NC0000396_J15030137report_20150823

DUKE Analytical Laboratory
ENERGY
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Order Number: J15030137
Project Name: AB GW ASSESSMENT WATER
Customer Name(s): Todd Plating, Kathy Webb, John Toepfer, Tim Hunsucker
Customer Address: 200 CP and L Drive
Arden,NC 28704
Lab Contact: Mary Ann Ogle Phone: [phone]
Mary Ann Ogle
Report Authorized By: 2015.04.06 14:22:43 Date:
(Signature) -04'00'
Mary Ann Ogle
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
4/2/2015
Page 1 of 58
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
Collected By
Sample Description
2015006202
ASHEVILLE
03 -Mar -15 9:15 AM
Synterra
MW-13BR
2015006210
ASHEVILLE
03 -Mar -15 9:15 AM
Synterra
MW-13BR Dup
2015006211
ASHEVILLE
03 -Mar -15 1:45 PM
Synterra
MW -17
2015006212
ASHEVILLE
04 -Mar -15 8:55 AM
Synterra
MW -15
2015006213
ASHEVILLE
04 -Mar -15 10:10 AM
Synterra
MW -15D
2015006214
ASHEVILLE
03 -Mar -15 11:30 AM
Synterra
Equipment Blank
2015006215
ASHEVILLE
03 -Mar -15 11:30 AM
Synterra
Filter Blank
2015006216
ASHEVILLE
04 -Mar -15 1:10 PM
Synterra
Equipment Blank
2015006217
ASHEVILLE
04 -Mar -15 1:10 PM
Synterra
Filter Blank
9 Total Samples
Page 2 of 58

Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals Yes No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes No
All laboratory QA/QC requirements are acceptable. (] Yes ❑ No
Report Sections Included:
LU Job Summary Report
❑ Sample Identification
P/1 Technical Validation of Data Package
J❑ Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
Page 3 of 58
LVI Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
d❑ Chain of Custody
LVI Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: DBA Account Date: 4/2/2015

Certificate of Laboratory Analysis Page 4 of 58
This report shall not be reproduced, except in full.
Order # J15030137
Site: MW-13BR
Collection Date: 03 -Mar -15 9:15 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
BGN9034
1 EPA 300.0
Vendor Parameter
Complete
1 EPA 245.1
03/10/2015 12:50
NITRITE + NITRATE (COLORIMETRIC)
1 EPA 245.1
03/12/2015 15:17
Nitrite + Nitrate (Colorimetric)
0.244
mg-N/L
0.01
INORGANIC IONS BY IC
03/11/2015 10:26
MHH7131
1 EPA 200.7
Chloride
4.6
mg/L
0.1
Sulfate
2.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
03/11/2015 10:26
MHH7131
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
MHALL3
1 EPA 200.7
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
1 EPA 200.7
03/17/2015 11:20
MHALL3
Aluminum (AI)
0.012
mg/L
0.005
Barium (Ba)
0.026
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.144
mg/L
0.01
Manganese (Mn)
0.250
mg/L
0.005
Strontium (Sr)
0.028
mg/L
0.005
Zinc (Zn)
0.009
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
10.3
mg/L
0.01
Magnesium (Mg)
2.24
mg/L
0.005
Potassium (K)
1.48
mg/L
0.1
Sodium (Na)
2.64
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.173
mg/L
0.005
Barium (Ba)
0.027
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.335
mg/L
0.01
Manganese (Mn)
0.268
mg/L
0.005
Strontium (Sr)
0.031
mg/L
0.005
Zinc (Zn)
0.009
mg/L
0.005
Sample #: 2015006202
Matrix: GW WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
03/09/2015 11:42
TLINN
1 EPA 300.0
03/09/2015 21:28
BGN9034
1 EPA 300.0
03/09/2015 21:28
BGN9034
1 EPA 245.1
03/10/2015 12:50
ACPAYNE
1 EPA 245.1
03/12/2015 15:17
ACPAYNE
1 EPA 200.7
03/11/2015 10:26
MHH7131
1 EPA 200.7
03/11/2015 10:26
MHH7131
1 EPA 200.7
03/11/2015 10:26
MHH7131
1 EPA 200.7
03/11/2015 10:26
MHH7131
1 EPA 200.7
03/11/2015 10:26
MHH7131
1 EPA 200.7
03/11/2015 10:26
MHH7131
1 EPA 200.7
03/11/2015 10:26
MHH7131
1 EPA 200.7
03/17/2015 11:20
MHALL3
1 EPA 200.7
03/17/2015 11:20
MHALL3
1 EPA 200.7
03/17/2015 11:20
MHALL3
1 EPA 200.7
03/17/2015 11:20
MHALL3
1 EPA 200.7
03/09/2015 09:45
MHH7131
1 EPA 200.7
03/09/2015 09:45
MHH7131
1 EPA 200.7
03/09/2015 09:45
MHH7131
1 EPA 200.7
03/09/2015 09:45
MHH7131
1 EPA 200.7
03/09/2015 09:45
MHH7131
1 EPA 200.7
03/09/2015 09:45
MHH7131
1 EPA 200.7
03/09/2015 09:45
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030137
Site: MW-13BR
Collection Date: 03 -Mar -15 9:15 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.68
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
1.05
Selenium (Se)
< 1
Thallium (TI) Low Level
0.211
Vanadium (V) Low Level
0.459
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.70
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
1.31
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.879
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
67
Total Carbon
03/24/2015 12:18
TOC
0.430
TOTAL SUSPENDED SOLIDS
1
TSS
7.0
Page 5 of 58
ug/L
1
1
Sample #:
2015006202
DJSULL1
ug/L
1
1
Matrix:
GW WW
DJSULL1
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
03/24/2015 12:18
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:18
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:18
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:18
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:18
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:18
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:18
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:18
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:18
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:18
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:18
DJSULL1
ug/L
0.2
1
EPA 200.8
03/24/2015 12:18
DJSULL1
ug/L
0.3
1
EPA 200.8
03/24/2015 12:18
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:06
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:06
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:06
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:06
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:06
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:06
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:06
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:06
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:06
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:06
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:06
DJSULL1
ug/L
0.2
1
EPA 200.8
03/12/2015 11:06
DJSULL1
ug/L
0.3
1
EPA 200.8
03/12/2015 11:06
DJSULL1
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
03/10/201512:15
GHUTCHI
mg/L
0.1
1
SM5310C/EPA9060A
03/10/201511:40
TJA7067
mg/L
5
1
SM2540D
03/06/201511:10
GHUTCHI

