NC0000396_J15020366report_20150823

DUE Analytical Laboratory Page 1of39
' ENERGY
Order Number:
Project Name:
Customer Name(s):
Customer Address:
Lab Contact:
Report Authorized By:
(Signature)
Program Comments:
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
J15020366
AB GW ASSESSMENT WATER
Todd Plating, Kathy Webb, John Toepfer, Tim Hunsucker
200 CP and L Drive
Arden,NC 28704
Mary Ann Ogle
Mary Ann Ogle
Phone: [phone]
Mary Ann Ogle
2015.03.04 10:56:30 Date:
-05'00'
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
3/2/2015
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Collection
Sample ID Plant/Station Date and Time
2015004084
2015004086
2015004087
2015004088
2015004089
2015004098
6 Total Samples
Collected By
Sample Description
ASHEVILLE
12 -Feb -15 10:15 AM
illegible
MW 13D
ASHEVILLE
12 -Feb -15 2:05 PM
illegible
MW 11D
ASHEVILLE
13 -Feb -15 11:00 AM
illegible
MW 14BR
ASHEVILLE
13 -Feb -15 12:00 PM
illegible
Equipment Blank
ASHEVILLE
12 -Feb -15 1:20 PM
illegible
Filter Blank
ASHEVILLE
13 -Feb -15 12:00 PM
illegible
Filter Blank
Page 2 of 39

Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals Yes No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes No
All laboratory QA/QC requirements are acceptable. (] Yes ❑ No
Report Sections Included:
LU Job Summary Report
❑ Sample Identification
P/1 Technical Validation of Data Package
J❑ Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
Page 3 of 39
LVI Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
d❑ Chain of Custody
LVI Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: DBA Account Date: 3/2/2015

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020366
Site: MW 13D
Collection Date: 12 -Feb -15 10:15 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 300.0
02/19/2015 12:04
Vendor Parameter
Complete
EPA 300.0
02/19/2015 12:04
NITRITE + NITRATE (COLORIMETRIC)
1
EPA 245.1
Nitrite + Nitrate (Colorimetric)
0.236
mg-N/L
0.01
INORGANIC IONS BY IC
ACPAYNE
1
EPA 200.7
Chloride
4.4
mg/L
0.1
Sulfate
4.0
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
MHH7131
1
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
02/18/2015 09:33
MHH7131
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
EPA 200.7
02/18/2015 09:33
MHH7131
Aluminum (AI)
0.011
mg/L
0.005
Barium (Ba)
0.028
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.129
mg/L
0.01
Manganese (Mn)
0.556
mg/L
0.005
Strontium (Sr)
0.076
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
02/20/2015 11:32
MHALL3
Calcium (Ca)
33.2
mg/L
0.1
Magnesium (Mg)
2.78
mg/L
0.005
Potassium (K)
3.96
mg/L
0.1
Sodium (Na)
4.62
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.339
mg/L
0.005
Barium (Ba)
0.034
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
0.515
mg/L
0.01
Manganese (Mn)
0.563
mg/L
0.005
Strontium (Sr)
0.092
mg/L
0.005
Zinc (Zn)
0.006
mg/L
0.005
Sample #: 2015004084
Matrix: GW WW
Page 4 of 39
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
02/14/2015 11:47
TLINN
1
EPA 300.0
02/19/2015 12:04
BGN9034
1
EPA 300.0
02/19/2015 12:04
BGN9034
1
EPA 245.1
02/20/2015 09:55
TLINN
1
EPA 245.1
02/25/2015 11:14
ACPAYNE
1
EPA 200.7
02/18/2015 09:33
MHH7131
1
EPA 200.7
02/18/2015 09:33
MHH7131
1
EPA 200.7
02/18/2015 09:33
MHH7131
1
EPA 200.7
02/18/2015 09:33
MHH7131
1
EPA 200.7
02/18/2015 09:33
MHH7131
1
EPA 200.7
02/18/2015 09:33
MHH7131
1
EPA 200.7
02/18/2015 09:33
MHH7131
10
EPA 200.7
02/18/2015 12:32
MHH7131
1
EPA 200.7
02/18/2015 12:32
MHH7131
1
EPA 200.7
02/18/2015 12:32
MHH7131
1
EPA 200.7
02/18/2015 12:32
MHH7131
1
EPA 200.7
02/20/2015 11:32
MHALL3
1
EPA 200.7
02/20/2015 11:32
MHALL3
1
EPA 200.7
02/20/2015 11:32
MHALL3
1
EPA 200.7
02/20/2015 11:32
MHALL3
1
EPA 200.7
02/20/2015 11:32
MHALL3
1
EPA 200.7
02/20/2015 11:32
MHALL3
1
EPA 200.7
02/20/2015 11:32
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020366
Site: MW 13D
Collection Date: 12 -Feb -15 10:15 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
4.27
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
2.65
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.780
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
4.11
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
3.04
Nickel (Ni)
1.05
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
1.67
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
110
Total Carbon
02/24/2015 13:23
TOC
0.478
TOTAL SUSPENDED SOLIDS
1
TSS
< 5
Page 5 of 39
ug/L
1
1
Sample #:
2015004084
DJSULL1
ug/L
1
1
Matrix:
GW WW
DJSULL1
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
02/24/2015 13:23
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:23
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:23
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:23
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:23
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:23
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:23
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:23
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:23
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:23
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:23
DJSULL1
ug/L
0.2
1
EPA 200.8
02/24/2015 13:23
DJSULL1
ug/L
0.3
1
EPA 200.8
02/24/2015 13:23
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:24
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:24
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:24
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:24
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:24
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:24
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:24
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:24
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:24
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:24
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:24
DJSULL1
ug/L
0.2
1
EPA 200.8
02/24/2015 11:24
DJSULL1
ug/L
0.3
1
EPA 200.8
02/24/2015 11:24
DJSULL1
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
02/19/201515:07
GHUTCHI
mg/L
0.1
1
SM5310C/EPA9060A
02/23/201517:31
TJA7067
mg/L
5
1
SM2540D
02/16/201511:45
GHUTCHI

