HomeMy WebLinkAboutNC0001422_Well Water Lab Results_20150805 (3)Environmental Chemists, Inc.
envirochem 6602 Windmill Way • Wilmington, NC 25405
(910) 392-0223 (Lab) • (910) 392-4424 (Fax)
SM
710 Bowsertown Road • Manteo, NC 27954
(252)473-5702
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DL$ CERTIFICATE #37729
Duke Energy -Laboratory
Date of Report: Apr 20, 2015
1339 Hagers Ferry Road/Bld 7405 MG03A2
Customer PO #:
Huntersville NC 28078
Customer ID: 15030001
Attention: Peggy Kendall
Report #: 2015-02737
Project ID: Ash Pond Investigation
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
15-06244 Site: Reg # 4055 Well # 2
3/5/2015
10:45 AM DW Ray Porter/Cindy McDonald
Test
Method
Results Date Analyzed
Bicarbonate as CaCO3
Bicarbonate as CaCO3
1 mg/L
03/19/2015
Carbonate as CaCO3
Carbonate as CaCO3
<1 mg/L
03/19/2015
Aluminum
EPA 200.7
0.070 mg/L
03/11/2015
Boron
EPA 200.7
0.25 mg/L
03/11/2015
Calcium
EPA 200.7
9.50 mg/L
03/12/2015
Iron
EPA 200.7
0.120 mg/L
03/11/2015
Magnesium
EPA 200.7
2.19 mg/L
03/12/2015
Potassium
EPA 200.7
1.79 mg/L
03/12/2015
Sodium
EPA 200.7
11.8 mg/L
03/12/2015
Strontium
EPA 200.7
0.133 mg/L
03/11/2015
Zinc
EPA 200.7
0.015 mg/L
03/11/2015
Antimony
EPA 200.8
<0.000099mg/L
03/10/2015
Arsenic
EPA 200.8
0.000293J mg/L
03/10/2015
J: Estimated. Between Method Detection Limit and Reporting Limit.
Barium
EPA 200.8
0.045 mg/L
03/10/2015
Beryllium
EPA 200.8
<0.000146mg/L
03/10/2015
Cadmium
EPA 200.8
<0.0000827mg/L
03/10/2015
Chromium
EPA 200.8
<0.000148mg/L
03/10/2015
Cobalt
EPA 200.8
0.004 mg/L
03/11/2015
Copper
EPA 200.8
0.008 mg/L
03/10/2015
Lead
EPA 200.8
0.000520 J mg/L
03/10/2015
J: Estimated. Between Method Detection Limit and Reporting Limit.
Manganese
EPA 200.8
0.142 mg/L
03/11/2015
Molybdenum
EPA 200.8
<0.0001 15 mg/L
03/10/2015
Nickel
EPA 200.3
< 0.100 mg/L
03/10/2015
Selenium
EPA 200.8
0.00059408 J mg/L
03/27/2015
J: Estimated. Between Method Detection Limit and Reporting Limit.
Report #:: 2015-02737 Page 1 of 2
00 7 1
gn:v7irochem'
ANALYTICAL & CONSULTING
CHEMISTS
Environmental Chemists, Inc.
Duke Energy -Laboratory
1339 Hagers Ferry Road/Bid 7405 MG03A2
Huntersville NC 28078
Attention: Peggy Kendall
6602 Windmill Way • Wilmington, NC 28405
(910)392-0223 (Lab) • (910) 392-4424 (Fax)
710 Bowsertown Road • Manteo, NC 27954
(252)473-5702
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Date of Report: Apr 20, 2015
Customer PO #:
Customer ID: 15030001
Report #: 2015-02737
Project ID: Ash Pond Investigation
Thallium
EPA 200.8
<0.0001 mg/L
03/10/2015
Vanadium
EPA 200.8
0.000236 J mg/L
03/11/2015
J: Estimated. Between Method Detection Limit and Reporting Limit.
SM 2540 C
85 mg/L
Hexavalent Chromium
EPA 218-7
<0.02 pg/L
03/09/2015
Mercury
EPA 245.1
<0.0004 mg/L
03/09/2015
Sulfate
EPA 300.0
33mg/L
03/11/2015
Turbidity
SM2130B
0.2NTU
03/06/2015
Field Turbidity 0.2 NTU.
Dissolved Oxygen
SM 4500 o G
4.10 mg/L
Alkalinity
SM 2320B
1 mg/L
03/13/2015
Conductivity
SM 2510 B
156 umho/cm
03/12/2015
Total Dissolved Solids (TDS)
SM 2540 C
85 mg/L
03/06/2015
Residue Suspended (TSS)
SM2540D
<2.5 mg/L
03/09/2015
Temperature
SM 2550 B
18.7 C
03/05/2015
Chloride
SM 4500 CI B
19 mg/L
03/12/2015
pH
SM4500H8
5.21 units
03/05/2015
Dissolved Oxygen
SM 4500 o G
4.10 mg/L
03/05/2015
Comment: Turbidity, temperature, pH and dissolved oxygen measured in field at sample collection. All non -
detects for metals
reported to MDL.
