WQ0033677_Monitoring - 11-2016_20161230 (2)

A' -
GROUNDWATER QUALITY 19CINITORING:
COMPLIANCE REPORT FORM�FACILITY
�� please �iinl ClEnd; ,o, Type i
n 0ERMIIT Number: /� �, " j- Expiration Date:
Facility Name: C)'jl�, yyt g,8Q�?Pt _ G.� _ Non-Discharge 1/ UIC
Permit Name (if different): T _ V
NPDES Other
Facility Address: o %'✓ l'P in9A� TYPs. E OF PERMITTED .OPERATION BEING MONITORED
County (,I r B ❑ L oon
❑ Remediation: Infiltration Gallery
//^a^ r �" L!� Spray Field ❑ Remediation:
Contact Person: f GtJ• l��►��5 Telephone;t;E:���g� ��V �%8B Rotary Qistribtitor, ❑
Well Location/Site Name: Y� — ' .
ry Land Application of Sludge
sy/ No. pf wails to 6e sampled: ❑.Water Source Heat Pump El Other:
SAMPLING INFORMATION
f If WELL
ELL ID NUMBER(from Permit): Date sample collected: ��%b %�y FIELD ANALYSES: WAS.
Well DeI the _ft i Well Diameter: In. (-� o
`� ' pH (punits . Temp... ( C DRY at
Depth to Water Level I Screened Interval: ft. to g�j ft. Spec. Cond. f � _I Mhos time of
P f% ft below measuring poinE,
Measuring Point is ,ft albove;land sr ace Relativi: M.P. Elevation: ft,. Odor sampling,
Volume of water pumped/bailed:before stnpitng ( ; 9. Illons check
f.. . e_ .
,, I Appearance (�', eqf here:❑
Samples for metals.were collected u ill Bred �*'fE5 . I ' ❑ N , , and field acidified: ❑ YES ❑ NO
Ill II.. i T i
Date sample analyzed: _ p pv`�f Laboratory Name: Qf J `e� �(,� P
PARAMETERS NOTE: Values�sf�Hul '.reflect �issolvedrand colloidal ponceptmtlons.• ^ Certification No.
ilI I i
COD I t mg/l { Nitrite; (NC1 as N
mg/I Pb = Lead/IWG
Coliform: MF Fecal III ) .! j lt00mi Nitrate (NCS,). as N
I U.1111. mgll Zn - Zinc Da D3'.i mg/I
Coliform: MF Total All, , I I-L100m1 r?hosphorus: To�a6as P mg/I DEC O ZO16
(Note: Use MPN method for luphlq turbid m es} d
I I fl, 11'. oph,sphate m9/l Other _(Specq Compounds and Concentration Units):
Dissolved Solids: Total I mg/I Ali- Alurriinum m jl
pH (when analyzed) _ t� .i units ;Ba; Barium 9p '
i m
TOC L l �P- D. t� r� — �o` IJ Y►1�1 %L_
i m /I E I = Ca - Calcium
Chloride 8� 1 1 mgn
€ + I Cd Cadmium I , i m /I
Arsenic �T d �? .:I +o '
I. 9
r?t9f{ C s; o + BI� hromium Total 1 m /I
iy1
Grease and Oils i I i �l r I: I m9 E' Cu (Copper 1
Phenol jl,`I f ' 'm /l . C���N ` n mgh ORGANICS:j by GC GC1MS, HPLC)
9 a -Iron '
Sulfate II I I.11il �� Uri m9ll (Specify testand method #. ATTACH LAB REPORT.)
PRgCESSING ,
/,�p,T�Qi� Hg Mercury ' , mg/l Rep ort' Attached? Ye
1 ❑ 'No 0
I
Specific Conductance i I �� �tos I' ; O ( )
P. I, I{ i KIj PoEassium 3', d ? mgl�{l VOC, ,method # : �®a�i0
Total Ammonia. Q a.�` I I' mg/l Mg ,Magnesium mgh
- (Ammonia NlVogen;lNH,as N Ammonia �je ; Totap '4 " ,method#
1 Mn JMan anese m !I
I I I g 9 method #.
TKN as N t
I' I,m9/I { NI1Nickel mgll method#
_� ...�
For.:Remediatlon.Systems Onfyk to h(La¢� orfs ".In uetit To tilOCs:
!? P) (z 1 rn, L Effl elitTotal VOCs:
u
I m9IL VOC, Removal /.
tib f
`
uthorized Agent) Name and Title Pease P1 or ty -
I I �, Slgnatu "i
of Penn. eq (o[ Autho ed Agent) (Date).
