WQ0004967_Monitoring - 11-2016_20170103 (2)

GW -59A COMPLIANCE REPORT FORM Permit #--WQQ44 q(o 7
(Submit one each monitoring period with GW-59formx)
1
Enter date monitoring results were due.( I Z - 1 Will this monitoring report (GW -69 and GW -59A)
YES
NO
be submitted after the established due date?
2
Was any required Information missing on the GW -59 report forms?
YES
CO:
IF the answer to question 1 or 2 is "YES" list in the space provided below the well identification numbers) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? yrthe answer is "Yes". contact the Regional ice for guidance.
4
Are any monitored constituents equal to or above the established standards?
YES
NO
ti the answer to question 4 is "NO", skip to section &
If the answer to question 4 is "YES"list the affected wells,individually with constituents) and concentration(s)
exceeding standards in the space provided below.,
MtN Z 4580/L
5
For the constituents Identified In question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) In the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section S.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date fqr each occurrence (for the last two }rears).
MW - z- 2-ZO1S - 78ao 11.7,016 - y 5$O
Il -2Dt5—fofo7Zl
3- zol6 - 2.I 2a
T- zolto - 6
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
H the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem? ,
If the answer to question 7 is NES", describe those actions in the space provided below.
H the answer to question 7 is NO" contact the Regional Office within 90 days., an evaluation may
required to determine the Impact the waste disposal system is havina at the review and compilertce
boundaries surroundina this facility. Failure to i so may subject the permittee to a Notice of Violation.
Naas, and/orpenalties. p
z
ow
O m71
y Cwt -
c�
8
The person completing this portion (GW -59 itoagg report should sign below and submit this
form with GW -59 forms for required wells to eddr4p A"ded at the top of the current GW -59 form.
nth tttir►' __ ._.
51 ature of Permute or Authorized Agent) Date
GW -59A 12/8/2903

SUBM) I t-UKM UN YtLLUVa I'AI'CK UKLT
GROUNDWATER QUALITY MONITORING;
r� rt ifAL1 lotkN )Bf�IA r.. . {
COMPLIANCE REPORT FORM
Certification No.
Date sample analyzed:
Please PontCleadyorrype
FACILITY INFORMATION
PERMIT Number: Expiration Date: • O
�t
A it i'.e
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
Non -Discharge W0004CH01 UIC
Facility Name: L(C
mg/L
Nitrite (NO,) as N 00615
NPDES Other
Permit Name (if different):
Coliform: MF Fecal 31616
/100mL
TYPE OF PERMITTED OPERATION BEING MONITORED
mg/L
Facility Address: g
-t b C �e
Coliform: MF Total 31504
/100mL
g Lagoon ❑ Remediation: Infiltration Gallery
nl Z County SO
U'
fcly; SIm4� Drj
(Nate; Use MPN method for Ng* turbid semPbs)
❑ Spray Field ❑ Remediation:
Contact Person:
/097-ao�3
Telephone#: � -
Dissolved Solids:Total 70300
❑Rotary Distributor E3 Land Application of Sludge
At - Aluminum o11o5
No. of wells to be sampled: '
❑ Water Source Heat Pump ❑ Other:
Well Location/Site Name:
_
m Pem °
Be - Barium 01007
If WELL
SAMPLING INFORMATION n A
W 1i
Date sample collected: I (' 30 -1 ip FIELD ANALYSES:
WAS DR
WELL ID NUMBER (from Permit): I v `
in.
pH 00400: units Temp. 00010: oC
at time of
Well Depth: ft. Well Diameter: _
2546 ft. below measuring point Screened Interval: _ft. to
Depth to Water Level 82546:-
_
_ft. Spec. Cond. 00094: pMhos
sampling.
check
Measuring Point is ft. above land surface
Relative M.P. Elevation: _eft.
Odor 000es:
here:
Volume of water pumped/balled before sampling:
gallons
Appearance
ug/L
Samoles for metals were collected unfiltered: ❑ YES
❑ NO and field acidified: ❑ YES ❑ NO
mg/L
Cu - Copper 01042
LA9URAI UKY [Nt-UKMAI IUK
-Laboratory Name:
Certification No.
Date sample analyzed:
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO,) as N 00615
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616
/100mL
Nitrate (NO3) as N 00620
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P00665
(Nate; Use MPN method for Ng* turbid semPbs)
Orthophosphate 7asb!"i0°`��`
mg/L '
Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300
mg1L
At - Aluminum o11o5
mg/C
pH (Lab) 00403
units
Be - Barium 01007
/L
TOC aoeeo
mg/L
Ca - Calcium oogle JAN V
LU Mg/L
Chloride oog4o
mg/1­
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron oloa5
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate oo945
mg/L
Hg - Mercury 71goo
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 , method #
Total Ammonia costo
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nllrogen: N%as N; Ammonia Nitrogen, Total)
Mn - Manganese olo55
ug/L
, method #
TKN as N 00625
mg/L
NI - Nickel 01087
uglL
, method #
-11 vrv: Ramnvale/
For Remediation Systems Only (Attach Lab Reports):
0
or Authorized AAent) Name and Title- Please Drint or tvoe
GW -59 Rev. 812013
Innuent ictal vwa. --
©'

