NC0000396_J15040071report MH_20150823

DUKE Analytical Laboratory
ENERGY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Order Number: J15040071
Project Name: AB GW ASSESSMENT WATER
Customer Name(s): Todd Plating, Kathy Webb, John Toepfer, Tim Hunsucker
Customer Address: 200 CP and L Drive
Arden,NC 28704
Lab Contact: Mary Ann Ogle Phone: [phone]
V „ ( Mary Ann Ogle
Report Authorized By: 2015.04.23 Date:
(Signature) 1.2.011.4 -04'OV
Mary Ann Ogle
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
4/22/2015
Page 1 of 59
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
2015009463
2015009464
2015009465
2015009466
2015009467
2015009468
2015009469
7 Total Samples
Collected By
Sample Description
ASHEVILLE
01 -Apr -15 11:52 AM
Synterra
F-01
ASHEVILLE
01 -Apr -15 11:17 AM
Synterra
F-02
ASHEVILLE
01 -Apr -15 2:05 PM
Synterra
E-01
ASHEVILLE
01 -Apr -15 2:30 PM
Synterra
D-01
ASHEVILLE
01 -Apr -15 2:52 PM
Synterra
C-01
ASHEVILLE
01 -Apr -15 3:29 PM
Synterra
B-01
ASHEVILLE
Synterra
TRIP BLANK
Page 2 of 59

Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals Yes No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes No
All laboratory QA/QC requirements are acceptable. (] Yes ❑ No
Report Sections Included:
LU Job Summary Report
❑ Sample Identification
P/1 Technical Validation of Data Package
J❑ Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
Page 3 of 59
LVI Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
d❑ Chain of Custody
LVI Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: DBA Account Date: 4/22/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040071
Site: F-01
Collection Date: 01 -Apr -15 11:52 AM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 353.2
Vendor Parameter
Complete
20
EPA 300.0
NITRITE + NITRATE (COLORIMETRIC)
JAHERMA
20
Nitrite + Nitrate (Colorimetric)
0.062
mg-N/L
0.01
INORGANIC IONS BY IC
V_SHEALY
1
Chloride
19
mg/L
2
Sulfate
150
mg/L
2
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
MHALL3
Vendor Parameter
Complete
04/06/2015 12:26
MHALL3
DISSOLVED METALS BY ICP
EPA 200.7
04/06/2015 12:26
MHALL3
Aluminum (AI)
0.022
mg/L
0.005
Barium (Ba)
0.052
mg/L
0.005
Boron (B)
0.871
mg/L
0.05
Iron (Fe)
0.825
mg/L
0.01
Manganese (Mn)
0.908
mg/L
0.005
Strontium (Sr)
0.270
mg/L
0.005
Zinc (Zn)
0.008
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
04/07/2015 10:42
MHH7131
Calcium (Ca)
36.4
mg/L
0.01
Magnesium (Mg)
13.9
mg/L
0.005
Potassium (K)
2.59
mg/L
0.1
Sodium (Na)
17.9
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
EPA 200.7
04/07/2015 10:42
Aluminum (AI)
0.200
mg/L
0.005
Barium (Ba)
0.051
mg/L
0.005
Boron (B)
0.862
mg/L
0.05
Iron (Fe)
1.89
mg/L
0.01
Manganese (Mn)
0.928
mg/L
0.005
Strontium (Sr)
0.267
mg/L
0.005
Zinc (Zn)
0.005
mg/L
0.005
Page 4 of 59
Sample #: 2015009463
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
04/07/2015 12:29
BGN9034
20
EPA 300.0
04/06/2015 16:50
JAHERMA
20
EPA 300.0
04/06/2015 16:50
JAHERMA
Vendor Method
V_SHEALY
1
EPA 200.7
04/06/2015 12:26
MHALL3
1
EPA 200.7
04/06/2015 12:26
MHALL3
1
EPA 200.7
04/06/2015 12:26
MHALL3
1
EPA 200.7
04/06/2015 12:26
MHALL3
1
EPA 200.7
04/06/2015 12:26
MHALL3
1
EPA 200.7
04/06/2015 12:26
MHALL3
1
EPA 200.7
04/06/2015 12:26
MHALL3
1
EPA 200.7
04/06/2015 13:31
MHALL3
1
EPA 200.7
04/06/2015 13:31
MHALL3
1
EPA 200.7
04/06/2015 13:31
MHALL3
1
EPA 200.7
04/06/2015 13:31
MHALL3
1
EPA 200.7
04/07/2015 10:42
MHH7131
1
EPA 200.7
04/07/2015 10:42
MHH7131
1
EPA 200.7
04/07/2015 10:42
MHH7131
1
EPA 200.7
04/07/2015 10:42
MHH7131
1
EPA 200.7
04/07/2015 10:42
MHH7131
1
EPA 200.7
04/07/2015 10:42
MHH7131
1
EPA 200.7
04/07/2015 10:42
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040071
Site: F-01
Collection Date: 01 -Apr -15 11:52 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.29
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.61
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.380
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
290
Total Carbon
04/17/2015 12:52
TOC
0.893
TOTAL SUSPENDED SOLIDS
1
TSS
13
Page 5 of 59
ug/L
1
1
Sample #:
2015009463
JAHERMA
ug/L
1
1
Matrix:
GW -WW
JAHERMA
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
04/17/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:52
DJSULL1
ug/L
0.2
1
EPA 200.8
04/17/2015 12:52
DJSULL1
ug/L
0.3
1
EPA 200.8
04/17/2015 12:52
DJSULL1
ug/L
1
1
EPA 200.8
04/16/2015 12:07
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:07
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:07
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:07
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:07
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:07
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:07
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:07
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:07
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:07
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:07
JAHERMA
ug/L
0.2
1
EPA 200.8
04/16/2015 12:07
JAHERMA
ug/L
0.3
1
EPA 200.8
04/16/2015 12:07
JAHERMA
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
04/08/201514:41 AGIBBS5
mg/L
0.1 1 SM5310C/EPA9060A
04/09/201514:12 GHUTCHI
mg/L
5 1 SM2540D
04/06/2015 08:47 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040071
Site: F-02
Collection Date: 01 -Apr -15 11:17 AM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 353.2
Vendor Parameter
Complete
20
EPA 300.0