I Rev. 112007 t I I I i
( l' j

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: Ce k"_
Permit Name (if different): _
Facility Address: l�(p
8 /c
d-7
. Contact Person:
Well Location/Site Name: Q
ease: ri7nf C/4 tid)•!ar' T1'Pe
OERMIT Nurtibe'r:LWD033``j;Expiration Date:Oee-51-;au,
Non -Discharge o/ UIC
NPDES
-- Other
TYPE OF PERMITTED OPERATION BEING MONITORED
goon El Remediation: Infiltration Gallery
» SPfay Field El Remediation:
di n °` 5; Telephone;Sc: W6 -13949L7,9 ❑ Rotary Distribdtor ❑ Land Application of Sludge
S I No. of wells to be sampled:_ ❑ •Water Source El Pump Other:
PLING i INFORMATION _ •�� frWIL.. t
r If WELL .
L ID NUMBER!(from Permit): Date sample collected:r f - r FIELD collected: -AN WAS.
Depth: 1 ft: k j Wial Diameter.-
pH units Temp. .:5 °C DRY at
h to Water Level: pft. below measuring paint' Screened Interval:ft. toff. Spec. Coad. µMhos time of -
surin Point isabove� f ����✓ samp
9 ft aand surface .I Relative M.P. Elevation: - 4' Lft• . Odor Q �.
me of water pumped/b.ailed:befo�ef's fnplirig:.l' chect
- jt9,llons Appearance C' 1 2A r
sample i
AMETEF
COD
❑ NO
and field acidified: ❑ YES ❑ NO
Coliform: MF Fecal
Colifgrm: MF Total
-
.:(Note: Use MPN method for....
;Iurbid,"
�"Iilh, Dissolved.Solids:Total ;I i
. me: �a4e,,. �r'C�
pH (when arialyzed)
b / �i � Certification Nb.
'TOC Z4
jd conoidal
Chloride
i
Arsenic ,LI fi�fd
Grease and Oils
I
i
Phenol
mg/I
j
Sulfate { { J111
/;1001n1.s
{11o0mi
'Specific Conductance 7
j
{ .I
Phosphor
Total Ammonia L•D ; {;1
mg/1
'(Ammonia Nitrogen;'NH,a3 N Anmonie hGtrd;
est
I
i
TKN as
I Ortfophpsphate '
m 11
, For Remediatlon.Systems Ontyl(, t?
i'
mg/I
Other.(SpecifX Compountls and Concentration Units):
?
mg/I
units
AI- Alwminum i
€6a. Barium
mg/I
emiittee (or horized Agenq Name and le '
(
'GW 59 ; Rev. 112007 j
I (,
mgA�
�..
m9/1 ,
mg/1
ei ed:.
•
S _ I "
❑ NO
and field acidified: ❑ YES ❑ NO
here.
E^
is
l S
.Laboratory
. me: �a4e,,. �r'C�
tq
b / �i � Certification Nb.
I reflecCIssolNi6d:i
jd conoidal
ronceci,itrations.
mg/I j
i
Nitrite (NU2) as N
mg/I
Pb - Lead " mg/I
/;1001n1.s
{11o0mi
j
{ .I
Phosphor
Nitrate (t10 as N " tg ��.
us:TotIa6as.P �,
mg/1
Zinc g3)
Zn - /r
�J m
est
I Ortfophpsphate '
m 11
mg/I
Other.(SpecifX Compountls and Concentration Units):
?
mg/I
units
AI- Alwminum i
€6a. Barium
mg/I
i
IMVI,
I rrt9ll
Ca Calcium
mgA�
�..
m9/1 ,
mg/1
` j
Cd Cadmium i
y.
Chromium: Total
mg/l
L ®,ewi
{:mg/lCu
-Copper D; i?,0�
mgh •
ORGANICS::(by GC GC/MS, HPLC)
{ m9ll
Fe!- Iron
g
(Specify testland method #. ATTACH LAB REPORT.)
ii
{ >iMhas
Hg Mercury {
Kj- PoEassium �,
mg%I
mg/I
Report Attaehed9 Yes (1) ❑ No (0) "<
VOC•
L_�
(:Magnesium
`I
,. method # _� I D
�
Tatap
:1
mgJl
i
Mq 1:
i
Mn !Manganese I
mg/l
mg/I
, method #
9
Ni Nickel _ I_mgll
��
method # .
