NC0000396_AS11-Prism-FR_20150823

P R I S M Full -Service Analytical &
Environmental Solutions
LABORATORIES, INC.
NC Division of Water Resources/DW Well Testing
Eric G. Smith
1636 Mail Service Center
Raleigh, NC 27699-1636
NC Certification No. 402
SC Certification No. 99012
NC Drinkinq Water Cert No. 37735
VA Certification No. 460211
DOD ELAP: L -A -B Accredited Certificate No. L2307
ISO/IEC 17025: L -A -B Accredited Certificate No. L2307
Project: Cruz, Ricardo (AS11)
Project No.: AS11
Lab Submittal Date: 03/04/2015
Prism Work Order: 5030079
Case Narrative
03/23/2015
This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample
Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed
according to the referenced methods.
Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case
narrative.
Narrative Notes:
ORP Reading in the field:-243mv.
Please call if you have any questions relating to this analytical report.
Respectfully,
PRISM LABORATORIES, INC.
Robbi A. Jones Reviewed By Robbi A. Jones
President/Project Manager President/Project Manager
Data Qualifiers Key Reference:
J Detected but below the Reporting Limit; therefore, result is an estimated concentration (CLP J -Flag).
BRL Below Reporting Limit
MDL Method Detection Limit
RPD Relative Percent Difference
* Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and
reporting limit indicated with a J.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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PRISM Sample Receipt Summary
�r Full -Service Analytical R
/ environmental Solutions 03/23/2015
LABORATORIES, INC.
Prism Work Order: 5030079
Client Sample ID Lab Sample ID Matrix Date Sampled Date Received
AS11 5030079-01 Water 03/04/15 03/04/15
Samples were received in good condition at 2.2 degrees C unless otherwise noted.
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 2 of 12

�] ISM
`- n n Full -Service Analytical &
P J' V' Environmental Solutions
LABORATORIES INC.
NC Division of Water Resources/DW Well l Project: Cruz, Ricardo (AS11)
Attn: Eric G. Smith
1636 Mail Service Center Project No.: AS11
Raleigh, NC 27699-1636
Field Data
Laboratory Report
03/23/2015
Prism Work Order: 5030079
Laboratory ID Client ID Field Parameter Result
5030079-01 AS11
pH 8.6
Temperature (C) 15.3
Dissolved Oxygen (mg/L) 2.0
Conductivity (umho) 713
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 3 of 12

