NC0000396_J15040110 MH report_20150823

DUKE Analytical Laboratory
ENERGY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Order Number: J15040110
Project Name: AB GW ASSESSMENT WATER
Customer Name(s): Todd Plating, Kathy Webb, John Toepfer, Tim Hunsucker
Customer Address: 200 CP and L Drive
Arden,NC 28704
Lab Contact: Mary Ann Oale Mary Ann Ogle Phone: [phone]
2015.04.23 13:14:07
Report Authorized By: ✓ -04'00' Date: 4/22/2015
(Signature)
Mary Ann Ogle
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
Page 1 of 55
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
Collected By
Sample Description
2015009638
ASHEVILLE
02 -Apr -15 10:40 AM
Matt Huddleston
SW -04
2015009639
ASHEVILLE
02 -Apr -15 11:00 AM
Matt Huddleston
FIELD BLANK
2015009640
ASHEVILLE
02 -Apr -15 11:25 AM
Matt Huddleston
A-01
2015009641
ASHEVILLE
02 -Apr -15 12:10 PM
Matt Huddleston
SW -01
2015009642
ASHEVILLE
02 -Apr -15 2:20 PM
Matt Huddleston
P-01
2015009643
ASHEVILLE
02 -Apr -15 2:30 PM
Matt Huddleston
P-01 Dup
6 Total Samples
Page 2 of 55

Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals Yes No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes No
All laboratory QA/QC requirements are acceptable. (] Yes ❑ No
Report Sections Included:
LU Job Summary Report
❑ Sample Identification
P/1 Technical Validation of Data Package
J❑ Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
Page 3 of 55
LVI Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
d❑ Chain of Custody
LVI Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: DBA Account Date: 4/22/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # A 5040110
Site: SW -04
Collection Date: 02 -Apr -15 10:40 AM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 353.2
Vendor Parameter
Complete
20
EPA 300.0
NITRITE + NITRATE (COLORIMETRIC)
JAHERMA
10
Nitrite + Nitrate (Colorimetric)
0.236
mg-N/L
0.01
INORGANIC IONS BY IC
V_SHEALY
1
Chloride
150
mg/L
2
Sulfate
64
mg/L
1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
MHALL3
Vendor Parameter
Complete
04/08/2015 11:26
MHALL3
DISSOLVED METALS BY ICP
EPA 200.7
04/08/2015 11:26
MHALL3
Aluminum (AI)
0.007
mg/L
0.005
Barium (Ba)
0.147
mg/L
0.005
Boron (B)
1.24
mg/L
0.05
Iron (Fe)
1.13
mg/L
0.01
Manganese (Mn)
0.391
mg/L
0.005
Strontium (Sr)
0.404
mg/L
0.005
Zinc (Zn)
0.013
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
04/08/2015 12:49
MHH7131
Calcium (Ca)
66.7
mg/L
0.01
Magnesium (Mg)
22.0
mg/L
0.005
Potassium (K)
2.52
mg/L
0.1
Sodium (Na)
9.56
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
EPA 200.7
04/08/2015 12:49
Aluminum (AI)
1.84
mg/L
0.005
Barium (Ba)
0.180
mg/L
0.005
Boron (B)
1.21
mg/L
0.05
Iron (Fe)
20.1
mg/L M4
0.05
Manganese (Mn)
0.500
mg/L
0.005
Strontium (Sr)
0.404
mg/L
0.005
Zinc (Zn)
0.013
mg/L
0.005
Page 4 of 55
Sample #: 2015009638
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
04/07/2015 12:47
BGN9034
20
EPA 300.0
04/08/2015 22:14
JAHERMA
10
EPA 300.0
04/08/2015 22:14
JAHERMA
Vendor Method
V_SHEALY
1
EPA 200.7
04/08/2015 11:26
MHALL3
1
EPA 200.7
04/08/2015 11:26
MHALL3
1
EPA 200.7
04/08/2015 11:26
MHALL3
1
EPA 200.7
04/08/2015 11:26
MHALL3
1
EPA 200.7
04/08/2015 11:26
MHALL3
1
EPA 200.7
04/08/2015 11:26
MHALL3
1
EPA 200.7
04/08/2015 11:26
MHALL3
1
EPA 200.7
04/08/2015 13:20
MHALL3
1
EPA 200.7
04/08/2015 13:20
MHALL3
1
EPA 200.7
04/08/2015 13:20
MHALL3
1
EPA 200.7
04/08/2015 13:20
MHALL3
1
EPA 200.7
04/08/2015 12:49
MHH7131
1
EPA 200.7
04/08/2015 12:49
MHH7131
1
EPA 200.7
04/08/2015 12:49
MHH7131
5
EPA 200.7
04/08/2015 12:49
MHH7131
1
EPA 200.7
04/08/2015 12:49
MHH7131
1
EPA 200.7
04/08/2015 12:49
MHH7131
1
EPA 200.7
04/08/2015 12:49
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # A 5040110
Site: SW -04
Collection Date: 02 -Apr -15 10:40 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
2.31
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
1.76
Cobalt (Co)
2.48
Copper (Cu)
1.71
Lead (Pb)
1.96
Molybdenum (Mo)
< 1
Nickel (Ni)
1.60
Selenium (Se)
6.34
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
2.77
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
620
Total Carbon
04/20/2015 12:20
TOC
2.8
TOTAL SUSPENDED SOLIDS
1
TSS
63
Page 5 of 55
ug/L
1
1
Sample #:
2015009638
JAHERMA
ug/L
1
1
Matrix:
GW -WW
JAHERMA
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
04/20/2015 12:20
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:20
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:20
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:20
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:20
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:20
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:20
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:20
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:20
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:20
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:20
DJSULL1
ug/L
0.2
1
EPA 200.8
04/20/2015 12:20
DJSULL1
ug/L
0.3
1
EPA 200.8
04/20/2015 12:20
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:06
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:06
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:06
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:06
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:06
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:06
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:06
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:06
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:06
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:06