JJEM AQUEOUS SAMPLE COLLECTION/LAB REPORT FORM (NC CERT 482)
Regulated by NCOENRIDWQ-Groundwater section
To assign test, label shaded area with sample type (C=composite; G=grab)
CHAIN OF CUSTODY
LOCATION ALL JUICE COUNTY HENDERSON SPECIAL INFORMATION(S)
ONITORING WEL
IDI
D NO. MW -t (3 WELLS)
INITIAL TEMP MARCH
I
GRAB 0
,sample time JULY
COMP start
aam ,time NOV
COMP end
date/ time
laiiiiiiiiiia NMI
TEMP @RECEIPT: °C TEMP @RECEIPT: °C
NOTE: THE ABOVE TEMP INDICATES THE TEMP. NOTE: THE ABOVE TEMP INDICATES THE TEMP.
FOR ALL CONTAINERS) WITHIN. FOR ALL CONTAINER(S) WITHIN.
AMMONIA SAMPLES PRESERVED WITH HzSOa, pH=<2.0----YES NO—
AMMONIA SAMPLES NEUTRALIZED WITH NazS03, C(=<0-1 ----YES NO—
FECAL SAMPLES PRESERVED WITH N82S03, Cl=< 0.1 YES NO_
COLLECTED BY: C—L
ALL SAMPLES COLLECTED AND PRESERVED AT TIMEOF-COLLECTION IN PLASTIC CONTAINERS UNLESS NOTED OTHERWISE BY.,
RELINQUISHED BY DATE t TWE RECEIVED BY SPLIT SAMPLE(S) INFO
II-30-I � I y
rfulliGonni
G
PH
ODOR
APPEARANCE
WATER LEVE
By the abate s:ynature t cw;ty that all idnrmatm is accwte to the bur aP my aawledya.
COMMENTS Q means QC not meL Wei I Dr\j c oo(d nOk SOm