Laboratory Report
PRISM Full -Service Analytical 03/23/2015
Environmental Solutionss
LABORATORIES, INC.
NC Division of Water Resources/DW Well Te: Project: Cruz, Ricardo (AS11) Client Sample ID: AS11
Attn: Eric G. Smith Prism Sample ID: 5030079-01
1636 Mail Service Center Project No.: AS11 Prism Work Order: 5030079
Raleigh, NC 27699-1636 Sample Matrix: Water Time Collected: 03/04/15 10:55
Time Submitted: 03/04/15 15:15
Parameter
Result
Units
Report
MDL
Dilution
Method
Analysis Analyst
Batch
Limit
Factor
Date/Time
ID
Anions by Ion Chromatography
Chloride
56
mg/L
1.0
0.13
1
300.0
3/9/15 20:17
CDE
P5C0155
Sulfate
340
mg/L
5.0
0.64
5
300.0
3/10/15 9:51
CDE
P5C0155
General Chemistry Parameters
Hexavalent Chromium
BRL
mg/L
0.010
0.0037
1
SM3500-Cr B
3/4/15 16:40
CDE
P5C0097
Total Alkalinity to pH 4.5
13
mg/L
5.0
0.77
1
SM2320 B
316/15 13:50
MES
P5C0131
Total Dissolved Solids
560
mg/L
50
1.4
1
SM2540 C
3/6/15 16:00
CDE
P5C0119
Total Suspended Solids
BRL
mg/L
3.1
1.0
1
SM 2540 D
3/6/15 11:05
EGC
P5C0124
Turbidity
0.29 d
NTU
1.0
0.13
1
180.1
3/5/15 14:15
MES
P5C0101
Carbonate Alkalinity
BRL
mg/L
5.0
0.59
1
SM2320 B
3/6/15 13:50
MES
P5C0134
Bicarbonate Alkalinity
13
mg/L
5.0
0.59
1
SM2320 B
3/6/15 13:50
MES
P5C0133
Total Metals
Aluminum
BRL
mg/L
0.050
0.0069
1
200.8
3/10/15 20:37
BGM
P5C0157
Mercury
BRL
mg/L
0.00020
0.000012
1
245.1
3/17/15 14:35
JAB
P5CO272
Antimony
0.00023 J
mg/L
0.0010
0.000031
1
200.8
3/10/15 20:37
BGM
P5C0157
Arsenic
BRL
mg/L
0.0010
0.00029
1
200.8
3/10/15 20:37
BGM
P5C0157
Barium
0.0056
mg/L
0.0050
0.00015
1
200.8
3/10/15 20:37
BGM
P5C0157
Beryllium
BRL
mg/L
0.0010
0.000061
1
200.8
3/13/15 21:52
BGM
P5C0157
Boron
0.076 J
mg/L
0.50
0.038
1
200.7
3/12/15 18:25
BGM
P5CO200
Cadmium
BRL
mg/L
0.0010
0.000054
1
200.8
3/10/15 20:37
BGM
P5C0157
Calcium
97
mg/L
0.20
0.0095
1
200.7
3/12/15 18:25
BGM
P5CO200
Chromium
BRL
mg/L
0.0010
0.00011
1
200.8
3/10/15 20:37
BGM
P5C0157
Cobalt
BRL
mg/L
0.0010
0.000067
1
200.8
3/10/15 20:37
BGM
P5C0157
Copper
0.0014 j
mg/L
0.0050
0.00020
1
200.8
3/10/15 20:37
BGM
P5C0157
Iron
BRL
mg/L
0.050
0.020
1
200.8
3/10/15 20:37
BGM
P5C0157
Lead
0.00029 1
mg/L
0.0010
0.000047
1
200.8
3/10/15 20:37
BGM
P5C0157
Magnesium
1.0
mg/L
0.10
0.0044
1
200.7
3/12/15 18:25
BGM
P5CO200
Manganese
0.0049 ,1
mg/L
0.0050
0.00051
1
200.8
3/10/15 20:37
BGM
P5C0157
Molybdenum
0.0084
mg/L
0.0020
0.000086
1
200.8
3/13/15 21:52
BGM
P5C0157
Nickel
BRL
mg/L
0.0020
0.00018
1
200.8
3/10/15 20:37
BGM
P5C0157
Potassium
1.6
mg/L
0.50
0.031
1
200.7
3/12/15 18:25
BGM
P5CO200
Selenium
BRL
mg/L
0.0010
0.00049
1
200.8
3/10/15 20:37
BGM
P5C0157
Strontium
0.21
mg/L
0.0010
0.00023
1
200.8
3/10/15 20:37
BGM
P5C0157
Sodium
72
mg/L
0.50
0.025
1
200.7
3/12/15 18:25
BGM
P5CO200
Thallium
BRL
mg/L
0.0010
0.000049
1
200.8
3/10/15 20:37
BGM
P5C0157
Vanadium
BRL
mg/L
0.0050
0.00043
1
200.8
3/10/15 20:37
BGM
P5C0157
Zinc
0.018
mg/L
0.0050
0.0032
1
200.8
3/10/15 20:37
BGM
P5C0157
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 4 of 12

P R I S M EService Analytical &
Environmental Solutions
LABORATORIES, INC.
NC Division of Water Resources/DW Well Te: Project: Cruz, Ricardo (AS 11)
Attn: Eric G. Smith
1636 Mail Service Center Project No: AS11
Raleigh, NC 27699-1636
Total Metals - Quality Control
Level II QC Report
3/23/15
Prism Work Order: 5030079
Time Submitted: 3/4/2015 3:15:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5C0157 - 200.8
Blank (P5C0157-BLK1)
Prepared &Analyzed: 03/10/15
Aluminum
BRL
0.050
mg/L
Antimony
0.000215
0.0010
mg/L
J
Arsenic
BRL
0.0010
mg/L
Barium
BRL
0.0050
mg/L
Beryllium
BRL
0.0010
mg/L
Cadmium
BRL
0.0010
mg/L
Chromium
BRL
0.0010
mg/L
Cobalt
BRL
0.0010
mg/L
Copper
BRL
0.0050
mg/L
Iron
BRL
0.050
mg/L
Lead
0.000206
0.0010
mg/L
J
Manganese
BRL
0.0050
mg/L
Molybdenum
0.000199
0.0020
mg/L
J
Nickel
BRL
0.0020
mg/L
Selenium
BRL
0.0010
mg/L
Strontium
BRL
0.0010
mg/L
Thallium
BRL
0.0010
mg/L
Vanadium
BRL
0.0050
mg/L
Zinc
BRL
0.0050
mg/L
LCS (P5C0157-BSI)
Prepared &Analyzed: 03/10/15
Aluminum
0.914
0.050
mg/L
1.000 91
85-115
Antimony
0.0909
0.0010
mg/L
0.1000 91
85-115
Arsenic
0.0902
0.0010
mg/L
0.1000 90
85-115
Barium
0.0946
0.0050
mg/L
0.1000 95
85-115
Beryllium
0.0923
0.0010
mg/L
0.1000 92
85-115
Cadmium
0.0927
0.0010
mg/L
0.1000 93
85-115
Chromium
0.0930
0.0010
mg/L
0.1000 93
85-115
Cobalt
0.0883
0.0010
mg/L
0.1000 88
85-115
Copper
0.0945
0.0050
mg/L
0.1000 95
85-115
Iron
0.913
0.050
mg/L
1.000 91
85-115
Lead
0.0957
0.0010
mg/L
0.1000 96
85-115
Manganese
0.0887
0.0050
mg/L
0.1000 89
85-115
Molybdenum
0.0924
0.0020
mg/L
0.1000 92
85-115
Nickel
0.0901
0.0020
mg/L
0.1000 90
85-115
Selenium
0.0902
0.0010
mg/L
0.1000 90
85-115
Strontium
0.0928
0.0010
mg/L
0.1000 93
85-115
Thallium
0.0948
0.0010
mg/L
0.1000 95
85-115
Vanadium
0.0912
0.0050
mg/L
0.1000 91
85-115
Zinc
0.0916
0.0050
mg/L
0.1000 92
85-115
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 5 of 12