NITRITE + NITRATE (COLORIMETRIC)
JAHERMA
20
Nitrite + Nitrate (Colorimetric)
0.035
mg-N/L
0.01
INORGANIC IONS BY IC
V_SHEALY
1
Chloride
14
mg/L
2
Sulfate
150
mg/L
2
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
MHALL3
Vendor Parameter
Complete
04/06/2015 12:30
MHALL3
DISSOLVED METALS BY ICP
EPA 200.7
04/06/2015 12:30
MHALL3
Aluminum (AI)
0.027
mg/L
0.005
Barium (Ba)
0.042
mg/L
0.005
Boron (B)
0.383
mg/L
0.05
Iron (Fe)
0.549
mg/L
0.01
Manganese (Mn)
0.155
mg/L
0.005
Strontium (Sr)
0.180
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
04/07/2015 10:55
MHH7131
Calcium (Ca)
40.2
mg/L
0.01
Magnesium (Mg)
14.0
mg/L
0.005
Potassium (K)
1.73
mg/L
0.1
Sodium (Na)
12.0
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
EPA 200.7
04/07/2015 10:55
Aluminum (AI)
0.049
mg/L
0.005
Barium (Ba)
0.042
mg/L
0.005
Boron (B)
0.395
mg/L
0.05
Iron (Fe)
0.688
mg/L
0.01
Manganese (Mn)
0.156
mg/L
0.005
Strontium (Sr)
0.187
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Page 6 of 59
Sample #: 2015009464
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
04/07/2015 12:31
BGN9034
20
EPA 300.0
04/06/2015 17:08
JAHERMA
20
EPA 300.0
04/06/2015 17:08
JAHERMA
Vendor Method
V_SHEALY
1
EPA 200.7
04/06/2015 12:30
MHALL3
1
EPA 200.7
04/06/2015 12:30
MHALL3
1
EPA 200.7
04/06/2015 12:30
MHALL3
1
EPA 200.7
04/06/2015 12:30
MHALL3
1
EPA 200.7
04/06/2015 12:30
MHALL3
1
EPA 200.7
04/06/2015 12:30
MHALL3
1
EPA 200.7
04/06/2015 12:30
MHALL3
1
EPA 200.7
04/06/2015 13:35
MHALL3
1
EPA 200.7
04/06/2015 13:35
MHALL3
1
EPA 200.7
04/06/2015 13:35
MHALL3
1
EPA 200.7
04/06/2015 13:35
MHALL3
1
EPA 200.7
04/07/2015 10:55
MHH7131
1
EPA 200.7
04/07/2015 10:55
MHH7131
1
EPA 200.7
04/07/2015 10:55
MHH7131
1
EPA 200.7
04/07/2015 10:55
MHH7131
1
EPA 200.7
04/07/2015 10:55
MHH7131
1
EPA 200.7
04/07/2015 10:55
MHH7131
1
EPA 200.7
04/07/2015 10:55
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040071
Site: F-02
Collection Date: 01 -Apr -15 11:17 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
290
Total Carbon
04/17/2015 12:57
TOC
3.0
TOTAL SUSPENDED SOLIDS
1
TSS
< 5
Page 7 of 59
ug/L
1
1
Sample #:
2015009464
JAHERMA
ug/L
1
1
Matrix:
GW -WW
JAHERMA
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
04/17/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 12:57
DJSULL1
ug/L
0.2
1
EPA 200.8
04/17/2015 12:57
DJSULL1
ug/L
0.3
1
EPA 200.8
04/17/2015 12:57
DJSULL1
ug/L
1
1
EPA 200.8
04/16/2015 12:21
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:21
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:21
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:21
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:21
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:21
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:21
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:21
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:21
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:21
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:21
JAHERMA
ug/L
0.2
1
EPA 200.8
04/16/2015 12:21
JAHERMA
ug/L
0.3
1
EPA 200.8
04/16/2015 12:21
JAHERMA
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
04/08/201514:41 AGIBBS5
mg/L
0.1 1 SM5310C/EPA9060A
04/09/201514:12 GHUTCHI
mg/L
5 1 SM2540D
04/06/2015 08:47 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040071
Site: E-01
Collection Date: 01 -Apr -15 2:05 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 353.2
Vendor Parameter
Complete
20
EPA 300.0
NITRITE + NITRATE (COLORIMETRIC)
JAHERMA
20
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
V_SHEALY
1
Chloride
31
mg/L
2
Sulfate
140
mg/L
2
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
MHALL3
Vendor Parameter
Complete
04/06/2015 12:34
MHALL3
DISSOLVED METALS BY ICP
EPA 200.7
04/06/2015 12:34
MHALL3
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
0.064
mg/L
0.005
Boron (B)
0.682
mg/L
0.05
Iron (Fe)
0.398
mg/L
0.01
Manganese (Mn)
2.27
mg/L
0.005
Strontium (Sr)
0.310
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
04/07/2015 10:59
MHH7131
Calcium (Ca)
39.5
mg/L
0.01
Magnesium (Mg)
12.3
mg/L
0.005
Potassium (K)
3.97
mg/L
0.1
Sodium (Na)
26.7
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
EPA 200.7
04/07/2015 10:59
Aluminum (AI)
0.176
mg/L
0.005
Barium (Ba)
0.065
mg/L
0.005
Boron (B)
0.676
mg/L
0.05
Iron (Fe)
1.34
mg/L
0.01
Manganese (Mn)
2.22
mg/L
0.005
Strontium (Sr)
0.303
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Page 8 of 59
Sample #: 2015009465
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
04/07/2015 12:32
BGN9034
20
EPA 300.0
04/06/2015 17:26
JAHERMA
20
EPA 300.0
04/06/2015 17:26
JAHERMA
Vendor Method
V_SHEALY
1
EPA 200.7
04/06/2015 12:34
MHALL3
1
EPA 200.7
04/06/2015 12:34
MHALL3
1
EPA 200.7
04/06/2015 12:34
MHALL3
1
EPA 200.7
04/06/2015 12:34
MHALL3
1
EPA 200.7
04/06/2015 12:34
MHALL3
1
EPA 200.7
04/06/2015 12:34
MHALL3
1
EPA 200.7
04/06/2015 12:34
MHALL3
1
EPA 200.7
04/06/2015 13:39
MHALL3
1
EPA 200.7
04/06/2015 13:39
MHALL3
1
EPA 200.7
04/06/2015 13:39
MHALL3
1
EPA 200.7
04/06/2015 13:39
MHALL3
1
EPA 200.7
04/07/2015 10:59
MHH7131
1
EPA 200.7
04/07/2015 10:59
MHH7131
1
EPA 200.7
04/07/2015 10:59
MHH7131
1
EPA 200.7
04/07/2015 10:59
MHH7131
1
EPA 200.7
04/07/2015 10:59
MHH7131
1
EPA 200.7
04/07/2015 10:59
MHH7131
1
EPA 200.7
04/07/2015 10:59
MHH7131

Certificate of Laboratory Analysis Page 9 of 59
This report shall not be reproduced, except in full.