Certificate of Laboratory Analysis Page 6 of 39
This report shall not be reproduced, except in full.
Order # J15020366
Site: MW 11 D
Collection Date: 12 -Feb -15 2:05 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 300.0
02/19/2015 13:34
Vendor Parameter
Complete
EPA 300.0
02/19/2015 13:34
NITRITE + NITRATE (COLORIMETRIC)
1
EPA 245.1
Nitrite + Nitrate (Colorimetric)
2.3
mg-N/L
0.02
INORGANIC IONS BY IC
ACPAYNE
1
EPA 200.7
Chloride
130
mg/L
2
Sulfate
22
mg/L
1
MERCURY (COLD VAPOR) IN WATER
MHH7131
1
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
02/18/2015 09:46
MHH7131
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
EPA 200.7
02/18/2015 09:46
MHH7131
Aluminum (AI)
0.032
mg/L
0.005
Barium (Ba)
0.238
mg/L
0.005
Boron (B)
0.090
mg/L
0.05
Iron (Fe)
1.76
mg/L
0.01
Manganese (Mn)
0.551
mg/L
0.005
Strontium (Sr)
0.385
mg/L
0.005
Zinc (Zn)
0.016
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
02/20/2015 11:36
MHALL3
Calcium (Ca)
50.0
mg/L
0.1
Magnesium (Mg)
16.5
mg/L
0.005
Potassium (K)
5.41
mg/L
0.1
Sodium (Na)
33.0
mg/L
0.5
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.214
mg/L
0.005
Barium (Ba)
0.242
mg/L
0.005
Boron (B)
0.088
mg/L
0.05
Iron (Fe)
1.87
mg/L
0.01
Manganese (Mn)
0.503
mg/L
0.005
Strontium (Sr)
0.383
mg/L
0.005
Zinc (Zn)
0.018
mg/L
0.005
Sample #: 2015004086
Matrix: GW WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
2
EPA 353.2
02/14/2015 11:57
TLINN
20
EPA 300.0
02/19/2015 13:34
BGN9034
10
EPA 300.0
02/19/2015 13:34
BGN9034
1
EPA 245.1
02/20/2015 10:04
TLINN
1
EPA 245.1
02/25/2015 11:16
ACPAYNE
1
EPA 200.7
02/18/2015 09:46
MHH7131
1
EPA 200.7
02/18/2015 09:46
MHH7131
1
EPA 200.7
02/18/2015 09:46
MHH7131
1
EPA 200.7
02/18/2015 09:46
MHH7131
1
EPA 200.7
02/18/2015 09:46
MHH7131
1
EPA 200.7
02/18/2015 09:46
MHH7131
1
EPA 200.7
02/18/2015 09:46
MHH7131
10
EPA 200.7
02/18/2015 12:36
MHH7131
1
EPA 200.7
02/18/2015 12:36
MHH7131
1
EPA 200.7
02/18/2015 12:36
MHH7131
10
EPA 200.7
02/18/2015 12:36
MHH7131
1
EPA 200.7
02/20/2015 11:36
MHALL3
1
EPA 200.7
02/20/2015 11:36
MHALL3
1
EPA 200.7
02/20/2015 11:36
MHALL3
1
EPA 200.7
02/20/2015 11:36
MHALL3
1
EPA 200.7
02/20/2015 11:36
MHALL3
1
EPA 200.7
02/20/2015 11:36
MHALL3
1
EPA 200.7
02/20/2015 11:36
MHALL3

Certificate of Laboratory Analysis Page 7 of 39
This report shall not be reproduced, except in full.
Order # J15020366
Site: MW 11 D
Sample #: 2015004086
Collection Date: 12 -Feb -15 2:05 PM
Matrix: GW
WW
Analyte
Result
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
DISSOLVED METALS BY ICP -MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 13:38
DJSULL1
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 13:38
DJSULL1
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 13:38
DJSULL1
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 13:38
DJSULL1
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 13:38
DJSULL1
Cobalt (Co)
4.71
ug/L
1
1
EPA 200.8
02/24/2015 13:38
DJSULL1
Copper (Cu)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 13:38
DJSULL1
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 13:38
DJSULL1
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 13:38
DJSULL1
Nickel (Ni)
3.51
ug/L
1
1
EPA 200.8
02/24/2015 13:38
DJSULL1
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 13:38
DJSULL1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
02/24/2015 13:38
DJSULL1
Vanadium (V) Low Level
0.421
ug/L
0.3
1
EPA 200.8
02/24/2015 13:38
DJSULL1
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
ug/L
1
1
EPA 200.8
02/24/2015 11:44
DJSULL1
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 11:44
DJSULL1
Beryllium (Be)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 11:44
DJSULL1
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 11:44
DJSULL1
Chromium (Cr)
1.07
ug/L
1
1
EPA 200.8
02/24/2015 11:44
DJSULL1
Cobalt (Co)
4.21
ug/L
1
1
EPA 200.8
02/24/2015 11:44
DJSULL1
Copper (Cu)
1.10
ug/L
1
1
EPA 200.8
02/24/2015 11:44
DJSULL1
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 11:44
DJSULL1
Molybdenum (Mo)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 11:44
DJSULL1
Nickel (Ni)
3.70
ug/L
1
1
EPA 200.8
02/24/2015 11:44
DJSULL1
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
02/24/2015 11:44
DJSULL1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
02/24/2015 11:44
DJSULL1
Vanadium (V) Low Level
1.21
ug/L
0.3
1
EPA 200.8
02/24/2015 11:44
DJSULL1
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
350
mg/L
25
1
SM2540C
02/19/201515:07
GHUTCHI
Total Carbon
TOC
0.905
mg/L
0.1
1
SM5310C/EPA9060A
02/23/201517:31
TJA7067
TOTAL SUSPENDED SOLIDS
TSS
<5
mg/L
5
1
SM2540D
02/16/2015 11:45
GHUTCHI

