NC0000396_J15040667report_20150823

DUKE Analytical Laboratory
ENERGY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Order Number: J15040667
Project Name: ASHEVILLE - AB GW ASSESSMENT WATER
Customer Name(s): Todd Plating, Kathy Webb, John Toepfer, Tim Hunsucker
Customer Address: 200 CP and L Drive
Arden,NC 28704
Lab Contact: Mary Ann Ogle Phone: [phone]
0 �, Mary Ann Ogle
Report Authorized By: �&_///S 2015.05.11 Date:
(Signature) 14:56:11 -04'00'
Mary Ann Ogle
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
5/11/2015
Page 1 of 41
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
2015012277
2015012278
2015012279
2015012280
2015012281
5 Total Samples
Collected By
Sample Description
ASHEVILLE
27 -Apr -15 9:35 AM
Russo
CB -09 SL
ASHEVILLE
27 -Apr -15 11:40 AM
Russo
CB -09 BR
ASHEVILLE
27 -Apr -15 1:50 PM
Russo
MW -09S
ASHEVILLE
27 -Apr -15 8:45 AM
Russo
Equipment Blank
ASHEVILLE
27 -Apr -15 8:45 AM
Russo
Filter Blank
Page 2 of 41

Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals Yes No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes No
All laboratory QA/QC requirements are acceptable. (] Yes ❑ No
Report Sections Included:
LU Job Summary Report
❑ Sample Identification
P/1 Technical Validation of Data Package
J❑ Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
Page 3 of 41
LVI Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
d❑ Chain of Custody
LVI Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: DBA Account Date: 5/11/2015

Certificate of Laboratory Analysis Page 4 of 41
This report shall not be reproduced, except in full.
Order # J15040667
Site: CB -09 SL
Collection Date: 27 -Apr -15 9:35 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
BGN9034
1 EPA 300.0
Vendor Parameter
Complete
1 EPA 245.1
04/29/2015 14:42
NITRITE + NITRATE (COLORIMETRIC)
1 EPA 245.1
04/29/2015 15:27
Nitrite + Nitrate (Colorimetric)
0.086
mg-N/L
0.01
INORGANIC IONS BY IC
04/29/2015 11:02
MHALL3
1 EPA 200.7
Chloride
6.1
mg/L
0.1
Sulfate
0.74
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
04/29/2015 11:02
MHALL3
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
MHALL3
1 EPA 200.7
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
1 EPA 200.7
04/29/2015 12:30
MHALL3
Aluminum (AI)
0.012
mg/L
0.005
Barium (Ba)
0.029
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.065
mg/L
0.01
Manganese (Mn)
0.096
mg/L
0.005
Strontium (Sr)
0.029
mg/L
0.005
Zinc (Zn)
0.039
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
4.15
mg/L
0.01
Magnesium (Mg)
2.56
mg/L
0.005
Potassium (K)
1.41
mg/L
0.1
Sodium (Na)
8.54
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
1.28
mg/L
0.005
Barium (Ba)
0.046
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.475
mg/L
0.01
Manganese (Mn)
0.125
mg/L
0.005
Strontium (Sr)
0.040
mg/L
0.005
Zinc (Zn)
0.049
mg/L
0.005
Sample #: 2015012277
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
04/30/2015 09:49
LSTARL1
1 EPA 300.0
04/29/2015 00:01
BGN9034
1 EPA 300.0
04/29/2015 00:01
BGN9034
1 EPA 245.1
04/29/2015 14:42
ACPAYNE
1 EPA 245.1
04/29/2015 15:27
ACPAYNE
1 EPA 200.7
04/29/2015 11:02
MHALL3
1 EPA 200.7
04/29/2015 11:02
MHALL3
1 EPA 200.7
04/29/2015 11:02
MHALL3
1 EPA 200.7
04/29/2015 11:02
MHALL3
1 EPA 200.7
04/29/2015 11:02
MHALL3
1 EPA 200.7
04/29/2015 11:02
MHALL3
1 EPA 200.7
04/29/2015 11:02
MHALL3
1 EPA 200.7
04/29/2015 12:30
MHALL3
1 EPA 200.7
04/29/2015 12:30
MHALL3
1 EPA 200.7
04/29/2015 12:30
MHALL3
1 EPA 200.7
04/29/2015 12:30
MHALL3
1 EPA 200.7
05/01/2015 12:36
MHALL3
1 EPA 200.7
05/01/2015 12:36
MHALL3
1 EPA 200.7
05/01/2015 12:36
MHALL3
1 EPA 200.7
05/01/2015 12:36
MHALL3
1 EPA 200.7
05/01/2015 12:36
MHALL3
1 EPA 200.7
05/01/2015 12:36
MHALL3
1 EPA 200.7
05/01/2015 12:36
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040667
Site: CB -09 SL
Collection Date: 27 -Apr -15 9:35 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper(Cu)
1.79
Lead (Pb)
< 1
Molybdenum (Mo)
1.28
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
2.86
Cobalt (Co)
1.21
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
2.13
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.560
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
92
Total Carbon
04/30/2015 15:14
TOC
0.397
TOTAL SUSPENDED SOLIDS
1
TSS
110
Page 5 of 41
ug/L
1
1
Sample #:
2015012277
DJSULL1
ug/L
1
1
Matrix:
GW -WW
DJSULL1
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
04/30/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:14
JAHERMA
ug/L
0.2
1
EPA 200.8
04/30/2015 15:14
JAHERMA
ug/L
0.3
1
EPA 200.8
04/30/2015 15:14
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 12:34
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 12:34