SUBMIT FORM ON YELLOW PAPER ONLY
TER QUALITY MONITORING:
E REPORT FORM
Facility Name: A -,Mt_i C e
Permit Name (if different):
Facility Address: e
I, marl are/,,n t%:I1.o "rep 1" �- County & O
act Person: t:TLLav%Aa :fames Teiephone#:&B'&,47-60(.3
Location/Site Name: No. of wells to be sampled: -3
PERMIT Number: Expiration Date: q-01-13
Non -Discharge WQ004r- 44 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FLING INFORMAI ION
L ID NUMBER (from Permit): Date sample collected: II 30- 10
M\1J ' o�
Depth: q5 ft. Well Diameter.in.
T to Water Level 82546: IZ .q ft. below measuring point Screened Interval: y O ft. to 4
wring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: gallons
3les for metals were collected unfiltered: ❑ YES 0 - NO and field acidified: ❑ YES ❑ NO
FIELD ANALYSES: WAS DR`
pH 00400a� units Temp. 00010: Ito .O °C at time of
Spec. Cord. 00094: µMhos sampling,
check
Odor 000as: N ON r? here:
Appearance 1 e A R
80RATORY INFORMATION
as JaWV5
enui
�dCe Adgl Certification No. g�_1I
y
ite sample analyzed: 1(- 3 O - I (� '
i a' S - I
- Laboratory Name: ^-�
(Lo
tRAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
Pb -Lead 01051 ug/L
COD 00335
mg/L
Nitrite (NO2) as N ooe15
mg/L
Coliform: MF Fecal 3161e <-/100mL
Nitrate (NO,) as N 00620 r.} , 3 mg/L
2n -Zinc 01062 mglL
Coliform: MF Total 31504
I100ml- Phosphorus: Total as P ooe85
mg/L
mg1L
Other (Specify Compounds and Concentration Units):
(Note: Use MPN meawo for N9h1r Wrolo samples)
Orthophosphate 70507
lsolved Solids:Total 70300
mg/L
At - Aluminum o11os
mglc
pH (Lab) 00403
units
Be - Barium 01007
ug/L
TOC omeo
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Grease and Oils 00552
mg/L
Cu - Copper 01042
Fe Iron L{ S CS
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Phenol 32730
uglL
mg/L
- 01045
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Sulfate oog4s
tecific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 method #
Total Ammonia ooslo
mg/L
Mg - Magnesium 00927
mg/L
, method #
method #
(Ammonia Nitrogen; N%as N; Ammonia Nit gan. Touo
Mn - Manganese 01055
ug/L
,
TKN as N 00626
mg/L
Ni - Nickel 01057
ug/L
method #
For Remediation Systems Only (Attach Lab Reports):
GW -59 Rev. 812013
Influent Total VOCs:
mg/L
Effluent Total VOCs:
mg/L
VOC Removal%

JJEM AQUEOUS SAMPLE COLLECTION/LAB REPORT FORM (NC CERT 482)
Regulated by WDENRIDWO-Groundwater section
To assign test, label shaded area with sample type (C=composite; G=grab)
CHAIN (1F CI LCTnnV
LOCATION ALL JUICE COUNTY HENDERSON SPECIAL INFORMATION(S
ONITORING WEL
ID NO. MW -2
(3 WELLS)
INITIAL TEMP
PC G C
MARCH
GRAB
sample time
JULY
NOV
COMP start
sam Ie time
COMP end
date/ time
" a+
.,5,'
+
EMP @RECEIPT: 1C
NOTE: THE ABOVE TEMP INDICATES THE TEMP.
FOR ALL CONTAINER(S) WITHIN.
TEMP 9RECEIPT: °C
NOTE: THE ABOVE TEMP INDICATES THE TEMP.
FOR ALL CONTAINER(S) WITHIN,
AMMONIA SAMPLES PRESERVED WITH H2SO4, pH=<2.0 YES NO_
AMMONIA SAMPLES NEUTRALIZED WITH Na2SO3, CI=<0.1 ES NO—
FECAL SAMPLES PRESERVED WITH Na2S03, CI=< 0.1 YES NO_
COLLECTED BY: –7 I– `e
ALL SAMPLES COLLECTED AND PRESERVED AT TIMI OF COLLECTION W PLASTIC CONTAINERS UNLESS NOTED OTHERWISE BY..
RELINQUISHED BY
DATE / TIME
RECEIVED BY SPLIT SAMPLE(S) INF
cfulloomlG
VAT DJ
PH
ODOR Nome
APPEARANCE e A R–
WATER LEVE
By the above signature I certify that all informationis accurate to the best ofmyrknowledge. Q
COMMENTS (Z) means OC not met. `t �� U �� 1 �1 — F7 I