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020366
Site: MW 14BR
Collection Date: 13 -Feb -15 11:00 AM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy Labs)
EPA 300.0
02/19/2015 13:51
Vendor Parameter
Complete
EPA 300.0
02/19/2015 13:51
NITRITE + NITRATE (COLORIMETRIC)
1
EPA 245.1
Nitrite + Nitrate (Colorimetric)
0.822
mg-N/L
0.01
INORGANIC IONS BY IC
ACPAYNE
1
EPA 200.7
Chloride
6.9
mg/L
0.1
Sulfate
160
mg/L
2
MERCURY (COLD VAPOR) IN WATER
MHH7131
1
Mercury (Hg)
< 0.05
ug/L
0.05
Mercury Dissolved (cold vapor) in Water (Filtered)
02/18/2015 09:41
MHH7131
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
EPA 200.7
02/18/2015 09:41
MHH7131
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
0.093
mg/L
0.005
Boron (B)
0.422
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
0.220
mg/L
0.005
Strontium (Sr)
0.295
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
UNDIGESTED METALS BY ICP
EPA 200.7
02/20/2015 11:40
MHALL3
Calcium (Ca)
73.3
mg/L
0.1
Magnesium (Mg)
14.8
mg/L
0.005
Potassium (K)
6.33
mg/L
0.1
Sodium (Na)
13.6
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.070
mg/L
0.005
Barium (Ba)
0.093
mg/L
0.005
Boron (B)
0.421
mg/L
0.05
Iron (Fe)
0.076
mg/L
0.01
Manganese (Mn)
0.216
mg/L
0.005
Strontium (Sr)
0.295
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
Sample #: 2015004087
Matrix: GW WW
Page 8 of 39
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1
EPA 353.2
02/14/2015 11:52
TLINN
1
EPA 300.0
02/19/2015 13:51
BGN9034
20
EPA 300.0
02/19/2015 13:51
BGN9034
1
EPA 245.1
02/20/2015 10:11
TLINN
1
EPA 245.1
02/25/2015 11:19
ACPAYNE
1
EPA 200.7
02/18/2015 09:41
MHH7131
1
EPA 200.7
02/18/2015 09:41
MHH7131
1
EPA 200.7
02/18/2015 09:41
MHH7131
1
EPA 200.7
02/18/2015 09:41
MHH7131
1
EPA 200.7
02/18/2015 09:41
MHH7131
1
EPA 200.7
02/18/2015 09:41
MHH7131
1
EPA 200.7
02/18/2015 09:41
MHH7131
10
EPA 200.7
02/18/2015 12:40
MHH7131
1
EPA 200.7
02/18/2015 12:40
MHH7131
1
EPA 200.7
02/18/2015 12:40
MHH7131
1
EPA 200.7
02/18/2015 12:40
MHH7131
1
EPA 200.7
02/20/2015 11:40
MHALL3
1
EPA 200.7
02/20/2015 11:40
MHALL3
1
EPA 200.7
02/20/2015 11:40
MHALL3
1
EPA 200.7
02/20/2015 11:40
MHALL3
1
EPA 200.7
02/20/2015 11:40
MHALL3
1
EPA 200.7
02/20/2015 11:40
MHALL3
1
EPA 200.7
02/20/2015 11:40
MHALL3

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020366
Site: MW 14BR
Collection Date: 13 -Feb -15 11:00 AM
Analyte
Result
DISSOLVED METALS BY ICP -MS
Sample #:
Antimony (Sb)
< 1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
< 1
Lead (Pb)
< 1
Molybdenum (Mo)
5.69
Nickel (Ni)
< 1
Selenium (Se)
18.2
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
< 0.3
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
<1
Arsenic (As)
< 1
Beryllium (Be)
< 1
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Cobalt (Co)
< 1
Copper (Cu)
<1
Lead (Pb)
< 1
Molybdenum (Mo)
5.88
Nickel (Ni)
< 1
Selenium (Se)
16.5
Thallium (TI) Low Level
< 0.2
Vanadium (V) Low Level
0.528
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
TOTAL DISSOLVED SOLIDS
ug/L
TDS
350
Total Carbon
02/24/2015 13:43
TOC
0.940
TOTAL SUSPENDED SOLIDS
1
TSS
< 5
Page 9 of 39
ug/L
1
1
Sample #:
2015004087
DJSULL1
ug/L
1
1
Matrix:
GW WW
DJSULL1
Units Qualifiers
RDL
DF
Method
Analysis Date/Time
Analyst
ug/L
1
1
EPA 200.8
02/24/2015 13:43
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:43
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:43
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:43
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:43
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:43
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:43
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:43
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:43
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:43
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 13:43
DJSULL1
ug/L
0.2
1
EPA 200.8
02/24/2015 13:43
DJSULL1
ug/L
0.3
1
EPA 200.8
02/24/2015 13:43
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:49
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:49
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:49
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:49
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:49
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:49
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:49
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:49
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:49
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:49
DJSULL1
ug/L
1
1
EPA 200.8
02/24/2015 11:49
DJSULL1
ug/L
0.2
1
EPA 200.8
02/24/2015 11:49
DJSULL1
ug/L
0.3
1
EPA 200.8
02/24/2015 11:49
DJSULL1
Vendor Method
V_SHEALY
Vendor Method
V_ELE1
mg/L
25
1
SM2540C
02/19/201515:07
GHUTCHI
mg/L
0.1
1
SM5310C/EPA9060A
02/23/201517:31
TJA7067
mg/L
5
1
SM2540D
02/16/201511:45
GHUTCHI