method#
q
forts i i influJ ent Tot1,VOCs ' 1. m
-. -- :._8/I- ..Eff1
eOtTotal OCs: man vnrtae.,,...,�c°i
x

GROUNDWATER QUALITY ]MONITORING:
COMPLIANCE REPORT FOFt14I
acility Name:
ermit Name (if different):
acility Address: ,5-0 e
' icnv:
C
Contact Person: l `
Well Location/Site Name:
-tease ,ani 044111plorType
RERMIT"Number:?Qd3 WExpiration Date:
`--- �� Non -Discharge - UIC
NPDES Other
q'' =----_ TYPE OF PERMITTED OPERATION BEING MONITORED
County to r ��� ❑,�, L�a oon ❑ Remediation: Infiltration Gallery
C ; - -1 / L]YSpray Field ❑Remediation:
Telephoned: o�� 3y-fs4,0z ❑ Rotary Distrib.Otor ❑ Land Application of Sludge
No. of wells to be sampled: ❑ 'Water Source :Heat Pump ❑Other:
from Penrili : . t
SAMPLING INFOR TION : If WELL
WELL ID NUMBER(from Permit): .I Date sample* collected: '� �!') �® FIELD.ANALYSES: WAS.
— Well Depth: 'S ft: l i VVfal Diameter: in. pTemp...
°C DR
H "units1 t1a Y at
��-- .
Depth to Water Level: ✓ai,`T ft. below measutl{Ig pooh; .S reeved Interval:.36 _ft. to L7 ft. Spec. Corid. I� µMhos time of
MeasuringPoint is sampling,
ft "above I tand stirI I' Relative M.P. Elevation: ��-ft,. Odor jn PYN-?„
Volume of water pumped/bailed:befor�e:s mpling:. L chec
�J,,._ g!�Ilons A earance � � •� � '
Samples for metals'.vdere coliecied:,iu! it
j Date sample analyzed: Lu p Irl
PARAMETERS NOTE: Values 61'
COD
Coliform: MF Fecal ' 1 k'
Coliform: MF Total j^R
(Note:' Usa MPN imelhod for Nu hly turbid f F
I {
Dissolved Solids:.Total ;3 Iii
pH (when analyzed)
TOC
Chloride
I'1
�Arsenlc
�d l
Grease and Oils
Phenol j i Ii�ifl
Sulfate I I Hill
SpecificConductance
Total Ammonia L 11I)
(Ammon!a Nitrogen; 'NH, as N:
Anunonl Ni
TKN as N
For:Remedlation.Systems Only!( t
y
P.
i Pehnittep (or Whorized Agent) Name and Ie u
l . ,
'GW -
59 Rev. 112007"'!
r
i l l 1
r �
� r
y�
L.
-tu
•ed:. K;
(S j ❑ Ni,
and field acidified: ❑ YES ❑ NO
PP U
here
L
I
Laboratory Name %G / �G�
6 Certification No. Lob
eflect.
�lss v�ad,and
aoll.btdal concentrations ,
_ d, ,j
rng/l
I /J OOmI ;
I
Nitrite(NOZ) as N mgA
Nitrate (N W as N
Pb -'Lead mg/I
—mg/l
/100m1
j hosphotus:
Total
, ps mg/I
I.
as P 1 `�
Zn - Zinc ,f%
.'
�aOrft oph!
rrigll'
sphate img/I
Other.(S"pecio Compounds and Concentration Units):
units��
•
Al Aluminum r mg/I
I' �.ea =Barium
mg/l
I
mgA
Ca Calcium i mg/I
14 91
o
Lmg/l
mg/I i'
i
j •Cd Cadmium
Chroggmiu'
j mg/I
:TotalV
HT
i�
mg/I
Cu -
mg/I
;Copper mg/l
;�f
ORG`ANICS:.,(by GC GC/MS, HPLC)
I.m9/l
I_mg/I
r Fe-- I"rn 1 rng/I.:
Hg
(Spe6fy testj1and method #. ATTACH LAB REPORT.)
IuMhos `
Mercury mgll
K;'- Potassium {
� m9�1
Report Attached7. 'Yes (1) ❑ 'No (0) '<
VOC, 'I
� j
I mgA
, method # �ya`ZJD b
7dr�U.j
I
Mg =;Magnesium i
; mg%I
Mn `Manganese I rng%I
method #
l
i
Ni 'Nickel mg/l
method # .
method #
4a� RA`nnrtcl•:
e. I Infl�m6n1 T..�:,riinrS. i - .. ___I
- .
of

GW -59A .COMPLIANCE REPORT FORM Permit # "0033.677
(Submit one each monitoring period with GW -59 forms.)
1
Enter date monitoring results were due. CQeC3, Jle) Will this monitoring report (GW -59 and GW -59A)
YES
NO
be submitted after the established due date?
2
Was any required information missing on the GW -59 report forms?