Certificate of Laboratory Analysis Page 6 of 58
This report shall not be reproduced, except in full.
Order # J15030137
Site: MW-13BR Dup
Collection Date: 03 -Mar -15 9:15 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
BGN9034
1 EPA 300.0
Vendor Parameter
Complete
1 EPA 245.1
03/10/2015 12:53
NITRITE + NITRATE (COLORIMETRIC)
1 EPA 245.1
03/12/2015 15:29
Nitrite + Nitrate (Colorimetric)
0.248
mg-N/L
0.01
INORGANIC IONS BY IC
03/11/2015 10:46
MHH7131
1 EPA 200.7
Chloride
4.6
mg/L
0.1
Sulfate
2.0
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
03/11/2015 10:46
MHH7131
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
MHALL3
1 EPA 200.7
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
1 EPA 200.7
03/17/2015 11:32
MHALL3
Aluminum (AI)
0.011
mg/L
0.005
Barium (Ba)
0.025
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.142
mg/L
0.01
Manganese (Mn)
0.249
mg/L
0.005
Strontium (Sr)
0.029
mg/L
0.005
Zinc (Zn)
0.010
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
10.5
mg/L
0.01
Magnesium (Mg)
2.25
mg/L
0.005
Potassium (K)
1.48
mg/L
0.1
Sodium (Na)
2.68
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.162
mg/L
0.005
Barium (Ba)
0.026
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.319
mg/L
0.01
Manganese (Mn)
0.269
mg/L
0.005
Strontium (Sr)
0.030
mg/L
0.005
Zinc (Zn)
0.009
mg/L
0.005
Sample #: 2015006210
Matrix: GW WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
03/09/2015 11:43
TLINN
1 EPA 300.0
03/09/2015 21:44
BGN9034
1 EPA 300.0
03/09/2015 21:44
BGN9034
1 EPA 245.1
03/10/2015 12:53
ACPAYNE
1 EPA 245.1
03/12/2015 15:29
ACPAYNE
1 EPA 200.7
03/11/2015 10:46
MHH7131
1 EPA 200.7
03/11/2015 10:46
MHH7131
1 EPA 200.7
03/11/2015 10:46
MHH7131
1 EPA 200.7
03/11/2015 10:46
MHH7131
1 EPA 200.7
03/11/2015 10:46
MHH7131
1 EPA 200.7
03/11/2015 10:46
MHH7131
1 EPA 200.7
03/11/2015 10:46
MHH7131
1 EPA 200.7
03/17/2015 11:32
MHALL3
1 EPA 200.7
03/17/2015 11:32
MHALL3
1 EPA 200.7
03/17/2015 11:32
MHALL3
1 EPA 200.7
03/17/2015 11:32
MHALL3
1 EPA 200.7
03/09/2015 09:49
MHH7131
1 EPA 200.7
03/09/2015 09:49
MHH7131
1 EPA 200.7
03/09/2015 09:49
MHH7131
1 EPA 200.7
03/09/2015 09:49
MHH7131
1 EPA 200.7
03/09/2015 09:49
MHH7131
1 EPA 200.7
03/09/2015 09:49
MHH7131
1 EPA 200.7
03/09/2015 09:49
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030137
Site: MW-13BR Dup
Collection Date: 03 -Mar -15 9:15 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.73
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
1.09
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.449
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.74
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
1.05
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.820
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
58
Total Carbon
03/24/2015 12:49
TOC
0.411
TOTAL SUSPENDED SOLIDS
1
TSS
< 5
Page 7 of 58
ug/L
1
1
Sample #:
2015006210
DJSULL1
ug/L
1
1
Matrix:
GW WW
DJSULL1
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
03/24/2015 12:49
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:49
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:49
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:49
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:49
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:49
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:49
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:49
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:49
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:49
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:49
DJSULL1
ug/L
0.2
1
EPA 200.8
03/24/2015 12:49
DJSULL1
ug/L
0.3
1
EPA 200.8
03/24/2015 12:49
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:12
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:12
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:12
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:12
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:12
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:12
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:12
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:12
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:12
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:12
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:12
DJSULL1
ug/L
0.2
1
EPA 200.8
03/12/2015 11:12
DJSULL1
ug/L
0.3
1
EPA 200.8
03/12/2015 11:12
DJSULL1
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
03/10/201512:15
GHUTCHI
mg/L
0.1
1
SM5310C/EPA9060A
03/10/201511:40
TJA7067
mg/L
5
1
SM2540D
03/06/201511:10
GHUTCHI

Certificate of Laboratory Analysis Page 8 of 58
This report shall not be reproduced, except in full.
Order # J15030137
Site: MW -17
Collection Date: 03 -Mar -15 1:45 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 300.0
03/10/2015 08:56
Vendor Parameter
Complete
EPA 300.0
03/10/2015 08:56
NITRITE + NITRATE (COLORIMETRIC)
1
EPA 245.1
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
ACPAYNE
1
EPA 200.7
Chloride
330
mg/L
5
Sulfate
140
mg/L
5
MERCURY (COLD VAPOR) IN WATER
MHH7131
5
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
03/11/2015 10:50
MHH7131
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
EPA 200.7
03/11/2015 10:50
MHH7131
Aluminum (AI)
0.058
mg/L
0.005
Barium (Ba)
0.139
mg/L
0.005
Boron (B)
1.24
mg/L
0.05
Iron (Fe)
23.0
mg/L
0.05
Manganese (Mn)
17.3
mg/L
0.005
Strontium (Sr)
0.569
mg/L
0.005
Zinc (Zn)
0.018
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
03/09/2015 09:53
MHH7131
Calcium (Ca)
132
mg/L
0.1
Magnesium (Mg)
39.8
mg/L
0.05
Potassium (K)
4.23
mg/L
0.1
Sodium (Na)
15.4
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.321
mg/L
0.005
Barium (Ba)
0.154
mg/L
0.005
Boron (B)
1.06
mg/L
0.05
Iron (Fe)
8.97
mg/L
0.01
Manganese (Mn)
12.8
mg/L
0.005
Strontium (Sr)
0.507
mg/L
0.005
Zinc (Zn)
0.019
mg/L
0.005
Sample #: 2015006211
Matrix: GW WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
03/09/2015 11:45
TLINN
50
EPA 300.0
03/10/2015 08:56
BGN9034
50
EPA 300.0
03/10/2015 08:56
BGN9034
1
EPA 245.1
03/10/2015 12:55
ACPAYNE
1
EPA 245.1
03/12/2015 15:36
ACPAYNE
1
EPA 200.7
03/11/2015 10:50
MHH7131
1
EPA 200.7
03/11/2015 10:50
MHH7131
1
EPA 200.7
03/11/2015 10:50
MHH7131
5
EPA 200.7
03/11/2015 10:50
MHH7131
1
EPA 200.7
03/11/2015 10:50
MHH7131
1
EPA 200.7
03/11/2015 10:50
MHH7131
1
EPA 200.7
03/11/2015 10:50
MHH7131
10
EPA 200.7
03/17/2015 11:36
MHALL3
10
EPA 200.7
03/17/2015 11:36
MHALL3
1
EPA 200.7
03/17/2015 11:36
MHALL3
1
EPA 200.7
03/17/2015 11:36
MHALL3
1
EPA 200.7
03/09/2015 09:53
MHH7131
1
EPA 200.7
03/09/2015 09:53
MHH7131
1
EPA 200.7
03/09/2015 09:53
MHH7131
1
EPA 200.7
03/09/2015 09:53
MHH7131
1
EPA 200.7
03/09/2015 09:53
MHH7131
1
EPA 200.7
03/09/2015 09:53
MHH7131
1
EPA 200.7
03/09/2015 09:53
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030137
Site: MW -17
Collection Date: 03 -Mar -15 1:45 PM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
1.08
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
28.2
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
4.06
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
26.3
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
5.16
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.401
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
1300
Total Carbon
03/24/2015 12:54
TOC
5.1
TOTAL SUSPENDED SOLIDS
1
TSS
19
Page 9 of 58
ug/L
1
1
Sample #:
2015006211
DJSULL1
ug/L
1
1
Matrix:
GW WW
DJSULL1
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
03/24/2015 12:54
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:54
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:54
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:54
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:54
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:54
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:54
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:54
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:54
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:54
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:54
DJSULL1
ug/L
0.2
1
EPA 200.8
03/24/2015 12:54
DJSULL1
ug/L
0.3
1
EPA 200.8
03/24/2015 12:54
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:17
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:17
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:17
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:17
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:17
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:17
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:17
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:17
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:17
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:17
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:17
DJSULL1
ug/L
0.2
1
EPA 200.8
03/12/2015 11:17
DJSULL1
ug/L
0.3
1
EPA 200.8
03/12/2015 11:17
DJSULL1
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
03/10/201512:15
GHUTCHI
mg/L
0.1
1
SM5310C/EPA9060A
03/10/201511:40
TJA7067
mg/L
5
1
SM2540D
03/06/201511:10
GHUTCHI

