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Home My WebLink AboutWQ0001817_Monitoring - 11-2016_20161230 (2)GW -59A COMPLIANCE REPORT FORM QJg` ap C 1 g 1l (Submit one each monitoring period with (79' 59 jorms.) I Enter date monitoring results were due. - WIII this monitoring report (GW -69 and GW -69A) YES be submitted after the established due date? 2 Was any required information missing on the GW -59 report forms? YES IF the answer to question f or 2 is 'YES, list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information - 3 An any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES identification plate, area overgrown, etc)? fjthe answer is "yes", contact the Regional Office for guidance. 4 Are any monitored constituents equal to or above the established standards? NO If the answer to question 4 is 'NO" skip to section 8. H the answer to question 4 is "YES" list the aBected wells individually with pyr�1 nn(S) exceeding standards in the space provided below: ✓ ro�(1SSGg rto5g Pk I , -la DEC 30 2016 ac 63t: 6O— PK 5 For the constitvehtb identified In question 4 above, have standards been exceeded previously for the NO same const)tuent(s) in the same well(s) In the last two years? ff the answer to question 5 is 'NO' slop to section 8. Hthe answer to question 5 is 'YESn list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). 6 Are the monitoring wells listed in section 6 located at or beyond the review boundary? YES H the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REG)ONi1L OFFICE IMMEDIATELY FOR GUIDANCE. if the answer is "NO", monitoring wells maybe improperly located; contact the Regional OfFrce. 7 Is the permittee implementing previously approved actions required by the Division involving this YFS groundwater quality problem? If the answer to question 7 is 'YES', describe those actions in the space provided below. Hthe answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the vermittee to a Notice of floes, and/or penalties. WG DEC 3 0 2016 8 The parson completing this portion (G WS9A) of the monitoring report should sign below and submit this form with GW -59 forms for required wells to the address provided at the top of the current G*59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW -69A) is true and complete to the best of my knowledge. Signature or (or AUNoA>7d NRVDate GW -59A 1218/2003 SUBMIT FORM ON YELLOW PAPER ONLY oROUNDWATER QUALITY MONITORING: OM's }'Sj �`b•;'r ir'St1r 7(�iE"�i: C' ';i il�+�` b��j" , ;OMPLIANCE REPORT FORM'`° pH (when analyzed) /a rt 1 units TOC I PERMITNo. EXPIRA710N DATE: r' 7 'ACILITYINFORMATION Please Print Clearly or Type )0IS(__ -� mg/I (, n 1 ., / 1 J. • 1:�. i Lvs r)U C.+ )IDO _u1C Non•Olecherpa �2Q� Phenol )acillty Name. �% r r � o r i NPDES u hos )ermit Name (If different): )acility Address: TYPE OF PERMITTED OPERATION BEING MONRORED Total Ammonia G e i County Q(gftl M arn. S _ --- ✓ lnpoon Rem#dlatlon: IMlaration GMlery Contecl Person: /�/1-r�C�[.[L� `%%GIBS �N Teleptrone#: ,�,U r• Nn • ua 1.,.:w� No. of wells to be sampled: 1 h Spray Field Ramedletorn:�— wry Distributor __land ADPsc'=lon of Sludge Heat Pump Well Location/Site Name: HCl � o Water Souroe Number (from t�7 - I g WELL WAS DRY Well Other m time of sampling, Check here Well Dia): Well Depth: '�� ft. Well Diameter: Z. in. Depth' For Remediation System Onty (Attach Lab Reports. Screened Interval: ft. to -_tft. Semple is from system: ❑Influent effluent VOC COM"traent ad.myl (Total VOC Concmtrallon) (Total VOC Conoemragon) Depth to Water Level: i ft. below measuring point. ;. ft. above land surface. Relative M.P. Elevation in It. Effluent mglL VOC Removal S Measuring Point is Gallons of water purn d/balled before sam lin S, 0 Date sample collected: I ° Dale sample analyzed: - o / t' - t 9 edfic Conducts 1m uMhos FIELD ANALYSIS: pH P Appearance G (`-i Temp. l^i 5 °C Odor,_$Ic3y� APP _ , r t%C^,S ♦ $ Laboratory Nems: CeNflcalionNo.CL 9 TN C PARAMETERS (Samples for metals were collected unfiltered ----YES _ NO and field acidlfied_.YES _NO.) NOTE: Values should reflect dissolved and colloidal concentrations. Nitrite (14%) as N C-01 mg/I Ni - Nickel mg/I mg/I COD mg/I _ Nitrate(NO3)s N t Coliform: MF Fecal 1 1100m1 ( e) d • 0 Z moll . P6 -Lead Zn - Zinc moll �^^^-Phos horus; Total asP moll Coliform: MF Total (Nora: Use MPN meN°d for hlphM WNW eemebe) moll Dissolved Solids: Total k 3g -- mgll pH (when analyzed) /a rt 1 units TOC I mg/I _q Chloride 20 mg/I — mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I mg/I Sulfate u hos Specific Conductance moll Total Ammonia G e i mg/1 mg/I (Ammonle Nitrogen; NH) ea N; Amrronle Nitrogen, Totep TKN as N mg/I P Orthophosphate mg/I A I- Aluminum mgll Be - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mgfl Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg -Magnesium mg/1 mg/I Mn - Manganese Other (Specify Compounds and Concentration Units) ORGANICS: (by GC, GC/MS, HPLC) Rt Report Attached? Yea _V _0) NoH B REPORT.) VOC : method #_ method#= method #= _ Rev. 11/2005 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: 1 =" "' ""Y•i'z"'w"a ••'. w` �.)r n ' ',y�Kv 81 ksr 'z, COMPLIANCE REPORT FORM I 9 81. ' ra �� 1f�5'' fRALEIe, . rNCR'f PERMIT No. EXPIRATION DATE: FACILITY INFORMATION please Print or Type �__ A uIC 7cllearly Facility Name: fniihem 'r i� u."+'i 'rcrle3 1lJ�+ No Discharge Ir1QAaOOLI NPDES Permit Name (if different): mg/I Facility Address: 1t&2n"' County. P 1 ma..� S TYPE OF PERMITTED OPERATION BEING MONITORED® Remedialbn: infiltration Gallery vI) Telephone#::&52-u22._1002 ✓ Spray Field Remedielbn:_,�-- Land Application of Sludge Contact Person: -�� Well Location/Site Name: S.L ,,,,,, i'f f.aIo, �_ No. of wells to be sampled: 1 A 1F'F� _ Rotary Source Hs Water Source Heel Pump Identification Number (from Permit):Ir WELL WAS DRY Other. Well Depth: 12- ft. Well Diameter.._ -in. elthneasampling, Check bare For Remediation System InfluenUEHluent Only (Attach tab Reports.) Screened Interval: Z ft. I Z- ft. Sample is from system: ❑Influent effluent yL (Total Yoc concentration) Influent mEfflwnt Depth toWater Level: 't,t ft. below measuring point. mg1L (Total VOC concentration) Measuring Point is_ K above land surface. Relative M.P. Elevation In ft. VOC Removal % Gallons of water pumpedibailed before sampling: $ Date sample collected: Date sample analyzed: FIELD ANALYSIS: pH 5-;6 Specific Conductance umhos Temp. 19. 9 OC Odor SI • G � l- Appearances �- Laboratory Name: ,�'A IN Qf� Certification PARAMETERS (Samples for metals were collected unBltered_YES _ NO and field acidified YES NOTE: Values should reflect dissolved and colloidal concentrations. N Q m9/1 nigh Ni - Nickel COD mg/1 Nitrite (NO2) as r0 mgA Pb - Lead MFF 1 Q O 2 /looml Nitrate (NO3) as N G O k O 9, mg/I _mgA Collfonn. eca mgA Coliform: MF Total /100m1 pat.: UwMPNmRuWtor Wa ItuNN WS) mgll Dissolved Solids: Total 1 -)7 mg/I PH (when analyzed) q S units TOC IC 'Z mg/I Chloride <'4 mg/I Arsenic mg/I Grease and Oils mg/l Phenol mgt) Sulfate mg/l Specific Conductance uMhos Total Ammonia r i mg/1 (Ammonia Narogen: NHS es N; Ammonfe Mtragen, Taaq TKN as N mg/I Phosphorus: Total as P mgA Orthophosphate mgA A I- Aluminum mgll Be - Barium mgll Ca - Calcium mgll Cd - Cadmium mgA Chromium: Total mgll Cu - Copper mgA Fe - Iron mg/I Hg - Mercury mgn K - Potassium mgA Mg - Magnesium mg/1 Mn - Manganese mgA GW -59 Signature of Permiftea Rev. 1112005 `� Zn -Zinc Other (Specify Compounds and Concentration Units) ORGANICS: (by GC, GCIMS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? Yes �(1) No (0) VOC : method #-- method _method #= method #_ • method QUALITY MONITORING: E REPORT FORM Name: Name (d Address: SUBMIT FORM ON PAPER ONLY act Person: 1 r 4)Y�}A-% Telephone#:1S1.y2t.-loo-7 Locatlon/SitaName:S_ e:sP��'re(d No. of wells to be sampled: WLQW— Well Depth: I -2-- ft. Well Diameter. 2- in. Screened Interval:_ ft. to— Depth to Water Level: C,G ft. balow measuring point. Measuring Point is_�3 ft. above land surface. Gallons of water pumpedlbailed_ b_e_ fore sampling: FIELD ANALYSIS: pH ,2 Specific Conductor Temp. L4.6 OC Odor M; L Check tore Appearance .Ic•(,I, sl4fus b., OF PERMITTED OPERATION BEING MONITORED tagooe Rorm axilm Intoragon Gallery Spay FkW Remedeaorg _ Rotary Dhddbutor -Lard Apprualon of Sludge GTT ,nt_ mail. (Total VOC concentration) )M malt. (Total VOC Concentration) Removal _% rsample analyzed: y/-30— /L• xatory Name: A4 v_ , "o n," nen PARAMETERS (Samples for metals were collected unffltemo_YES _ NO and field acidified YES _NO.) NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO,) as N Q . j'>, mg/I Ni - Nickel Coliform: MF Fecal , 1 /100ml Nitrate (NO3) as N <0,f)7, argil Pb - Lead Moll Zn - Zinc mg/I mgn mg/I Coliform: MF Total /1 DOml Phosphorus. Total as P - jl a U. tare mw,oa tar No* war a"* Orthophosphate Mg/l mgn Other (Specify Compounds and Concentration Units) Dissolved Solids: Total 10 mgn A I- Aluminum PH (when analyzed) C, 23 units Be - Barium mgn TOC ls, t, mg/l Ca - Calcium m911 Chloride S4 moll Cd - Cadmium rng/l Arsenic mgA Chromium: Total mgA Grease and Oils mg/I Cu - Copper mgn mg/) ORGANICS: (by GC. GC/MS, HPLC) Phenol mora Fe -Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mg/I Report Attached? Yes�_(1) No (0) Specific Conductance uMhos K -Potassium moll VOC : method #= Total Ammonia 3.4. mgn Mg - Magnesium : method (AmmorA Nirogen: NH, es N: Ammcraa Muogen. Total) Mn - Manganese mon method f1#= TKN as N rngn : method l= GW -59 Rev. 112005 SUBMIT FORM ON YELLOW PAPER ONLY TER QUALITY MONITORING: COMPLIANCE REPORT FORM Name: Name( act Person: AlV41y /'ter-GY-XJ TelefihoneM a4253_ IbS o'�_ Local]on/Site Name: ,.�R[ Atel d No. of wells to be sampled: ) h OF PERMITTED OPERATION BEING MONITORED TORED lydlHmdon Gallery Lagoon -- Spray —Remedlldon:� _ Rotary Distributor __Land Appllcalmn of Sludge Werer Source Heal PUMP Well Depth: 1 Z ft. Well Diameter: 2- in. M gmeot sempling, cnerx ere For Remedlatlon System Influent/Effluent Only (Attach Lab Reports. Screened Interval:. 