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 12:34
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 12:34
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 12:34
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 12:34
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 12:34
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 12:34
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 12:34
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 12:34
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 12:34
DJSULL1
ug/L
0.2
1
EPA 200.8
04/30/2015 12:34
DJSULL1
ug/L
0.3
1
EPA 200.8
04/30/2015 12:34
DJSULL1
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
04/28/201514:19 AGIBBS5
mg/L
0.1 1 SM5310C/EPA9060A
05/04/201512:15 GHUTCHI
mg/L
9 1 SM2540D
04/29/201511:24 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040667
Site: CB -09 BR
Collection Date: 27 -Apr -15 11:40 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
BGN9034
1 EPA 300.0
Vendor Parameter
Complete
1 EPA 245.1
04/29/2015 14:44
NITRITE + NITRATE (COLORIMETRIC)
1 EPA 245.1
04/29/2015 15:34
Nitrite + Nitrate (Colorimetric)
0.065
mg-N/L
0.01
INORGANIC IONS BY IC
04/29/2015 11:26
MHALL3
1 EPA 200.7
Chloride
6.4
mg/L
0.1
Sulfate
3.9
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
04/29/2015 11:26
MHALL3
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
MHALL3
1 EPA 200.7
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
1 EPA 200.7
04/29/2015 12:42
MHALL3
Aluminum (AI)
0.033
mg/L
0.005
Barium (Ba)
0.019
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
0.012
mg/L
0.005
Strontium (Sr)
0.110
mg/L
0.005
Zinc (Zn)
0.017
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
24.7
mg/L
0.01
Magnesium (Mg)
2.53
mg/L
0.005
Potassium (K)
4.23
mg/L
0.1
Sodium (Na)
8.39
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.405
mg/L
0.005
Barium (Ba)
0.026
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.460
mg/L
0.01
Manganese (Mn)
0.021
mg/L
0.005
Strontium (Sr)
0.115
mg/L
0.005
Zinc (Zn)
0.008
mg/L
0.005
Sample #: 2015012278
Matrix: GW -WW
Page 6 of 41
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
04/30/2015 09:52
LSTARL1
1 EPA 300.0
04/29/2015 00:19
BGN9034
1 EPA 300.0
04/29/2015 00:19
BGN9034
1 EPA 245.1
04/29/2015 14:44
ACPAYNE
1 EPA 245.1
04/29/2015 15:34
ACPAYNE
1 EPA 200.7
04/29/2015 11:26
MHALL3
1 EPA 200.7
04/29/2015 11:26
MHALL3
1 EPA 200.7
04/29/2015 11:26
MHALL3
1 EPA 200.7
04/29/2015 11:26
MHALL3
1 EPA 200.7
04/29/2015 11:26
MHALL3
1 EPA 200.7
04/29/2015 11:26
MHALL3
1 EPA 200.7
04/29/2015 11:26
MHALL3
1 EPA 200.7
04/29/2015 12:42
MHALL3
1 EPA 200.7
04/29/2015 12:42
MHALL3
1 EPA 200.7
04/29/2015 12:42
MHALL3
1 EPA 200.7
04/29/2015 12:42
MHALL3
1 EPA 200.7
05/01/2015 12:25
MHALL3
1 EPA 200.7
05/01/2015 12:25
MHALL3
1 EPA 200.7
05/01/2015 12:25
MHALL3
1 EPA 200.7
05/01/2015 12:25
MHALL3
1 EPA 200.7
05/01/2015 12:25
MHALL3
1 EPA 200.7
05/01/2015 12:25
MHALL3
1 EPA 200.7
05/01/2015 12:25
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040667
Site: CB -09 BR
Collection Date: 27 -Apr -15 11:40 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
7.01
Nickel (Ni)
< 1
Selenium (Se)
1.44
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
2.01
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
8.25
Cobalt (Co)
< 1
Copper (Cu)
1.16
Lead (Pb)
< 1
Molybdenum (Mo)
7.40
Nickel (Ni)
4.42
Selenium (Se)
1.56
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
3.03
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
130
Total Carbon
04/30/2015 15:19
TOC
0.308
TOTAL SUSPENDED SOLIDS
1
TSS
25
Page 7 of 41
ug/L
1
1
Sample #:
2015012278
DJSULL1
ug/L
1
1
Matrix:
GW -WW
DJSULL1
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
04/30/2015 15:19
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:19
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:19
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:19
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:19
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:19
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:19
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:19
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:19
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:19
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:19
JAHERMA
ug/L
0.2
1
EPA 200.8
04/30/2015 15:19
JAHERMA
ug/L
0.3
1
EPA 200.8
04/30/2015 15:19
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:15
DJSULL1
ug/L
0.2
1
EPA 200.8
04/30/2015 13:15
DJSULL1
ug/L
0.3
1
EPA 200.8
04/30/2015 13:15
DJSULL1
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