Reviewed by
Report #:: 2015-02737 Page 2 of 2
Environmental Chemists, Inc.
envirochem 6602 Windmill Way • Wilmington, NC 28405
(910)392-0223 (Lab) • (910) 392-4424 (Fax)
SM
710 Bowsertown Road • Manteo, NC 27954
(252)473-5702
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
QC for Duke Energy - 2015-02737
LCS
Parameter
True Value
m 2
Result
m
%True Value
Limits
Alkalinity
12.5
13
104
90-110
Aluminum
0.05
0.05
100
90-110
Antimony
0.01
0.01
100
90-110
Arsenic
0.01
0.01
100
90-110
Barium
0.01
0.01
100
90-110
Beryllium
0.01
0.01
100
90-110
Boron
0.05
0.05
100
90-110
Cadmium
0.01
0.01
100
90-110
Calcium
0.5
0.5
100
90-110
Chloride
50
48
96
90-110
Chromium
0.01
0.01
100
90-110
Cobalt
0.01
0.01
100
90-110
Conductivity
10000
99900
99.9
90/110
Copper
0.01
0.01
100
90-110
Iron
0.05
0.05
100
90-110
Lead
0.01
0.01
100
90-110
Magnesium
0.5
0.5
100
90-110
Manganese
0.01
0.01
100
90-110
Mercury
0.0040
0.0037
92
90-110
Molybdenum
0.01
0.01
100
90-110
Nickel
0.0050
0.0048
96
90-110
Potassium
0.5
0.5
100
90-110
TSS
248.8
274.4
110
90-110
Selenium
0.01
0.01
100
90-110
Sodium
0.5
0.5
100
90-110
Strontium
0.05
0.05
100
90-110
Sulfate
50
50
100
90-110
Thallium
0.0050
0.0048
96
90-110
TDS
600
601
100
f 10
Turbidity
N/A
N/A
N/A
N/A
Vanadium
0.01
0.01
100
90-110
Zinc
0.05
0.05
100
90-110
1/M. XYM
Parameter
True Value
mg/L
Result
mg/L
%
Recovery
%
Difference
Limits %
Recovery
Limits %
Difference
Alkalinity
N/A
N/A
N/A
N/A
N/A
N/A
Aluminum
0.100
0.099/0.100
99/100
1
80-120
<20
Antimony
0.025
0.028/0.028
112/112
0
80-120
<_ 20
Arsenic
0.025
0.030/0.030
120/120
0
80-120
<20
Barium
0.025
0.025/0.025
100/100
0
80-120
<_ 20
Beryllium
0.025
0.029/0.029
116/116
0
80-120
<20
Boron
0.100
0.097/0.095
97/95
2
80-120
<20
Cadmium
0.025
0.028/0.028
112/112
0
80-120
<20
Calcium
1.0
0.98/0.99
98/99
1
80-120
<20
Chloride
N/A
N/A
N/A
N/A
N/A
N/A
Chromium
0.025
0.024/0.025
96/100
4
80-120
<_ 20
Cobalt
0.025
0.024/0.025
96/100
4
80-120
<20
Conductivity
N/A
N/A
N/A
N/A
N/A
N/A
Copper
0.025
0.027/0.028
108/112
4
80-120
<_ 20
Iron
0.100
0.098/100
98/100
2
80-120
<20
Lead
0.025
0.023/0.023
92/92
0
80-120
<_ 20
Magnesium
1.0
0.98/1.0
98/100
2
80-120
<20
Manganese
0.025
0.024/0.025
96/100
4
80-120
<_ 20
Mercury
0.0020
0.0022/0.0019
110/95
15
80-120
<20
Molybdenum
0.025
0.028/0.028
112/112
0
80-120
<20
Nickel
0.0100
0.0099/0.0103
99/103
4
80-120
<_ 20
Potassium
1.0
1.0/1.0
100/100
0
80-120
<20
TSS
N/A
N/A
N/A
N/A
N/A
N/A
Selenium
0.025
0.030/0.030
120/120
0
80-120
<20
Sodium
1.0
1.0/1.0
100/100
0
80-120
<_ 20
Strontium
0.100
0.098/0.105
98/105
7
80-120
<_ 20
71TTVT WA'TV 4ZA1% PT.Ti.0
Parameter
10.0
10.5/10.6
105/106
1
80-120
<_ 20
0
0.0100
0.0102/0.0105
102/105
3
80-120
<_ 20
Antimony
N/A
N/A
N/A
N/A
N/A
N/A
MVanadium
N/A
N/A
N/A
N/A
N/A
N/A
N/A
0.025
0.024/0.025
96/100
4
80-120
<_20
N/A
0.100
0.099/0.102
99/102
3
80-120
20
71TTVT WA'TV 4ZA1% PT.Ti.0
Parameter
Results mg/L
% Difference
Limits
Alkalinity
36
36
0
<_ 10
Aluminum
N/A
N/A
N/A
N/A
Antimony
N/A
N/A
N/A
N/A
Arsenic
N/A
N/A
N/A
N/A
Barium
N/A
N/A
N/A
N/A
Beryllium
N/A
N/A
N/A
N/A
Boron
N/A
N/A
N/A
N/A
Cadmium
N/A
N/A
N/A
N/A
Calcium
N/A
N/A
N/A
N/A
Chloride
467
462
1
<10
Chromium
N/A
N/A
N/A
N/A
Cobalt
N/A
N/A
N/A
N/A
Conductivity
156
156
0
<_ 10
Copper
N/A
N/A
N/A
N/A
Iron
N/A
N/A
N/A
N/A
Lead