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:06
JAHERMA
ug/L
0.2
1
EPA 200.8
04/17/2015 12:06
JAHERMA
ug/L
0.3
1
EPA 200.8
04/17/2015 12:06
JAHERMA
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
04/08/201514:41 AGIBBS5
mg/L
0.1 1 SM5310C/EPA9060A
04/09/201514:12 GHUTCHI
mg/L
5 1 SM2540D
04/08/2015 09:44 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # A 5040110
Site: FIELD BLANK
Collection Date: 02 -Apr -15 11:00 AM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
BGN9034
Vendor Parameter
Complete
JAHERMA
1 EPA 300.0
NITRITE + NITRATE (COLORIMETRIC)
JAHERMA
Vendor Method
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
1 EPA 200.7
04/08/2015 12:23
MHALL3
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
04/08/2015 12:23
Vendor Parameter
Complete
04/08/2015 12:23
MHALL3
DISSOLVED METALS BY ICP
04/08/2015 13:58
MHALL3
1 EPA 200.7
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
< 0.01
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Page 6 of 55
Sample #: 2015009639
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
04/07/2015 12:49
BGN9034
1 EPA 300.0
04/08/2015 22:50
JAHERMA
1 EPA 300.0
04/08/2015 22:50
JAHERMA
Vendor Method
V_SHEALY
1 EPA 200.7
04/08/2015 12:23
MHALL3
1 EPA 200.7
04/08/2015 12:23
MHALL3
1 EPA 200.7
04/08/2015 12:23
MHALL3
1 EPA 200.7
04/08/2015 12:23
MHALL3
1 EPA 200.7
04/08/2015 12:23
MHALL3
1 EPA 200.7
04/08/2015 12:23
MHALL3
1 EPA 200.7
04/08/2015 12:23
MHALL3
1 EPA 200.7
04/08/2015 13:58
MHALL3
1 EPA 200.7
04/08/2015 13:58
MHALL3
1 EPA 200.7
04/08/2015 13:58
MHALL3
1 EPA 200.7
04/08/2015 13:58
MHALL3
1 EPA 200.7
04/08/2015 13:01
MHH7131
1 EPA 200.7
04/08/2015 13:01
MHH7131
1 EPA 200.7
04/08/2015 13:01
MHH7131
1 EPA 200.7
04/08/2015 13:01
MHH7131
1 EPA 200.7
04/08/2015 13:01
MHH7131
1 EPA 200.7
04/08/2015 13:01
MHH7131
1 EPA 200.7
04/08/2015 13:01
MHH7131

Certificate of Laboratory Analysis Page 7 of 55
This report shall not be reproduced, except in full.
Order # A 5040110
Site: FIELD BLANK
Sample #: 2015009639
Collection Date: 02 -Apr -15 11:00
AM
Matrix: GW
-WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP -MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:34
DJSULL1
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:34
DJSULL1
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:34
DJSULL1
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:34
DJSULL1
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:34
DJSULL1
Cobalt (Co)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:34
DJSULL1
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:34
DJSULL1
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:34
DJSULL1
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:34
DJSULL1
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:34
DJSULL1
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:34
DJSULL1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/20/2015 12:34
DJSULL1
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/20/2015 12:34
DJSULL1
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:10
JAHERMA
Arsenic (As)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:10
JAHERMA
Beryllium (Be)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:10
JAHERMA
Cadmium (Cd)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:10
JAHERMA
Chromium (Cr)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:10
JAHERMA
Cobalt (Co)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:10
JAHERMA
Copper (Cu)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:10
JAHERMA
Lead (Pb)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:10
JAHERMA
Molybdenum (Mo)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:10
JAHERMA
Nickel (Ni)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:10
JAHERMA
Selenium (Se)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:10
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/17/2015 12:10
JAHERMA
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/17/2015 12:10
JAHERMA
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
< 25
mg/L
25
1
SM2540C
04/08/2015 14:41
AGIBBS5
Total Carbon
TOC
1.8
mg/L
0.1
1
SM5310C/EPA9060A
04/09/201514:12
GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS
<5
mg/L
5
1
SM2540D
04/08/2015 09:44
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # A 5040110
Site: A-01
Collection Date: 02 -Apr -15 11:25 AM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 353.2
Vendor Parameter
Complete
20
EPA 300.0
NITRITE + NITRATE (COLORIMETRIC)
JAHERMA
10
Nitrite + Nitrate (Colorimetric)
0.910
mg-N/L
0.01
INORGANIC IONS BY IC
V_SHEALY
1
Chloride
100
mg/L
2
Sulfate
72
mg/L
1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
MHALL3
Vendor Parameter
Complete
04/08/2015 11:15
MHALL3
DISSOLVED METALS BY ICP
EPA 200.7
04/08/2015 11:15
MHALL3
Aluminum (AI)
0.020
mg/L
0.005
Barium (Ba)
0.159
mg/L
0.005
Boron (B)
1.51
mg/L
0.05
Iron (Fe)
0.350
mg/L
0.01
Manganese (Mn)
0.483
mg/L
0.005
Strontium (Sr)
0.308
mg/L
0.005
Zinc (Zn)
0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
04/08/2015 13:05
MHH7131
Calcium (Ca)
46.3
mg/L
0.01
Magnesium (Mg)
19.3
mg/L
0.005
Potassium (K)
2.57
mg/L
0.1
Sodium (Na)
9.56
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
EPA 200.7
04/08/2015 13:05
Aluminum (AI)
3.21
mg/L
0.005
Barium (Ba)
0.184
mg/L
0.005
Boron (B)
1.46
mg/L
0.05
Iron (Fe)
5.67
mg/L
0.01
Manganese (Mn)
0.552
mg/L
0.005
Strontium (Sr)
0.310
mg/L
0.005
Zinc (Zn)
0.020
mg/L
0.005
Page 8 of 55
Sample #: 2015009640
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