YES
IF the answer to question 1 or 2 is "YES', list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO ,
identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Once for guidance.
X/
- 4 -Are
any_monito_aed constituents equal to above_the_established standards?
YES
N
-Itthe_6nswer-to-question.-_4_is_NO",,-_ skip -to -section 8..
If the answer to -question 4 is "YES"=list-the affecfedwells=i_ndivi-dual/y with constituents) and concentration(s)--
-
exceeding standards in the space provided below:
5-
--Forthe-constituents-identified-in question 4 above have -standards been exceeded previously -for the -
YES
NO
-- -
same constituents) in the same well(s) in -the last two -years?
If the answer to question 5 is "NO", skip to section 8. - - -
If the answer to question 5 is "YES", list in thespace provided below, each well with constituent(s) exceeding
standards, concentrations) repdited and sample collection -date -for each -occurrence (for the last two years).
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
if the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO" contact the Regional Office within 90 days: an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility, Failure to do so may subiect the permittee to a Notice of Violation,
fines, and/or penalties.
8
The person completing this portion (GW -59A) of the monitoring report should sign below and submit this
form with GW -59 forms for required wells to the address provided at the top of the current GW -59 form.
report(Compliance Report G -59A) is true'and complete to the best.of, my knowledge
r_A 0. J_ - Z62
Signa ure by pe iftee (or Authorized Agent) Date
GW -59A 12/8/2003

wivr ivirtCH LAHS,Inc.
POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE.' Case Farms -Hatchery COLLECTION DATE. 11/16/2016
PERMIT #. COLLECTION TIME. 12:45
ADDRESS., Case Farms Hatchery RECEIVED DATE
-1-11
} t ANALYSIS
ANALYSIS EFFLUENT
UNITS
BOD
77.8
m9/L..
TSS
90.0
mg/L
NH3
12.50
mg/L
Fecal Coliform
820
/100mL
Conductivity
580
umhos/cm
NO3-N
1.20
mg/L
TKN
19.3
mg/L
T. Nitrogen
20.50
mg/L
T. Phosphorus
1.73
mg/L
Chloride
56
mg/L
TDS
348
mg/L
RECEIVED TIME. 14:45
REPORTED: 12/9/2016
_.DATE-_
11/17/16
11/18/16
11/18/16
11/16/16
11/18/16
11/18/16
11/17/16
11/18/16
11/25/16
11/18/16
11/17/16
VAL Y_S.T
jdg
jrg
jrg
jrg
jrg
jdg
jdg
jdg
jdg
lag
lag
LOG ID: 1611-315 REPORTED BY: NC CERTIFIED LAB # 50
— Tony Gragg, Lab Supervisor
}

URT'ER TECH LITAF .IRC-
.
POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE.- Case Farms-Hatchery-MW#3 COLLECTION DATE: 11/16/2016
PERMIT #: COLLECTION TIME: 13:00
ADDRESS: Case Farms Hatchery RECEIVED DATE: 11/16/2016
RECEIVED TIME: 14:45
REPORTED: 12/13/2016
,4NALYSIS , RESULTS UNITS DATE ANALY57 � �;
u y ,
TDS 68 mg/L 11/17/16 lag
TOC <1.0 mg/L 11/18/16
NH3 <0.2 mg/L 11/18/16 jrg
Chloride 7.8 mg/L 11/18/16 lag
Arsenic <0.005 mg/L 11/22/16
NO3-N 0.16 mg/L 11/18/16 jdg
TKN 0.28 mg/L 11/17/16 jdg
T. Nitrogen 0.44 mg/L 11/18/16 jdg
T. Phosphorus 2.28 mg/L 11/25/16 jdg
Zinc 0.032 mg/L 11/22/16
MBAS <0.1 mg/L 11/18/16
Sodium 8.15 mg/L 11/22/16
Formaldehyde <0.25 mg/L 11/23/16
Conductivity 112 umhos/cm 11/18/16 jrg
Copper 0.010 mg/L 11/22/16
Potassium 3.23 mg/L 11/22/16
7:7
............... «,. .... .. ._..mom__. , .... � .... t",., ..-s _,........,.,. ,,. ,..,.y. �'..,...., �.. ..-,. ._ �v ......,w.�,.. .,�. :..,... s_,.... _.. .J.,..._., _� .w�.l w�. ...�..t_..�..C_... .,,. ,..�,. ......,....,.,s. l :.S
fttn
...-.t__:z �., s,. .... .. .s ,..ck,, _,...Ti _,..>_. _, _.. ...m...._... .. ....sv..,._ -._ v.>3=.. ._�'i�...;.... ....., �•...�. �.. .<,. .+a..- '.Y nv:Z.:v :_•
LOG ID: 1611-316 REPORTED BY: NC CERTIFIED LAB # 50
Tony Gragg, Lab Supervisor

jrrrR rffcH m .1nc.
POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE. Case Farms-Hatchery-MW#4 COLLECTION DA TE: 11/16/2016
PERMIT #: COLLECTION TIME: 13:50
ADDRESS: Case Farms Hatchery RECEIVED DATE., 11/16/2016
RECEIVED TIME: 14:45
REPORTED: 12/13/2016
TDS
47
mg/L
11/17/16
lag
TOC
<1.0
mg/L
11/18/16
NH3
<0.2
mg/L
11/18/16
jrg
Chloride
8.5
mg/L
11/18/16
lag
Arsenic
<0.005
mg/L
11/22/16
NO3-N
5.60
mg/L
11/18/16
jdg
TKN
0.56
mg/L
11/17/16
jdg
T. Nitrogen
6.16
mg/L
11/18/16
jdg
T. Phosphorus
1.24
mg/L
11/25/16
jdg
Zinc
0.035
mg/L
11/22/16
MBAS
<0.1
mg/L _
11/18/16
Sodium
5.56
mg/L
11/22/16
Formaldehyde
<0.25
mg/L
11/23/16
Conductivity
78
umhos/cm
11/18/16
jrg
Copper
0.007
mg/L
11/22/16
Potassium
1.64
mg/L
11/22/16
k{
LOG ID: 1611-317 REPORTED BY: NC CERTIFIED LAB # 50
Tony Gragg, Lab Supervisor

wl,rKR rKCH ' LfiffS.1nc.
POST OFFICE BOX 1056 • #5 PINEWOOD PLAZA DR.
GRANITE FALLS, NORTH CAROLINA 28630
[phone]
SAMPLE. Case Farms-Hatchery-MW#5 COLLECTIONDATE.
11/16/2016
PERMIT #. COLLECTION TIME:
13:25 ,
ADDRESS: Case Farms Hatchery RECEIVED DATE.,
11/16/2016
RECEIVED TIME.,
14:45
REPORTED:
12/13/2016
ANALYSIS RESULTS
UNITS'
DATE
ANALYST
_ ..
TDS
39
mg/1-3
11/17/16
lag
TOC
<1.0
mg/L
11/18/16
NH3
<0.2
mg/L
11/18/16
jrg
Chloride
7.8
mg/L
11/18/16
lag
Arsenic
<0.005
mg/L
11/22/16
NO3-N
4.70
mg/L
11/18/16
jdg
TKN
0.28
mg/L
11/17/16
jdg
T. Nitrogen
4.98
mg/L
11/18/16
jdg
T. Phosphorus
1.79
mg/L
11/25/16
jdg
Zinc
0.030
mg/L
11/22/16
MBAS
0.148
mg/L
11/18/16
Sodium
4.69
mg/L
11/22/16
Formaldehyde
<0.25
mg/L
11/23/16
Conductivity
64
umhos/cm
11/18/16
jrg
Copper
0.007
mg/L
11/22/16
Potassium
1.24
mg/L
11/22/16
,11
�. __._.... _..... .._ .., _..;._ ,. ..
...z.. .�_.., .....,
t.... .. _.. __..,.
..��..._. .. ._, .....
_.... _ .,., .. ,. ._ .. .�..... 4.. r..1
LOG ID: 1611-318 REPORTED BY: NC CERTIFIED LAB # 50
fo� *
Tony Gragg, Lab Supervisor

RESEARCh ANALyTICA1 Report of Analysis
LA o RATO RI ES, INC* 12/7/2016
For: Water Tech Labs, Inc.
P.O. Box 1056
Granite Falls, NC 28630
Attn: Joe Gragg
Client Sample ID:
Site:
Case Farms MW3
Water Tech Labs
Lab Sample ID:
Collection Date:
27440-01
11/16/2016 13:00
Site:
Parameter
Method
Result
Units
Req Limit Analyst Analysis Date/Time
Arsenic, Total
EPA 200.7
<0.005
mg/L
0.005
KL 11/22/2016
Copper, Total
EPA 200.7
0.010
mg/L
0.005
KL 11/22/2016
Formdldehyde
In House
<0.25
mg/L
0.25
DW 11/23/2016
MBAS
SM'5540 C-2000
<0.1
mg1L
0.1
AW 11/18/2016 1500
.Sample received
out of hold time
mg/L
0.1
AW 11/18/2016 1500
Sample received
Potassium, Total
EPA 200.7
3.23
mg/L
0.5
KL 11/22/2016
Sodium, Total
EPA 200.7
8.15
mg/L
0.5
KL 11/22/2016
Total Organic Carbon SM 5310 B-2000
<1.0
mg/L
1
MG 11/18/2016
Zinc, Total
EPA 200.7
0.032
mg/L
0.01
KL 11/22/2016
Client Sample ID:
. Case Farms MW4 .