Order # J15040071
Site: E-01
Sample #: 2015009465
Collection Date: 01 -Apr -15 2:05
PM
Matrix: GW
-WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP -MS
Antimony (Sb)
<1
ug/L
1
1
EPA 200.8
04/17/2015 13:01
DJSULL1
Arsenic (As)
<1
ug/L
1
1
EPA 200.8
04/17/2015 13:01
DJSULL1
Beryllium (Be)
<1
ug/L
1
1
EPA 200.8
04/17/2015 13:01
DJSULL1
Cadmium (Cd)
<1
ug/L
1
1
EPA 200.8
04/17/2015 13:01
DJSULL1
Chromium (Cr)
<1
ug/L
1
1
EPA 200.8
04/17/2015 13:01
DJSULL1
Cobalt (Co)
<1
ug/L
1
1
EPA 200.8
04/17/2015 13:01
DJSULL1
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
04/17/2015 13:01
DJSULL1
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/17/2015 13:01
DJSULL1
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
04/17/2015 13:01
DJSULL1
Nickel (Ni)
< 1
ug/L
1
1
EPA 200.8
04/17/2015 13:01
DJSULL1
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
04/17/2015 13:01
DJSULL1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/17/2015 13:01
DJSULL1
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/17/2015 13:01
DJSULL1
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:25
JAHERMA
Arsenic (As)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:25
JAHERMA
Beryllium (Be)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:25
JAHERMA
Cadmium (Cd)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:25
JAHERMA
Chromium (Cr)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:25
JAHERMA
Cobalt (Co)
1.01
ug/L
1
1
EPA 200.8
04/16/2015 12:25
JAHERMA
Copper (Cu)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:25
JAHERMA
Lead (Pb)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:25
JAHERMA
Molybdenum (Mo)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:25
JAHERMA
Nickel (Ni)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:25
JAHERMA
Selenium (Se)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:25
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/16/2015 12:25
JAHERMA
Vanadium (V) Low Level
0.333
ug/L
0.3
1
EPA 200.8
04/16/2015 12:25
JAHERMA
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
310
mg/L
25
1
SM2540C
04/08/201514:41
AGIBBS5
Total Carbon
TOC
2.7
mg/L
0.1
1
SM5310C/EPA9060A
04/09/201514:12
GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS
110
mg/L
5
1
SM2540D
04/06/2015 08:47
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040071
Site: D-01
Collection Date: 01 -Apr -15 2:30 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 353.2
Vendor Parameter
Complete
50
EPA 300.0
NITRITE + NITRATE (COLORIMETRIC)
JAHERMA
50
Nitrite + Nitrate (Colorimetric)
0.029
mg-N/L
0.01
INORGANIC IONS BY IC
V_SHEALY
1
Chloride
93
mg/L
5
Sulfate
220
mg/L
5
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
MHALL3
Vendor Parameter
Complete
04/06/2015 12:37
MHALL3
DISSOLVED METALS BY ICP
EPA 200.7
04/06/2015 12:37
MHALL3
Aluminum (AI)
0.017
mg/L
0.005
Barium (Ba)
0.072
mg/L
0.005
Boron (B)
1.45
mg/L
0.05
Iron (Fe)
0.896
mg/L
0.01
Manganese (Mn)
1.46
mg/L
0.005
Strontium (Sr)
0.464
mg/L
0.005
Zinc (Zn)
0.011
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
04/07/2015 11:03
MHH7131
Calcium (Ca)
94.4
mg/L
0.01
Magnesium (Mg)
24.9
mg/L
0.005
Potassium (K)
3.34
mg/L
0.1
Sodium (Na)
28.0
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
EPA 200.7
04/07/2015 11:03
Aluminum (AI)
0.074
mg/L
0.005
Barium (Ba)
0.073
mg/L
0.005
Boron (B)
1.46
mg/L
0.05
Iron (Fe)
1.22
mg/L
0.01
Manganese (Mn)
1.50
mg/L
0.005
Strontium (Sr)
0.467
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Page 10 of 59
Sample #: 2015009466
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
04/07/2015 12:33
BGN9034
50
EPA 300.0
04/06/2015 17:43
JAHERMA
50
EPA 300.0
04/06/2015 17:43
JAHERMA
Vendor Method
V_SHEALY
1
EPA 200.7
04/06/2015 12:37
MHALL3
1
EPA 200.7
04/06/2015 12:37
MHALL3
1
EPA 200.7
04/06/2015 12:37
MHALL3
1
EPA 200.7
04/06/2015 12:37
MHALL3
1
EPA 200.7
04/06/2015 12:37
MHALL3
1
EPA 200.7
04/06/2015 12:37
MHALL3
1
EPA 200.7
04/06/2015 12:37
MHALL3
1
EPA 200.7
04/06/2015 13:43
MHALL3
1
EPA 200.7
04/06/2015 13:43
