NC0000396_J15050736report_20150823

+ DUKE Analytical Laboratory
ENERGY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Order Number: J15050736
Project Name: ASHEVILLE - AB GW ASSESSMENT WATER
Customer Name(s): Todd Plating, Kathy Webb, John Toepfer, Tim Hunsucker
Customer Address: 200 CP and L Drive
Arden, NC 28704
Lab Contact: Mary Ann Ogle Phone: [phone]
Mary Ann Ogle
Report Authorized By: j "I �b 2015.06.10 16:38:34Date:
(Signature) -04'00'
Mary Ann Ogle
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
6/10/2015
Page 1 of 69
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
Collected By
Sample Description
2015016286
ASHEVILLE
27 -May -15 9:41 AM
illegible
ABMW-02
2015016287
ASHEVILLE
27 -May -15 9:45 AM
illegible
ABMW-05BR
2015016288
ASHEVILLE
27 -May -15 11:45 AM
illegible
ABMW-07S
2015016289
ASHEVILLE
27 -May -15 12:50 PM
illegible
MW -08S
2015016290
ASHEVILLE
27 -May -15 2:12 PM
illegible
MW -05D
2015016291
ASHEVILLE
27 -May -15 12:05 PM
illegible
ABMW-02S-DUP
2015016292
ASHEVILLE
27 -May -15 11:40 AM
illegible
ABMW-02S
2015016293
ASHEVILLE
27 -May -15 2:44 PM
illegible
GW-01BR
2015016294
ASHEVILLE
27 -May -15 9:45 AM
illegible
Filter Blank
2015016295
ASHEVILLE
27 -May -15 9:45 AM
illegible
Equipment Blank
10 Total Samples
Page 2 of 69

Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals Yes No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes F./] No
All laboratory QA/QC requirements are acceptable.❑ Yes ❑ No
Report Sections Included:
U Job Summary Report
❑ Sample Identification
n Technical Validation of Data Package
❑ Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
Page 3 of 69
Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
66 Chain of Custody
[I/0] Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: Peggy Kendall Date: 6/10/2015

Certificate of Laboratory Analysis Page 4 of 69
This report shall not be reproduced, except in full.
Order # J15050736
Site: ABMW-02
Collection Date: 27 -May -15 9:41 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 300.0
06/02/2015 09:09
Vendor Parameter
Complete
EPA 300.0
06/02/2015 09:09
NITRITE + NITRATE (COLORIMETRIC)
1
EPA 245.1
Nitrite + Nitrate (Colorimetric)
0.014
mg-N/L
0.01
INORGANIC IONS BY IC
ACPAYNE
1
EPA 200.7
Chloride
5.5
mg/L
0.1
Sulfate
250
mg/L
5
MERCURY (COLD VAPOR) IN WATER
MHALL3
1
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
05/29/2015 10:49
MHALL3
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
EPA 200.7
05/29/2015 10:49
MHALL3
Aluminum (AI)
0.020
mg/L
0.005
Barium (Ba)
0.271
mg/L
0.005
Boron (B)
1.71
mg/L
0.05
Iron (Fe)
3.35
mg/L
0.01
Manganese (Mn)
4.32
mg/L
0.005
Strontium (Sr)
5.26
mg/L
0.005
Zinc (Zn)
0.020
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
06/02/2015 09:22
MHH7131
Calcium (Ca)
163
mg/L
0.1
Magnesium (Mg)
45.0
mg/L
0.005
Potassium (K)
17.8
mg/L
0.1
Sodium (Na)
25.2
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.407
mg/L
0.005
Barium (Ba)
0.301
mg/L
0.005
Boron (B)
1.78
mg/L
0.05
Iron (Fe)
3.44
mg/L
0.01
Manganese (Mn)
3.26
mg/L
0.005
Strontium (Sr)
5.86
mg/L
0.005
Zinc (Zn)
0.020
mg/L
0.005
Sample #: 2015016286
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/01/2015 13:34
LSTARL1
1
EPA 300.0
06/02/2015 09:09
BGN9034
50
EPA 300.0
06/02/2015 09:09
BGN9034
1
EPA 245.1
05/29/2015 15:32
ACPAYNE
1
EPA 245.1
06/01/2015 15:52
ACPAYNE
1
EPA 200.7
05/29/2015 10:49
MHALL3
1
EPA 200.7
05/29/2015 10:49
MHALL3
1
EPA 200.7
05/29/2015 10:49
MHALL3
1
EPA 200.7
05/29/2015 10:49
MHALL3
1
EPA 200.7
05/29/2015 10:49
MHALL3
1
EPA 200.7
05/29/2015 10:49
MHALL3
1
EPA 200.7
05/29/2015 10:49
MHALL3
10
EPA 200.7
06/01/2015 11:24
MHALL3
1
EPA 200.7
06/01/2015 11:24
MHALL3
1
EPA 200.7
06/01/2015 11:24
MHALL3
1
EPA 200.7
06/01/2015 11:24
MHALL3
1
EPA 200.7
06/02/2015 09:22
MHH7131
1
EPA 200.7
06/02/2015 09:22
MHH7131
1
EPA 200.7
06/02/2015 09:22
MHH7131
1
EPA 200.7
06/02/2015 09:22
MHH7131
1
EPA 200.7
06/02/2015 09:22
MHH7131
1
EPA 200.7
06/02/2015 09:22
MHH7131
1
EPA 200.7
06/02/2015 09:22
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050736
Site: ABMW-02
Collection Date: 27 -May -15 9:41 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
1020
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
6.46
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
172
Nickel (Ni)
2.72
Selenium (Se)
< 1
Thallium (TI) Low Level
0.434
Vanadium (V) Low Level
0.927
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
Arsenic (As)
1240
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
5.12
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
194
Nickel (Ni)
2.48
Selenium (Se)
< 1
Thallium (TI) Low Level
1.11
Vanadium (V) Low Level
2.15
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
770
Total Carbon
06/05/2015 16:25
TOC
0.725
TOTAL SUSPENDED SOLIDS
1
TSS
22
Page 5 of 69
ug/L
1
1
Sample #:
2015016286
SLS2560
ug/L
10
Matrix:
GW -WW
06/08/2015 13:33
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
06/05/2015 16:25
JAHERMA
ug/L
10
10
EPA 200.8
06/05/2015 16:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:25
JAHERMA
ug/L
0.2
1
EPA 200.8
06/05/2015 16:25
JAHERMA
ug/L
0.3
1
EPA 200.8
06/05/2015 16:25
JAHERMA
ug/L
1
1
EPA 200.8
06/08/2015 13:33
SLS2560
ug/L
10
10
EPA 200.8
06/08/2015 13:33
SLS2560
ug/L
1
1
EPA 200.8
06/08/2015 13:33
SLS2560
ug/L
1
1
EPA 200.8
06/08/2015 13:33
SLS2560
ug/L
1
1
EPA 200.8
06/08/2015 13:33
SLS2560
ug/L
1
1
EPA 200.8
06/08/2015 13:33
SLS2560
ug/L
1
1
EPA 200.8
06/08/2015 13:33
SLS2560
ug/L
1
1
EPA 200.8
06/08/2015 13:33
SLS2560
ug/L
1
1
EPA 200.8
06/08/2015 13:33
SLS2560
ug/L
1
1
EPA 200.8
06/08/2015 13:33
SLS2560
ug/L
1
1
EPA 200.8
06/08/2015 13:33
SLS2560
ug/L
0.2
1
EPA 200.8
06/08/2015 13:33
SLS2560
ug/L
0.3
1
EPA 200.8
06/08/2015 13:33
SLS2560
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
05/28/201514:15
AGIBBS5
mg/L
0.1
1
SM5310C/EPA9060A
06/03/201516:49
TJA7067
mg/L
5
1
SM2540D
06/01/2015 08:52
AGIBBS5