Lab Sample ID:
27440-02
Site:
Water Tech Labs
Collection Date:
11/16/2016 13:50
Parameter
Method
Result
Units
Req Limit Analyst Analysis Date/Time
Arsenic, Total
EPA 200.7
<0.005
mg/L
0.005
KL 11/22/2016
Copper, Total
EPA 200.7
0.007
mg/L
0.005
KL 11/22/2016
Formaldehyde
In House
<0.25
mg/L
0.25
DW 11/23/2016
MBAS
SM 5540 C-2000
<0.1
mg/L
0.1
AW 11/18/2016 1500
Sample received
out of hold time
Potassium, Total
EPA 200.7
1.64
mg/L
0.5
KL 11/22/2016
Sodium, Total
EPA 200.7
5.56
mg/L
0.5
KL 11/22/2016
Total Organic Carbon SM 5310 B-2000
<1.0
mg/L
1
MG 11/18/2016
_._........... _-......._.. _.. ------ .._..._.__..:... .._... ........... ._.......
.._:..._.._.:..... .
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284. Tel: [phone] Fax: [phone] www.randalabs.com Page 1
rai coa basic vid

RESEARCh NALY-FiCAI. Report of Analysis
LA oRATORiES, INC. 12/7/2016
Client Sample ID:
Case Farms MW4
<0.25
mg/L
Lab Sample ID: 27440-02
Site:
Water Tech Labs
MBAS
SM 5540 C-2000
Collection Date: 11/16/2016 13:50
Parameter
Method
Result
Units
Rep Limit Anal st Analysis DatelTime
Zinc, Total
EPA 200.7
0.035
mg/L
0.01 KL 11/22/2016
Potassium, Total
EPA 200.7
1.24
mg/L
0.5
Client Sample ID:
Case Farms MW5
Sodium, Total
EPA 200.7
Lab Sample ID: 27440-03
Site:
Water Tech Labs
KL
11/22/2016
Collection Date; 11/16/2016 13:25
Parameter
Method
Result
Units
Rep Limit Analyst Analysis Date/Time
Arsenic, Total
EPA 200.7
<0.005
mg/L
0.005 KL 11/22/2016
Copper, Total
EPA 200.7
0.007
mg/L
0.005 KL 11/22/2016
Formaldehyde
In House
<0.25
mg/L
0.25
DW
11/23/2016
MBAS
SM 5540 C-2000
0.148
mg/L
0.1
AW
11/18/2016 1500
Sample received out of hold time
Potassium, Total
EPA 200.7
1.24
mg/L
0.5
KL
11/22/2016
Sodium, Total
EPA 200.7
4.69
mg/L
0.5
KL
11/22/2016
Total Organic Carbon
SM 5310 B-2000
<1.0
mg/L
1
MG
11/18/2016
Zinc, Total
EPA 200.7
0.030
mg/L
0.01
KL
11/22/2016
NA = not analyzed
_—._.----.._........... ... _.._._----._..-...._._..___....,._-..... _....... _ ........... ..........___-____.. __.._.__. .._......._....._
........ _.
P.O. Box 473 106 Short Street Kernersville, North Carolina 27284 Tel: [phone] Fax: [phone] www.randalabs.com Page 2
raI caa bas+c vi;7

RESEARCh 1& ANALYTICAL
LAbORATORIES, INC.