MHALL3
1
EPA 200.7
04/06/2015 13:43
MHALL3
1
EPA 200.7
04/06/2015 13:43
MHALL3
1
EPA 200.7
04/07/2015 11:03
MHH7131
1
EPA 200.7
04/07/2015 11:03
MHH7131
1
EPA 200.7
04/07/2015 11:03
MHH7131
1
EPA 200.7
04/07/2015 11:03
MHH7131
1
EPA 200.7
04/07/2015 11:03
MHH7131
1
EPA 200.7
04/07/2015 11:03
MHH7131
1
EPA 200.7
04/07/2015 11:03
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040071
Site: D-01
Collection Date: 01 -Apr -15 2:30 PM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.51
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.72
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
570
Total Carbon
04/17/2015 13:06
TOC
1.2
TOTAL SUSPENDED SOLIDS
1
TSS
7.0
Page 11 of 59
ug/L
1
1
Sample #:
2015009466
JAHERMA
ug/L
1
1
Matrix:
GW -WW
JAHERMA
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
04/17/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:06
DJSULL1
ug/L
0.2
1
EPA 200.8
04/17/2015 13:06
DJSULL1
ug/L
0.3
1
EPA 200.8
04/17/2015 13:06
DJSULL1
ug/L
1
1
EPA 200.8
04/16/2015 12:30
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:30
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:30
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:30
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:30
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:30
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:30
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:30
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:30
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:30
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:30
JAHERMA
ug/L
0.2
1
EPA 200.8
04/16/2015 12:30
JAHERMA
ug/L
0.3
1
EPA 200.8
04/16/2015 12:30
JAHERMA
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
04/08/201514:41 AGIBBS5
mg/L
0.1 1 SM5310C/EPA9060A
04/09/201514:12 GHUTCHI
mg/L
5 1 SM2540D
04/06/2015 08:47 AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040071
Site: C-01
Collection Date: 01 -Apr -15 2:52 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 353.2
Vendor Parameter
Complete
50
EPA 300.0
NITRITE + NITRATE (COLORIMETRIC)
JAHERMA
50
Nitrite + Nitrate (Colorimetric)
0.194
mg-N/L
0.01
INORGANIC IONS BY IC
V_SHEALY
1
Chloride
120
mg/L
5
Sulfate
360
mg/L
5
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
MHALL3
Vendor Parameter
Complete
04/06/2015 12:57
MHALL3
DISSOLVED METALS BY ICP
EPA 200.7
04/06/2015 12:57
MHALL3
Aluminum (AI)
0.011
mg/L
0.005
Barium (Ba)
0.046
mg/L
0.005
Boron (B)
1.75
mg/L
0.05
Iron (Fe)
0.292
mg/L
0.01
Manganese (Mn)
7.06
mg/L
0.005
Strontium (Sr)
1.82
mg/L
0.005
Zinc (Zn)
0.006
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
04/07/2015 11:07
MHH7131
Calcium (Ca)
158
mg/L
0.1
Magnesium (Mg)
39.8
mg/L
0.005
Potassium (K)
7.37
mg/L
0.1
Sodium (Na)
24.0
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
EPA 200.7
04/07/2015 11:07
Aluminum (AI)
0.735
mg/L
0.005
Barium (Ba)
0.048
mg/L
0.005
Boron (B)
1.73
mg/L
0.05
Iron (Fe)
1.36
mg/L
0.01
Manganese (Mn)
7.21
mg/L
0.005
Strontium (Sr)
1.90
mg/L
0.005
Zinc (Zn)
0.009
mg/L
0.005
Page 12 of 59
Sample #: 2015009467
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
04/07/2015 12:43
BGN9034
50
EPA 300.0
04/06/2015 18:01
JAHERMA
50
EPA 300.0
04/06/2015 18:01
JAHERMA
Vendor Method
V_SHEALY
1
EPA 200.7
04/06/2015 12:57
MHALL3
1
EPA 200.7
04/06/2015 12:57
MHALL3
1
EPA 200.7
04/06/2015 12:57
MHALL3
1
EPA 200.7
04/06/2015 12:57
MHALL3
1
EPA 200.7
04/06/2015 12:57
MHALL3
1
EPA 200.7
04/06/2015 12:57
MHALL3
1
EPA 200.7
04/06/2015 12:57
MHALL3
10
EPA 200.7
04/06/2015 13:47
MHALL3
1
EPA 200.7
04/06/2015 13:47
MHALL3
1
EPA 200.7
04/06/2015 13:47
MHALL3
1
EPA 200.7
04/06/2015 13:47
MHALL3
1
EPA 200.7
04/07/2015 11:07
MHH7131
1
EPA 200.7
04/07/2015 11:07
MHH7131
1
EPA 200.7
04/07/2015 11:07
MHH7131
1
EPA 200.7
04/07/2015 11:07
MHH7131
1
EPA 200.7
04/07/2015 11:07
MHH7131
1
EPA 200.7
04/07/2015 11:07
MHH7131
1
EPA 200.7
04/07/2015 11:07
MHH7131

Certificate of Laboratory Analysis Page 13 of 59
This report shall not be reproduced, except in full.
