NC0000396_J15060054report_20150823

DUE Analytical Laboratory
ENERGY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Order Number: J15060054
Project Name: ASHEVILLE - AB GW ASSESSMENT WATER
Customer Name(s): Todd Plating, Kathy Webb, John Toepfer, Tim Hunsucker
Customer Address: 200 CP and L Drive
Arden,NC 28704
Lab Contact: Mary Ann Ogle Phone: [phone]
Mary Ann Ogle
�Ir 2015.06.18
Report Authorized By: I V \7iDate:
(Signature) 16:24:12 -04'00'
Mary Ann Ogle
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
6/18/2015
Analytical Lab
Page 1 of 44
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
2015016933
2015016934
2015016935
3 Total Samples
Collected By
Sample Description
ASHEVILLE
01 -Jun -15 8:58 AM
TDP
MW -24D
ASHEVILLE
01 -Jun -15 7:45 AM
TDP
Filter Blank
ASHEVILLE
01 -Jun -15 7:45 AM
TDP
Equipment Blank
Analytical Lab
Page 2 of 44

Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals 0 Yes No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes 0 No
All laboratory QA/QC requirements are acceptable. 0 Yes F-] No
Report Sections Included:
E%-'] Job Summary Report
❑� Sample Identification
Technical Validation of Data Package
❑� Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
Analytical Lab
Page 3 of 44
❑d Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
❑� Chain of Custody
❑� Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Mary Ann Ogle Date: 6/18/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060054
Site: MW -24D
Collection Date: 01 -Jun -15 8:58 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 300.0
06/05/2015 23:56
Vendor Parameter
Complete
EPA 300.0
06/05/2015 23:56
NITRITE + NITRATE (COLORIMETRIC)
1
EPA 245.1
Nitrite + Nitrate (Colorimetric)
1.2
mg-N/L
0.01
INORGANIC IONS BY IC
ACPAYNE
1
EPA 200.7
Chloride
13
mg/L
1
Sulfate
0.62
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
MHALL3
1
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
06/04/2015 12:08
MHALL3
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
EPA 200.7
06/04/2015 12:08
MHALL3
Aluminum (AI)
0.039
mg/L
0.005
Barium (Ba)
0.057
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.037
mg/L
0.01
Manganese (Mn)
0.137
mg/L
0.005
Strontium (Sr)
0.041
mg/L
0.005
Zinc (Zn)
0.009
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
06/02/2015 15:16
MHALL3
Calcium (Ca)
3.15
mg/L
0.01
Magnesium (Mg)
3.40
mg/L
0.005
Potassium (K)
1.54
mg/L
0.1
Sodium (Na)
3.25
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.091
mg/L
0.005
Barium (Ba)
0.055
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.060
mg/L
0.01
Manganese (Mn)
0.136
mg/L
0.005
Strontium (Sr)
0.036
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015016933
Matrix: GW WW
Analytical Lab
Page 4 of 44
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/02/2015 14:26
LSTARLI
10
EPA 300.0
06/05/2015 23:56
BGN9034
1
EPA 300.0
06/05/2015 23:56
BGN9034
1
EPA 245.1
06/04/2015 14:39
ACPAYNE
1
EPA 245.1
06/10/2015 14:57
ACPAYNE
1
EPA 200.7
06/04/2015 12:08
MHALL3
1
EPA 200.7
06/04/2015 12:08
MHALL3
1
EPA 200.7
06/04/2015 12:08
MHALL3
1
EPA 200.7
06/04/2015 12:08
MHALL3
1
EPA 200.7
06/04/2015 12:08
MHALL3
1
EPA 200.7
06/04/2015 12:08
MHALL3
1
EPA 200.7
06/04/2015 12:08
MHALL3
1
EPA 200.7
06/05/2015 10:54
MHALL3
1
EPA 200.7
06/05/2015 10:54
MHALL3
1
EPA 200.7
06/05/2015 10:54
MHALL3
1
EPA 200.7
06/05/2015 10:54
MHALL3
1
EPA 200.7
06/02/2015 15:16
MHALL3
1
EPA 200.7
06/02/2015 15:16
MHALL3
1
EPA 200.7
06/02/2015 15:16
MHALL3
1
EPA 200.7
06/02/2015 15:16
MHALL3
1
EPA 200.7
06/02/2015 15:16
MHALL3
1
EPA 200.7
06/02/2015 15:16
MHALL3
1
EPA 200.7
06/02/2015 15:16
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060054
Site: MW -24D
Collection Date: 01 -Jun -15 8:58 AM
Analyte
Result
Units Qualifiers
RDL
TOTAL RECOVERABLE METALS BY ICP -MS (DISSOLVED)
EPA 200.8
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
TOTAL RECOVERABLE METALS BY ICP -MS
SLS2560
1
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
1.02
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
1.07
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
RADIOLOGICAL - (Analysis Performed by GEL)
Vendor Parameter
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
TDS 66 mg/L 25
Total Carbon
TOC 0.211 mg/L 0.1
Sample #: 2015016933
Matrix: GW WW
Analytical Lab
Page 5 of 44
DF
Method
Analysis Date/Time
Analyst
1
EPA 200.8
06/17/2015 12:39
JAHERMA
1
EPA 200.8
06/17/2015 12:39
JAHERMA
1
EPA 200.8
06/17/2015 12:39
JAHERMA
1
EPA 200.8
06/17/2015 12:39
JAHERMA
1
EPA 200.8
06/17/2015 12:39
JAHERMA
1
EPA 200.8
06/17/2015 12:39
JAHERMA
1
EPA 200.8
06/17/2015 12:39
JAHERMA
1
EPA 200.8
06/17/2015 12:39
JAHERMA
1
EPA 200.8
06/17/2015 12:39
JAHERMA
1
EPA 200.8
06/17/2015 12:39
JAHERMA
1
EPA 200.8
06/17/2015 12:39
JAHERMA
1
EPA 200.8
06/17/2015 12:39
JAHERMA
1
EPA 200.8
06/17/2015 12:39
JAHERMA
1
EPA 200.8
06/08/2015 17:47
SLS2560
1
EPA 200.8
06/08/2015 17:47
SLS2560
1
EPA 200.8
06/08/2015 17:47
SLS2560
1
EPA 200.8
06/08/2015 17:47
SLS2560
1
EPA 200.8
06/08/2015 17:47
SLS2560
1
EPA 200.8
06/08/2015 17:47
SLS2560
1
EPA 200.8
06/08/2015 17:47
SLS2560
1
EPA 200.8
06/08/2015 17:47
SLS2560
1
EPA 200.8
06/08/2015 17:47
SLS2560
1
EPA 200.8
06/08/2015 17:47
SLS2560
1
EPA 200.8
06/08/2015 17:47
SLS2560
1
EPA 200.8
06/08/2015 17:47
SLS2560
1
EPA 200.8
06/08/2015 17:47
SLS2560
Vendor Method
V_SHEALY
Vendor Method v GEL
Vendor Method V_ELE1
1 SM2540C 06/05/201510:40 AGIBBS5
1 SM5310C/EPA9060A 06/06/201514:09 TJA7067