Analytical/Process Consultatlorls
Chemical Analysis for Seleded Parameters and Water Sample Idenhhed as Case Farms
(A Water Tech Labs, Inc. ProiecA colleded 16 November 2016)
L Volatile Organics
Quantitation
EPA Method 8260 B
Limit
MW 3
MW 4
MW 5
Parameter
jji b
jppbj
jBpb1
j
Acetone
25
BQL
BQL
BQL
Acralein
100
BQL
BQL
BQL
Aetylonitrile
100
BQL
BQL
BQL
Benzene
0.5
BQL
BQL
BQL
Bramobeamc
0.5
BQL
BQL
BQL
Bmmochimurarthane
0.5
BQL
BQL
BQL
Bramodichlaromerhone
0.5
BQL
BQL
BQL
Bromoform
1.0
BQL
BQL
BQL
Bromomethane
1.0
BQL
BQL
BQL
2-Butcnone
25
BQL
BQL
BQL
Carbon Disulfide
5.0
BQL
BQL
BQL
Carbon Tetrachloride
0.5
BQL
BQL
BQL
Chlambenseae
0.5
BQL
BQL
BQL
Chlomethane
1.0
BQL
BQL
BQL
2-Chloroethyl vinyl ether
5.0
BQL
BQL
BQL
Chloroform
0.5
BQL
BQL
BQL
Cb1oromethaae
1.0
BQL
BQL
BQL
2-Chlorotolucnc
0.5
BQL
BQL
BQL
4-Chlorotoluenc
0.5
BQL
BQL
BQL
Cis-1,2-Dichlornethme
0.5
BQL
BQL
BQL
Cis-1,3-Dichlompmpere
0.5
BQL
BQL
BQL
1,2-Dibmmo-3-Chlorcpropanc(DBCP)
5.0
BQL
BQL
BQL
1,2-Dibmmoethme (EDB)
0.5
BQL
BQL
BQL
Dibramochlommclhase
0.5
BQL
BQL
BQL
Dibromomethanc
0.5
BQL
BQL
BQL
1,2-Dichlombeazme
0.5
BQL
BQL
BQL
1,3 -Dichlorobenzene
0.5
BQL
BQL
BQL
' 1,4-Dirhlorobrsamc
0.5
BQL
BQL
BQL
1,1-Dichloroethane
0.5
BQL
BQL
BQL
1,2-Dichloroca me
0.5
BQL
BQL
SQL
1,1-Dichlaroethene
0.5
BQL
BQL
BQL
Diehlaroflouromethane
0.5
BQL
BQL
BQL
1,2-Dirhloroprol me
0.5
BQL
BQL
BQL
1,3-Dichlompmpaae
0.5
BQL
BQL
BQL
2,2-Dichlampmpane
0.5
BQL
BQL
BQL
IJ-Dichlompropece
0.5
BQL
BQL
BQL
Ethyl Become
0.5
BQL
BQL
BQL
2-H -=m^
5.0
BQL
BQL
BQL
IPE
0.5
BQL
BQL
BQL
I-Propylbcn me
0.5
BQL
BQL
BQL
4-Mcthyl-2-Pmaaone
5.0
BQL
BQL
BQL
Methyl Iodide
1.0
BQL
BQL
BQL
Methylene Chloride
5.0
BQL
BQL
BQL
MTBE
0.5
BQL
BQL
BQL
Naphthalene
0.5
BQL
BQL
BQL
N-Butylbmzme
0.5
BQL
BQL
:BQL
N-Pmpylbmzme
0.5
BQL
HQL
BQL
p-Lsapropyholueae
0.5
BQL
BQL
BQL
Seo-Butylbmzeae
0.5
BQL
BQL
BQL
Styrene
0.5
BQL
BQL
BQL
Tert-Butylbmzme
0.5
BQL
BQL
BQL
1,1,1,2-Tetmch1omcthme
0.5
BQL
BQL
BQL
I,IA2-Tetrachloroethane
0.5
BQL
BQL
BQL
Tetrac hloroethme
0.5
BQL
BQL
BQL
Toluene
0.5
BQL
BQL
BQL
Tracts-l,2-Dicblotoethme
0.5
BQL
BQL
BQL
Traces-1,3-Dichloropropcne
0.5
BQL
BQL
BQL
Trans-l,4-Diahlaro-2-butene
5.0
BQL
BQL
BQL
1,2,3-Tricddombenzene
0.5
BQL
BQL
BQL
1,2,4-Trichlombenzene
0.5
BQL
BQL
BQL
1,1,1 -Trichloroethane
OS
BQL
BQL
BQL
1,1,2-Trichloroedtene
0.5
BQL
BQL
BQL
Trichlomethme
0.5
BQL
BQL
BQL
Tzichlorefluommcthane
0.5
BQL
BQL
BQL
1,2,3-Trichloropropene
0.5
BQL
BQL
BQL
1,2,4-Trimethylbmrme
0.5
BQL
BQL
BQL
1,3,5 Triaethylbmzene
0.5
BQL
BQL
BQL
Vinyl Agate
1.0
BQL
BQL
BQL
Vinyl Chloride
0.5
BQL
BQL
BQL
T0a1 Xylmes
1.0
BQL
BQL
BQL
Dilution Factor
1
1
1
Sample Number
27440.01
27440-02
27440-03
Sample Date
11/16/16
11/16/16
11/16/16
Sample Time (hrs)
1300
1350
1325
Analyst
NM
NM
NM
Date Analyzed
1120/16
11/20/16
1120116
BQL - Belm Q - I - Lich pyb - F -P bM-
��p111M11/I,,
o/nullsr`

Water Tech Labs, Inc.