Certificate of Laboratory Analysis Page 6 of 69
This report shall not be reproduced, except in full.
Order # J15050736
Site: ABMW-05BR
Collection Date: 27 -May -15 9:45 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 300.0
06/01/2015 21:38
Vendor Parameter
Complete
EPA 300.0
06/01/2015 21:38
NITRITE + NITRATE (COLORIMETRIC)
1
EPA 245.1
Nitrite + Nitrate (Colorimetric)
0.028
mg-N/L
0.01
INORGANIC IONS BY IC
ACPAYNE
1
EPA 200.7
Chloride
8.7
mg/L
0.1
Sulfate
19
mg/L
1
MERCURY (COLD VAPOR) IN WATER
MHALL3
1
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
05/29/2015 11:01
MHALL3
Mercury (Hg)
< 0.05
ug/L
M2 0.05
DISSOLVED METALS BY ICP
EPA 200.7
05/29/2015 11:01
MHALL3
Aluminum (AI)
0.009
mg/L
0.005
Barium (Ba)
0.029
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
7.74
mg/L
0.01
Manganese (Mn)
0.149
mg/L
0.005
Strontium (Sr)
0.192
mg/L
0.005
Zinc (Zn)
0.008
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
06/02/2015 09:34
MHH7131
Calcium (Ca)
21.9
mg/L
0.01
Magnesium (Mg)
6.01
mg/L
0.005
Potassium (K)
7.93
mg/L
0.1
Sodium (Na)
18.3
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.062
mg/L
0.005
Barium (Ba)
0.031
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
11.4
mg/L
0.01
Manganese (Mn)
0.157
mg/L
0.005
Strontium (Sr)
0.210
mg/L
0.005
Zinc (Zn)
0.017
mg/L
0.005
Sample #: 2015016287
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/01/2015 13:35
LSTARL1
1
EPA 300.0
06/01/2015 21:38
BGN9034
10
EPA 300.0
06/01/2015 21:38
BGN9034
1
EPA 245.1
05/29/2015 15:34
ACPAYNE
1
EPA 245.1
06/01/2015 15:59
ACPAYNE
1
EPA 200.7
05/29/2015 11:01
MHALL3
1
EPA 200.7
05/29/2015 11:01
MHALL3
1
EPA 200.7
05/29/2015 11:01
MHALL3
1
EPA 200.7
05/29/2015 11:01
MHALL3
1
EPA 200.7
05/29/2015 11:01
MHALL3
1
EPA 200.7
05/29/2015 11:01
MHALL3
1
EPA 200.7
05/29/2015 11:01
MHALL3
1
EPA 200.7
06/01/2015 11:28
MHALL3
1
EPA 200.7
06/01/2015 11:28
MHALL3
1
EPA 200.7
06/01/2015 11:28
MHALL3
1
EPA 200.7
06/01/2015 11:28
MHALL3
1
EPA 200.7
06/02/2015 09:34
MHH7131
1
EPA 200.7
06/02/2015 09:34
MHH7131
1
EPA 200.7
06/02/2015 09:34
MHH7131
1
EPA 200.7
06/02/2015 09:34
MHH7131
1
EPA 200.7
06/02/2015 09:34
MHH7131
1
EPA 200.7
06/02/2015 09:34
MHH7131
1
EPA 200.7
06/02/2015 09:34
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050736
Site: ABMW-05BR
Collection Date: 27 -May -15 9:45 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
3.54
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
5.61
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
10.5
Cobalt (Co)
4.21
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
4.21
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
180
Total Carbon
06/05/2015 16:57
TOC
1.5
TOTAL SUSPENDED SOLIDS
1
TSS
27
Page 7 of 69
ug/L
1
1
Sample #:
2015016287
JAHERMA
ug/L
1
1
Matrix:
GW -WW
JAHERMA
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
06/05/2015 16:57
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:57
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:57
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:57
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:57
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:57
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:57
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:57
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:57
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:57
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 16:57
JAHERMA
ug/L
0.2
1
EPA 200.8
06/05/2015 16:57
JAHERMA
ug/L
0.3
1
EPA 200.8
06/05/2015 16:57
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:10
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:10
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:10
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:10
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:10
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:10
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:10
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:10
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:10
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:10
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:10
JAHERMA
ug/L
0.2
1
EPA 200.8
06/06/2015 13:10
JAHERMA
ug/L
0.3
1
EPA 200.8
06/06/2015 13:10
JAHERMA
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
05/28/201514:15
AGIBBS5
mg/L
0.1
1
SM5310C/EPA9060A
06/03/201516:49
TJA7067
mg/L
5
1
SM2540D
06/01/2015 08:52
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050736
Site: ABMW-07S
Collection Date: 27 -May -15 11:45 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 300.0
06/02/2015 09:42
Vendor Parameter
Complete
EPA 300.0
06/02/2015 09:42
NITRITE + NITRATE (COLORIMETRIC)
1
EPA 245.1
Nitrite + Nitrate (Colorimetric)
0.326
mg-N/L
0.01
INORGANIC IONS BY IC
ACPAYNE
1
EPA 200.7
Chloride
7.3
mg/L
0.1
Sulfate
120
mg/L
2.5
MERCURY (COLD VAPOR) IN WATER
MHALL3
1
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
05/29/2015 11:08
MHALL3
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
EPA 200.7
05/29/2015 11:08
MHALL3
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
0.045
mg/L
0.005
Boron (B)
0.783
mg/L
0.05
Iron (Fe)
0.093
mg/L
0.01
Manganese (Mn)
0.740
mg/L
0.005
Strontium (Sr)
0.433
mg/L
0.005
Zinc (Zn)
0.022
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
06/02/2015 09:38
MHH7131
Calcium (Ca)
30.6
mg/L
0.01
Magnesium (Mg)
6.59
mg/L
0.005
Potassium (K)
10.1
mg/L
0.1
Sodium (Na)
11.6
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.008
mg/L
0.005
Barium (Ba)
0.047
mg/L
0.005
Boron (B)
0.789
mg/L
0.05
Iron (Fe)
0.170
mg/L
0.01
Manganese (Mn)
0.763
mg/L
0.005
Strontium (Sr)
0.442
mg/L
0.005
Zinc (Zn)
0.007
mg/L
0.005
Sample #: 2015016288
Matrix: GW -WW
Page 8 of 69
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/01/2015 13:36
LSTARL1
1
EPA 300.0
06/02/2015 09:42
BGN9034
25
EPA 300.0
06/02/2015 09:42
BGN9034
1
EPA 245.1
05/29/2015 15:37
ACPAYNE
1
EPA 245.1
06/01/2015 16:31
ACPAYNE
1
EPA 200.7
05/29/2015 11:08
MHALL3
1
EPA 200.7
05/29/2015 11:08
MHALL3
1
EPA 200.7
05/29/2015 11:08
MHALL3
1
EPA 200.7
05/29/2015 11:08
MHALL3
1
EPA 200.7
05/29/2015 11:08
MHALL3
1
EPA 200.7
05/29/2015 11:08
MHALL3
1
EPA 200.7
05/29/2015 11:08
MHALL3
1
EPA 200.7
06/01/2015 11:32
MHALL3
1
EPA 200.7
06/01/2015 11:32
MHALL3
1
EPA 200.7
06/01/2015 11:32
MHALL3
1
EPA 200.7
06/01/2015 11:32
MHALL3
1
EPA 200.7
06/02/2015 09:38
MHH7131
1
EPA 200.7
06/02/2015 09:38
MHH7131
1
EPA 200.7
06/02/2015 09:38
MHH7131
1
EPA 200.7
06/02/2015 09:38
MHH7131
1
EPA 200.7
06/02/2015 09:38
MHH7131
1
EPA 200.7
06/02/2015 09:38
MHH7131
1
EPA 200.7
06/02/2015 09:38
MHH7131

Certificate of Laboratory Analysis Page 9 of 69
This report shall not be reproduced, except in full.
Order # J15050736
Site: ABMW-07S
Sample #: 2015016288
Collection Date: 27 -May -15 11:45
AM
Matrix: GW -WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP -MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 17:11
JAHERMA
Arsenic (As)
<1
ug/L
1
1
EPA 200.8
06/05/2015 17:11
JAHERMA
Beryllium (Be)
<1
ug/L
1
1
EPA 200.8
06/05/2015 17:11
JAHERMA
Cadmium (Cd)
<1
ug/L
1
1
EPA 200.8
06/05/2015 17:11
JAHERMA
Chromium (Cr)
<1
ug/L
1
1
EPA 200.8
06/05/2015 17:11
JAHERMA
Cobalt (Co)
3.17
ug/L
1
1
EPA 200.8
06/05/2015 17:11
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 17:11
JAHERMA
Lead (Pb)
<1
ug/L
1
1
EPA 200.8
06/05/2015 17:11
JAHERMA
Molybdenum (Mo)
119
ug/L
1
1
EPA 200.8
06/05/2015 17:11
JAHERMA
Nickel (Ni)
<1
ug/L
1
1
EPA 200.8
06/05/2015 17:11
JAHERMA
Selenium (Se)
1.75
ug/L
1
1
EPA 200.8
06/05/2015 17:11
JAHERMA
Thallium (TI) Low Level
0.426
ug/L
0.2
1
EPA 200.8
06/05/2015 17:11
JAHERMA
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
06/05/2015 17:11
JAHERMA
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
ug/L
1
1
EPA 200.8
06/06/2015 13:29
JAHERMA
Arsenic (As)
<1
ug/L
1
1
EPA 200.8
06/06/2015 13:29
JAHERMA
Beryllium (Be)
<1
ug/L
1
1
EPA 200.8
06/06/2015 13:29
JAHERMA
Cadmium (Cd)
<1
ug/L
1
1
EPA 200.8
06/06/2015 13:29
JAHERMA
Chromium (Cr)
<1
ug/L
1
1
EPA 200.8
06/06/2015 13:29
JAHERMA
Cobalt (Co)
3.50
ug/L
1
1
EPA 200.8
06/06/2015 13:29
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 13:29
JAHERMA
Lead (Pb)
<1
ug/L
1
1
EPA 200.8
06/06/2015 13:29
JAHERMA
Molybdenum (Mo)
122
ug/L
1
1
EPA 200.8
06/06/2015 13:29
JAHERMA
Nickel (Ni)
<1
ug/L
1
1
EPA 200.8
06/06/2015 13:29
JAHERMA
Selenium (Se)
1.65
ug/L
1
1
EPA 200.8
06/06/2015 13:29
JAHERMA
Thallium (TI) Low Level
0.664
ug/L
0.2
1
EPA 200.8
06/06/2015 13:29
JAHERMA
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
06/06/2015 13:29
JAHERMA
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
200
mg/L
25
1
SM2540C
05/28/201514:15
AGIBBS5
Total Carbon
TOC
0.424
mg/L
0.1
1
SM5310C/EPA9060A
06/03/201516:49
TJA7067
TOTAL SUSPENDED SOLIDS
TSS
< 5
mg/L
5
1
SM2540D
06/01/2015 08:52
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050736
Site: MW -08S
Collection Date: 27 -May -15 12:50 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 300.0
06/02/2015 09:58
Vendor Parameter
Complete
EPA 300.0
06/02/2015 09:58
NITRITE + NITRATE (COLORIMETRIC)
1
EPA 245.1
Nitrite + Nitrate (Colorimetric)
0.123
mg-N/L
0.01
INORGANIC IONS BY IC
ACPAYNE
1
EPA 200.7
Chloride
450
mg/L
5
Sulfate
290
mg/L
5
MERCURY (COLD VAPOR) IN WATER
MHALL3
1
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
05/29/2015 11:12
MHALL3
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
EPA 200.7
05/29/2015 11:12
MHALL3
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
0.222
mg/L
0.005
Boron (B)
5.21
mg/L
0.05
Iron (Fe)
0.030
mg/L
0.01
Manganese (Mn)
2.97
mg/L
0.005
Strontium (Sr)
4.14
mg/L
0.005
Zinc (Zn)
0.011
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
06/02/2015 09:42
MHH7131
Calcium (Ca)
245
mg/L
0.1
Magnesium (Mg)
78.5
mg/L
0.005
Potassium (K)
1.91
mg/L
0.1
Sodium (Na)
15.0
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.007
mg/L
0.005
Barium (Ba)
0.223
mg/L
0.005
Boron (B)
5.33
mg/L
0.05
Iron (Fe)
0.017
mg/L
0.01
Manganese (Mn)
2.83
mg/L
0.005
Strontium (Sr)
4.16
mg/L
0.005
Zinc (Zn)
0.014
mg/L
0.005
Sample #: 2015016289
Matrix: GW -WW
Page 10 of 69
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/01/2015 13:38
LSTARL1
50
EPA 300.0
06/02/2015 09:58
BGN9034
50
EPA 300.0
06/02/2015 09:58
BGN9034
1
EPA 245.1
05/29/2015 15:39
ACPAYNE
1
EPA 245.1
06/01/2015 16:33
ACPAYNE
1
EPA 200.7
05/29/2015 11:12
MHALL3
1
EPA 200.7
05/29/2015 11:12
MHALL3
1
EPA 200.7
05/29/2015 11:12
MHALL3
1
EPA 200.7
05/29/2015 11:12
MHALL3
1
EPA 200.7
05/29/2015 11:12
MHALL3
1
EPA 200.7
05/29/2015 11:12
MHALL3
1
EPA 200.7
05/29/2015 11:12
MHALL3
10
EPA 200.7
06/01/2015 10:37
MHALL3
1
EPA 200.7
06/01/2015 10:37
MHALL3
1
EPA 200.7
06/01/2015 10:37
MHALL3
1
EPA 200.7
06/01/2015 10:37
MHALL3
1
EPA 200.7
06/02/2015 09:42
MHH7131
1
EPA 200.7
06/02/2015 09:42
MHH7131
1
EPA 200.7
06/02/2015 09:42
MHH7131
1
EPA 200.7
06/02/2015 09:42
MHH7131
1
EPA 200.7
06/02/2015 09:42
MHH7131
1
EPA 200.7
06/02/2015 09:42
MHH7131
1
EPA 200.7
06/02/2015 09:42
MHH7131