Certificate of Laboratory Analysis Page 10 of 58
This report shall not be reproduced, except in full.
Order # J15030137
Site: MW -15
Collection Date: 04 -Mar -15 8:55 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 300.0
03/09/2015 22:17
Vendor Parameter
Complete
EPA 300.0
03/09/2015 22:17
NITRITE + NITRATE (COLORIMETRIC)
1
EPA 245.1
Nitrite + Nitrate (Colorimetric)
0.125
mg-N/L
0.01
INORGANIC IONS BY IC
ACPAYNE
1
EPA 200.7
Chloride
43
mg/L
1
Sulfate
5.3
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
MHH7131
1
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
03/11/2015 10:54
MHH7131
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
EPA 200.7
03/11/2015 10:54
MHH7131
Aluminum (AI)
0.081
mg/L
0.005
Barium (Ba)
0.113
mg/L
0.005
Boron (B)
0.062
mg/L
0.05
Iron (Fe)
0.627
mg/L
0.01
Manganese (Mn)
1.08
mg/L
0.005
Strontium (Sr)
0.117
mg/L
0.005
Zinc (Zn)
0.009
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
03/09/2015 09:57
MHH7131
Calcium (Ca)
9.55
mg/L
0.01
Magnesium (Mg)
4.61
mg/L
0.005
Potassium (K)
1.11
mg/L
0.1
Sodium (Na)
14.8
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.165
mg/L
0.005
Barium (Ba)
0.117
mg/L
0.005
Boron (B)
0.061
mg/L
0.05
Iron (Fe)
0.879
mg/L
0.01
Manganese (Mn)
1.06
mg/L
0.005
Strontium (Sr)
0.120
mg/L
0.005
Zinc (Zn)
0.007
mg/L
0.005
Sample #: 2015006212
Matrix: GW WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
03/09/2015 11:46
TLINN
10
EPA 300.0
03/09/2015 22:17
BGN9034
1
EPA 300.0
03/09/2015 22:17
BGN9034
1
EPA 245.1
03/10/2015 12:58
ACPAYNE
1
EPA 245.1
03/12/2015 15:39
ACPAYNE
1
EPA 200.7
03/11/2015 10:54
MHH7131
1
EPA 200.7
03/11/2015 10:54
MHH7131
1
EPA 200.7
03/11/2015 10:54
MHH7131
1
EPA 200.7
03/11/2015 10:54
MHH7131
1
EPA 200.7
03/11/2015 10:54
MHH7131
1
EPA 200.7
03/11/2015 10:54
MHH7131
1
EPA 200.7
03/11/2015 10:54
MHH7131
1
EPA 200.7
03/17/2015 11:40
MHALL3
1
EPA 200.7
03/17/2015 11:40
MHALL3
1
EPA 200.7
03/17/2015 11:40
MHALL3
1
EPA 200.7
03/17/2015 11:40
MHALL3
1
EPA 200.7
03/09/2015 09:57
MHH7131
1
EPA 200.7
03/09/2015 09:57
MHH7131
1
EPA 200.7
03/09/2015 09:57
MHH7131
1
EPA 200.7
03/09/2015 09:57
MHH7131
1
EPA 200.7
03/09/2015 09:57
MHH7131
1
EPA 200.7
03/09/2015 09:57
MHH7131
1
EPA 200.7
03/09/2015 09:57
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030137
Site: MW -15
Collection Date: 04 -Mar -15 8:55 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.15
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
1.25
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
120
Total Carbon
03/24/2015 12:59
TOC
0.583
TOTAL SUSPENDED SOLIDS
1
TSS
< 5
Page 11 of 58
ug/L
1
1
Sample #:
2015006212
DJSULL1
ug/L
1
1
Matrix:
GW WW
DJSULL1
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
03/24/2015 12:59
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:59
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:59
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:59
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:59
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:59
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:59
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:59
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:59
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:59
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 12:59
DJSULL1
ug/L
0.2
1
EPA 200.8
03/24/2015 12:59
DJSULL1
ug/L
0.3
1
EPA 200.8
03/24/2015 12:59
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:22
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:22
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:22
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:22
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:22
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:22
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:22
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:22
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:22
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:22
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:22
DJSULL1
ug/L
0.2
1
EPA 200.8
03/12/2015 11:22
DJSULL1
ug/L
0.3
1
EPA 200.8
03/12/2015 11:22
DJSULL1
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
03/11/201511:36
GHUTCHI
mg/L
0.1
1
SM5310C/EPA9060A
03/10/201511:40
TJA7067
mg/L
5
1
SM2540D
03/06/201511:10
GHUTCHI

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030137
Site: MW -15D
Collection Date: 04 -Mar -15 10:10 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
BGN9034
1 EPA 300.0
Vendor Parameter
Complete
1 EPA 245.1
03/10/2015 13:00
NITRITE + NITRATE (COLORIMETRIC)
1 EPA 245.1
03/12/2015 15:41
Nitrite + Nitrate (Colorimetric)
0.666
mg-N/L
0.01
INORGANIC IONS BY IC
03/13/2015 10:53
MHALL3
1 EPA 200.7
Chloride
7.3
mg/L
0.1
Sulfate
0.67
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
03/13/2015 10:53
MHALL3
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
MHALL3
1 EPA 200.7
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
1 EPA 200.7
03/17/2015 11:44
MHALL3
Aluminum (AI)
0.005
mg/L
0.005
Barium (Ba)
0.062
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.012
mg/L
0.01
Manganese (Mn)
0.196
mg/L
0.005
Strontium (Sr)
0.112
mg/L
0.005
Zinc (Zn)
0.026
mg/L
0.005
UNDIGESTED METALS BY ICP
Calcium (Ca)
8.90
mg/L
0.01
Magnesium (Mg)
2.41
mg/L
0.005
Potassium (K)
2.89
mg/L
0.1
Sodium (Na)
6.94
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.134
mg/L
0.005
Barium (Ba)
0.062
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.202
mg/L
0.01
Manganese (Mn)
0.167
mg/L
0.005
Strontium (Sr)
0.108
mg/L
0.005
Zinc (Zn)
0.009
mg/L
0.005
Sample #: 2015006213
Matrix: GW WW
Page 12 of 58
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
03/09/2015 11:47
TLINN
1 EPA 300.0
03/09/2015 22:33
BGN9034
1 EPA 300.0
03/09/2015 22:33
BGN9034
1 EPA 245.1
03/10/2015 13:00
ACPAYNE
1 EPA 245.1
03/12/2015 15:41
ACPAYNE
1 EPA 200.7
03/13/2015 10:53
MHALL3
1 EPA 200.7
03/13/2015 10:53
MHALL3
1 EPA 200.7
03/13/2015 10:53
MHALL3
1 EPA 200.7
03/13/2015 10:53
MHALL3
1 EPA 200.7
03/13/2015 10:53
MHALL3
1 EPA 200.7
03/13/2015 10:53
MHALL3
1 EPA 200.7
03/13/2015 10:53
MHALL3
1 EPA 200.7
03/17/2015 11:44
MHALL3
1 EPA 200.7
03/17/2015 11:44
MHALL3
1 EPA 200.7
03/17/2015 11:44
MHALL3
1 EPA 200.7
03/17/2015 11:44
MHALL3
1 EPA 200.7
03/09/2015 10:01
MHH7131
1 EPA 200.7
03/09/2015 10:01
MHH7131
1 EPA 200.7
03/09/2015 10:01
MHH7131
1 EPA 200.7
03/09/2015 10:01
MHH7131
1 EPA 200.7
03/09/2015 10:01
MHH7131
1 EPA 200.7
03/09/2015 10:01
MHH7131
1 EPA 200.7
03/09/2015 10:01
MHH7131

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030137
Site: MW -15D
Collection Date: 04 -Mar -15 10:10 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
7.00
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
1.06
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.333
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
76
Total Carbon
03/24/2015 13:04
TOC
0.410
TOTAL SUSPENDED SOLIDS
1
TSS
< 5
Page 13 of 58
ug/L
1
1
Sample #:
2015006213
DJSULL1
ug/L
1
1
Matrix:
GW WW
DJSULL1
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
03/24/2015 13:04
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 13:04
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 13:04
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 13:04
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 13:04
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 13:04
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 13:04
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 13:04
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 13:04
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 13:04
DJSULL1
ug/L
1
1
EPA 200.8
03/24/2015 13:04
DJSULL1
ug/L
0.2
1
EPA 200.8
03/24/2015 13:04
DJSULL1
ug/L
0.3
1
EPA 200.8
03/24/2015 13:04
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:27
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:27
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:27
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:27
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:27
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:27
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:27
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:27
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:27
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:27
DJSULL1
ug/L
1
1
EPA 200.8
03/12/2015 11:27
DJSULL1
ug/L
0.2
1
EPA 200.8
03/12/2015 11:27
DJSULL1
ug/L
0.3
1
EPA 200.8
03/12/2015 11:27
DJSULL1
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
03/11/201511:36
GHUTCHI
mg/L
0.1
1
SM5310C/EPA9060A
03/10/201511:40
TJA7067
mg/L
5
1
SM2540D
03/06/201511:10
GHUTCHI

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030137
Site: Equipment Blank
Collection Date: 03 -Mar -15 11:30 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
1 EPA 300.0
Vendor Parameter
Complete
1 EPA 300.0
03/09/2015 10:16
NITRITE + NITRATE (COLORIMETRIC)
1 EPA 245.1
03/10/2015 13:02
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
03/17/2015 11:49
MHALL3
1 EPA 200.7
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
03/09/2015 10:05
MHH7131
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY ICP
MHH7131
1 EPA 200.7
03/09/2015 10:05
Calcium (Ca)
< 0.01
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
03/12/2015 10:56
DJSULL1
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Page 14 of 58
Sample #: 2015006214
Matrix: GW WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
03/09/2015 11:52
TLINN
1 EPA 300.0
03/09/2015 10:16
BGN9034
1 EPA 300.0
03/09/2015 10:16
BGN9034
1 EPA 245.1
03/10/2015 13:02
ACPAYNE
1 EPA 200.7
03/17/2015 11:49
MHALL3
1 EPA 200.7
03/17/2015 11:49
MHALL3
1 EPA 200.7
03/17/2015 11:49
MHALL3
1 EPA 200.7
03/17/2015 11:49
MHALL3
1 EPA 200.7
03/09/2015 10:05
MHH7131
1 EPA 200.7
03/09/2015 10:05
MHH7131
1 EPA 200.7
03/09/2015 10:05
MHH7131
1 EPA 200.7
03/09/2015 10:05
MHH7131
1 EPA 200.7
03/09/2015 10:05
MHH7131
1 EPA 200.7
03/09/2015 10:05
MHH7131
1 EPA 200.7
03/09/2015 10:05
MHH7131
1 EPA 200.8
03/12/2015 10:56
DJSULL1
1 EPA 200.8
03/12/2015 10:56
DJSULL1
1 EPA 200.8
03/12/2015 10:56
DJSULL1
1 EPA 200.8
03/12/2015 10:56
DJSULL1
1 EPA 200.8
03/12/2015 10:56
DJSULL1
1 EPA 200.8
03/12/2015 10:56
DJSULL1
1 EPA 200.8
03/12/2015 10:56
DJSULL1
1 EPA 200.8
03/12/2015 10:56
DJSULL1
1 EPA 200.8
03/12/2015 10:56
DJSULL1
1 EPA 200.8
03/12/2015 10:56
DJSULL1
1 EPA 200.8
03/12/2015 10:56
DJSULL1
1 EPA 200.8
03/12/2015 10:56
DJSULL1
1 EPA 200.8
03/12/2015 10:56
DJSULL1