Analytical Lab
Certificate of Laboratory Analysis Page 6 of 44
This report shall not be reproduced, except in full.
Order # J15060054
Site: MW -24D Sample #: 2015016933
Collection Date: 01 -Jun -15 8:58 AM Matrix: GW WW
Analyte Result Units Qualifiers RDL DF Method Analysis Date/Time Analyst
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 06/05/2015 09:55 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060054
Site: Filter Blank
Collection Date: 01 -Jun -15 7:45 AM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
EPA 245.1
06/10/2015 14:59
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
1
EPA 200.7
06/04/2015 12:12
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
0.011
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP -MS (DISSOLVED)
1
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
1.00
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015016934
Matrix: GW WW
Analytical Lab
Page 7 of 44
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
06/10/2015 14:59
ACPAYNE
1
EPA 200.7
06/04/2015 12:12
MHALL3
1
EPA 200.7
06/04/2015 12:12
MHALL3
1
EPA 200.7
06/04/2015 12:12
MHALL3
1
EPA 200.7
06/04/2015 12:12
MHALL3
1
EPA 200.7
06/04/2015 12:12
MHALL3
1
EPA 200.7
06/04/2015 12:12
MHALL3
1
EPA 200.7
06/04/2015 12:12
MHALL3
1
EPA 200.8
06/17/2015 13:35
JAHERMA
1
EPA 200.8
06/17/2015 13:35
JAHERMA
1
EPA 200.8
06/17/2015 13:35
JAHERMA
1
EPA 200.8
06/17/2015 13:35
JAHERMA
1
EPA 200.8
06/17/2015 13:35
JAHERMA
1
EPA 200.8
06/17/2015 13:35
JAHERMA
1
EPA 200.8
06/17/2015 13:35
JAHERMA
1
EPA 200.8
06/17/2015 13:35
JAHERMA
1
EPA 200.8
06/17/2015 13:35
JAHERMA
1
EPA 200.8
06/17/2015 13:35
JAHERMA
1
EPA 200.8
06/17/2015 13:35
JAHERMA
1
EPA 200.8
06/17/2015 13:35
JAHERMA
1
EPA 200.8
06/17/2015 13:35
JAHERMA

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060054
Site: Equipment Blank
Collection Date: 01 -Jun -15 7:45 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
1 EPA 300.0
Vendor Parameter
Complete
1 EPA 245.1
06/04/2015 14:41
NITRITE + NITRATE (COLORIMETRIC)
1 EPA 200.7
06/05/2015 11:11
Nitrite + Nitrate (Colorimetric)
0.027
mg-N/L
0.01
INORGANIC IONS BY IC
06/05/2015 11:11
MHALL3
1 EPA 200.7
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
06/02/2015 15:19
MHALL3
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY ICP
MHALL3
1 EPA 200.7
06/02/2015 15:19
Calcium (Ca)
< 0.01
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
06/08/2015 17:52
SLS2560
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Analytical Lab
Page 8 of 44
Sample #: 2015016935
Matrix: GW WW
DF Method Analysis Date/Time Analyst
Vendor Method V_SHEALY
1 EPA 353.2
06/02/2015 14:30
LSTARLI
1 EPA 300.0
06/05/2015 21:29
BGN9034
1 EPA 300.0
06/05/2015 21:29
BGN9034
1 EPA 245.1
06/04/2015 14:41
ACPAYNE
1 EPA 200.7
06/05/2015 11:11
MHALL3
1 EPA 200.7
06/05/2015 11:11
MHALL3
1 EPA 200.7
06/05/2015 11:11
MHALL3
1 EPA 200.7
06/05/2015 11:11
MHALL3
1 EPA 200.7
06/02/2015 15:19
MHALL3
1 EPA 200.7
06/02/2015 15:19
MHALL3
1 EPA 200.7
06/02/2015 15:19
MHALL3
1 EPA 200.7
06/02/2015 15:19
MHALL3
1 EPA 200.7
06/02/2015 15:19
MHALL3
1 EPA 200.7
06/02/2015 15:19
MHALL3
1 EPA 200.7
06/02/2015 15:19
MHALL3
1 EPA 200.8
06/08/2015 17:52
SLS2560
1 EPA 200.8
06/08/2015 17:52
SLS2560
1 EPA 200.8
06/08/2015 17:52
SLS2560
1 EPA 200.8
06/08/2015 17:52
SLS2560
1 EPA 200.8
06/08/2015 17:52
SLS2560
1 EPA 200.8
06/08/2015 17:52
SLS2560
1 EPA 200.8
06/08/2015 17:52
SLS2560
1 EPA 200.8
06/08/2015 17:52
SLS2560
1 EPA 200.8
06/08/2015 17:52
SLS2560
1 EPA 200.8
06/08/2015 17:52
SLS2560
1 EPA 200.8
06/08/2015 17:52
SLS2560
1 EPA 200.8
06/08/2015 17:52
SLS2560
1 EPA 200.8
06/08/2015 17:52
SLS2560
METHANE - (Analysis Performed by Shealy Labs)
Methane (CH4) Complete Vendor Method V_SHEALY

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15060054
Site: Equipment Blank
Collection Date: 01 -Jun -15 7:45 AM
Analyte Result Units Qualifiers RDL DF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L 25 1
Total Carbon
Sample #: 2015016935
Matrix: GW WW
Analytical Lab
Page 9 of 44
Method Analysis Date/Time Analyst
Vendor Method
V_ELE1
SM2540C 06/05/201510:40 AGIBBS5
TOC 0.167 mg/L 0.1 1 SM5310C/EPA9060A 06/06/201514:09 TJA7067
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 06/05/2015 09:55 AGIBBS5

Analytical Lab
Page 10 of 44
Element One Inc.
6319-D Carolina Beach Rd.
Wilmington, NC 28412
Rhone: 910 793-0128
Fax: [phone]
[e-mail]
REPORT OF ANALYSES
Duke Energy June 11, 2015
Laboratory Services Client Project Name AB GW Assessment water Asheville
13339 Hagers Ferry Road Bld. MG03A Client Project Number J15060054
Huntersville, NC 28078 PO Number
Sample Matrix GW WW Sample Type Grab Date Received 06/03/2015
Date Analyzed 06/04/2015 Method SM 4500 S2- D Time Received 1420
Delivered by FedEx
eOne ID Duke Energy ID Parameter Result Unit Dil
24947-1
MW -24D
Sulfide
< 0.1
24947-2
Equipment Blank
Sulfide
< 0.1
mg/L 1
Received by JRC
DL Date Time
Sampled Sampled
0.1 06/01/15 0858
mg/L 1 0.1 06/01/15 0745
4
Ken Smith, Laboratory Director
24947 Duke Report Packet Compiled by�
NC Certifications: DW 37788 and DWQ DENR 604