Certificate of Laboratory Analysis Page 11 of 69
This report shall not be reproduced, except in full.
Order # J15050736
Site: MW -08S
Sample #: 2015016289
Collection Date: 27 -May -15 12:50
PM
Matrix: GW -WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP -MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 17:16
JAHERMA
Arsenic (As)
<1
ug/L
1
1
EPA 200.8
06/05/2015 17:16
JAHERMA
Beryllium (Be)
<1
ug/L
1
1
EPA 200.8
06/05/2015 17:16
JAHERMA
Cadmium (Cd)
<1
ug/L
1
1
EPA 200.8
06/05/2015 17:16
JAHERMA
Chromium (Cr)
<1
ug/L
1
1
EPA 200.8
06/05/2015 17:16
JAHERMA
Cobalt (Co)
3.00
ug/L
1
1
EPA 200.8
06/05/2015 17:16
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
06/05/2015 17:16
JAHERMA
Lead (Pb)
<1
ug/L
1
1
EPA 200.8
06/05/2015 17:16
JAHERMA
Molybdenum (Mo)
3.03
ug/L
1
1
EPA 200.8
06/05/2015 17:16
JAHERMA
Nickel (Ni)
1.89
ug/L
1
1
EPA 200.8
06/05/2015 17:16
JAHERMA
Selenium (Se)
1.21
ug/L
1
1
EPA 200.8
06/05/2015 17:16
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
06/05/2015 17:16
JAHERMA
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
06/05/2015 17:16
JAHERMA
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
ug/L
1
1
EPA 200.8
06/06/2015 13:33
JAHERMA
Arsenic (As)
<1
ug/L
1
1
EPA 200.8
06/06/2015 13:33
JAHERMA
Beryllium (Be)
<1
ug/L
1
1
EPA 200.8
06/06/2015 13:33
JAHERMA
Cadmium (Cd)
<1
ug/L
1
1
EPA 200.8
06/06/2015 13:33
JAHERMA
Chromium (Cr)
<1
ug/L
1
1
EPA 200.8
06/06/2015 13:33
JAHERMA
Cobalt (Co)
3.09
ug/L
1
1
EPA 200.8
06/06/2015 13:33
JAHERMA
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
06/06/2015 13:33
JAHERMA
Lead (Pb)
<1
ug/L
1
1
EPA 200.8
06/06/2015 13:33
JAHERMA
Molybdenum (Mo)
3.20
ug/L
1
1
EPA 200.8
06/06/2015 13:33
JAHERMA
Nickel (Ni)
1.65
ug/L
1
1
EPA 200.8
06/06/2015 13:33
JAHERMA
Selenium (Se)
1.41
ug/L
1
1
EPA 200.8
06/06/2015 13:33
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
06/06/2015 13:33
JAHERMA
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
06/06/2015 13:33
JAHERMA
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
1900
mg/L
25
1
SM2540C
05/28/201514:15
AGIBBS5
Total Carbon
TOC
0.294
mg/L
0.1
1
SM5310C/EPA9060A
06/03/201516:49
TJA7067
TOTAL SUSPENDED SOLIDS
TSS
< 5
mg/L
5
1
SM2540D
06/01/2015 08:52
AGIBBS5