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030137
Page 15 of 58
Site: Equipment Blank
Sample #: 2015006214
Collection Date: 03 -Mar -15 11:30
AM
Matrix: GW WW
Analyte
Result
Units Qualifiers
RDL
DF
Method Analysis Date/Time
Analyst
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
< 25
mg/L
25
1
SM2540C 03/10/2015 12:15
GHUTCHI
Total Carbon
TOC
0.143
mg/L
0.1
1
SM5310C/EPA9060A 03/10/201511:40
TJA7067
TOTAL SUSPENDED SOLIDS
TSS
< 5
mg/L
5
1
SM2540D 03/06/2015 11:10
GHUTCHI

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030137
Site: Filter Blank
Collection Date: 03 -Mar -15 11:30 AM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
EPA 245.1
03/12/2015 15:43
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
1
EPA 200.7
03/11/2015 10:58
Aluminum (Al)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
DISSOLVED METALS BY ICP -MS
1
EPA 200.8
03/24/2015 12:38
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015006215
Matrix: GW WW
Page 16 of 58
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
03/12/2015 15:43
ACPAYNE
1
EPA 200.7
03/11/2015 10:58
MHH7131
1
EPA 200.7
03/11/2015 10:58
MHH7131
1
EPA 200.7
03/11/2015 10:58
MHH7131
1
EPA 200.7
03/11/2015 10:58
MHH7131
1
EPA 200.7
03/11/2015 10:58
MHH7131
1
EPA 200.7
03/11/2015 10:58
MHH7131
1
EPA 200.7
03/11/2015 10:58
MHH7131
1
EPA 200.8
03/24/2015 12:38
DJSULL1
1
EPA 200.8
03/24/2015 12:38
DJSULL1
1
EPA 200.8
03/24/2015 12:38
DJSULL1
1
EPA 200.8
03/24/2015 12:38
DJSULL1
1
EPA 200.8
03/24/2015 12:38
DJSULL1
1
EPA 200.8
03/24/2015 12:38
DJSULL1
1
EPA 200.8
03/24/2015 12:38
DJSULL1
1
EPA 200.8
03/24/2015 12:38
DJSULL1
1
EPA 200.8
03/24/2015 12:38
DJSULL1
1
EPA 200.8
03/24/2015 12:38
DJSULL1
1
EPA 200.8
03/24/2015 12:38
DJSULL1
1
EPA 200.8
03/24/2015 12:38
DJSULL1
1
EPA 200.8
03/24/2015 12:38
DJSULL1

Certificate of Laboratory Analysis Page 17 of 58
This report shall not be reproduced, except in full.
Order # J15030137
Site: Equipment Blank
Collection Date: 04 -Mar -15 1:10 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
1 EPA 300.0
Vendor Parameter
Complete
1 EPA 300.0
03/09/2015 10:33
NITRITE + NITRATE (COLORIMETRIC)
1 EPA 245.1
03/10/2015 13:05
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
03/17/2015 11:53
MHALL3
1 EPA 200.7
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
03/09/2015 10:10
MHH7131
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY ICP
MHH7131
1 EPA 200.7
03/09/2015 10:10
Calcium (Ca)
< 0.01
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
03/12/2015 11:01
DJSULL1
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015006216
Matrix: GW WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
03/09/2015 11:53
TLINN
1 EPA 300.0
03/09/2015 10:33
BGN9034
1 EPA 300.0
03/09/2015 10:33
BGN9034
1 EPA 245.1
03/10/2015 13:05
ACPAYNE
1 EPA 200.7
03/17/2015 11:53
MHALL3
1 EPA 200.7
03/17/2015 11:53
MHALL3
1 EPA 200.7
03/17/2015 11:53
MHALL3
1 EPA 200.7
03/17/2015 11:53
MHALL3
1 EPA 200.7
03/09/2015 10:10
MHH7131
1 EPA 200.7
03/09/2015 10:10
MHH7131
1 EPA 200.7
03/09/2015 10:10
MHH7131
1 EPA 200.7
03/09/2015 10:10
MHH7131
1 EPA 200.7
03/09/2015 10:10
MHH7131
1 EPA 200.7
03/09/2015 10:10
MHH7131
1 EPA 200.7
03/09/2015 10:10
MHH7131
1 EPA 200.8
03/12/2015 11:01
DJSULL1
1 EPA 200.8
03/12/2015 11:01
DJSULL1
1 EPA 200.8
03/12/2015 11:01
DJSULL1
1 EPA 200.8
03/12/2015 11:01
DJSULL1
1 EPA 200.8
03/12/2015 11:01
DJSULL1
1 EPA 200.8
03/12/2015 11:01
DJSULL1
1 EPA 200.8
03/12/2015 11:01
DJSULL1
1 EPA 200.8
03/12/2015 11:01
DJSULL1
1 EPA 200.8
03/12/2015 11:01
DJSULL1
1 EPA 200.8
03/12/2015 11:01
DJSULL1
1 EPA 200.8
03/12/2015 11:01
DJSULL1
1 EPA 200.8
03/12/2015 11:01
DJSULL1
1 EPA 200.8
03/12/2015 11:01
DJSULL1

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15030137
Page 18 of 58
Site: Equipment Blank
Sample #: 2015006216
Collection Date: 04 -Mar -15 1:10
PM
Matrix: GW WW
Analyte
Result
Units Qualifiers
RDL
DF
Method Analysis Date/Time
Analyst
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
< 25
mg/L
25
1
SM2540C 03/11/2015 11:36
GHUTCHI
Total Carbon
TOC
0.122
mg/L
0.1
1
SM5310C/EPA9060A 03/10/201511:40
TJA7067
TOTAL SUSPENDED SOLIDS
TSS
< 5
mg/L
5
1
SM2540D 03/06/2015 11:10
GHUTCHI

Certificate of Laboratory Analysis Page 19 of 58
This report shall not be reproduced, except in full.
Order # J15030137
Site: Filter Blank
Collection Date: 04 -Mar -15 1:10 PM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
EPA 245.1
03/12/2015 15:46
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
1
EPA 200.7
03/11/2015 10:38
Aluminum (Al)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
DISSOLVED METALS BY ICP -MS
1
EPA 200.8
03/24/2015 12:44
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015006217
Matrix: GW WW
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
03/12/2015 15:46
ACPAYNE
1
EPA 200.7
03/11/2015 10:38
MHH7131
1
EPA 200.7
03/11/2015 10:38
MHH7131
1
EPA 200.7
03/11/2015 10:38
MHH7131
1
EPA 200.7
03/11/2015 10:38
MHH7131
1
EPA 200.7
03/11/2015 10:38
MHH7131
1
EPA 200.7
03/11/2015 10:38
MHH7131
1
EPA 200.7
03/11/2015 10:38
MHH7131
1
EPA 200.8
03/24/2015 12:44
DJSULL1
1
EPA 200.8
03/24/2015 12:44
DJSULL1
1
EPA 200.8
03/24/2015 12:44
DJSULL1
1
EPA 200.8
03/24/2015 12:44
DJSULL1
1
EPA 200.8
03/24/2015 12:44
DJSULL1
1
EPA 200.8
03/24/2015 12:44
DJSULL1
1
EPA 200.8
03/24/2015 12:44
DJSULL1
1
EPA 200.8
03/24/2015 12:44
DJSULL1
1
EPA 200.8
03/24/2015 12:44
DJSULL1
1
EPA 200.8
03/24/2015 12:44
DJSULL1
1
EPA 200.8
03/24/2015 12:44
DJSULL1
1
EPA 200.8
03/24/2015 12:44
DJSULL1
1
EPA 200.8
03/24/2015 12:44
DJSULL1