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020366
Site: Equipment Blank
Collection Date: 13 -Feb -15 12:00 PM
Analyte
Result
Units
Qualifiers RDL
ALKALINITY - (Analysis Performed by Shealy
Labs)
1 EPA 300.0
Vendor Parameter
Complete
1 EPA 300.0
02/19/2015 11:46
NITRITE + NITRATE (COLORIMETRIC)
1 EPA 245.1
02/20/2015 10:13
Nitrite + Nitrate (Colorimetric)
< 0.01
mg-N/L
0.01
INORGANIC IONS BY IC
02/18/2015 13:15
MHH7131
1 EPA 200.7
Chloride
< 0.1
mg/L
0.1
Sulfate
< 0.1
mg/L
0.1
MERCURY (COLD VAPOR) IN WATER
02/20/2015 11:44
MHALL3
Mercury (Hg)
< 0.05
ug/L
0.05
UNDIGESTED METALS BY ICP
MHALL3
1 EPA 200.7
02/20/2015 11:44
Calcium (Ca)
0.017
mg/L
0.01
Magnesium (Mg)
< 0.005
mg/L
0.005
Potassium (K)
< 0.1
mg/L
0.1
Sodium (Na)
< 0.05
mg/L
0.05
TOTAL RECOVERABLE METALS BY ICP
02/24/2015 11:54
DJSULL1
Aluminum (AI)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Page 10 of 39
Sample #: 2015004088
Matrix: GW WW
DF Method Analysis Date/Time Analyst
Vendor Method
V_SHEALY
1 EPA 353.2
02/14/2015 11:53
TLINN
1 EPA 300.0
02/19/2015 11:46
BGN9034
1 EPA 300.0
02/19/2015 11:46
BGN9034
1 EPA 245.1
02/20/2015 10:13
TLINN
1 EPA 200.7
02/18/2015 13:15
MHH7131
1 EPA 200.7
02/18/2015 13:15
MHH7131
1 EPA 200.7
02/18/2015 13:15
MHH7131
1 EPA 200.7
02/18/2015 13:15
MHH7131
1 EPA 200.7
02/20/2015 11:44
MHALL3
1 EPA 200.7
02/20/2015 11:44
MHALL3
1 EPA 200.7
02/20/2015 11:44
MHALL3
1 EPA 200.7
02/20/2015 11:44
MHALL3
1 EPA 200.7
02/20/2015 11:44
MHALL3
1 EPA 200.7
02/20/2015 11:44
MHALL3
1 EPA 200.7
02/20/2015 11:44
MHALL3
1 EPA 200.8
02/24/2015 11:54
DJSULL1
1 EPA 200.8
02/24/2015 11:54
DJSULL1
1 EPA 200.8
02/24/2015 11:54
DJSULL1
1 EPA 200.8
02/24/2015 11:54
DJSULL1
1 EPA 200.8
02/24/2015 11:54
DJSULL1
1 EPA 200.8
02/24/2015 11:54
DJSULL1
1 EPA 200.8
02/24/2015 11:54
DJSULL1
1 EPA 200.8
02/24/2015 11:54
DJSULL1
1 EPA 200.8
02/24/2015 11:54
DJSULL1
1 EPA 200.8
02/24/2015 11:54
DJSULL1
1 EPA 200.8
02/24/2015 11:54
DJSULL1
1 EPA 200.8
02/24/2015 11:54
DJSULL1
1 EPA 200.8
02/24/2015 11:54
DJSULL1

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020366
Page 11 of 39
Site: Equipment Blank
Sample #: 2015004088
Collection Date: 13 -Feb -15 12:00
PM
Matrix: GW WW
Analyte
Result
Units Qualifiers
RDL
DF
Method Analysis Date/Time
Analyst
METHANE - (Analysis Performed by
Shealy Labs)
Methane (CH4)
Complete
Vendor Method
V_SHEALY
SULFIDE - (Analysis Performed by
Element One)
Vendor Parameter
Complete
Vendor Method
V_ELE1
TOTAL DISSOLVED SOLIDS
TDS
< 25
mg/L
25
1
SM2540C 02/19/2015 15:07
GHUTCHI
Total Carbon
TOC
0.131
mg/L
0.1
1
SM5310C/EPA9060A 02/26/201512:47
TJA7067
TOTAL SUSPENDED SOLIDS
TSS
< 5
mg/L
5
1
SM2540D 02/16/2015 11:45
GHUTCHI

Certificate of Laboratory Analysis Page 12 of 39
This report shall not be reproduced, except in full.
Order # J15020366
Site: Filter Blank
Collection Date: 12 -Feb -15 1:20 PM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
EPA 245.1
02/25/2015 11:21
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
1
EPA 200.7
02/18/2015 09:50
Aluminum (Al)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
DISSOLVED METALS BY ICP -MS
1
EPA 200.8
02/24/2015 13:48
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015004089
Matrix: GW WW
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
02/25/2015 11:21
ACPAYNE
1
EPA 200.7
02/18/2015 09:50
MHH7131
1
EPA 200.7
02/18/2015 09:50
MHH7131
1
EPA 200.7
02/18/2015 09:50
MHH7131
1
EPA 200.7
02/18/2015 09:50
MHH7131
1
EPA 200.7
02/18/2015 09:50
MHH7131
1
EPA 200.7
02/18/2015 09:50
MHH7131
1
EPA 200.7
02/18/2015 09:50
MHH7131
1
EPA 200.8
02/24/2015 13:48
DJSULL1
1
EPA 200.8
02/24/2015 13:48
DJSULL1
1
EPA 200.8
02/24/2015 13:48
DJSULL1
1
EPA 200.8
02/24/2015 13:48
DJSULL1
1
EPA 200.8
02/24/2015 13:48
DJSULL1
1
EPA 200.8
02/24/2015 13:48
DJSULL1
1
EPA 200.8
02/24/2015 13:48
DJSULL1
1
EPA 200.8
02/24/2015 13:48
DJSULL1
1
EPA 200.8
02/24/2015 13:48
DJSULL1
1
EPA 200.8
02/24/2015 13:48
DJSULL1
1
EPA 200.8
02/24/2015 13:48
DJSULL1
1
EPA 200.8
02/24/2015 13:48
DJSULL1
1
EPA 200.8
02/24/2015 13:48
DJSULL1