Certificate of Laboratory Analysis Page 12 of 69
This report shall not be reproduced, except in full.
Order # J15050736
Site: MW -05D
Collection Date: 27 -May -15 2:12 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
1
EPA
Vendor Parameter
Complete
BGN9034
25
NITRITE + NITRATE (COLORIMETRIC)
300.0
06/02/2015 10:31
Nitrite + Nitrate (Colorimetric)
1.0
mg-N/L
0.01
INORGANIC IONS BY IC
ACPAYNE
1
EPA
Chloride
9.2
mg/L
0.1
Sulfate
190
mg/L
2.5
MERCURY (COLD VAPOR) IN WATER
EPA
200.7
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
05/29/2015 11:16
MHALL3
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
1
EPA
200.7
Aluminum (AI)
0.501
mg/L
0.005
Barium (Ba)
0.047
mg/L
0.005
Boron (B)
0.524
mg/L
0.05
Iron (Fe)
0.534
mg/L
0.01
Manganese (Mn)
0.459
mg/L
0.005
Strontium (Sr)
0.265
mg/L
0.005
Zinc (Zn)
0.064
mg/L
0.005
UNDIGESTED METALS BY ICP
200.7
06/01/2015 11:45
MHALL3
Calcium (Ca)
27.9
mg/L
0.01
Magnesium (Mg)
7.61
mg/L
0.005
Potassium (K)
2.79
mg/L
0.1
Sodium (Na)
22.7
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
200.7
06/02/2015 09:46
Aluminum (AI)
0.481
mg/L
0.005
Barium (Ba)
0.047
mg/L
0.005
Boron (B)
0.518
mg/L
0.05
Iron (Fe)
0.484
mg/L
0.01
Manganese (Mn)
0.456
mg/L
0.005
Strontium (Sr)
0.267
mg/L
0.005
Zinc (Zn)
0.063
mg/L
0.005
Sample #: 2015016290
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA
353.2
06/01/2015 13:39
LSTARL1
1
EPA
300.0
06/02/2015 10:31
BGN9034
25
EPA
300.0
06/02/2015 10:31
BGN9034
1
EPA
245.1
05/29/2015 15:41
ACPAYNE
1
EPA
245.1
06/01/2015 16:35
ACPAYNE
1
EPA
200.7
05/29/2015 11:16
MHALL3
1
EPA
200.7
05/29/2015 11:16
MHALL3
1
EPA
200.7
05/29/2015 11:16
MHALL3
1
EPA
200.7
05/29/2015 11:16
MHALL3
1
EPA
200.7
05/29/2015 11:16
MHALL3
1
EPA
200.7
05/29/2015 11:16
MHALL3
1
EPA
200.7
05/29/2015 11:16
MHALL3
1
EPA
200.7
06/01/2015 11:45
MHALL3
1
EPA
200.7
06/01/2015 11:45
MHALL3
1
EPA
200.7
06/01/2015 11:45
MHALL3
1
EPA
200.7
06/01/2015 11:45
MHALL3
1
EPA
200.7
06/02/2015 09:46
MHH7131
1
EPA
200.7
06/02/2015 09:46
MHH7131
1
EPA
200.7
06/02/2015 09:46
MHH7131
1
EPA
200.7
06/02/2015 09:46
MHH7131
1
EPA
200.7
06/02/2015 09:46
MHH7131
1
EPA
200.7
06/02/2015 09:46
MHH7131
1
EPA
200.7
06/02/2015 09:46
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050736
Site: MW -05D
Collection Date: 27 -May -15 2:12 PM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
39.0
Copper (Cu)
12.6
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
27.3
Selenium (Se)
2.10
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
39.1
Copper (Cu)
10.5
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
26.1
Selenium (Se)
2.00
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
250
Total Carbon
06/05/2015 17:20
TOC
0.279
TOTAL SUSPENDED SOLIDS
1
TSS
< 5
Page 13 of 69
ug/L
1
1
Sample #:
2015016290
JAHERMA
ug/L
1
1
Matrix:
GW -WW
JAHERMA
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
06/05/2015 17:20
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:20
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:20
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:20
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:20
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:20
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:20
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:20
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:20
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:20
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:20
JAHERMA
ug/L
0.2
1
EPA 200.8
06/05/2015 17:20
JAHERMA
ug/L
0.3
1
EPA 200.8
06/05/2015 17:20
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:38
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:38
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:38
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:38
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:38
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:38
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:38
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:38
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:38
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:38
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:38
JAHERMA
ug/L
0.2
1
EPA 200.8
06/06/2015 13:38
JAHERMA
ug/L
0.3
1
EPA 200.8
06/06/2015 13:38
JAHERMA
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
05/28/201514:15
AGIBBS5
mg/L
0.1
1
SM5310C/EPA9060A
06/03/201516:49
TJA7067
mg/L
5
1
SM2540D
06/01/2015 08:52
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050736
Site: ABMW-02S-DUP
Collection Date: 27 -May -15 12:05 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 353.2
06/01/2015 13:40
Vendor Parameter
Complete
EPA 300.0
06/02/2015 11:36
NITRITE + NITRATE (COLORIMETRIC)
100
EPA 300.0
Nitrite + Nitrate (Colorimetric)
1.3
mg-N/L
0.01
INORGANIC IONS BY IC
ACPAYNE
1
EPA 245.1
Chloride
14
mg/L
1
Sulfate
720
mg/L
10
MERCURY (COLD VAPOR) IN WATER
MHALL3
1
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
05/29/2015 11:20
MHALL3
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
EPA 200.7
05/29/2015 11:20
MHALL3
Aluminum (AI)
15.7
mg/L
0.005
Barium (Ba)
0.016
mg/L
0.005
Boron (B)
0.767
mg/L
0.05
Iron (Fe)
0.206
mg/L
0.01
Manganese (Mn)
16.7
mg/L
0.005
Strontium (Sr)
0.253
mg/L
0.005
Zinc (Zn)
0.514
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
06/02/2015 09:50
MHH7131
Calcium (Ca)
83.2
mg/L
0.01
Magnesium (Mg)
22.7
mg/L
0.005
Potassium (K)
5.08
mg/L
0.1
Sodium (Na)
15.7
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
15.3
mg/L
0.005
Barium (Ba)
0.017
mg/L
0.005
Boron (B)
0.761
mg/L
0.05
Iron (Fe)
0.453
mg/L
0.01
Manganese (Mn)
16.5
mg/L
0.005
Strontium (Sr)
0.262
mg/L
0.005
Zinc (Zn)
0.484
mg/L
0.005
Page 14 of 69
Sample #: 2015016291
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/01/2015 13:40
LSTARL1
10
EPA 300.0
06/02/2015 11:36
BGN9034
100
EPA 300.0
06/02/2015 11:36
BGN9034
1
EPA 245.1
05/29/2015 15:53
ACPAYNE
1
EPA 245.1
06/01/2015 16:38
ACPAYNE
1
EPA 200.7
05/29/2015 11:20
MHALL3
1
EPA 200.7
05/29/2015 11:20
MHALL3
1
EPA 200.7
05/29/2015 11:20
MHALL3
1
EPA 200.7
05/29/2015 11:20
MHALL3
1
EPA 200.7
05/29/2015 11:20
MHALL3
1
EPA 200.7
05/29/2015 11:20
MHALL3
1
EPA 200.7
05/29/2015 11:20
MHALL3
1
EPA 200.7
06/01/2015 11:57
MHALL3
1
EPA 200.7
06/01/2015 11:57
MHALL3
1
EPA 200.7
06/01/2015 11:57
MHALL3
1
EPA 200.7
06/01/2015 11:57
MHALL3
1
EPA 200.7
06/02/2015 09:50
MHH7131
1
EPA 200.7
06/02/2015 09:50
MHH7131
1
EPA 200.7
06/02/2015 09:50
MHH7131
1
EPA 200.7
06/02/2015 09:50
MHH7131
1
EPA 200.7
06/02/2015 09:50
MHH7131
1
EPA 200.7
06/02/2015 09:50
MHH7131
1
EPA 200.7
06/02/2015 09:50
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050736
Site: ABMW-02S-DUP
Collection Date: 27 -May -15 12:05 PM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
15.5
Beryllium (Be)
11.6
Cadmium (Cd)
3.21
Chromium (Cr)
< 1
Cobalt (Co)
563
Copper (Cu)
3.88
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
236
Selenium (Se)
10.4
Thallium (TI) Low Level
0.256
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
Arsenic (As)
16.0
Beryllium (Be)
12.6
Cadmium (Cd)
3.24
Chromium (Cr)
< 1
Cobalt (Co)
576
Copper (Cu)
4.54
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
245
Selenium (Se)
10.3
Thallium (TI) Low Level
0.329
Vanadium (V) Low Level
0.421
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
660
Total Carbon
06/05/2015 17:25
TOC
0.363
TOTAL SUSPENDED SOLIDS
1
TSS
7.0
Page 15 of 69
ug/L
1
1
Sample #:
2015016291
JAHERMA
ug/L
1
1
Matrix:
GW -WW
JAHERMA
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
06/05/2015 17:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:25
JAHERMA
ug/L
10
10
EPA 200.8
06/05/2015 17:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:25
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:25
JAHERMA
ug/L
0.2
1
EPA 200.8
06/05/2015 17:25
JAHERMA
ug/L
0.3
1
EPA 200.8
06/05/2015 17:25
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:43
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:43
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:43
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:43
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:43
JAHERMA
ug/L
10
10
EPA 200.8
06/06/2015 13:43
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:43
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:43
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:43
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:43
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:43
JAHERMA
ug/L
0.2
1
EPA 200.8
06/06/2015 13:43
JAHERMA
ug/L
0.3
1
EPA 200.8
06/06/2015 13:43
JAHERMA
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
05/28/201514:15
AGIBBS5
mg/L
0.1
1
SM5310C/EPA9060A
06/03/201516:49
TJA7067
mg/L
5
1
SM2540D
06/01/2015 08:52
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050736
Site: ABMW-02S
Collection Date: 27 -May -15 11:40 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 353.2
06/01/2015 13:41
Vendor Parameter
Complete
EPA 300.0
06/02/2015 12:09
NITRITE + NITRATE (COLORIMETRIC)
100
EPA 300.0
Nitrite + Nitrate (Colorimetric)
1.4
mg-N/L
0.01
INORGANIC IONS BY IC
ACPAYNE
1
EPA 245.1
Chloride
14
mg/L
1
Sulfate
730
mg/L
10
MERCURY (COLD VAPOR) IN WATER
MHALL3
1
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
05/29/2015 11:24
MHALL3
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
EPA 200.7
05/29/2015 11:24
MHALL3
Aluminum (AI)
15.6
mg/L
0.005
Barium (Ba)
0.016
mg/L
0.005
Boron (B)
0.770
mg/L
0.05
Iron (Fe)
0.198
mg/L
0.01
Manganese (Mn)
16.6
mg/L
0.005
Strontium (Sr)
0.254
mg/L
0.005
Zinc (Zn)
0.517
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
06/02/2015 09:54
MHH7131
Calcium (Ca)
81.5
mg/L
0.01
Magnesium (Mg)
22.2
mg/L
0.005
Potassium (K)
5.05
mg/L
0.1
Sodium (Na)
15.7
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
15.1
mg/L
0.005
Barium (Ba)
0.019
mg/L
0.005
Boron (B)
0.751
mg/L
0.05
Iron (Fe)
0.557
mg/L
0.01
Manganese (Mn)
16.2
mg/L
0.005
Strontium (Sr)
0.259
mg/L
0.005
Zinc (Zn)
0.480
mg/L
0.005
Page 16 of 69
Sample #: 2015016292
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
06/01/2015 13:41
LSTARL1
10
EPA 300.0
06/02/2015 12:09
BGN9034
100
EPA 300.0
06/02/2015 12:09
BGN9034
1
EPA 245.1
05/29/2015 16:00
ACPAYNE
1
EPA 245.1
06/01/2015 16:40
ACPAYNE
1
EPA 200.7
05/29/2015 11:24
MHALL3
1
EPA 200.7
05/29/2015 11:24
MHALL3
1
EPA 200.7
05/29/2015 11:24
MHALL3
1
EPA 200.7
05/29/2015 11:24
MHALL3
1
EPA 200.7
05/29/2015 11:24
MHALL3
1
EPA 200.7
05/29/2015 11:24
MHALL3
1
EPA 200.7
05/29/2015 11:24
MHALL3
1
EPA 200.7
06/01/2015 12:01
MHALL3
1
EPA 200.7
06/01/2015 12:01
MHALL3
1
EPA 200.7
06/01/2015 12:01
MHALL3
1
EPA 200.7
06/01/2015 12:01
MHALL3
1
EPA 200.7
06/02/2015 09:54
MHH7131
1
EPA 200.7
06/02/2015 09:54
MHH7131
1
EPA 200.7
06/02/2015 09:54
MHH7131
1
EPA 200.7
06/02/2015 09:54
MHH7131
1
EPA 200.7
06/02/2015 09:54
MHH7131
1
EPA 200.7
06/02/2015 09:54
MHH7131
1
EPA 200.7
06/02/2015 09:54
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050736
Site: ABMW-02S
Collection Date: 27 -May -15 11:40 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
15.4
Beryllium (Be)
11.7
Cadmium (Cd)
3.17
Chromium (Cr)
< 1
Cobalt (Co)
567
Copper (Cu)
4.16
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
232
Selenium (Se)
10.1
Thallium (TI) Low Level
0.243
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
Arsenic (As)
16.0
Beryllium (Be)
12.5
Cadmium (Cd)
3.30
Chromium (Cr)
< 1
Cobalt (Co)
578
Copper (Cu)
4.56
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
247
Selenium (Se)
10.8
Thallium (TI) Low Level
0.333
Vanadium (V) Low Level
0.666
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
670
Total Carbon
06/05/2015 17:30
TOC
0.359
TOTAL SUSPENDED SOLIDS
1
TSS
12
Page 17 of 69
ug/L
1
1
Sample #:
2015016292
JAHERMA
ug/L
1
1
Matrix:
GW -WW
JAHERMA
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
06/05/2015 17:30
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:30
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:30
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:30
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:30
JAHERMA
ug/L
10
10
EPA 200.8
06/05/2015 17:30
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:30
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:30
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:30
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:30
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:30
JAHERMA
ug/L
0.2
1
EPA 200.8
06/05/2015 17:30
JAHERMA
ug/L
0.3
1
EPA 200.8
06/05/2015 17:30
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:47
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:47
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:47
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:47
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:47
JAHERMA
ug/L
10
10
EPA 200.8
06/06/2015 13:47
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:47
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:47
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:47
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:47
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:47
JAHERMA
ug/L
0.2
1
EPA 200.8
06/06/2015 13:47
JAHERMA
ug/L
0.3
1
EPA 200.8
06/06/2015 13:47
JAHERMA
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
05/28/201514:15
AGIBBS5
mg/L
0.1
1
SM5310C/EPA9060A
06/03/201516:49
TJA7067
mg/L
5
1
SM2540D
06/01/2015 08:52
AGIBBS5

