WQ0009267_Monitoring - 12-2016_20170117

GW -59A COMPLIANCE REPORT. FORM Permit 4 WQ00092.67
(Submit one each monitoring period with GW-59"forms.)
1
Enter date monitoring results were due. (1/30/17) Will this monitoring report (GW -59 and GW -59A) be
YE
NO
submitted after the established due.date?
2
Was any required information missing on the GW -59 report forms?
YES
O
IF the answer to question 1 or 2 is "YES"; list in the space provided below the well. identification number(s) ,and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
O
identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance...
4
Are any monitored constituents equal to or above the established standards?
nES
NO
If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES' list the affected wells
individually with constituent(s) and concentration(s) exceeding standards in the space provided below:
MW 10 —TDS 658 mg/I
MW11—1.74pg/l P-Isopropyltoluene
MW 16 — 0.88 pg/I ortho-Xylene
5
For the constituents identified in question 4 above, have standards been exceeded previously for the same
YES
NO
constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES', -list in the space
provided below, each well with constituent(s) exceeding standards, concentrations) reported, and sample
collection date for each occurrence (for the last two years).
MW10 — all TDS — 6/17/14(541 mg/1), 12/3/14(615 mg/1), 3/9/15(612 mg/1), 6/7/15(678 mg/1), 9/9/15(582
mg/1), 12/9/15(609 mg/1) 3/2016(635.6 mg/1), 6/2016(785.5 mg/I)-
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YE :
NO
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE
IMMEDIATELY FOR GUIDANCE_ . If the answer is "NO", monitoring wells may be improperly located; contact
the Regional Office.
7
Is the permittee implementing previously approved actions required -by the Division involving this groundwate
YES
NO
quality problem?
If the answer to question 7 is "YES', describe those actions in f .b space provded below. If the answer to
question 7 is "NO", contact the Regional Office within 90 days; evaluations'glay berequired to determine the
impact the waste disposal system is having at the review and cLm ianc`�boMaries surrounding this facility.
Failure_ to do so may subject the permittee to a Notice of Violatig�; - enalties.
t5 tpanes�nd/inr
�+
MW10 — high background TDS-- noted in current permit -M -1
8
The person completing this portion (GW -59A) of.the monitoring report should sign below and submit this form
with GW -59 forms for required wells to the address provided at the top of the current GW -59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Report. GW -59A) is true and complete to the best of my knowledge
XzZ� . '4s—, (_3_
Signature of Permittee(or, Authorized Agent) Date

SUtiIV I i r-UKM UN YtLLUIN PAYER UNLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION i­iease Print ctearny or Type
Facility Name: - - City of Jacksonville_ LandTreatmentSystem
Permit Name (if different):
Facility Address: 716 Firetower Road_
County Onslow
Contact Person: Jill Puff Telephone#:_ 0
(910)938 362.
Well Location/Site Name._ _ _ MW -1 _ No. of wells to be sampled -17 _
DEPARTMENT OF ENVIRONMENT A NATURAL RESOURCES
DIVISION OF WATER RESOURCES - INFORMATION
PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
PERMIT Number:
Expiration Date: 2/2812016
Non -Discharge WQ0009267
UIC
NPDES
Other
TYPE OF PERMITTED OPERATION
BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
X Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
C Water Source Heat Pump
❑ Other:
WELL ID NUMBER (from Permit): - MW -1 Date sample collected_ 122412016_ FIELD ANALYSES:
Well Depth: 16.6 ft. Well Diameter- 2 in. pH 00400: 4.5 units Temp. 000lc 15.3 °C
Depth to Water Level 82546: 7.4 ft. below measuring point: Screened Interval: 3 ft. to 13 ft. Spec. Cond. 00094: µMhos
Measuring Point is 3.2- ft. above land surface Relative M.P. Elevation: 4.2 ft. Odor doom:
Volume of water pumped/bailed before sampling: 4.42 gallons Appearance
SaMples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
ite sample analyzed:_ -_12/4/2016- - Laboratory Name: 1. Jacksonville 2. Environmental_ Chemists Certification No. 1. 128 2: 94
kRAMETERS NOTE. Values should reflect dissolved and colloidal concentrations. ---
COD 00335 mg/L Nitrite (NO2) as N omis X0.02 mg/L Pb - Lead o1o51 ug/L
--
Coliform: MF Fecal 31615 <1 /1OOmL Nitrate (NO3) as N 00520 X0,02 mg/L Zn - Zinc 01092 mg /L
Coliform: MF Total 31504
/1OOmL
Phosphorus: Total as P ocssF
mg/L
(Note: Use MPN method for highly
turbid samples)
Orthophosphate 7050 _ _
_ _ mg/L
Outer (Specify Compounds and Concentration Units).
solved Solids:Total 70300
138,5 _
rng/L
Al = Aluminum o11o5
mg1L
_ Total Suspended Solids <1
mg/I
pH (Lab) 00403
4.5 _
units
Ba - Barium 01007
ug/L
TOC oo600
_ 12.2 _
mg1L
Ca - Calcium oog16
mg/L
Chloride 00940
_ _
—
mg/L
Cd - Cadmium c1c27
ug/l_
9 9
t
- 3 -
Arsenic 01,002
ug/L
Chromium: Total 01034 -
ug/i_
Grease and Oils 00552
-
mg/L
Cu - Copper 01042
_ mg1L
ORGANICS; (by GC, GC/MS, HPLC)
Phenol 32730 _-
uglL
Fe iron 01085
-
- ug/L
--
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
12 _-
rrlg/L
Hg -Mercury 71909
ug/L
Lab Report Attached? ❑ Yes (1)
❑ No (0)
ecific Conductance 00094
-__
µMhos
K - Potassium 00937 _--_
mg/L-
-
VOC 7873 method #
SM 6200C
Total Ammonia omlo
=0.1
mg/L
Mg - Magnesium 00927
mg1L
--
, method #
(Ammonia Niirogen¢ NH3as N, Ammonia Nitrogen Total)
Mn a Manganese 01055 -
uglL
--_ ,method
TKN as N 00625
mg/L
Ni - Nickel 01057 _ _ _
ug/L
method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs:
mg/L Effluent Total VOCs:
mg/L VOC Removal%
WAS
DRY at
time of
sampling,
check
here:�
GW -59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
o e
DEPARTMENT OF ENVIRONMENT iii NATURAL RESOURCES
s ®o
o
DIVISION OF WATER RESOURCES t INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, SEC 27699-1617 Phone_ 919-807-6306
FACILITY INFORMATION
Please Print CleanyorType
PERMIT [Number: Expiration Date: -2/2.8/2018__
Facility Name: -_ _City of Jacksonville Land Treatment System
_
Non -Discharge VUQo009267 UIC
Permit Name (if different): -
,
NPDES Other
Facility Address: _ _
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
_
County Onslow
0 Lagoon 0 Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: - -__. Jill Puff
Telephone#: [phone] _
0 Rotary Distributor Q Land Application of Sludge
Well Location/Site Name _MW-2
No. of wells to be sampled: _ _ 17
F-1 Water Source Heat Pump El Other:
SAMPLING INFORMATION
If WELL
WELL it) NUMBER (from Permit): MW -2
Date sample collected: 12/4/2016
FIELD ANALYSES:
WAS
Well Depth: 17,0 ft.
Well Diameter: _ _2 in.
pH oo400: 4.8 units Temp. noolr 16.1 °C
DRY at
Depth to Water Level 82546: 6.9_ _ -ft_ below measuring point Screened Interval, 3 ft. to
13 ft. Spec. Cond. 00094= µMhos
time of
Measuring Point is 2.4 ft. above land surface
Relative M.P. Elevation: 4.5 ft.
-- -- - -- --
Odor moss: — _
sampling,
check-
Volume of water pumped/bailed before sampling
4_85
gallons
Appearance _ _-
here:L
Samples for metals were collected unfiltered: X
YES
Q NO and field acidified. X YES El NO
LABORATORY INFORMATION
Date sample analyzed: -_ _ _ 12/4/20.16
LaboratoryName. 1. Jacksonville 2
Environmental Chemists Certification No. 1. 1282. 94
PARAMETERS NOTE; Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead o1o51 ug/L
ColiforM: MF Fecal 31616 5
/TOOmL
Nitrate (NO3) as N 00620 O'1 -
mg/L Zn -Zinc 01092
Coliform: MF Total 31504 - -
/100mL
Phosphorus: Total as P o0665
mg/L
(Note: Use MPN method for highly Turbid samples)
Orthophosphate 70507 _
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids: Total 70300 160.5
mg/L
Al -Aluminum o11o5
mg/L Total Suspended Solids 2.5 mg/l
pH (Lab) o0403 4.8 _ —units
Ba - Barium 01007 -
uglL
TOC 00680 3.2
mg/L
Ca - Calcium co916 ---- _
mg/L _
Chloride oo940 -
mg1L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total o1o34
ug/L
Grease and Oils oo552 _ _
mg/L
Cu - Copper 01042 a.
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730u
_
g /L
Fe - Iron 01045 . _ ,
ug/L (Specify test and method #. ATTACH LAB REPORT.).
Sulfate 00945 <5
mg/L
Hg - Mercury 71900 o'y _
ug/L Lab Report Attached? 0 Yes (1) Q No (0)
Specific Conductance 00095 -
µMhos
K - Potassium 00937 _
mg/L VOC 7873 method # SM 62000
Total Ammonia 00610 <0.1
mg/L
Mg - Magnesium 00927
mg/L _ method #
(Ammonia Nitrogen; N%as N; Ammonia Nitrogen, Total)
Mn -Manganese 01055
ug/L ,method #
TKN as N 00625
mg/L
Ni - Nickel 01067
uglL __ , method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
mg/L Effluent Total VOCs:
mg/L VOC Removal%
William E. Brown n - ORC 1/9/_2_017
Permittee (or Authorized Aqent; Name and Tit;e Please print ortvpe Signatu'e of Permittee (or Authorized Agent) (Date)
CW -59 Rev. 8/2013