Order # J15040071
Site: C-01
Sample #: 2015009467
Collection Date: 01 -Apr -15 2:52
PM
Matrix: GW
-WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP -MS
Antimony (Sb)
<1
ug/L
1
1
EPA 200.8
04/17/2015 13:11
DJSULL1
Arsenic (As)
<1
ug/L
1
1
EPA 200.8
04/17/2015 13:11
DJSULL1
Beryllium (Be)
<1
ug/L
1
1
EPA 200.8
04/17/2015 13:11
DJSULL1
Cadmium (Cd)
<1
ug/L
1
1
EPA 200.8
04/17/2015 13:11
DJSULL1
Chromium (Cr)
<1
ug/L
1
1
EPA 200.8
04/17/2015 13:11
DJSULL1
Cobalt (Co)
16.0
ug/L
1
1
EPA 200.8
04/17/2015 13:11
DJSULL1
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
04/17/2015 13:11
DJSULL1
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
04/17/2015 13:11
DJSULL1
Molybdenum (Mo)
109
ug/L
1
1
EPA 200.8
04/17/2015 13:11
DJSULL1
Nickel (Ni)
10.0
ug/L
1
1
EPA 200.8
04/17/2015 13:11
DJSULL1
Selenium (Se)
2.46
ug/L
1
1
EPA 200.8
04/17/2015 13:11
DJSULL1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/17/2015 13:11
DJSULL1
Vanadium (V) Low Level
< 0.3
ug/L
0.3
1
EPA 200.8
04/17/2015 13:11
DJSULL1
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:35
JAHERMA
Arsenic (As)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:35
JAHERMA
Beryllium (Be)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:35
JAHERMA
Cadmium (Cd)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:35
JAHERMA
Chromium (Cr)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:35
JAHERMA
Cobalt (Co)
16.9
ug/L
1
1
EPA 200.8
04/16/2015 12:35
JAHERMA
Copper (Cu)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:35
JAHERMA
Lead (Pb)
<1
ug/L
1
1
EPA 200.8
04/16/2015 12:35
JAHERMA
Molybdenum (Mo)
115
ug/L
1
1
EPA 200.8
04/16/2015 12:35
JAHERMA
Nickel (Ni)
10.7
ug/L
1
1
EPA 200.8
04/16/2015 12:35
JAHERMA
Selenium (Se)
2.64
ug/L
1
1
EPA 200.8
04/16/2015 12:35
JAHERMA
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
04/16/2015 12:35
JAHERMA
Vanadium (V) Low Level
1.08
ug/L
0.3
1
EPA 200.8
04/16/2015 12:35
JAHERMA
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
880
mg/L
25
1
SM2540C
04/08/201514:41
AGIBBS5
Total Carbon
TOC
0.800
mg/L
0.1
1
SM5310C/EPA9060A
04/09/201514:12
GHUTCHI
TOTAL SUSPENDED SOLIDS
TSS
13
mg/L
5
1
SM2540D
04/06/2015 08:47
AGIBBS5

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040071
Site: B-01
Collection Date: 01 -Apr -15 3:29 PM
Analyte
Result
Units Qualifiers
RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 353.2
Vendor Parameter
Complete
100
EPA 300.0
NITRITE + NITRATE (COLORIMETRIC)
JAHERMA
100
Nitrite + Nitrate (Colorimetric)
0.124
mg-N/L
0.01
INORGANIC IONS BY IC
V_SHEALY
1
Chloride
510
mg/L
10
Sulfate
260
mg/L
10
MERCURY IN WATER - (Analysis Performed by
Shealy Labs)
MHALL3
Vendor Parameter
Complete
04/06/2015 12:45
MHALL3
DISSOLVED METALS BY ICP
EPA 200.7
04/06/2015 12:45
MHALL3
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
0.115
mg/L
0.005
Boron (B)
4.01
mg/L
0.05
Iron (Fe)
0.031
mg/L
0.01
Manganese (Mn)
0.054
mg/L
0.005
Strontium (Sr)
2.25
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
04/07/2015 11:11
MHH7131
Calcium (Ca)
296
mg/L
0.5
Magnesium (Mg)
60.6
mg/L
0.005
Potassium (K)
6.49
mg/L
0.1
Sodium (Na)
14.9
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
EPA 200.7
04/07/2015 11:11
Aluminum (AI)
0.468
mg/L
0.005
Barium (Ba)
0.119
mg/L
0.005
Boron (B)
4.20
mg/L
0.05
Iron (Fe)
0.879
mg/L
0.01
Manganese (Mn)
0.092
mg/L
0.005
Strontium (Sr)
2.32
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Page 14 of 59
Sample #: 2015009468
Matrix: GW -WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
04/07/2015 12:46
BGN9034
100
EPA 300.0
04/07/2015 08:31
JAHERMA
100
EPA 300.0
04/07/2015 08:31
JAHERMA
Vendor Method
V_SHEALY
1
EPA 200.7
04/06/2015 12:45
MHALL3
1
EPA 200.7
04/06/2015 12:45
MHALL3
1
EPA 200.7
04/06/2015 12:45
MHALL3
1
EPA 200.7
04/06/2015 12:45
MHALL3
1
EPA 200.7
04/06/2015 12:45
MHALL3
1
EPA 200.7
04/06/2015 12:45
MHALL3
1
EPA 200.7
04/06/2015 12:45
MHALL3
50
EPA 200.7
04/06/2015 13:51
MHALL3
1
EPA 200.7
04/06/2015 13:51
MHALL3
1
EPA 200.7
04/06/2015 13:51
MHALL3
1
EPA 200.7
04/06/2015 13:51
MHALL3
1
EPA 200.7
04/07/2015 11:11
MHH7131
1
EPA 200.7
04/07/2015 11:11
MHH7131
1
EPA 200.7
04/07/2015 11:11
MHH7131
1
EPA 200.7
04/07/2015 11:11
MHH7131
1
EPA 200.7
04/07/2015 11:11
MHH7131
1
EPA 200.7
04/07/2015 11:11
MHH7131
1
EPA 200.7
04/07/2015 11:11
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15040071
Site: B-01
Collection Date: 01 -Apr -15 3:29 PM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
2.03
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
2.58
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.804
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
2200
Total Carbon
04/17/2015 13:15
TOC
1.1
TOTAL SUSPENDED SOLIDS
1
TSS
21
Page 15 of 59
ug/L
1
1
Sample #:
2015009468
JAHERMA
ug/L
1
1
Matrix:
GW -WW
JAHERMA
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
04/17/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/17/2015 13:15
DJSULL1
ug/L
0.2
1
EPA 200.8
04/17/2015 13:15
DJSULL1
ug/L
0.3
1
EPA 200.8
04/17/2015 13:15
DJSULL1
ug/L
1
1
EPA 200.8
04/16/2015 12:39
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:39
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:39
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:39
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:39
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:39
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:39
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:39
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:39
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:39
JAHERMA
ug/L
1
1
EPA 200.8
04/16/2015 12:39
JAHERMA
ug/L
0.2
1
EPA 200.8
04/16/2015 12:39
JAHERMA
ug/L
0.3
1
EPA 200.8
04/16/2015 12:39
JAHERMA
Vendor Method V SHEALY
Vendor Method
V_ELE1
mg/L
25 1 SM2540C
04/08/201514:41 AGIBBS5
mg/L
0.1 1 SM5310C/EPA9060A
04/09/201514:12 GHUTCHI
mg/L
5 1 SM2540D
04/06/2015 08:47 AGIBBS5

Certificate of Laboratory Analysis Page 16 of 59
This report shall not be reproduced, except in full.