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J15020366
Site: Filter Blank
Collection Date: 13 -Feb -15 12:00 PM
Analyte
Result
Units
Qualifiers RDL
Mercury Dissolved (cold vapor) in Water (Filtered)
EPA 245.1
02/25/2015 11:23
Mercury (Hg)
< 0.05
ug/L
0.05
DISSOLVED METALS BY ICP
1
EPA 200.7
02/18/2015 09:54
Aluminum (Al)
< 0.005
mg/L
0.005
Barium (Ba)
< 0.005
mg/L
0.005
Boron (B)
< 0.05
mg/L
0.05
Iron (Fe)
< 0.01
mg/L
0.01
Manganese (Mn)
< 0.005
mg/L
0.005
Strontium (Sr)
< 0.005
mg/L
0.005
Zinc (Zn)
< 0.005
mg/L
0.005
DISSOLVED METALS BY ICP -MS
1
EPA 200.8
02/24/2015 13:53
Antimony (Sb)
< 1
ug/L
1
Arsenic (As)
< 1
ug/L
1
Beryllium (Be)
< 1
ug/L
1
Cadmium (Cd)
< 1
ug/L
1
Chromium (Cr)
< 1
ug/L
1
Cobalt (Co)
< 1
ug/L
1
Copper (Cu)
< 1
ug/L
1
Lead (Pb)
< 1
ug/L
1
Molybdenum (Mo)
< 1
ug/L
1
Nickel (Ni)
< 1
ug/L
1
Selenium (Se)
< 1
ug/L
1
Thallium (TI) Low Level
< 0.2
ug/L
0.2
Vanadium (V) Low Level
< 0.3
ug/L
0.3
Sample #: 2015004098
Matrix: GW WW
Page 13 of 39
DF
Method
Analysis Date/Time
Analyst
1
EPA 245.1
02/25/2015 11:23
ACPAYNE
1
EPA 200.7
02/18/2015 09:54
MHH7131
1
EPA 200.7
02/18/2015 09:54
MHH7131
1
EPA 200.7
02/18/2015 09:54
MHH7131
1
EPA 200.7
02/18/2015 09:54
MHH7131
1
EPA 200.7
02/18/2015 09:54
MHH7131
1
EPA 200.7
02/18/2015 09:54
MHH7131
1
EPA 200.7
02/18/2015 09:54
MHH7131
1
EPA 200.8
02/24/2015 13:53
DJSULL1
1
EPA 200.8
02/24/2015 13:53
DJSULL1
1
EPA 200.8
02/24/2015 13:53
DJSULL1
1
EPA 200.8
02/24/2015 13:53
DJSULL1
1
EPA 200.8
02/24/2015 13:53
DJSULL1
1
EPA 200.8
02/24/2015 13:53
DJSULL1
1
EPA 200.8
02/24/2015 13:53
DJSULL1
1
EPA 200.8
02/24/2015 13:53
DJSULL1
1
EPA 200.8
02/24/2015 13:53
DJSULL1
1
EPA 200.8
02/24/2015 13:53
DJSULL1
1
EPA 200.8
02/24/2015 13:53
DJSULL1
1
EPA 200.8
02/24/2015 13:53
DJSULL1
1
EPA 200.8
02/24/2015 13:53
DJSULL1

H1
Page 14 of 39
Elernent One Onc.
3319-D Carolina Beach Rd.
WHmington, MIC 28412
Phone: [phone]
Fax: [phone]
IN H, 11 iaa.com
REPORT OF ANALYSES
Duke Energy February 20, 2015
Laboratory Services Client Project Name AB GW Assessment water
13339 Hagers Ferry Road Bld. MG03A Client Project Number J15020336
Huntersville, NC 28078 PO Number
Sample Matrix
GW -WW
Sample Type
Grab
Date Received
02/17/2015
Date Analyzed
02/18/2015
Method
SM 4500 S2- D
Time Received
1300
Delivered by
FedEx
Received by
LLB
eOne ID
Duke Energy ID
Parameter
Result
Unit
Dil
DL Date
Time
Sampled
Sampled
24065-1
MW -13D
Sulfide
< 0.1
mg/L
1
0.1 02/12/15
1015
24065-2
MW -11 D
Sulfide
< 0.1
mg/L
1
0.1 02/12/15
1405
24065-3
MW-14BR
Sulfide
< 0.1
mg/L
1
0.1 02/13/15
1100
24065-4
Equipment Blank
Sulfide
< 0.1
mg/L
1
0.1 02/13/15
1200
_ 9
-4 -
Ken griifh, Laboratory Director
24065 Duke Report Packet Compiled by
NC Certifications: DW 37788 and DWQ DENR 604

Page 15 of 39
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lementOne SAMPLE SUBMISSION FORM
TAT 7 BD
Hold Time Expiration 02.19.15 @ 1015 AM
Client: Duke Energy
LIMS No J15020366
Project ID Groundwater Assessment
Sample Identification & Collection Information
Lab fly 10665
Analysis Due Date 02.18.15
Report Due Date 02.26.15
Lab ID
Date Rec:
02.17.15
Analysis Requested
Time Rec:
1300
02.12.15 1015 AM
Rec By
LLB
Lab ID
Client ID
Collection Date Collection Time
Analysis Requested
1
MW -13D
02.12.15 1015 AM
ulfide
2
MW -11 D
02.12.15. 1405.._ .._
PM
ulfid
3
MW -146R _... _ __._..
02.1 3.1 5 1100...
AM
ulfide
4
Equipment Blank
02.13.15 1200 PM
Sulfide
NOTE for Sulfide The MS/MSD spike should approximate 2 to 3 times the sample concentration. If no sulfide detected
at 100 pg/L spike the sample to render the final spike concentration at — 500 pg/L
Lab Communications
SS Page 1 of 1 Prep By / Date
SS by Labeled By / Date Q1 S
2/18/201 10:18:10 AM ID Verification By /Date