2 ft• to l�ff. Sample is from system: lnnuen� argil. (Total VOC Concentration) Depth to Water Level: 1r t ft. below measuring poin4 ❑Influent [Hluent Effluent marl (Total VOC concentration) Measuring Point is ft. above land surface. Relative M.P. Elevation in ft. voc Removal X Gallons of wafer um edtbailed before sampli r Date sa le wllectetl: 2 _ a - L G uMhos Date sample analyzed: e } FIELDANALYSIS: pH r 24 Specific Conductance �,,, Laboretory Name: Temp. 19.3 eC Odor Svc' t SOliti� Appearance [.* T Certification No. PARAMETERS (Samples for metals were collected untlltered_YES ,_ NO and field acidified YES NOTE: Values should reflect dissolved and colloidal concentrations. mg/I COD mg/I Nitrite (NO,) as N O O_ 14 mg Ni -Nickel 111w, U /loom] Nitrate (NOa) as N 40,01L mii/I Pb - Lead mg/I Coliform: MF Fecal I 00- Coliform: MF Total _ /100ml (NON: Un WN rrad o br NO)y IurNE 3eOPdeN I s4 mg/I Dissolved Solids: Total mgA PH (when analyzed) (' L- u - _ units TOC 6.6I mgli Chloride l0 mgA Arsenic mgn Grease and Oils mg/I Phenol mg/I Sulfate mgA Specific Conductance uMhos Total Ammonia 1. 1 mg/I (Arnmonla Nitrogen: NH, as N: Amnwda Nitrogen, Toler) mgn TKN as N _ mg/1 Phosphorus: Total as P mgA Orthophosphate mgA A I. Aluminum mgn Ba - Barium mgli Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mgn Mn -Manganese �mg/ zn - zinc Other (Specify Compounds and Concentration Units) ORGANICS: ( by GC, GCIMS, HPLC) (specify test and method #. ATTACH LAB REPORT.) Report Attached? YBs__,�_(l) No (0) VOC : method #_ method # — : method #= __ ,TER QUALITY MONITORING: REPORT FORM Name: Name (if act Person: LocallonlSite Well Depth: h. Well Diameter. Z in. Screened Interval:/lot- ft. to .02- ft. Depth to Water Level: 1.3 ft. below measuring point. Measuring Point is, 3 ft. above land surface. Gallons of water Dumoedlbailed before sampling: S'0 SUBMIT FORM ON YELLOW PAPER ONLY Telephone#.ir,�s _u�y- f C No. of wells to be sampled: it) Date Check here GC Odor AAmnn- Appearance F PERMITTED OPERATION BEING MONITORED _Remediation: IfdAlralion Gallery Spray Field _Remedatlon: Rotary Distributor _Land Application of Sludge Water Source Heal Pump 0tw. imediation System IntluenVEffluent Only (Attach Lab Reports.) mg/L (Total VOC Concerdntion) m.ar frotal VOC COnoanlraeon) Name: i No. PARAMETERS (Samples for metals were collected unfiitered_,YES _ NO and field acidified YES _NO.) NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N 4CO.O 'L mg/I Ni - Nickel Collform: MF Fecal G 1 1100ml Coliform: MF Total 1100ml (tura'. Ur MGN m hG for N9* luNW smp.q mgll Dissolved Solids: Total 5 6$ mg/I pH (when analyzed) 6.17 units TOC S'ck mg/I Chloride It 15 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mgA Sulfate mg/l Specific Conductance uMhos Total Ammonia 40.2 mg/I (Ammonia Nitrogen; NH3 as N; Ammunie Mirmen. Total) m911 TKN as N mg/i Nitrate (NO3) as N <0,0 7_ mgll Phosphorus: Total as P mgll Orthophosphate - mg1l A 1- Aluminum mgA Be - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mgll Chromium: Total mgli Cu - Copper mgll Fe - Iron mg/I Hg - Mercury mg/i K - Potassium m911 Mg - Magnesium mgll Mn - Manganese 111911 Pb - Lead Zn - Zinc Other (Specify Compounds and Concentration Units) ORGANICS: (by GC, GC/MS, HPLC) (Specify lest and method #. ATTACH LAB REPORT.) Report Attached? Ye3_/ _(I) No— (0) VOC : method #= method #= method #_ rear mg/I mg/I Rev. 11/2005 GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM or Name: Name (if, Address: SUBMIT FORM ON YELL W PAPER ONLY act Person: M� -/ _Telephone#::Z5 Ups 1007 Localion/Site Name:, ryizr - • • 9 No. of wells to be sampled: 1 n F PERMITTED OPERATION BEING MONITORED Lagoon __Rembdistim: InnMrelwn Gallery spray Field _R°nleNIA1011 Rotary Dlsidtador ----- tend Application of Sludge Waley source Beat Pump Olken Laep well runnun..uu.n........,.., al Ume of sampling, Check hero Well Depth: 12 ft. Well Diameter. �— in. Sample !s from s stem: For Ramediatlon System InguenUEfftuent Only (Aftac(AttachScreened Interval: - Z ft. to �-1 Z ft. y Influent mg 1. (Total VOC Concentradon) Depth to Water Level: O� fL below measuring point ❑ InBuent [ invent Effluent myL (Total voc concemrouon) Measuring Point is__3_ ft above tend surface. Relative M.P. Elevatbn in ft.,�— VOC Removal --!% Gallons of water pumped/bailed before sampli : SO Date sam to collected: 1 "jd' « uMhos Date sample analyzed: a-4 t n. FIELD ANALYSIS: pH Specific conductance „ ry ' i (jfa Laboreto Name: Temp. 11,t C Odor Ne„�_ Appearance LIS --�- Certification No. PARAMETERS (Samples for metals were collected unfiltered_YFES _NO and Held acidified YES _NO.) mg/I NOTE: Values should reflect dissolved and colloidal concentrations. m�( Ni -Nickel mg/( COD mgll Nitrite (NO2) as N C , o 3 It OOmI Nitrate (NO,) as N / p O L mgll Pb - Lead mg/I z----- Coliform: MF Fecal N,. 1100ml Coliform: MF Total — (NMO: Um WN m%Md tm hi” WNW SWO") mgll Dissolved Solids: Total g/I pH (when analyzed) t 3 units TOC U • to mgA Chloride 6 L mgA Arsenic mgA Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia <o• mg/I (Amnioma Nirogen; NH, as N: Arrvrionia Noogan• 1010) TKN as N Mgt GW -5g Rev. 1112005 Phosphorus: Total as P—— Mgll mg/I Orthophosphate — A 1- Aluminum mg/I m gll Be - Barium g/I Ca - Calcium mg/I Cd - Cadmium mg/I mg/I Chromium: Total Cu - Copper Fe - Iron mg/l mg ll Hg - Mercury mgA K - Potassium Mg -magnesium —g g/I Mn - Manganese _�m Zn -Zinc Other (Specify Compounds and Concentration Units) ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? Yes_[_(I)No. method #_ (0) VOC_ : method #-- - : method #_ (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING:-^' _ mg/1 vies wcunu* +rn, rn ^ �a N .µ��P44� v .{ n� ' COMPLIANCE REPORT FORM (thele: VM MPN mealoe M1r tare/ WNM unplaq Ll G yy ,yy hp%EyDy17H(Itl':2T geiT �,.. od�e�8%779.722+. s �. r':• Please Print Clearly orT a FACILITY INFORMATION y Type 7Facility PERMIT No. FJlPIRATION OATS' A/5 I� u+�es rite. Facility Nemo: M "" r units �, nDD iS I % NPDOl UIC Permit Name (if different): Address: TYPE OF PER OPERATION BEING MONITORED mgA Count .1 ry sw .S RemedateM Inllaraecn Gallery AAdY MyfY1Q� Contact Person:RoLmy m.G Telephorre/F: 1!c2.r{j/�_l00'7 No. of wells to be sampled:_ ✓ Spray Flaw __Ramemlwn: a —Land APPIkei n of Shwgo 'Well LocatioNSite Name: r,_•IJT e„y} I�ul L-4,�[ — VYatar Source Heat Pump v4", Pw Total Ammonia --0,1, mgn Other. Well Identification Nxmbar (from Permit): – Ir WELL WAS DRY Well Depth: 16 • l ft Well Diameter, in. � me of =! na• cneuc here System Influeni/Eftluent Only (Attach Lab Reports.) Screened lntervaLiI.r} ft. to Ib�q tl. Semplefstromsysfem: �fflueM For Remediation InaMen< myrL(rotalvocconcenuadonl mgiL Depth to Water Level: 4 • o f, below measuring point. Olnfluent Emu.nt (Tam vac Corwentratlonl Measuring Point is 1, $ ft. above land sudace. Relathre M.P. Elevation in ft. ypc R.ma al % Gallons of water pumpeftailed before II Sic Date sample collected:_ c - c Date sample analyzed: FIELD ANALYSIS: PH c•63 Specific Conductance Laboratory Name: r1 V '!O �v. Temp. 0,44 OC Odor Alan . Appearance rr,. A Certification No. PARAMETERS (Samples for metals were collected unfiltered—YES _ NO and field acidiRed YES _NO.) NOTE: Values should reflect dissolved and colloidal concentrations. 2 mgA Ni -Nickel mgA COD mgll Nibite (N%) as N L O O mgA p /100m1 Nitrate (NO,) as N G O O Z mgn Pb - Lead mnn CORD= MF eca _ mg/1 CoHfonn: MF Total /100ml (thele: VM MPN mealoe M1r tare/ WNM unplaq Ll G mgA Dissolved Solids: Total 2 mg/I PH (when analyzed) 5 G ; units TOC l N mgA Chloride mg/I Arsenic mgA Grease an Oils mg/I Phenol mg/I Sulfate mgA Specific Conductance uMhos Total Ammonia --0,1, mgn (Annwnta Nemgen; NH, es N; AminoNa Nitrogen. Total) TKN as N mgA Phosphorus: Total as P _ mg/1 Orthophosphate mgll A F Aluminum mgA Be - Barium mgA Ca - Calcium mgA Cd - Cadmium mgA Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mgA Hg - Mercury mg/I K - Potassium mgA Mg - Magnesium mgn Mn - Manganese mg/I GM9 Signature of Permmae(4/Aulhorized Ag"o P."iiOnn5 L Zn - Zinc Other (Specify Compounds and Concentration Units) ORGANICS: (by GC, GC/MS. HPLC) (spaciy test and method P. ATTACH LAB REPORT.) Report Attached? Yes_V—(1) No__ (0) VOC : method it= method #-- method =method #= mu1hM iL— TER QUALITY MONITORING: REPORT FORM Name: Name (if Address: SUBMIT FORM ON YELLOW PAPER ONLY aclPerson: 'Q�Telephone#:;-;1-y2/-_10o-7 Locetlon/Site Name:Re_.4gp" lejej No. ofwells to be sampled: Well Depth: :.S_ ft. Well Diameter:_in. let Om d sampling, Check here Screened Interval: 5 ft. to 1$' ft. Semple k ham system: Depth to Water Level: y. s ft. below measuring point. ❑ Influent Oftluent Measuring Point is_g,- ft above land surface. Relative M.P. Elevation in ft. Gallons of water pumped1balled before sampling,.__,E. 9 Date sample collected: - FIELDANALYSIS: pH L.49 Specific Conductance uMhos Temp. 14.4 C- OC Odor #I. ) cli Sq jl; ,, Appearance aryt / Ph as T ,,in 1nor-01#11 ra WMEMENNo F PERMITTED OPERATION BEING MONITORED Lagoon _ ReavdWoa: IMikaaon Gallmy Splay Fitltl _Remedalbn: Rolary DaIrIbulor _Land Application d Sludge Water Scarce Most Pump Concentration) Name: PARAMETERS (Samples for metals were collected unfiltered ... YES _ NO and field acidifloc _YES _NO.) NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/1 Nitrite (NO2) as IN p, iJ L, mg/1 Ni - Nickel Coliform: MF Fecal -.70 /100m1 Nitrate (NO3) as N < mgll Pb - Lead Coliform: MF Total /100ml (Nob: a MPN methal W highly kuA eaTO..) Dissolved Solids: Total to p i pH (when analyzed) t-, rc 9 TOC It 7, O Chloride [yT Arsenic Grease and Oils Phenol Sulfate Specific Conductance Total Ammonia S./ tArnnonla Nitrogen; NH3 as N; Ammonla Nbogen. Total) TKN as N mg/1 units mg/I mg/I mgA Mg/1 Mg/1 mg/I uMhos mgA Phosphorus: Total as P T mgll Orthophosphate mg/I A I- Aluminum mg/I Be - Barium mgn Ca - Calcium mgA Cd - Cadmium mg/l Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/1 K - Potassium mg/I Mg - Magnesium mgA Mn - Manganese m9/1 Zn -Zino Other (Specify Compounds and Concentration Units) mg/I mg/I mgll ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? Yes ✓ (1) No— (0) VOC : method #= method If= method #_ __ TER QUALITY MONITORING: REPORT FORM Name: Name [if Address: SUBMIT FORM ON YELLOW PAPER ONLY act Person: .4V �V Alrj.f-- a -A Telephone#: AS�•�f26-100 LocationfSite Name: No. of wells to be sampled: I I� Well Depth:__ft. Well Diameteriin. —let time of sampNq, Check ham Screened Interval: ft. to pf ft Semple is Irom system: Depth to Water Leve(: 4. 