Duke Energy
Laboratory Services
13339 Hagers Ferry Road Bid. MG03A
Huntersville, NC 28078
Page 20 of 58
Mernent One Inc.
6319-D Carolina Beach Rd.
Wilmington, IVC 28412
Phone: [phone]
Fax: [phone]
[e-mail]
REPORT OF ANALYSES
March 23, 2015
Client Project Name Asheville
Client Project Number J15030137
PO Number
Sample Matrix
GW WW
Sample Type
Grab
Date Received
03/10/2015
Date Analyzed
03/12/2015
Method
SM 4500
S2_ D
Time Received
1120
Delivered by
FedEx
Received by
LLB
eOne ID
Duke Energy ID
Parameter
Result
Unit
Dil
DL Date
Time
Sampled
Sampled
24224-1 *
MW -1 313R
Sulfide
< 0.5
mg/L
5
0.1 03/03/15
915
24224-2
MW -1 313R Dup
Sulfide
< 0.1
mg/L
1
0.1 03/03/15
915
24224-3*
MW -17
Sulfide
< 0.5
mg/L
5
0.1 03/03/15
1345
24224-4*
MW -15
Sulfide
< 0.5
mg/L
5
0.1 03/04/15
0855
24224-5
MW -15 D
Sulfide
< 0.1
mg/L
1
0.1 03/04/15
1000
24224-6*
Equipment Blank
Sulfide
< 0.5
mg/L
5
0.1 03/03/15
1130
24224-7
Equipment Blank
Sulfide
< 0.1
mg/L
1
0.1 03/04/15
1310
Samples were received and analyzed outside of hold time.
*Sample spike recovery outside of QA limits of 85-115%; dilution necessary to meet laboratory QA limits.
This is the first revision to this report; it was necessary to analyze an additional curve point to meet the requested detection limit
of < 0.1 mg/L.
Ken meth, Laboratory Director
24224 Duke Report Packet Rev 3.23.15 Compiled byQft,%
NC Certifications: DW 37788 and DWQ DENR 604

7-
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Page 21 of 58
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elernen One SAMPLE SUBMISSION FORM Lab I&ge X4114
TAT 7 BD
Hold Time Expiration 03.10.15 @ 0915 AM
Client: Duke Energy
LIMS No J15030137
Project ID Asheville
H >9 YeV No 11Tem <_ 6°C
If No, Record %If No, Record
Sample Identification & Collection Information
Yes
Analysis Due Date 03.11.15
Report Due Date 03.18.15
Date Rec:
03.10.15
Time Rec:
1120
Rec By
LLB
No Ref. Method:
—d SM4500 S2 D
Lab ID
Client ID
Collection Date
Collection Time
Analysis Requested
1
MW -13 BR
03.03.15
0915 AM
Sulfide
2
MW -136R Dup
03.03.15
0915 AM
Sulfide
3
MW -17
03.03.15
1345 PM
- Sulfide
4
MW -15
03.04.15
0855 AM
Sulfide
5
6
7
MW -15 D
Equipment Blank
Equipment Blank
03.04.15
03.03.15
03.04.15
1000 AM
1130 AM
1310 PM
Sulfide
Sulfide
Sulfide
NOTE for Sulfide The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final spike concentration at - 500 pg/L
Lab Communications
Per Jay via a -mail, analyze samples out of hold time and document on report ---03.10.15 LLB
SS Page 1 o Prep By / Date _ Dk 12 3/ I (/1
SS by Labeled By/ Date Y`;& 3 •io -,--5'-'
3/11/2015 10:13:03 AM ID Verification By /DateLm{ , IVITT—

METHOD:
ELEMENT ASSAY:
CLIENT:
Lab ID#
Date:
Time Analvsis Beaw
ug5Ili
)LUTION
0.00
1.00
2.50
5.00
7.50
10.00
SM 4500 S2- D ELEMENT ONE
1115
Y;;
0000
STD D.
ABS__..,' asaa
0.000 0400
0.064 I o3aa
0.170 ow
0.341 Dim
Dam
Page 23 of 58
Spectrophotometer UNITS OF ANSWER u mL
Wave Length 664 DETECTION LIMIT u
SPK LEVEL u 5
MAX ALI UOT 10.00
N82S•91-12O Lot 5010904 STANDARD conc(ppm) X
W C2-62-1 10
W C2-62-2
STD ABSORPTION Y
- a - -
0.482 0.00 zoo 400 oa0 000 10.00 120
0.626 x
0.6
Slope
170
ae4
Correlation
0.999000882'
SAMPLE
I.D.
SAMP
ABS
0.482 0.00 zoo 400 oa0 000 10.00 120
0.626 x
Sulfide 2
Slope
0.06298022
Correlation
0.999000882'
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
LRB
0.000
10
10
10
<0.1
LRB SPK
0.341
5.3348
10
10
10
0.533
107%
5.0
24222-1
0.005
-0.2269
10
10
10
<0.1
24222-1 s k
0.094
1.2463
10
10
10
0.125
25%
5.0
24222-2
0.004
-0.2435
10
10
10
<0.1
24222-2 s k
0.226
3.4312
10
10
10
0.343
69%
5.0
24223-1
0.003
-0.2600
10
10
10
<0.1
24223-1 s k
0.215
3.2491
10
10
10
0.325
65%
5.0
24223.2
0.001
-0.2931
10
10
10
<01
24223-2 dup
0.003
-0.2600
10
10
10
<0:,1
-12%
24223.2 sa
0.338
5.2851
10
10 J
10_
0.529
106% . '
5.0
24223.3
0.005
-0,2269_
10
10
10
<0.1
24223,3 s k
0.320
4.9872
10
10
10
0.499
140%
5.0
24223-4
0.013
-0.0945
10
10
10
<0.1
24223-4 s k
0.147
2.1235
10
10
10
0.212
43%
5.0
24223-5
0.002
-0.2766
10
10 ,
10,
<0.1
24223-5 s k
0.307
4.7720
10
10
10'
0.477
960/9
5.0
24224-1
0.005
-0.2269
10
10
10
<0.1
24224-1 s k
0.234
3.5636
10
10
10
0.356
71%
5.0
24224-2
0.003
-0.2600
10
10
10
<0.1
24224-2 dup
0.002
-0.2766
10
10
10
<0.1
-6%
24224-2 s k
0.308
4.7385:
10
10
10
0.479
96%d
5.0
Blank
0.000
0.0000
10
10
10
<0.1
QC
Submitted r Q
0.335
QC-
5.2355
Date:
10
3
10
By: (Print)
10
0.524
105%
(sign).
10. 5.0
Sulfide 2

Page 24 of 58
METHOD:
SM 4500 S2- D
ELEMENT ONE
ABS
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Length 664
UNITS OF ANSWER
DETECTION LIMIT uc
SPK LEVEL u
u__ L
5
CLIENT:
Duke
Lab ID#
24224, 24227, 24228
3/11/15
12:45
17:00
KAM
Y
Na2S•9H2O Lot 5010904
WC2-62-1
WC2-62-2
MAX ALI UOT
STANDARD conc(ppm)
ISTD ABSORPTION
10.00
X
10
Y
Date:
Time Analysis Begun
Time Analysis Ended
Analyst:
X
ug STD
o1w
STD opo
SOLUTION
ABS
0.00
0.000 0 o0
1.00
0.064
2.50
0.170 02M
5.00
0.341 "0
0000
7.50
10.00
0.48'2
0.626
0.0o
zao
<.00
a.0a
.,w
00o aoo
°
Slope
0.0629$022
Correlation
0.999000863
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
.941
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
LRB
0.000
0.0000
10
--
10
<0.1
-
0
LRB SPK
0.341
5.3348
10
10
10
0.533
7.50
10.00
0.48'2
0.626
0.0o
zao
<.00
a.0a
.,w
00o aoo
°
Slope
0.0629$022
Correlation
0.999000863
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
LRB
0.000
0.0000
10
10
10
<0.1
0
LRB SPK
0.341
5.3348
10
10
10
0.533
1070A0
5.0
24224-3
0.000
0.0000
10
10
10
<0.1
24224-3 s k
0.215
3.2491
10
10
10
0.325
65%
5.0
24224-4
0.002
-0.2766
10
10
10
<0.1
242244 s k
0.224
3.3981
10
10
10
0.340
68%
5.0
g v , v
"r
5.0
24224-6
0.003
-0.2600
10
10
10
<0.1
24224-6 s k
0.263
4.0437
10
10
10
0.404
81%
5.0
24224.7
0.002
-0,2766
10
1A
10
<0.1
24224-7 du
0.:006
-0.2104.
10
10 '
10
<0,1
-27%
24224-7 s k-
0.290
4.4906:
10
10
10
0:449
90%
5.0
24227
0.001
-0.2931
10
10
10
<0.1
24227 s k
0.033
0.2365
10
10
10
<0.1
5%
5.0
24228-1
0.003
-0.2600
10
10.
1.0
<0.1
2422841 s k
24228-3
0.320
0,001
4.9872 10 10 10
-0.2931 10 10 10
0.499
<0.1
100'/0.
5.0
5.0
24228-3 s k
24228-4
0.309
0.002
4.8051
-0.2766
10
10
10
10
10 "
10
0.481
<0.1
96"k
5.0
24228-4 dup
0.001
-0.2931
10
10
10
<0.1
-6%
24228-4 s k
0.231
3.5140
10
10
10
0.351
70%
5.0
Blank
QC
Su m # r Q
0.000
0.335
C -
0.0000
5.2355
Date:j
10
10
10
10
By: (Print)
10
10
<0.1
0.524
105%
,�; ,,,�• . -,�„ _
5.0
Sulfide 3