N/A
N/A
N/A
N/A
Magnesium
N/A
N/A
N/A
N/A
Manganese
N/A
N/A
N/A
N/A
Mercury
N/A
N/A
N/A
N/A
Molybdenum
N/A
N/A
N/A
N/A
NickelN/A
N/A
N/A
N/A
Potassium
N/A
N/A
N/A
N/A
TSS
313.3
303.3
3
<_ 10
Selenium
N/A
N/A
N/A
N/A
Sodium
N/A
N/A
N/A
N/A
Strontium
N/A
N/A
N/A
N/A
Sulfate
28
29
4
<10
Thallium
N/A
N/A
N/A
N/A
TDs
403
404
0
:510
Turbidity
0.37
0.37
0
<10
Vanadium
N/A
N/A
N/A
N/A
Zinc
N/A
N/A
N/A
N/A
BLANKS
Parameter
Rmg�'
Limit, mg/L
Alkalinity
1
1
Aluminum
<0.005
0.005
Antimony
<0.0005
0.0005
Arsenic
<0.0005
0.0005
Barium
<0.0005
0.0005
Beryllium
<0.0005
0.0005
Boron
<0.005
0.005
Cadmium
<0.0005
0.0005
Calcium
<0.5
0.5
Chloride
<2.5
2.5
Chromium
<0.0005
0.0005
Cobalt
<0.0005
0.0005
Conductivity
<5
5
Copper
<0.0005
0.0005
Iron
<0.005
0.005
Lead
<0.0005
0.0005
Magnesium
<0.5
0.5
Manganese
<0.0005
0.0005
Mercury
<0.0002
0.0002
Molybdenum
<0.0005
0.0005
Nickel
<0.00005
0.00005
Potassium
<0.5
0.5
TSS
<2.5
2.5
Selenium
<0.0005
0.0005
Sodium
<0.5
0.5
Strontium
<0.005
0.005
Sulfate
<2.5
2.5
Thallium
<0.00005
0.00005
TDS
<2.5
2.5
Turbidity
N/A
N/A
Vanadium
<0.0005
0.0005
Zinc
<0.005
0.005
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elementOne
Ray Porter
Environmental Chemists, Inc.
66002 Windmill Way
Wilmington, NC 28405
Sample #
Sample Matrix DW
Date Sampled 03/05/2015
Delivered by Client
Parameter
Chromium VI
Element One Inc.
6319-D Carolina Beach Rd.
Wilmington, NC 28412
Phone: 910 793-0128
Fax: 910 792-6853
ellab@ellab.com
FINAL REPORT OF ANALYSES
March 09, 2015
Client Project Name:
Client Project Number:
E1 Project Number e24189
Sample ID 15-06244
Sample Type Date Received 03/06/2015
Time Sampled 1045 Time Received 0810
Sampler Received by KMS
E1 Sample # 24189-5
Result Unit Dilution DL Method Date
< 0.02 pg/L 1 0.02 EPA 218.7 03/09/2015
Ken mith, Laboratory Director
24189 Envirochem Cr6+Report Compiled by �'w
NC Certifications: DW 37788 and DWQ DENR 604
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Facility Name: Environmental Chemists, Inc Permit# 94'
PLEASE CIRCLE METER USED FOR IDENTIFICATION PURPOSES
Meter Id: 11277 Meter Id: 11250 Meter Id: 09996 - Meter Id: NYI-11373 ---
Facility/Sample location
Time Sampled*
Time Analyzed+•
Temp (°C) ■ I
pH Result
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Comment
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►Indicates a recommended drift check (Use Buffer 7.0) Should be within 0.1 units of the buffeNs true value)
a Document the temperature of the sample at the time of analysis. Note: This temperature is not to be used for reporting on the monthly monitoring report
Calibration drift check is recommended when performing analysis at multiple sampling locations,
*All pH results in pH units (i.e., s.u.).
check standard's obtained true value)
Dissolved OMen (DO)
Reference Method: SM 4500 O G, 20th Edition, —YSI DO 550 A Model—YSI PRO 20
Temperature
°C
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*Analysis time and sampling time the same. (Ideally the sample should be analyzed m -situ):.
"Temperature Sewer Annual Check Date (550 A): INPROCESS Tempentnre Season Annual Check Date (PR020):IN PROCESS
Temperature
'=--. --- Reference Method: SM 2550 B 201h Edition
Facility/Sample Location
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