7 ft. below measuring point. ❑Influent Dfflue Measuring Point is_: ft. above land surface. Relative M.P. Elevation in ft._ Gallons of water pumped/bailed before sampling:J�Q_ Data sample collected: t 1 — Specific Conductance umrws °C Odor :TO na Appearance F PERMITTED OPERATION BEING MONITORED tagouiri Renvaellon: Infiltration Galery Spray Field _Remedwaon: Rotary Dishibulor _Lend Application or Sludge Water Source Heat Pump Other. mglL (Total VOC Concentration) men. (Total VOC Concemnt m) Name: i No. PARAMETERS (Samples for metals were collected unfiltered—YES _NO and field acidified—YES _NO.) NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/l Nitrite (NO2) as N < p , p Z mg/I Ni - Nickel Coliform: MF Fecal -C ( 11 00m Nitrate (NO3) as N p .0,21 mgA Pb - LeadV Coliform: MF Total /100ml (NoW: Un MPN mnhoe for Ng* IurbM annpW) mgA Dissolved Solids: Total b 9 mg/I pH (when analyzed) S OT, units TOC 3.8 mg/I Chloride 13 mg/I Arsenic mg/1 Grease and 011s mg/I Phenol mg/I Sulfate mg/l Specific Conductance uMhos Total Ammonia < 0.,;i% mg/1 (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) mg/I TKN as N mg/I Phosphorus: Total as P mgA Orthophosphate mg/I A 1- Aluminum mg/I Ba - Barium mgA Ca - Calcium mgA Cd - Cadmium mg/1 Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mgll Hg - Mercury mg/I K - Potassium mg/I Mg - Magneslum mg/I Mn - Manganese mgA GW -59 Signature of Rev. 11/2005 Zn - ZinC Other (Specify Compounds and Concentration Units) ORGANICS: (by GC, GC/MS. HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? yesJ'el—'(1) No_(0) VOC : method f� method iK method #= method tit 1.2 mg/I mgA mgA TER QUALITY MONITORING: REPORT FORM Name: Name (if i Address: SUBMIT FORM ON YELLOW PAPER ONLY act Person: �I I LjqK Tele0hone#: 15].r(246-100-7 Location/Site Name: No. of wells to be sampled: Well Depth:/s- ft. Well Diameters in. at am of smnpgng, Check here Screened Interval: $ fl. to 81—ft.Semple is from system: Depth to Water Level: 9q ft. below measuring point. ❑ Influent Measuring Point Is_3_ R. above land surface. Relative M.P. Elevation it Gallons of water Dumped/balled before sampling: .r. b Date sample collected:_ D/1• PERMITTED OPERATION BEING MONITORED Own Ramedatiom InflWation Grery my Field _Remedaliom otaq Distributor _Land Application or sludge War Source Feat Pump Other: ,.k_m9FL (Total VOC concentration) mt mall. (Total VOC concentration) Removal % �pemnc (.oncuuanw �^ °C Odor nonL Appearance C-4ce, 4 rtit iI0Tui6 Laboratory Name: PARAMETERS (Samples for metals were collected unfiltered YES —NO and field acidified YES _NO.) NOTE: Values should reflect dissolved and colloidal concentrations. COD mgA Nitrite (NO,) as N D . e a, mg/I Ni -Nickel Coliform: MF Fecal < ( /100ml Coliform: MF Total /100ml (Hots U» WN rnee W hig* Wd sunga�) m9/1 Dissolved Solids: Total 3 3 mgA pH (when analyzed) 9"('1 units TOC r? S? mg/I Chloride 10, mgA Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate mgA Specific Conductance uMhos Total Ammonia C O 'i mgA (Amnonia Mtmgen; NH3 as N; Ammonia Nlrogan, TOW mgA TKN as N - mgA Nitrate (NO,) as N < D . D .>\ m9/1 Phosphorus: Total as P mg/l Orthophosphate mgA A 4 Aluminum mgA Be - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mgA Cu - Copper mgA Fe - Iron mgA Hg - Mercury mgA K - Potassium mgA Mg - Magnesium mgA Mn - Manganese mg/1 Pb - Lead Zn - Zinc Other (Specify Compounds and Concentration Units) --------------- ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ACH LAB REPORT.) Report Attached? Yes (1) No_ (D) VOC : method #= method #= method #= mg/1 mgA mg/I /ch so is" A« -rp5 mwlr _ �g 3 Nov 0�-v rte. m, ti- 1 o S (� -7 1 TOS Mv4's -j10 1"p5 NwU6 C,S1 CYh 10�-4� .4y1 11, 5= 3si fig� , ->O 13 ,411 1nl*-leIl /-to bczfow m},, �h ml4uolZt64, TDS-G plov , �V) 13 InIftl4its a, 3 G, 7 Y, 9, /U bebv u n mw 06o G/.,3 T ds Aml 4;1-41f m w I, �-, `, 7, �, .� �o _ D e-l"D mw �` 5 TDs 5-Z) 9 e�,sr Ph �O G i- 4mc0. Yiwu4 f 3. ?l �wK v S— "�wN$ .,gyp V - -TUC m w5 b. Y � 2-� � � m w�- In mw `/ hr�u 7 31f-3 .,gyp V - ioc Mlw 3 14.3 - Ml we.tt GL' e-belo".) C14 !h•w►A4 ,#p6 t 7L0/3 1- 10 a.(t QoA ov i�. •5� t'`.:. P i� i P S int" 5 - Y's, b%'ii Wit Tf)c Mwok;,L _ 1g'.9 fns.* )_ 1!. G pd" it �L- 4p ! Fo u. - MAO 0 � ��c 4 n,a« E by m Atw2" In � 7 N300 Environmental Chemists, Inc. !e:n: rocche7m6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax sM 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax - 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 15, 2016 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report M 2016-17198 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-41452 Site: MW -1 11/30/2016 10:45 AM Water Will Coggins Test Method Results Date Analyzed Color color Grey 11/30/2016 Depth to water, ft. Depth to water. Ft. 12.8 feet 11/30/2016 Ammonia Nitrogen EPA 350.1 <0.2mg/L 12/01/2016 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/30/2016 Odor Qualitative Slight 11/30/2016 Total Dissolved Solids (TDS) SM 2540 C 138 mg/L 12/01/2016 Temperature SM 25508 19.3C 11/30/2016 Chloride SM 4500 CI E 20 mg/L 12/06/2016 pH SM 4500 H B 4.92 units 11/30/2016 Total Organic Carbon (TOC) SM 5310 B 5.2 mg/L 12/06/2016 1,1,1,2 -Tetrachloroethane SM 6200C <0.50pg/L 12/7/2016 1,1,1 -Trichloroethane SM 6200C <0.50Ng/L 12/7/2016 1,1,2,2 -Tetrachloroethane SM 6200C <0.50pg/L 12/7/2016 1,1,2 -Trichloroethane SM 0200C <0.50Ng/L 12/7/2016 1,1-Dichloroethane SM 6200C <0.50pg/L 12/7/2016 1,1-Dichloroethene SM6200C <0.50pg/L 12/7/2016 1,1-Dichloropropene SM 62000 < 0.50 ug/L 12/7/2016 1,2,3-Trichlorobenzene SM 6200C <0.50pg/L 12/7/2016 1,2,3-Trichloropropane SM 62000 < 0.50 pg/L 12/7/2016 1,2,4-Trichlorobenzene SM 62000 < 0.50 ug/L 12/7/2016 1,2,4-Trimethylbenzene SM 6200C <0.50Ng/L 12/7/2016 1,2-Dibromo-3-Chloropropane SM 6200C <0.50Ug/L 12/7/2016 1,2-Dibromoethane SM 6200C < 0.50 Ng/L 12/7/2016 1,2 -Dichlorobenzene SM 6200C < 0.50 Ng/L 12/7/2016 1,2-Dichloroethane SM 62000 < 0.50 Ng/L 12/7/2016 1,2-Dichloropropane SM 6200C <0.50Ng/L 12/7/2016 Report #': 2016-17198 Page 1 of 30 Environmental Chemists, Inc. IL 1 / 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax SM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 15, 2016 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2016-17198 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene SM 6200C < 0.50 Ng/L 12/7/2016 1,3 -Dichlorobenzene SM 62000 < 0.50 ug/L 12/7/2016 1,3-Dichloropropane SM 62000 < 0.50 Ng/L 12/7/2016 1,4 -Dichlorobenzene SM 6200C <0.50pg/L 12/7/2016 2,2-Dichloropropane SM 62000 < 0.50 pg/L 12/7/2016 2-Chlorotoluene SM 6200C < 0.50 Ng/L 12/7/2016 4-Chlorotoluene SM 62000 < 0.50 Ng/L 12/7/2016 Benzene SM 62000 < 0.50 Ng/L 12/7/2016 Bromobenzene SM 62000 < 0.50 Ng/L 12/7/2016 Bromochloromethane SM 62000 < 0.50 pg/L 12/7/2016 Bromodichloromethane SM 82000 < 0.50 pg/L 12/7/2016 Bromoform SM 62000 < 0.50I1g/L 12/7/2016 Bromomethane SM 6200C < 0.50 Ng/L 12/7/2016 Carbon tetrachloride SM 62000 < 0.50 Ng/L 12/7/2016 Chlorobenzene SM 62000 < 0.50 Ng/L 12/7/2016 Chloroethane SM 62000 < 0.50 Ng/L 12/7/2016 Chloroform SM 62000 < 0.50 Ng/L 12/7/2016 Chloromethane SM 62000 < 0.50 Ng/L 12/7/2016 cis-1,2-Dichloroethene SM 6200C < 0.50 Ng/L 12/7/2016 cis-1,3-Dichloropropene SM 62000 < 0.50 pg/L 12/7/2016 Dibromochloromethane SM 62000 < 0.50 Ng/L 12/7/2016 Dibromomethane SM 62000 < 0.50 pg/L 12/7/2016 Dichlorodifluoromethane SM 62000 < 0.50 Ng/L 12/7/2016 Ethylbenzene SM 62000 < 0.50 pg/L 12/7/2016 Hexachlorobutadiene SM 62000 < 0.50 Ng/L 12/7/2016 Isopropylbenzene SM 62000 < 0.50 Ng/L 12/7/2016 M+P Xylene SM 62000 < 1.00 pg/L 12/7/2016 Methylene chloride SM 62000 < 0.50 Ng/L 12/7/2016 Naphthalene SM 62000 < 0.50 Ng/L 12/7/2016 n-Butylbenzene SM 6200C < 0.50 pg/L 12/7/2016 Report #:: 2016-17198 Page 2 of 30 :envirachem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Albemarle Utility Date of Report: Dec 15, 2016 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2016-17198 Project ID: Monitoring Wells n-Propylbenzene SM 6200C < 0.50 pg/L 12/7/2016 ortho-Xylene SM 6200C < 0.50 pg/L 12/7/2016 p-Isopropyltoluene SM 6200c < 0.50 Ng/L 12/7/2016 sec-Butylbenzene SM 62000 < 0.50 Ng/L 12/7/2016 Styrene SM 6200c < 0.50 pg/L 1217/2016 tert-Butylbenzene SM 6200C < 0.50 Ug/L 12/7/2016 Tetrachloroethene SM 6200c < 0.50 Ng/L 12/7/2016 Toluene SM 6200c < 0.50 pg/L 12/7/2016 Trans-1,2-Dichloroethene SM 6200C < 0.50 Ng/L 12/7/2016 Trans- l,3-dichloropropene SM 6200c <0.50Ng/L 12/7/2016 Trichloroethene SM 6200c < 0.50 pg/L 12/7/2016 Trichlorofluoromethane SM 62000 < 0.50 pg/L 12/7/2016 Vinyl chloride SM 6200C < 0.50 pg/L 12/7/2016 Fecal Coliform SM 92220 MF <1 Colonies/100ml- 11/30/2016 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 0.07 mg/L 12/01/2016 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/09/2016 ReportA:: 2016-17198 Page 3 0! 