Certificate of Laboratory Analysis Page 18 of 69
This report shall not be reproduced, except in full.
Order # J15050736
Site: GW -01 BR
Collection Date: 27 -May -15 2:44 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
BGN9034
1 EPA 300.0
Vendor Parameter
Complete
1 EPA 245.1
05/29/2015 16:03
NITRITE + NITRATE (COLORIMETRIC)
1 EPA 245.1
06/01/2015 16:42
Nitrite + Nitrate (Colorimetric)
0.019
mg-N/L
0.01
INORGANIC IONS BY IC
05/29/2015 11:28
MHALL3
1 EPA 200.7
Chloride
1.5
mg/L
0.1
Sulfate
8.3
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
05/29/2015 11:28
MHALL3
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
MHALL3
1 EPA 200.7
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
1 EPA 200.7
06/01/2015 12:05
MHALL3
Aluminum (AI)
0.010
mg/L
0.005
Barium (Ba)
0.011
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.445
mg/L
0.01
Manganese (Mn)
0.063
mg/L
0.005
Strontium (Sr)
0.091
mg/L
0.005
Zinc (Zn)
0.013
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
18.5
mg/L
0.01
Magnesium (Mg)
3.52
mg/L
0.005
Potassium (K)
3.33
mg/L
0.1
Sodium (Na)
6.25
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.069
mg/L
0.005
Barium (Ba)
0.011
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.946
mg/L
0.01
Manganese (Mn)
0.066
mg/L
0.005
Strontium (Sr)
0.088
mg/L
0.005
Zinc (Zn)
0.009
mg/L
0.005
Sample #: 2015016293
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
06/01/2015 13:42
LSTARL1
1 EPA 300.0
06/01/2015 23:17
BGN9034
1 EPA 300.0
06/01/2015 23:17
BGN9034
1 EPA 245.1
05/29/2015 16:03
ACPAYNE
1 EPA 245.1
06/01/2015 16:42
ACPAYNE
1 EPA 200.7
05/29/2015 11:28
MHALL3
1 EPA 200.7
05/29/2015 11:28
MHALL3
1 EPA 200.7
05/29/2015 11:28
MHALL3
1 EPA 200.7
05/29/2015 11:28
MHALL3
1 EPA 200.7
05/29/2015 11:28
MHALL3
1 EPA 200.7
05/29/2015 11:28
MHALL3
1 EPA 200.7
05/29/2015 11:28
MHALL3
1 EPA 200.7
06/01/2015 12:05
MHALL3
1 EPA 200.7
06/01/2015 12:05
MHALL3
1 EPA 200.7
06/01/2015 12:05
MHALL3
1 EPA 200.7
06/01/2015 12:05
MHALL3
1 EPA 200.7
06/02/2015 09:58
MHH7131
1 EPA 200.7
06/02/2015 09:58
MHH7131
1 EPA 200.7
06/02/2015 09:58
MHH7131
1 EPA 200.7
06/02/2015 09:58
MHH7131
1 EPA 200.7
06/02/2015 09:58
MHH7131
1 EPA 200.7
06/02/2015 09:58
MHH7131
1 EPA 200.7
06/02/2015 09:58
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15050736
Site: GW -01 BR
Collection Date: 27 -May -15 2:44 PM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
1.34
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.969
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
1.28
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
1.08
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
110
Total Carbon
06/05/2015 17:34
TOC
0.401
TOTAL SUSPENDED SOLIDS
1
TSS
< 5
Page 19 of 69
ug/L
1
1
Sample #:
2015016293
JAHERMA
ug/L
1
1
Matrix:
GW -WW
JAHERMA
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
06/05/2015 17:34
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:34
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:34
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:34
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:34
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:34
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:34
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:34
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:34
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:34
JAHERMA
ug/L
1
1
EPA 200.8
06/05/2015 17:34
JAHERMA
ug/L
0.2
1
EPA 200.8
06/05/2015 17:34
JAHERMA
ug/L
0.3
1
EPA 200.8
06/05/2015 17:34
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:52
JAHERMA
ug/L
1
1
EPA 200.8
06/06/2015 13:52
JAHERMA
ug/L
0.2
1
EPA 200.8
06/06/2015 13:52
JAHERMA
ug/L
0.3
1
EPA 200.8
06/06/2015 13:52
JAHERMA
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
05/28/201514:15
AGIBBS5
mg/L
0.1
1
SM5310C/EPA9060A
06/03/201516:49
TJA7067
mg/L
5
1
SM2540D
06/01/2015 08:52
AGIBBS5

Certificate of Laboratory Analysis Page 20 of 69
This report shall not be reproduced, except in full.
Order # J15050736
Site: Filter Blank
Collection Date: 27 -May -15 9:45 AM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
EPA 245.1
06/01/2015 16:45
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
1
EPA 200.7
05/29/2015 11:31
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
DISSOLVED METALS BY ICP -MS
1
EPA 200.8
06/05/2015 17:39
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015016294
Matrix: GW WW
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
06/01/2015 16:45
ACPAYNE
1
EPA 200.7
05/29/2015 11:31
MHALL3
1
EPA 200.7
05/29/2015 11:31
MHALL3
1
EPA 200.7
05/29/2015 11:31
MHALL3
1
EPA 200.7
05/29/2015 11:31
MHALL3
1
EPA 200.7
05/29/2015 11:31
MHALL3
1
EPA 200.7
05/29/2015 11:31
MHALL3
1
EPA 200.7
05/29/2015 11:31
MHALL3
1
EPA 200.8
06/05/2015 17:39
JAHERMA
1
EPA 200.8
06/05/2015 17:39
JAHERMA
1
EPA 200.8
06/05/2015 17:39
JAHERMA
1
EPA 200.8
06/05/2015 17:39
JAHERMA
1
EPA 200.8
06/05/2015 17:39
JAHERMA
1
EPA 200.8
06/05/2015 17:39
JAHERMA
1
EPA 200.8
06/05/2015 17:39
JAHERMA
1
EPA 200.8
06/05/2015 17:39
JAHERMA
1
EPA 200.8
06/05/2015 17:39
JAHERMA
1
EPA 200.8
06/05/2015 17:39
JAHERMA
1
EPA 200.8
06/05/2015 17:39
JAHERMA
1
EPA 200.8
06/05/2015 17:39
JAHERMA
1
EPA 200.8
06/05/2015 17:39
JAHERMA

Certificate of Laboratory Analysis Page 21 of 69
This report shall not be reproduced, except in full.
Order # J15050736
Site: Equipment Blank
Collection Date: 27 -May -15 9:45 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
1 EPA 300.0
Vendor Parameter
Complete
1 EPA 300.0
06/01/2015 20:49
NITRITE + NITRATE (COLORIMETRIC)
1 EPA 245.1
05/29/2015 16:05
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
06/01/2015 12:09
MHALL3
1 EPA 200.7
Chloride
< 0.1
mg/L
0.1
Sulfate
0.28
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
06/02/2015 10:03
MHH7131
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY ICP
MHH7131
1 EPA 200.7
06/02/2015 10:03
Calcium (Ca)
0.022
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
06/06/2015 13:56
JAHERMA
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
METHANE - (Analysis Performed by Shealy Labs
Methane (CH4) Complete
Sample #: 2015016295
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
06/01/2015 13:44
LSTARL1
1 EPA 300.0
06/01/2015 20:49
BGN9034
1 EPA 300.0
06/01/2015 20:49
BGN9034
1 EPA 245.1
05/29/2015 16:05
ACPAYNE
1 EPA 200.7
06/01/2015 12:09
MHALL3
1 EPA 200.7
06/01/2015 12:09
MHALL3
1 EPA 200.7
06/01/2015 12:09
MHALL3
1 EPA 200.7
06/01/2015 12:09
MHALL3
1 EPA 200.7
06/02/2015 10:03
MHH7131
1 EPA 200.7
06/02/2015 10:03
MHH7131
1 EPA 200.7
06/02/2015 10:03
MHH7131
1 EPA 200.7
06/02/2015 10:03
MHH7131
1 EPA 200.7
06/02/2015 10:03
MHH7131
1 EPA 200.7
06/02/2015 10:03
MHH7131
1 EPA 200.7
06/02/2015 10:03
MHH7131
1 EPA 200.8
06/06/2015 13:56
JAHERMA
1 EPA 200.8
06/06/2015 13:56
JAHERMA
1 EPA 200.8
06/06/2015 13:56
JAHERMA
1 EPA 200.8
06/06/2015 13:56
JAHERMA
1 EPA 200.8
06/06/2015 13:56
JAHERMA
1 EPA 200.8
06/06/2015 13:56
JAHERMA
1 EPA 200.8
06/06/2015 13:56
JAHERMA
1 EPA 200.8
06/06/2015 13:56
JAHERMA
1 EPA 200.8
06/06/2015 13:56
JAHERMA
1 EPA 200.8
06/06/2015 13:56
JAHERMA
1 EPA 200.8
06/06/2015 13:56
JAHERMA
1 EPA 200.8
06/06/2015 13:56
JAHERMA
1 EPA 200.8
06/06/2015 13:56
JAHERMA
Vendor Method V_SHEALY

Certificate of Laboratory Analysis Page 22 of 69
This report shall not be reproduced, except in full.
Order # J15050736
Site: Equipment Blank
Collection Date: 27-Mav-15 9:45 AM
Analyte Result Units Qualifiers RDL DF
SULFIDE - (Analysis Performed by Element One)
Vendor Parameter Complete
TOTAL DISSOLVED SOLIDS
TDS < 25 mg/L 25 1
Total Carbon
Sample #: 2015016295
Matrix: GW WW
Method Analysis Date/Time Analyst
Vendor Method
V_ELE1
SM2540C 05/28/201514:15 AGIBBS5
TOC 0.108 mg/L 0.1 1 SM5310C/EPA9060A 06/03/201516:49 TJA7067
TOTAL SUSPENDED SOLIDS
TSS < 5 mg/L 5 1 SM2540D 06/01/2015 08:52 AGIBBS5
Qualifiers:
M2 Matrix spike recovery was Low: the associated Laboratory Control Spike (LCS) was acceptable.