m iossrT Mnoss nnr VP1 1 MA[ PAPPP nNt Y
DWATER QUALITY MONITORING:
IANCE REPORT FORM
TY INFORMATION/'cease rant oreany or type
N
Name: It �1L�C2
Name (if different):
Address: e
rlor<tSn Ili 11? "1900 N C 287'?z County_ O
act Person: laa n) a Ta vyte j Telephone#:
Location/Site Name: No. of wells to be sampled:
SAWLII4l9 nyryKmAI WN
WELL ID NUMBER (from Permit):
Well Depth: a5 ft.
Depth to Water Level 82546: 13 I ft. below measuring point
Measuring Point is ft. above land surface
Volume of water pumped/bailed before sampling:
Samples for metals were collected unfiltered: ❑ YES ❑
Date sample collected: J 1- 30-1(p
Well Diameter. �_ in.
Screened Interval: -Vto -15 ft.
Relative M.P. Elevation: ft.
gallons
NO and
YES
:RMIT Number: Expiration Date: q- Of - 77
in -Discharge W0004CR02 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
0( Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES:
pH ooaoo: _.0 units
Spec. Cond. 00094:
Odor 000e5: _
Appearance _
Temp. 00010:/(P,3 OC at time of
µMhos sampling,
X
LABORATORY INFORMATION
1 �J-1
I of - 5 I%
�{
Laboratory Name: T na 6_ d�ag�rtu•
�
�d L° Ana 1aI.cd ( Certification No. R/g� �b
Date sample analyzed: !
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
ug/L
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L
Pb - Lead o1051
Coliform: MF Fecal 31616 /1
Nitrate (NO3) as N 00820 �- a
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31so4
highlylurblo samples)Orthophosphate
1100mL Phosphorus: Total as P 00685
mg/L
mg/L
Other (Specify Compounds and Concentration Units):
(Note: Use MPN method for
70507
issolved Solids:Total 70300 -
mg/L
Al - Aluminum 01105
mg/LI
pH (Lab) 00403
units
Be - Barium 01007
ug/L
TOC coeso
mg/L
Ca - Calcium 00916
mg/L
VM
Chloride oog4o
mg1L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils oos52
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
ug/L
Fe - Iron o1o4s /
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
32730
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 7873 , method #
Total Ammonia ooelo
mg1L
Mg - Magnesium 00927
mg/L
method #
(ATMNe NKM9811; NHs ae N;Amma�la Nitrogen, Tote[)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625
mg/L
Ni - Nickel 01067
uglL
method #
mo/L VOC Removal%
For Remediation systems only (Arracn Lao Keporrs):
0
or Authorized Anent) Name and Tlae - Plea4e onnt or
GW -59 Rev. 812013
u niurnu iv.ai ...w.
C.
V
�2-

JJF.M AQUEOUS SAMPLE COLLECDONJLAB REPORT FORM (NC CERT 482)
Regulated by NCDENRIDWQ-Gmundwater section
To assign test, label shaded area with sample type (C=composite; G=grab)
is :'inrenw� w.: CHAIN OF CUSTODY
�• ...• /1t�LJYIIiC COUNTY HENDERSON SPECIALINFORLIATIONs
ONITORING WEL
iD t�i0. MW
(3 WELL
INITIAL TEMP
MARCH
GRAB ;y ; ,_
'�"Ji'1!
sam leeime
JULY
COMP start
sam a timeV
COMP and
datel time
EMP @RECEIPT:4 : i °C
TEMP @RECEIPT: o C
NOTE: THE ABOVE TEMP INDICATES THE TEMP.
NOTE: THE ABOVE TEMP INDICATES THE TEMP.
FOR ALL CONTAINERJS) WITHIN.
FOR ALL CONTAINER(S) WITHIN.
AMMONIA SAMPLES PRESERVED WITH H2SO4, pH=<2.0
�S NO—
SAMPLES NEUTRALIZED WITH Na2SOa, Ci=< 0.1
FECAL SES NO_
FECAL SAMPLES PRESERVED WITH NazSOa C1=< 0.1
YES NO_
COLLECTED BY:
ALLSAMPLESCOLLECTEDANDPRESERVEDA TI EOFCOLLECTIONINPLASTICCONTAINERSUNLESS NOTEDOTNERWISEBY:
RELINQUISHED BY
DATE T TIME RECEIVEp BY SPLIT SAMPLE(5j INF
n
J
n
G Lt
PH
ODOR O e
APPEARANCE C
WATER LEVE
3
By Me abase signature I certify that alt information is accurate to the best of my knowledge.
COMMENTS ® — i e b �r = 2
Mans not met
QC