30 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax SM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Date of Report: Dec 15, 2016 Customer PO #: Customer ID: 09110024 Report #: 2016-17198 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-41453 Site: MW -2 11/30/2016 10:35 AM Water Will Coggins Test Method Results Date Analyzed Color Color Grey 11/30/2016 Depth to water, ft. Depth to water, Ft. 7.2 feet 11/30/2016 Ammonia Nitrogen EPA 350.1 0.5 mg/L 12/01/2016 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/30/2016 Odor Qualitative Slight 11/30/2016 Total Dissolved Solids (TDS) SM 2540 c 177 mg/L 12/01/2016 Temperature SM2550B 19.8C 11/30/2016 pH SM 4500 H B 5.86 units 11/30/2016 Total Organic Carbon (TOC) SM 5310 B 16.2 mg/L 12/06/2016 1,1,1,2 -Tetrachloroethane SM 6200C <0.50Ng/L 12/7/2016 1,1,1 -Trichloroethane SM 6200C <0.50pg/L 12/7/2016 1,1,2,2 -Tetrachloroethane SM 6200C <0.50Ng/L 12/7/2016 1,1,2 -Trichloroethane SM 6200C <0.50pg/L 12/7/2016 1,1-Dichloroethane SM 6200C <0.50Ng/L 12/7/2016 1,1-Dichloroethene SM 6200C <0.50pg/L 12/7/2016 1,1-Dichloropropene SM 6200C <0.50Ng/L 12/7/2016 1,2,3-Trichlorobenzene SM 6200C <0.50Ng/L 12/7/2016 1,2,3-Trichloropropane SM 6200C < 0.50 Ug/L 12/7/2016 1,2,4-Trichlorobenzene SM 6200C <0.50ug/L 12/7/2016 1,2,4-Trimethylbenzene SM 6200C <0.50Ng/L 12/7/2016 1,2-Dibromo-3-Chloropropane SM 6200C <0.50Ng/L 12/7/2016 1,2-Dibromoethane SM 6200C <0.50pg/L 12/7/2016 1,2 -Dichlorobenzene SM 6200C < 0.50 Ng/L 12/7/2016 1,2-Dichloroethane SM 8200C <0.50ug/L 12/7/2016 1,2-Dichloropropane SM 6200C <0.50Ng/L 12/7/2016 1,3,5-Trimethylbenzene SM 6200C <0.50Ng/L 12/7/2016 Report #:: 2016-17198 Page 4 of 30 Environmental Chemists, Inc. & 6602 Windmill Way, 1Niimington, NC 28405 -c)10342.02231-ab • 910.39'_.4424 Fax 710 8owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/ Fax " 255-A Wilmington I lighway, Jacksonville, NC 28510 • 910.317.5843 Lab/ Fax ANALYTICAL & CONSULTING CHEMISTS into(genvironmentalchemists.com Albemarle Utility Revised Report: Dec 27, 2016 862 Holiday Island Road Original Report Date: Dec 15, 2016 Hertford NC 27944 Report #: 2016-17198 Attention: Anita Elliott Customer ID: 09110024 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-41453 Site: MW -2 11/30/2016 10:35 AM Water Will Coggins Test Method Results Date Color cwor Grey 11/30/2016 Depth to water, ft. DePm to water. Pt 7.2 feet 11/30/2016 Ammonia Nitrogen EPA 3501 0.5 mg/L 12/01/2016 Gallons bailed before sampling caHwsBa1Wbefore aamgino 5.Ogallons 11/30/2016 Odor oualnative Slight 11/30/2016 Total Dissolved Solids (TDS) SM 2540 C 177 mg/L 12/01/2016 Temperature SM 25506 19.8C 11/30/2016 Chloride SM 4500 CI E 54 mg/L 12/21/2016 pH SM 4500 H e 5.86 units 11/3012016 Total Organic Carbon (TOC) SM 5310 a 16.2 mg/L 12/06/2016 1,1,1,2 -Tetrachloroethane SM 620C <0.50Ug/L 12/7/2016 1,1,1 -Trichloroethane SM 6200C <0.50pg/L 12/7/2016 1,1,2,2 -Tetrachloroethane SM 6200C <0.50Ng/L 12/7/2016 1,1,2 -Trichloroethane SM 6200C <0.50pg/L 12/7/2016 1,1-Dichloroethane SM 6200C <0.50pg/L 1217/2016 1,1-Dichloroethene SM 62W <0.50ug/L 12/7/2016 1,1-Dichloropropene SM 62W <0.50pg/L 12/7/2016 1,2,3-Trichlorobenzene SM62000 <0.50pg/L 12/7/2016 1,2,3-Tdchloropropane SM62000 <0,50Ug/L 12/7/2016 1,2,4-Trichlorobenzene SM 6200C < 0.50 u9/L 12/72016 1,2,4-Trimethylbenzene SMe2000 <0.5041g/L 12!7/2016 1,2-Dibromo-3-Chloropropane SM 6200C <0.50pg/L 12/72016 1,2-Dibromoethane SM 8200C < 0.50 pg/L 12/7/2016 1,2 -Dichlorobenzene SM 6200C < 0.50 ug/L 12/7/2016 1,2-Dichloroethane SM 6200C <0.50pg/L 12/7/2016 1,2-Dichloropropane SM 6200C <0.50Ng/L 12/7/2016 ReponN 2016-17196 Pape 4 of 30 Environmental Chemists, Inc. 1 I 1J 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 'sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott 27944 Date of Report: Dec 15, 2016 Customer PO #: Customer ID: 09110024 Report #: 2016-17198 Project ID: Monitoring Wells 1,3 -Dichlorobenzene SM 6200C < 0.50 Ng/L 12/7/2016 1,3-Dichloropropane SM 6200C < 0.50 u9/L 12/7/2016 1,4 -Dichlorobenzene SM 6200C < 0.50 Ng/L 12/7/2016 2,2-Dichloropropane SM 62000 < 0.50 Ng/L 12/7/2016 2-Chlorotoluene SM 62000 < 0.50 pg/L 12/7/2016 4-Chlorotoluene SM 6200C < 0.50 pg/L 12/7/2016 Benzene SM 6200C < 0.50 pg/L 12/7/2016 Bromobenzene SM 6200C < 0.50 pg/L 12/7/2016 Bromochloromethane SM 62000 < 0.50 Ng/L 12/7/2016 Bromodichloromethane SM 62000 < 0.50 Ng/L 12/7/2016 Bromoform SM 6200C < 0.50 Ng/L 12/7/2016 Bromomethane SM 62000 < 0.50 pg/L 12/7/2016 Carbon tetrachloride SM 62000 < 0.50 Ng/L 12/7/2016 Chlorobenzene SM 6200C < 0.50 ug/L 12/7/2016 Chloroethane SM 62000 < 0.50 Ng/L 12/7/2016 Chloroform SM 62000 < 0.50 Ng/L 12/7/2016 Chloromethane SM 6200C < 0.50 Ng/L 12/7/2016 cis-1,2-Dichloroethene SM 6200C <0.50pg/L 12/7/2016 cis-1,3-Dichloropropene SM 62000 < 0.50 pg/L 12/7/2016 Dibromochloromethane SM 6200c < 0.50 Ng/L 12/7/2016 Dibromomethane SM 6200c < 0.50 pg/L 12/7/2016 Dichlorodifluoromethane SM 62000 < 0.50 Ng/L 12/7/2016 Ethylbenzene SM 62000 < 0.50 Ng/L 12/7/2016 Hexachlorobutadiene SM 62000 < 0.50 pg/L 12/7/2016 Isopropylbenzene SM 62000 < 0.50 Ng/L 12/7/2016 M+P Xylene SM 6200C < 1.00 ug/L 12/7/2016 Methylene chloride SM 62000 < 0.50 Ng/L 12/7/2016 Naphthalene SM 6200C < 0.50 pg/L 12/7/2016 n-Butylbenzene SM 62000 < 0.50 Ng/L 12/7/2016 n-Propylbenzene SM 62000 < 0.50 Ng/L 12/7/2016 Report #" 201 6-1 71 98 Page 5 of 30 Environmental Chemists, Inc. envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax hkh�s" 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott 27944 Date of Report: Dec 15, 2016 Customer PO M Customer ID: 09110024 Report M 2016-17198 Project ID: Monitoring Wells ortho-Xylene SM 6200C < 0.50 pg/L 12/7/2016 p-Isopropyltoluene SM 62000 < 0.50 Ng/L 12/7/2016 sec-Butylbenzene SM 6200c < 0.50 Ng/L 12/7/2016 Styrene SM 6200c < 0.50 pg/L 12/7/2016 tert-Butylbenzene SM 6200c < 0.50 Ng/L 12/7/2016 Tetrachloroethene SM 6200c < 0.50 ug/L 12/7/2016 Toluene SM 6200c < 0.50 Ng/L 12/7/2016 Trans-1,2-Dichloroethene SM 6200c < 0.50 Ug/L 12/7/2016 Trans-1,3-dichloropropene SM 62000 < 0.50 ug/L 12/7/2016 Trichloroethene SM 6200c < 0.50 pg/L 12/7/2016 Trichlorofluoromethane SM 6200C < 0.50 Ug/L 12/7/2016 Vinyl chloride SM 6200c < 0.50 Ng/L 12/7/2016 Fecal Coliform SM9222DMF <1 Colonies/100mL 11/30/2016 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 0.07 mg/L 12/01/2016 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/09/2016 Report #:: 201 6-171 98 Page 6 of 30 envirochem su ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott Lab ID Sample ID: 16-41454 Site: MW -3 Test Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environ men to Ichemists.com Date of Report: Dec 16, 2016 Customer PO M 27944 Customer ID: 09110024 Report M 2016-17198 Project ID: Monitoring Wells Color Depth to water, ft. Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Organic Carbon (TOC) 1,1,1,2 -Tetrachloroethane 1,1,1 -Trichloroethane 1,1,2,2 -Tetrachloroethane 1,1,2 -Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1,2,3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane 1,2 -Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane Method Collect Date/Time Matrix 11/30/2016 11:30AM Water Results Sampled by Will Coggins Date Analyzed Color GreyNery Turbid 11/30/2016 Depth to water, Ft. 6.6 feet 11/30/2016 EPA 350.1 3.8 mg/L 12/01/2016 Gallons Bailed before sampling 5.0 gallons 11/30/2016 Qualitative Mild Sulfur 11/30/2016 SM 2540 c 214 mg/L 12/01/2016 SM 2550 8 19.6 C 11/30/2016 SM 4500 Cl E 54 mg/L 12/06/2016 SM 4500 H B 6.23 units 11/30/2016 SM 5310 B 18.1 mg/L 12/06/2016 SM 6200C < 0.50 Ng/L 12/7/2016 SM 62000 < 0.50 pg/L 12/7/2016 SM 62000 < 0.50 pg/L 12/7/2016 SM 6200C < 0.50 ug/L 12/7/2016 SM 6200c < 0.50 ug/L 12/7/2016 SM 62000 < 0.50 pg/L 12/7/2016 SM 62000 < 0.50 pg/L 12/7/2016 SM 6200C < 0.50 pg/L 12/7/2016 SM 6200C < 0.50 pg/L 12/7/2016 SM 62000 < 0.50 pg/L 12/7/2016 SM 6200c < 0.50 pg/L 12/7/2016 SM 62000 < 0.50 ug/L 12/7/2016 SM 62000 < 0.50 ug/L 12!7/2016 SM 62000 < 0.50 pg/L 12/7/2016 SM 6200c < 0.50 Ng/L 12/7/2016 SM 62000 < 0.50 pg/L 12/7/2016 Report #:'. 201617198 Page 7 of 30 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road; Manteo, NC 27954 • 252.473.5702 Lab/Fax SM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL R CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 15, 2016 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2016-17198 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene SM 6200C <0.50pg/L 12/7/2016 1,3 -Dichlorobenzene SM 6200C <0.50ug/L 12/7/2016 1,3-Dichloropropane SM 6200C <0.50Ng/L 12/7/2016 1,4 -Dichlorobenzene SM 6200C < 0.50 Ng/L 12/7/2016 2,2-Dichloropropane SM 62000 < 0.50 pg/L 12/7/2016 2-Chlorotoluene SM 62000 < 0.50 Ng/L 12/7/2016 4-Chlorotoluene SM 6200C < 0.50 Ng/L 12/7/2016 Benzene SM 62000 < 0.50 Ug/L 12/7/2016 Bromobenzene SM 6200C < 0.50 Ng/L 12/7/2016 Bromochloromethane SM 6200C < 0.50 Ng/L 12/7/2016 Bromodichloromethane SM 62000 < 0.50 Ng/L 12/7/2016 Bromoform SM 62000 < 0.50 Ng/L 12/7/2016 Bromomethane SM 62000 < 0.50 ug/L 12/7/2016 Carbon tetrachloride SM 6200C < 0.50 Ng/L 12/7/2016 Chlorobenzene SM 6200C < 0.50 Ng/L 12/7/2016 Chloroethane SM 6200C < 0.50 pg/L 12/7/2016 Chloroform SM 6200C < 0.50 pg/L 12/7/2016 Chloromethane SM 62000 < 0.50 Ng/L 12/7/2016 cis-1,2-Dichloroethene SM 62000 < 0.50 pg/L 12/7/2016 cis-1,3-Dichloropropene SM 6200C <0.50pg/L 12/7/2016 Dibromochloromethane SM 62000 < 0.50 pg/L 12/7/2016 Dibromomethane SM 62000 < 0.50 Ng/L 12/7/2016 Dichlorodifluoromethane SM 62000 < 0.50 Ug/L 12/7/2016 Ethylbenzene SM 62000 < 0.50 Ug/L 12/7/2016 Hexachlorobutadiene SM 5200C < 0.50 ug/L 12/7/2016 Isopropylbenzene SM 62000 < 0.50 Ng/L 12/7/2016 M+P Xylene SM 62000 < 1.00 Ng/L 12/7/2016 Methylene chloride SM 62000 < 0.50 pg/L 12/7/2016 Naphthalene SM 62000 < 0.50 pg/L 12/7/2016 n-Butylbenzene SM 6200C < 0.50 Ng/L 12/7/2016 Report #" 201 6-171 98 Page 8 of 30 Environmental Chemists, Inc. 4 1 1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax M. 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 tab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott 27944 Date of Report: Dec 15, 2016 Customer PO #: Customer ID: 09110024 Report #: 2016-17198 Project ID: Monitoring Wells n-Propylbenzene SM 62000 < 0.50 pg/L 12/7/2016 ortho-Xylene SM 62000 < 0.50 pg/L 12/7/2016 p-Isopropyltoluene SM 6200C < 0.50 pg/L 12/7/2016 sec-Butylbenzene SM 5200C < 0.50 pg/L 12/7/2016 Styrene SM 62000 < 0.50 pg/L 12/7/2016 tert-Butylbenzene SM 6200C < 0.50 pg/L 12/7/2016 Tetrachloroethene SM 62000 < 0.50 pg/L 12/7/2016 Toluene SM 62000 79.8 pg/L 12/9/2016 Trans-1,2-Dichloroethene SM 6200C <0.50pg/L 12/7/2016 Trans-1,3-dichloropropene SM 6200C <0.50pg/L 12/7/2016 Trichloroethene SM 62000 < 0.50 pg/L 12/7/2016 Trichlorofluoromethane SM 6200C < 0.50 pg/L 12/7/2016 Vinyl chloride SM 62000 < 0.50 pg/L 12/7/2016 Fecal Coliform SM 9222D MF 77 Colonies/100ml- 11/30/2016 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 0.32 mg/L 12/01/2016 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/09/2016 Report # 2016-17198 Page 9 of 30 envirochem SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Albemarle Utility Date of Report: Dec 15, 2016 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2016-17198 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-41455 Site: Mw -4 11/30/2016 11:40 AM Water Eric McHorney Test Method Results Date Analyzed Color Color Lt Tan 11/30/2016 Depth to water, ft. Depth to Water, Ft. 7.1 feet 11/30/2016 Ammonia Nitrogen EPA 350.1 1.1 mg/L 12/01/2016 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/30/2016 