04/07/2015 12:50
BGN9034
20
EPA 300.0
04/08/2015 22:32
JAHERMA
10
EPA 300.0
04/08/2015 22:32
JAHERMA
Vendor Method
V_SHEALY
1
EPA 200.7
04/08/2015 11:15
MHALL3
1
EPA 200.7
04/08/2015 11:15
MHALL3
1
EPA 200.7
04/08/2015 11:15
MHALL3
1
EPA 200.7
04/08/2015 11:15
MHALL3
1
EPA 200.7
04/08/2015 11:15
MHALL3
1
EPA 200.7
04/08/2015 11:15
MHALL3
1
EPA 200.7
04/08/2015 11:15
MHALL3
1
EPA 200.7
04/08/2015 13:28
MHALL3
1
EPA 200.7
04/08/2015 13:28
MHALL3
1
EPA 200.7
04/08/2015 13:28
MHALL3
1
EPA 200.7
04/08/2015 13:28
MHALL3
1
EPA 200.7
04/08/2015 13:05
MHH7131
1
EPA 200.7
04/08/2015 13:05
MHH7131
1
EPA 200.7
04/08/2015 13:05
MHH7131
1
EPA 200.7
04/08/2015 13:05
MHH7131
1
EPA 200.7
04/08/2015 13:05
MHH7131
1
EPA 200.7
04/08/2015 13:05
MHH7131
1
EPA 200.7
04/08/2015 13:05
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # A 5040110
Site: A-01
Collection Date: 02 -Apr -15 11:25 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.71
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
5.16
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
1.00
Cadmium (Cd)
< 1
Chromium (Cr)
2.88
Cobalt (Co)
3.23
Copper (Cu)
1.83
Lead (Pb)
2.26
Molybdenum (Mo)
< 1
Nickel (Ni)
2.99
Selenium (Se)
6.18
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
3.61
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
450
Total Carbon
04/20/2015 12:43
TOC
2.7
TOTAL SUSPENDED SOLIDS
1
TSS
51
Page 9 of 55
ug/L
1
1
Sample #:
2015009640
JAHERMA
ug/L
1
1
Matrix:
GW -WW
JAHERMA
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
04/20/2015 12:43
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:43
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:43
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:43
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:43
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:43
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:43
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:43
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:43
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:43
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:43
DJSULL1
ug/L
0.2
1
EPA 200.8
04/20/2015 12:43
DJSULL1
ug/L
0.3
1
EPA 200.8
04/20/2015 12:43
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:15
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:15
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:15
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:15
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:15
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:15
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:15
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:15
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:15
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:15
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:15
JAHERMA
ug/L
0.2
1
EPA 200.8
04/17/2015 12:15
JAHERMA
ug/L
0.3
1
EPA 200.8
04/17/2015 12:15
JAHERMA
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
04/08/201514:41 AGIBBS5
mg/L
0.1 1 SM5310C/EPA9060A
04/09/201514:12 GHUTCHI
mg/L
5 1 SM2540D
04/08/2015 09:44 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # A 5040110
Site: SW -01
Collection Date: 02 -Apr -15 12:10 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 353.2
Vendor Parameter
Complete
1
EPA 300.0
NITRITE + NITRATE (COLORIMETRIC)
JAHERMA
20
Nitrite + Nitrate (Colorimetric)
0.025
mg-N/L
0.01
INORGANIC IONS BY IC
V_SHEALY
1
Chloride
7.8
mg/L
0.1
Sulfate
19
mg/L
2
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
MHALL3
Vendor Parameter
Complete
04/08/2015 11:34
MHALL3
DISSOLVED METALS BY ICP
EPA 200.7
04/08/2015 11:34
MHALL3
Aluminum (AI)
0.010
mg/L
0.005
Barium (Ba)
0.013
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.398
mg/L
0.01
Manganese (Mn)
0.374
mg/L
0.005
Strontium (Sr)
0.039
mg/L
0.005
Zinc (Zn)
0.086
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
04/08/2015 13:10
MHH7131
Calcium (Ca)
7.03
mg/L
0.01
Magnesium (Mg)
2.94
mg/L
0.005
Potassium (K)
1.25
mg/L
0.1
Sodium (Na)
7.25
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
EPA 200.7
04/08/2015 13:10
Aluminum (AI)
0.062
mg/L
0.005
Barium (Ba)
0.014
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.948
mg/L
0.01
Manganese (Mn)
0.397
mg/L
0.005
Strontium (Sr)
0.040
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Page 10 of 55
Sample #: 2015009641
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
04/07/2015 12:51
BGN9034
1
EPA 300.0
04/09/2015 16:11
JAHERMA
20
EPA 300.0
04/09/2015 16:11
JAHERMA
Vendor Method
V_SHEALY
1
EPA 200.7
04/08/2015 11:34
MHALL3
1
EPA 200.7
04/08/2015 11:34
MHALL3
1
EPA 200.7
04/08/2015 11:34
MHALL3
1
EPA 200.7
04/08/2015 11:34
MHALL3
1
EPA 200.7
04/08/2015 11:34
MHALL3
1
EPA 200.7
04/08/2015 11:34
MHALL3
1
EPA 200.7
04/08/2015 11:34
MHALL3
1
EPA 200.7
04/08/2015 13:43
MHALL3
1
EPA 200.7
04/08/2015 13:43
MHALL3
1
EPA 200.7
04/08/2015 13:43
MHALL3
1
EPA 200.7
04/08/2015 13:43
MHALL3
1
EPA 200.7
04/08/2015 13:10
MHH7131
1
EPA 200.7
04/08/2015 13:10
MHH7131
1
EPA 200.7
04/08/2015 13:10
MHH7131
1
EPA 200.7
04/08/2015 13:10
MHH7131
1
EPA 200.7
04/08/2015 13:10
MHH7131
1
EPA 200.7
04/08/2015 13:10
MHH7131
1
EPA 200.7
04/08/2015 13:10
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # A 5040110
Site: SW -01
Collection Date: 02 -Apr -15 12:10 PM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
69
Total Carbon
04/20/2015 12:48
TOC
2.1
TOTAL SUSPENDED SOLIDS
1
TSS
< 5
Page 11 of 55
ug/L
1
1
Sample #:
2015009641
JAHERMA
ug/L
1
1
Matrix:
GW -WW
JAHERMA
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
04/20/2015 12:48
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:48
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:48
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:48
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:48
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:48
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:48
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:48
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:48
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:48
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:48
DJSULL1
ug/L
0.2
1
EPA 200.8
04/20/2015 12:48
DJSULL1
ug/L
0.3
1
EPA 200.8
04/20/2015 12:48
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 11:52
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 11:52
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 11:52
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 11:52
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 11:52
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 11:52
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 11:52
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 11:52
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 11:52
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 11:52
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 11:52
JAHERMA
ug/L
0.2
1
EPA 200.8
04/17/2015 11:52
JAHERMA
ug/L
0.3
1
EPA 200.8
04/17/2015 11:52
JAHERMA
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
04/08/201514:41 AGIBBS5
mg/L
0.1 1 SM5310C/EPA9060A
04/09/201514:12 GHUTCHI
mg/L
5 1 SM2540D
04/08/2015 09:44 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # A 5040110
Site: P-01
Collection Date: 02 -Apr -15 2:20 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
BGN9034
Vendor Parameter
Complete
JAHERMA
1 EPA 300.0
NITRITE + NITRATE (COLORIMETRIC)
JAHERMA
Vendor Method
Nitrite + Nitrate (Colorimetric)
1.4
mg-N/L
0.01
INORGANIC IONS BY IC
1 EPA 200.7
04/08/2015 11:38
MHALL3
Chloride
9.3
mg/L
0.1
Sulfate
9.4
mg/L
0.1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
04/08/2015 11:38
Vendor Parameter
Complete
04/08/2015 11:38
MHALL3
DISSOLVED METALS BY ICP
04/08/2015 13:09
MHALL3
1 EPA 200.7
Aluminum (AI)
0.027
mg/L
0.005
Barium (Ba)
0.030
mg/L
0.005
Boron (B)
0.052
mg/L
0.05
Iron (Fe)
0.173
mg/L
0.01
Manganese (Mn)
0.023
mg/L
0.005
Strontium (Sr)
0.074
mg/L
0.005
Zinc (Zn)
0.016
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
7.05
mg/L
0.01
Magnesium (Mg)
2.81
mg/L
0.005
Potassium (K)
1.79
mg/L
0.1
Sodium (Na)
6.64
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.335
mg/L
0.005
Barium (Ba)
0.032
mg/L
0.005
Boron (B)
0.051
mg/L
0.05
Iron (Fe)
0.746
mg/L
0.01
Manganese (Mn)
0.059
mg/L
0.005
Strontium (Sr)
0.071
mg/L
0.005
Zinc (Zn)
0.243
mg/L
0.005
Page 12 of 55
Sample #: 2015009642
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
04/07/2015 12:52
BGN9034
1 EPA 300.0
04/09/2015 16:31
JAHERMA
1 EPA 300.0
04/09/2015 16:31
JAHERMA
Vendor Method
V_SHEALY
1 EPA 200.7
04/08/2015 11:38
MHALL3
1 EPA 200.7
04/08/2015 11:38
MHALL3
1 EPA 200.7
04/08/2015 11:38
MHALL3
1 EPA 200.7
04/08/2015 11:38
MHALL3
1 EPA 200.7
04/08/2015 11:38
MHALL3
1 EPA 200.7
04/08/2015 11:38
MHALL3
1 EPA 200.7
04/08/2015 11:38
MHALL3
1 EPA 200.7
04/08/2015 13:09
MHALL3
1 EPA 200.7
04/08/2015 13:09
MHALL3
1 EPA 200.7
04/08/2015 13:09
MHALL3
1 EPA 200.7
04/08/2015 13:09
MHALL3
1 EPA 200.7
04/08/2015 13:14
MHH7131
1 EPA 200.7
04/08/2015 13:14
MHH7131
1 EPA 200.7
04/08/2015 13:14
MHH7131
1 EPA 200.7
04/08/2015 13:14
MHH7131
1 EPA 200.7
04/08/2015 13:14
MHH7131
1 EPA 200.7
04/08/2015 13:14
MHH7131
1 EPA 200.7
04/08/2015 13:14
MHH7131

Certificate of Laboratory Analysis Page 13 of 55
This report shall not be reproduced, except in full.
Order # A 5040110
Site: P-01
Sample #: 2015009642
Collection Date: 02 -Apr -15 2:20
PM
Matrix: GW
-WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP -MS
Antimony (Sb)
<1
ug/L
1
1
EPA 200.8
04/20/2015 12:52
DJSULL1
Arsenic (As)
<1
ug/L
1
1
EPA 200.8
04/20/2015 12:52
DJSULL1
Beryllium (Be)
<1
ug/L
1
1
EPA 200.8
04/20/2015 12:52
DJSULL1
Cadmium (Cd)
<1
ug/L
1
1
EPA 200.8
04/20/2015 12:52
DJSULL1
Chromium (Cr)
<1
ug/L
1
1
EPA 200.8
04/20/2015 12:52
DJSULL1
Cobalt (Co)
<1
ug/L
1
1
EPA 200.8
04/20/2015 12:52
DJSULL1
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:52
DJSULL1
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:52
DJSULL1
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:52
DJSULL1
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:52
DJSULL1
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/20/2015 12:52
DJSULL1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/20/2015 12:52
DJSULL1
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/20/2015 12:52
DJSULL1
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:19
JAHERMA
Arsenic (As)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:19
JAHERMA
Beryllium (Be)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:19
JAHERMA
Cadmium (Cd)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:19
JAHERMA
Chromium (Cr)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:19
JAHERMA
Cobalt (Co)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:19
JAHERMA
Copper (Cu)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:19
JAHERMA
Lead (Pb)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:19
JAHERMA
Molybdenum (Mo)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:19
JAHERMA