METHOD: SM 4500 S2- D
ELEMENT ASSAY: Sulfide
Date: 3/12/15
Time Analysis Begun 15:00
Time Analvsls Ended 17:00
ugtiIU
SOLUTION
0.00
1.00
2.50
5.00
7.50
10.00
Y
STD o,
ABS
0.000 o.
0.064
0.170 °
0.341 °
0.482 °
0.626
Page 25 of 58
ELEMENT ONE
Wave Length 664 . SPK LEVEL u 5
MAX ALIQUOT 10.00
>S•91 -1z0 Lot 5010904 STANDARD conc(ppm) X
WC2-62-1 10
WC2-62-2
STD ABSORPTION Y
X
Sulfide 7
S1022
0.06298022
Correlation
0.999000862
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
LRB
0.000
10
10
10
<0.1
0
LRB SPK
0.341
5.3348
10
10
10
0.533
107%
5.0
24218-1
0.003
-0.2600
10
10
2
<0.5
24218-1 s k
0.088
1.1469
10
10
2
<0.5
23%
5.0
24218-6
0.004
-0.2435
10
10
2
<0.5
24218-6 du
0.003
-0.2600
10
10
2
<0.5
24218-6 s k
0.254
3.8947
10
10
2
1.947
78%
5.0
24219
0.005
-0.2269
10
1,0
2
<0.5
24219 6 k
0.339 1
5.3017
10,
10
2:
2.651
106%
5.0
24220.
0.001
-0.2931 `
10
10
2
<0.5
24220 s k
0.323
5.0368
10
10
2
2.518
101%
5.0
24222-2
0.003
-0.2600
10
10
2
<0.5
24222-2 s k
0.344
5.3844
10
10 �
2
2.692
108%
5.0
24223-1 .
0.001
,
-0.2931;
10
10
2
24223-1 s k
0.321
5.0037
10
10
2
2.502
100%
5.0
242241
0.004
-0.2435°
10
10
2
<0.5
24224-1 s k
0.332
5.1858
10
10
2
2.593
104%
5.0
24224-3
0.005
-0.2269
10
101,
2
<0.5
24224-3 dup
0.002
-0.2766
10
10
2
<0.5
24224-3 3 k
0.290
4.4906
10
10
2
2.245
90%,
5.0
24224-4
0.002
-0.2766
10
10
2
.50.5
24224-4 s k
0.318
4.9541`
10
10
2
2.477
99%
5.0
Blank
070-00--F0.0000
10
10
10
<0.1
QC
Submitted r
0.335
C-
5.2355
Date:
10
10
By: (Print)
10
0.524
, 105%
(sign):
Sulfide 7

Page 26 of 58
METHOD:
SM 4500 S2- D
SOLUTION
ELEMENT ONE
0.00
ELEMENT ASSAY:
Sulfide
0.064 I °°
Spectrophotometer
Wave Length 664
U-- OF ANSWER
DETECTION LIMIT u
un/mL
CLIENT:
Duke
SPK LEVEL u
5
Lab ID#
24224 228 229, 230 231
3112/15
15:00
17:00
KAM DMR
lNa2S.9H20 Lot 5010904
WC2-62-1
WC2-62-2
MAX ALIQUOT
10.00
Date:
STANDARD conc(ppm)
X
Time Analysis Begun
LESS THAN
10
Time Analysis Ended
ABS
ALIQUOT
Analyst:
ISTD ABSORPTIONy
- --
y
-
u/mL
ug STD
°,°°
STD °
SOLUTION
ABS °
0.00
0.000
1.00
0.064 I °°
2.50
0.170
5.00
0.341
7.50
0.4 °
10.00
0.626
°°°
z°°
Sloe
i-
0.999000862
SAMPLE
SAMP
ug PER
ALI in mL
PREP
ALI in mL
RESULTS
LESS THAN
SPIKE
I.D.
ABS
ALIQUOT
ANALYZED
10.00
0.626
°°°
z°°
Sloe
0.06298022 Correlation
0.999000862
SAMPLE
SAMP
ug PER
ALI in mL
PREP
ALI in mL
RESULTS
LESS THAN
SPIKE
I.D.
ABS
ALIQUOT
ANALYZED
VOL in mL
TAKEN
u/mL
% SPK REC
LEVEL
LRB
0.000
10
10
10
<0.1
0
LRB SPK
0.341
5.3348
10
`
10
10
0.533
107%_
5.0
24224-5
0.003
-0.2600
10
101,
2
<0.5
24224-5 s k
0.318
4,9541
10
10
'21,
2.477''
99%
5.0
24224.6
0.003
-0.2600
10
10
2
<0.5
!4224.6 s k
0.358
5.6162
10
10
2
2.808;
112°/a'
5.0
?42247
0.001
-0.2931
10
10
2
<0.5
?4224-7 s k
0.353
5.5334
10
10
2
2.767
t 11 % ,
5.0
!4228-2
0.002
-0.2766
10
10
2,
<0;5 '
!4228.2 s k
0.358
5.6162
10
10
2
2.808
112%
5.0
!4228-4
0.003
-0.2600
10
10
!4228.4 s k'
0.337
5.2686
10
10
2"
2.634
105%
5.0
>42291
0.001
0.2931
10
10
2
<0.5
!4229-1 s k
0.338
5.2851
10
10
2
2.643
1l)6%`
5.0
!4229-2
0.000
10
40
2
<0.5
9229-2, k
0.354
5.5500
10
10
2
2.775
111%
!4229-3
0.002
-0.2766
10
10
2
<0.5
5.0
!4229-3 s k
0.369
5.7982
10
10
2
2.899
116%
5.0
J,
4229.5
0.003
-0.2600
1010
2 '
5.0
4229-6 s k
0.356
5.5831
10 -
10
2
<0.5
4229 6
0.002
-0.2766
10
10
2.792'
112% .
5.0
4229-6 s k
0.337
5.2686
10
10
2
<0.5
4229-7
0.001
-0,2931
10
10
2
2.634
105%
5.0
4229-7 s k
0.340
5.3182
10
10
2
<0.5
4230-1
0.002
-0.2766
90
10
2
2.659
108%
5.0
4230-1 s k
0.335
5.2355
10
10
2
<0.5
4230-2
0.000
0.0000
10
2 :
2.618
105°%
5.0
4230-2 du
0.001
-0.2931
10
10
2
<0.5
4230-2 s k
0.351
5.5003
10
10
2
<0.5
4231
0.002
-0.2766
10
10
2
2.750
1.10°fo
5.0
1231 5 k
0.345
5.4010
1 p
10
10
2
<0.5
Blank
0.000
0.0000
10
10
2
2.700
108%
5.0
QC
0.335
5.2355
10
10 1
10
<0.1
ubmitted for O
QC -
Date:
10
0 .524
105%
5.0
By: (Print)
(sign):
Sulfide 8