P.O. Box 1056
Granite Falls, NC 28630
Attention: John Gragg
Chemical Analysis for Selected Parameters and Sampling Location Identified as Case Farms
RESEARCk
a
--
I. Miscellaneous
Zone #1
Zone #2
..
_Voi_
Zone #4
Parameters
Results
NC #34 toC
r"
Analytical/Process Consultations
4.6
:,
my v
mg 'v
ma a
e
1,030
897
666
All
r.r"r't��
December 9, 2016
16.3
4.65
Water Tech Labs, Inc.
P.O. Box 1056
Granite Falls, NC 28630
Attention: John Gragg
Chemical Analysis for Selected Parameters and Sampling Location Identified as Case Farms
A Water Tech Labs. Inc. Pro'ect. collected 16 November 2016)
Zone #3
Zone #4
I. Miscellaneous
Zone #1
Zone #2
Zone #3
Zone #4
Parameters
Results
Results
Results
Results
4.6
ma a
my v
mg 'v
ma a
Calcium, Total
1,030
897
666
1,070
Copper, Total
16.3
4.65
5.44
9.35
Potassium, Total
720
601
1,360
821
Phosphorus, Total
477
217
79.3
442
Sodium, Total
184
237
52.4
113
Manganese, Total
75.0
112
73.8
92.4
Magnesium, Total
976
803
1,450
1,050
Zinc, Total
34.8
19.1
18.3
26.0
11. Miscellaneous
Zone #1
Zone #2
Zone #3
Zone #4
Parameters
Results
Results
Results
Results
%
%
Percent Humic Matter
15.2
10.6
8.89
9.36
Exchangeable Sodium
6.9
7.9
5.2
3.5
Percent Base Saturation
71.2
79.9
72.4
50.7
111. Miscellaneous
Zone #1
Zone #2
Zone #3
Zone #4
Parameters
Results
Results
Results
Results
(SU)
SU
(SU)
SU
pH
6.26
6.44
6.14
5.88
IV. Miscellaneous
Parameters
Cation Exchange Capacity
Acidity
Sample Number:
Sample Collected Date:
Sample Collected Time:
Zone #1
Zone #2
Zone #3
Zone #4
Results
Results
Results
Results
(meq/100 a)
(meq/100 g)
(meq/100 e)
(meq/100 s)
7,8
6.6
4.6
4.1
2.24
1.32
1.28
2.02
27441-01
11/16/16
meq/100 g = miliequivalents per 100 grams
mg/kg = milligrams per kilogram = parts per million
% = Percent
Std. Units = Standard Units
27441-02 27441-03 27441-04
11/16/16 11/16/16 11/16/16
---- = Not Available

-'A TER TE---.'.C-H-'.' L'A',,
Bs,
5 Pinewood Plaza Drive - P.O. Box 1056
Granite Falls, NC 28630
Phone [phone] - Fax [phone]
CLIENT: Case Farms Hatchery
c/o Cindy McGinnis
Manager
PHONE NUMBER: 828-438-6900 ext.6975
TYPE SAMPLE: n/a
No. LOCATIONS: 4
SAMPLER NAME:
Sample Collection
Information
TYPE
CONTAINERS
ANALYSIS REQUIRED
Sample Location
FacilityName
DATE
TIME
TEMP.
Grab/
Composite
No
Plastic/
Glass
EffluentGrab
8
Plastic
Fecal Coliform, Chloride, TDS
BOD -5, TSS, Conductivity
NO3-N,TKN, NI -13-N
Monitoring Well #3Grab
`-j6
-��
130
17-D
12
Plastic/
Glass
TDS, Chloride, MBAS,
Formaldehyde, Conductivity
As, Cu, K, Zn, Na
NH3-N, NO3-N, T.P., TKN
36
TOc
VOC(Annual Nov. only)
Monitoring Well #4
�, �b
/ 3
Grab
12
Plasc
Glass/
Same As #3
Monitoring Well #5
6,
/ 3.2.5
/ . 0
Grab
12
Plastic/
Glass
Same As #3
Relin ed By/�
Date:
Time:
Rec' a
Date:
Time:
Relin uisi-ihed y:
Date:
Time:
ceived By:
Date:
Time:
F' EbEKVA I IUN:
Coo/ 4°C
2SO4
(JNaOH
Yr',�.1NO3 RN03
(J Dechlornating Agent
(] Other
SAMPLE TEMP. @ LAB (°C) S3. D
Chlorine Residu mg/l
IT
NC CERTIFIED LAB # 50