Nickel (Ni)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:19
JAHERMA
Selenium (Se)
<1
ug/L
1
1
EPA 200.8
04/17/2015 12:19
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/17/2015 12:19
JAHERMA
Vanadium (V) Low Level
0.570
ug/L
0.3
1
EPA 200.8
04/17/2015 12:19
JAHERMA
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
66
mg/L
25
1
SM2540C
04/08/201514:41
AGIBBS5
Total Carbon
TOC
1.3
mg/L
0.1
1
SM5310C/EPA9060A
04/09/201514:12
GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS
13
mg/L
5
1
SM2540D
04/08/2015 09:44
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # A 5040110
Site: P-01 Dup
Collection Date: 02 -Apr -15 2:30 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
BGN9034
Vendor Parameter
Complete
JAHERMA
1 EPA 300.0
NITRITE + NITRATE (COLORIMETRIC)
JAHERMA
Vendor Method
Nitrite + Nitrate (Colorimetric)
1.4
mg-N/L
0.01
INORGANIC IONS BY IC
1 EPA 200.7
04/08/2015 11:30
MHALL3
Chloride
9.3
mg/L
0.1
Sulfate
9.3
mg/L
0.1
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
04/08/2015 11:30
Vendor Parameter
Complete
04/08/2015 11:30
MHALL3
DISSOLVED METALS BY ICP
04/08/2015 12:47
MHALL3
1 EPA 200.7
Aluminum (AI)
0.026
mg/L
0.005
Barium (Ba)
0.029
mg/L
0.005
Boron (B)
0.053
mg/L
0.05
Iron (Fe)
0.170
mg/L
0.01
Manganese (Mn)
0.022
mg/L
0.005
Strontium (Sr)
0.073
mg/L
0.005
Zinc (Zn)
0.006
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
6.79
mg/L
0.01
Magnesium (Mg)
2.74
mg/L
0.005
Potassium (K)
1.73
mg/L
0.1
Sodium (Na)
6.49
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.348
mg/L
0.005
Barium (Ba)
0.032
mg/L
0.005
Boron (B)
0.051
mg/L
0.05
Iron (Fe)
0.765
mg/L
0.01
Manganese (Mn)
0.060
mg/L
0.005
Strontium (Sr)
0.072
mg/L
0.005
Zinc (Zn)
0.084
mg/L
0.005
Page 14 of 55
Sample #: 2015009643
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
04/15/2015 09:18
BGN9034
1 EPA 300.0
04/09/2015 16:50
JAHERMA
1 EPA 300.0
04/09/2015 16:50
JAHERMA
Vendor Method
V_SHEALY
1 EPA 200.7
04/08/2015 11:30
MHALL3
1 EPA 200.7
04/08/2015 11:30
MHALL3
1 EPA 200.7
04/08/2015 11:30
MHALL3
1 EPA 200.7
04/08/2015 11:30
MHALL3
1 EPA 200.7
04/08/2015 11:30
MHALL3
1 EPA 200.7
04/08/2015 11:30
MHALL3
1 EPA 200.7
04/08/2015 11:30
MHALL3
1 EPA 200.7
04/08/2015 12:47
MHALL3
1 EPA 200.7
04/08/2015 12:47
MHALL3
1 EPA 200.7
04/08/2015 12:47
MHALL3
1 EPA 200.7
04/08/2015 12:47
MHALL3
1 EPA 200.7
04/08/2015 13:18
MHH7131
1 EPA 200.7
04/08/2015 13:18
MHH7131
1 EPA 200.7
04/08/2015 13:18
MHH7131
1 EPA 200.7
04/08/2015 13:18
MHH7131
1 EPA 200.7
04/08/2015 13:18
MHH7131
1 EPA 200.7
04/08/2015 13:18
MHH7131
1 EPA 200.7
04/08/2015 13:18
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # A 5040110
Site: P-01 Dup
Collection Date: 02 -Apr -15 2:30 PM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.586
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
68
Total Carbon
04/20/2015 12:57
TOC
3.2
TOTAL SUSPENDED SOLIDS
1
TSS
14
Page 15 of 55
ug/L
1
1
Sample #:
2015009643
JAHERMA
ug/L
1
1
Matrix:
GW -WW
JAHERMA
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
04/20/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/20/2015 12:57
DJSULL1
ug/L
0.2
1
EPA 200.8
04/20/2015 12:57
DJSULL1
ug/L
0.3
1
EPA 200.8
04/20/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:24
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:24
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:24
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:24
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:24
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:24
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:24
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:24
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:24
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:24
JAHERMA
ug/L
1
1
EPA 200.8
04/17/2015 12:24
JAHERMA
ug/L
0.2
1
EPA 200.8
04/17/2015 12:24
JAHERMA
ug/L
0.3
1
EPA 200.8
04/17/2015 12:24
JAHERMA
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
04/08/201514:41 AGIBBS5
mg/L
0.1 1 SM5310C/EPA9060A
04/09/201514:12 GHUTCHI
mg/L
5 1 SM2540D
04/08/2015 09:44 AGIBBS5

Site: P-01 Dup
Collection Date: 02 -Apr -15 2:30 PM
Certificate of Laboratory Analysis Page 16 of 55
This report shall not be reproduced, except in full.
Order # A 5040110
Sample #: 2015009643
Matrix: GW -WW
Analyte Result Units Qualifiers RDL DF Method Analysis Date/Time Analyst
Qualifiers:
M4 The spike recovery value was unusable since the analyte concentration in the sample was disproportionate
to the spike level. The associated Laboratory Control Spike recovery was acceptable.

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water - Asheville
Project Number:J15040110
Lot Number:QD08015
Date Completed:04/16/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
* QD0801 5*
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SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QD08015
Project Name: AB GW Assessment Water - Asheville
Project Number: J15040110
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QD08015
Project Name: AB GW Assessment Water - Asheville
Project Number: J15040110
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
2015009638
Aqueous
04/02/20151040
04/08/2015
002
2015009639
Aqueous
04/02/20151100
04/08/2015
003
2015009640
Aqueous
04/02/20151125
04/08/2015
004
2015009641
Aqueous
04/02/20151210
04/08/2015
005
2015009642
Aqueous
04/02/20151420
04/08/2015
006
2015009643
Aqueous
04/02/20151430
04/08/2015
(6 samples)
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SHEALY ENVIRONMENTAL SERVICES, INC.