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Analytical Lab
Page 11 of 44
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Analytical Lab
Page 11 of 44
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Analytical Lab
dementOne SAMPLE SUBMISSION FORM LabPtD 12124947
TAT 7 BD
Hold Time Expiration 06.08.15 @ 7:45
Client: Duke Energy
LIMS No J15060054
Project ID Asheville
Analysis Due Date 06.05.15
Report Due Date 06.12.15
Date Rec:
06.03.15
Time Rec:
1420
Rec By
J RC
H >9 Y No; _ 6°C re -s)-
- No Ref. Method:
If No, Record I If No, Record SM4500 S2 D
Sample Identification & Collection Information
Lab ID Client ID Collection Date Collection Time Analysis Requested
1 MW -24D 06/01/15 0858 i e
2 Equipment Blank 06/01/15 0745
NOTE for Sulfide
The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final spike concentration at - 500 pg/L
Lab Communications
All AB Groundwater Assessment jobs need a RL of 0.1
SS Page 1 of 1 Prep By / Date ftft^ G/, L-(, 1;
SS by Labeled By / Date —� - IS
6/4/2015 9:05:46 AM ID Verification By /Date �-t ,1

Analytical Lab
Page 13 of 44
METHOD:
SM 4500 S2- p
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER ug/mL
DETECTION LIMIT u 1.000
CLIENT:
Duke
SPK LEVEL u 5
Lab ID#
24946-/ 947 / 948 / 949 / 950 / 951
Na2S•9H2O Lot #
40721
MAX ALIQUOT 10.00
Date:
06/04/15
STANDARD c_onc(ppm) X
Time Analysis Begun
9:30
Cal Std Lot: - WC2-86-1 10
Time Analysis Ended
11:40
JQC Std Lot: WC2-86-2 10
Analyst:
KAM
IRM ARRC)PPTIOKI I V
X
Y
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.104
2.50
0.232
5.00
0.446
7.50
0.637
1000
0 830
Page 1 of 4
X
I
�� .:.fir.,.. ...
SAMPLE SAMP
I.D. ABS
ug PERALI
ALIQUOT
�
in mL PREP
ANALYZED VOL in mL
Sloe
ALI in mL
TAKEN
0.082362637:
RESULTS
ug/mL
Correlation
LESS THAN
% SPK REC
- 0.999221856
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.100
0.8544
10
10
10
<
85.44%
1.0
Std. B. 2.50
0.236
2.5759
10
10
10
0.258
103.04%
2.5
Std. B. 5.00
0.446
5.2342
10
10
10
0.523
104.68%
5.00
Std. B. 7.50
0.634
7.6139
10
10
10
0.761
101.52%
7.5
Std. B. 10.00
0.807
9.8038
10
10
10
0.980
98.04%
10.00
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.445
5.2215
10
10
10
0.522
105%
5.0
QC
0.447
5.2468
10
10
10
0.525
105%
5.0
24946-1
0.077
0.5633
10
10
10
<
24946-1 s k
0.087
0.6899
10
10
10
<
14%
5.0
24946-2
0.006
-0.3354
10
10
10,<
0
24946-2 dup
0.003
-0.3734
10
10
10
< 0.1
24946-2 s k
0.440
5.1582
10
10
10
0.516
103%
5.0
24946-3
0.022
-0.1329
10
10
10
24946-3 s k
0.421
4.9177
10
10
10
0.492
98%
5.0
24947-1
0.005
-0.3481
10
10
10
24947-1 s k
0.436
5.1076
10
10
10
0.511
102%
5.0
24947-2
0.003
-0.3734
10
10
10:=
p,;1®
24947-2 s k
0.447
5.2468
10
10
10
0.525
105%
5.0
24948-1
0.001
-0.3987
10
10
10
=n 4"d
24948-1 s k
0.463
5.4494
10
10
10
0.545
109%
5.0
24948-2
0.004
-0.3608
10
10
10(�
,?
24948-2 s k
0.408
4.7532
10
10
10
0.475
95%
5.0
24949-1
0.093
0.7658
10
10
10
<
24949-1 s k
0.269
2.9937
10
10
10
0.299
60%
5.0
24949-2
0.024
-0.1076
10
10
10
24949-2 s k
0.393
4.5633
10
10
10
0.456
91%
5.0
Blank
0.000
0.0000
10
10
10
<
QC 0.448
Submitted fOr QA/QC-
5.2595
Date: 06/04/15
10
10
By: (Print)
10
0.526
KAM
105%
(sign):
5.0
Page 1 of 4

Analytical Lab
Page 14 of 44
METHOD:
SM 4500 S2 -'D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
ug/mL
DETECTION LIMIT u
1.000
CLIENT:
Duke
SPK LEVEL u
5
Lab ID#
24946 / 947
06/04/15
9:30
11:40
KAM
Y
/ 948 / 949 /
°.m
950 / 951
Na2S•9H2O Lot #
40721
MAX ALIQUOT
STANDARD conc(ppm)
Cal Std Lot: WC2-86-1
QC Std Lot: WC2-86-2
STD ABSORPTION
10.00
X
10
10
Y
Date:
Time Analysis Begun
Time Analysis Ended
Analyst:
X
ug STD
SOLUTION
STD
I 0.8m
°.sm
ABS
0.703
--- ---------------- ------
17
-°�
M
0.00
1.00
2.50
5.00
7.50
10.00
0.000
06°°
-�
0.104
0,500
0d0°
406
0.300
- --
0.232
0,200-------232
0.200
-- --
.
-
0.446
DAM
M7.50
-
0.637
0.830
°°°°
0.00
2.00
4.00
8.00
X
B00
,000 12.00
SAMPLE SAMP ug PER
I.D. ABS ALIQUOT
ALI in mL PREP
ANALYZED VOL in mL
Sloe
ALI in mL
TAKEN
0.082362637
RESULTS
ug/mL
Correlation
LESS THAN
% SPK REC
0.999221855
SPIKE
LEVEL
Std, B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. 13, 1.00
0.100
0.8544
10
10
10
<
85.44%
1.0
Std. B. 2.50
0.236
2.5759
10
10
10
0.258
103.04%
2.5
Std. B. 5.00
0.446
5.2342
10
10
10
0.523
104.68%
5.00
Std. B. 7.50
0.634
7.6139
10
10
10
0.761
101.52%
7.5
Std. B. 10.00
0.807
9.8038
10
10
10
0.980
98.04%
10.00
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.445
5.2215
10
10
10
0.522
105%
5.0
QC
0.447
5.2468
10
10
10
0.525
5.0
24949-3
0.003
-0.3734
10
10
10
24949-3 s k
0.461
5.4241
10
10
10
0.542
108%
5.0
24950-1
0.020
-0.1582
10
1 10
10
24950-1 du
0.014
-0.2342
10
10
10
< 0.1
24950-1 s k
0.407
4.7405
10
10
10
0.474
95%
5.0
24950-2
0.005
-0.3481
10
10
10
< 0~1
24950-2 spk
0.397
4.6139
10
10
10
0.461
92%
5.0
24950-3
0.083
0.6392
10
10
10,0'
.. -.-... -.. .
x
24950-3 s k
0.451
5.2975
10
10
10
0.530
106%
5.0
24950-4
0.006
-0.3354
10
10
10
<
24950-4 s k
0.216
2.3228
10
10
10
0.232
46%
5.0
24950-5
0.004
-0.3608
10
10
10
24950-5 spk
0.402
4.6772
10
10
10
0.468
94%
5.0
24950-6
0.004
-0.3608
10
10
10
<
24950-6 s k
0.230
2.5000
10
10
10
0.250
50%
5.0
24950-7
0.017
-0.1962
10
10
10.1
24950-7 spk
0.383
4.4367
10
10
10
0.444
89%
5.0
24950-8
0.013
-0.2468
10
10
-7777777.
10
i x'1
24950-8 spk
0.378
4.3734
10
10
10
0.437
87%
5.0
Blank
-0.001
0.0000
10
10
10
<
QC
0.447
5.2468
10
10
10
0.525
105%
5.0
Submitted fOC QA/QC- Date: 06/04/15
By: (Print)
KAM
(sign):
l
Page 2 of 4