Odor Qualitative Mild Sulfur 11/30/2016 Total Dissolved Solids (TDS) SM2540C 154 mg/L 12/01/2016 Temperature SM2550B 19.3C 11/30/2016 Chloride SM 4500 Cl E 10 mg/L 12/06/2016 pH SM4500HB 6.24 units 11/30/2016 Total Organic Carbon (TOC) SM 5310 B 16.6 mg/L 12/06/2016 1,1,1,2 -Tetrachloroethane SM 6200C <0.50pg/L 12/8/2016 1,1,1 -Trichloroethane SM 6200C <0.50pg/L 12/8/2016 1,1,2,2 -Tetrachloroethane SM 6200C <0.50pg/L 12/8/2016 1,1,2 -Trichloroethane SM 6200C <0.50pg/L 12/8/2016 1,1-Dichloroethane SM 6200C <0.50pg/L 12/8/2016 1, 1 -Dichloroethene SM 6200C <0.50pg/L 12/8/2016 1,1-Dichloropropene SM 6200C <0.50pg/L 12/8/2016 1,2,3-Trichlorobenzene SM 6200C <0.50pg/L 12/8/2016 1,2,3-Trichloropropane SM 6200C <0.50pg/L 12/8/2016 1,2,4-Trichlorobenzene SM 6200C <0.50pg/L 12/8/2016 1,2,4-Trimethylbenzene SM 6200C <0.50pg/L 12/8/2016 1,2-Dibromo-3-Chloropropane SM 62000 < 0.50 pg/L 12/8/2016 1,2-Dibromoethane SM 6200C <0.50pg/L 12/8/2016 1,2 -Dichlorobenzene SM 6200C <0.50pg/L 12/8/2016 1,2-Dichloroethane SM 6200C <0.50pg/L 12/8/2016 1,2-Dichloropropane SM 6200C <0.50pg/L 12/8/2016 Report #:: 2016-17198 Page 10 of 30 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott 27944 Date of Report: Dec 15, 2016 Customer PO #: Customer ID: 09110024 Report #: 2016-17198 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene sM620oc <0.50pg/L 12/8/2016 1,3 -Dichlorobenzene SM 62000 < 0.50 Ng/L 12/8/2016 1,3-Dichloropropane SM 6200C < 0.50 Ng/L 12/8/2016 1,4 -Dichlorobenzene SM 6200C < 0.50 Ng/L 12/8/2016 2,2-Dichloropropane SM 6200C < 0.50 pg/L 12/8/2016 2-Chlorotoluene SM 62000 < 0.50 pg/L 12/8/2016 4-Chlorotoluene SM 62000 < 0.50 Ng/L 12/8/2016 Benzene SM 6200C < 0.50 Ng/L 12/8/2016 Bromobenzene SM 62000 < 0.50 pg/L 12/8/2016 Bromochloromethane 6M 62000 < 0.50 Ng/L 12/8/2016 Bromodichloromethane SM 62000 < 0.50 Ng/L 12/8/2016 Bromoform SM 62000 < 0.50 Ng/L 12/8/2016 Bromomethane SM 62000 < 0.50 pg/L 12/8/2016 Carbon tetrachloride SM 62000 < 0.50 ug/L 12/8/2016 Chlorobenzene SM 6200C < 0.50 pg/L 12/8/2016 Chloroethane SM 6200C < 0.50 pg/L 12/8/2016 Chloroform SM 62000 < 0.50 pg/L 12/8/2016 Chloromethane SM 6200C < 0.50 Ng/L 12/8/2016 cis-1,2-Dichloroethene SM 6200C <0.50Ng/L 12/8/2016 cis-1,3-Dichloropropene SM 6200C <0.50pg/L 12/8/2016 Dibromochloromethane SM 62000 < 0.50 Ng/L 12/8/2016 Dibromomethane SM 6200C < 0.50 Ng/L 12/8/2016 Dichlorodifluoromethane SM 6200C < 0.50 Ng/L 12/6/2016 Ethylbenzene SM 62000 < 0.50 pg/L 12/8/2016 Hexachlorobutadiene SM 6200C < 0.50 pg/L 12/8/2016 Isopropylbenzene SM 62000 < 0.50 ug/L 12/8/2016 M+P Xylene SM 62000 < 1.00 Ng/L 12/8/2016 Methylene chloride SM 6200C < 0.50 Ng/L 12/8/2016 Naphthalene SM 6200C < 0.50 Ng/L 12/8/2016 n-Butylbenzene SM 6200C < 0.50 ug/L 12/8/2016 Report # 2016-17198 Page 11 of 30 envirochem SM ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Albemarle Utility Date of Report: Dec 15, 2016 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2016-17198 Project ID: Monitoring Wells n-Propylbenzene SM e200C < 0.50 Ug/L 12/8/2016 ortho-Xylene SM 62000 < 0.50 Ng/L 12/8/2016 p-Isopropyltoluene SM 6200C < 0.50 Ng/L 12/8/2016 sec-Butylbenzene SM e200C < 0.50 pg/L 12/8/2016 Styrene SM e200C < 0.50 ug/L 12/8/2016 cert-Butylbenzene SM 6200C < 0.50 Ng/L 12/8/2016 Tetrachloroethene SM e200C < 0.50 Ng/L 12/8/2016 Toluene SM e200C 0.96 Ng/L 12/8/2016 Trans-1,2-Dichloroethene SM e200C < 0.50 Ng/L 12/8/2016 Trans-1,3-dichloropropene SM 6200C < 0.50 Ng/L 12/8/2016 Trichloroethene SM 62000 < 0.50 pg/L 12/8/2016 Trichlorofluoromethane SM 82000 < 0.50 pg/L 12/8/2016 Vinyl chloride SM e200C < 0.50 Ng/L 12/8/2016 Fecal Coliform SM 9222D MF 1400 Colonies/100ml- 11/30/2016 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 0.04mg/L 12/01/2016 N itrate+N itrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/09/2016 Report #It 2018-17198 Page 12 of 30 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax hill --.0As«" 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Date of Report: Dec 15, 2016 Customer PO #: Customer ID: 09110024 Report #: 2016-17198 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-41456 Site: MW -5 11/30/2016 11:55 AM Water Will Coggins Test Method Results Date Analyzed Color Color Lt Tan/Mild Turb 11/30/2016 Depth to water, ft. Depth to water, Ft 7.3 feet 11/30/2016 Ammonia Nitrogen EPA 350.1 <0.2mg/L 12/01/2016 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/30/2016 Odor Qualitative None 11/30/2016 Total Dissolved Solids (TDS) SM 2540 C 568 mg/L 12/01/2016 Temperature SM 2550 B 19.7 C 11/30/2016 Chloride SM 4500 Cl E 118 mg/L 12/0612016 pH SM 4500 H B 6.17 units 11/30/2016 Total Organic Carbon (TOC) SM 5310 8 5.9 mg/L 12/06/2016 1,1,1,2 -Tetrachloroethane SM 6200C <0.50ug/L 12/8/2016 1,1,1 -Trichloroethane SM 6200C <0.50Ng/L 12/8/2016 1,1,2,2 -Tetrachloroethane SM 6200C <0.50Ng/L 12/8/2016 1,1,2 -Trichloroethane SM 6200C <0.50pg/L 12/8/2016 1,1-Dichloroethane SM 6200C <0.50pg/L 12/8/2016 1,1-Dichloroethene SM 6200C <0.50Ng/L 12/8/2016 1,1-Dichloropropene SM 6200C <0.50pg/L 12/8/2016 1,2,3-Trichlorobenzene SM 6200C <0.50Ng/L 12/8/2016 1,2,3-Trichloropropane SM 6200C < 0.50 Ng/L 12/8/2016 1,2,4-Trichlorobenzene SM 6200C < 0.50 Ng/L 12/8/2016 1,2,4-Trimethylbenzene SM 62000 < 0.50 pg/L 12/8/2016 1,2-Dibromo-3-Chloropropane SM 62000 < 0.50 Ng/L 12/8/2016 1,2-Dibromoethane SM 6200C <0.50ug/L 12/8/2016 1,2 -Dichlorobenzene SM 6200C < 0.50 Ng/L 12/8/2016 1,2-Dichloroethane SM 6200C < 0.50 Ng/L 12/812016 1,2-Dichloropropane SM 62000 < 0.50 Ng/L 12/8/2016 Report #'- 2016-17198 Page 13 of 30 Environmental Chemists, Inc. 4 1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax M. 255 -A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemistscom Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott 27944 Date of Report: Dec 15, 2016 Customer PO #: Customer ID: 09110024 Report M 2016-17198 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene SM 6200C <0.50pg/L 12/8/2016 1,3 -Dichlorobenzene SM 6200C <0.50ug/L 12/8/2016 1,3-Dichloropropane sM62000 < 0.50 ug/L 12/8/2016 1,4 -Dichlorobenzene SM 6200C < 0.50 pg/L 12/8/2016 2,2-Dichloropropane SM 6200C < 0.50 Ng/L 1218/2016 2-Chlorotoluene SM 62000 < 0.50 Ng/L 12/8/2016 4-Chlorotoluene SM 6200C < 0.50 pg/L 12/8/2016 Benzene SM 62000 < 0.50 Ng/L 12/8/2016 Bromobenzene SM 6200C < 0.50 Ng/L 12/8/2016 Bromochloromethane SM 6200C < 0.50 Ng/L 12/8/2016 Bromodichloromethane SM 62000 < 0.50 Ng/L 12/8/2016 Bromoform SM 62000 < 0.50 Ng/L 12/8/2016 Bromomethane SM 62000 < 0.50 Ng/L 12/8/2016 Carbon tetrachloride SM 62000 < 0.50 Ng/L 12/8/2016 Chlorobenzene SM 6200C < 0.50 pg/L 12/8/2016 Chloroethane SM 62000 < 0.50 pg/L 12/8/2016 Chloroform SM 6200C < 0.50 pg/L 12/8/2016 Chloromethane SM 62000 < 0.50 pg/L 12/8/2016 cis-1,2-Dichloroethene SM 6200C < 0.50 pg/L 12/8/2016 cis-1,3-Dichloropropene SM 6200C <0.50pg/L 12/8/2016 Dibromochloromethane SM 6200C <0.50pg/L 12/8/2016 Dibromomethane SM 62000 < 0.50 Ng/L 12/8/2016 Dichlorodifluoromethane SM 6200C < 0.50 ug/L 12/8/2016 Ethylbenzene SM 62000 < 0.50 Ng/L 12/8/2016 Hexachlorobutadiene SM 6200C < 0.50 Ng/L 12/8/2016 Isopropylbenzene SM 6200C < 0.50 Ng/L 12/8/2016 M+P Xylene SM 6200C < 1.00 Ng/L 12/8/2016 Methylene chloride SM 62000 < 0.50 Ng/L 1218/2016 Naphthalene SM 62000 < 0.50 Ng/L 12/8/2016 n-Butylbenzene SM 62000 < 0.50 Ng/L 12/8/2016 Report #:. 201 6-171 98 Page 14 of 30 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 15, 2016 < 0.50 pg/L 862 Holiday Island Road Customer PO #: SM e200c Hertford NC 27944 Customer ID: 09110024 Tetrachloroethene Attention: Anita Elliott Report #: 2016-17198 12/8/2016 Toluene Project ID: Monitoring Wells < 0.50 Ng/L n-Propylbenzene SM 6200C < 0.50 pg/L 1218/2016 ortho-Xylene SM 6200c < 0.50 Ng/L 12/8/2016 p-Isopropyltoluene SM 6200c < 0.50 Ng/L 12/8/2016 sec-Butylbenzene SM 62000 < 0.50 pg/L 12/8/2016 Styrene SM 62000 < 0.50 pg/L 12/8/2016 tert-Butylbenzene SM e200c < 0.50 pg/L 12/8/2016 Tetrachloroethene SM 6200C < 0.50 Ng/L 12/8/2016 Toluene SM 62000 < 0.50 Ng/L 12/8/2016 Trans-1,2-Dichioroethene SM 6200C <0.50pg/L 12/8/2016 Trans-1,3-dichloropropene SM 6200c <0.50pg/L 12/8/2016 Trichloroethene SM 6200c < 0.50 pg/L 12/8/2016 Trichlorofluoromethane SM 6200c < 0.50 pg/L 12/8/2016 Vinyl chloride SM 6200c < 0.50 Ng/L 12/8/2016 Fecal Coliform SM 9222D MF <1 Colonies/100ml- 11/30/2016 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/01/2016 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016 Nitrate Nitrogen Subtraction Method <0.02mg/L 12/09/2016 Report #:: 201 6-171 98 Page 15 of 30 Environmental Chemists, Inc. envirrocchhem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Flighway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 15, 2016 862 Holiday Island Road Customer PO #: Hertford INC 27944 Customer ID: 09110024 Attention: Anita Elliott Report M 2016-17198 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-41457 Site: MW -6 11/30/2016 12:05 PM Water Eric McHorney Test Method Results Date Analyzed Color color Light Grey 11/30/2016 Depth to water, ft. Depth to water, Pt. 8.3 feet 11/30/2016 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 12/01/2016 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/30/2016 Odor Qualitative None 11/30/2016 Total Dissolved Solids (TDS) SM 2540 C 638 mg/L 12/01/2016 Temperature SM 2550 B 19.5 C 11/30/2016 Chloride SM 4500 Cl E 162 mg/L 12/06/2016 pH SM 4500 H B 6.13 units 11/30/2016 Total Organic Carbon (TOC) SM 5310 B 4.6 mg/L 12/06/2016 1,1,1,2 -Tetrachloroethane SM 6200C <0.50pg/L 12/8/2016 1,1,1 -Trichloroethane SM 6200C <0.50Ng/L 12/8/2016 1,1,2,2 -Tetrachloroethane 8M62000 <0.50Ng/L 12/8/2016 1,1,2 -Trichloroethane SM 6200C <0.50pg/L 12/8/2016 1,1-Dichloroethane SM 6200C <0.50Ng/L 12/8/2016 1,1-Dichloroethene SM 0200C <0.50Ng/L 12/8/2016 1,1-Dichloropropene SM 6200C <0.50pg/L 12/8/2016 1,2,3-Trichlorobenzene SM 6200C <0.50pg/L 12/8/2016 1,2,3-Trichloropropane SM 6200C <0.50pg/L 12/8/2016 1,2,4-Trichlorobenzene SM 6200C <0.50pg/L 12/8/2016 1,2,4-Trimethylbenzene SM 6200C < 0.50 Ng/L 12/8/2016 1,2-Dibromo-3-Chloropropane SM 6200C <0.50pg/L 12/8/2016 1,2-Dibromoethane SM 6200C < 0.50 ug/L 12/8/2016 1,2 -Dichlorobenzene SM 62000 < 0.50 ug/L 12/8/2016 1,2-Dichloroethane SM 62000 < 0.50 pg/L 12/8/2016 1,2-Dichloropropane SM 62000 < 0.50 ug/L 12/8/2016 Report #:: 2016-17198 Page 18 of 30 Environmental Chemists, Inc. 1 1 1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM. 