(12 detections)
Shealy Environmental Services, Inc. Page: 4 of 22
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Executive Summary
Duke Energy
Lot Number: QD08015
Project Name: AB GW Assessment Water - Asheville
Project Number: J15040110
Sample Sample ID
Matrix
Parameter Method Result Q
Units
Page
001
2015009638
Aqueous
Methane RSK - 175
34
ug/L
6
001
2015009638
Aqueous
Mercury (CVAFS) 1631E
7.67
ng/L
7
003
2015009640
Aqueous
Mercury (CVAFS) 1631E
36.7
ng/L
13
004
2015009641
Aqueous
Alkalinity SM 2320B-
15
mg/L
14
004
2015009641
Aqueous
Bicarbonate Alkalinity SM 2320B-
15
mg/L
14
004
2015009641
Aqueous
Mercury (CVAFS) 1631E
1.68
ng/L
16
005
2015009642
Aqueous
Alkalinity SM 2320B-
15
mg/L
17
005
2015009642
Aqueous
Bicarbonate Alkalinity SM 2320B-
15
mg/L
17
005
2015009642
Aqueous
Mercury (CVAFS) 1631E
2.12
ng/L
19
006
2015009643
Aqueous
Alkalinity SM 2320B-
15
mg/L
20
006
2015009643
Aqueous
Bicarbonate Alkalinity SM 2320B-
15
mg/L
20
006
2015009643
Aqueous
Mercury (CVAFS) 1631E
2.11
ng/L
22
(12 detections)
Shealy Environmental Services, Inc. Page: 4 of 22
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QD08015-001
Description: 2015009638 Matrix: Aqueous
Date Sampled:04/02/2015 1040 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/09/2015 1348
HMA 72090
1
(Bicarbonate ) SM 2320B-2011
1 04/09/2015 1348
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/09/2015 1348
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 22
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CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QD08015-001
Description: 2015009638 Matrix: Aqueous
Date Sampled:04/02/2015 1040 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/10/2015 1152 DCS 72301
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 34 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QD08015-001
Description: 2015009638 Matrix: Aqueous
Date Sampled:04/02/2015 1040 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 04/10/2015 2018 COH 04/08/2015 1131 72107
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 7.67 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QD08015-002
Description: 2015009639 Matrix: Aqueous
Date Sampled:04/02/2015 1100 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/09/2015 1353
HMA 72090
1
(Bicarbonate ) SM 2320B-2011
1 04/09/2015 1353
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/09/2015 1353
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 22
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CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QD08015-002
Description: 2015009639 Matrix: Aqueous
Date Sampled:04/02/2015 1100 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/10/2015 1204 DCS 72301
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QD08015-002
Description: 2015009639 Matrix: Aqueous
Date Sampled:04/02/2015 1100 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 04/10/2015 2022 COH 04/08/2015 1131 72107
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631 E ND 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QD08015-003
Description: 2015009640 Matrix: Aqueous
Date Sampled:04/02/2015 1125 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/09/2015 1400
HMA 72090
1
(Bicarbonate ) SM 2320B-2011
1 04/09/2015 1400
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/09/2015 1400
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 22
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CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QD08015-003
Description: 2015009640 Matrix: Aqueous
Date Sampled:04/02/2015 1125 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/10/2015 1222 DCS 72301
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QD08015-003
Description: 2015009640 Matrix: Aqueous
Date Sampled:04/02/2015 1125 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 8 04/10/2015 2152 COH 04/08/2015 1131 72107
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 36.7 4.00 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QD08015-004
Description: 2015009641 Matrix: Aqueous
Date Sampled:04/02/2015 1210 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/09/2015 1419
HMA 72090
1
(Bicarbonate ) SM 2320B-2011
1 04/09/2015 1419
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/09/2015 1419
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 14 of 22
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CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
15
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
15
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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Methane
Client: Duke Energy Laboratory ID: QD08015-004
Description: 2015009641 Matrix: Aqueous
Date Sampled:04/02/2015 1210 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/10/2015 1448 DCS 72301
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 15 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QD08015-004
Description: 2015009641 Matrix: Aqueous
Date Sampled:04/02/2015 1210 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 04/10/2015 2045 COH 04/08/2015 1131 72107
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 1.68 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 16 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QD08015-005
Description: 2015009642 Matrix: Aqueous
Date Sampled:04/02/2015 1420 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/09/2015 1425
HMA 72090
1
(Bicarbonate ) SM 2320B-2011
1 04/09/2015 1425
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/09/2015 1425
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 17 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
15
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
15
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 17 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QD08015-005
Description: 2015009642 Matrix: Aqueous
Date Sampled:04/02/2015 1420 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/10/2015 1458 DCS 72301
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 18 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QD08015-005
Description: 2015009642 Matrix: Aqueous
Date Sampled:04/02/2015 1420 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 04/10/2015 2050 COH 04/08/2015 1131 72107
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 2.12 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 19 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QD08015-006
Description: 2015009643 Matrix: Aqueous
Date Sampled:04/02/2015 1430 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/09/2015 1431
HMA 72090
1
(Bicarbonate ) SM 2320B-2011
1 04/09/2015 1431
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/09/2015 1431
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 20 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
15
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
15
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 20 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QD08015-006
Description: 2015009643 Matrix: Aqueous
Date Sampled:04/02/2015 1430 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/10/2015 1509 DCS 72301
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 21 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QD08015-006
Description: 2015009643 Matrix: Aqueous
Date Sampled:04/02/2015 1430 Project Name: AB GW Assessment Water -
Date Received: 04/08/2015 Project Number: J15040110
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 04/10/2015 2054 COH 04/08/2015 1131 72107
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 2.11 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 22 of 22
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QD08015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - Ii
Sample ID: QQ72090-001 Matrix: Aqueous
Batch: 72090
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 04/09/20151141
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD08015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ72090-002 Matrix: Aqueous
Batch: 72090
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 96 1 96 90-110 04/09/20151147
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD08015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MS
Sample ID: QD08015-006MS Matrix: Aqueous
Batch: 72090
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 15 100 110 1 96 70-130 04/09/20151437
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD08015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MSD
Sample ID: QD08015-006MD Matrix: Aqueous
Batch: 72090
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Alkalinity 15 100 110 1 99 1.9 70-130 20 04/09/20151443
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD08015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ72301-001 Matrix: Aqueous
Batch: 72301
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 04/10/2015 0943
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD08015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ72301-002 Matrix: Aqueous
Batch: 72301
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 140 1 90 70-130 04/10/2015 0919
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD08015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ72301-003 Matrix: Aqueous
Batch: 72301
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 140 1 95 5.1 70-130 30 04/10/2015 0929
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD08015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS) - MB
Sample ID: QQ72107-001 Matrix: Aqueous
Batch: 72107 Prep Method: 1631E
Analytical Method: 1631E Prep Date: 04/08/2015 1131
Parameter Result Q Dil PQL Units Analysis Date
Mercury (CVAFS) ND 1 0.500 ng/L 04/10/2015 1940
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD08015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS) - LCS
Sample ID: QQ72107-002 Matrix: Aqueous
Batch: 72107 Prep Method: 1631E
Analytical Method: 1631E Prep Date: 04/08/2015 1131
Spike
Amount Result % Rec
Parameter (ng/L) (ng/L) Q Dil % Rec Limit Analysis Date
Mercury (CVAFS) 5.00 4.42 1 88 75-125 04/10/2015 1945
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD08015
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Shealy PnuerormeniA SeMoc¢, Inc. Fl, V l d 1
Dwvincnl Nurnbcr-, FAD -016 Replaaee Dow 07115134
Rweaue riiim$er. 15 r'.#e Aiv4! DaW I leI F114
irtple Receipt Checklist (SRC)
Client: Cooler inspecletl by/date: + 1Lrat #: T , C .-
Meam ofrecseillt: ❑ SESI ❑ Client Ej UPS 0 1"cdEx ❑ Airbomn Rv L] Other
Yes 2q N, 1. Were czstod seals present on the oa>oler?