Page 23 of 69
Element One Inc.
6319-D Carolina Beach Rd.
Wilmington, NC 28412
Rhone: 910 793-0128
Fax: [phone]
ella&�@allele
*Sample spike recovery outside of QA limits of 85-115%; dilution necessary to meet laboratory QA limits.
Ken mith, Laboratory Director
24882 Duke Report Packet Compiled by__��A-
NC Certifications: DW 37788 and DWQ DENR 604
.coma
eBe entOne
REPORT OF ANALYSES
Duke Energy
June 9, 2015
Laboratory Services
Client Project Name
AB GW
Assessment water (wells)
13339 Hagers Ferry Road Bid. MG03A
Client Project Number J15050736
Huntersville, NC 28078
PO Number
Sample Matrix GW WW
Sample Type Grab
Date Received
05/29/2015
Date Analyzed 05/29/2015
Method
SM 4500 S2- D
Time Received
0900
Delivered by FedEx
Received by
LLB
eOne ID Duke Energy ID
Parameter
Result Unit
Dil
DL Date
Time
Sampled
Sampled
24882-1 ABMW-02
Sulfide
< 0.1 mg/L
1
0.1 05/27/15
0941
24882-2* ABMW-05 BR
Sulfide
< 0.5 mg/L
5
0.1 05/27/15
0945
24882-3* ABMW-07 S
Sulfide
< 0.2 mg/L
2
0.1 05/27/15
1145
24882-4* ABMW-08 S
Sulfide
< 0.2 mg/L
2
0.1 05/27/15
1250
24882-5 ABMW-05D
Sulfide
< 0.1 mg/L
1
0.1 05/27/15
1412
24882-6* ABMW-02S DUP
Sulfide
< 0.2 mg/L
2
0.1 05/27/15
1205
24882-7* ABMW-02S
Sulfide
< 0.2 mg/L
2
0.1 05/27/15
1140
24882-8 GW -01 BR
Sulfide
< 0.1 mg/L
1
0.1 05/27/15
1444
*Sample spike recovery outside of QA limits of 85-115%; dilution necessary to meet laboratory QA limits.
Ken mith, Laboratory Director
24882 Duke Report Packet Compiled by__��A-
NC Certifications: DW 37788 and DWQ DENR 604

ma I
Duke Energy
Laboratory Services
13339 Hagers Ferry Road Bld. MG03A
Huntersville, NC 28078
Sample Matrix GW WW Sai
Date Analyzed 05/29/2015 Me
Delivered by FedEx
eOne ID Duke Energy ID
24882-9 Equipment Blank
Page 24 of 69
Hernent One Inc.
6319-D Carolina Beach Rd.
Wilmington, NC 28412
Phone: [phone]
(fax: [phone]
[e-mail]
REPORT OF ANALYSES
June 9, 2015
Client Project Name AB GW Assessment water (wells)
Client Project Number J15050736
PO Number
iple Type Grab Date Received 05/29/2015
hod SM 4500 S2- D Time Received 0900
Parameter Result Unit Dil
Received by LLB
DL Date Time
Sampled Sampled
Sulfide < 0.1 mg/L 1 0.1 05/27/15 0945
I
Ken SrAith, Laboratory Director
24882 Duke Report Packet Compiled by
NC Certifications: DW 37788 and DWQ DENR 604

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elemen One SAMPLE SUBMISSION FORM
TAT 7 BD
Hold Time Expiration 06.03.15 @ 0941
Client: Duke Energy
LIMS No J15050736
Project ID Asheville
Lab ibge 2 N98
Analysis Due Date 06.02.15
Report Due Date 06.09.15
Date Rec: 05.29.15
Time Rec: 0900
Rec By LLB
H >9a No Temp:5 6°C a No Ref. Method:
If No, Record 11 If No, Record SM4500 S2 D
Sample Identification & Cnller_tinn Infnrmatinn
Lab ID
Client ID
Collection Date
Collection Time Analysis Requested
1
ABMW-02
05/27/15
0941 Sulfide
2
ABMW-05 BR
05/27/15
0945
3
ABMW-07S
05/27/15
1145 Sulfid
4
ABMW-08S
05/27/15
1250 ulfide
5
ABMW-05D
05/27/15
1412
6
ABMW-02S-DUP
05/27/15
1205 Sulfid
7
ABMW-02S
05/27/15
1140 F ulfide
8
GW -01 BR _
05/27/15
1444 Sulf" e
9
Equipment Blank —___t05/27/15
0945 _ Sulfide
NOTE for Sulfide
The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final spike concentration at - 500 pg/L
Lab Communications
_ .................
All AB Groundwater Assessment jobs need a RL of 0.1
SS Page 1 f Prep By / Date 5 --. 9 S
SS by Labeled By / Date eZ12 S, a7- /
5/29/2015 10:45:37 AM ID Verification By /Date M" 5• -3-°►' IS

METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Duke
Lab
Lab ID#
24879 / 880 / 881 / 882 1883
Date:
5/29/15
Time Analysis Begun
1330
Time Ana1vs1s Ended
1554
X
Y
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0,095
2.50
0.218
5.00
0.415
7.50
0.610
10,00
0.778
Page 27 of 69
ELEMENT ONE
Wave Length 664
SPK LEVEL (ug)
MAX ALIQUOT
Na2S-9H2O Lot # STANDARD conc(ppm)
40721 Cal Std Lot: WC2-;
QC Std Lot: WC2-
ISTID ABSORPTION
Iwo
SAMP
ABS
ug PER ALI in mL
ALIQUOT ANALYZED
PREP
VOL in mL
Slope
ALI in mL
TAKEN
0.077810989
RESULTS
ug/mL
Correlation
LESS THAN
% SPK REC
D'sw
o.
�5W
Std. B. 0.00
0.000
0.0000
10
10
0.7.
<
0.0
Std. B. 1.00
0.096
0.9229
10
10
0.400
<
92.29%
1.0
Std. B. 2.50
0.224
2.6237
0.300
10
10
0.262
104.95%
2.5
Std. B. 5.00
0,20D
5.1616
10
10
10
0.516
103.23%
. 00
Std. B. 7.50
0.609
7.7393
10
10
10
0.000
0.00
103.19%
200
4.00
6.00
8.00
10.00 12.
x
SAMPLE
I.D.
SAMP
ABS
ug PER ALI in mL
ALIQUOT ANALYZED
PREP
VOL in mL
Slope
ALI in mL
TAKEN
0.077810989
RESULTS
ug/mL
Correlation
LESS THAN
% SPK REC
0.999163155
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.096
0.9229
10
10
10
<
92.29%
1.0
Std. B. 2.50
0.224
2.6237
10
10
10
0.262
104.95%
2.5
Std. B. 5.00
0.415
5.1616
10
10
10
0.516
103.23%
5.0
Std. B. 7.50
0.609
7.7393
10
10
10
0,774
103.19%
7.5
Std. B. 10.00
0.776
9.9584
10
10
10
0.996
99.58%
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.412
5.1217
10
10
10
0.512
103%
5.0
QC
0.422
5.2546
10
10
10
0.525
105%
5.0
24879-1
0.004
-0.2996
10
10
24879-1spk
0.400
4.9623
10
10
10
0.496
99%
5.0
24879-2
0.002
-0.3261
10
10
10
-7
24879-2 du p
0.009
-0.2331
10
10
10
< 0.1
24879-2 s
0.408
5.0686
10
10
10
0.507
101%
5.0
24880-1
0.007
-0.2597
10
10
10
<
24880-1spk
0.328
4.0056
10
10
10
0.401
80%
5.0
24880-2
0,004
-0.2996
10
10
10
-77777
24880-2 spk
0.411
5.1084
10
10
10
0.511
102%
5.0
24881-1
0.006
-0.2730
10
10
10
4 �,Z,
0
24881-1spk
0.362
4.4573
10
10
10
0.446
89%
5.0
24881-2
0.008
-0.2464
10
10
10
24881-2 s
0.365 1
4.4972
10
10
10
0.450
90%
5.0
24881-3
0.005
-0.2863
10
10
10
<
24881-3 s
0.298
3.6070
10
10
10
0.361
72%
5.0
24881-4
0.006
-0.2730
10
10
10
24881-4 s
0,367
4.5238
10
10
10
0.452
90%
5.0
24881-5
0.009
-0.2331
10
10
10
<
24881-5 s
0.308
3.7398
10
10
10
0.374
75%
5.0
Blank
0.000
0.0000
10
1 10
10
<
QC
0.422
5.2546
10
1po
10
0.525
105%
5.0
Submitted for QA/QC-
Date: 5/29/15
By..(rint)
KAM
(sign):
Page 1 of 4

Page 28 of 69
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
UNITS OF ANSWER
ug/mL
CLIENT:
Duke
Wave Length
664
DETECTION LIMIT u
1.000
Lab ID#
24879 / 880 / 881 1 882 / 883
SPK LEVEL u
MAX ALIQUOT
5
Date:
5/29/15
Na2S•9H2O
Lot #
STANDARD conc(ppm)
10.00
X
Time Analysis Begun
1330
40721
Cal Std Lot:
WC2-84-1
10
Time Analysis Ended
1554
QC Std Lot:
WC2-84-2
10
Analyst:
KAM
STD ABSORPTION
y
L g STD
STD
°.9DO
°.eoo
SOLUTION
ABS
0.00
0.000
°�°°
01
-
--oma
-,
1.00
0.095
°°°°
2.50
0.218
°.3 -------
0.2W----
-- - - - ----- --
- -
---- ---
- - -----
_,So
5.00
0.415
0.10
-,ate
7.50
0.610
0.0D
21400
10.00
0.778
X
8.00
10.00
:.w
Sloe
0.077810989"
Correlation
0.999153155f
SAMPLE
SAMP
ug PER
ALI in
mL PREP
ALI in mL
RESULTS
LESS THAN
SPIKE
I.D.
Std. B. 0.00
ABS
ALIQUOT
ANALYZED VOL in mL
TAKEN
ug/mL
% SPK REC
LEVEL
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.096
0.9229
10
10
10
<
92.29%
1.0
Std. B. 2.50
0.224
2.6237
10
10
10
0.262
104.95%
2.5
Std. B. 5.00
0.415
5.1616
10
10
10
0.516
103.23%
5.0
Std. B. 7.50
0.609
7.7393
10
10
10
0.774
103.19%
7.5
Std. B. 10.00
0.776
9.9584
10
10
10
0.996
99.58%
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.412
5.1217
10
10
10
0.512
103%
5.0
QC
0.422
5.2546
10
10
10
0.525
5.0
24881-6
0.002
-0.3261
10
10
10
<
24881-6 spk
0.414
5.1483
10
10
10
0.515
103%
5.0
24882-1
0.010
-0.2198
10
10
10KO:�
24882-1 du
0.008
-0.2464
10
10
10
< 0.1
24882-1 s k
0.371
4.5769
10
10
10
0.458
92%
5.0
24882-2
0.019
-0.1002
10
10
10
<
24882-2 s k
0.280
3.3678
10
10
10
0.337
67%
5.0
24882-3
0.004
-0.2996
10
10
10
24882-3 s k
0.337
4.1252
10
10
10
<
0.413
83%
5.0
24882-4
0.010
-0.2198
10
10
10
<
24882-4 s k
0.318
3.8727
10
10
10
0.387
77%
5.0
24882-5
0.006
-0.2730
10
10
10
v q� j
24882-5 s k
0.358
4.4042
10
10
10
0.440
88%
5.0
24882-6
0.007-0.2597
10
10
10
<
24882-6 s k
0.344
4.2182
10
10
10
0.422
84%
5.0
24882-7
0.006
-0.2730
10
10
10
24882-7 s k
0.328
4.0056
10
10
10
<
0.401
80%
24882-8
0.005
-0.2863
10
10
10
, � (-
5.0
24882-8 spk
0.400
4.9623
10
10
10
0.496
99%
5.0
Blank
0.000
0.0000
10
10
10
<
QC 0.420 5.2280
Submiffed for QA/QC-
10
10
10
0.523
105%
5.0
Date:
5/29/15
Bv: (Print)
knnn
Page 2 of 4