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 15, 2016 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2016-17198 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene SM 6200C <0.50pg/L 12/8/2016 1,3 -Dichlorobenzene SM 6200C <0.50Ng/L 12/8/2016 1,3-Dichloropropane SM 6200C < 0.50 Ng/L 12/8/2016 1,4 -Dichlorobenzene SM 62000 < 0.50 pg/L 12/8/2016 2,2-Dichloropropane SM 6200C < 0.50 Ng/L 1218/2016 2-Chlorotoluene SM 6200C < 0.50 u9/L 12/8/2016 4-Chlorotoluene SM 82000 < 0.50 ug/L 12/8/2016 Benzene SM 5200C < 0.50 pg/L 12/8/2016 Bromobenzene SM 62000 < 0.50 pg/L 12/8/2016 Bromochloromethane SM 6200C < 0.50 Ng/L 12/8/2016 Bromodichloromethane SM 62000 < 0.50 Ng/L 12/8/2016 Bromoform SM 62000 < 0.50 Ng/L 12/8/2016 Bromomethane SM 6200C < 0.50 pg/L 12/8/2016 Carbon tetrachloride SM 62000 < 0.50 pg/L 12/8/2016 Chlorobenzene SM 62000 < 0.50 pg/L 12/8/2016 Chloroethane SM 62000 < 0.50 Ng/L 12/8/2016 Chloroform SM 62000 < 0.50 pg/L 12/8/2016 Chloromethane SM 62000 < 0.50 Ng/L 12/8/2016 cis-1,2-Dichloroethene SM 62000 < 0.50 Ng/L 12/8/2016 cis-1,3-Dichloropropene SM 6200C <0.50Ng/L 12/8/2016 Dibromochloromethane SM 62000 < 0.50 NgIL 1218/2016 Dibromomethane SM 62000 < 0.50 NgIL 1218/2016 Dichlorodifluoromethane SM 62000 < 0.50 Ng/L 12/8/2016 Ethylbenzene SM 6200C < 0.50 pg/L 12/8/2016 Hexachlorobutadiene SM 62000 < 0.50 pg/L 12/8/2016 Isopropylbenzene SM 62000 < 0.50 pg/L 12/8/2016 M+P Xylene SM 62000 < 1.00 Ug/L 12/8/2016 Methylene chloride SM 62000 < 0.50 pg/L 12/8/2016 Naphthalene SM 62000 < 0.50 Ng/L 12/8/2016 n-Butylbenzene SM 6200C < 0.50 Ng/L 12/8/2016 Report #:: 201 6-171 98 Page 17 of 30 Environmental Chemists, Inc. 4 / 16602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM, 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott 27944 Date of Report: Dec 15, 2016 Customer PO #: Customer ID: 09110024 Report #: 2016-17198 Project ID: Monitoring Wells n-Propylbenzene SM 62000 < 0.50 pg/L 12/8/2016 ortho-Xylene SM 6200C < 0.50 ug/L 12/8/2016 p-Isopropyltoluene sM 6200C < 0.50 Ng/L 12/8/2016 sec-Butylbenzene SM 62000 < 0.50 pg/L 12/8/2016 Styrene SM 6200C < 0.50 pg/L 12/8/2016 tert-Butylbenzene SM 62000 < 0.50 Ng/L 12/8/2016 Tetrachloroethene SM 6200C < 0.50 pg/L 12/8/2016 Toluene SM 62000 < 0.50 pg/L 12/8/2016 Trans-1,2-Dichloroethene SM 6200C <0.50pg/L 12/8/2016 Trans- l,3-dichloropropene SM 6200C <0.50pg/L 12/8/2016 Trichloroethene SM 8200C < 0.50 Ng/L 12/8/2016 Trichlorofluoromethane SM 62000 < 0.50 Ng/L 12/8/2016 Vinyl chloride SM 62000 < 0.50 Ng/L 12/8/2016 Fecal Coliform SM92220MF <1 Colonies/100mL 11/30/2016 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 0.03mg/L 12/01/2016 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/09/2016 Report#.: 2016-17198 Page 18 of 30 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax SM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 15, 2016 862 Holiday Island Road Customer PO M Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report M 2016-17198 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-41458 Site: MW -7 11/30/2016 10:20 AM Water Will Coggins Test Method Results Date Analyzed Color color Tan 11/30/2016 Depth to water, ft. Depth to water, Ft. 4.0 feet 11/30/2016 Ammonia Nitrogen EPA 350.1 <0.2mg/L 12/01/2016 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/30/2016 Odor Qualitative None 11/30/2016 Total Dissolved Solids (TDS) sM2540C 246 mg/L 12/01/2016 Temperature SM2550a 17.4C 11/30/2016 Chloride SM 4500 Cl E 39 mg/L 12/06/2016 pH SM 4500 H s 5.63 units 11/30/2016 Total Organic Carbon (TOC) SM 5310 a 13.4 mg/L 12/06/2016 1,1,1,2 -Tetrachloroethane SM 8200C <0.50pg/L 12/8/2016 1,1,1 -Trichloroethane SM 8200C <0.50Ng/L 12/8/2016 1,1,2,2 -Tetrachloroethane SM 6200C <0.50Ng/L 12/8/2016 1,1,2 -Trichloroethane SM6200C <0.50Ng/L 12/8/2016 1,1-Dichloroethane SM 6200C <0.50pg/L 12/8/2016 1,1-Dichloroethene SM 6200C <0.50Ng/L 12/8/2016 1,1-Dichloropropene SM 6200C <0.50Ng/L 12/8/2016 1,2,3-Trichlorobenzene SM 6200C < 0.50 pg/L 12/8/2016 1,2,3-Trichloropropane SM 6200C <0.50Ng/L 12/8/2016 1,2,4-Trichlorobenzene SM 6200C <0.50ug/L 12/8/2016 1,2,4-Trimethylbenzene SM 6200C <0.50Ng/L 12/8/2016 1,2-Dibromo-3-Chloropropane SM 6200C <0.50pg/L 12/8/2016 1,2-Dibromoethane SM 62000 < 0.50 Ng/L 12/8/2016 1,2 -Dichlorobenzene SM 6200C < 0.50 pg/L 12/8/2016 1,2-Dichloroethane SM 6200C < 0.50 pg/L 12/8/2016 1,2-Dichloropropane SM 62000 < 0.50 Ng/L 12/8/2016 Reportft:: 201 6-171 98 Page 19 of 30 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalcheniists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott 27944 Date of Report: Dec 15, 2016 Customer PO #: Customer ID: 09110024 Report #: 2016-17198 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene SM 6200C <0.50pg/L 1218/2016 1,3 -Dichlorobenzene SM 62000 < 0.50 pg/L 1218/2016 1,3-Dichloropropane SM 6200C <0.50pg/L 12/8/2016 1,4 -Dichlorobenzene SM 6200C < 0.50 pg/L 12/8/2016 2,2-Dichloropropane SM 6200C < 0.50 pg/L 1218/2016 2-Chlorotoluene SM 62000 < 0.50 pg/L 12/8/2016 4-Chlorotoluene SM 62000 < 0.50 pg/L 12/8/2016 Benzene SM 8200C < 0.50 pg/L 12/8/2016 Bromobenzene SM 62000 < 0.50 pg/L 12/8/2016 Bromochloromethane SM 6200C < 0.50 pg/L 12/8/2016 Bromodichloromethane SM 62000 < 0.50 pg/L 12/8/2016 Bromoform SM 6200C < 0.50 pg/L 12/8/2016 Bromomethane SM 6200C < 0.50 pg/L 12/8/2016 Carbon tetrachloride SM 62000 < 0.50 pg/L 12/8/2016 Chlorobenzene SM 62000 < 0.50 pg/L 12/8/2016 Chloroethane SM 62000 < 0.50 pg/L 12/8/2016 Chloroform SM 62000 < 0.50 pg/L 12/8/2016 Chloromethane SM 62000 < 0.50 pg/L 12/8/2016 cis-1,2-Dichloroethene SM 6200C <0.50pg/L 12/8/2016 cis-1,3-Dichloropropene SM 6200C <0.50pg/L 12/8/2016 Dibromochloromethane SM 6200C <0.50pg/L 12/8/2016 Dibromomethane SM 62000 < 0.50 pg/L 12/8/2016 Dichlorodifluoromethane SM 82000 < 0.50 pg/L 12/8/2016 Ethylbenzene SM 6200C < 0.50 pg/L 12/8/2016 Hexachlorobutadiene SM 62000 < 0.50 pg/L 12/8/2016 Isopropylbenzene SM 62000 < 0.50 pg/L 12/8/2016 M+P Xylene SM 6200C < 1.00 pg/L 12/8/2016 Methylene chloride SM 6200C < 0.50 pg/L 12/8/2016 Naphthalene SM 62000 < 0.50 pg/L 12/8/2016 n-Butylbenzene SM 6200C < 0.50 pg/L 12/8/2016 Report #r: 2016-17198 Page 20 of 30 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 's"' 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 15, 2016 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2016-17198 Project ID: Monitoring Wells n-Propylbenzene SM 6200C < 0.50 Ng/L 12/8/2016 ortho-Xylene SM 62000 < 0.50 U9/L 12/8/2016 p-Isopropyltoluene SM 6200C < 0.50 Ng/L 12/8/2016 sec-Butylbenzene SM 62000 < 0.50 Ng/L 12/8/2016 Styrene SM 62000 < 0.50 pg/L 12/8/2016 tert-Butylbenzene SM 62000 < 0.50 pg/L 12/8/2016 Tetrachloroethene SM 62000 < 0.50 Ng/L 12/8/2016 Toluene SM 62000 < 0.50 Ng/L 12/8/2016 Trans-1,2-Dichloroethene SM 62000 < 0.50 pg/L 12/8/2016 Trans-1,3-dichloropropene SM 62000 < 0.50 pg/L 12/8/2016 Trichloroethene SM 62000 < 0.50 Ng/L 12/8/2016 Trichlorofluoromethane SM 62000 < 0.50 Ng/L 12/8/2016 Vinyl chloride SM 62000 < 0.50 pg/L 12/8/2016 Fecal Coliform SM 9222D MF 17 Colonies/100ml- 11/30/2016 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 <0.02mg/L 12/01/2016 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/09/2016 Report #:: 2016-17198 Page 21 of 30 4M. ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott Lab ID Sample ID: 16-41459 Site: MW -8 Test Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Dec 15, 2016 Customer PO M 27944 Customer ID: 09110024 Report #: 2016-17198 Project ID: Monitoring Wells Color Depth to water, ft. Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Organic Carbon (TOC) 1,1,1,2 -Tetrachloroethane 1,1,1 -Trichloroethane 1,1,2,2 -Tetrachloroethane 1,1,2 -Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trichlorobenzene 1, 2, 3-Trich loropropa ne 1, 2,4-Trich to robenzen e 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane 1,2 -Dichlorobenzene 1,2-Dichloroethane 1,2-Dichloropropane Method Collect Datelrime Matrix 11/30/2016 10:30 AM Water Results Sampled by Eric McHorney Date Color Grey/Mild Turb 11/30/2016 Depth to Water, Ft. 4.5 feet 11/30/2016 EPA 350.1 5.1 mg/L 12/01/2016 Gallons Bailed before sampling 5.0 gallons 11/3012016 Qualitative Mild Sulfur 11/30/2016 SM 2540 C 603 mg/L 12/01/2016 SM 2550 B 18.8 C 11/30/2016 SM 4500 CI E 145 mg/L 12/06/2016 SM 4500 H B 6.69 units 11/30/2016 SM 5310 B 47.0 mg/L 12/06/2016 SM 6200C < 0.50 pg/L 12/8/2016 SM 6200c < 0.50 Ng/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 SM 6200C < 0.50 pg/L 12/8/2016 SM 6200c < 0.50 Ng/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 SM 6200c < 0.50 pg/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 SM 62000 < 0.50 Ug/L 12/8/2016 SM 6200C < 0.50 pg/L 12/8/2016 SM 62000 < 0.50 Ng/L 12/8/2016 SM 6200C < 0.50 pg/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 Report #:: 201&17198 Page 22 of 30 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-AWilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott 27944 Date of Report: Dec 15, 2016 Customer PO #: Customer ID: 09110024 Report #: 2016-17198 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene SM 6200C < 0.50 pg/L 12/8/2016 1,3 -Dichlorobenzene SM 6200C < 0.50 pg/L 12/8/2016 1,3-Dichloropropane SM 6200C < 0.50 Ng/L 12/8/2016 1,4 -Dichlorobenzene SM 5200C < 0.50 pg/L 12/8/2016 2,2-Dichloropropane SM 6200c <0.50Ng/L 12/8/2016 2-Chlorotoluene SM 62000 < 0.50 Ng/L 12/8/2016 4-Chlorotoluene SM 6200C < 0.50 pg/L 12/8/2016 Benzene SM 62000 < 0.50 Ng/L 12/8/2016 Bromobenzene SM 6200c < 0.50 Ng/L 12/8/2016 Bromochloromethane SM 62000 < 0.50 pg/L 12/8/2016 Bromodichloromethane SM 6200c < 0.50 pg/L 12/8/2016 Bromoform SM 6200c < 0.50 pg/L 1218/2016 Bromomethane SM 6200c < 0.50 Ug/L 12/8/2016 Carbon tetrachloride SM 6200c < 0.50 Ng/L 12/8/2016 Chlorobenzene SM 6200c < 0.50 Ng/L 12/8/2016 Chloroethane SM 6200c < 0.50 Ng/L 12/8/2016 Chloroform SM 6200c < 0.50 Ng/L 12/8/2016 Chloromethane SM 6200c < 0.50 pg/L 12/8/2016 cis-1,2-Dichloroethene SM 6200C <0.50pg/L 12/8/2016 cis-1,3-Dichloropropene SM 6200C <0.50Ng/L 12/8/2016 Dibromochloromethane