Order # J15040071
Site: TRIP BLANK
Collection Date:
Analyte Result Units Qualifiers RDL DF
MERCURY IN WATER - (Analysis Performed by Shealy Labs)
Vendor Parameter Complete
Sample #: 2015009469
Matrix: GW WW
Method Analysis Date/Time Analyst
Vendor Method V_SHEALY

1
Page 17 of 59
Element One lnc.
6319-D Carolina Beach Rel.
Wllrnington, YAC 28412
Phone: [phone]
Fax: [phone]
el lab@ el labcorn
e�emv,e%ntOne
REPORT OF ANALYSES
Duke Energy April 8, 2015
Laboratory Services Client Project Name AB GW Assessment Water— Asheville
13339 Hagers Ferry Road Bld. MG03A Client Project Number J15040071
Huntersville, NC 28078 PO Number
Sample Matrix
GW WW
Sample Type
Grab
Date Received
04/07/2015
Date Analyzed
04/07/2015
Method
SM 4500 S2- D
Time Received
1040
Delivered by
FedEx
Received by
JRC
eOne ID
Duke Energy ID
Parameter
Result
Unit
Dil
DL Date
Time
Sampled
Sampled
24438-1
F-01
Sulfide
< 0.1
mg/L
1
0.1 04/01/15
1152
24438-2
F-02
Sulfide
< 0.1
mg/L
1
0.1 04/01/15
1117
24438-3
E-01
Sulfide
< 0.1
mg/L
1
0.1 04/01/15
1405
24438-4
D-01
Sulfide
< 0.1
mg/L
1
0.1 04/01/15
1430
24438-5*
C-01
Sulfide
< 0.2
mg/L
2
0.1 04/01/15
1452
24438-6
B-01
Sulfide
< 0.1
mg/L
1
0.1 04/01/15
1529
*Sample spike recovery outside of QA limits of 85-115% with 81 % at a two -fold dilution; analyzed at a five -fold dilution resulting
in 94% recovery.
Ken S th, Laboratory Director
24438 Duke Report Packet Compiled by
NC Certifications: DW 37788 and DWQ DENR 604

W
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Page 18 of 59
L�
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elementOne SAMPLE SUBMISSION FORM Lab I'De 124438
TAT 7 BD Analysis Due Date 04.07.15
Hold Time Expiration 04.08.15 @ 1117 AM Report Due Date 04.15.15
Client: Duke Energy Date Rec: 04.07.15
LIMS No J15040071 Time Rec: 1040
Project ID AB GW Assessment Water - Asheville Rec By JRC
H >9 'des No Tem <_ 6°C Yes No Ref. Method:
If No, Record If No, Record SM4500 S2 D
Samole Identification & Collection Information
Lab ID
I Client ID
Collection Date
Collection Time
Analysis Requested
1
F-01
04.01.15
1152 AM
ulfi
2
F-02
04.01.15
1117 AM
u
3
E-01
04.01.15
1405 PM
u '
4
D-01
_
04.01.15
_
1430 PM
Sul i
5
C-01
04.01.15
1452 PM
u i
6
B-01
04.01.15
1529 PM
_
ulfi
The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
NOTE for Sulfide at 100 pg/L spike the sample to render the final spike concentration at - 500 pg/L
All AB Groundwater Assessment jobs need a RL of 0.1
Lab Communications
SS Page 1 of 1 Prep By / Date _K4,AN L+` 7 ` l 5
SS by Labeled By/ Date �4"r— ��- S
4/7/2015 :06:29 PM ID Verification By / ate (4i-- L-(•?- l

Page 20 of 59
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
Na2S•9H2O Lot #
40721
UNITS OF ANSWER
ug/mL
DETECTION LIMIT u
1.000
CLIENT:
Lab ID#
DUKE
24437 / 24438
SPK LEVELLuca
MAX ALIQUOT
5
10.00
Date:
4/7/15
STANDARD conc(ppm)
X
Time Analysis Begun
14:00
Cal Std Lot:
10
Time Analysis Ended
17:20
QC Std Lot:
Analyst:
KAM
STD ABSORPTION
Y
X Y
ug STD STD
SOLUTION ABS
0.00 0.000
1.00 0.088
2.50 0.209
5.00 0.388
7.50 0.564
10.00 0.799
SAMPLE SAMP
I.D. ABS
0900
0800
010°
°° os °°
°^°°
°,°°
° °°°
000
ug PER
ALIQUOT
200
ALI in mL
ANALYZED
A00
PREP
VOL in mL
000
x
Sloe
ALI in mL
TAKEN
B00
0.077747253
RESULTS
ug/mL
10.00
Correlation
LESS THAN
% SPK REC
. 7.