Analytical Lab
Page 15 of 44
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
ug/mL
DETECTION LIMIT u
1.000
CLIENT: Duke
SPK LEVEL u
5
Lab ID#
24946 / 947 / 948 / 949 1950 / 951
Na2S•9H2O Lot #
40721
MAX ALIQUOT
10.00
Date: 06/04/15
STANDARD conc(ppm)
X
Time Analysis Begun 9:30
Cal Std Lot: WC2-86-1
10
Time Analysis Ended 11:40
1 QC Std Lot: WC2-86-2
10
Analyst: KAM
ISTID ABSORPTION
Y
X
ug STD
SOLUTION
0.00
1.00
2.50
5,00
7.500.637
10.00
Y
STD
ABS
0.000
0.104
0.232
0.446
0.830
0.800
0.700
0.E00
0.300 ---
0.200
0,:
0.000
- -- - -- --- ------
- -- --
.232
2.00 4.00
--
e.0o
X
-- 7 --- -
-
e.a0
°.
- - - ---
_--
10,00
_ _oaa
„
12.00
SAMPLE SAMP
I.D. ABS
e- a
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
Slope
ALI in mL
TAKEN
0.082362637
RESULTS
ug/ml-
Correlation
LESS THAN
% SPK REC
0.999221856
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.100
0.8544
10
10
10
<
85.44%
1.0
Std. B, 2.50
0.236
2.5759
10
10
10
0.258
103.04%
2.5
Std. B. 5.00
0.446
5.2342
10
10
10
0.523
104.68%
5.00
Std. B. 7.50
0.634
7.6139
10
10
10
0.761
101.52%
7.5
Std, B. 10.00
0.807
9.8038
10
10
10
0.980
98.04%
10.00
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.445
5.2215
10
10
10
0.522
105%
5.0
QC
0.447
5.2468
10
10
10
0.525
5.0
24950-9
0.008
-0.3101
10
10
10
'qt1
24950-9 s k
0.376
4.3481
10
10
10
0.435
87%
5.0
24950-10
0.208
2.2215
10
10
10
24950-10 s k
0.599
7.1709
10
10
10
0.717
99%
5.0
24950-11
0.002
-0.3861
10
10
10
24950-11 dup
0.002
-0.3861
10
10
10
< 0.1
24950-11 spk
0.444
5.2089
10
10
10
0.521
104%
5.0
24950-12
0.004
-0.3608
10
10
24950-12 s k
0.450
5.2848
10
10
10
0.528
106%
5.0
24951
0.003
-0.3734
10
10
10
24951 s k
0.441
5.1709
10
10
10
0.517
103%
5.0
24946-1
0.046
0.1709
10
10
5
<
24946-1 spk
0.178
1.8418
10
10
5
0.368
37%
5.0
24949-1
0.062
0.3734
10
10
5
24949-1 s k
0.375
4.3354
10
10
5
0.867
87%
5.0
24950-4
0.009
-0.2975
10
10
5
<
24950-4 s k
0.303
3.4241
10
10
5
0.685
68%
5.0
24950-6
0.004
-0.3608
10
10
5
<
24950-6 s k
0.317
3.6013
10
10
5
0.720
72%
5.0
Blank
-0.001
0.0000
10
10
10
<
QC
0.444
5.2089
10
10
10
0.521 1
104%
5.0
Submitted for QA/QC-
Date: 06/04/15
By: (Print)
KAM
(sign):
09
//
Page 3 of 4

METHOD: SM 4500 S2- D
ELEMENT ASSAY: Sulfide
CLIENT: Duke
Lab ID# 24946 / 947 / 948 / 949 / 950 /
Date: 06/04/15
Time Anal is Begun 9:30
Time Analysis Ended 11:40
Ug 5TD
SOLUTION
STD I
ABS
0.00
0.000
1.00
0.104
2.50
0.232
5.00
0.446
7.50
0.637
10.00
0.830
Analytical Lab
Page 16 of 44
ELEMENT ONE
Spectrophotometer UNITS OF ANSWER
Wave Length 664 DETECTION LIMIT u
SPK LEVELu
MAX ALIQUOT
Na2S•9H2O Lot # STANDARD conc(ppm)
40721 Cal Std Lot: WC2-86-1
QC Std Lot: WC2-86-2
STD ABSORPTION
X
10
�]SO
,oma
10.00 1200
X j
s}
0.082362637
Correlation
SAMPLE
0.999221855
SAMP
ug PER
ALI in mL
PREP
RESULTS
LESS THAN
SPIKE
I.D.
Std. B. 0.00
ABS
ALIQUOT
ANALYZED
VOL in mL
R
Ug/mL
% SPK REC
LEVEL
0.000
0.0000
10
10
<
0.0
Std. B. 1.00
0.100
0.8544
10
10
<
85.44%
1.0
Std. B. 2.50
0.236
2.5759
10
10
0.258
103.04%
2.5
Std. B. 5.00
0.446
5.2342
10
10
10
0.523
104.68%
5.00
Std. B. 7.50
0.634
7.6139
10
10
10
0.761
101.52%
7.5
Std. B. 10.00
0.807
9.8038
10
10
10
0.980
98.04%
10.00
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.445
5.2215
10
10
10
0.522
105%
5.0
QC
0.447
5.2468
10
10
10
0.525
105%
5.0
24946-1
0.020
-0.1582
10
10
2
<
24946-1 spk
0.310
3.5127
10
10
2
1.756
70%
5.0
24950-4
0.006
-0.3354
10
10
2
24950-4 spk
0.381
4.4114
10
10
2
2.206
88%
5.0
24950-6
0.002
-0.3861
10
10
2
24950-6 s k
0.385
4.4620
10
10
2
2.231
89%
5.0
24946-1
0.011
-0.2722
10
10
1
24946-1 spk
0.371
4.2848
10
10
1
4.285
86%
5.0
Blank
0.000
0.0000
1010
10
QC 0.448 5.2595
Submitted for QA/QC-
10
10
10
<
0.526
105%
5.0
Date:
06/04/15
Bv: (Print)
LeARA
Page 4 of 4