METHOD:
ELEMENT ASSAY:
Sulfid(
CLIENT:
Duke
Lab ID#
24062,
Date:
2/18/15
Time Analysis Begun
9:50
Time Analysis Ended
10:40
Analyst:
KAM
X
Y
ug STD
SOLUTION
STD
ABS
0.00
2.50
5.00
7.50
10.00
0.000
0.084
0.163
0.245
0.329
Page 17 of 39
SM 4500 S2- D I ELEMENT ONE
Wave Length 664
1000 ppm Sulfide Standard
Lot # 5010904
w
0.300
0.328
0250
0.03276
Correlation
0.53995006
0.x00
SAMP
ABS
ug PER
ALIQUOT
ALIin mL
ANALYZED
Y
0.,50
ALI in mL
TAKEN
,63
LESS THAN
% SPK REC
0,00
LRB
0.000
0.0000
om
.oee
25
<
0.000
0.00
200
LRB SPK
0.164
X
L
Slope
e
0.03276
Correlation
0.53995006
SAMPLE
1. D.
SAMP
ABS
ug PER
ALIQUOT
ALIin mL
ANALYZED
PREP
VOL in mL
ALI in mL
TAKEN
RESULTS
ug/mL
LESS THAN
% SPK REC
SPIKE
LEVEL
LRB
0.000
0.0000
25
25
25
<
LRB SPK
0.164
4.9940
25
25
25
0.200
100%
5.0
24062
-0.005
0.0000
25
25
25
24063
-0.004
0.0000
25
25
25
<
24063 du
-0.001
0.0000
25
25
25
<
24065-1
-0.002
0.0000
25
25
25
<
24065-1 SPK
0.150
4.5774
25
25
25
0.183
92%
5.0
24065-2
-0.003
0.0000
25
25
25
<
24065-3
0.000
0.0000
25
25
25
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24065-4
-0.002
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0.000
0.0000
25
25
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QC
0.153
4.6667
25
25
25
0.187
93%
5.0
Submiffed for QA/QC-
Date: 2/18/15
By: (Print)
KAM
(sign):

Page 18 of 39
METHOD:
SM 4500 S2- D
ELEMENT ONE
ELEMENT ASSAY:
Sulfide
Spectrophotometer
Wave Len
Length 664
Na2S•9H2OLot#
Sv 1? IoOvM 5
r
UNITS OF ANSWER
DETECTION u '
LIMITSPK
CLIENT:
Lab ID#
LRB
LEVEL u
MAXALIQUOT
Date:
, (
STANDARD conc(ppm)
Time Analysis Begun
0
Time Analysis Ended
i0 i, -JA
Ug 5i
)LUTI
0.00
2.50
5.00
7.50
10.00
Y
I no
STD
ABS
10�y0f d 0,800
J
0.700
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STD ABSORPTION
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750
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1200
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..
SAMPLE
I.D.
SAMP
ABS
ug PER
ALIQUOT
ALI in mL
ANALYZED
PREP
VOL in mL
Slope
ALI in mL
TAKEN
#DIV/01
RESULTS
ug/mL
Correlation
LESS THAN
% SPK REC
#DIV/01
SPIKE
LEVEL
LRB
02000
25
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Submitted for QA/QC-
Date:
25
1
By: (Print)
1
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0%
(sign):
5.0

SHEALY ENVIRONMENTAL SERVICES, INC.
Report of Analysis
Duke Energy
13339 Hagers Ferry Rd
Bldg 7405
Huntersville, NC 28078
Attention: Mary Ann Ogle
Project Name: AB GW Assessment Water
Project Number:J15020366
Lot Number:QB17014
Date Completed:02/25/2015
Grant Wilton
Project Manager
This report shall not be reproduced, except in its entirety, without the written approval of Shealy Environmental Services, Inc.
The following non -paginated documents are considered part of this report: Chain of Custody Record and Sample Receipt Checklist.
*QB17014*
Shealy Environmental Services, Inc. Page: 1 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
SC DHEC No: 32010 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Duke Energy
Lot Number: QB17014
Project Name: AB GW Assessment Water
Project Number: J15020366
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary following this Case Narrative. The sample
receiving date is documented in the header information associated with each sample.
All results listed in this report relate only to the samples that are contained within this report.
Sample receipt, sample analysis, and data review have been performed in accordance with the most current approved NELAC standards, the
Shealy Environmental Services, Inc. ("Shealy") Quality Assurance Management Plan (QAMP), standard operating procedures (SOPS), and Shealy
policies. Any exceptions to the NELAC standards, the QAMP, SOPs or policies are qualified on the results page or discussed below.
If you have any questions regarding this report please contact the Shealy Project Manager listed on the cover page
Shealy Environmental Services, Inc. Page: 2 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
Sample Summary
Duke Energy
Lot Number: QB17014
Project Name: AB GW Assessment Water
Project Number: J15020366
Sample Number
Sample ID
Matrix
Date Sampled
Date Received
001
2015004084
Aqueous
02/12/20151015
02/17/2015
002
2015004086
Aqueous
02/12/20151405
02/17/2015
003
2015004087
Aqueous
02/12/20151100
02/17/2015
004
2015004088
Aqueous
02/12/20151200
02/17/2015
(4 samples)
Shealy Environmental Services, Inc. Page: 3 of 12
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SHEALY ENVIRONMENTAL SERVICES, INC.
Executive Summary
Duke Energy
Lot Number: QB17014
Project Name: AB GW Assessment Water
Project Number: J15020366
Sample Sample ID Matrix Parameter Method Result Q Units Page
001
2015004084
Aqueous
Alkalinity
SM 2320B-
89
mg/L
5
001
2015004084
Aqueous
Bicarbonate Alkalinity
SM 2320B-
89
mg/L
5
002
2015004086
Aqueous
Alkalinity
SM 2320B-
50
mg/L
7
002
2015004086
Aqueous
Bicarbonate Alkalinity
SM 2320B-
50
mg/L
7
003
2015004087
Aqueous
Alkalinity
SM 2320B-
98
mg/L
9
003
2015004087
Aqueous
Bicarbonate Alkalinity
SM 2320B-
97
mg/L
9
(6 detections)
Shealy Environmental Services, Inc. Page: 4 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QB17014-001
Description: 2015004084 Matrix: Aqueous
Date Sampled:02/12/2015 1015 Project Name: AB GW Assessment Water
Date Received: 02/17/2015 Project Number: J15020366
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 02/23/2015 1808
TAF 68537
1
(Bicarbonate ) SM 2320B-2011
1 02/23/2015 1808
TAF 02/23/2015 1808
1
(Carbonate Al) SM 2320B-2011
1 02/23/2015 1808
TAF 02/23/2015 1808
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
89
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
89
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 5 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QB17014-001
Description: 2015004084 Matrix: Aqueous
Date Sampled:02/12/2015 1015 Project Name: AB GW Assessment Water
Date Received: 02/17/2015 Project Number: J15020366
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 02/19/2015 1434 DCS 68226
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QB17014-002
Description: 2015004086 Matrix: Aqueous
Date Sampled:02/12/2015 1405 Project Name: AB GW Assessment Water
Date Received: 02/17/2015 Project Number: J15020366
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 02/23/2015 1812
TAF 68537
1
(Bicarbonate ) SM 2320B-2011
1 02/23/2015 1812
TAF 02/23/2015 1812
1
(Carbonate Al) SM 2320B-2011
1 02/23/2015 1812
TAF 02/23/2015 1812
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
50
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
50
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 7 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QB17014-002
Description: 2015004086 Matrix: Aqueous
Date Sampled:02/12/2015 1405 Project Name: AB GW Assessment Water
Date Received: 02/17/2015 Project Number: J15020366
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 02/19/2015 1445 DCS 68226
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 8 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QB17014-003
Description: 2015004087 Matrix: Aqueous
Date Sampled:02/12/2015 1100 Project Name: AB GW Assessment Water
Date Received: 02/17/2015 Project Number: J15020366
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 02/23/2015 1819
TAF 68537
1
(Bicarbonate ) SM 2320B-2011
1 02/23/2015 1819
TAF 02/23/2015 1819
1
(Carbonate Al) SM 2320B-2011
1 02/23/2015 1819
TAF 02/23/2015 1819
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
98
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
97
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QB17014-003
Description: 2015004087 Matrix: Aqueous
Date Sampled:02/12/2015 1100 Project Name: AB GW Assessment Water
Date Received: 02/17/2015 Project Number: J15020366
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 02/19/2015 1500 DCS 68226
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals
Client: Duke Energy Laboratory ID: QB17014-004
Description: 2015004088 Matrix: Aqueous
Date Sampled:02/12/2015 1200 Project Name: AB GW Assessment Water
Date Received: 02/17/2015 Project Number: J15020366
Run Prep Method
Analytical Method
Dilution Analysis Date
Analyst Prep Date Batch
1
(Alkalinity) SM 2320B-2011
1 02/23/2015 1824
TAF 68537
1
(Bicarbonate ) SM 2320B-2011
1 02/23/2015 1824
TAF 02/23/2015 1824
1
(Carbonate Al) SM 2320B-2011
1 02/23/2015 1824
TAF 02/23/2015 1824
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
Alkalinity
SM 2320B-20
ND
10
mg/L
1
Bicarbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
Carbonate Alkalinity
SM 2320B-20
ND
10
mg/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 11 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane
Client: Duke Energy Laboratory ID: QB17014-004
Description: 2015004088 Matrix: Aqueous
Date Sampled:02/12/2015 1200 Project Name: AB GW Assessment Water
Date Received: 02/17/2015 Project Number: J15020366
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 RSK - 175 1 02/19/2015 1513 DCS 68226
CAS Analytical
Parameter Number Method Result Q PQL Units Run
Methane 74-82-8 RSK - 175 ND 10 ug/L 1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
NO = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 12 of 12
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