James & James Environmental Management
3801 Asheville Hwy., Hendersonville, NC 28791
OFFICE: (828) 6974NW FAX: [phone]
NC Certified Laboratory NC wastewater #482 NC Drinking Water #37763
All Juice Food & Beverage
352 Jet Street
Hendersonville, NC 28792
Enclosed are the results of the analysis performed by our staff on your samples dated
November 30, 2016. The analysis performed conform to Standard Methods 20m Edition.
Sample ID
Analysis
Method
Result
Units
MDL
Units
Date Run
Analyst
MW -2 K3016
FECAL
9222D
<4.0
c/100mL
<1
c/100ml,
11-30-16
HT/DJ
MW -3K3016
FECAL
9222D
<4.0
c/100mL
<1
c/100mL
I1-30-16
HT/DJ
If you have any questions regarding these results please feel free to contact me at the lab.
Thank you,
C:9::P-4-t 4
Trish Bryan for Juanita James
Lab Manager
[e-mail]

ceAnaly kWe
wnepcNetis.mn
i
December 07, 2016
Ms. Juanita James
James & James Env. Mgmt.
3801 Asheville Hwy.
Hendersonville, NC 28791
RE: Project: All Juice 11/30
Pace Project No.: 92321373
Dear Ms. James:
Pace Analytical Services, LLC
2225 Riverside Or.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 30, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Chris Derouen
[e-mail]
Project Manager
Endosures
r��
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the wntten consent of Pace Analytical Services, LLC.
Page 1 of 12

IceAnaa&*.al a
Project: All Juice 11/30
Pace Project No.: 92321373
Asheville Certification IDs
Pace Ana"cal services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
2225 Riverside Drive, Asheville, NC 28804
FloridalNELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinldng Water Certification #: 37712
CERTIFICATIONS
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analyfical Services, I.I.C. Page 2 of 12

W�4f12�1ICB�e
weses'-0rorhbamrs
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
All Juice 11/30
92321373
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92321373001
Ill
EPA 200.7
SER
1
PASI-A
EPA 353.2
WRC
2
PASI-A
92321373002
MW -3
EPA 200.7
SER
1
PASI-A
EPA 353.2
WRC
2
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 12

awepKshpt:mm
ANALYTICAL RESULTS
Pau Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)2547176
Project: All Juice 11/30
Pace Project No.: 92321373
Sample: MW -2 Lab ID: 92321373001 Collected: 11/30/1610:00 Received: 11/30/1615:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Dual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Iron 4580 ug/L 50.0 1 12/01/1618:50 12/05/1622:12 7439-89-6
353.2 Nitrogen, NO2/NO3 DW Analytical Method: EPA 353.2
Nitrogen, Nitrate 4.3 mg/L 0.020 1 11/30/1618:29
Nitrogen, Nitrite 0.035 mg/L 0.020 1 11/30/1618:29
Date: 12/07/2016 11:10 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 4 of 12

An*&,N*
aws-0eoei"M
ANALYTICAL RESULTS
Pace Analytical Services, LLL
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: All Juice 11/30
Pace Project No.: 92321373
Sample: MW -3 Lab ID: 92321373002 Collected: 11/30/1609:40 Received: 11/30/1615:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Iron 132 ug/L 50.0 1 12/01/1618:50 12/05/1622:15 7439-8M
353.2 Nitrogen, NO2/NO3 DW Analytical Method: EPA 353.2
Nitrogen, Nitrate 3.2 mg/L 0.020 1 11/30/1618:24
Nitrogen, Nitrite ND mg/L 0.020 1 11/30/1618:24
Date: 12/07/2016 11:10 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 12

QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: All Juice 11/30
Pace Project No.: 92321373
QC Batch: 338882 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92321373001, 92321373002
METHOD BLANK: 1879178 Matrix: Water
Associated Lab Samples: 92321373001, 92321373002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Iron ug/L ND 50.0 12/05/1621:34
LABORATORY CONTROL SAMPLE: 1879179
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Iron ug/L 5000 4800 96 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1879180 1879181
MS MSD
92321259001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Iron ug/L 331 5000 5000 5070 5010 95 94 74130 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1879182 1879183
MS MSD
92321374005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Iron ug/L 2.6 5000 5000 7050 7120 89 91 74130 1
mg/L
Rewlla pms@m1ad on this page am In the unka Indicated 0y Me'Unks' column except where an aRemate unh Is presented to Me right of the reauk.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/07/201611:10AM without the written consent of Pace Analytical Services,LLC.
Page 6 of 12

QUALITY CONTROL DATA
Project: Al Juice 11/30
Pace Project No.: 92321373
QC Batch: 338849 Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2 Analysis Description: 353.2 Nitrogen, NO2/NO3 DW
Associated Lab Samples: 92321373001, 92321373002
METHOD BLANK: 1878953
Matrix: Water
Associated Lab Samples:
92321373001, 92321373002
Blank Reporting
MSD
Parameter
Units
Result Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/L
NO 0.020
11/30/1618:13
Nitrogen, Nitrite
mg/L
NO 0.020
11/30/1618:13
Pau Anatytiul Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)2547178
LABORATORY CONTROL SAMPLE: 1878954
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 2.5 2.4 98 90-110
Nitrogen, Nitrite mg/L 1 1.0 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1878955
1878956
MS
MSD
92321171001
Spike
Spike
MS
MSD
MS MSD % Rec
Parameter
Units
Result Conc.
Conc.
Result
Result
% Rec % Rec Limits
RPD Qual
Nitrogen, Nitrate
mg/L
ND 2.5
2.5
2.4
2.5
95 98 90-110
3
Nitrogen, Nitrite
mg/L
NO 1
1
1.2
1.3
125 126 90-110
1 J(M1)
Results prevented an this page are in the units Indicated by the "Unna" column except whem an alternate unit Is, pne saxes! to Its right of the maul
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/07/2016 11:10 AM without the written consent of Pace Analytical Services, LLC.
Page 7 of 12

awrpsphbs:exa
QUALIFIERS
Project: All Juice 11130
Pace Project No.: 92321373
DEFINITIONS
OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL- Reporting Limit.
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
(828)2547178
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unfounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvi%l ether.
A separate vial preserved to a pH of 45 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
ANALYTE QUALIFIERS
J(M1) Estimated Value. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS)
recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 12/0712016 11:10 AM without the written consent of Pace Analytical Services, LLC. Page 8 of 12

mvw.peroleDe.tan
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
All Juice 11/30
92321373
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92321373001
MW -2
EPA 200.7
338882
EPA 200.7
339067
92321373002
MW -3
EPA 200.7
338882
EPA 200.7
339067
92321373001
MW -2
EPA 353.2
338849
92321373002
MW -3
EPA 353.2
338849
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 12/07/2016 11:10 AM without the written consent of Pace Analytical Services, LLC. Page 9 of 12