04/28/201514:19 AGIBBS5
mg/L
0.1 1 SM5310C/EPA9060A
05/04/201512:15 GHUTCHI
mg/L
5 1 SM2540D
04/29/201511:24 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040667
Site: MW -09S
Collection Date: 27 -Apr -15 1:50 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 353.2
04/30/2015 09:54
Vendor Parameter
Complete
EPA 300.0
05/04/2015 10:52
NITRITE + NITRATE (COLORIMETRIC)
100
EPA 300.0
Nitrite + Nitrate (Colorimetric)
0.695
mg-N/L
0.01
INORGANIC IONS BY IC
ACPAYNE
1
EPA 245.1
Chloride
560
mg/L
10
Sulfate
250
mg/L
10
MERCURY (COLD VAPOR) IN WATER
MHALL3
1
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
04/29/2015 11:05
MHALL3
Mercury (Hg)
0.08
ug/L
0.05
DISSOLVED METALS BY ICP
EPA 200.7
04/29/2015 11:05
MHALL3
Aluminum (AI)
0.064
mg/L
0.005
Barium (Ba)
0.225
mg/L
0.005
Boron (B)
4.87
mg/L
0.05
Iron (Fe)
0.105
mg/L
0.01
Manganese (Mn)
4.58
mg/L
0.005
Strontium (Sr)
3.26
mg/L
0.005
Zinc (Zn)
0.009
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
05/01/2015 12:40
MHALL3
Calcium (Ca)
293
mg/L
0.2
Magnesium (Mg)
91.3
mg/L
0.1
Potassium (K)
4.76
mg/L
0.1
Sodium (Na)
18.1
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.035
mg/L
0.005
Barium (Ba)
0.215
mg/L
0.005
Boron (B)
4.73
mg/L
0.05
Iron (Fe)
0.070
mg/L
0.01
Manganese (Mn)
4.29
mg/L
0.005
Strontium (Sr)
3.08
mg/L
0.005
Zinc (Zn)
0.009
mg/L
0.005
Page 8 of 41
Sample #: 2015012279
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
04/30/2015 09:54
LSTARL1
100
EPA 300.0
05/04/2015 10:52
BGN9034
100
EPA 300.0
05/04/2015 10:52
BGN9034
1
EPA 245.1
04/29/2015 14:47
ACPAYNE
1
EPA 245.1
04/29/2015 15:36
ACPAYNE
1
EPA 200.7
04/29/2015 11:05
MHALL3
1
EPA 200.7
04/29/2015 11:05
MHALL3
1
EPA 200.7
04/29/2015 11:05
MHALL3
1
EPA 200.7
04/29/2015 11:05
MHALL3
1
EPA 200.7
04/29/2015 11:05
MHALL3
1
EPA 200.7
04/29/2015 11:05
MHALL3
1
EPA 200.7
04/29/2015 11:05
MHALL3
20
EPA 200.7
04/29/2015 12:45
MHALL3
20
EPA 200.7
04/29/2015 12:45
MHALL3
1
EPA 200.7
04/29/2015 12:45
MHALL3
1
EPA 200.7
04/29/2015 12:45
MHALL3
1
EPA 200.7
05/01/2015 12:40
MHALL3
1
EPA 200.7
05/01/2015 12:40
MHALL3
1
EPA 200.7
05/01/2015 12:40
MHALL3
1
EPA 200.7
05/01/2015 12:40
MHALL3
1
EPA 200.7
05/01/2015 12:40
MHALL3
1
EPA 200.7
05/01/2015 12:40
MHALL3
1
EPA 200.7
05/01/2015 12:40
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040667
Site: MW -09S
Collection Date: 27 -Apr -15 1:50 PM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
17.4
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
5.27
Selenium (Se)
41.9
Thallium (TI) Low Level
0.225
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
15.8
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
5.24
Selenium (Se)
36.6
Thallium (TI) Low Level
0.294
Vanadium (V) Low Level
< 0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
1700
Total Carbon
04/30/2015 15:24
TOC
0.357
TOTAL SUSPENDED SOLIDS
1
TSS
< 5
Page 9 of 41
ug/L
1
1
Sample #:
2015012279
DJSULL1
ug/L
1
1
Matrix:
GW -WW
DJSULL1
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
04/30/2015 15:24
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:24
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:24
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:24
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:24
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:24
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:24
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:24
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:24
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:24
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 15:24
JAHERMA
ug/L
0.2
1
EPA 200.8
04/30/2015 15:24
JAHERMA
ug/L
0.3
1
EPA 200.8
04/30/2015 15:24
JAHERMA
ug/L
1
1
EPA 200.8
04/30/2015 13:19
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:19
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:19
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:19
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:19
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:19
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:19
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:19
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:19
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:19
DJSULL1
ug/L
1
1
EPA 200.8
04/30/2015 13:19
DJSULL1
ug/L
0.2
1
EPA 200.8
04/30/2015 13:19
DJSULL1
ug/L
0.3
1
EPA 200.8
04/30/2015 13:19
DJSULL1
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
04/28/201514:19 AGIBBS5
mg/L
0.1 1 SM5310C/EPA9060A
05/04/201512:15 GHUTCHI
mg/L
5 1 SM2540D
04/29/201511:24 AGIBBS5

Certificate of Laboratory Analysis Page 10 of 41
This report shall not be reproduced, except in full.