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water - Asheville
Project Number:J15030137
Lot Number:QC05049
Date Completed:03/17/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
*QC05049*
Shealy Environmental Services, Inc. Page: 1 of 18
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SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QC05049
Project Name: AB GW Assessment Water - Asheville
Project Number: J15030137
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 18
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SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QC05049
Project Name: AB GW Assessment Water - Asheville
Project Number: J15030137
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
2015006202
Aqueous
03/03/2015 0915
03/05/2015
002
2015006210
Aqueous
03/03/2015 0915
03/05/2015
003
2015006211
Aqueous
03/03/20151345
03/05/2015
004
2015006212
Aqueous
03/04/2015 0855
03/05/2015
005
2015006213
Aqueous
03/04/20151010
03/05/2015
006
2015006214
Aqueous
03/03/20151130
03/05/2015
007
2015006216
Aqueous
03/04/20151310
03/05/2015
(7 samples)
Shealy Environmental Services, Inc. Page: 3 of 18
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SHEALY ENVIRONMENTAL SERVICES, INC.
(10 detections)
Shealy Environmental Services, Inc. Page: 4 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
Executive Summary
Duke Energy
Lot Number: QC05049
Project Name: AB GW Assessment Water - Asheville
Project Number: J15030137
Sample Sample ID
Matrix
Parameter Method Result Q
Units
Page
001
2015006202
Aqueous
Alkalinity SM 2320B-
32
mg/L
5
001
2015006202
Aqueous
Bicarbonate Alkalinity SM 2320B-
32
mg/L
5
002
2015006210
Aqueous
Alkalinity SM 2320B-
30
mg/L
7
002
2015006210
Aqueous
Bicarbonate Alkalinity SM 2320B-
30
mg/L
7
002
2015006210
Aqueous
Methane RSK - 175
12
ug/L
8
003
2015006211
Aqueous
Alkalinity SM 2320B-
36
mg/L
9
003
2015006211
Aqueous
Bicarbonate Alkalinity SM 2320B-
36
mg/L
9
003
2015006211
Aqueous
Methane RSK - 175
11
ug/L
10
005
2015006213
Aqueous
Alkalinity SM 2320B-
39
mg/L
13
005
2015006213
Aqueous
Bicarbonate Alkalinity SM 2320B-
39
mg/L
13
(10 detections)
Shealy Environmental Services, Inc. Page: 4 of 18
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QC05049-001
Description: 2015006202 Matrix: Aqueous
Date Sampled:03/03/2015 0915 Project Name: AB GW Assessment Water -
Date Received: 03/05/2015 Project Number: J15030137
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 03/06/2015 1850
BWS 69407
1
(Bicarbonate ) SM 2320B-2011
1 03/06/2015 1850
BWS 03/06/2015 1850
1
(Carbonate Al) SM 2320B-2011
1 03/06/2015 1850
BWS 03/06/2015 1850
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 18
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CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
32
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
32
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 18
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Methane
Client: Duke Energy Laboratory ID: QC05049-001
Description: 2015006202 Matrix: Aqueous
Date Sampled:03/03/2015 0915 Project Name: AB GW Assessment Water -
Date Received: 03/05/2015 Project Number: J15030137
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 03/15/2015 1418 JJG 70039
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 18
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Inorganic non-metals
Client: Duke Energy Laboratory ID: QC05049-002
Description: 2015006210 Matrix: Aqueous
Date Sampled:03/03/2015 0915 Project Name: AB GW Assessment Water -
Date Received: 03/05/2015 Project Number: J15030137
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 03/06/2015 1907
BWS 69407
1
(Bicarbonate ) SM 2320B-2011
1 03/06/2015 1907
BWS 03/06/2015 1907
1
(Carbonate Al) SM 2320B-2011
1 03/06/2015 1907
BWS 03/06/2015 1907
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
30
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
30
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QC05049-002
Description: 2015006210 Matrix: Aqueous
Date Sampled:03/03/2015 0915 Project Name: AB GW Assessment Water -
Date Received: 03/05/2015 Project Number: J15030137
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 03/15/2015 1429 JJG 70039
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 12 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QC05049-003
Description: 2015006211 Matrix: Aqueous
Date Sampled:03/03/2015 1345 Project Name: AB GW Assessment Water -
Date Received: 03/05/2015 Project Number: J15030137
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 03/06/2015 1924
BWS 69407
1
(Bicarbonate ) SM 2320B-2011
1 03/06/2015 1924
BWS 03/06/2015 1924
1
(Carbonate Al) SM 2320B-2011
1 03/06/2015 1924
BWS 03/06/2015 1924
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
36
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
36
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QC05049-003
Description: 2015006211 Matrix: Aqueous
Date Sampled:03/03/2015 1345 Project Name: AB GW Assessment Water -
Date Received: 03/05/2015 Project Number: J15030137
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 03/16/2015 2034 JJG 70156
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 11 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QC05049-004
Description: 2015006212 Matrix: Aqueous
Date Sampled:03/04/2015 0855 Project Name: AB GW Assessment Water -
Date Received: 03/05/2015 Project Number: J15030137
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 03/06/2015 1929
BWS 69407
1
(Bicarbonate ) SM 2320B-2011
1 03/06/2015 1929
BWS 03/06/2015 1929
1
(Carbonate Al) SM 2320B-2011
1 03/06/2015 1929
BWS 03/06/2015 1929
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QC05049-004
Description: 2015006212 Matrix: Aqueous
Date Sampled:03/04/2015 0855 Project Name: AB GW Assessment Water -
Date Received: 03/05/2015 Project Number: J15030137
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 03/16/2015 2050 JJG 70156
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 12 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QC05049-005
Description: 2015006213 Matrix: Aqueous
Date Sampled:03/04/2015 1010 Project Name: AB GW Assessment Water -
Date Received: 03/05/2015 Project Number: J15030137
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 03/06/2015 1933
BWS 69407
1
(Bicarbonate ) SM 2320B-2011
1 03/06/2015 1933
BWS 03/06/2015 1933
1
(Carbonate Al) SM 2320B-2011
1 03/06/2015 1933
BWS 03/06/2015 1933
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 13 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
39
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
39
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 13 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QC05049-005
Description: 2015006213 Matrix: Aqueous
Date Sampled:03/04/2015 1010 Project Name: AB GW Assessment Water -
Date Received: 03/05/2015 Project Number: J15030137
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 03/16/2015 2133 JJG 70156
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 14 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QC05049-006
Description: 2015006214 Matrix: Aqueous
Date Sampled:03/03/2015 1130 Project Name: AB GW Assessment Water -
Date Received: 03/05/2015 Project Number: J15030137
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 03/06/2015 1938
BWS 69407
1
(Bicarbonate ) SM 2320B-2011
1 03/06/2015 1938
BWS 03/06/2015 1938
1
(Carbonate Al) SM 2320B-2011
1 03/06/2015 1938
BWS 03/06/2015 1938
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 15 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 15 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QC05049-006
Description: 2015006214 Matrix: Aqueous
Date Sampled:03/03/2015 1130 Project Name: AB GW Assessment Water -
Date Received: 03/05/2015 Project Number: J15030137
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 03/15/2015 1446 JJG 70039
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 16 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QC05049-007
Description: 2015006216 Matrix: Aqueous
Date Sampled:03/04/2015 1310 Project Name: AB GW Assessment Water -
Date Received: 03/05/2015 Project Number: J15030137
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 03/06/2015 1942
BWS 69407
1
(Bicarbonate ) SM 2320B-2011
1 03/06/2015 1942
BWS 03/06/2015 1942
1
(Carbonate Al) SM 2320B-2011
1 03/06/2015 1942
BWS 03/06/2015 1942
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 17 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 17 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QC05049-007
Description: 2015006216 Matrix: Aqueous
Date Sampled:03/04/2015 1310 Project Name: AB GW Assessment Water -
Date Received: 03/05/2015 Project Number: J15030137
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 03/16/2015 2204 JJG 70156
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 18 of 18
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QC05049
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - Ii
Sample ID: QQ69407-001 Matrix: Aqueous
Batch: 69407
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 03/06/20151816
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC05049
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ69407-002 Matrix: Aqueous
Batch: 69407
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 100 1 100 90-110 03/06/20151822
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC05049
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MS
Sample ID: QC05049-001 MS Matrix: Aqueous
Batch: 69407
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 32 100 120 1 89 70-130 03/06/20151856
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC05049
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - MSD
Sample ID: QC05049-001MD Matrix: Aqueous
Batch: 69407
Analytical Method: SM 2320B-2011
Sample Spike
Amount Amount Result % Rec % RPD
Parameter (mg/L) (mg/L) (mg/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Alkalinity 32 100 120 1 91 1.0 70-130 20 03/06/20151902
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC05049
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ70039-001 Matrix: Aqueous
Batch: 70039
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 03/15/20151129
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC05049
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ70039-002 Matrix: Aqueous
Batch: 70039
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 50 48 1 96 70-130 03/15/20151034
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC05049
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ70039-003 Matrix: Aqueous
Batch: 70039
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 50 46 1 90 6.0 70-130 30 03/15/20151052
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC05049
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ70156-001 Matrix: Aqueous
Batch: 70156
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 03/16/20151848
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC05049
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ70156-002 Matrix: Aqueous
Batch: 70156
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 50 43 1 85 70-130 03/16/20151627
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC05049
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ70156-003 Matrix: Aqueous
Batch: 70156
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 50 51 1 101 18 70-130 30 03/16/20151703
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QC05049
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
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Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