r UNM UN YtLLUVV FAHEIN UNLY
GROUNDWATER QUALITY MONITORING -
COMPLIANCE REPORT FORM
FACILITY INFORMATION crease ennt cieariy or Type
Facility Name: _ _ _ _ City of Jacksonville Land Treatment System
(Permit Name (if different)
Facility Address: 716 Firetower Road
gv c n
98540
County Onslow
Contact Person: __ _ Jill Puff _ Telephone#: [phone]_____
Well Location/Site Name _ - MW -3 No. of wells to be sampled: 17
PARTMENT OF ENVIRONMENT & NATURAL RESOURCES
VISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
117 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
ERMIT Number: Expiration Date: 212.8/2018
on -Discharge WQ0009267 UIC
PDES Other
YPE OF PERMITTED OPERATION BEING MONITORED
0 Lagoon D Remediation: Infiltration Gallery
X Spray Field © Remediation:
Rotary Distributor 12o Land Application of Sludge
Water Source Meat Pump GI Other. _
WELL ID NUMBER (from Permit): MW -3
Date sample collected:
12/4/2016-
FIELD ANALYSES:
WAS
Well Depth: 17.0 ft.
Well Diameter:
_-_2 in,
-
pH 000o: 4.2 units Temp. 000lc 14.6 °C
Orthophosphate 70507 _
DRY at
-- _
Depth to Water Level 82546 8.4 ft. below measuring point
Screened Interval:
3 IL to 13 ft.
- - -- -
Spec. Cond. 00094: uMhos
mg/L
time of
Measuring Point is 3.2 - - ft. above land surface
Relative M.P. Elevation:
- -
6.2 ft.
_-
Odor 00085:
_ 4.16
sampling-
check
Volume of water pumped/bailed before sampling: 4.13 gallons
Appearance _ _ _ _ _
here:�j
Samples for metals were collected unfiltered: X YES 0 NO
and field acidified: X
YES 0 NO
mg1L
-ug/L
Date sample analyzed. 12/4/2016 - Laboratory Name: 1..Jacksonville2. Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should refleei dissolved and colloidal concentrations..
COD 00335 mg%L Nitrite (NO2) as N oc615 <0.02 mg/L Pb - Lead cimi ug/L
Coliform: MF f=ecal 31616 <1 /100mL Nitrate (NO3) as N om2o <0.02 mg/L Zn - Zinc a1092 mg/L
Coliform: MF Total 31504
i100mL
Phosphorus: Total as P oo665
mg/L
(Note: Use MPN method forhighly
turbid sampiesj —
Orthophosphate 70507 _
mg/L
Other (Specify Compounds and Concentration Units):
Issolved Solids:Total 70300
27
mg/L
Al - Aluminum o11o5
_.
mg/L
Total Suspended Solids 8.2 mg/I
pH (Lab) 00403 _
_ 4.16
units
Ba - Barium 01007
ug/L
TOC 00680
1_7_____ __
mg/L
Ca- Calcium 00916
mg1L
-ug/L
Chloride oosao
mg/L
Cd - Cadmium 01o27
-- _
Arsenic 01.002
ug/L
Chromium: Total o1o34
ug/L
Grease and Oils 005-52
mg/L
Cu = Copper 01042
�;_ n
mg/L
ORGANICS: (by GC, GC/MS: HPL -G)
Phenol 32730
-
uglL
Fe - iron 01045
,
uglL
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate co945
<5 _
mg/L
Hg - Mercury 71900
-
ug/L
Lab Report Attached? UYes (1) No (0)
pecific Conductance 0oo95
µMhos
K - Potassium 00937
mg/L
VOC 7871 method # SM 6200C
Total Ammonia 00610
<0.1
mg/L
Mg = Magnesium oo927
--
mg/L-
- _ method # _
(Ammonia Nitrogen: NH�as N, Ammonia nitrogen, Total)
Mn -Manganese o1055
ug/L
method #
TKN as N 00625
mg/L
Ni - Nickel 01067ug/L
,method
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
William E. Brown - ORC
Peirnittee (or Authorized Agent) Name and Title - Please print or type
GW -59 Rev. 812013
mg/L Effluent Total VOCs: mg/L VOC Removal%
(or
17

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
• ®
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
e � .
e
QMWON OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-161.7 Phone: [phone]
FACILITY INFORMATION
- -
Please Print clearly or Type
PERMIT Number: Expiration Date: 2/28/2018
Facility Name: _- City of Jacksonville Land Treatment System _ _ _
_
Non -Discharge _ WQ..0009267 UIC
Permit Name (if different): - _ _ _
NPDES Other
Facility Address: - - - --
716 Firetower Road
-- -
TYPE OF PERMITTED OPERATION BEING MONITORED
a0 sc iM
2854 CCounty Onslow
0 Lagoon 0 Remediation: Infiltration Gallery
X Spray Field 11 Remediation:
Contact Person: Jill Puff
-
-- -
Telephone#: (910)938=3620 _ - .. _
- -
( Rotary Distributor 0 Land Application of Sludge
Well Location/Site Name- _ _ _.__— MW -4
No. of wells to be sampled: 17
Water Source Heat Pump 0 Other:
..._ —_
;tom Permd
-- - .. --
SAMPLING INFORMATION - - -
- -- -- -
- -- - - -- --if
-
WELL
WELL ID NUMBER (from Permit): MW -4
Date sample coliected° 12/4/2016
F1ELD ANALYSES:
WAS
Well Depth: 16.0 ft.
Well Diameter: 2 in,
pH 00400: 4.3 units Temp- 0ooic 13.1 oC
DRY at
Depth to Water Level 82546: _5.3 ft. below measuring point
Screened Interval: 5.8 ft. to
14 ft. Spec. Cond. oo094: µMhos
time of
Measuring Point is 2.68_ ft. above land surface
Relative M.P. Elevation: _ 2.62 ft.
-- - ----
Odor 00085 _ _-
sampling,
check
Volume of water pumped/bailed before sampling:
_ 5._14
_ gallons
Appearance _ _ _ - _
here:
Samples for metals were collected unfiltered: X
YES
NO and field acidified: X YES ❑ NO
-
LABORATORY INFORMATION
---- -
- ----
Date sample analyzed: 12/4/2016
Laboratory Name: 1. Jacksonville 2._-_
Environmental Chemists Certification No. 1. 128 2_. 94
PARAMETERS NOTE: Values should reflectd_ issolved and colloidal concentrations.
GOD 00335
mg/L
Nitrite (NO2) as N oo615 c0.02
mg/L Pb = Lead oio51 ug/L
Coliform: MF Fecal 3i6is <1
/100mL
Nitrate (NO3) as N oo62o <0-02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL-
Phosphorus: Total as P oo665
mg/L
(Note: Use TOPNrhethod far highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 121.5
mg/L
AI -Aluminum ciios
mg/L Total Suspended Solids <1 m /c, I
pH (Lab) 00403 _ _ _ 4.34
units
Ba - Barium 01007
ug/L _
TOC ooe8o - _ 1.5
rng/L
Ca - Calcium oogle _
mg/L
Chloride 00940 -
mg/L
Cd - Cadmium o1o27
uglL
Arsenic 01002
ug/L
Chromium: Total oio34 , -
ug/L
Grease and Oils 00562 __- _ _
m /L
g
_ Copper 01042
Cu - Co E
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32790 _
ug/L
Fe -Iron 0i 045nj
uglL (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00949 30 _
mglL
9
Hg -Mercury 71900 - `t_ =_
uglL Lab Report Attached? 0 Yes (1) 0 No (0)
pecific Conductance 00095
pMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia ooh �o <0.1
mg/L
Mg - Magnesium 00927
mg/L- ; method #
(Ammonia Nitroget: NH3as N; Arrmonia Nitrogen,Totalj
Mn - Manganese 01055
Ug(I_ method
— -- -
TKN as N 00625
mg/L
Ni - Nickel 01067____
ug/L .method #
For Remediation Systems Only (Attach lab Reports): Influent Total VOCs'.
William E. Brown - OIRC
Permittee (or Authorized Agent) Mame and Title - Pleass print or type
GvV-59 Rev. 8/2013
mg/L Effluent Total VOCs:
El
mg/L VOC Removal%
1/9/2017

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
• a
DEPARTMENT OF ENVIRONMENT 8 NATURAL RESOURCES
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
• : m
•
1617 MAIL SERVICE CENTER,, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITYINF'ORMATION
-
Please Print Clearly or Type
PERMIT Number: Expiration Date: 2/28/2018
- - --
Facility Name: Ci of Jacksonville
Land Treatment System -__- _
Non=Discharge - WQ0009267 - UIC
NPDES Other
Permit Name (if different):
Facility Address:_ _— __ _ __
716 Firetower Road _ _ _
TYPE OF PERMITTED OPERATION BEING MONITORED
2854, County Onslowry
Lagoon En Remediation: infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: _ All Puff
_ _
-- Telephone#: [phone]
Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MW -5
-No. of wells to be sampled: 17
D Water Source Heat Pump 0 Other:
-- -
-
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from. Permit): MWS _ _
Date sample collected: 12/4/2016
FIELD ANALYSES:
WAS
Well Depth: 18.1 ft.
Well Diameter: 2 in.
pH 00400: 4.1 units Temp. cooic 14.7 °C
DRY at
Depth to Water Level 82546: 7.4 ft below measuring
point Screened Interval: 5 ft to
15 ft. Spec. Cond. oocm: µMhos
time of
Measuring Point is _ 2.57 ft. above land surface
Relative M_P. Elevation: - 4 83 ft.
-- -
Odor 000w5.
sampling,
check
Volume of water pumped/bailed before sampling:
5.14
gallons
Appearance -
here:
Samples for metals were collected unfiltered: X
YES
NO and field acidified: X YES D NO
-
LABORATORY INFORMATION
Date sample analyzed: 12/4/2016-
Laboratory Name: 1. Jacksonville 2_
Environmental_ Chemists Certification No. 1. 128. 2.94
PARAMETERS NOTE: VMuies should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 0o615 <0.02
mg/L Pb - Lead o1051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 315o4
/100mL
Phosphorus: Total as P oo665
mg/L
(Note: use MFIN method for highlytuftid samples)
Orthophosphate 70507 _
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70330 8
mg/L
Al -Aluminum 01105 _
mg/L Total Suspended Solids 5.3 mgll
pH (Lab) 00403 4.05
units
Ba - Barium oioo7
ug/L
TOC oo680 <0.5
mg/L
Ca - Calcium oo91s
mg/L
Chloride oo940 _
mg/L
Cd - Cadmium oio27 _ _
ug/L
Arsenic olo02
ug/L
Chromium.- Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu = Copper ol04Z � � r�
mg/L ORGANICS: (by GC; GC/MS; HPLC)
Phenol 32730 --
ug/L
Fe - Iron o1045 -`
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71'soo r'.T�'
ug/L Lab Report Attached? D Yes (1) D No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937 -mg/L
VOC 7873 method # _ SM 6200C
Total Ammonia 00510 <0.1 -
mglL
Alfg -Magnesium 00927
mg/L method # ---
(Ammonia Nitrogen; NH3 as W, Ammorrra Nitrogen, Total)
—
Mn -Manganese 01055ug/L
—
method #
TKN as N 00625
mg/L
Ni - Nickel oio67
ug/L method
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs:
mq/L Effluent Total VOCs;
mel/L VOC Removal%
William E. Brown = ORG
Perm"ttee (or Authorize. d Agent` Name and Title - Please ornt or type
GW -59 Rev. 8!2013