Order # J15040667
Site: Equipment Blank
Collection Date: 27 -Apr -15 8:45 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
1 EPA 300.0
Vendor Parameter
Complete
1 EPA 300.0
05/04/2015 09:37
NITRITE + NITRATE (COLORIMETRIC)
1 EPA 245.1
04/29/2015 14:49
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
04/29/2015 13:08
MHALL3
1 EPA 200.7
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
05/01/2015 13:03
MHALL3
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY ICP
MHALL3
1 EPA 200.7
05/01/2015 13:03
Calcium (Ca)
< 0.01
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
04/30/2015 12:47
DJSULL1
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015012280
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
04/30/2015 09:55
LSTARL1
1 EPA 300.0
05/04/2015 09:37
BGN9034
1 EPA 300.0
05/04/2015 09:37
BGN9034
1 EPA 245.1
04/29/2015 14:49
ACPAYNE
1 EPA 200.7
04/29/2015 13:08
MHALL3
1 EPA 200.7
04/29/2015 13:08
MHALL3
1 EPA 200.7
04/29/2015 13:08
MHALL3
1 EPA 200.7
04/29/2015 13:08
MHALL3
1 EPA 200.7
05/01/2015 13:03
MHALL3
1 EPA 200.7
05/01/2015 13:03
MHALL3
1 EPA 200.7
05/01/2015 13:03
MHALL3
1 EPA 200.7
05/01/2015 13:03
MHALL3
1 EPA 200.7
05/01/2015 13:03
MHALL3
1 EPA 200.7
05/01/2015 13:03
MHALL3
1 EPA 200.7
05/01/2015 13:03
MHALL3
1 EPA 200.8
04/30/2015 12:47
DJSULL1
1 EPA 200.8
04/30/2015 12:47
DJSULL1
1 EPA 200.8
04/30/2015 12:47
DJSULL1
1 EPA 200.8
04/30/2015 12:47
DJSULL1
1 EPA 200.8
04/30/2015 12:47
DJSULL1
1 EPA 200.8
04/30/2015 12:47
DJSULL1
1 EPA 200.8
04/30/2015 12:47
DJSULL1
1 EPA 200.8
04/30/2015 12:47
DJSULL1
1 EPA 200.8
04/30/2015 12:47
DJSULL1
1 EPA 200.8
04/30/2015 12:47
DJSULL1
1 EPA 200.8
04/30/2015 12:47
DJSULL1
1 EPA 200.8
04/30/2015 12:47
DJSULL1
1 EPA 200.8
04/30/2015 12:47
DJSULL1

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040667
Page 11 of 41
Site: Equipment Blank
Sample #: 2015012280
Collection Date: 27 -Apr -15 8:45
AM
Matrix: GW—WW
Analyte
Result
Units Qualifiers
RDL
DF
Method Analysis Date/Time
Analyst
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
< 25
mg/L
25
1
SM2540C 04/28/2015 14:19
AGIBBS5
Total Carbon
TOC
< 0.1
mg/L
0.1
1
SM5310C/EPA9060A 05/04/2015 12:15
GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS
< 5
mg/L
5
1
SM2540D 04/29/2015 11:24
AGIBBS5

Certificate of Laboratory Analysis Page 12 of 41
This report shall not be reproduced, except in full.
Order # J15040667
Site: Filter Blank
Collection Date: 27 -Apr -15 8:45 AM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
EPA 245.1
04/29/2015 15:38
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
1
EPA 200.7
04/29/2015 11:09
Aluminum (Al)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
DISSOLVED METALS BY ICP -MS
1
EPA 200.8
04/30/2015 15:28
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015012281
Matrix: GW -WW
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
04/29/2015 15:38
ACPAYNE
1
EPA 200.7
04/29/2015 11:09
MHALL3
1
EPA 200.7
04/29/2015 11:09
MHALL3
1
EPA 200.7
04/29/2015 11:09
MHALL3
1
EPA 200.7
04/29/2015 11:09
MHALL3
1
EPA 200.7
04/29/2015 11:09
MHALL3
1
EPA 200.7
04/29/2015 11:09
MHALL3
1
EPA 200.7
04/29/2015 11:09
MHALL3
1
EPA 200.8
04/30/2015 15:28
JAHERMA
1
EPA 200.8
04/30/2015 15:28
JAHERMA
1
EPA 200.8
04/30/2015 15:28
JAHERMA
1
EPA 200.8
04/30/2015 15:28
JAHERMA
1
EPA 200.8
04/30/2015 15:28
JAHERMA
1
EPA 200.8
04/30/2015 15:28
JAHERMA
1
EPA 200.8
04/30/2015 15:28
JAHERMA
1
EPA 200.8
04/30/2015 15:28
JAHERMA
1
EPA 200.8
04/30/2015 15:28
JAHERMA
1
EPA 200.8
04/30/2015 15:28
JAHERMA
1
EPA 200.8
04/30/2015 15:28
JAHERMA
1
EPA 200.8
04/30/2015 15:28
JAHERMA
1
EPA 200.8
04/30/2015 15:28
JAHERMA

Page 13 of 41
Element One Inc.
6319-D Carolina Beach Rd.