SM 6200c < 0.50 pg/L 12/8/2016 Dibromomethane SM 6200c < 0.50 pg/L 12/8/2016 Dichlorodifluoromethane SM 6200c < 0.50 pg/L 12/8/2016 Ethylbenzene SM 6200C < 0.50 pg/L 12/8/2016 Hexachlorobutadiene SM 6200c < 0.50 pg/L 12/8/2016 Isopropylbenzene SM 6200c < 0.50 Ng/L 12/8/2016 M+P Xylene SM 6200c < 1.00 pg/L 12/8/2016 Methylene chloride SM 6200c < 0.50 Ng/L 12/8/2016 Naphthalene SM 6200c < 0.50 Ng/L 12/8/2016 n-Butylbenzene SM 62000 < 0.50 pg/L 12/8/2016 Report #:: 2016-17198 Page 23 of 30 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax s 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott 27944 Date of Report: Dec 15, 2016 Customer PO #: Customer ID: 09110024 Report #: 2016-17198 Project ID: Monitoring Wells n-Propylbenzene SM 6200C < 0.50 pg/L 12/8/2016 ortho-Xylene SM 52000 < 0.50 Ng/L 12/8/2016 p-Isopropyltoluene SM 82000 < 0.50 Ng/L 12/8/2016 sec-Butylbenzene SM 6200C < 0.50 Ng/L 12/8/2016 Styrene SM 62000 < 0.50 pg/L 12/8/2016 tert-Butylbenzene SM 62000 < 0.50 Ng/L 12/8/2016 Tetrachloroethene SM 62000 < 0.50 Ng/L 12/8/2016 Toluene SM 62000 < 0.50 Ng/L 12/8/2016 Trans-1,2-Dichloroethene SM 6200C <0.50pg/L 12/8/2016 Trans-1,3-dichloropropene SM 6200C <0.50pg/L 12/8/2016 Trichloroethene SM 62000 < 0.50 pg/L 12/8/2016 Trichlorofluoromethane SM 6200C < 0.50 pg/L 12/8/2016 Vinyl chloride SM 62000 < 0.50 pg/L 12/8/2016 Fecal Coliform SM 9222D MF 30 Colonies/100ml- 11/30/2016 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 0.06mg/L 12/01/2016 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016 Nitrate Nitrogen subtraction Method <0.02 mg/L 12/09/2016 Report # 201 6-171 98 Page 24 of 30 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax ;SM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemistscom Albemarle Utility 862 Holiday Island Road Hertford NC 27944 Attention: Anita Elliott Date of Report: Dec 15, 2016 Customer PO #: Customer ID: 09110024 Report #: 2016-17198 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-41460 Site: MW -9 11/30/2016 11:10 AM Water Eric McHorney Test Method Results Date Analyzed Color color Mostly Clear 11/30/2016 Depth to water, ft. Depth to water. Ft. 6.7 feet 11/30/2016 Ammonia Nitrogen EPA 350.1 < 0.2 mg/L 12/01/2016 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/30/2016 Odor Qualitative None 11/30/2016 Total Dissolved Solids (TDS) SM 2540 C 69 mg/L 12/01/2016 Temperature SM2550B 19.0C 11/30/2016 Chloride SM 4500 Cl E 13 mg/L 12/06/2016 pH SM 4500 H B 5.05 units 11/30/2016 Total Organic Carbon (TOC) SM 5310 B 3.8 mg/L 12/06/2016 1,1,1,2 -Tetrachloroethane SM 6200C <0.50Ng/L 12/8/2016 1,1,1 -Trichloroethane SM 6200C <0.50Ng/L 12/8/2016 1,1,2,2 -Tetrachloroethane SM 6200C <0.50Ng/L 12/8/2016 1,1,2 -Trichloroethane SM 6200C <0.50pg/L 12/8/2016 1,1-Dichloroethane SM 6200C <0.50Ng/L 12/8/2016 1,1-Dichloroethene SM 6200C <0.50Ng/L 12/8/2016 1,1-Dichloropropene SM 6200C <0.50pg/L 12/8/2016 1,2,3-Trichlorobenzene SM 62000 < 0.50 Ng/L 12/8/2016 1,2,3-Trichloropropane SM 62000 < 0.50 pg/L 12/8/2016 1,2,4-Trichlorobenzene SM 62000 < 0.50 pg/L 12/8/2016 1,2,4-Tdmethylbenzene SM 6200C <0.50pg/L 12/8/2016 1,2-Dibromo-3-Chloropropane SM 6200C <0.50Ng/L 12/8/2016 1,2-Dibromoethane SM 62000 < 0.50 pg/L 12/8/2016 1,2 -Dichlorobenzene SM 6200C <0.50Ng/L 12/8/2016 1,2-Dichloroethane SM 6200C < 0.50 ug/L 12/8/2016 1,2-Dichloropropane SM 6200C < 0.50 ug/L 12/8/2016 Report #:: 2016-17198 Page 25 of 30 Environmental Chemists, Inc. enviroc:h7em 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott 27944 Date of Report: Dec 15, 2016 Customer PO M Customer ID: 09110024 Report #: 2016-17198 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene SM 6200C <0.50pg/L 12/8/2016 1,3 -Dichlorobenzene SM 6200C <0.50pg/L 12/8/2016 1,3-Dichloropropane SM 6200C <0.50pg/L 12/8/2016 1,4 -Dichlorobenzene SM 6200C <0,50pg/L 12/8/2016 2,2-Dichloropropane SM 62000 < 0.50 pg/L 12/8/2016 2-Chlorotoluene SM 6200c < 0.50 pg/L 12/8/2016 4-Chlorotoluene SM 6200c < 0.50 pg/L 12/8/2016 Benzene SM 6200c < 0.50 pg/L 12/8/2016 Bromobenzene SM 6200c < 0.50 pg/L 12/8/2016 Bromochloromethane SM 6200c < 0.50 pg/L 12/8/2016 Bromodichloromethane SM 62000 < 0.50 pg/L 12/8/2016 Bromoform SM 62000 < 0.50 pg/L 12/8/2016 Bromomethane SM 62000 < 0.50 pg/L 12/8/2016 Carbon tetrachloride SM 6200c < 0.50 pg/L 12/8/2016 Chlorobenzene SM 62000 < 0.50 pg/L 12/8/2016 Chloroethane SM 62000 < 0.50 pg/L 12/8/2016 Chloroform SM 62000 < 0.50 pg/L 12/8/2016 Chloromethane SM 62000 < 0.50 pg/L 12/8/2016 cis-1,2-Dichloroethene SM 6200C < 0.50 pg/L 12/8/2016 cis-1,3-Dichloropropene SM 6200C <0.50pg/L 12/8/2016 Dibromochloromethane SM 6200c < 0.50 pg/L 12/8/2016 Dibromomethane SM 62000 < 0.50 pg/L 12/8/2016 Dichlorodifluoromethane SM 62000 < 0.50 pg/L 12/8/2016 Ethylbenzene SM 6200c < 0.50 pg/1- 12/8/2016 Hexachlorobutadiene SM 62000 < 0.50 pg/L 12/8/2016 Isopropyl benzene SM 6200c < 0.50 pg/L 12/8/2016 M+P Xylene SM 6200c < 1.00 pg/L 12/8/2016 Methylene chloride SM 6200c < 0.50 pg/L 12/8/2016 Naphthalene SM 6200c < 0.50 pg/L 12/8/2016 n-Butylbenzene SM 62000 < 0.50 pg/L 12/8/2016 Reportk: 2016-17198 Page 26 of 30 e:n l ochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Albemarle Utility Date of Report: Dec 15, 2016 < 0.50 Ng/L 862 Holiday Island Road Customer PO M SM 6200C Hertford NC 27944 Customer ID: 09110024 Tetrachloroethene Attention: Anita Elliott Report M 2016-17198 12/8/2016 Toluene Project ID: Monitoring Wells < 0.50 Ng/L n-Propylbenzene SM 52000 < 0.50 pg/L 12/8/2016 ortho-Xylene SM 5200C < 0.50 pg/L 12/8/2016 p-Isopropyltoluene SM 6200C < 0.50 pg/L 12/8/2016 sec-Butylbenzene SM 6200C < 0.50 pg/L 12/8/2016 Styrene SM 62000 < 0.50 Ng/L 12/8/2016 tert-Butyl benzene SM 6200C < 0.50 Ng/L 12/8/2016 Tetrachloroethene SM 62000 < 0.50 Ng/L 12/8/2016 Toluene SM 6200C < 0.50 Ng/L 12/8/2016 Trans-1,2-Dichloroethene SM 6200C <0.50Ng/L 12/8/2016 Trans-1,3-dichloropropene SM 6200C <0.50pg/L 12/8/2016 Trichloroethene SM 62000 < 0.50 Ng/L 12/8/2016 Trichlorofluoromethane SM 6200c < 0.50 Ng/L 12/8/2016 Vinyl chloride SM 62000 < 0.50 Ng/L 12/8/2016 Fecal Coliform SM9222DMF <1 Colonies/100ml- 11/30/2016 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/01/2016 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/09/2016 Reportk* 2016-17198 Page 27 of 30 envivachem ANALYTICAL & CONSULTING CHEMISTS Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott Lab ID Sample ID: 16-41461 Site: MW -10 Test Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax i n fo (wenvi ro nmen t alchem i sts. cont Date of Report: Dec 16, 2016 Customer PO #: 27944 Customer ID: 09110024 Report #: 2016-17198 Project ID: Monitoring Wells Color Depth to water, ft. Ammonia Nitrogen Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Organic Carbon (TOC) 1,1,1,2 -Tetrachloroethane 1,1,1 -Trichloroethane 1,1,2,2 -Tetrachloroethane 1,1,2 -Trichloroethane 1,1-Dichloroethane 1,1-Dichloroethene 1,1-Dichloropropene 1,2,3-Trich lorobenzene 1, 2, 3-Trich loropropane 1,2,4-Trichlorobenzene 1, 2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane 1,2 -Dichlorobenzene 1, 2-Dichloroethane 1,2-Dichloropropane Method Collect Date/Time Matrix 11/30/2016 10:50AM Water Results Sampled by Eric McHorney Date Ana Color Clear/Mild Turb 11/30/2016 Depth to water, Ft. 9.1 feet 11/30/2016 EPA 350.1 < 0.2 mg/L 12/01/2016 Gallons Bailed before sampling 5.0 gallons 11/30/2016 Qualitative None 11/30/2016 SM 2540 c 335 mg/L 12101/2016 SM 2550 B 19.8 C 11/30/2016 SM 4500 Cl E 102 mg/L 12/06/2016 SM 4500HB 5.61 units 11/30/2016 SM 5310 B 4.8 mg/L 12/06/2016 SM 6200C < 0.50 Ug/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 SM 62000 < 0.50 ug/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 SM 6200C < 0.50 pg/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 SM 62000 < 0.50 ug/L 12/8/2016 SM 62000 < 0.50 ug/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 SM 62000 < 0.50 ug/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 SM 62000 < 0.50 ug/L 12/8/2016 SM 62000 < 0.50 yg/L 12/8/2016 SM 62000 < 0.50 pg/L 12/8/2016 Reportk. 2016-17198 Page 28 of 30 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility 862 Holiday Island Road Hertford NC Attention: Anita Elliott 27944 Date of Report: Dec 15, 2016 Customer PO #: Customer ID: 09110024 Report #: 2016-17198 Project ID: Monitoring Wells 1,3,5-Trimethylbenzene SM 62000 < 0.50 pg/L 12/8/2016 1,3 -Dichlorobenzene SM 6200C < 0.50 pg/L 12/8/2016 1,3-Dichloropropane SM 6200C <0.50pg/L 12/8/2016 1,4 -Dichlorobenzene SM 6200C < 0.50 pg/L 12/8/2016 2,2-Dichloropropane SM 6200C <0.50pg/L 12/8/2016 2-Chlorotoluene SM 62000 < 0.50 pg/L 12/8/2016 4-Chlorotoluene SM 62000 < 0.50 pg/L 12/8/2016 Benzene SM 62000 < 0.50 pg/L 12/8/2016 Bromobenzene SM 62000 < 0.50 pg/L 12/8/2016 Bromochloromethane SM 6200C < 0.50 pg/L 12/8/2016 Bromodichloromethane SM 6200C < 0.50 pg/L 12/8/2016 Bromoform SM 62000 < 0.50 pg/L 12/8/2016 Bromomethane SM 6200C < 0.50 pg/L 12/8/2016 Carbon tetrachloride SM e200C < 0.50 pg/L 12/8/2016 Chlorobenzene SM 62000 < 0.50 pg/L 12/8/2016 Chloroethane SM 62000 < 0.50 pg/L 12/8/2016 Chloroform SM 8200C < 0.50 pg/L 12/8/2016 Chloromethane SM 62000 < 0.50 pg/L 12/8/2016 cis-1,2-Dichloroethene SM 6200C <0.50pg/L 12/8/2016 cis-1,3-Dichloropropene SM 6200C <0.50pg/L 12/8/2016 Dibromochloromethane sM 6200C < 0.50 pg/L 12/8/2016 Dibromomethane SM 62000 < 0.50 pg/L 12/8/2016 Dichlorodifluoromethane SM 62000 < 0.50 pg/L 12/8/2016 Ethylbenzene SM 62000 < 0.50 pg/L 12/8/2016 Hexachlorobutadiene SM 62000 < 0.50 pg/L 12/8/2016 Isopropylbenzene SM 6200C < 0.50 pg/L 12/8/2016 M+P Xylene SM 6200C < 1.00 pg/L 12/8/2016 Methylene chloride SM 62000 < 0.50 pg/L 12/8/2016 Naphthalene SM 62000 < 0.50 pg/L 12/8/2016 n-Butylbenzene SM 6200C < 0.50 pg/L 12/8/2016 Report #'- 201 6-171 98 Page 29 of 30 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax O 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sm 255-A Wilmington 1-lighway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com Albemarle Utility Date of Report: Dec 15, 2016 862 Holiday Island Road Customer PO #: Hertford NC 27944 Customer ID: 09110024 Attention: Anita Elliott Report #: 2016-17198 Project ID: Monitoring Wells n-Propylbenzene SM 6200C < 0.50 Ng/L 12/8/2016 ortho-Xylene SM 62000 < 0.50 