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
m m
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
m m e
m
DIVISION OF WATER RESOURCES -INFORMATION PROCESS114G UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Please pant
clearly o Type -
--
PERMIT Number: Exp.
nation Date: 2/2812018__
Facility Name: City of Jacksonville Land Treatment System -
Non -Discharge _ . W00009267 UIC
Permit Name (if different):
NPOES Other
Facility Address: -116 Firetower Road
---
TYPE_ OF PERMITTED OPERATION BEING MONITORED
-
Lagoon Q Remediation: Infiltration Gallery
County Onslow
0 Spray Field 0 Remediation: -
Contact Person: _ _ Jill Puff _ -
Telephone#: _ __(910)938=3620
0 Rotary Distributor 0 Land Application of Sludge
Well Location/Site Name MW -6
No. of wells to be sampled: 17
0 Water Source Heat Pump Other:
SAMPLING INFORMATION
-
-- --_ .. ___ - -- - -
If WELL
WELL iD NUMBER (from Permit): MW -6 _ _ -
__.. Date sample collected: 12/4/2016
_ FIELD ANALYSES:
WAS
Well Depth: 16.6 ft.
Well Diameter: 2 in_
pH 004eo: 4.9 units Temp. 00010 13.3 °C
DRY at
Depth to Water Level 82549 4.3 ft. below measuring point
Screened Interval: 3._5 ft. to
---
14 ft. Spec. Cond. ooO94: µMhos
time of
_ -
Measuring Point is ---2.-65- ft above land surface
Relative M.P. Elevation: 1.65 _ft.
- - - ------:..:-
Odor 00085:
sampling,
check
Volume of water pumped/bailed before sampling: 5.90
gallons
Appearance _
here:
❑
Samples for metals were collected unfiltered: X YES
0 NO and field acidified: X YES 0 NO
X
LABORATORY INFORMATION
Date sample analyzed.- - __ 12/412016 _- _
LaboratoryName: 1. Jacksonville 2.
Environmental Chemists . Certification No. 1._ 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD oo335 mg/L
Nitrite (NO2) as N oosis 0.09
mg/L Pb - Lead 01051 ug/L
Coliform' MF Fecal 31616 <1. /100mL
Nitrate (NO3) as N 00920 <0.02
mg/L-Zn = Zinc o1os2 mg/L
Coliform: MF Total 3i504 - 1100mL
Phosphorus.- Total as P oosss _-_ ..__
mg/L
(Note: Use MPN method for htgfily turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 - 204 _ _ _ mg/L
--
Ai - Aluminum oil o5-___
mg/L Total Suspended. Solids 41.5
-
pH (Lab) 00403 4.94 units
- -
Ba - Barium o1oo7 -
__.
ug/L
TOC oo6so $ mg/L
Ca y Calcium o0916
mg/L
Chloride 00940 mg/L
Cd - Cadmium o;o27
ug/L
Arsenic o', 032_ ug/L
Chromium: Total =347"' �
ug/L
Grease and Oils oo552 _ _ mg/L
Cu - Copper OI042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ugiL
Fe - Iran oto45
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 38 mg/L
Hg - Mercury 719eo ._.— -
ug/L Lab Report Attached? 0 Yes (1) 0 No (0)
pecific Conductance 00095 _ µMhos
K - Potassium oo937
mg/L VOC 7873 method # _ SM 6200C
Total Ammonia 00610 . 0.11 mg/L
Mg - Magnesium oo927 _
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Tatar)
Mn - Manganese 01055
ug/L method #
TKN as N oo625mg/L
_
Ni - Nickel o1oa7
ug]L - - -- _. _ ,method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs:
mp/L Effluent Total VOCs:
mg/L VOC Removal%
William E. Brown ORC
Permittee (crAuthorized Agent) 1larne and Tine -Please print or type
GW -59 Rev. 812013

ZUI510I t-UKIYI UN YtLLUVV VAT—LK UNLY
Y , m m
GROUNDWATER QUALITY MONITORING: a m m m
COMPLIANCE REPORT FORM
WELL
DEPARTMENT OF ENVIRONMENT '& NATURAL RESOURCES:
DIVISION OF SEATER RESOURCES -INFORMATION PROCESSING UNIT
4617 MAIL SERVICE CENTER, RALEIGH, NC 27699-4617 Phone: 919=807-6306
PERMIT Number: Expiration Date: 2/28/2018
FACILITY INFORMATION Please Pnnt Clearly or Type
Facility Name: Cityof .Jacksonville Land Treatment System
Non -Discharge WQ0009267 UIC -
Permit Name (if different):
NPDES - - Other
Facility Address: 716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
County- -_ Onslow _
C] Lagoon 0 Remediation: Infiltration Gallery
sla-e-
X Spray Field Ll Remediation:
Contact Person. Jill Puff Telephone#: [phone]
Rotary Distributor El Land Application of Sludge
_
Well Location/Site Name _ MW -7 No. of wells to be sampled. 17
ther:
El Water Source Heat Pump M Other----
WELL 1D NUMBER (from Permit): - MW -7
Date sample collected:
12/4/2016
FIELD ANALYSES:
WAS
Well Depth: 15.0 ft.
Weil Diameter:
- 2 in.
pH ooao0: 3.7 units Temp. 0o01c 14
DRY at
Depth to Water Level 82"546: 6.8_- ft. below measuring point
Screened Interval:
2.5 ft. to 13 ft.
Spec. Cond. 00094: pMhps
time of
Grease and Oils 00652
Hg - Mercury 71900 x - _ ug/L
-
---- ---
sampling,
Measuring Point is 3 - ft. above land surface
Relative M.P. Elevation:
3.8 ft.
Odor =85: _ - _
check
Volume of water pumped/bailed before sampling: 3.94 __gallons
µMhos
Appearance
here:
❑
Samples for metals were collected unfiltered: X YES ❑
NO and field acidified, X
YES ll NO
-
LABORATORY INFORMATION- -- - -
- _ — --
Date sample analyzed. 12/4/2016 Laboratory Name: I. Jacksonville _ 2. Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N 00615 <0,02. mg/L Pb - Lead olm5. ug/L
Coliform: MF Fecal 31616 <1 1100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 /L
- mg -
Coliform: MF Total 31504 /1OOmL Phosphorus: Total as P 00685 mg/L
(Note_ Use MPN method for highlyturbid samples)h h h
ved Solids:Total 70300 -
95.5
mg/L
pH (Lab) o-o4o3 .
- 3.67
units
TOC ooeso
4.6
_ mg/L
Chloride 00940
_
mg/L
Arsenic o1002
-
ug1L
Grease and Oils 00652
Hg - Mercury 71900 x - _ ug/L
mg/L
Phenol 32730
ug/L
Sulfate 0094$
26 - -
mg/L
fic Conductance 00095 --
-- ---
µMhos
Total. Ammonia costo
90.1
mg/Ltap
(Ammonia Nitrogen, NH3as N; Ammonia Nitrogen, To
TKN as N 00625 _ - - - -_ mg/L
Ort op osp ate 7o5o7
mg/L
Al -Aluminum o11o5
mg/L
Ba = Barium o 007
ug/L
-
Ca - Calcium oo9 6 _ _
gIL
_
Cd - Cadmium 01027
Chromium: Total wo34
ug/L
Cu -Copper 01042
mg/L
Fe - iron o16a s ' `
uglL
Hg - Mercury 71900 x - _ ug/L
K - Potassium 00937
mg/L
Mg - Magnesium 00927
mg1L
Mn - Manganese o1o56
ug/L-.
Ni - Nickel o?067
ug/L
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
Other (Specify Compounds and Concentration Units):
Total Suspended Solids <1 mg/l___
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method # ATTACH LAB REPORT.)
Lab Report Attached? 0 Yes (1) ❑ No (0)
VOC 7873 method # SM 6200C
method #
method #
-- -- method #
mg/L Effluent Total VOCs:
mg/L VOC Removal%
William E. Brown - ORC -` A^ 7
- -- - - .�� � e _ _ 1 /91201.
Permittee (or Autho ized Agent) Name and Title - Please print or tvpe Signature of Permittee (or Author zed Agent) (Date)
GVV-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:m
u •
DEPARTMENT OF ENVIRONMENT 8 NATURAL RESOURCES`
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FTM
� u
�
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1,617 Phone: [phone]'
FACILITY INFORMATION
Please Print CleariyofType
PERMIT Humber: Expiration Date: 2/2.812018
Facility Name; _ CL of Jacksonville Land Treatment System
Non -Discharge WQ0009267 U IC
Permit Name (if different):
NPDES Other
Facility Address: __.
716 Firetower Road -
TYPE OF PERMITTED OPERATION BEING MONITORED
NC
- -- --
2Ei54v County _ Onslow
l] Lagoon 0 Remediation: Infiltration Gallery
-
X Spray Field L1 Remediation:
Contact Person: _ _ _-- Jill Puff
_ Telephone#: (91_0)938-3620
Rotary Distributor ❑ Land Application of Sludge
Well Location/site Name _ MW -8
No, of wells to be sampled: 17❑
Water Source Heat Pump Other
(itor•_Permit)
--._
- - - - -
_. - -
SAMPLINGINFORMATION
- -- - --- - -
If WELL
WELL ip NUMBED (from Permit).- _ MW -8
Date sample collected: 121512016
FIELD ANALYSES:
WAS
Well Depth: 12,1 ft.
Well Diameter: 2in.
pH 00400: 4 units Temp. 000lc OC
DRY at
_
Depth to Water Level 82546 8.5 below measuring point Screened Interval: ft. to
_15.3
- --- _
9 ft. Spec. Cond. 00094:uMhos
time of.
.
-.ft-
--3
- - ----
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: = 5.5 ft.
Odor 00085: _ _--
check
Volume of water pumped/bailed before sampling
1.73
gallons
Appearance -_-_
here:
Samples for metals were collected unfiltered` X
YES
❑ NO and field acidified: X YES ❑ NO
-
LABORATORY INFORMATION --
-
- - - - _ - — -- -
Date sample analyzed. 12/5/2016
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOPE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N oo615 <0.02
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 <1
/100mi-
Nitrate (NO3) as N oos20 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform.- MF Total 31504
M00mL
Phosphorus: Total as P oo6e5 _
mg/L
(Not@l Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids. -Total 70300 250
mg/L
Al = Aluminum o110s
mg/L Total Suspended Solids 4.5 _mg/i -
pH (Lab) 00403 3.97
units
Ba - Barium 01007 _
ug/L
TOC cow.7 3
_- ______
mg/L
Ca -Calcium 00915 - _- _
mgiL
Chloride 00940
mg/L
Cd - Cadmium o1027
ug/L
Arsenic o1002 _
ug/L
Chromium: Total 01034 J
LYS/L
Grease and Oils oo552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 _
ug/L
Fe = Iron 01045 '" +'
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate oo945 136_ -___
mg/L
Hg - Mercury 71000
ug/L Lab Report Attached? Q Yes (1) ❑ No (0)
pecific Conductance 00095
µMhos
K - POtaSSIUm 00937 _-___-_ _
mg/L VOC 7873 method # SM 62000
Total Ammonia 00610 0.11
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen' NH,as N: A rnon'a Nitrogen, Total)_
Mn - Manganese 01055
ug/L method #
TKN as N 0o^025 -
mg1L
N! - Nickel 01067ugJL
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs:
William E. Broom - ORCji
Permittee (or Authorized Agent) Mame and Trite - Please print or tvpe Signature of Permittee (or
GIAI-59 Rev_ M013
mg/L VOC Removal%