soo
1200
0.998877848
SPIKE
LEVEL
LRB
0.00
0.0000
10
10
10
<
0
LRB SPK
0.406
5.1643
10
10
10
0.516
104%
5.0
QC
0.367
4.6632
10
10
10
0.466
93%
5.0
24437-1
0.007
0.0371
10
10
10
< 0.1
24437-1 s k
0.379
4.8174
10
10
10
0.482
96%
5.0
24437-2
0.002
-0.0272
10
10
10
< 0.1
24437-2 dup
0.002
-0.0272
10
10
10
< 0.1
24437-2 s k
0.402
5.1129
10
10
10
0.511
102%
5.0
24438-1
0.008
0.0499
10
10
10
< 0.1
24438-1 s k
0.363
4.6118
10
10
10
0.461
92%
5.0
24438-2
0.002
-0.0272
10
10
10
< 0.1
24438-2 s k
0.454
5.7811
10
10
10
0.578
116%
5.0
24438-3
0.007
0.0371
10
10
10
< 0.1
24438-3 s k
0.357
4.5347
10
10
10
0.453
91%
5.0
24438-4
0.004
-0.0015
10
10
10
< 0.1
24438-4 s k
0.335
4.2519
10
10
10
0.425
85%
5.0
24438-5
0.006
0.0242
10
10
10
<
24438-5 s k
0.232
2.9284
10
10
10
0.293
59%
5.0
24438-6
0.004
-0.0015
10
10
10
< 0.1
24438-6 s k
0.347
4.4062
10
10
10
0.441
88%
5.0
24438-5
0.003
-0.0143
10
10
2
<
24438-5 s k
0.369
4.6889
10
10
2
2.344
94%
5.0
24438-5
0.007
0.0371
10
10
5
< 0.2
24438-5 s k
0.32
4.0592
10
10
5
0.812
81%
5.0
1000 ppm Std QC
0.618
7.8886
10
10
10
0.789
99%
8.0
Blank
0 1
0.0000
10
10
10
<
QC 0.362 1 4.5989
Submitted for QA/QC- Date: 04/07/15
10
10
By: (Print)
10
0.460 92%
K:AM (sign):
5.0
mv-

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water - Asheville
Project Number:J15040071
Lot Number:QD07013
Date Completed:04/16/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
* QD0701 3*
Shealy Environmental Services, Inc. Page: 1 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QD07013
Project Name: AB GW Assessment Water - Asheville
Project Number: J15040071
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QD07013
Project Name: AB GW Assessment Water - Asheville
Project Number: J15040071
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
2015009463
Aqueous
04/01/20151152
04/07/2015
002
2015009464
Aqueous
04/01/20151117
04/07/2015
003
2015009465
Aqueous
04/01/20151405
04/07/2015
004
2015009466
Aqueous
04/01/20151430
04/07/2015
005
2015009467
Aqueous
04/01/20151452
04/07/2015
006
2015009468
Aqueous
04/01/20151529
04/07/2015
007
2015009469
Aqueous
04/01/2015
04/07/2015
(7 samples)
Shealy Environmental Services, Inc. Page: 3 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

(16 detections)
Shealy Environmental Services, Inc. Page: 4 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QD07013
Project Name:
AB GW Assessment Water - Asheville
Project Number: J15040071
Sample Sample ID
Matrix
Parameter Method Result Q
Units
Page
001
2015009463
Aqueous
Mercury (CVAFS) 1631E
1.69
ng/L
7
002
2015009464
Aqueous
Alkalinity SM 2320B-
13
mg/L
8
002
2015009464
Aqueous
Bicarbonate Alkalinity SM 2320B-
13
mg/L
8
002
2015009464
Aqueous
Mercury (CVAFS) 1631E
0.623
ng/L
10
003
2015009465
Aqueous
Alkalinity SM 2320B-
25
mg/L
11
003
2015009465
Aqueous
Bicarbonate Alkalinity SM 2320B-
25
mg/L
11
003
2015009465
Aqueous
Methane RSK - 175
12
ug/L
12
003
2015009465
Aqueous
Mercury (CVAFS) 1631E
3.62
ng/L
13
004
2015009466
Aqueous
Alkalinity SM 2320B-
54
mg/L
14
004
2015009466
Aqueous
Bicarbonate Alkalinity SM 2320B-
54
mg/L
14
005
2015009467
Aqueous
Alkalinity SM 2320B-
76
mg/L
17
005
2015009467
Aqueous
Bicarbonate Alkalinity SM 2320B-
76
mg/L
17
005
2015009467
Aqueous
Mercury (CVAFS) 1631E
1.04
ng/L
19
006
2015009468
Aqueous
Alkalinity SM 2320B-
36
mg/L
20
006
2015009468
Aqueous
Bicarbonate Alkalinity SM 2320B-
36
mg/L
20
006
2015009468
Aqueous
Mercury (CVAFS) 1631E
10.4
ng/L
22
(16 detections)
Shealy Environmental Services, Inc. Page: 4 of 23
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QD07013-001
Description: 2015009463 Matrix: Aqueous
Date Sampled:04/01/2015 1152 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/09/2015 1229
HMA 72090
1
(Bicarbonate ) SM 2320B-2011
1 04/09/2015 1229
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/09/2015 1229
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 23
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Methane
Client: Duke Energy Laboratory ID: QD07013-001
Description: 2015009463 Matrix: Aqueous
Date Sampled:04/01/2015 1152 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/09/2015 1641 DCS 72229
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 23
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Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QD07013-001
Description: 2015009463 Matrix: Aqueous
Date Sampled:04/01/2015 1152 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 04/10/2015 1520 COH 04/08/2015 1131 72067
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 1.69 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QD07013-002
Description: 2015009464 Matrix: Aqueous
Date Sampled:04/01/2015 1117 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/09/2015 1235
HMA 72090
1
(Bicarbonate ) SM 2320B-2011
1 04/09/2015 1235
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/09/2015 1235
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
13
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
13
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QD07013-002
Description: 2015009464 Matrix: Aqueous
Date Sampled:04/01/2015 1117 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/10/2015 1006 DCS 72301
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QD07013-002
Description: 2015009464 Matrix: Aqueous
Date Sampled:04/01/2015 1117 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 04/10/2015 1534 COH 04/08/2015 1131 72067
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 0.623 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QD07013-003
Description: 2015009465 Matrix: Aqueous
Date Sampled:04/01/2015 1405 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/09/2015 1242
HMA 72090
1
(Bicarbonate ) SM 2320B-2011
1 04/09/2015 1242
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/09/2015 1242
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
25
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
25
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QD07013-003
Description: 2015009465 Matrix: Aqueous
Date Sampled:04/01/2015 1405 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/10/2015 1020 DCS 72301
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 12 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 12 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QD07013-003
Description: 2015009465 Matrix: Aqueous
Date Sampled:04/01/2015 1405 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 04/10/2015 1538 COH 04/08/2015 1131 72067
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 3.62 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 13 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QD07013-004
Description: 2015009466 Matrix: Aqueous
Date Sampled:04/01/2015 1430 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/09/2015 1300
HMA 72090
1
(Bicarbonate ) SM 2320B-2011
1 04/09/2015 1300
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/09/2015 1300
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 14 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
54
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
54