Yes No 1�IAI 2. If cusludx scalswese Prasent, wort thcy intact and unbrolrerp?
Wooler [Wor4inal temperaluiv upon receipt Merived ( rt' cmd) ie.mperature upon rcr,t:ipt:
hiartltod: E] Temperature l Aa�ainst Bottles TR Gur1 ID. #4 IR Gun Correction Factor: 0 °C
method of coolant= et lee El Blue Ice Dry Ice ❑ None
If temperature of any cooler exceeded 6.4°C, was. Pro)ccl Manager notitied?
I Yes ❑ No ❑ NA PM notified ty SRC, phone. Role (circle one), other:
(Foi coolers received via eomillerciral ckxrncrr, PMs are to be notified
Yos IZI
J90
I NA LJ
14. Is the scrmnusrdal courier's LbnA slip aaachcd to this form?
Yes.
a Q
5. Were pro r Custody roccduresresin uisherlftecoived followed?
Yes
a ❑
NA
5a Werc sautples resin uished by cJiant to commercial cptiri tO
Ye
s Q
[i. Were sample IDs listed on the +fit C1
Yes ,
' ❑
a. Were &aale IDLh. listed on all sample litainets?
YEs
�t ❑
8_ Waro clollecdon date & tinw listed on the COC?
Yep
e ❑
9. Wm call ection date & rime listed an all sale le enntairle . ?
Yes
o ❑
10. Did all container label informalion ID, date, time a ret with the COC?
Yip
0
11. W rc tests to be performed listed tin the CCC'
Yes
[]
12. Did all, sanTpIe8.avTj%T 1n the proper coatainexs for each test?
Yes
❑
13. Did all containers r3 nve in gpQd condil ion unbroken, lids on, etc,)?
Yrs
No ❑
14. Was ad ualc saWk, volume available?
Yes ❑
No
15. Were all samples reAxived within',A the holding time or 48 hours, w i,chever
comes fit -50
Yes ❑
N0
MWereany sant kiicontainer%missin
Yes ❑
Nd
17. Were there any excess sono les not listed on CSC?
Yes ❑
NoW
Iw1A ❑8.
Were bubbIcs rcm nt "yea-ciax" ' .i or 6mm in diaroe$er in �n VOA vials?
yes C]
No ❑
NA.
4. Were all metals,'C G?H7=[4'llnutrient 9 s rcccivcd ata pF of <2?
Yes ❑
No [31
NZT7
2.0. Were all cyanide andtctr sulfi de samples received at a PH >12?
Yes E]
I Tc.r El
NA21.
Were all applicable NH3rTl[c;N;acytlnidelrphevirA (<U.?rn �i.,) samples free. of
residual chIcaine?
Y�n U No U NA Pj 1 22, Were cotlecliom rempeTatums documented on the ODC for NC 3arn les?
Yes L. Nf7t U ra,1 .t. 23. Were client remarl[a,+requests (i.e. rcyuestcd dilutions, Iv VIVISD designalions,
eta,.. rrecctly transcribed from the COC into the c0rtmtent section in Ll Ms?
`Yes L D s 24Was Ills quote number used taken f om the container label?
SAMple PMervatiuo (Must N OULn leled fur any sarnple(s) incorrwly prescfwd or with bcadspam)
Samples) were received incorrectly prer�tved and wereadjustcd
-accor-dingly in sample receiving with H O4,I MO,-,HCI,Na.Ill asi ng SR #
Sa i ;, s were rectived v111 bubbles >b mm in diameter.
sampwswcrL; rcLcivcd with TRC >0.2 mitiL (lf#21 is NO)

el,
elementOne
Duke Energy
Laboratory Services
13339 Hagers Ferry Road Bid. MG03A
Huntersville, NC 28078
Sample Matrix
GW WW
Date Analyzed
04/08/2015
Delivered by
FedEx
eOne ID Duke Energy ID
24450-1 SW -04
Page 51 of 55
Element One Inc.
6319-D Carolina Beach Rd.
Wilmington, NC 28412
Phone: [phone]
Fax: [phone]
[e-mail]
REPORT OF ANALYSES
April 10, 2015
Client Project Name AB GW Assessment Water - Asheville
Client Project Number J15040110
PO Number
Sample Type
Grab
Date Received
04/08/2015
Method
SM 4500 S2- D
Time Received
1018
1100
24450-3
Received by
JRC
Parameter
Result Unit Dil
DL Date
Time
04/02/15
1125
Sampled
Sampled
Sulfide
< 0.1 mg/L 1
0.1 04/02/15
1040
24450-2
Field Blank
Sulfide
< 0.1
mg/L
1
0.1
04/02/15
1100
24450-3
A-01
Sulfide
< 0.1
mg/L
1
0.1
04/02/15
1125
24450-4
SW -01
Sulfide
< 0.1
mg/L
1
0.1
04/02/15
1210
24450-5
P-01
Sulfide
< 0.1
mg/L
1
0.1
04/02/15
1420
24450-6
P-01 Dup
Sulfide
< 0.1
mg/L
1
0.1
04/02/15
1430
lb-apilne Woodman, QA Officer
24450 Duke Report Packet Compiled by -N5 -
NC Certifications: DW 37788 and DWQ DENR 604

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Page 52 of 55
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elementOne SAMPLE SUBMISSION FORM
TAT 7 BD
Hold Time Expiration 04.09.15 @ 1040 AM
Client: Duke Energy
LIMS No J15040110
Project ID AB GW Assessment Water — Asheville
r
Lab I'De 5124450
Analysis Due Date 04.08.15
Report Due Date 04.16.15
Date Rec:
04.08.15
Time Rec:
1018
Rec By
JRC
04.02.15
1040 AM
H >9 Yes No
Temp <_ 6°C Yes No
Ref. Method:
SM4500 S2 D
If No, Record
If No, Record
Samnle Identification & Collection Information
Lab ID
Client ID
Collection Date
Collection Time Analysis Requested
1
SW -04
04.02.15
1040 AM
2
Field Blank
04.02.15
1100 AM
3
A-01
04.02.15
1125 AM
4
SW -01
04.02.15
1210 PM
5
P-01
04.02.15
1420 PM
6
P-01 Dup.