SUBMIT FORM ON YELLOW PAPPR ONi Y
GROUNDWATER QUALITY MONITORING:
JJJRLe a
.
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COM-PLIANCE REPORT FORM
` � m
®
1617 MAIL SERVICE CENTER, RALEIGH, ITEC 27699-1617 Phone: [phone]
FACILITY -INFORMATION
-Pease Pr`rt Clearly or Type
PERMIT Number: Expiration Date: 2/28/2018
Facility Name: _ DIof Jacksonville Land Treatment System
Non=Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address: _
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING (MONITORED
28"4w County Onslow
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field 173 Remediation:
Contact Person: Jill Puff
- Telephone#: [phone]
❑ Rotary Distributor ❑- Land Application of Sludge
Well Location/Site Name MW -9
No. of wells to be sampled: 17
LJ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION --- -
_
- - - - -
If WELL
WELL ID NUMBER (frons Permit): MW -9
-- ---
Date sample collected: 1215/2016
FIELD ANALYSES:
WAS
Well Depth: 14.0 fL
Well Diameter: 2 in.
_
pH 00400: 3.8 units Temp. 000lc___17_7 °C
DRY at
_
Depth to Water Level 82546:_ 6_ ft. below measuring point Screened Interval: 7 ft. to
11_ ft. Spec. Cond. 00094: µMhos
time of
Measuring Point is _2.55 ft. _above land surface
Relative M.P. Elevation: _ 3.45 - ft.
_
Odor 00085: - -_
sampling,
cheek
Volume of water um ed/bailed before sampling:
P P p 9�
3.84
_
gallons
9
Appearance -
pp
here:
Samp!es for metals were collected unfiltered: X
YES
G NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 12/5/2016
Laboratory Name, 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb = Lead o1o51 ug/L
-
Coliform: MF Fecal 31616 <1
1100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Totai as P 0os65
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507 _ _
mg/L Other (Specify Compounds and Concentration Units):
issoived Sclids:Total 70300 208.5
mg/L
Al = Aluminum o11o5
mg1L Total Suspended Solids 1 m_ /�
pH (Lab) 00403 3.75
units
Ba - Barium 01007
ug1L
TOC ooaso 2,2
mg1L
Ca - Calcium oosls ___
mg/L - -
Chloride 00940
mg/L
Cd - Cadmium 01027-
-- ---
uglL
Arsenic 01002-
ug/L
Chromium: Total oio34 ! �' `
ug/L _
Grease and Oils 00552
mg/L
Cu -Capper 01042
mg/L ORGANICS: (by GC, GCIMS: HPLC)
Phenol 32730
ug/L
Fe - Iron 01045 t `-' =
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate oo945 _ _ 88 _
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095 -
itMhos
K _ Potassium 00937
mg/L VOC 787' _ method # SM 6200C
Total Ammonia o0610 0.14 _
mg/L
Mg - Magnesium 00927
mg/L method #
(Air;mona Nitrogen; Nrl3as N, Arttmorra Nifr6gen,
Mn NIn - Manganese o1o55
ug1L method #
TKN as N 00625 _ _ _
mg1L
Ni - Nickel 01067 -
ug/L - - method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs:
mq/L Effluent Total VOCs:
mg/L VOC Removal%
William E. Brown - ORC
Permittee for Authcrizea Apent) Name and Tile = Please print or hpe
GW -59 Rev. 8/2013

LINDWATER QUALiTY MONITORING°
PLIANCE REPORT FORM
Print Clearfv or
JUt91Vll l FUKM UN YLL-LUW FAHLK ONLY
acility Name:- - City of Jacksonville Land Treatment System
ermit Name (if different). _
acility Address: 716 Rretower Road
; so.,v::i - 28-54C -County Onslow - -
(Contact Person: Jill Puff - _ Telephone#: X911)938-3620
Well LocationiSite Name MW -10 No. of wells to be sampled: 17
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOURCES -INFORMATION
PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
PERMIT_ Number:
Expiration Date: 2128_1_20.1.8__
Non -Discharge WQ0009267
—
_ _ UIC --
NPDES —
Other
TYPE OF PERMITTED OPERATION
BEiNG MONITORED
0 Lagoon
❑ Remediation: Infiltration Gallery
X Spray Field
Remediation:_
Rotary Distributor
❑ Land Application of Sludge
0 Water Source Heat Pump
0 Other: - -
WELL ID NUMBER (from Permit): MW -10 _ -__ Date sample collected: -_ -_92/5/2016
Well Depth: 30,1 ft_ Well Diameter: 2 in.
Depth to Water Level 82546 86-- ft. below measuring point Screened Interval: 17 ft. to 27 ft.
Measuring Point is 2.9 ft. above land surface Relative M.P. Elevation: 5;7 ft.
Volume of water pumped/bailed before sampling: 10.32_ _ gallons
Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO
FIELD ANALYSES:
pH 00400: 6.3 units
Spec. Ccnd. 00094:
Odor oroos5: _
Appearance
Temp. 000ic_ 17.1 °C
pMhos
Date sample analyzed. 12J5i2016 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2.94
PARAMETE=RS NOTE:. Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N 00615 <0.02 mg/L Pb - Lead oio5i ug/L
Coliform' MF Fecal 31616 <1 /1OOmL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 -
/1OOmL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly
turbid samples-)_-
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300
658_
mg/L
AI = Aluminum 0iim
mg/L
Total Suspended Soiids 16 mg/i
pH (Lab) 00403
-
6:26_
-
units
13a - Barium 01007 __. _
ug/L
- — --
TOC 00680
3.1
mg/L
Ca - CaICiUm 00916
mg/L
Chloride oo94o
mg/L
Cd = Cadmium 01027 _
ug/L
Arsenic 01002 _
_ _ _ _
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
_ _
-- -
mglL
Cu - Copper 0104 _ -__
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
w
Fe - Iron QJ94i 7 'fr r
. a , r..
—_ 091L
(Specify test and method #. ATTACH LAB REPORT:)
Sulfate 00945
209
mg/L
Hg - Mercury 71900
_ ug1L
Lab Report Attached? ❑ Yes (1) 0 No (0)
Specific Conductance 00095
pMhos
_
K -Potassium 00s37,� cas,3 }
mgiL
,
VOC 787.. ,method # SM 62000-
- -- -
Total Ammonia oosio
__<0.1
rng1L
Mg - Magnesium 000,27
mg/L
_ _ _ method # _
(Ammonia Nitrogen; NH3 as N; Ammon!a Nitrogen, Total)
Mn =Manganese 01066 ___
_ ug/L
,method
TKN as N 00625
mg/L
Ni - Nickel 01o&7
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
mg/L Effluent Total VOCs mgJL VOC Removal%
WAS
DRY at
time of
sampling,
check
here:❑
_ William E. Brown - ORC_ ,�
a��'�,/fie' ,�` �' � �`-�.�,�": _ 1!912017
Permittee (or Authorised Aqent) Name arra Title - r lease print or tVoe Signature of Permittee (or Authorized Aoent; (Date)
GW -59 Rev. 8/2013

SUt3Ml I �-UKM ON YLLLUVV PAPER ONLY
e
GROUNDWATER QUALITY MONITORING:
DEPARTMENT of ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOURCES • INFORMATION PROCESSING UNIT
o e o o
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NG 27699-1617 Phone: [phone]
FACILITY INFORMATION Please Printc%arlyorType
PERMIT Number: Expiration Date: 2/28/2018
Facility Name: City of ,iacksonville Land Treatment System
Non -Discharge - WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address: 716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
- -_
0 Lagoon ❑ Remediation: Infiltration Gallery
Al County Onslow -
,Cr.;' stets. Z..,,.. — -.--- - - -
X Spray Field ❑ Remediation:
Contact Person: Jill Puff Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name MIN -11 No. of wells to be sampled: 17
❑ Water Source Heat Pump ❑ Other.
WELL ID NUMBER (from Permit): MW -11
Well Depth: 222 ft --— ---
Depth to Water Level 82546 11 it. below measuring_ point
Measuring Point is 2.25 ft. above land surface
Volume of water pumped/bailed before sampling: - 5.57 gallons
Samples for metals were collected unfiltered: X YES ❑ NO
Date sample collected:
Relative
12/4/2016
Well Diameter:
2 in.
Screened Interval:
5 ft. to 20 ft.
M -P. Elevation_
8.35 fit,
field acidified: X YES
FIELD ANALYSES: I WAS
pH 00400: 4.7 units Temp. 0001c 15.9 °C IDRY at
Spec. Cond. 00094: µMhos time of
- sampling,
Odor coo>5: _- check
Appearance - - - _—_ - here: El
Date sample analyzed: - _ _ 12/4/2016 Laboratory Name: 1. Jacksonville 2_ Environmental Chemists Certification No. 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N oo615 <0.02 mg/L Pb - Lead 0105l ug/L
Coliform; MF Fecal 31616 _ z -
1 /100mL Nitrate (NO3) as N 00620 X0.02 mg/L 2n - Zine 01092 m
-- g/L
-
Coliforrn: MF Total 31504 -I100mL Phosphorus: Total as P 00665 mg/L
(Note: Use MPN method for highly turbid samples)
O h h h
ved Solids:Total 70300
29.5
mg/L
pH (Lab) oo4o3
4.72
units
TOC oosso ---
1.3
-- -_--
mg/L
Chloride oo940
Chromium: Total olo34
mg/L
Arsenic 01002
i mg/L
ug/L
Grease and Oils 00552
----
-----
mg/L
Phenol 32730
_ mg/L
ug/L
Sulfate 00945
<5
mg/L
fic Conductance 00095
— uglL
pMhos
Total Ammonia 0o6lo _-_<0.1 - mg/L
m
(Amonia Nitrogen; NH3asN Ammonia Nitrogen, Total)
TKN as N 00625 _ ___ mg/L
rt op osp ate 70507 _
mg/L
Al -Aluminum o,, im
_ mg/L
Ba - Barium 01007
ug1L
Ca - Calcium oo916
mg/L
Cd - Cadmium o1o27 -_-�
ug/L
Chromium: Total olo34
ugiL
Cu - Copper 01042
i mg/L
Fe - iron o1o45
ug/L
Hg - Mercury 71 goo
_ -_ _ ugiL
K = Potassium oo937
_ mg/L
Mg - Magnesium oo927 _
mg1L
Mn - Manganese 01055
ugiL
Ni - Nickel 01067
— uglL
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
Other (Specify Compounds and. Concentration Units);
Total Suspended Solids 22 mg/l
ORGANICS: (by GC; GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes (1) ❑ No (0)
VOC 7873 method # SM 6200C
method #
method #
mg/L Effluent Total VOCs:
, method #
mg/L VOC Removal%
William E. Brown - ORC %�%� ,��
9/2017
Permittee (or Authorized Aaent) Name and Tine - Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW -59 Rev. 812013

SUBMIT FORM ON YELLOW PAPER ON] Y
GROUNDWATER QUALITY MONITORING--
a
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOURCES- INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
� d Q
m
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617Phone: 9i9-807-6306
FACILITY INFORMATION
Aewe Print Clearly or Type
PERMIT Number: Expiration Dates 2/281201.8_
Facility Name: _ City_of JacksonvilleLandTreatment System
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address:
716 Firetower
Road
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
28 2 County Onslow
X Spray Field ❑ Remediation:
Contact Person: Jill Puff
-
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name - MW -12
No. of wells to be sampled: 17____-
Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
- - — -
If WELL
WELL ID NUMBER (from Permit): MWA2 _ -
- ---
Date sample collected: .12/412016
FIELDANALYSES,:
WAS
Well Depth: 18.3 ft_
Well Diameter: 2 in.
pH 00400: 4.2 units Temp. 0001C aC
DRY at
Depth to Water Level 82546: 7.6 - ft. below measuring point Screened Interval: 6 ft. to
15
_13-4
ft. Spec. Cond. 00094: µMhos
time of
Measuring Point is 3.04_- ft. above land surface
Relative M.P. Elevation_ 4.56 ft.
-
- -
r 00 _
Odor
sampling,
check
Volume of water pumped/bailed before sampling:
5.14
gallons
Appearance -_
here:
Samples for metals were collected unfiltered: X
YES
{❑- NO and field acidified: X YES ❑ NO
LA60RATOR Y IN- FQRMAT10N
Date sample analyzed: 12/4!2016
LaboratoryName: 1_ Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2.94
PARAMETERS NOTE. Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N oc615 0.08
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn -Zinc 0i o92 m /L
Coiiform: MF Total 31504 _
/100ml-
Phosphorus: Total as P ooam -
mg/L
(Note: Use PdFN method for highly turbid sam- ples) —
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Totai 703oo 235.5
_.
mg/L
Al- Aluminum 01105
rang/L Total Suspended Solids 112 mg/l-.-
- -
pH (Lab) 00403 4.2- _
units
Ba - Barium 01007 _
ug/L
TOC om8o 44.3
mg/L
Ca - Calcium oos16
mg/L
Chloride 00940
mg/L
Cd = Cadmium 010.27
ug/L
01002
u /L
Chromium: Total�ZArsenic
ug1L
Grease and Oils 00552
mg/L
Cu - Copper o1p4
mglL ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe -Iron o1
ug/L (Specify test and method #, ATTACH LAB REPORT.)
Sulfate 00946 15
mg/L
Hg _ Mercury 71909
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
pecific Conductance 00096
µMhos
K - Potassium 00937
mg/L VOC 787x__ _ method # SM 6200C
Total Ammonia 00610 - - _<0.1 -
mg/L
Mg - Magnesium 00927
mg/L _- method #
(Ammonia Nitrogen; NH., as N; Ammons Nitrogen, Total)
Mn -Manganese 01055
uglL
,method
TKN as N oo625 -
mg/L
Ni _ Nickel oio67
ug1L
method #
For Remediation Systems Only (Attach Lab Reports): influent Total VOCs:
William E. Brown - ORC
Permittee for Al thciazed A,e.7t1 Name and Title -Please print or ivpe
OW -59 Rev. 812013
mg/L Effluent Total VOCs:
(or
mg/L VOC Removal%