Page 29 of 69
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
ug/mL
DETECTION LIMIT u
1.000
CLIENT:
Duke
SPK LEVELNg)
5
Lab ID#
24879 /
5/29/15
1330
1554
KAM
Y
880 / 881 / 882
a eoo
/ 883°
Na2S•9H2O Lot #
40721
MAX ALIQUOT
STANDARD conc(ppm)
Cal Std Lot: WC2-84-1
QC Std Lot: WC2-84-2
STD ABSORPTION
10.00
X
10
10
Y
Date:
Time Analysis Begun
Time Analysis Ended
Analyst:
X
ug STD
SOLUTION
STD
; ueaa
ABS 0.700
-- - - -- --- --- --- - -- -- - - - -- -- ---- --- - -
J_o�
0.00
1.00
2.50
5.00
7.50
10.00
0.000
05M
0.095 04M
1"
-- -----------
-sao
0.218 azao
-------- _.------ ---._-
-,so
0.415 1 o,-
0.610
0.778
a.aoo
000
2m
aoo
coo
x
8.00
toad 1200
"'i
Sloe
0.077810989
Correlation
0.9991531551
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI inmLPREP
ANALYZED
VOL in mL
ALI in mL
TAKEN
RESULTS
u /mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.0
Std. B. 1.00
0.096
0.9229
10
10
10
<
92.29%
1.0
Std. B. 2.50
0.224
2.6237
10
10
10
0.262
104.95%
2.5
Std. B. 5.00
0.415
5.1616
10
10
10
0.516
103.23%
5.0
Std. B. 7.50
0.609
7.7393
10
10
10
0.774
103.19%
7.5
Std. B. 10.00
0.776
9.9584
10
10
10
0.996
99.58%
10.0
LRB
0.000
0.0000
10
10
10
<
0.0
LRB SPK
0.412
5.1217
10
10
10
0.512
103%
5.0
QC
0.422
5.2546
10
10
10
0.525
5.0
24882-9
0.005
-0.2863
10
10
10�
c 0;
24882-9 spk
0.416
5.1749
10
10
10
0.517
103%
5.0
24883-1
0.007
-0.2597
10
10
10
<
24883-1 s k
0.147
1.6005
10
10
10
0.160
32%
5.0
24883-2
0.007
-0.2597
10
10
10
¢ `0.`1
24883-2 dup
0.002
-0.3261
10
10
10
-'
< 0.1
24883-2 spk
0.411
5.1084
10
10
10
0.511
102%
5.0
24883-3
0.006
-0.2730
10
10
10
24883-3 spk
0.392
4.8560
10
10
10
0.486
97%
5.0
24880-1
0.009
-0.2331
10
10
5
24880-1 spk
0.360
4.4308
10
10
5
0.886
89%
5.0
24881-3
0.006
-0.2730
10
10
5
<
24881-3 spk
0.340
4.1650
10
10
5
0.833
83%
5.0
24881-5
0.005
-0.2863
10
10
5
<
24881-5 spk
0.274
3.2881
10
10
5
0.658
66%
5.0
24882-2
0.006
-0.2730
10
10
5
<
24882-2 spk
0.325
3.9657
10
10
5
0.793
79%
5.0
24882-3
0.004
-0.2996
10
10
5
24882-3 spk
0.373
4.6035
10
10
5
0.921
92%
5.0
Blank
0.000
0.0000
10
10
10
<
QC
0.419
5.2147
10
10
10
0.521
104%
5.0
Submitted for QA/QC-
Date: 5/29/15
By: (Print)
K:AM
(sign):
Page 3 of 4
2�

METHOD:
SM 4500 S2- D'`
ELEMENT ASSAY :
CLIENT:
Lab ID#
Sulfide
Duke
24879 / 880 / 881 /882 / 883
Date:
5/29/15
Time Analysis Begun
1330
Time Analysis Ended
1554
Analyst:
X
KAM
y
ug STD
pectrophotometer
Wave Length 664
Na2S•91-12O Lot #
40721
STD !
o'moo'
SOLUTION
Cal Std Lot: WC2-84-1 10
ABS
0700
0.00
LRB SPK
0.000
°800
1.00
10
0.095
Y
°^W
2.50
5.2546
0.218
°.'
5.00
24882-4
0.415
0.+m
7.50
10
0.610
M000
0
Page 30 of 69
ELEMENT ONE
pectrophotometer
Wave Length 664
Na2S•91-12O Lot #
40721
UNITS OF ANSWER u /rnL
DETECTION LIMIT u 1.000
SPK LEVEL u 5
MAX ALIQUOT 10.00
STANDARD conc(ppm) X
Cal Std Lot: WC2-84-1 10
QC Std Lot: WC2-84-2 10
STD ABSORPTION y
10.00 0.778
SAMPLE SAMP ug PER
I.D. ABS ALIQUOT
Std. B. 0.00 0.000 0.0000
Std. B. 1.00 0.096 0.9229
Std. B. 2.50 0.224 2.6237
Std. B. 5.00 0.415 5.1616
Std. B. 7.50 0.609 7.7393
Std. B. 10.00 0.776 9.9584
ALI in mL PREP
ANALYZED VOL in mL
10 10
10 10
10 10
10 10
10 10
10 10
X
Slope
ALI in m
TAKEN
10
10
10
10
10
10
LRB
0.000
0.0000
10
10
10
LRB SPK
0.412
5.1217
10
10
10
QC
0.422
5.2546
10
10
10
24882-4
0.002
-0.3261
10
10
5
24882-4 s k
0.361
4.4441
10
10
5
24882-6
0.005
-0.2863
10
10
5
24882-6 s k
0.387
4.7895
10
10
5
24882-7
0.007
-0.2597
10
10
5
24882-7 s k
0.401
4.9756
10
10
5
24883-1
0.007
-0.2597
10
10
5
24883-1 s k
0.226
2.6503
10
10
5
24881-3
0.005
-0.2863
10
10
2
24881-3 dup
0.006
-0.2730
10
10
2
24881-3 s k
0.395
4.8958
10
10
2
24881-5
0.005
70.2863
10
10
2
24881-5 sppk
0.356
4.3776
10
10
2
24882-2
0.003
-0.3128
10
10
2
24882-2 s k
0.394
4.8825
10
10
2
24833-1
0.007
-0.2597
10
102
24883-1 s k
0.318
3.8727
10
10
2
24883-1
0.008
-0.2464
10
10
1
24883-1 s k
0.345
4.2315
10
10
1
Blank
0.000
0.0000
10
10
10
QC 0.423 5.2679
Submitted fOr QA/QC- Date: 5/29/15
10
10
By: (Print)
10
Page 4 of 4
0.996
0.512
0.525
0.889
0.995
< 0.5
2.448
2.189
777777
2.441
1.936
4.231
0.527
LtSS IHAN
% SPK REC
SPIKE
LEVEL
0.0
92.29%
1.0
104.95%
2.5
103.23%
5.0
103.19%
7.5
99.58%
10.0
0.0
103%
50
98%
5.0
89%
5.0
96%
5.0
100%
5.0
53%
5.0
98%
5.0
88%
5.0
98%
5.0
77%
5.0
85%
5.0
105%^ 1 5.0