QC Summary
Shealy Environmental Services, Inc. QC Data for Lot Number: QB17014
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - Ii
Sample ID: QQ68537-001 Matrix: Aqueous
Batch: 68537
Analytical Method: SM 2320B-2011
Parameter Result Q Dil PQL Units Analysis Date
Alkalinity ND 1 10 mg/L 02/23/20151622
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QB17014
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Inorganic non-metals - LCS
Sample ID: QQ68537-002 Matrix: Aqueous
Batch: 68537
Analytical Method: SM 2320B-2011
Spike
Amount Result % Rec
Parameter (mg/L) (mg/L) Q Dil % Rec Limit Analysis Date
Alkalinity 100 97 1 97 90-110 02/23/20151628
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QB17014
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - MB
Sample ID: QQ68226-001 Matrix: Aqueous
Batch: 68226
Analytical Method: RSK - 175
Parameter Result Q Dil PQL Units Analysis Date
Methane ND 1 10 ug/L 02/19/20151355
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QB17014
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCS
Sample ID: QQ68226-002 Matrix: Aqueous
Batch: 68226
Analytical Method: RSK - 175
Spike
Amount Result % Rec
Parameter (ug/L) (ug/L) Q Dil % Rec Limit Analysis Date
Methane 150 130 1 83 70-130 02/19/20151214
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QB17014
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

Methane - LCSD
Sample ID: QQ68226-003 Matrix: Aqueous
Batch: 68226
Analytical Method: RSK - 175
Spike
Amount Result % Rec % RPD
Parameter (ug/L) (ug/L) Q Dil % Rec % RPD Limit Limit Analysis Date
Methane 150 120 1 80 3.6 70-130 30 02/19/20151329
PQL = Practical quantitation limit P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL + = RPD is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Note: Calculations are performed before rounding to avoid round -off errors in calculated results
Shealy Environmental Services, Inc. QC Data for Lot Number: QB17014
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