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water
Project Number:J15060054
Lot Number:QF03017
Date Completed:06/09/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
* QF0301 7*
Shealy Environmental Services, Inc. Page: 1 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QF03017
Project Name: AB GW Assessment Water
Project Number: J15060054
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 8
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QF03017
Project Name: AB GW Assessment Water
Project Number: J15060054
Sample Number Sample ID Matrix Date Sampled Date Received
001 2015016933 Aqueous 06/01/2015 0858 06/03/2015
002 2015016935 Aqueous 06/01/2015 0745 06/03/2015
(2 samples)
Shealy Environmental Services, Inc. Page: 3 of 8
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QF03017
Project Name: AB GW Assessment Water
Project Number: J15060054
Sample Sample ID Matrix Parameter Method Result Q Units Page
(0 detections)
Shealy Environmental Services, Inc. Page: 4 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF03017-001
Description: 2015016933 Matrix: Aqueous
Date Sampled:06/01/2015 0858 Project Name: AB GW Assessment Water
Date Received: 06/03/2015 Project Number: J15060054
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/04/2015 2238
HMA 76563
1
(Bicarbonate ) SM 2320B-2011
1 06/04/2015 2238
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/04/2015 2238
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF03017-001
Description: 2015016933 Matrix: Aqueous
Date Sampled:06/01/2015 0858 Project Name: AB GW Assessment Water
Date Received: 06/03/2015 Project Number: J15060054
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/04/2015 2255 JJG 76593
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QF03017-002
Description: 2015016935 Matrix: Aqueous
Date Sampled:06/01/2015 0745 Project Name: AB GW Assessment Water
Date Received: 06/03/2015 Project Number: J15060054
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/04/2015 2243
HMA 76563
1
(Bicarbonate ) SM 2320B-2011
1 06/04/2015 2243
HMA
1
(Carbonate Al) SM 2320B-2011
1 06/04/2015 2243
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QF03017-002
Description: 2015016935 Matrix: Aqueous
Date Sampled:06/01/2015 0745 Project Name: AB GW Assessment Water
Date Received: 06/03/2015 Project Number: J15060054
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/04/2015 2305 JJG 76593
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 8
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QF03017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - Ii
Sample ID: QQ76563-001 Matrix: Aqueous
Batch: 76563
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 06/04/2015 2153
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF03017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ76563-002 Matrix: Aqueous
Batch: 76563
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 98 1 98 90-110 06/04/2015 2159
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF03017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ76593-001 Matrix: Aqueous
Batch: 76593
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 06/04/2015 2042
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF03017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ76593-002 Matrix: Aqueous
Batch: 76593
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 50 48 1 94 70-130 06/04/2015 2015
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF03017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ76593-003 Matrix: Aqueous
Batch: 76593
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 50 44 1 88 6.7 70-130 30 06/04/2015 2031
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QF03017
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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fly avircmmmw Servicm 1W. rapjs l U(
DG"mtMNumber F -AD -016 KtVlacm pgiw L1M14
Rcvigiao Nlumbcr: 17 ElTm4ive aa[is G4.hVIS
Sample Receipt Checklist ( R.Q
Client. V n opw -_ Cooler Imported by/dale=: A/5- } 4AAs Lot #_ a y: Q.3 o i �
Meaw orreolakot 1-1 SEST F-1 Client F-1 UPS D FedEx ❑ Airborne Exp R` rIer I
Yes
El
I No
1. Ware custody seals pTuwnt on thu *Leder?
Yep1 3 1wT, 2. if custoci seals a e ip etit were they >.Ltact and unbroken?
Cooler ECl/Original tempemhue upon /r ipllberived i; otre tem0C Iperature upon rrccipt�
i+
N10hod_ ❑ Tennierature .lank �Agairlst BoLuc3 1R Gun ID: IR Clan CbrrectiDn Factor. � °C
Method of wolant F Wct Ice Blue Ice ❑ Iet 0140ifte
YcS ❑ No ❑ NA
3. If "eratnre of any cooler excelled 6.00C, was Project N ainisger notif"ted! -
PM notified by SRC, phone, note: (circle ant), outer:
(For ondilcra received via c(n=crs,ral ctxmer, PNI$ are to be uttttfied .
immedialtvly,
Yes C] No [] AIA
4- Is the commercial courier's actin slipattached to this Fanra?'
Yea Na El
Yes El No EE]
5. l,L�ere proper custard rneedures (reli h�dlrec�eived) Followed?
Sa Were saris les refi uishcd b • chart to mesial cvuricr?
Yes No
6. �9 "a saimle TDs listEd on the. COC?
Yes Nc
7. Were. soar le IDs listed oris all jum3pte contail`ters'?
Yes R No ❑
$. Was colleadon date & time listod Da thz COC
Yes No El
9. WRs collet on date & time listed on all sample contuincrr3?
7e—sP To ❑
10. Did all coutaisier label iwforanatiDn ID, date, time agroe with the COL?
YC3 a ❑
lfes Inc ❑
11. W= tests to be pfffUrm5A listed om Lhe COC?
12. Did all samples arrive in the pmW c ntainen for each tm?
Yeso
EH
11 Did all tamers atrivo n �d coridniou (unbroken, lids
' Yrs
Ido ❑
14. Was a uatl; s le voluntt avaibble?
Yes ❑
fir. Rr
15, Were all samples rcccivod within `/a dr holding Lime cc 4$ hours, WhielVti.�r
♦Dross first?
Y ❑ :
W,
16. Were any swn les containen nAssiiY ?
Yr=., ❑
N::
17. Were there any excess es not listed on CDC?
Yc ❑
Net NA ElI&
_
Were bubbles pfesent.>" size' 64"gar 6mm in dipmetin int ail ' va �1a15?
Yea ❑
Na ❑, NA [X
19. 11i+'ere all metaW0&G1HEWiaah t sawn les received at a pll of <2?
Y77
I+lo NA ff
20- W= all cyanide and+'or sulfide samples rrxscivcd ata pH >127
Yes ❑
No ❑ NA
21- Wert all apphcabla Nt rl'KU1cyanid&phenol 4<02m 'L) samples free of
residual chlorine?
Yes
Nei NA
2.2. Were, collection winplamtcres dnmrnented on the COC for NC smn lm?
Yes ❑
Nor ❑ NA &e
3. Were ciieW r arkcVxaq aes% (i, o. mquedtcd diluticros, l' S MSD clesl�atiar�s,
etc...) coinctly tran&cnbed firom the COC Luty the comment si ialw m LEES?
Yes ❑
NCS
M. Was the quote number used # ken from the contaitfr label?
sample Fr ;ervatiun (Must be Qomploted for any sarnplr,(s) ix:mrectly presuved or with thea&para,)
sample(s) gore received ince=eLly prescr�vd and wlzre adjusted
acc2ni- 1v instun 1; `rt:ccivin withx504 03BC1,T nO us Sly #
Sample(s)
w= rmeived with bubbim >6 mm in dinmetrr.
SaM lc(s)
were received with TRC >0.2 m +T, Of V21 is No
SC I' riaking Water Proj ect saraple(s) pH vnificd to be -- 2 by Date.
sample(s) werc not rwnved ata p14 of -I and %,= add ustcd aczordin ly using SR4
LEny le',, els 2P -Ll ted by:_
Vcrificd bye;-_ Datc:
g+ommealts.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