Wilmington, NC 28412
Phone: [phone]
Fax: [phone]
[e-mail]
ehe,mermtOne
REPORT OF ANALYSES
Duke Energy May 5, 2015
Laboratory Services Client Project Name AB GW Assessment water - Asheville
13339 Hagers Ferry Road Bld. MG03A Client Project Number J15040667
Huntersville, NC 28078 PO Number
Sample Matrix
GW WW
Sample Type
Grab
Date Received
04/30/2015
Date Analyzed
04/30/2015
Method
SM 4500 S2- D
Time Received
1155
Delivered by
FedEx
Received by
LLB
eOne ID
Duke Energy ID
Parameter
Result
Unit
Dil
DL Date
Time
Sampled
Sampled
24636-1 *
CB-09SL
Sulfide
< 0.5
mg/L
5
0.1 04/27/15
0935
24636-2*
CB-09BR
Sulfide
< 0.2
mg/L
2
0.1 04/27/15
1140
24636-3*
MW -09S
Sulfide
< 0.5
mg/L
5
0.1 04/27/15
1350
24636-4
Equipment Blank
Sulfide
< 0.1
mg/L
1
0.1 04/27/15
0845
*Sample spike recovery outside of QA limits of 85-115%; dilution necessary to meet laboratory QA limits.
(-7� /00�—
Ken Smith, Taboratory Director
24636 Duke Report Packet Compiled b&�-
NC Certifications: DW 37788 and DWQ DENR 604

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Page 14 of 41
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e emen One SAMPLE SUBMISSION FORM
TAT 7 BD
Hold Time Expiration 05.04.15 @ 0845
Client: Duke Energy
LIMS No J15040667
Project ID Asheville
Lab Idage2406
Analysis Due Date 05.01.15
Report Due Date 05.11.15
H >9
Date Rec:
04.30.15
Ref. Method:
SM4500 S2 D
Time Rec:
1155
1
Rec By
LLB
H >9
Yes
No Tem <_ 6°C Yes No
Ref. Method:
SM4500 S2 D
If No, Record If No, Record
DarnJAe wenuncanvn a inIUMNALivn
Lab ID
Client ID
Collection Date
Collection Time
Anal sis Requested
1
CB-09SL
04.27.15
0935
S
2
CB-09BR
04.27.15
1140
S e
3
MW -09S _.._____ ...,..
04.27.15
1350 _ _
S
4
Equipment Blank
04.27.15
0845
Sulfi
NOTE for Sulfide The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final spike concentration at — 500 pg/L

METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Duke
Lab ID#
24634 / 24635 / 24636 / 24637
Date:
4/30/15
Time Anal sis Begun
14:00
Time AnaIvsIs Ended
17:14
X
Y
ug STD
STD
SOLUTION
ABS
0.00
0.000
1.00
0.092
2.50
0.223
5.00
0.422
7.50
0.605
10.00
0.777
Page 16 of 41
ELEMENT ONE
Wave Length 664 ut I EC TION LIMIT u 1.000
SPK LEVEL u 5
MAX ALIQUOT 10.00
Na2S-9H2O Lot # STANDARD conc(ppm) X
40721 Cal Std Lot: \",7-- -11n - 5 10
nr,Qr,giM. 1.)/"7-7 n -
-
SAMPLE SAMP
I.D. ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
Slope
ALI in mL
TAKEN
0.0776
RESULTS
ug/mL
Correlation
LESS THAN
% SPK REC
0.998884275
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
.
i'^..��i1i111•�����
-
SAMPLE SAMP
I.D. ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
Slope
ALI in mL
TAKEN
0.0776
RESULTS
ug/mL
Correlation
LESS THAN
% SPK REC
0.998884275
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.00
Std. B. 1.00
0.099
0.9105
10
10
10
<
91%
1.00
Std. B. 2.50
0.230
2.6747
10
10
10
0.267
107%
2.50
Std. B. 5.00
0.428
5.3411
10
10
10
0.534
107%
5.00
Std. B. 7.50
0.601
7.6709
10
10
10
0.767
102%
7.50
Std. B. 10.00
0.759
9.7987
10
10
10
0.980
98%
10.00
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.431
5.3815
10
10
10
0.538
108%
5.0
QC
0.432
5.3950
10
10
10
0.539
5.0
24634-1
-0.001
0.0000
10
10
10
24634-1 s k
0.353
4.3311
10
10
10
0.433
87%
5.0
24634-2
0.005
-0.3554
10
10
10
"0,1
24634-2 du
-0.001
0.0000
10
10
10
< 0.1
24634-2 s k
0.368
4.5331
10
10
10
0.453
91%
5.0
24634-3
-0.003
0.0000
10
10
10,1
24634-3 spk
0.382
4.7216
10
10
10
0.472
94%
5.0
24635
0.001
-0.4093
10
10
10
<
24635 s k
0.003
-0.3824
10
10
10
<
-8%
5.0
24636-1
0.004
-0.3689
10
10
10
<
24636-1 s k
0.216
2,4861
10
10
10
0.249
50%
5.0
24636-2
0.012
-0.2611
10
10
10
<
24636-2 s k
0.297
3.5769
10
10
10
0.358
72%
5.0
24636-3
-0.002
0.0000
10
10
10
<
24636-3s k
0.305
3.6847
10
10
10
0.368
74%
5.0
24636-4
0.003
-0.3824
10
10
10
'�� Q'.