pg/L 12/8/2016 p-Isopropyltoluene SM 62000 < 0.50 Ng/L 12/8/2016 sec-Butylbenzene SM 62000 < 0.50 Ng/L 12/8/2016 Styrene SM 62000 < 0.50 Ng/L 12/8/2016 tert-Butylbenzene SM 62000 < 0.50 pg/L 12/8/2016 Tetrachloroethene SM 62000 < 0.50 pg/L 12/8/2016 Toluene SM 62000 < 0.50 pg/L 12/8/2016 Trans-1,2-Dichloroethene SM 62000 < 0.50 Ng/L 12/8/2016 Trans- 1,3-dichloropropene SM 6200C < 0.50 Ng/L 12/8/2016 Trichloroethene SM 62000 < 0.50 pg/L 12/8/2016 Trichlorofluoromethane SM 62000 < 0.50 Ng/L 12/8/2016 Vinyl chloride SM 6200C <0.50Ng/L 12/8/2016 Fecal Coliform SM9222DMF <1 Colonies/100mL 11/30/2016 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2 <0.02mg/L 12/01/2016 Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016 Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/09/2016 Comment: ,��((��,, ((�� MM , Reviewed by: 1'I�.I. ^^,, 1, & �Jl➢1(a/1(L Report #:: 2016-17198 Page 30 of 30 r� ENVIRONMENTAL CHEMISTS, INC 6602 OFFICE millW yWilmAgton, 28405 Analytical 8 Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: /(o— 1 % I Ff ADDRESS: CONTACT NAME: Anita Elliot PO NO: PRESERVATION REPORT TO: PHONE/FAX: Time COPY TO: email: Sampled By: (0V # 6T T SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection r f a E a a _ NO ` q E U U a E U m W a J Z PRESERVATION ANALYSIS REQUESTED Date Time Temp z 2 x 0 t 0 0 z o w O Well: �f� C P Chloride, TDS i flUl G G Depth to water: Nitrate, TOC, NH3 G G pH (field): C P n Fecal G G Gallons Bailed: C P VOC's (November) G G [F, Color: C P G G A` Field odor: �lt C P G G C P G G C P G G C P G G C P G G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: Delivered By: Z" A— By •^- ," #« ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way Wilmington, NC 28405 NCDENR: DWQ CERTIFICATION # 94 NCOHHS: OLS CERTIFICATION # 37729 OFFICE: 910-392-0223 FAX 910-392-4424 Analytical &Consulting Chemists COLLECTION AND CHAIN OF CUSTODY CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Anita Elliot PO NO: REPORT TO: PHONE/FAX: Temp COPY TO: email: Sampled Bv: (-( t( CO,141 w % SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection r E y e aPRESERVATION 6. o 2 3 8 o o o. `o a r E 0 m m ANALYSIS REQUESTED DatekTime Temp i ° i o " i s a ° i w r ° 2 Well: �q r7 6 C P /` Chloride, TDS l7 G G �f Depth to water: l C P /Y Nitrate, TOC, NH3 G G pH (field): �4 C P Y �` Fecal G G Gallons Bailed: 1 C P VOC's (November) G G Color: V C P G G �y y Field odor: > t�d1 I C P G G C P G G C P G G C P G G C P G G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: ` ii Accepted: Rejected: Resample Reque ted: Delivered By: Received By. I _Date: 30 1 1(o Time: Ito Z U ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 NCDENR: DWO CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Analytical & Consulting Chemists COLLECTION AND CHAIN OF CUSTODY CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Anita Elliot PO NO: PRESERVATION REPORT TO: PHONE/FAX: Temp COPY TO: email: Sampled Bv: W-0 Co q q -. � S SAMPLE TYPE: I= Influent, E =Effluent, W= Well, ST =Stream, SO= Soil, SL =Sludge, Other: Sample Identification P Collection r ° E v 'a n o 2 `0 o w o n 5 B,m t E M z PRESERVATION ANALYSIS REQUESTED Date Time Temp i o `< $ " z a o w o Well: !�/�W S C P Chloride, TDS 11 3r Ib It o G G Depth to water: , C P L Nitrate, TOC, NH3 G G pH (field): C 113 C P Fecal G G Gallons Bailed: C P VOC's (November) G G GrAl / 1 Color: J �� w�; tt C P G G Field odor: IM' �a S . )t t C P G G C P G G C P G G C P G G C P G G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 2. Temperature when Received: I • D Accepted: Re]ecte Resample Fj que t ed: Delivered Bv: Received B �� L� �. Date: I 7JU (0 Time: �O ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way Wilmington, NC 26405 p_ OFFICE: 910-392-0223 FAX 910-3924424 NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 Analytical & Consulting Chemists COLLECTION AND CHAIN OF CUSTODY CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Anita Elliot PO NO: PRESERVATION REPORT TO: PHONEIFAX: Temp COPY TO: email: Sampled Bv: 12V rriL LiyooiSAMPLE TYPE: I= Influent, E =Effluent, W =Well, ST= Stream, SO= Soil, SL =Sludge, Other: Identification Collection E y v _ o °.U o 0 W i PRESERVATION ANALYSIS REQUESTEDSample Time Temp =i r °Date Well: C P �( Chloride, TDS G G II Depth to water C P X Z Nitrate, TOC, NH3 G G I' pH (field): �` Z / C P Fecal G G Gallons Bailed: C P VOC's (November) G G q Color: L19hr rq� C P G G Field odor: VVII �� Sal �h�� C P G G C P G G C P G G C P G G C P G G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: DatelTime 1. 2. Temperature when Received: •% Accepted Delivered By: f i M pie Reque ted: e: I 3C I(a Time: ((D Tsee etas Analytical & Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wilmington, NC 28405 OFFICE: 910-392-0223 FAX 910-392-4424 CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Anita Elliot PO NO: PRESERVATION REPORT TO: PHONEWAX: Temp COPY TO: email: Sampled By: W i It Ca(,jcA,',% SSAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream. SO = Soil. SL = Sludoe. Other: Sample Identification Collection n n E a m7 oa `o : 5 ej v a 5 _o` m v E o w m i '' i PRESERVATION ANALYSIS REQUESTED Date Time Temp z x o i i x ¢ g F w o Well: M1J` )� C P Chloride, TDS 11 3 Ih II' A^ G G Depth to water: Sari C P K Nitrate, TOC, NH3 G G pH (field): �. 1 -7 C P x Fecal G G Gallons Bailed: C P VOC's (November) G G de,,� LE: -1`&^ Color: Mt Id -Citr16 C P G G Field odor: t.�41L C P G G C P G G C P G G C P G G C P G G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: I .Y Accepted: Delivered By: Received �d Time: �O ENVIRONMENTAL CHEMISTS, INC 6602 OFF in mill Wa2y Wilmin FAgton, 0240 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Anita Elliot PO NO: PRESERVATION REPORT TO: PHONE/FAX: Temp COPY TO: email: Sampled By: L VfG 7V t' K SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection rI H c E a c E 2 W M E Z PRESERVATION ANALYSIS REQUESTED Time Temp i o i N i z o aDate o o I r / t XWell: Chloride, TDS Q ��} +Depth to water:` d� I Nitrate, TOC, NH3 1 pH (field): 6 ?% C P Y Fecal G G GallonsBailed:: C P VOC's (November) G G Color: lff ��7�1rIV�� G I G ,,, Field odor: 401 e C P G G C P G G C P G G C P G G C P G G Total of 10 wells due In March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: • D Accepted: / Delivered By: Receiv ENVIRONMENTAL CHEMISTS, INC 6602 Win mill Way Wilmington, FAX 910NC -392-4424 924424 NCDOFFICE:ENR: DWQ CERTIFICATION # 94 NCDHHS: OLS CERTIFICATION # 37729 Analytical & Consulting Chemists COLLECTION AND CHAIN OF CUSTODY CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Anita Elliot PO NO: PRESERVATION REPORT TO: PHONE/FAX: Temp COPY TO: email: Sampled By: Ai, i L (0jy/`45 SAMPLE TYPE: I= Influent, E =Effluent, W= Well, ST =Stream, SO= Soil, SL =Sludge, Other: Sample Identification Collection ° E y e E o o O o. 0 " - `o 61 r E m z PRESERVATION ANALYSIS REQUESTED Date Time Temp i O o 0 z o a g E w r 0 'J Well: C —7 I C P Chloride, TDS C Z G G 1) Depth to water: u C P G Nitrate, TOC, NH3 G G pH (field): e C P Fecal G G Gallons Bailed: C P VOC's (November) G G {pp Color: I /l C P G G r�QJ Field odor: I �" ' - C P G G C P G G C P G G C P G G C P G G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: l ° Accepted: / Reje ed: Resample Rel que ted: Delivered By: Received By: Date: � � l3G 1 (0 Time: I (OZO A- a =a4@ ENVIRONMENTAL CHEMISTS, INC602Wi:9 illWay WilFAgton, 028405 424 Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Anita Elliot PO NO: REPORT TO: PHONE/FAX: Temp COPY TO: email: Sampled By: f . -k ill �i-o r.. e y SAMPLE TYPE: I= Influent, E =Effluent, W= Well, ST =Stream. SO= Soil. SL = Sludoe. Other: Sample Identification P CcillectionPRESERVATION a E N a a e b E c o o a — o m c E m m ¢ J ANALYSIS REQUESTED Date Time Temp w z o v x o w "= z x x 0 ¢ zo o x p w x Well: /141 g �g Q C P /� Chloride, TDS If 3! L /p:?� G G Depth to water: Sy C P Nitrate, TOC, NH3 G G pH (field): C• 69 C P Fecal G G Gallons Bailed: S C P VOC's (November) G G CGS Gy w:ld}�rb. /"'; C P G G Field odor: y„i�� Stipa" C P G G C P G G C P G G C P G G C P G G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: 1.r0 Accepted:ejected: Resample Requested: Delivered By: Received B__ Date: I U I (O Time: L (p Z r �r ENVIRONMENTAL CHEMISTS, INC 6602 OFF WEdmill ay Wil FAgton, NC 28405 92-4424 Analytical 8 Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Anita Elliot PO NO: REPORT TO: PHONE/FAX: Temp COPY TO: email: Sampled By: �-V- C W A0✓ C7 SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identification Collection aPRESERVATION F n y N U °o `o 2 0 E +, e y _ C o rn c E 2 W m M ANALYSIS REQUESTED DatekTime Temp i O x o o x a x o 4 w x 0 Well: C P X Chloride, TDS (' o�'a G G Depth to water: C P �( C Nitrate, TOC, NH3 G G pH (field): b— C P V /1 Fecal G G Gallons Bailed: C P VOC's (November) G G �DSiIy pa Color. / r� � C P G G Field odor C P G G C P G G C P G G C P G G C P G G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2. Temperature when Received: Accepted: Rejec ed: Resample Reques d:_ Delivered By: Received BY: VKC-h it_, ,Date: t I I 3 (] 1 (o ,r ENVIRONMENTAL CHEMISTS, INC 6602 OFF inmillWay WilE: 910-392-0223 FAgton, 02840 924424 Analytical 8 Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 COLLECTION AND CHAIN OF CUSTODY CLIENT: Albemarle Plantation PROJECT NAME: Monitoring Wells REPORT NO: ADDRESS: CONTACT NAME: Anita Elliot PO NO: PRESERVATION REPORT TO: PHONE/FAX: Temp COPY TO: email: Sampled By: fr r� o - SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other: Sample Identificationn Colfection H E y .o y cl7 E o b o U U a c� 3 E U ❑w Q J Z PRESERVATION ANALYSIS REQUESTED Date Time Temp i z m $ x z o z o_ w O Well, Mt✓ " O ` f �' 4 C P Chloride, TDS I Jo rV pao G G n Depth to water: /e 5 C P Nitrate, TOC, NH3 G G pH (field): S �' 1 C P Fecal G G Gallons Bailed: C P VOC's (November) G G tAbr4l) 46.e Color: C P G G Field odor: C P G G C P G G C P G G C P G G C P G G Total of 10 wells due in March, July, November. Transfer Relinquished By: Date/Time Received By: Date/Time 1. 2 r Temperature when Received: \ . V Accepted: Reje ted: Resample R qu ted: Delivered -By: Received By: � Date: i 11,301 ) �f Time: (OZ�7