Laboratory receiving sa les:
Asheville Eden Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑
" I Client Name:,i C i �O# Name:.92321373
)c eS. 0" J4 fJ C' EAV Pro)eR q:
Courier: LJW Ex OUPS OUSPS Client
❑ Commercial Mpace []Other:_ O U1373
Custody seal Present? ❑Yes n No Seals tact? ❑Yes ❑NO
Data/midals Person examining Wntertts:G�
Packing Material, []Bubble Wrap ubble Bags ❑None ❑Other:__- •13, �''
Thermometer: f [ et ❑glue ❑None ❑samples on ie, cooling process Na 1k,
IRGun ID: J Typo of lee:
Correction Factor: Cooler Temp Corrected ('C): Biological Tissue Frozen? ❑Yes []NO ❑N/A
Temp should be above freezing to 6'C
USDA Regulated Sall (❑ N/A, water sample)
NY nrqr!(rhack=psJ? Did samples Originate from a forei n source intematbnal
Including Hawaii and Puerto Rleo)2 as
No
C] YV
Document Name:
Document Revised: Sept, 21, 2016
Sample Condition Upon Recel t SCUR
Pae 1 of2..
Document No.:
Issuing Authority:
A
F-CAR-CS-033-Rev.01
Pace Qualltv Office
Laboratory receiving sa les:
Asheville Eden Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville❑
" I Client Name:,i C i �O# Name:.92321373
)c eS. 0" J4 fJ C' EAV Pro)eR q:
Courier: LJW Ex OUPS OUSPS Client
❑ Commercial Mpace []Other:_ O U1373
Custody seal Present? ❑Yes n No Seals tact? ❑Yes ❑NO
Data/midals Person examining Wntertts:G�
Packing Material, []Bubble Wrap ubble Bags ❑None ❑Other:__- •13, �''
Thermometer: f [ et ❑glue ❑None ❑samples on ie, cooling process Na 1k,
IRGun ID: J Typo of lee:
Correction Factor: Cooler Temp Corrected ('C): Biological Tissue Frozen? ❑Yes []NO ❑N/A
Temp should be above freezing to 6'C
USDA Regulated Sall (❑ N/A, water sample)
NY nrqr!(rhack=psJ? Did samples Originate from a forei n source intematbnal
Including Hawaii and Puerto Rleo)2 as
No
C] YV
comments/Discrepancy:
Chain of Custody Present?
No
A
1.
Samples Arrived within Hold Time?
es
N/A
2.
Short Hold Time Analysis (02 hr.)?
es
N
N A
3. Ala
Rush Turn Around Time Re uested?Y
J&
ONJA
4.
Sufficient Volume?
Y
No
ON/A
5.
Correct Containers Used?
-Pace Containers Used?
es
❑N
o
❑N/A
ON/A
6.
Containers Intact?
Yes
No
ONJA
7.
Samples Field Filtered?
Y
o
ON/A
B. Note if sediment is visible In the dissolved comairter
Sample labels Match COC?
-Includes Date/11me/tD Anal is Matrix:
EfYes
1N
[IN,
❑N/A
9.
Heads ace in VOA Vials (>5.6mm)?
Oyes
ONO
A
10.
Trip Blank Present?
T BlankealsPe
❑Yes
Yes
ONO
nN.
Gfi#11.
/A
CLIENT NOTIFICATION/RESOWTION
Person Contacted:
Comments/Sample
Discrepancy:
Project Manager SCURF Review:
Project Manager SRF Review:
Field Data Regaueor UTes UNo
Date/Time:
Date: (AJtI(a
Date: lSfrri
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina OEHNR Certification Office (i.e.
Out of hold, Incorrect preservative, out of temp, incorrect containers)
Page 10 of 12

*Check mark top half of box if PH and/or dechlorination Project p 'W #:92321373-'
is verified and within the acceptance range for PH: Col
preservation samples. Due Batu 12/07/1®
CLIENT: 97—J8J
**Bottom half of box is to list number of bottles
Document Name:
Document Revised: Sept. 21, 2016
6,N .
o�
Sample Condition U Recei SCUR
P 2.0f 2
Document No.:
Issuing Authority:
F-CAR-CS-033•Rev.01
Pace Quality Office
*Check mark top half of box if PH and/or dechlorination Project p 'W #:92321373-'
is verified and within the acceptance range for PH: Col
preservation samples. Due Batu 12/07/1®
CLIENT: 97—J8J
**Bottom half of box is to list number of bottles
pH Adjustment Log for Preserved Samples
Sample to
Type of Presemadve
PH upon receipt
Date preservation adlusted
Time preservation
adjusted
Amount of Preservative
added
tot N
j
`MFURE
MEM
DER
ii
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0
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®►M■MON►EMO►MENMEN��iii►iii
®EN■M►NNOMME�►�►0
EMM
pH Adjustment Log for Preserved Samples
Sample to
Type of Presemadve
PH upon receipt
Date preservation adlusted
Time preservation
adjusted
Amount of Preservative
added
tot N
Page 11 of 12

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CHAIN-OF-CUSTODY If Ana"cal Request Document
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