246364spk
0.424
5.2872
10
10
10
0.529
106%
5.0
24637-1
0.005
-0.3554
10
10
10
r c,0 y ,
24637-1 s k
0.431
5.3815
10
10
10
0.538
108%
5.0
Blank
0.000
0.0000
10
10
10
<
QC
0.424
5.2872
10
10
10
0.529
106%
5.0
Submitted for QAIQC-
Date: 4/30/15
By: (Print)
KAM
(sign):
Page 1 of 3

METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Duke
Lab ID#
24634 / 24635 / 24636 12463
Date:
4/30/15
Time Analysis Begun
14:00
Time Analysis Ended
17:14
Ug S I U STU
SOLUTION ABS
"" " i "",
0.00 0.006-
1.00 0.092
Sloe
2.50 0,223
MAX ALIQU
5.00 0.422
SAMPLE
I.D.
7.50 0.605
40721
10.00 0.777
Cal Std Lot:
Page 17 of 41
ELEMENT ONE
Wave Length 664
"" " i "",
SPK LEVEL
Sloe
0.0776
MAX ALIQU
Na2S•9H2O Lot #
SAMPLE
I.D.
STANDARD
40721
ALI in mL
ANALYZED
Cal Std Lot:
ALI in mL
TAKEN
RESULTS
ug/mL
QC Std Lot:
SPIKE
LEVEL
Std. B. 0.00
STD ABSOF
E.
X
Page 2 of 3
Sloe
0.0776
Correlation
0.998884276
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
0.00
Std. B. 1.00
0.099
0.9105
10
10
10
<
91%
1.00
Std. B. 2.50
0.230
1 2.6747
10
10
10
0.267
107%
2.50
Std. B. 5.00
0.428
1 5.3411
10
10
10
0.534
107%
5.00
Std. B. 7.50
0.601
7.6709
10
10
10
0.767
102%
7.50
Std. B. 10.00
0.759
9.7987
10
10
10
0.980
98%
10.00
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.431
5.3815
10
10
10
0.538
108%
5.0
QC
0.432
5.3950
10
10
10
0.539
5.0
24637-2
0.037
0.0755
10
10
10
24637-2 s k
0.433
5.4084
10
10
10
0.541
108%
5.0
24637-3
0.001
-0.4093
10
10
10
24637-3 dup
0.002
-0.3958
10
10
10
< 0.1
24637-3 s k
0.382
4.7216
10
10
10
0.472
94%
5.0
24637-4
0.072
0.5469
10
10
10
<,0:1
24637-4 s k
0.458
5.7451
10
10
10
0.575
115%
5.0
24637-5
0.063
0.4257
10
10
10
24637-5 s k
0.460
5.7721
10
10
10
0.577
115%
5.0
24637-6
0.029
-0.0322
10
10
10<¢1
°:�',
24637-6 s k
0.416
5.1795
10
10
10
0.518
104%
5.0
24637-7
-0.002
0.0000
10
10
10
24637-7 s k
0.413
5.1391
10
10
10
0.514
103%
5.0
24635
-0.001
0.0000
10
10
5
<
24635 spk
0.051
0.2641
10
10
5
<
5%
5.0
24636-1
0.011
-0.2746
10
10
5
<
24636-1 s k
0.254
2.9979
10
10
5
0.600
60%
5.0
24636-2
0.001
-0.4093
10
10
5
< (},.
24636-2 s k
0.388
4.8024
10
10
5
0.960
96%
5.0
Blank
0.000
0.0000 1
10
10
10
<
QC
0.423
5.2738 1
10
10
10
0.527
105%
5.0
Subm►tted for QA/QC-
Date: 4/30/15
By: (Print)
KAM
(sign):
Page 2 of 3

METHOD:
SM 4500 S2- D
ELEMENT ASSAY:
Sulfide
CLIENT:
Duke
Lab ID#
24634 / 24635 / 24636 / 2463
Date:
4/30/15
Time Analysis Begun
14;00
Time Analysis Ended
17:14
x
y
ug STD
STD
ELUTION
ABS
0.00
0.000
1.00
0.092
2.50
0.223
5.00
0.422
7.50
0.605
10.00
n 777
Page 18 of 41
ELEMENT ONE
Wave Length 664 Ur- i M, I iUN u14i i lugl
SPK LEVEL (ugj
MAX ALIQUOT
Na2S•9H2O Lot # STANDARD conc(ppm)
40721 Cal Std Lot: WG2- -A,-
QC Std Lot: vJL2--1 ko-
STD ABSORPTION
X
10
Y
a�
I SG
WOO ,200
x
Page 3 of 3
SAMPLE
SAMP
ug PER
ALI in mL
PREP
Slope
0.0776'
Correlation
0.998884275
I.D.