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Ctie rtt= Cooler Inspected b rddate: x'ro , Ir oo ,tit 9: 14A
Means ofiweipt:
iscsf ❑ Client ❑ UPS Ej YedEx ❑ Airborne Exp ❑ Othcr
yes F1
INO[ZI1-
WcTe cii stcdy se a 1E; veseaat on the cooler?
Yes ❑
II+1(i
N,4 2_ lrf uuStOd saalq rovers 3r�ent, v.ere khcy intact and unbroken`
C'leroler 1010riginal tomperature upon remipjDerived(corTected) temperature upon receipt:
I N- d{� --:I,— D I I oc: d J OC f 11 41C
Method; [r "Tern yeratnre 111ank ❑ Against Bortles 1R'Garr IJ7: IRGlin Carrectioi'I Factor- Ct
Method of coolant. L�J'Wct lco ❑ Blue Ic_c ❑ F2Z Ice El N031e e
Yes ❑
No ❑
3. If temperature of any cloaler exceeded 6. VC, was Project Manager notified?
WA PM notified by SRC.. Phoue, note (dale onc), Cather_ _
(For coolers received via c rnrnerelal courier, PMs are to be notified
iiminediatel -)
YEWr
Iso ❑
Nab CT 4. Is the ourrimerciat courier's packing slip attached to this fortrt7
Yes
No❑
5, Wererte r etastixl nocedures relin uishedlrveceived followed'?
Yes ❑
No ❑
NA 5a Wcra sam Ics rclin uisbcd by client to Danlmerciat courier?
Yes
No ❑
6. Wem sarn p le Yr)s l i sted ori the COC'
Yes
No ❑
7. Were sant Ze U)s listed on all sample containers?
Yes
No ❑
- Was cnIiection date & tirue listed on tyle COC?
Yes
No ❑
9- Was collection date & time lisle¢ on All sample { ontaincrs?
Yes
No ❑
110. Did all container lahcl information D, elate time) agree with the CGC?
Yes
yes
No []
No ❑
11. Were tests to be performed listed on tlae ff"
12. Did rill samples firrive in the pr6per containevs fqr each test?
Yes
Yes
0 ❑
No ❑
13. Did all containers arrive itt ood C-Onditiun (unbn;ken, lids on, e%. '-a
14. Was adequate sarr le vial-ime availa,bte?
Yes .
No C
15. Were all Samples received within f. the holding time kir 48 hours, whichever
camas f!FSV
Yes ❑
NQ
16, Were any Sam les containers missing?
Yes EF
No 1
17- Were there any exof-s -arnF les not listed on COC?
Yes ❑
No
NA ❑ IS. Were bubbles present >` ca -size}' 1,4"or 6nim in dialmocr) in an ' _ CJA via1a'
Yes ❑
No ❑
NA 19. Fere all nl-MW &Cy/HMM1nutnent samples received alta pH el' -2?
Yes ❑
No Ll
NA j- 201. Were r11i c snide andfor sulfide samples reaeivcd ata pH >12"
Yes ❑
Yes ❑
No ❑
No ❑
NA a 21= Were all applicable NT43ITKNiryanidOphenol (<O 2mgd _) sainplts free Of
residual chlorine7 _
NA 22- Were collection temperatures documented art the COC for NC sam les I
`Yes ❑
No ❑
NA 2-1- aJ cm £tient remwks,dregnests (Le requested dilutions, MS/ Sp designstiorrs,
elc... ) carnet] , transcribed from the COC into the commeatt section in LIMS?
Yes ❑
No
'�4- Was the qkiote number used taken from the conlsiinsr label?
!Sample Presenation (Midst be ci3rripleied for any samples) inl-arrectly Preserved or with headspace-)
ample(.) _ were received incorrectly preserved and were ac4justed
accord in gly in sam ple receivin g wiih (H?S4d,HN0'3.HCI N&0H) using SIS
sa n le(s) wcm received with bubbles >,G mrn in diamctur,
SA1npl s were received with 'TRC }{I,2 m +L If 421 is No
SC Drinking Water Pr*ct Sample(s) pH verified tc be- 2 by Dice-,
Sam les were rent receivtd at a pH of <2 apld were adjusted accordingly using SR#
S�mplc labels applied by:.. Verified by: Date-
Comments
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM
--------------- ---
Duke Energy Analytical Laboratory
+r-----------------------
j Anal al Laborato
Use Onl
Date/Time
Page 58 of 58
DUke Ener 9y
j
Mall Cods M@O3A4 (Building 7405)
I !Ord@r # Matrix GW -WW W
Sampler Orlainelirp From
NC_
i Page _1_ of _1 —
Analytical Laboratory
13339 Halters Ferry Rd
I 15 0 1
Relinquished 8 Daterrime
Co
Accepted By: Daternmm]e
ScIT
! DISTRIBUTION
! Chain Of Custody&
Humeravllk, N. C. 4,078
1704) . N. C.
! L
I j egged By PFI Date a Time
.3. 5.15 `i 3
SAMPLE
PROGRAM
'_
i ORIGINAL to LAB, COPY to CLIENT
' Sample Log
j
Faa_pn44 B -----6 -_-_-_•-,-,i
! rr
EMS
Ground Water_
NPDES_
• 48 Hr
- ......... -
i Project Name AB GW Assessment water P^«'� "O0
Element 1
)
41
Dunking Water UST
_
RCRA Waste
PO 1142133
Cooler em19L.._...._.._.._..--------------------•-.........................................................
ttion(0.45um)
comri,ama--
ELEMEN b ICP_ RM): As, Be, Cd, Co, Cr, Cu, Mo, Ni, Pb, Sb, Se, TI (LL), V (LL)
Unfiltered
b filtered
E
Clientgype•75.5032
w
_ASAP
`Add. Cost Will Apply
Dissolved metals: all metals ICP, IMS,Hg
Preservative Ice
)r Volume (mL) 2000
kat
Ice ICs H2a04
40 II11 300 +z6
IGe eOMI
500 500
wn+>wr
500 250
.`€ Business Unitt::
Procece:
Reap. Canter To:
x Project ID:
nct'vev'O:
.—:
Mao `edea
M
SHEALY
n-,nnn
:ontainer Type PET
gl8ss PET PET
PET PET
I HDPE HDPE
Wateraoay: station.
i'
_.._-._..—.._..—..I
i
I '•
i
! I
13`
!
Relinguished By.
Date/Time:
Received By:
Date/Time:
901500 lea 14
i
a. a
ation
1.U9[VIrICr lV el 1
Date/Tlme
S
Accept y:
Date/Time
U
Requested Turnaround
JS
G
V
'14 Days
Relinquished 8 Daterrime
Co
Accepted By: Daternmm]e
N
a °
E
7Days
Relinquished Date/Tlme
Acce y: �Daaje1nme r
/r� rot >
EMS
0I 7
� �
Cl d
• 48 Hr
Sea1/L By + Date/Tlme
algid/Lock Opened By Date/Time
- a
a
a
o
'Other
comri,ama--
ELEMEN b ICP_ RM): As, Be, Cd, Co, Cr, Cu, Mo, Ni, Pb, Sb, Se, TI (LL), V (LL)
Y ■■©moi■■■moo■■■■■■■oo■�
ELEME&S by ICP (TRM): Al, Be, B. Fe, Mn, Sr, Zn ICP -Undigested Ca, Mg, K, Na
Hg by 245.1
w
_ASAP
`Add. Cost Will Apply
Dissolved metals: all metals ICP, IMS,Hg
U
rM ■®■
1c'i�r■■DD■■0■■�����0
!'
■■■0■■■■®■■
Filter Blank
� �■ .' ■■0000■■■■■■0■■O
Rellnquish By
1.U9[VIrICr lV el 1
Date/Tlme
S
Accept y:
Date/Time
U
Requested Turnaround
JS
G
V
'14 Days
Relinquished 8 Daterrime
Co
Accepted By: Daternmm]e
N
a °
E
7Days
Relinquished Date/Tlme
Acce y: �Daaje1nme r
/r� rot >
a j�/�
0I 7
� �
Cl d
• 48 Hr
Sea1/L By + Date/Tlme
algid/Lock Opened By Date/Time
- a
a
a
o
'Other
comri,ama--
ELEMEN b ICP_ RM): As, Be, Cd, Co, Cr, Cu, Mo, Ni, Pb, Sb, Se, TI (LL), V (LL)
ELEME&S by ICP (TRM): Al, Be, B. Fe, Mn, Sr, Zn ICP -Undigested Ca, Mg, K, Na
Hg by 245.1
w
_ASAP
`Add. Cost Will Apply
Dissolved metals: all metals ICP, IMS,Hg
U
Total 11