PRISM Full -Service Analytical
Environmental Solutions
LABORATORIES, INC.
NC Division of Water Resources/DW Well Te: Project: Cruz, Ricardo (AS 11)
Attn: Eric G. Smith
1636 Mail Service Center Project No: AS11
Raleigh, NC 27699-1636
Total Metals - Quality Control
Level II QC Report
3/23/15
Prism Work Order: 5030079
Time Submitted: 3/4/2015 3:15:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5130200 - 200.7
Blank (P5CO200-BLK1)
Prepared &Analyzed: 03/12/15
Boron
BRL
0.50
mg/L
Calcium
BRL
0.20
mg/L
Magnesium
BRL
0.10
mg/L
Potassium
BRL
0.50
mg/L
Sodium
BRL
0.50
mg/L
LCS (P5CO200-BSI)
Prepared &Analyzed: 03/12/15
Boron
4.93
0.50
mg/L
5.000 99
85-115
Calcium
4.98
0.20
mg/L
5.000 100
85-115
Magnesium
5.09
0.10
mg/L
5.000 102
85-115
Potassium
5.03
0.50
mg/L
5.000 101
85-115
Sodium
5.02
0.50
mg/L
5.000 100
85-115
Batch P5CO272 - 245.1
Blank (P5CO272-BLK1)
Prepared &Analyzed: 03/17/15
Mercury
BRL
0.00020
mg/L
LCS (P5CO272-BS1)
Prepared &Analyzed: 03/17/15
Mercury
0.00904
0.00020
mg/L
0.009375 96
85-115
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 6 of 12

PRISM Full -Service Analytical
Environmental Solutions
LABORATORIES, INC.
NC Division of Water Resources/DW Well Te: Project: Cruz, Ricardo (AS 11)
Attn: Eric G. Smith
1636 Mail Service Center Project No: AS11
Raleigh, NC 27699-1636
Anions by Ion Chromatography - Quality Control
Level II QC Report
3/23/15
Prism Work Order: 5030079
Time Submitted: 3/4/2015 3:15:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5CO155 - NO PREP
LCS (P5C0155-BS1) Prepared &Analyzed: 03/09/15
Chloride 42.2 1.0 mg/L 40.00 106 90-110
Sulfate 43.1 1.0 mg/L 40.20 107 90-110
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone]
Page 7 of 12

PRISM Full -Service Analytical
Environmental Solutions
LABORATORIES, INC.
NC Division of Water Resources/DW Well Te: Project: Cruz, Ricardo (AS 11)
Attn: Eric G. Smith
1636 Mail Service Center Project No: AS11
Raleigh, NC 27699-1636
General Chemistry Parameters - Quality Control
Level II QC Report
3/23/15
Prism Work Order: 5030079
Time Submitted: 3/4/2015 3:15:OOPM
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch P5CO097 - NO PREP
Blank (P5C0097-BLK1)
Prepared &Analyzed: 03/04/15
Hexavalent Chromium
BRL 0.010 mg/L
LCS (P5C0097-BS1)
Prepared &Analyzed: 03/04/15
Hexavalent Chromium
0.363 0.010 mg/L
0.4000 91 90-110
Matrix Spike (P5C0097-MS1)
Source: 5030079-01
Prepared & Analyzed: 03/04/15
Hexavalent Chromium
0.362 0.010 mg/L
0.4000 BRL 91 85-115
Matrix Spike Dup (P5C0097-MSD1)
Source: 5030079-01
Prepared & Analyzed: 03/04/15
Hexavalent Chromium
0.367 0.010 mg/L
0.4000 BRL 92 85-115 1 20
Batch P5CO101 - NO PREP
Blank (P5C0101-BLK1) Prepared &Analyzed: 03/05/15
Turbidity 0.160 0.40 NTU J
LCS (P5C0101-BSI) Prepared &Analyzed: 03/05/15
Turbidity 3.77 0.40 NTU 4.000 94 90-110
Duplicate (P5C0101-DUP1) Source: 5030079-01 Prepared & Analyzed: 03/05/15
Turbidity 0.290 0.40 NTU 0.290 0 20 J
Batch P5CO119 - NO PREP
Blank (P5C0119-BLK1) Prepared &Analyzed: 03/06/15
Total Dissolved Solids BRL 50 mg/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 8 of 12