ABS
ALIQUOT
ANALYZED
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std. B. 0.00
0.000
0.0000
10
10
10
<
Std. B. 1.00
0.099
0.9105
10
10
10
<
0.00
Std. B. 2.50
0.230
2.6747
10
10
10
0.267
91 %
107%
1.00
2.50
Std. B. 5.00
0.428
5.3411
10
10
10
0.534
107%
5.00
Std. B. 7.50
0.601
7.6709
10
10
10
0.767
102%
7.50
Std. B. 10.00
0.759
9.7987
10
10
10
0.980
98%
10.00
LRB
0.000
0.0000
10
10
10
<
0
LRB SPK
0.431
5.3815
10
10
10
0.538
108%
5.0
QC
0.432
5.3950
10
10
10
0.539
5.0
24636-3
-0.002
0.0000
10
10
5
<
24636-3 s k
0.304
3.6712
10
10
5
0.734
73%
5.0
24635
-0.004
0.0000
10
10
2
<
24635 s k
0.137
1.4222
10
10
2
0.711
28%
5.0
24636-1
0.005
-0.3554
10
10
2
4aK
24636-1 s k
0.357
4.3850
10
10
2
2.192
88%
5.0
24636-3
-0.003
0.0000
10
10
2
,,'
24636-3 du
-0.002
0.0000
10
10
2
< 0.5
24636-3 s k
0.348
4.2638
10
10
2
2.132
85%
5.0
24635
-0.004
0.0000
10
10
0.5
<
24635 sok
0.265
3.1460
10
10
0.5
6.292
63%
5.0
24635
-0.001
0.0000
10
10
0.25
4�Q
24635 spk
0.311
3.7655
10
10
0.25
15.062
75%
5.0
Blank
0
0.0000
10
10
10
<
QC 0.423
Subm/tf@d for QA/QC-
5.2738
10
10
10
0.527
105%
5.0
Date: 4/30/15
Bv: (Print)
WARA _:__.-
Page 3 of 3

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water - Asheville
Project Number:J15040667
Lot Number:QD28033
Date Completed:05/07/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
* QD28033*
Shealy Environmental Services, Inc. Page: 1 of 12
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SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QD28033
Project Name: AB GW Assessment Water - Asheville
Project Number: J15040667
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QD28033
Project Name: AB GW Assessment Water - Asheville
Project Number: J15040667
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
2015012277
Aqueous
04/27/2015 0935
04/28/2015
002
2015012278
Aqueous
04/27/20151140
04/28/2015
003
2015012279
Aqueous
04/27/20151350
04/28/2015
004
2015012280
Aqueous
04/27/2015 0845
04/28/2015
(4 samples)
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QD28033
Project Name: AB GW Assessment Water - Asheville
Project Number: J15040667
Sample Sample ID Matrix Parameter Method Result Q Units Page
001
2015012277
Aqueous
Alkalinity
SM 2320B-
25
mg/L
5
001
2015012277
Aqueous
Bicarbonate Alkalinity
SM 2320B-
25
mg/L
5
002
2015012278
Aqueous
Alkalinity
SM 2320B-
76
mg/L
7
002
2015012278
Aqueous
Bicarbonate Alkalinity
SM 2320B-
76
mg/L
7
003
2015012279
Aqueous
Alkalinity
SM 2320B-
46
mg/L
9
003
2015012279
Aqueous
Bicarbonate Alkalinity
SM 2320B-
46
mg/L
9
(6 detections)
Shealy Environmental Services, Inc. Page: 4 of 12
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QD28033-001
Description: 2015012277 Matrix: Aqueous
Date Sampled:04/27/2015 0935 Project Name: AB GW Assessment Water -
Date Received: 04/28/2015 Project Number: J15040667
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 23208-2011
1 04/30/2015 1128
HMA 73722
1
(Bicarbonate ) SM 2320B-2011
1 04/30/2015 1128
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/30/2015 1128
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
25
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
25
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QD28033-001
Description: 2015012277 Matrix: Aqueous
Date Sampled:04/27/2015 0935 Project Name: AB GW Assessment Water -
Date Received: 04/28/2015 Project Number: J15040667
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 RSK - 175 1 05/05/2015 1055 DCS 74077
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 2
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QD28033-002
Description: 2015012278 Matrix: Aqueous
Date Sampled:04/27/2015 1140 Project Name: AB GW Assessment Water -
Date Received: 04/28/2015 Project Number: J15040667
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/30/2015 1137
HMA 73722
1
(Bicarbonate ) SM 2320B-2011
1 04/30/2015 1137
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/30/2015 1137
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
76
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
76
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QD28033-002
Description: 2015012278 Matrix: Aqueous
Date Sampled:04/27/2015 1140 Project Name: AB GW Assessment Water -
Date Received: 04/28/2015 Project Number: J15040667
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 RSK - 175 1 05/05/2015 1117 DCS 74077
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 2
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QD28033-003
Description: 2015012279 Matrix: Aqueous
Date Sampled:04/27/2015 1350 Project Name: AB GW Assessment Water -
Date Received: 04/28/2015 Project Number: J15040667
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/30/2015 1140
HMA 73722
1
(Bicarbonate ) SM 2320B-2011
1 04/30/2015 1140
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/30/2015 1140
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
46
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
46
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QD28033-003
Description: 2015012279 Matrix: Aqueous
Date Sampled:04/27/2015 1350 Project Name: AB GW Assessment Water -
Date Received: 04/28/2015 Project Number: J15040667
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 RSK - 175 1 05/05/2015 1159 DCS 74077
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 2
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QD28033-004
Description: 2015012280 Matrix: Aqueous
Date Sampled:04/27/2015 0845 Project Name: AB GW Assessment Water -
Date Received: 04/28/2015 Project Number: J15040667
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/30/2015 1144
HMA 73722
1
(Bicarbonate ) SM 2320B-2011
