atlantic Drilling
Mike Small
Direct Push
6600 Track Rig (Serial # 99103P66)
2.25"
SILT (ML) (Ash); dark tan (occasional black/gray);
wet; occasional gravel
fine to medium SAND with silt (SP-SM) (Soil);
gray; wet
3.5'
2.5'
Sample Collected; NP
Environmental Sample: SS-MB2 (76.0-80.0)-20140625
Clean out the borehole with water
Boring Terminated at 84 ft
6/25/2014
Michael Patinkin
84 ft
198526.3
2305458.9
44.6 ft (NAVD88)
MB-2 (within the 1971 Pond)
Dual Tube

APPENDIX 3.A2

Geotechnical Laboratory Test Results
Excel Geotechnical Testing, Inc. Test Results Summary
"Excellence in 'resting"
953 Forrest Street, Roswell, Georgia 30075 Project [Name. Duke Sutton Closure
sT e
Tel: [phone] Fax: [phone]
Project No.: 647
Sample inrormation
Test Information
Site
ID
Lab
No.
Moisture
Content
ASFM
D2216
Grain Sire Analysis
ASTM D 422
Gravel Sand Fines Silt Clay
Content Content Cooteot Content Content
Atterberg Limits
ASTM D 4318
Engineering
Clamification
ASTM
D2487
Remarks
Ill.
PL
Pi
GP-13, S-17 (64-68')
14G002
NP
NP
NP
GP-13, S-18 (68-72)
14GO03
NP
NP
NP
GP-14, S-18 (68-72)
14GO04
NP
NP
NP
GP-14, S-19 (74.5-75.5)
14GO05
NP
NP
NP
OP-15, S-16 (60-64)
14GO06
NP
NP
NP
GP-17, S-11 (43.344')
14GO07
85
40
45
GP-17, S-12 (4445.7')
14GO08
126
60
66
GP-17, S-12 (45.746J)
14GO09
67
31
36
GP-17, S-13 (48-52')
14GO10
50
24
26
GP-17, S-14 (52-56)
14G011
0.1
58.8
41.1
24.7
16.4
NP
NP
NP
SM
GP-17, S-15 (56-6U)
14GO12
0
44.4
55.6
33.8
21.8
26
22
4
CIrML
MB-2, S-14 (64-68)
14GO13
NP
NP
NP
1R-2, S-17 (76-803
140014
NP
NP
NP
Notes:

[EG Excel Geotechnical Testing} inc. Project Name: Duke Sutton Closure
"Excellence in Testing" Project No: 647
953 Forrest Street, Roswell, Georgia 30075 Client Sample Wi GP-17, S-14 (52-56)
Tel: [phone] Fax: [phone]
Lab Sample No: 140011
ASTM c:, Q 422, n aW, SAIL INDEX PROPERTIES c�- 5 ors„f>, Moro. CWu
D 1140„ Q 2E16, Q Ei67, D•t318 E°R. Ctassi �cario°, Ancrbeg Limits
U.S. Standard Sieve Sizes and Numbers
12" 3" 2" 1.5' 1'314" 112"3I8" #4 #10 #20 #Nn #50 #10
0
tt2U4
100
90
80
70
60
> 50
4' 40
E
i
I
3
I
30
20
1 o - -�
0
1000 100 10 1 0.1 0.01 0.001 0.0001
Grain Size ( min)
;0
70
'U' Line
LL
OH
r�
=' nc
� 40
30
O
MH or OH
0 L°rOL
4 10 20 30 40 50 60 70 80 90 100 1I0 120
Liquid Limit { LL ]
Coeff. Unit (Cu}:Nd
Specific Gravity (-): 2.7f7 Coetf. Cure. (Ce):
Note(s): Engineering classification is based on the assumption that the fines are either W or MH.
An assumed specific gravity of 2.70 was used when analyzing the hydrometer test results.
Sieve No.
Clay
60
0.0054 16.6 y p CH or
D.aoz7 14.7 "A' Li
20 CL or
Sand
lD
'-
Caarse
pine
Coarse
Medium
Fine
Silt
Sire {mm)
°l4 Finer
3"
75
1fl4.0
2"
SD
]00.0
i.5"
37.5
1DQ0
1"
25
iD0.0
3J4"
19
1DD.4
318"
9.5
100.4
#4
4.75
49.9
ale
z.D4
99.s
#2o
D.ssD
99,7
q44
a.4zs
99.z
#6D
4250
94.9
#1D0
4.150
71.5
#24o
D.o7s
41.1
Hydrometer
Particle Diameter
mm
°Io Finer
4,0257
25.4
O.O107
1$,3
Gravel (°i }:
0.1
Client
Sample
Lab
Sample
Moisture
Content
Fines Content
�1+Io.200
Atterberg Limits
Engineering Classification
LI_.
Ply
PI
GP-17, 5-14 {52-56)
14G011
32.I
41.1
TdP
IVP
NP
SM -Silty Sand