PRISM Full -Service Analytical
Environmental Solutions
LABORATORIES, INC.
NC Division of Water Resources/DW Well Te: Project: Cruz, Ricardo (AS 11)
Attn: Eric G. Smith
1636 Mail Service Center Project No: AS11
Raleigh, NC 27699-1636
General Chemistry Parameters - Quality Control
Analyte
Batch P5130119 - NO PREP
Reporting
Result Limit Units
Level II QC Report
3/23/15
Prism Work Order: 5030079
Time Submitted: 3/4/2015 3:15:OOPM
Spike Source %REC RPD
Level Result %REC Limits RPD Limit Notes
LCS (P5C0119-BS1)
Prepared &Analyzed: 03/06/15
Total Dissolved Solids
Batch P5CO124 - NO PREP
966
50
mg/L
1000 97 90-110
Blank (P5C0124-BLK1)
Prepared & Analyzed: 03/06/15
Total Suspended Solids
LCS (P5C0124-BS1)
BRL
5.0
mg/L
Prepared &Analyzed: 03/06/15
Total Suspended Solids
Batch P5CO131 - NO PREP
480
5.0
mg/L
468.0 104 90-110
Blank (P5C0131-BLK1)
Prepared &Analyzed: 03/06/15
Total Alkalinity to pH 4.5
LCS (P5C0131-BS1)
BRL
5.0
mg/L
Prepared &Analyzed: 03/06/15
Total Alkalinity to pH 4.5
LCS Dup (P5C0131-BSD1)
233
5.0
mg/L
250.0 93 90-110
Prepared & Analyzed: 03/06/15
Total Alkalinity to pH 4.5
Batch P5130133 - NO PREP
250
5.0
mg/L
250.0 100 90-110 7 200
Blank (P5C0133-BLK1)
Prepared &Analyzed: 03/06/15
Bicarbonate Alkalinity
BRL
5.0
mg/L
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
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This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 12
Level II QC Report
PRISMFull -Service Analytical
Environmental Solutions
3/23/15
LABORATORIES, INC.
NC Division of Water Resources/DW Well Te: Project:
Cruz, Ricardo (AS 11)
Prism Work Order: 5030079
Attn: Eric G. Smith
Time Submitted: 3/4/2015 3:15:OOPM
1636 Mail Service Center
Project No: AS11
Raleigh, NC 27699-1636
General Chemistry Parameters - Quality Control
Reporting
Spike Source %REC RPD
Analyte
Result
Limit
Units
Level Result %REC Limits RPD Limit Notes
Batch P5CO133 - NO PREP
LCS (P5C0133-BS1)
Prepared &Analyzed: 03/06/15
Bicarbonate Alkalinity
233
5.0
mg/L
250.0 93 90-110
LCS Dup (P5C0133-BSD1)
Prepared & Analyzed: 03/06/15
Bicarbonate Alkalinity
250
5.0
mg/L
250.0 100 90-110 7 200
Batch P5CO134 - NO PREP
Blank (P5C0134-BLK1)
Prepared & Analyzed: 03/06/15
Carbonate Alkalinity
BRL
5.0
mg/L
Sample Extraction
Data
Prep Method: 200.7
Lab Number Batch
Initial
Final
Date/Time
5030079-01 P5CO200
50 mL
50 mL
03/12/15 7:50
Prep Method: 200.8
Lab Number Batch
Initial
Final
Date/Time
5030079-01 P5C0157
50 mL
50 mL
03/10/15 7:45
5030079-01 P5C0157
50 mL
50 mL
03/10/15 7:45
Prep Method: 245.1
Lab Number Batch
Initial
Final
Date/Time
5030079-01 P5CO272
20 mL
30 mL
03/17/15 9:30
This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc.
449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543
Phone: [phone] - Toll Free Number: 1-800/529-6364 - Fax: [phone] Page 10 of 12

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