04.02.15
1430 PM u_�
The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
NOTE for Sulfide at 100 pg/L spike the sample to render the final spike concentration at — 500 pg/L
All AB Groundwater Assessment jobs need a RL of 0.1
Lab Communications
SS Page 1 q 1
SS by
4/8/2015 10:41:41 AM
Prep By / Date ( "' 114, , Is
Labeled By / Date eW 9. 9, j
ID Verification By /Date � Ll ,�'•l

Page 54 of 55
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
ug/mL
DETECTIONLIMIT u
1.000
CLIENT: Duke
SPK LEVEL (ugj
5
Lab ID#
Date:
Time Analysis Begun
Time Analysis Ended
Analyst:
X
ug STD
SOLUTION
0.00
1.00
2.50
5.00
7.50
10.00
24450
4/8/15
14:00
16:40
KAM
Y
STD
ABS
0.000
0.086
0.2081311
0.365
0.561
0.786
1.111
1.611
0,700
1.511
I 0410
0300
1111
O.000ow
201
Na2S•9H2O Lot #
40721
.365
4W 80o
X
MAX ALIQUOT
STANDARD conc(ppm)
Cal Std Lot:
QC Std Lot:
STD ABSORPTION
5,
60o ,o-
10.00
X
10
Y
,so
1200
Slope
0.07656044
Correlation
0.998616835
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
Std B. 0.00
0.00
10
10
10
<
0
Std B. 1.00
0.082
1.1112
10
10
10
0.111
111%
1.0
Std B. 2.50
0.183
2.4009
10
10
10
0.240
96%
2.5
Std B. 5.00
0.373
4.8271
10
10
10
0.483
97%
5.0
Std B. 7.50
0.56
7.2150
10
10
10
0.721
96%
7.5
Std B. 10.0
0.749
9.6284
10
10
10
0.963
96%
10.0
LRB
0
0.0000
10
10
10
<
LRB spk
0.374
4.8399
10
10
10
0.484
97%
5.0
QC
0.379
4.9037
10
10
10
0.490
98%
5.0
24450-1
0.013
0.2301
10
10
10
< 0.1
24450-1 spk
0.392
5.0697
10
10
10
0.507
101%
5.0
24450-2
0.010
0.1918
10
10
10
< 0.1
24450-2 dup
0
0.0000
10
10
10
< 0.1
NA
24450-2 spk
0.405
5.2357
10
10
10
0.524
105%
5.0
24450-3
0.017
0.2811
10
10
10
< 0.1
24450-3 spk
0.326
4.2269
10
10
10
0.423
85%
5.0
24450-4
0.004
0.1151
10
10
10
< 0.1
24450-4 spk
0.382
4.9420
10
10
10
0.494
99%
5.0
24450-5
0.002
0.0896
10
10
10
< 0.1
24450-5 spk
0.4
5.1719
10
10
10
0.517
103%
5.0
24450-6
0.003
0.1024
10
10
10
< 0.1
24450-6 spk
0.412
5.3251
10
10
10
0.533
107%
5.0
1000ppm Std QC
0.423
5.4656
10
10
10
0.547
109%
5.0
Blank
0
0.0000
10
10
10
<
QC
0.387
5.0059 1
10 1
10
10
0.501
100%
5.0
Submitted for QA/QC-
Date: 4/8/15
I
By: (Print)
KAM
(sign):

CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM
._. ---------------------------------------
- - - --- - -- ---- - ---- Energy --nal -ical Laboratory --t I---•-•-------._._._._._._._._,,..-----------------------•-•---•-------------------------._._._._._._._
Duke Energy ---� ._._._._._may � !
AnalWytical Lahorato Use Only
I Mau Cuae MGO3.az IBuiiding xdasl ! iorder L` Matrix GW_WW s.ma;a. orwdn.c;rrearcm HC—
Analytical Laboratory 13339 HagFerry Rd % < 7� SC
i Chain of Custody $ Hunterevi.e• N. G ..... L4 d B Date 7 ® a
Sample Log Ixogl9xssms i i age By - �.J �SAMPLE PROGRAM
i �u_�.g aTss.3e .___,______! i U T S EV Ground Water_ NPdES
._._._._._._._._._._._._._._._._._._._._...._.
Y Drinking Water U5T
Po H+ne/ AI3GWAssessm ntte Phonallo: jV' f 9
Ef 7v_ /Y+ e�S 1iSI�PsI/tih� 650-Sr1 f SHEAL`1� - - CoowrTemkh...................--.RCFta Waste—"- - - -
orax Ho: jF
Client 950-a75-5032 PO 1142089 tration (0.45 um) Unfiltered
B ' udIness Units— P f c`� Reap. Demar ra: i n Preservative Ice ice Ice H[Yt Ice
o --
Prn;ectlD: Actl�arle: N1p1JCad.: ier Volume (mL) 2000 40 ml 300 ,25 500 500
� r� MG03A3
wrterhndy: s,aemn V e m e ilt 1
Container Type PET glass PET PET RET PET dl
Page _t_Of_t_ SYNTERRA EDD
DISTRIBUTION Page 55 of 55
ORIGINAL to LAB, COPY to CLIENT
COC REV DATE 1122/2015
filtered
500 1 250
HDPEHDPE
PO 114L1Jj
Sample Description or ID c ,priare
non -shaded areas. -
Collection Information a st
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