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water - Asheville
Project Number:J15050736
Lot Number:QE29059
Date Completed:06/05/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
* QE29059*
Shealy Environmental Services, Inc. Page: 1 of 21
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SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QE29059
Project Name: AB GW Assessment Water - Asheville
Project Number: J15050736
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 21
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QE29059
Project Name: AB GW Assessment Water - Asheville
Project Number: J15050736
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
2015016286
Aqueous
05/27/2015 0941
05/29/2015
002
2015016287
Aqueous
05/27/2015 0945
05/29/2015
003
2015016288
Aqueous
05/27/20151145
05/29/2015
004
2015016289
Aqueous
05/27/20151250
05/29/2015
005
2015016290
Aqueous
05/27/20151412
05/29/2015
006
2015016291
Aqueous
05/27/20151205
05/29/2015
007
2015016292
Aqueous
05/27/20151140
05/29/2015
008
2015016293
Aqueous
05/27/20151444
05/29/2015
009
2015016295
Aqueous
05/27/2015 0945
05/29/2015
(9 samples)
Shealy Environmental Services, Inc. Page: 3 of 21
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(15 detections)
Shealy Environmental Services, Inc. Page: 4 of 21
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QE29059
Project Name:
AB GW Assessment Water - Asheville
Project Number: J15050736
Sample Sample ID
Matrix
Parameter Method Result Q
Units
Page
001
2015016286
Aqueous
Alkalinity SM 2320B-
350
mg/L
5
001
2015016286
Aqueous
Bicarbonate Alkalinity SM 2320B-
350
mg/L
5
001
2015016286
Aqueous
Methane RSK - 175
56
ug/L
6
002
2015016287
Aqueous
Alkalinity SM 2320B-
91
mg/L
7
002
2015016287
Aqueous
Bicarbonate Alkalinity SM 2320B-
91
mg/L
7
002
2015016287
Aqueous
Methane RSK - 175
68
ug/L
8
003
2015016288
Aqueous
Alkalinity SM 2320B-
60
mg/L
9
003
2015016288
Aqueous
Bicarbonate Alkalinity SM 2320B-
60
mg/L
9
003
2015016288
Aqueous
Methane RSK - 175
37
ug/L
10
004
2015016289
Aqueous
Alkalinity SM 2320B-
78
mg/L
11
004
2015016289
Aqueous
Bicarbonate Alkalinity SM 2320B-
78
mg/L
11
006
2015016291
Aqueous
Methane RSK - 175
11
ug/L
16
007
2015016292
Aqueous
Methane RSK - 175
11
ug/L
18
008
2015016293
Aqueous
Alkalinity SM 2320B-
65
mg/L
19
008
2015016293
Aqueous
Bicarbonate Alkalinity SM 2320B-
65
mg/L
19
(15 detections)
Shealy Environmental Services, Inc. Page: 4 of 21
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QE29059-001
Description: 2015016286 Matrix: Aqueous
Date Sampled:05/27/2015 0941 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 05/30/2015 2203
HMA 76152
1
(Bicarbonate ) SM 2320B-2011
1 05/30/2015 0000
HMA
1
(Carbonate Al) SM 2320B-2011
1 05/30/2015 0000
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 21
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CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
350
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
350
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 21
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Methane
Client: Duke Energy Laboratory ID: QE29059-001
Description: 2015016286 Matrix: Aqueous
Date Sampled:05/27/2015 0941 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/02/2015 1457 DCS 76333
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 56 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE29059-002
Description: 2015016287 Matrix: Aqueous
Date Sampled:05/27/2015 0945 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/02/2015 1230
HMA 76305
1
(Bicarbonate ) SM 2320B-2011
1 06/02/2015 1230
HMA 06/02/2015 1230
1
(Carbonate Al) SM 2320B-2011
1 06/02/2015 1230
HMA 06/02/2015 1230
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
91
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
91
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 21
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Methane
Client: Duke Energy Laboratory ID: QE29059-002
Description: 2015016287 Matrix: Aqueous
Date Sampled:05/27/2015 0945 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/02/2015 1916 JJG 76386
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 68 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE29059-003
Description: 2015016288 Matrix: Aqueous
Date Sampled:05/27/2015 1145 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/02/2015 1248
HMA 76305
1
(Bicarbonate ) SM 2320B-2011
1 06/02/2015 1248
HMA 06/02/2015 1248
1
(Carbonate Al) SM 2320B-2011
1 06/02/2015 1248
HMA 06/02/2015 1248
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
60
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
60
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE29059-003
Description: 2015016288 Matrix: Aqueous
Date Sampled:05/27/2015 1145 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/02/2015 1933 JJG 76386
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 37 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE29059-004
Description: 2015016289 Matrix: Aqueous
Date Sampled:05/27/2015 1250 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/02/2015 1253
HMA 76305
1
(Bicarbonate ) SM 2320B-2011
1 06/02/2015 1253
HMA 06/02/2015 1253
1
(Carbonate Al) SM 2320B-2011
1 06/02/2015 1253
HMA 06/02/2015 1253
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
78
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
78
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE29059-004
Description: 2015016289 Matrix: Aqueous
Date Sampled:05/27/2015 1250 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/02/2015 1946 JJG 76386
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 12 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE29059-005
Description: 2015016290 Matrix: Aqueous
Date Sampled:05/27/2015 1412 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/02/2015 1256
HMA 76305
1
(Bicarbonate ) SM 2320B-2011
1 06/02/2015 1256
HMA 06/02/2015 1256
1
(Carbonate Al) SM 2320B-2011
1 06/02/2015 1256
HMA 06/02/2015 1256
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 13 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 13 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE29059-005
Description: 2015016290 Matrix: Aqueous
Date Sampled:05/27/2015 1412 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/02/2015 1956 JJG 76386
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 14 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE29059-006
Description: 2015016291 Matrix: Aqueous
Date Sampled:05/27/2015 1205 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/02/2015 1300
HMA 76305
1
(Bicarbonate ) SM 2320B-2011
1 06/02/2015 1300
HMA 06/02/2015 1300
1
(Carbonate Al) SM 2320B-2011
1 06/02/2015 1300
HMA 06/02/2015 1300
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 15 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 15 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE29059-006
Description: 2015016291 Matrix: Aqueous
Date Sampled:05/27/2015 1205 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/02/2015 2009 JJG 76386
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 11 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 16 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE29059-007
Description: 2015016292 Matrix: Aqueous
Date Sampled:05/27/2015 1140 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/02/2015 1303
HMA 76305
1
(Bicarbonate ) SM 2320B-2011
1 06/02/2015 1303
HMA 06/02/2015 1303
1
(Carbonate Al) SM 2320B-2011
1 06/02/2015 1303
HMA 06/02/2015 1303
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 17 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 17 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE29059-007
Description: 2015016292 Matrix: Aqueous
Date Sampled:05/27/2015 1140 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/02/2015 2025 JJG 76386
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 11 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 18 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE29059-008
Description: 2015016293 Matrix: Aqueous
Date Sampled:05/27/2015 1444 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/02/2015 1310
HMA 76305
1
(Bicarbonate ) SM 2320B-2011
1 06/02/2015 1310
HMA 06/02/2015 1310
1
(Carbonate Al) SM 2320B-2011
1 06/02/2015 1310
HMA 06/02/2015 1310
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 19 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
65
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
65
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 19 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QE29059-009
Description: 2015016295 Matrix: Aqueous
Date Sampled:05/27/2015 0945 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 06/02/2015 1331
HMA 76305
1
(Bicarbonate ) SM 2320B-2011
1 06/02/2015 1331
HMA 06/02/2015 1331
1
(Carbonate Al) SM 2320B-2011
1 06/02/2015 1331
HMA 06/02/2015 1331
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 20 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 20 of 21
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QE29059-009
Description: 2015016295 Matrix: Aqueous
Date Sampled:05/27/2015 0945 Project Name: AB GW Assessment Water -
Date Received: 05/29/2015 Project Number: J15050736
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 06/02/2015 2036 JJG 76386
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - Ii
Sample ID: QQ76152-001 Matrix: Aqueous
Batch: 76152
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 05/30/20151910
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ76152-002 Matrix: Aqueous
Batch: 76152
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 95 1 95 90-110 05/30/20151917
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MS
Sample ID: QE29059-001MS Matrix: Aqueous
Batch: 76152
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 350 100 390 N 1 41 70-130 05/30/2015 2211
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MSD
Sample ID: QE29059-001MD Matrix: Aqueous
Batch: 76152
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Alkalinity 350 100 390 N 1 36 1.4 70-130 20 05/30/2015 2220
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - Ii
Sample ID: QQ76305-001 Matrix: Aqueous
Batch: 76305
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 06/02/20151220
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ76305-002 Matrix: Aqueous
Batch: 76305
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 93 1 93 90-110 06/02/20151225
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MS
Sample ID: QE29059-002MS Matrix: Aqueous
Batch: 76305
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 91 100 170 1 84 70-130 06/02/20151237
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MSD
Sample ID: QE29059-002MD Matrix: Aqueous
Batch: 76305
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Alkalinity 91 100 180 1 85 0.74 70-130 20 06/02/20151243
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ76333-001 Matrix: Aqueous
Batch: 76333
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 06/02/20151019
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ76333-002 Matrix: Aqueous
Batch: 76333
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 140 1 91 70-130 06/02/2015 0942
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ76333-003 Matrix: Aqueous
Batch: 76333
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 170 1 112 20 70-130 30 06/02/2015 0958
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ76386-001 Matrix: Aqueous
Batch: 76386
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 06/02/20151616
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ76386-002 Matrix: Aqueous
Batch: 76386
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 160 1 107 70-130 06/02/20151533
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ76386-003 Matrix: Aqueous
Batch: 76386
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 160 1 103 4.1 70-130 30 06/02/20151552
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QE29059
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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Mean-, of re.c4ip(: ❑ SM Llent ElUPS El FedEx L1 Airborne ExP (�J�t} r
Yes Nor L Wen custody seals present on the m{)ler?
Yes Ll I No EJ I NA 1 2_ If cu. tod .s#a1s were jweEwnt, were they mract and unbroken? _—
Cooler IDJOriginaal tem�wrature upon r oeixOuiue.d (corrected) temperature upon receipt:
lie€hod; ❑ Ternperatlrre €ark ainst Bulllns IR Gun 10 IR Gun Correclicn Fac€or; D -Q °C
Method of copla nt: LZ Wc€ Ice ❑ mue Ice ❑ Dry Ice n i+#orte
3- if tenVchturc of any CWler exceWed 6.0'C— was Proitt:t Manager tlotified?
Yes Q ]u ❑ NA Phi not4icd by IRC:, phone, nate (ci.rcic one), nth�en
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dDaples felinquis�cd lay tient tta rr#4iefCiBl tv�urier?
1p gel 113s Listed ori the CDC?
ale. IUs listed on all sample c�nnlainers?
,tion date & livae listed on the C".:?
:tion date & time listed on all §m le containers?
nt2ine.r label infonnatinn 17date, time � 4c with the C ?
x to be performed listed an the CIOC?
m resarn%T in t# e. prnper contaaraers for each test'?
stainers axrave in good condition (unbroken, lids on, etc.l`t
u'ate le volume available.?
sarnpies received within a/2 the hotding time or 48 hours, whichever
rst?
16. Wen --n+ samples c raitaincrs missin ,?
1'i7_ Were th-re any excess sant ]es r14t listed �n ICI t
13_ Fere bi bhles PreseTit >` ` -si c'" wfor Gram in diameter in any VQA-,ials?
19. Were al rtxet2tl 0&GJjMl 4''owlriont samples reccivrad at a H of -,2?
�.tl. Were a cyaanide and—/Or sulfide saMples received at a pH > 12?
21, Were AI Applicable. NH3,-TKNicyani(lelphemel (40_2meIL) samples free of
22. Were cc
23. Were cli
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Yes J I No Lk' € 124- Was thD
Sample Preservation (Must be comp
sample(s)
Accorchngly in sample. tweiving with
a>rnpws)
Satnpl 9)_
SC Drinldng Water project Sample(s) p
anaple(s) ware not rec
CyA)rnmcrrts;.
lochon temperatures docurnzn1rd on the COC fear NC: samples?
it rcmarkVrNutsts (i_e.re�queslcd dilutions. MSI11 SD designation,
dy transcribed from the COC 010 the comment section in LIMB?
mote number used takers from the enntainer label?
ft4d for any ssa lc(s) inoorrectly preserved or with. 11ead6pact,)
wtv!. received incorrectly preserved and were adjnsteei.
H 50'.HN 1 HC1,NaQH ItsinS SR €
vwcrerece''%red with bubbles >6 man in diameter.
Wer_c TEOF-iVIA with. TRC A.2 mp+L (If #Z1 is No)
I verified to be > 2 his Date:
ivied. a.t 3 pkKi of <2 and v:ere aditaslted acc 3rdinsly tlsine SR*
Verifi&l hw
Date.
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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ELEMENTS tvi IGP- MS �TRM: As. Be. Cd. Co. Cr, Cu, ft, Ni, Pb. Sb. St. TI (1-1.4. V 41 -LI
ELF-AMENTS bY JCP ITRMI; JU, EW, 0, FE, Mn, 3r—ZR lCP-1Jnd*stad C4L Mg, K, No Hg bV 246.1 'Add Call. Will Apply