® Laboratories LLC
a member of The GEL Group Ilei;
June 12, 2015
Mrs. Mary Ann Ogle
Duke Energy Analytical Laboratory
13339 Hagers Ferry Road
Mail Code: MGO3A2
Huntersville, North Carolina 28078
Re: AB GW Assessment Water
Work Order: 374528
SDG: J15060054
Dear Mrs. :
,Analytical Lab
We 33 of 44
Po Box 30712 Charleston, SC 29417
2040 Savage Road Charleston. SC 25407
F 843.556.8171
F 843.766.1178
GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the
sample(s) we received on June 05, 2015. This original data report has been prepared and reviewed in accordance
with GEL's standard operating procedures.
Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs
on time every time. We trust that you will find everything in order and to your satisfaction. If you have any
questions, please do not hesitate to call me at [phone], ext. 4443.
Purchase Order: 1142110
Enclosures
Page 1 of 11
Sincerely,
Lindsay Fabra
Project Manager
gel.com

Analytical Lab
Page 34 of 44
GEL LABORATORIES LLC
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis Report
for
DUP0002 Duke Energy
Client SDG: J15060054 GEL Work Order: 374528
The Qualifiers in this report are defined as follows:
* A quality control analyte recovery is outside of specified acceptance criteria
** Analyte is a Tracer compound
** Analyte is a surrogate compound
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the Certificate of Analysis.
The designation ND, if present, appears in the result column when the analyte concentration is not detected above
the limit as defined in the 'U' qualifier above.
This data report has been prepared and reviewed in accordance with GEL Laboratories LLC
standard operating procedures. Please direct any questions to your Project Manager, Lindsay Fabra.
Reviewed by
Page 2 of 11
JU,&Y ,

Analytical Lab
GEL LABORATORIES LLC Page 35 of 44
2040 Savage Road Charleston SC 29407 - [phone] - www.gel.com
Certificate of Analysis
Company:
Duke Energy Analytical Laboratory
Address :
13339 Hagers Ferry Road
Mail Code: MG03A2
Huntersville, North Carolina 28078
Contact:
Mrs. Mary Ann Ogle
Project:
AB GW Assessment Water
Client Sample ID:
Sample ID:
Matrix:
Collect Date:
Receive Date:
Collector:
2015016933
374528001
Ground Water
01 -JUN -15 08:58
05 -JUN -15
Client
Report Date: June 12, 2015
Project: DUKE00225
Client ID: DUP0002
Parameter Qualifier Result DL RL Units DF Analyst Date Time Batch Method
Metals Analysis -ICP -MS
SW846 3010A/6020A Liquid "As Received"
Uranium -238 U 9.10E-06
0.000067
0.0002
ug/mL
1
SKJ 06/10/15
1004 1483666 1
Uranium -233 U 0.00
0.00001
0.00005
ug/mL
1
SKJ 06/11/15
0850 1483666 2
Uranium -234 U 0.00
0.00001
0.00005
ug/mL
1
Uranium -236 U 1.00E-06
0.00001
0.00005
ug/mL
1
Rad Gas Flow Proportional Counting
GFPC, Ra228, Liquid "As Received"
Radium -228 U 0.538
2.02
3.00
pCi/L
AXM6 06/10/15
1610 1483789 3
Rad Radium -226
Lucas Cell, Ra226, liquid "As Received"
Radium -226 5.78
0.576
1.00
pCi/L
CXP3 06/11/15
1120 1483816 4
The following Prep Methods were performed:
Method Description
Analyst
Date
Time Prep Batch
SW846 3010A SW 846 3010 Acid Digestion
JP1
06/08/15
1545
1483665
The following Analytical Methods were performed:
Method Description Analyst Comments
1 SW846 3010A/6020A
2 SW846 3010A/6020A
3 EPA 904,0/SW846 9320 Modified
4 EPA 903.1 Modified
Surrogate/Tracer Recovery Test Result Nominal Recovery% Acceptable Limits
Barium -133 Tracer GFPC, Ra228, Liquid "As Received" 84.3 (15%-125%)
Notes:
Page 3 of 11

GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
QC Summary
Duke Energy Analytical Laboratory
13339 Hagers Ferry Road
Mail Code: MG03A2
Huntersville, North Carolina
Contact: Mrs. Mary Ann Ogle
Workorder: 374528
Analytical Lab
Page 36 of 44
Report Date: June 12, 2015
Page 1 of 3
Parmname
NOM
Sample
Qual
QC
Units
RPD%o
REC%
Range Anlst
Date Time
Metals Analysis - ICPMS
Batch 1483666
QC1203331839
374139001
DUP
Uranium -233
U
ND
U
ND
ug/mL
N/A
SKJ
06/11/1510:01
Uranium -234
U
ND
U
ND
ug/mL
N/A
Uranium -236
U
ND
U
ND
ug/mL
N/A
Uranium -238
U
ND
U
ND
ug/mL
N/A
06/11/15 07:39
QC1203331838
LCS
Uranium -238
0.0496
0.0528
ug/mL
106
(80%-120%)
06/11/15 07:37
QC1203333067
LCS
Uranium -233
0.0005
0.000502
ug/mL
100
(80%-120%)
06/11/15 08:45
Uranium -234
0.00055
0.000529
ug/mL
96.2
(80%-120%)
Uranium -236
0.005
0.0056
ug/mL
112
(80%-120%)
QC1203331837
MB
Uranium -233
U
ND
ug/mL
06/11/15 08:44
Uranium -234
U
ND
ug/mL
Uranium -236
U
ND
ug/mL
Uranium -238
U
ND
ug/mL
06/11/15 07:36
QC1203331840
374139001
MS
Uranium -238
0.0496
U
ND
0.0529
ug/mL
106
(75%-125%)
06/11/15 07:41
QC1203333068
374139001
MS
Uranium -233
0.0005
U
ND
0.000395
ug/mL
79
(75%-125%)
06/11/1510:02
Uranium -234
0.00055
U
ND
0.000415
ug/mL
75.5
(75%-125%)
Uranium -236
0.005
U
ND
0.0044
ug/mL
87.9
(75%-125%)
QC1203331841
374139001
SD1LT
Uranium -233
U
ND
U
ND
ug/L
N/A
06/11/1510:03
Page 4 of 11