SUUMI I i-UKM UN YELLUW F'AHLK UNLY
. e e .
GROUNDWATER QUALITY MONITORING: e m e o
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please PrfrrtclearlyorT,rpe -
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OFV9fATERRESOURCES - INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]. ;
PERMIT Number: Expiration Date: 2/28/2018
Facility Name: City of Jacksonville Land Treatment System
Non -Discharge WQ0009267 UIC
Permit Name (if different):
NPDES Other
Facility Address.- _ 716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
"ie 's= 41 u County Onslow -
Ej Lagoon 1:1 Remediation: Infiltration Gallery
ug/L
X Spray Field Q Remediation:
Contact Person: Jill Puff Telephone#: [phone] — _
1 Potary Distributor 0 Land Application of Sludge
Well Location/Site Name MW*13 No. of wells to be sampled: 17
El Water Source Heat Pump D Other:
SAMPLINU IIVI=UHMA I IUN
ug/L
Chromium: Total o1oU
ug/L
Grease and Oils 00552mg/L
If WELL
WELL ID NUMBER (from hermit): MW -13
Date sample collected:
12/5/2016
FIELD ANALYSES:
ug/L
WAS
Well Depth: 23.2 ft.
Well Diameter:
2 in.
mg1L
phi 00400: 4.1 units Temp. 000lc
17.1 °C
DRY at
Depth to Water Level a2546 15.7 ft. below measuring point Screened Interval:
10.5 ft.
to 232 ft.
—
Spec. Cond.-_00094:
--
gMhos
time of
Measuring Point is 2.75 ft. above land surface
Relative M.P. Elevation:
_ 12-95
-
ft.
- _ --
Odor 00085:
sampling,
check
Volume of water pumped/bailed before sampling: 3__6.0
gallons
TKN as N 00625
mg/L
Appearance _
ug/L
here:E—
Samples for metals were collected unfiltered'. X YES
NO and field acidified: X
YES El
NO
LABORATORYINFOR MATION
Date sample analyzed. _ 1.215/2016 -
Laboratory Name: 1. Jacksonville_-2=Environmental
Chemists Certification No.
1.128 2.94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
<0.02
mg/L
Pb - Lead o1o51
ug/L
Coliform: MF Fecal 01616 <1 /100mL
Nitrate (NO3) as N 00620
<0_02
mg/L
Zn - Zinc 01052
mg/L
Coliform: MF Total 31504 1100mL
Phosphorus: Total as P oo665
mglL
(Norte: Use MPN method for highly turbid samofes)
Orthophosphate 70507
_
_
mg/L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 7031DD _-_ 67 mg/L
Al -Alutrminum o11o5
mg/L
Total Suspended Solids <1
mg/l
pH (Lab) 00403 _ —4.07 _ units
Ba - Barium o1o07
ug/L
TOC oo6so 1.2 mg/L
Ca - Calcium oosls
Chloride 00540 _ mg/L
Cd - Cadmium 01027
ug/L
Arsenicoloo2_
ug/L
Chromium: Total o1oU
ug/L
Grease and Oils 00552mg/L
Cu = Copper o1042
s. _, ,r mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron olo45
— - ug/L
(Specify test and method #. ATTACH LAB REPORT,)
Sulfate 00945 <5
mg1L
Hg - Mercury 71500
.7� �T ug/L
Lab Report Attached? CI Yes (1) 0 No (0)
Specific Conductance ooc95
uMhos
K - Potassium oo937
mg/L
VOC 7573 method # SM 6200C
Total Ammonia m6lo <0.1
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn -Manganese 01056
ug/L
,method
TKN as N 00625
mg/L
Ni - Nickel o1os7
ug/L
method #
For Remediation Systems Only (Attach Lab Reports)
Influent Total VOCs:
mg/L- Effluent Total VOCs:
mg/L VOC Removal%
GVV-59 Rev. 812013

SUBMIT FORM ON YELLOW PAPER ONLY
e s DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: e m m DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FGRIVE 161,7 MAIL SERVICE QFNTER,_ RALEIGH,'NC 27699-1617 phone: [phone] ,
FACILITY INFORMATION Please Print Clearly or Type --- PERMIT Number: Expiration Date: 2/28/2018
Facility Name: _ City of Jacksonville Land Treatment System Non=Discharge WQ0009267 UIC
Permit Name (if different): — NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
County Onslow 0 Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: _- Jill Puff _ Telephone#: [phone]tor Distributor ❑Land Application of Sludge
Well Location/Site Name MWA4 No. of wells to be sampled: _ 17 D Water Source Heat Pump ❑Other:
wmvir irvu uvrummi l_iwN,
/100mL
Phosphorus: Total as P 00665
If WELL
WELL ID NUMBER (from Permit): - MW -14 _
Date
Date sample collected:
12/5/2016
FIELD ANALYSES:
Orthophosphate 70$07
WAS
Well Depth: 17.9 ft.
Well Diameter:
2 in.
pH 00400: 4.2 units
Temp. 000lc_15.5 °C
DRY at
Depth to Water Level 82546: 11 _ ft. below measuring point Screened interval:
5 ft. to 15 ft.
Spec Cond. 000aa:
µMho: 21
time of
Measuring Point is 3.2 ft. above land surface
Relative M.P. Elevation:
7.8 ft.
-
Odor 00085:
-- _.
sampling,
11.5
mg/L
Ca - Calcium oosls
— -
check
Volume of water pumped/bailed before sampling: 3.31
gallons
mg/L
Appearance
here:j
Samples for metals were collected unfiltered: X YES
❑ NO and field acidified: X
YES ❑ NO
ug/L
Chromium' Total 01034
{
LABORATORY INFORMATION
Grease and Oils 00562
-
mg/L
Cu - Copper olo42
Date sample analyzed: 12/5/2016
Laboratory Name: 1. Jacksonville
2. Environmental Chemists Certification No. 1. 128 2.94
Phenol 32730 -
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
Fe - Iron o1o45
_
uglL
(Specify test and method #. ATTACH LAB REPORT.)
COD oo335 mg/L
Nitrite (NO2) as N oo616
<0.02 mg/L
Pb - Lead oio51
ug/L
ug/L
Coliform: MF Fecal 31616 < 1 /100mL
Nitrate (NQ3) as N a0s20
--
X0.02 mg/L
Zn - Zinc 01092
-- m !L
--
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
("ole: use w"met"°° for highly
turbid samples) --
Orthophosphate 70$07
mg/L
Other (Specify Compounds and Concentration Units):
)issolved Solids:Total 70300
42
mg/L
Al -Aluminum oil o5
mg/L
Total Suspended Solids 1 mg/i
pH (Lab) 00406
_ 4.17 _
units
Ba - Barium oioo7
ug/L
TOC 00680
11.5
mg/L
Ca - Calcium oosls
/L
Chloride 00940
mg/L
Cd - Cadmium 01027
-
Arsenic 01002
ug/L
Chromium' Total 01034
ug/L
Grease and Oils 00562
mg/L
Cu - Copper olo42
4
=ted
_ mg/L
ORGANICS: (by GC; GC/MS, HPLC)
Phenol 32730 -
- ug/L
Fe - Iron o1o45
_
uglL
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00645 _
<5
(rig/L
Hg =Mercury 7190-
l __
ug/L
Lab Report Attached? El Yes (1) ❑ No (0)
Specific Conductance 000s5 . -_-
_
µMhos
K - Potassium oo937
--
mg/L
VOC 7873 method # SM 6200G
— -
Total Ammonia oo6lo
2.15
mg/L
Mg = Magnesium oo92
mg/L
method #
(Ammonia Nitrogen; NH3 as N: Ammonia
Nitrogen, Total)
Mn -Manganese o1d55
-----
-_
ug/L
_ - ,method #
TKN as N 00625
_--
mg/L
Ni - Nickel 01067
-- --
- ug/L
_ --- method # - --
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: rng/L VOC Removal%
William E. Brown - ORC, �,, 1/9/2017
Permittee (or Authorized Acient) Name and Title = Please p int or type Signattre of Permittee (or AuthcTlmd A.c nt) (Date)
GVV-59 Rev- Sl2013

JUd1Vll I rUKM UN YLLLUVV NAHLK UNLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: City of Jacksonville Land Treatment System -
Permit
stemPermit Name (f different):
Facility Address: 716 Firetower Road
`c ;'`c 2 14,3 County Onslow
Contact Person: _ _ _ Jill Puff Telephone#: [phone]
Well Location/Site Name -_- _ MW -15 No. of wells to be sampled: 17
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH; NC 27699-1617 Phone: [phone]
PERMIT Number: Expiration Date: - - 2/28/2018
Non -Discharge W00009267 UIC
NPDES — Other --
TYPE OF PERMITTED OPERATION BEING MONITORED
0 Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field 0 Remediation:
Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump 0 Other—
aAMKUNU-INN-QKMATION
12/4/2016
Laboratory Name: 1.
If WELL
WELL ID NUMBER (from Permit): MW -15
---
Date sample collected:
12/4/2016
FIELD ANALYSES:
WAS
Well Depth: 15_ ft.
Well Diameter:
2_ in.
pH 00400: 3.8 units Temp. ocolt 23 °C
DRY at
Depth to Water Level x2546 3.5__ ft. below measuring point
Screened Interval:
5 ft. to 15 ft.
------ -
Spec. Cond. =94: µMhos
time of
/100mL
Nitrate (NO3) as N 00620
-
-
_-.._ _
sampling,
Measuring Point is 2.9 ft. above land surface
Relative M.P. Elevation:
1 ft_
Odor 00085: _ _ - -
check
Volume of water pumped/bailed before sampling: 533gallons
Appearance
here:F
Samples for metals were collected unfiltered: X YES 0 NO
and field acidified: X
YES ❑ NO
mg/L
,- —
Date sample analyzed:
12/4/2016
Laboratory Name: 1.
Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2. 9.4
PARAMETERS NOTE: Values should -effect
dissolved and colloidal concentrations.
COD o0335
mg/L
Nitrite (NOZ) as N oo615
<0.02
mg/L
Pb - Lead 01061 ug/L
Coliform MF Fecal 31616
<1
/100mL
Nitrate (NO3) as N 00620
-
0.14
mg/L
Zn- Zinc 01092 mg/L
Coliform: MF Total 315o4
/100mL
Phosphorus: Total as P omc-5
_
mg/L
(Note: Use MPN method for
highly turbid samples; --
Orthophosphate 70507 _
mg/L
Other (Specify Compounds and Concentration Units):
issolved Solids.Total 10300
99
mg/L
Al -Aluminum 01105
mg!L
Total Suspended Solids <1 . _ __- _ mg/I
pH (Lab) oo to3
3.81
units
Ba - Barium oio07
ug/L
TOC omac
_- -__ _ 0.7
mg/L
Ca - Calcium costs
mg/L
/L g
Chloride oo240
_ _
mg/L
Cd - Cadmium oio27 _ _
_ _ _
ug/L.;,.
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils oo552
mg/L-
Cu - Copper 01042
mg/L
"ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
_
ug1L
Fe - Iron 01045_E
/L
-PORT.)
(Specify test and method #. ATTACH LAB R
Sulfate 00945
<5 _
mg/L
Hg - Mercury ilscc
---
ug/L
Lab Report Attached? ❑ Yes (1) CJ No (0)
Specific Conductance 00095
µMhos
K - Potassium oogsz _
._ W `u_
mg/L
VOC 7873 - _ _ _ method # SM 6200C
Total Ammonia 00610
<0.1
mg/L
Mg - Magnesium 0092-1
mg1L
method # _
(Ammonia Nitrogen; NHass N; Ammonia Nitrogen, Tota!)
Mn -Manganese cross
_
uglL
,method # _
TKN as N oo625-
_
mg/L
Ni - Nickel 01067
ug/L
_ _ _. method #
For Remediation Systems Only (Attach Lab Reports)
Influent Total VOCs:
mg/L Effluent Total VOCs:
mg/L VOC Removal%
GW -59 Rev. 8/2013