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 14 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QD07013-004
Description: 2015009466 Matrix: Aqueous
Date Sampled:04/01/2015 1430 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/10/2015 1030 DCS 72301
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 15 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QD07013-004
Description: 2015009466 Matrix: Aqueous
Date Sampled:04/01/2015 1430 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 04/10/2015 1543 COH 04/08/2015 1131 72067
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631 E ND 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 16 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QD07013-005
Description: 2015009467 Matrix: Aqueous
Date Sampled:04/01/2015 1452 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/09/2015 1307
HMA 72090
1
(Bicarbonate ) SM 2320B-2011
1 04/09/2015 1307
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/09/2015 1307
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 17 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
76
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
76
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 17 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QD07013-005
Description: 2015009467 Matrix: Aqueous
Date Sampled:04/01/2015 1452 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/10/2015 1051 DCS 72301
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 18 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QD07013-005
Description: 2015009467 Matrix: Aqueous
Date Sampled:04/01/2015 1452 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 04/10/2015 1548 COH 04/08/2015 1131 72067
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 1.04 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 19 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QD07013-006
Description: 2015009468 Matrix: Aqueous
Date Sampled:04/01/2015 1529 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 04/09/2015 1313
HMA 72090
1
(Bicarbonate ) SM 2320B-2011
1 04/09/2015 1313
HMA
1
(Carbonate Al) SM 2320B-2011
1 04/09/2015 1313
HMA
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 20 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
36
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
36
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 20 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QD07013-006
Description: 2015009468 Matrix: Aqueous
Date Sampled:04/01/2015 1529 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 04/10/2015 1105 DCS 72301
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 21 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QD07013-006
Description: 2015009468 Matrix: Aqueous
Date Sampled:04/01/2015 1529 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 10 04/10/2015 1911 COH 04/08/2015 1131 72067
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631E 10.4 5.00 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 22 of 23
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS)
Client: Duke Energy Laboratory ID: QD07013-007
Description: 2015009469 Matrix: Aqueous
Date Sampled:04/01/2015 Project Name: AB GW Assessment Water -
Date Received: 04/07/2015 Project Number: J15040071
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 1631 E 1 04/10/2015 1916 COH 04/08/2015 1131 72067
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Mercury (CVAFS) 7439-97-6 1631 E ND 0.500 ng/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QD07013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - Ii
Sample ID: QQ72090-001 Matrix: Aqueous
Batch: 72090
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 04/09/20151141
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD07013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ72090-002 Matrix: Aqueous
Batch: 72090
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 96 1 96 90-110 04/09/20151147
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD07013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ72229-001 Matrix: Aqueous
Batch: 72229
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 04/09/2015 0934
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD07013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ72229-002 Matrix: Aqueous
Batch: 72229
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 150 1 97 70-130 04/09/2015 0913
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD07013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ72229-003 Matrix: Aqueous
Batch: 72229
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 150 1 99 2.2 70-130 30 04/09/2015 0923
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD07013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ72301-001 Matrix: Aqueous
Batch: 72301
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 04/10/2015 0943
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD07013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ72301-002 Matrix: Aqueous
Batch: 72301
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 140 1 90 70-130 04/10/2015 0919
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD07013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ72301-003 Matrix: Aqueous
Batch: 72301
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 140 1 95 5.1 70-130 30 04/10/2015 0929
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD07013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS) - MB
Sample ID: QQ72067-001 Matrix: Aqueous
Batch: 72067 Prep Method: 1631E
Analytical Method: 1631E Prep Date: 04/08/2015 1131
Parameter Result Q Dil PQL Units Analysis Date
Mercury (CVAFS) ND 1 0.500 ng/L 04/10/2015 1424
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD07013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS) - LCS
Sample ID: QQ72067-002 Matrix: Aqueous
Batch: 72067 Prep Method: 1631E
Analytical Method: 1631E Prep Date: 04/08/2015 1131
Spike
Amount Result % Rec
Parameter (ng/L) (ng/L) Q Dil % Rec Limit Analysis Date
Mercury (CVAFS) 5.00 4.92 1 98 75-125 04/10/2015 1428
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD07013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS) - MS
Sample ID: QD07013-001 MS
Matrix: Aqueous
Batch: 72067
Prep Method: 1631E
Analytical Method: 1631E
Prep Date: 04/08/2015 1131
Sample
Spike
Amount
Amount
Result % Rec
Parameter
(ng/L)
(ng/L)
(ng/L) Q Dil % Rec Limit Analysis Date
Mercury (CVAFS)
1.69
5.00
5.86 1 83 71-125 04/10/2015 1524
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD07013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Mercury (CVAFS) - MSD
Sample ID: QD07013-001MD
Matrix: Aqueous
Batch: 72067
Prep Method: 1631E
Analytical Method: 1631E
Prep Date: 04/08/2015 1131
Sample
Spike
Amount
Amount
Result % Rec % RPD
Parameter
(ng/L)
(ng/L)
(ng/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Mercury (CVAFS)
1.69
5.00
5.7 1 80 2.8 71-125 24 04/10/2015 1529
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QD07013
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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Page 59 of 59
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