Analytical Lab
Page 37 of 44
GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
QC Summary
Workorder: 374528
1.33 pCi/L 21.2
(0%-100%) CXP3 06/08/1509:25
QC1203332254 LCS
Radium -226 24.7
29.5 pCi/L
Page 2 of 3
Parmname
NOM
Sample
Qual
QC
Units
RPD%
REC% Range Anlst
Date Time
Metals Analysis - ICPMS
23.8 pCi/L
89.8 (75%-125%) 06/08/15 09:25
Notes:
The Qualifiers in this report are defined as follows:
Batch 1483666
< Result is less than value reported
> Result is greater than value reported
Uranium -234
U
ND
U
ND
ug/L
N/A
FB Mercury was found present at quantifiable concentrations in field blanks received with these samples.
Uranium -236
U
ND
U
ND
ug/L
N/A
(0%-10%) SKJ
06/11/1510:03
Uranium -238
U
ND
U
ND
ug/L
N/A
(0%-10%)
06/11/15 07:42
Rad Gas Flow
Batch 1483789
QC1203332161 374528001 DUP
Radium -228
U
0.538
U
0.824
pCi/L
N/A
N/AAXM6
06/10/1516:10
QC1203332162 LCS
Radium -228
30.9
24.9
pCi/L
80.7 (75%-125%)
06/10/1516:10
QC1203332160 MB
Radium -228
U
0.530
pCi/L
06/10/1516:10
Rad Ra -226
Batch 1483816
QC1203332252 374527001 DUP
Radium -226 1.65
1.33 pCi/L 21.2
(0%-100%) CXP3 06/08/1509:25
QC1203332254 LCS
Radium -226 24.7
29.5 pCi/L
119 (75%-125%) 06/11/1511:20
QC1203332251 MB
Radium -226 U
0.574 pCi/L
06/11/1511:20
QC1203332253 374527001 MS
Radium -226 24.7 1.65
23.8 pCi/L
89.8 (75%-125%) 06/08/15 09:25
Notes:
The Qualifiers in this report are defined as follows:
** Analyte is a Tracer compound
< Result is less than value reported
> Result is greater than value reported
BD Results are either below the MDC or tracer recovery is low
E %difference of sample and SD is >10%. Sample concentration must meet flagging criteria
FA Failed analysis.
FB Mercury was found present at quantifiable concentrations in field blanks received with these samples.
Data associated with the blank are deemed
invalid for reporting to regulatory agencies
H Analytical holding time was exceeded
Page 5 of 11

GEL LABORATORIES LLC
2040 Savage Road Charleston, SC 29407 - [phone] - www.gel.com
QC Summary
Workorder: 374528
Parmname NOM Sample Qual QC Units RPD% REC'%
Analytical Lab
Page 38 of 44
Page 3 of 3
Range Anlst Date Time
J Value is estimated
K Analyte present. Reported value may be biased high. Actual value is expected to be lower.
L Analyte present. Reported value may be biased low. Actual value is expected to be higher.
M M if above MDC and less than LLD
M REMP Result > MDC/CL and < RDL
N Metals --The Matrix spike sample recovery is not within specified control limits
N/A RPD or %Recovery limits do not apply.
N1 See case narrative
ND Analyte concentration is not detected above the detection limit
NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER.
R Sample results are rejected
U Analyte was analyzed for, but not detected above the MDL, MDA, or LOD.
UI Gamma Spectroscopy --Uncertain identification
UJ Gamma Spectroscopy --Uncertain identification
UL Not considered detected. The associated number is the reported concentration, which may be inaccurate due to a low bias.
X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier
Y Other specific qualifiers were required to properly define the results. Consult case narrative.
^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry.
h Preparation or preservation holding time was exceeded
N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable.
^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than
five times (5X) the contract required detection limit (RL). In cases where either the sample or duplicate value is less than 5X the RL, a control limit of +/- the
RL is used to evaluate the DUP result.
* Indicates that a Quality Control parameter was not within specifications.
For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations.
Where the analytical method has been performed under NELAP certification, the analysis has met all of the
requirements of the NELAC standard unless qualified on the QC Summary.
Page 6of11