FORM ON YELLOW PAPER ONLY
W
a DEPARTMENT OF ENVIRONMENT S NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: . o a ® m DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NG 27699.1617 Phone: [phone]
FACILITY INFORMATION Please Pr, nt Clearly or type — - - PERMIT Number: Expiration Date:2/28/201.8
- - --
Facility Name: City of Jacksonville Land Treatment System Non -Discharge - WQ0009267 UIC
Permit Name (if different): NPDES Other
Facility Address: 716 Firetower Road TYPE OF PERMITTED OPERATION BEING MONITORED
-^��
'a " ` �` County Onslow [] Lagoon Rernediationo Infiltration Gallery
X Spray Field El Remediation:
Contact Person: -__ Jill Puff _ Telephone#: [phone] Rotary Distributor Land Application of Sludge
Well Location/Site Name MW -16 _ _ No. of wells to be sampled: _ 17 F-1 Water Source Heat Pump C Other:
1AIYIrL-INU INI-UKMAI ION
4.48 _ units
Laboratory Name: 1. Jacksonville
2. Environmental Chemists Certification No- 1. 128 2. 94
If WELL
WELL ID NUMBER (from Permit): MW -1.6 _ -__
Date sample collected:
12/4/2016
FIELD ANALYSES:
WAS
Well Depth: 25 fL
Well Diameter:
2 in.
pH 00400: 4.5 units Temp. 000lc 13.6 °C
DRY at
Depth to Water Level 82546: 10 ft. below measuring point
Screened Interval:
15 ft. to 20 ft.
Spec. Cond. 00094: uMhos
time of
Measuring Point is .2-4- _-_ ft. above land surface
,Relative M.P. Elevation:
-
- —sampling,
8 ft-
-- - -
Odorcheck
000w: ----
Orthophosphate 70507 --
Volume of water pumped/bailed before sampling: 7.01 gallons
Other (Specify Compounds and Concentration Units):
Appearance
here
Samples for metals were collected unfiltered, X YES [7 NO
and field acidified: X
YES El NO
uglL
- -
Date sample analyzed. 12/412016
4.48 _ units
Laboratory Name: 1. Jacksonville
2. Environmental Chemists Certification No- 1. 128 2. 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
-1.2 mg/L
Ca - Calcium o0916
COD oo335
mg/L
Nitrite (NO2) as N omi5 <0.02
mg/L
Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L
Zn - Zinc 61092 mg/L
Coliform: MF Total 31504 - _
/100mL
Phosphorus: Total as P oosse
mg/L
K - Potassium 00937
(Note: Use MPN method for highly turbid samples)
VOC 787 method # _ SM 62000
Orthophosphate 70507 --
mg/L
Other (Specify Compounds and Concentration Units):
)issolved Solids:Total 70300.---- 42.5
rang/L
Al - Aluminum ol1e5 -
mg/L
Total Suspended Solids 1 Mg/l
pH (Lab) 00403
4.48 _ units
Ba -. Barium 01007
ug1L _
TOC oo6m
-1.2 mg/L
Ca - Calcium o0916
mg/L -
Chloride 00°40
mg/L
Cd - Cadmium 01,027
ug/L
Arsenic 01002a
_-. -_---
ug/L
Chromium: Total 01034
- -
and Oils 00552 _
GreasePhenol
mg/L
Cu - Copper 01042
_ - mg/L
ORGANICS: (by GC, GC/MS, HPLC)
32730
- -
ug1L
��
Fe - Iron 01045 _ ____ }� %thwr'� ug/L
-
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5
mg/L
Hg - Mercury 71900
_ _ ug/L
Lab Report Attached? 0 Yes (1) ❑ No (0)
ipecific Conductance cows
-
µMhos
K - Potassium 00937
mg/L
VOC 787 method # _ SM 62000
Total Ammonia ooslo _ _ _ <0.1 _ _ _
mg/L
Mg - Magnesium 00927
- —
mg/L
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen. Total)
Mn - Manganese 01,055
uglL
-- -
;method #
TKN as N 00623
mgiL
Ni - Nickel a1o67
ug/L
_ _ __. method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mgiL Effluent Total VOCs: _ mg/L VOC Removal%
William E. Brown - ORCJ,«�"��./�/,J;�.�, :� ,.„��,�% 1x9/2017
Permittee (or Authorized Apant) Name and `rine _ Please pant or tvice Sigrature of Permittee (or Autnrized Agent) (Date)
G%N-59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING-
. mm
a
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOIURC15S - INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
®e
e
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION
Please Print ClearlyorTipe
PERMIT Number: Expiration Date: 2/28/2018
Facility Name: _ - City of Jacksonville
Land Treatment System -_
Non -Discharge WQ0009267 UIC
NPDES Other
Permit Name (if different):
Facility Address: _ _
716 Firetower Road
TYPE OF PERMITTED OPERATION BEING MONITORED
_ .
`65 3 ---
_ County Onslow
Lagoon❑temediation: Infiltration Gallery
X Spray Field Remediation:
Contact Person: Jill Puff
Telephone#: [phone]
E3 Rotary Distributor Land Application of Sludge
Well Location/Site Name MW47
No. of wells to be sampled: _. _17Ll
Water Source Heat Pump Cl Other:
_
(from
Permit)
-
- -
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW -17
—
Date sample collected: 12/4/2017' FIELD ANALYSES`
WAS
Well Depth: 25 ft.
Well Diameter: 2 in.
pH 00400, 4 units Temp. 000lc 16 °C
DRY at
Depth to Water Level 82546, 7._1 ft. below measuring point
Screened Interval: 15 ft- to
20 ft. Spec. Cond. 00094: µMhos
time of
Measuring Point is 1.9 ft. above land surface
Relative M.P. Elevation. 5.2 ft.
Odor 000e5:
sampling,
check
Volume of water pumped/bailed before sampling,
8..59
_ gallons
Appearance -_ -
here:—p
Samples for metals were collected unfiltered: X
YES
0 NO and field acidified, X YES 0 NO
—
LABORATORY INFORMATION
- —
Date sample analyzed: 1.2/4/2017
Laboratory Name: 1. Jacksonville 2.
Environmental Chemists Certification No. 1. 128 2.94
PARAMETERS NOTES Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead o1051U g(L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mgiL Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL-
Phosphorus: Total as P oo665
mg/L
;Note: USa MPNI method for highly turbid samofes>
Orthophosphate i0507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 153.5
mg/L
Ai -Aluminum oil os
mg/L Total Susp-enaed Solids <1 mg/i
PH (Lab) 00403 3.97
units
Ba - Barium 01007_ _ -
ug/L
TOC oo6so-1,9
-
mg/L
Ca - Calcium 00916
mg/L
Chloride oo94o
mg/L
Cd - Cadmium o1o27
---- ------
uglL
Arsenic o1002
ug/L
Chromium: Total 010341
ug/L
Grease and Oils 00552
mg/L
Cu - Copper o1 o42 _
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/
Fe - iron 01445 4 _
ug/L (Specify test and method #.. ATTACH LAB REPORT.)
Sulfate 00945 — <5
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? El Yes (1) El No (0)
pecific Conductance 000g5 - —
µMhos
K - Potassium 00937
mg/L VOC 7873 method # SM 6200C
Total Ammonia ooslo <0_1
mg/L
Mg - Magnesium oo927
mg/L _ method #
(Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total
Mn - Manganese of o55
ug/L ; method #
TKN as N 00625 -. -., ___ __ _ ___ __
mg/L
Ni - Nickel 01007
ug/L method #
For Remediation System_ s Only (Attach Lab Reports): Influent Total VOCs: mg/L
Effluent Total VOCs:
mg/L VOC Removal%
William E. Brown - ORC !� �i_✓� ' _ , � - , s 119/2017
Permittee (or Aut`iarized APent) Name and Title - Please Print or tvpe S;gnature of Permittee (or Authorized Arent) fDete;
GW -59 Rev. 812013

Environmental i , Inc.
6602 Windmill t1'ay, Wilmington, NC: 28405 > 9.10,392,0223 [.,ab e 910,392.4424 Fax
210 Bowsertot vi Road, Manteo, NC. 27954 0 252.=173.5702 Lab /Fax
255-A Wilmington I Iirhway, Jacksonville, NC.. 28540 • 91.0.347.5843 Lab/ Fax
info'ii enviroilmentitlefmiiists.com
City of Jacksonville Date of Report: Dec 16, 2016
Post Office Box 128 Customer PO #: 150011
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-41885 Site: MW -8 12/5/2016 9:48 AM Water JP
Test Method Results Date Analyzed
Sulfate
EPA 300.0
Total Organic Carbon (TOC)
SM 5310 B
1,1,1,2 -Tetrachloroethane
SM 6200C
1,1,1 -Trichloroethane
Sri 6200c
1,1,2,2 -Tetrachloroethane
SPA 6200C
1,1,2 -Trichloroethane
SM 6200C
1,1-Dichloroethane
SM 6200C
1, 1 -Dichloroethene
Sty 6200C
1,1-Dichloropropene
SM 6200C
1,2,3-Trichlorobenzene
SM 6200C
1,2,3-Trichloropropane
SM 6200C
1,2,4-Trichlorobenzene
SM 6200C
1,2,4-Trimethylbenzene
SM 6200C
12-Dibromo-3-Chloropropane
SM 6200C
1,2-Dibromoethane
Sty 6200C
1,2 -Dichlorobenzene
SM 6200C
1,2-Dichloroethane
SM 6200C
1,2-Dichloropropane
SM 6200C
1,3,5-Trimethylbenzene
SPA 6200C
1,3 -Dichlorobenzene
SM 6200C
1,3-Dichloropropane
San 6200C
1,4 -Dichlorobenzene
San 6200C
2,2-Dichloropropane
SM 6200c
2-Chlorotoluene
SM 6200c
4-Chlorotoluene
SPA 6200c
Benzene
Sari 6200C
136 mg/L
12/07/2016
3.7 mg/L
12/0612016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
1 211 0/201 6
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/1012016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
1211012016
< 0.50 pg/L
12/10/2016
Report #:: 2016-17367 Page 1 of 51