1 04/30/2015 1144
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/30/2015 1144
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QD28033-004
Description: 2015012280 Matrix: Aqueous
Date Sampled:04/27/2015 0845 Project Name: AB GW Assessment Water -
Date Received: 04/28/2015 Project Number: J15040667
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
2 RSK - 175 1 05/05/2015 1220 DCS 74077
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 2
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QD28033
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Inorganic non-metals - Ii
Sample ID: QQ73722-001 Matrix: Aqueous
Batch: 73722
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 04/30/2015 0000
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD28033
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Inorganic non-metals - LCS
Sample ID: QQ73722-002 Matrix: Aqueous
Batch: 73722
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 100 1 100 90-110 04/30/2015 0000
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD28033
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MS
Sample ID: QD28033-001 MS Matrix: Aqueous
Batch: 73722
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 25 100 130 1 100 70-130 04/30/20151132
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD28033
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MSD
Sample ID: QD28033-001MD Matrix: Aqueous
Batch: 73722
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Alkalinity 25 100 120 1 95 4.0 70-130 20 04/30/20151135
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD28033
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ74077-001 Matrix: Aqueous
Batch: 74077
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 05/05/20151004
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD28033
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ74077-002 Matrix: Aqueous
Batch: 74077
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 120 1 81 70-130 05/05/2015 0934
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD28033
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ74077-003 Matrix: Aqueous
Batch: 74077
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 130 1 84 2.9 70-130 30 05/05/2015 0921
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD28033
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Shealy FnvironmMUll 51rviVM,1114- Fade 1 of l
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Sample Receipt Checklist (SRC
(Client: fij... �� Corder Ltsp4ctad hedatt=lrr�r-r,�,13-[tt #
Mina of receipt. t9LBS1 ❑ Clicxxt ❑ UPS ❑ FedEx ❑ Airborne Exp Z(Xher
Ycs U I No 1 1 1. Were c-ustody seals prtsent on the cooler?
Yes U I No LJ I NA 2, If custody ":i werLMamt, were they intact and unbroken'.?
Cooler ID/Onghud tcmpmture upon receipL-'l rived (corrected) temperature upon receipt=
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Mcthtad. ❑ Tcmperature Blank 2rAgEllinst BoWes IR Gun LD: #4 fly Gun Correction Fact,nr. Q --v-'1 `�C
Maltod of olanl; E Wet lee EJ Blue Ice U 2X Ice None
3, If # p tore 4f any coolar exoetxW 6.r1 T, was Project Adan yer notif*icd?
Yec E] No E]N_k PILI notified by SRC, phone, dote (ctirde aye). outer.
{For coolers re vved via rommeiciml courier, PNIs are to be notified
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4- Is the comm=ial paurir~r`s paolcing slip attached to this form'
{. Were proper custody procedures (reliagiiishcd+recvived) fvllawc d?
Sa Were samples rclingwshod by climl to wi memial courier?
6. Were sate le DDs list -ed ca the COC? -
7. W= sample iD-s lis; cd un all sarrlple cootainers?
S. Was collection date & tune listed sm the COC?
9. Was w1lection date & time listed on all sample containm?
10. Did ell container label information (ID, dale, timt) agree wish die COC?
11. Wem teats to be puformod listed On the COC'7
12- Did al I samples arrive in the prgper containers for me h test?
13- Did all containers arrive in pod wndirion itnhrol€m lids on, etc -
14, Was arlerlualtl� sraiple volmiae available?
L5, Were all sampler rmeived within °'s the holding time or 48 hours, whichcNrcr
comes first?
16. Wcrr any samp1m containelrs suis"'?
17. were tlxcrre eny emesis Samples not f isted on t_ OIC`t
19- Were bubbles present >"pea-si " (%"or Emig in diameter) in any l,'0_4, V ials?
19. Were all metalrVO&GelH /nutrient sampica rw6veZ at a pli r,et` <2ry
20. is erc all cymide an&r,)r sulfide sentitsles received at a pH >12? _
21 - Were al -L applicable NW)TICU'cyanide)pbenol (<U.2mWL-) salinples free of
residual chlorine?
Yr.r ❑ No ❑ I NA U 122. Were wil lion Lewriperaturex dnmmented on the COC for NC samples?
Yep ❑ No ❑ NA E� 23, Were client remarks,{requests (i.e. requested dilutions, MS ASD dtsiginlins,
ate.., cciTeOly Umserfbed from the COC into the comment swim in L1M5?
Yes ❑ ND 24. Was the qucAo number used taken frum the cuntd*cr ]alae]?
Sample Preservatian (Mtt,t he complctcd fnr anv samplc(s)incurrcctly preserved or with h+eadsp e.)
Semple(s) were receives] in+cclrreetly preserved and were, adjusted
amordin in Enghe receivin with (1+SO4. N0-; HCl Na0H) using SR 4
5 k(s) wur4: received with bubblea >6mro in d_ianieter. _
S . le s ' mwe reMwd with TRC 201 al fl- If 121 is NQ
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"Inking WuLci Prujret Sample(s) pH verified to be = 2 by Date-.
Sara le( -s ) were not received at a -1 of <2 and were Austed accordinrjy rising SR#
Sarnvlc labels applicdhv: , Vcriticd bv: Dave: `-Wk A%
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

C14AIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM
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