Excel Gevtechnical Testing, Inc. Project Name: Duke Sutton Closure
G t T"Excellence in 'resting" Project No: 647
953 Forrest Street, Roswell, Georgia 30076 Client Sample ID: GP-17, S-I5 (56-60)
Tel: [phone] Fax: [phone] Lab Sample No: 14G012
D 1140, D 2216 D 2487DD -1318 SOIL INDEX. PROPERTIES �°854, �� c� as"n °� Co.[,
s CDC Fine C°arse Medium Fine Silt Clay
Cobbles
mGraveI Sand Fines
U.S. Standard Sieve Sizes and Numbers
12" 3" 2" P.5. 11314' 112'318' 114 tPlo *211 K4o "11 1100 112011
00
190
a80
to
70 f
60 !
,> 50
a 40 - -
30 ----- i
40
d
a 20 �M
10 -- '
0
1000 100 10 1 0.1 0.01 0.001 0.0001
Grain Size (mm )
70
"U"' Line
60
p CH or OH
SU
k
5 40
4
'y
ca
'a
20 CL or O Mli or OH
1Q
Q n OL
0 10 20 30 40 50 60 70 80 90 100 110 120
Liquid Limit ( LL }
CaefL Uuif. (Cu}:
Specific Gravity (-}: 2.74 C.ff. Cur,. (Ce}:IM
Note(s): An assumed specific gravity of 2.70 was used when analyzing the hydrometer test results.
Sieve No. Size
30
$0
'A' Line
(mm)
%Finer
3"
7S
1 Q0.4
2"
SD
140.4
LS"
37.5
1DD.4
1'"
25
140.4
3ia"
19
laO.Q
318"
9.5
140.D
#a
4.7s
laD.a
Hydrometer
Particle Diameter %Finer
mm
4.4237 33.9
0.410Q 24.2
Q.DQ52 21.9
4.DD26 20.6
4.D011 1b.7
Gravel (%);
Gravel (%);
Sand (°!°):
44.4
Silt (°lo}:
33.8
Clay
Client
Sample
Lab
Sample
Moisture
Content
Fines Content
e No. 200
Atterherg Limits
Engineering Classification
LL
PL
P[
GP-17, 5-15 (55-60)
14G01.2
34.6
55.6
26
22
4
CIrML. -Sandy Silty Clay

APPENDIX 3.A3

Photographic Record

GEOSYNTEC CONSULTANTS
Photographic Record
Client: Duke Energy Project Number: GC5592/05
Project Name: L.V. Sutton Conceptual Pond Closure Site Location: Wilmington, NC
Photograph 1

Date:
06/25/2014

Direction:
Not Applicable

Comments:
CCR Material with Dark
Tan Color Collected from
MB-2 (Depth from 64 to
68 ft below Ground
Surface)
Photograph 2

Date:
06/25/2014

Direction:
South

Comments:
Access Path Constructed
for MB-1

GEOSYNTEC CONSULTANTS
Photographic Record
Client: Duke Energy Project Number: GC5592/05
Project Name: L.V. Sutton Conceptual Pond Closure Site Location: Wilmington, NC
Photograph 3

Date:
06/26/2014
Direction:
Not Applicable

Comments:
Soil Sample Collected
from GP-10 (Depth from
20 to 24 ft below Ground
Surface)
Photograph 4

Date:
06/30/2014

Direction:
Southwest
Comments:
6600 Track-Mounted
Geoprobe Rig (at GP-17)

GEOSYNTEC CONSULTANTS
Photographic Record
Client: Duke Energy Project Number: GC5592/05
Project Name: L.V. Sutton Conceptual Pond Closure Site Location: Wilmington, NC
Photograph 5

Date:
06/30/2014
Direction:
Not Applicable

Comments:
Soil Sample Collected
from GP-17 (Depth from
48 to 52 ft below Ground
Surface)
Photograph 6

Date:
07/02/2014
Direction:
Not Applicable

Comments:
CCR Material Collected
from GP-12 (Depth from
20 to 24 ft below Ground
Surface)