SHEALY ENVIRONMENTAL SERVICES, INC.
filncaly [nvimmn"WIl smicm' lnr,-
Docurnenl Nlla ber. F -AD -016
Rcvi*nNam1) r_ 16
Pap IofI
Rc0lw.-s Date: 07il5r ] 4
E46fievdyc Date: ] ].'67, t4
Sample Receipt Checklist (•SRQ
Client. �.`� Cooler lr►1;pected byldate:.e+', L1t #:0
r a.
Mrran. (if receipt- [] SEM ❑ Client ❑ UPS L F'edhx ❑ Airborne F.xp ❑ Other
Yes No 7 1
1 L Were mstody seals prey&mt on the wolve7
Ycs No NA LJ
I �. If eustvdY seals were Rtlt rw°erc they intact a,n�l unbroken',
.I
Gaoler ID/Original temperature upon receiptiDeri d (corrected) temperature upon receipt=
/ 1--o L, C> oC I � ,r f °C l ! °C
Method: 27'Temperature lank ❑,against Bottles TR Gun IIS: 44 IR feud Correction FartOT: °C
Method of coolant: Wei Ioe ❑ slue Ice ❑ , Ice ❑ None
— 3. If temperature of any cooler weeded 6.00C, was Project Mailger notifitd?
PM notified by SRC, phone, note (circle cane), other:
4'rti ❑ NO ❑ KA
(For coolm receiver] vias wirmlncrcial courier, PINS are to be ltotifiied
irni-ned iate.lv_)
Yes ❑ No NA
4_ Is the commercial couriers Skislip srrached to this fdrrn7
Yes W No
5, Were proper oustod y procedurtti �LG�IU7l�liitil:G4�?r��Gi}CLI f�JiIL3u'C��?
5a Were saran ley Felin aislled c.lientty canunercial courier"?
1Es No TTA
lies t+lo ❑
Fs_ V4'eae sample IDs lista] on #hn tC1C7
yesErNo
7. Iklere nMle IDs listed on al11 sample contairim?
Yes No ❑
&. Was collection dare & time listed nn the COC'?
9. Was collecti.au date & time Iisted on Fall sam I.e contaliner5?
Yom Nw+ ❑
Y� ale ❑
-.
1t1. Did all wnft er label information D, dale, time agree wsril the CCC?
Nu ❑
11. Were w is tie he anued listed on the COC? _
12. Did all sawn les arrive in the propet- corl7n. ers 1pr each test`°
Nu ❑
No ❑
4Ves
13. Did all containers arriae in mid condition unhrtlken, lid;a cm, eft)?
N13
14. Was aduWasam le volume available?
� o
15. Wcre afl samples romivud within Y2 the holding time or 4:3 hours, whichever
r Crxncs first?
16.. Wee an sarn les cIDntainers Missing?
I
Yes ❑ No
Yrs ❑ Iv
Yes ❑ No 2' NAS
17. 'R'erc there any axvcss o-aamplcs noL listed on COC? �
18 Were bubbles pmwnt>° ea -sine" 'A"or 6mm in 4iamererf in an A'YOAviat►ls'?
Yes No Nei
19. Were all metaled]&GJHEI'1Vnutri,cnt man lens received ata H of ?
Yes ❑ No ❑ NA LF
20. Were all cyanide and/or sulfide sum les received ata pR>12?
Y E] W. E] N
1 1,11'ere allalTgalicahle NH341TI(Nicyanidelphenol (eO.2mglL) samples fine of
residmi cblrlrine?
Ycs Tho '�A
22. Ti'k'e rc collection temperaturcs documented on the COC for NC Gln les?
Yes ❑ No ❑ NA 2Te
23_ Were elioni relrlaukslrcquusts (i -e. requested dilutions, MS/ MSD designations,
M. F.) oarrectl transcribed from the CO into the car mant section in LIMS;�
yes
24, Was the quote number used taken from t1w container labrl?
Sample Yreservatlon (Must be completed for ally sample(s) incorrectly prewrVed or with hca dsTmix-)
Samples) were revived incorrectly preserved and were adjusted
axccordin lv in sawn le rrmeivin . with (Hi us usirl SIAL ilk
Sample(s)
were received with bubbles>6 nidi it diaa,rnuter.
Sate lir -s
wwre received with TFCC >0.2 TgtL if 921 i s No
ST_: Drinking Watm Project Sample(s) pH verified bo be > 2 by Dsto;
Sam l s were not received at a pH vrr2 and were adjusted accordirn I usin qM
Sam le labels applied by-,
Verified b ' Daae: --,
f. omtr>lents:
Shealy Environmental Services, Inc.
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com Level 1 Report v2.1

CHAINOF CUSTODY RECORD AND ANALYSIS REQUEST FORM
Duke Energy
Duke Energy Analytical Laborato
I
Analytical Laboratory
Mail Code MG03A2 (Building 7405)
j
13339 Hager, Ferry Rd
i Chain of Custody &
H.mer-ille, N. C. 28078
Sample Log
[phone]
j _ _ _ _ __________
_ _ _ _ __ _
Fax [phone]
Project Name AB GW Assessment water
Phone No:
Client
Fax No:
Drinking Water _ UST
980-875-5
Business Unit:
Procea,:
Reap. Center 1
Project to:
Activity In:
Mail Code:
Itration (0.45 um)
b Unfiltered
MG03A3
waterbody: Station:
ry i '•
Analytical Laborato
UseOnly
I iOrde�7
Matrix GWWW
—
Sample. Originating From INC_
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GPS Location Collection Information E a
Sc
:Logged gy Dat9,B l e C� J
<
SAMPLE PROGRAM
'c
•J
Ground Water NPDES
Date Time Signature 0�
Drinking Water _ UST
SH EALY
i
RCRA Waste
Relinquished gy DatelTime
Cooler Temp�CL--_.
1
PO 1142089
Itration (0.45 um)
b Unfiltered
1
Preservative Ice
Ice Ice IcesH2504 Ice 11..'
1�`o
Element 1 otainer Volume (mL) 2000
40 m1 300 125 500 500
PO 1142133
Container Type PET
glass PET PET PET PET
w
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W- iii- :Z 114 X
Y 1 N
Sample Description or ID ..tomer to complete all appropriate rr w m " C
non -shaded areas.
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GPS Location Collection Information E a
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Page 39 of 39
Page 1 of _1_
DISTRIBUTION
ORIGINAL to LAB, COPY to CLIENT
COC REV DATE 1/22/2015
.4 filtered
500 250
HDPE HDPE
CD
ty
N
N y
ON
T tv
X1a E
1 1
I I
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ze
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0
0
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Filter Blank / L fis 1 1
' 2 1 ' 1 '
a
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RelinguishfABy D te/Time
-/
Accepted By:
Date/Time
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Requested Turnaround
Relinquished gy DatelTime
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`14 Days
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Ace 'DatelThme
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----
7 Days
Seal/Locked By Date/Time
Sealed/Lock Opened By DatelTimeo
n t.
E N
d
48 Hr
Other
Comment.
ELEMENTS by ICP MS (TRM): As, Be, Cd, Co, Cr, Cu, Mo, Ni, Pb, Sb, Se, TI (LL), V (LL)
ELEMENTS by ICP (TRM): Al, Ba, B, Fe, Mn, Sr, Zn ICP Undigested Ca, Mg, K, Na
Hg by 245.1
a
in
_ASAP
`Add. Cost Will Apply
Dissolved metals : all metals ICP, IMS,Hg
v
1
Total E