I
V,
Page 7 of 11
Analytical Lab
Page 39 of 44
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m poper cendllon for traropo exior, —ofdoj to the appi:cable reguialorn of the Depailawll al Traespo taioh
This Memorandum is an acknowledgment that a Bill of Lading has been issued and is not the Original Bill of Lading, nor Analytical Lab
y.b eta af.grsduplicate, covering the property named herein, and is intended solely for filing or record. Shippere 40 of 44
Wt s
:3 «+Y
vs, $ cYa vpp
� gCarrier No.
Date
(Name of Carrier) (SCAC)
TO: J FROM:
Consignee Shipper
On Collect on Delivery shipments, the letters "COD" must appear before con'signee's name - - or as otherwis provided in Ire -m 43o Sec {
F
Street Street,-
Destination r Zip Code Origin Zip Code
Vehicle U.S.DOT Hazmat
Number Reg. Number
la— .
No. Shipping
Units
Kind of Packaging, Description of Articles,
HM Special Marks and Exceptions
Weight
(Subject to
Correction)
RATE
CHARGES
REMIT
C.O.D. TO:
ADDRESS
COD Amt: $
C.O.D. FEE:
PREPAID ❑ $
COLLECT ❑
Note - Where the rate Is dependent on value, Shippers are required t0
state specifically in writing the agreed or declared value of the property.
The agreed or declared value of the property is hereby specifically stated
by the shipper to be not exceeding
$ peris
Tltis is to corti(y that Iha above materials are ptopeily
classified, descdbad, packaged, marked, and labeled,
and are in proper condition for transportation according to
the applicable regNations of the Department o#Transportation.
Subject to Section 7 of the conditions, if this shipment is to be
delivered to the consignee without recourse on the consignor, the
coThecthr111 e shailgnothmakloodel'rveryofateftl4stshipmentvrllhouipayment
of Ireighl and all other lawful Chargas.
TOTAL
$
CHARGES:
FREIGHT pRAID RpEIIGHTCHARGES
Chook h-
ex -fat when ilchargasaro
box atrom lobs,
hocked I� collect
ISI nature
i nature of consignor)
RECEIVED, subject to the classifications and lawfully filed tariffs in effect on the date of the issue of this Din or Lading, the property desenom move In apparent g000 order, ex-fe, as a.,- fashion. aha —uha n si ..mems o, pacaages unmwwnr, mama.,
consigned, and destined as indicated above which said carrier (the word carrier being understood throughout this contract as meaning any person or corporation in possession of the property under the contract) agrees to carry to its usual place of delivery at said
destination, if on its route, otherwise to deliver to another carrier on the route to said destination. It is mutually agreed as to each carrier of all or any of, said property over all lir any portion of said route to destination and as to each party at any time interested
in all or any of said property, that every service to be performed hereunder shall be subject to all the bill of lading terms and conditions in the governing classification on the date of shipment,
Shipper hereby certifies that he Is familiar with all the bill of lading terms and conditions in the governing classification and the said terms and conditions are hereby agreed to by the shipper and accepted for himself and his assigns.
SHIPPER v r
PER
EMERGENCY RESPONSE
TELEPHONE NUMBER:
CIAs 2fl>
CARRIER
PER
DATE
Monitored at ell tim s the Hazardous Matelial is in transportation including storage incidental to uansportanon (§172-Go4)
BLGG&423 o- a, d 9 p ol T. , n. t � i y 'h" 1 r
TI _ use N W rn a a, od i. den„'i a=s, c1Ln, ,ala al, c of I',, tau Srcl.>, i,?.NI(..1 o T,.a -J. c�tle a Feline.
PRINTED IN U.S.A. .rs+a.a-s S�cl 172 204s,) of f,,' ll
nY alcd
on !Y to of uo,,a -u„ o se .v e'c-N.ron n t I . rt_ r=;< -J . V Reg a'n,, Iw a pz..'A. ro:;c,at
Page 8 of 11

Analytical Lab
Page 41 of 44
Laboratories 11C SAMPLE RECEIPT & REVIEW FORM
Client:
SDG/ARICOCIWorkOrder: 13-aS
Received By: °UKI*
Date Received: I LS
Information
*If Net Counts > 100cpm on samples not marked "radioactive", contact the Radiation Safet Group for further
Suspected Hazard
1
investigation.
COC/Samples marked as radioactive?
JX.
Maximum Net Counts Observed* (Observed Counts -Area Background Counts):
Classified Radioactive R or III by RSO?
If yes, Were swipes taken of sample containers < action levels?
COC/Samples marked containing PCBs?
I X1
Package, COC, and/or Samples marked as
beryllium or asbestos containing?
If yes, samples are to be segregated as Safety Controlled Samples, and opened by the GEL Safety Group.
Shipped as a DOT Hazardous?
Hazard Class Shipped: UN#:
Samples identified as Foreign Soil?
Sample Receipt Criteria
Z
Z
Comments/Qualifiers (Required for Non -Conforming Items)
1
Shipping containers received intact
Circle Applicable:
Seals broken Damaged container Leaking container Other (describe)
and sealed?
2
Samples requiring cold preservation
r Preservation Method: lee bags Blue ice Dry ice None Other (describe)
*all temperances are recorded in Ce sats
within (0 < 6 deg. C)?*
.,a
Daily check performed and passed on
Temperature Device Serial It: y
Secondary Temperature Device Serial It (If Applicable):
IR temperature gun?
Chain of custody documents included
3
with shipment?
Circle Applicable:
4
Sample containers intact and seated?
Seals broken Damaged container Leaking container Other (describe)
Samples requiring chemical
ISample
ID's, containers affected and observed p1l:
5
preservation at proper pfl?
y
If Preservation added, Loth;
Do Low Level Perchlorate samples
Sample ID's and containers affected:
6
(EPA 6850) have headspace as
required?
VOA vials free of headspace (defined
Sample ID's and containers affected:
as < 6mm bubble)?
(If yes, immediately deliver to Volatiles laboratory)
8
Are Encore containers present?
INX
Samples received within holding
ID's and tests affected:
9
time?
Sample ID's on COC match ID's on
Sample ID's and containers affected:
10
bottles?
Date & time on COC match date &
Sample ID's affected:
11
time on bottles?
Number of containers received match
Sample ID's affected:
12
number indicated on COC?
Are sample containers identifiable as
13
GEL provided?
COC form is properly signed in
14
relinquished/received sections?
,
Circle Applicable:
FedEx Air FedEx Ground UPS Field Services Courier Other
15
Carrier and tracking number.
�6 Z {r°'?'I°W
Comments (Use Continuation Form if needed):
n
PM (or PMA) review: Initials Date D to 0 5 Page of _„_ GL -CHL -SR -001 Rev t
Page 9 of 11

List of current GEL Certifications as of 12 June 2015
State
Certification
Alaska
UST -110
Arkansas
88-0651
CLIA
42DO904046
California
2940 Interim
Colorado
SC00012
Connecticut
PH -0169
Delaware
SC000122013-10
DoD ELAP/ ISO 17025 A2LA
2567.01
Florida NELAP
E87156
Foreign Soils Permit
P330 -12-00283,P330-12-00284
Georgia
SC00012
Georgia SDWA
967
Hawaii
SC000122013-10
Idaho Chemistry
SC00012
Idaho Radiochemistry
SC00012
Illinois NELAP
200029
Indiana
C—SC-01
Kansas NELAP
E-10332
Kentucky SDWA
90129
Kentucky Wastewater
90129
Louisiana NELAP
03046 (A133904)
Louisiana SDWA
LA150001
Maryland
270
Massachusetts
M—SCO 12
Michigan
9976
Mississippi
SC000122013-10
Nebraska
NE—OS-26-13
Nevada
SC000122014-1
New Hampshire NELAP
2054
New Jersey NELAP
SCO02
New Mexico
SC00012
New York NELAP
11501
North Carolina
233
North Carolina SDWA
45709
Oklahoma
9904
Pennsylvania NELAP
68-00485
Plant Material Permit
PDEP-12-00260
S.Carolina Radchem
10120002
South Carolina Chemistry
10120001
Tennessee
TN 02934
Texas NELAP
T104704235-15-10
Utah NELAP
SC000122015-17
Vermont
VT87156
Virginia NELAP
460202
Washington
C780
West Virginia
997404
Page 10 of 11
Analytical Lab
Page 42 of 44

Analytical Lab
There are no "Data Exception Reports" associated with this analytical rePAO.43 of 44
Page 11 of 11

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