Environmental Chemists,Inc.
6602 lVindmill V 13; Wilmington, NC.. 28405 * 910.392.0223 Lab - 91.0.392.4421 Fax
71.0 Bow ertaw n .[toad, iUianteo, NC 27954 g 252,473_5702 Lab/Fax
255-A 6,Vilmington Highway, Jacksonville, NC 285-40 a 9.10.347,5843 I..:<ab 1:`ax
inib(tL;environiiienla lclleinists.coiil
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
Bromochloromethane
SM 6200c
< 0.50 pg/L
12/10/2016
Bromodichloromethane
SM6200C
< 0.50 pg/L
12/10/2016
Bromoform
SM 6200c
< 0.50 pg/L
12/10/2016
Bromomethane
SM 6200C
< 0.50 pg/L
12/1012016
Carbon tetrachloride
SM 6200C
< 0.50 pg/L
12/10/2016
Chlorobenzene
SM 62000
< 0.50 pg/L
12/10/2016
Chloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
Chloroform
SM 62000
< 0.50 pg/L
12/10/2016
Chloromethane
SM 62000
< 0.50 pg/L
12/10/2016
cis-1.2-Dichloroethene
SM 62000
< 0.50 pg/L
12110/2016
cis- 1,3-Dichloropropene
SNA 62000
< 0.50 pg/L
12/10/2016
Dibromochloromethane
sM 6200C
< 0.50 pg/L
12/10/2016
Dibromomethane
SM 62000
< 0.50 pg/L
12/1012016
Dichlorodifluoromethane
SM 62000
< 0.50 pglL
12/10/2016
Ethylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
Hexachlorobutadiene
SM 6200c
< 0.50 pg/L
12/10/2016
Isopropylbenzene
SM 6200c
< 0,50 pg/L
12/10/2016
M+P Xylene
SM 6200c
< 1.00 pg/L
12/10/2016
Methylene chloride
SM 6200c
< 0.50 pg/L
12/10/2016
Naphthalene
SM 62000
< 0.50 pg/L
12/10/2016
n-Butylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
n-Propylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
ortho-Xylene
SM 62000
< 0.50 pg/L
12/10/2016
p-Isopropyltoluene
SM 6200c
< 0.50 pg/L
12/10/2016
sec-Butylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Styrene
SM 6200c
< 0.50 pg/L
12110/2016
tert-Butylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
Tetrachloroethene
SM 6200c
< 0.50 pg/L
12/10/2016
Toluene
SM 6200c
< 0.50 pg/L
12/10/2016
Report #:: 2016-17367
Page 2 of 51

6602 Windmill I'Vay; Wilmingtort, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
71.0 Bowsertowii Road, ,Manteo, NC 27954 0 252.473.5702 Lab/Fax
2:55-A Wilmirigton Highway, Jacksonville, NC 28540 - 910.347.3643 Lab/Fax
info<ri environmcntalehemists.eom
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Trans- 1,2-Dichloroethene SM 6200C
< 0.50 pg/L
12/10/2016
Trans- 1,3-dichloropropene SM 6200C
< 0.50 pg/L
12/10/2016
Trichloroethene SM 6200c
< 0.50 pg/L
12/10/2016
Trichlorofluoromethane SM 6200C
< 0.50 pg/L
12/10/2016
Vinyl chloride SM 6200c
< 0.50 pg/L
12/10/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/07/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2016
Reaort #:: 2016.17367 Page 3 of 51

ANALYTICAL & CONSULTING CHEMISTS
6602 Gtiindmill Way, Wilmington, NC 28405 o 910.392.0223 Lab @ 910.392.4-124Fax
710 Bowsertow.n Road, Manteo, NC 27954 m 252,473.5-702 Lair; :Fax
255-A Wilmington I lig way, Jackson��ille, NC 28540 a 910.347.5843 Lab Fax
iiirc);tF Liivifoiliiieiliitich£tnists.coin
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
16-41886 Site: MW -9 12/5/2016 9:24 AM Water JP
Test
Method
Results Date Analyzed
Sulfate
EPA 300.0
88 mg/L
Total Organic Carbon (TOC)
SM 5310 B
2.2 mg/L
1,1,1,2 -Tetrachloroethane
SM 62000
< 0.50 pg/L
1,1,1 -Trichloroethane
SM 6200C
< 0.50 pg/L
1,1,2,2-Tetrach loroethane
SM 6200C
< 0.50 pg/L
1,1,2 -Trichloroethane
SM 62000
< 0.50 pg/L
1,1-Dichloroethane
SM 65200C
< 0.50 pg/L
1,1-Dichloroethene
SM 6200C
< 0.50 pg/L
1, 1 -Dichloropropene
SM 62000
< 0.50 pg/L
1,2,3-Trichlorobenzene
SM 62000
< 0,50 pg/L
1,2,3-Trichloropropane
SM 62000
< 0.50 pg/L
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
1,2,4-Trimethy[benzene
SM 62000
< 0.50 pg/L
1,2-Dibromo-3-Chloropropane
SM 6200C
< 0.50 pg/L
1,2-Dibromoethane
SM 6200C
< 0.50 pg/L
1,2 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
1,2-Dichloroethane
SM 6200C
< 0.50 pg/L
1,2-Dichloropropane
SM 6200C
< 0.50 pg/L
1; 3,5-Trimethylbenzene
SM 62000
< 0.50 pg/L
1,3 -Dichlorobenzene
SM 62000
< 0.50 pg/L
1,3-Dichloropropane
SM 6200C
< 0.50 pg/L
1,4 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
2,2-Dichloropropane
SM 6200C
< 0.50 pg/L
2-Chlorotoluene
SM 62000
< 0.50 pg/L
4-Chlorotoluene
SM 62000
< 0.50 pg/L
Benzene
SM 6200C
< 0.50 pg/L
12/07/2016
12/06/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
12/10/2016
Report k:: 2016-1736,' Page 4 of 51
v

Environmental Ce . t
Hv
g602 4b`intlrni]t 41 ay, Wilmin-ton, NC 28.105 - 91.0392.11223 Lab a 910.392,442-4 Fax
710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab; Fax
255-A Wilmington Highway, Jacksonville, ltiC 28540 C 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS inCo�%:eilviri�nmentralcheruis4s.com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention: Jill Puff
28541
Date of Report: Dec 15, 2016
Customer PO #:
Customer ID: 08110015
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
Bromochloromethane
SM 6200c
< 0.50 pg/L
12/10/2016
Bromodichloromethane
SM 6200c
< 0.50 pg/L
12/1012016
Bromoform
SM 6200C
< 0.50 pg/L
12/10/2016
Bromomethane
SM 6200c
< 0.50 pg/L
12/10/2016
Carbon tetrachloride
SM 5200c
< 0.50 pg/L
12/10/2016
Chlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
Chloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
Chloroform
SM 6200C
< 0.50 pg/L
12/10/2016
Chloromethane
SM 6200c
< 0.50 pg/L
12/10/2016
cis- 1,2-Dichloroethene
San 6200c
< 0.50 pg/L
12110/2016
cis-1,3-Dichloropropene
SM 6200C
< 0.50 pg/L
12/10/2016
Dibromochloromethane
SM 6200c
< 0.50 pg/L
12/10/2016
Dibromomethane
SM 62000
< 0.50 pg/L
1 211 0/201 6
Dichlorodifluoromethane
SM 62000
< 0.50 pg/L
12/10/2016
Ethylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Hexachlorobutadiene
SM 6200c
< 0.50 pg/L
12/1012016
Isopropylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
M+P Xylene
SM 62000
< 1.00 pg/L
12/10/2016
Methylene chloride
SM 6200c
< 0.50 pg/L
12110/2016
Naphthalene
SM 6200c
< 0.50 pg/L
12/10/2016
n-Butylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
n-Propylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
ortho-Xylene
SM 6200C
< 0.50 pg/L
12/10/2016
p-Isopropyltoluene
SM 6200c
< 0.50 pg/L
12/10/2016
sec-Butylbenzene
SM 6200c
< 0.50 pg/L
12110/2016
Styrene
SM 6200c
< 0.50 pg/L
12/10/2016
tert-Butylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
Tetrachloroethene
SM 6200c
< 0.50 pg/L
12/10/2016
Toluene
SM 6200c
< 0.50 pg/L
12/10/2016
Report #:: 2016-17367
Page 5 of 51

6
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill Way, Wilmington, NC 26405 s 910.392,0223 Lab # 910.392.4424 Fax
710 Bowsertown Road, Manteo.. NC 27954 9 252.473.5702Lab/Fax
255-A Wilminiton:Highway, Jacksonville, NC. 28-140 Q 010.347.5843 Lab; Fax
info(aeii ironuleritalellemists.coiii
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Trans- 1.2-Dichloroethene
SM 6200c
< 0.50 pglL
12110!2016
Trans- 1,3-dichloropropene
SM 6200C
< 0.50 pg1L
12/10/2016
Trichloroethene
SM 6200c
< 0.50 pg/L
12/1012016
Trichlorofluoromethane
SM 6200c
< 0.50 pg/L
12/10/2016
Vinyl chloride
SM 6200c
< 0.50 pg/L
12/10/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/07/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2016
Report M: 2016-17367 Page 6 of 51
I

Environmental Cheis s, Inc.
6602 Windmill Way, Wilmington, NC 28405 o 9".10. 92.0223 Lab ® 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 + 252.473.5702 Lab,%l°ax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.3.17.584"3 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS info iien�"ironmetltalchernists.coert
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention.- Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-41887 Site: MW -10 12/5/2016 9:35 AM Water JP
Test Method Results Date Analyzed
Sulfate
EPA 300.0
209 mg/L
12/07/2016
Total Organic Carbon (TOC)
SM 5310 B
3.1 mg/L
12/06/2016
1,1,1,2 -Tetrachloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
1,1,1 -Trichloroethane
SM 62000
< 0.50 pg/L
12/10/2016
1,1,2,2 -Tetrachloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,1,2 -Trichloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
1, 1 -Dichloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
1, 1 -Dichloroethene
SM 6200C
< 0.50 pg/L
12/10/2016
1, 1 -Dichloropropene
SM 6200c
< 0.50 pg/L
12/10/2016
1,2,3-Trichlorobenzene
SM 62000
< 0.50 pg/L
12/10/2016
1,2,3-Trichloropropane
SM 62000
< 0.50 pg/L
12/10/2016
1,2,4-Trichlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
1,2,4-Trimethylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
1,2-Dibromo-3-Chloropropane
SM 6200C
<0.50pg/L
12/10/2016
1,2-Dibromoethane
SM 6200c
< 0.50 pg/L
12/10/2016
1,2 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
1,2-Dichloroethane
SM 62000
< 0.50 pg/L
12/10/2016
1,2-Dichloropropane
SM 6200c
< 0.50 pg/L
12/10/2016
1,3,5-Trimethylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
1, 3 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/10/2016
1, 3-Dichloropropane
SM 62000
< 0.50 pg/L
12/10/2016
1,4 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
2,2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/10/2016
2-Chlorotoluene
SM 6200c
< 0.50 pg/L
12/10/2016
4-Chlorotoluene
SM 6200c
< 0.50 pg/L
12/10/2016
Benzene
SM 6200c
< 0.50 pg/L
12/10/2016
Report ::: 2016-17367 Page 7 of 51

ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill btiay, Wilmington, NC 28405 - 910.302.0223 I..,ab m 410.392.4424 Fax
71.0 Soivse�rtown Road, llvIanteo, _NC 279:54 s 252.=173.5702 Lab,/Fax
2.55-A VViltnington Higbway, Jacksonville, NC 28540 m 910.347.5843I,ab/Fax
infor em=iroil mentalchetnists.com
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SNA 62000
< 0.50 pg/L
12/1012016
Brornochloromethane
SM 62000
< 0,50 pg/L
12/10/2016
Bromodichloromethane
SM 6200C
< 0,50 pg/L
12/10/2016
Bromoform
SM 62000
< 0.50 pg/L
12/10/2016
Bromomethane
SM 6200C
< 0.50 pg/L
1.2/10/2016
Carbon tetrachloride
SM 62000
< 0.50 pg/L
12/10/2016
Chlorobenzene
SM 62000
< 0.50 pg/L
12/10/2016
Chloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
Chloroform
SM 62000
< 0.50 pg/L
12/10/2016
Chloromethane
SM 6200C
< 0.50 pg/L
12/1012016
cis-1,2-Dichloroethene
SM 62000
< 0.50 pg/L
12/10/2016
cis-1,3-Dichloropropene
SM 6200C
< 0.50 pg/L
12/10/2016
Dibromochloromethane
SM 62000
< 0.50 pg/L
12/10/2016
Dibromomethane
SM 62000
< 0.50 pg/L
12/10/2016
Dichlorodifluoromethane
W 6200C
< 0.50 pg/L
12/10/2016
Ethylbenzene
3P+1 6200C
< 0.50 pg/L
12/10/2016
Hexachlorobutadiene
SM 6200C
< 0.50 pg/L
12/10/2016
Isopropylbenzene
SM 62000
< 0,50 pg/L
12/10/2016
M+P Xylene
SM 62000
< 1.00 pg/L
12/10/2016
Methylene chloride
SM 62000
< 0.50 pg/L
12/10/2016
Naphthalene
SM 62000
< 0.50 pg/L
12/10/2016
n-Butylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
n-Propylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
ortho-Xylene
SM 5200C
< 0.50 pg/L
12/10/2016
p-Isopropyltoluene
SM 62000
< 0.50 pg/L
12/10/2016
sec-Butylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Styrene
SM 62000
< 0.50 pg/L
12/10/2016
tert-Butylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Tetrachloroethene
SM 6200C
< 0.50 pg/L
12/10/2016
Toluene
SM 62000
< 0.50 pg/L
12/10/2016
Report #:: 2016.17367
Page 8 of 51

Environmental Chis s, Inc.
6602 Windmill Way, VVil.mington, NC 28405 * 910 392.0223 Lab m 910.392.4424 Fax
71.0 Bowsertown Road, Manteo, NC 27954 m 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NTC 28540 @ 910.347.5843 Lab/Fax
inEt�(�%anti°iranmei�t�tichemists.c:am
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200C
< 0.50 pg/L
12/10/2016
Trans-1,3-dichloropropene SM 6200C
< 0.50 pg/L
12/10/2016
Trichloroethene SM 62000
< 0.50 pg/L
12/10/2016
Trichlorofluoromethane SM 6200C
< 0.50 pg/L
12/10/2016
Vinyl chloride SM 6200c
< 0.50 pg/L
12/10/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/07/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2016
Report #:: 2016-17367 Page 9 of 51

:aEnvironmental i, Inez
6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 I-Ab * 9.10.392.4424 Fax
710 Boca serto�vn Road, Manteo, .NTC 2'954 0 252.4:3.5702 Lab/Fax
255-AWilr:ung-finn Highway, Jacksonville, NC 23540 s 910.317.58 3 Lala/Fax
ANALYTICAL & CONSULTING CHEMISTS info(�,;environinentalehemists.com
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-41888 Site: MW -13 12/5/2016 10:24 AM Water JP
Test Method Results Date Analyzed
Sulfate
EPA 300.0
<5 mg/L
12/07/2016
Total Organic Carbon (TOC)
SM 5310 B
1.2 mg/L
12/06/2016
1,1,1,2-Tetrachloroethhane
SM 62000
< 0.50 pg/L
12/10/2016
1,1,1 -Trichloroethane
W 6200C
< 0.50 pg/L
12/10/2016
1,1,2,2 -Tetrachloroethane
SM 62000
< 0.50 pg/L
12/10/2016
1,1,2 -Trichloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,1-Dichloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,1-Dichloroethene
SM 62000
< 0.50 pg/L
12/10/2016
1,1-Dichloropropene
Ski 6200C
< 0.50 pg/L
1211012016
1,2, 3-Trichlorobenzene
SM 6200c
< 0.50 pg/L
12/1012016
1;2,3-Trichloropropane
SM 6200C
< 0.50 pg/L
12110/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,4-Trimethylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
1,2-Dibromo-3-Chloropropane
SM 6200C
< 0.50 pg/L
12110/2016
1, 2-Dibromoethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,2 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/10/2016
1,2-Dichloroethane
SM 62000
< 0.50 pg/L
12/10/2016
1,2-Dichloropropane
SM 62000
< 0.50 pg/L
12/10/2016
1, 3, 5-Trimethylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,3 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/10/2016
1,3-Dichloropropane
SM 62000
< 0.50 pg/L
12/10/2016
1,4 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
2,2-Dichloropropane
SM 6200c
< 0.50 pg/L
12110/2016
2-Chlorotoluene
SM 62000
< 0.50 pg/L
12/10/2016
4-Chlorotoluene
SM 62000
< 0.50 pg/L
12/10/2016
Benzene
SM 62000
< 0.50 pg/L
12/10/2016
Report #:: 2016-17367 Page 10 of 51

Environmental q Inc..
6602 Windmill Way, Wilmington, NC 281115 a 910.392.0223 Lab - 910.392.1.12=1 Fax
710 Bowsertown Read, ,Manteo, NC 27954 o 252.=473.5702
2:55-A Wilmirigton Highway, jacksonville, NC 28510 ® 910.317.513-13 Lab/Fax
ill E06ll ;'nV1ron lellt.£1IC1101'111stS.Com
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 62000
< 0.50 pg/L
12/10/2016
Bromochloromethane
SM 6200C
< 0.50 pg/L
12/10/2016
Bromodichloromethane
SM 6200C
< 0,50 pg/L
12/10/2016
Bromoform
SM 6200C
< 0.50 pg/L
12/10/2016
Bromomethane
SM 62000
< 0.50 pg/L
12/10/2016
Carbon tetrachloride
SM 6200C
< 0.50 pg/L
12/10/2016
Chlorobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
Chloroethane
SM 62006
< 0.50 pg/L
12/10/2016
Chloroform
SM 6200c
< 0.50 pg/L
12/10/2016
Chloromethane
SM 62000
< 0.50 pg/L
12/10/2016
cis-1,2-Dichloroethene
SM 62000
< 0.50 pg/L
12/10/2016
cis -1, 3-Dichloropropene
SM 62000
< 0.50 pg/L
1211012016
Dibromochloromethane
SM 62000
< 0.50 pg/L
12/10/2016
Dibromomethane
SM 62000
< 0.50 pg/L
12/10/2016,
Dichlorodifluoromethane
SM 6200C
< 0.50 pg/L
12/10/2016
Ethylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Hexachlorobutadiene
SM 6200c
< 0.50 pg/L
12/10/2016
Isopropylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
M+P Xylene
SM 62000
< 1.00 pg/L
12/10/2016
Methylene chloride
SM 62000
< 0.50 pg/L
12/10/2016
Naphthalene
SM 6200C
< 0.50 pg/L
12/10/2016
n-Butylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
n-Propylbenzene
SN16200C
< 0.50 pg/L
12/10/2016
ortho-Xylene
SM 62000
< 0.50 pg/L
12/10/2016
p-Isopropyltoluene
SM 62000
< 0.50 pg/L
12/10/2016
sec-Butylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Styrene
SM 62000
< 0.50 pg/L
12/10/2016
tert-Butylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Tetrachloroethene
SM 6200C
< 0.50 pg/L
12/10/2016
Toluene
SM 62000
< 0.50 pg/L
12/10/2016
Report #:i 2016-17367
Page 11 of 51

r
ANALYTICAL & CONSULTING CHEMISTS
x
6602 Windmill Way, Wilmington, ILC: 28.411.5 ® 910.392.0223 Lab * 910.:34}2: 4124 Fax
710 Bowsertown Road, Manteo, NC 21 m 252.473.5702 Lab/Fax
255 :Ii Wilmirgtcm Highway, Jacksonville, NC 28540 o 910.347.5843 Lab/Fax
infc)( environmcizlalclxemist�.cofn
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report M 2016-17367
Project ID: Monitoring Wells
Trans -1 ,2-Dichloroethene stet 62000
< 0.50 pg/L
12/10/2016
Trans-1,3-dichloropropene SM 6200C
< 0.50 pg/L
12/10/2016
Trichloroethene SM 6244C
< 0.50 pg/L
12/10/2016
Trichlorofluoromethane SM 62440
< 0.50 pg/L
12/10/2016
Vinyl chloride SM 6244C
< 0.50 pg/L
12/10/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/07/2016
Nitrate Nitrogen subtraction fAethod <0,02 mg/L 12/15/2016
Report #.: 2416-17367 Page 12 of 51

10,160
"t`m f 3a
6602 Windmill Way, 61rilminl;ton, NC 28405 - 91.0.392.0223 Lab * 910.392.442.1 Fax
71.0 Bowsortown road, Manteo, QFC 27954: e 252.=173.5702 Lab/ F=ax .
255-A Wilmington Highway, jackson4ille, ITC 2854:0 - 910.347.5813 Lab/Fax
IT21')iuem' i1'is1ISIS1f:TititICI7E7n1SC5.Gt)Tll
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
1641889 Site: MW -14 12/5/2016 10:14 AM Water JP
Test Method Results Date Analyzed
Sulfate
EPA 30M
<5 mg/L
12/07/2016
Total Organic Carbon (TOC)
SM 5310 s
11.5 mg/L
12/06/2016
1,1,1,2 -Tetrachloroethane
SM62000
<0.50pg/L
12/10/2016
1,1,1 -Trichloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
1,1,2,2 -Tetrachloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,1,2 -Trichloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,1-Dichloroethane
sM 6200c
< 0.50 pg/L
12/10/2016
1,1-Dichloroethene
SM 62000
< 0.50 pg/L
12/10/2016
1,1-Dichloropropene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,3-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,3-Trichloropropane
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,4-Trimethylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2-Dibromo-3-Chloropropane
SM 6200C
< 0.50 pg/L
12/10/2016
1,2-Dibromoethane
SM 6200C
< 0.50 pg/L
12/10/2016
1.2 -Dichlorobenzene
SM6200C
< 0.50 pg/L
12/10/2016
1,2-Dichloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
1,2-Dichloropropane
SM 6200C
<-0.50 pg/L
12/10/2016
1,3,5-Trimethylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
1,3 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,3-Dichloropropane
SM 62000
< 0.50 pg/L
12/10/2016
1,4 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
12110/2016
2,2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/10/2016
2-Chlorotoluene
SM 6200C
< 0.50 pg/L
12/10/2016
4-Chlorotoluene
SM 6200c
< 0.50 pg/L
12/10/2016
Benzene
SM 6200C
< 0.50 pg/L
12/10/2016
Report #:: 2016-17367 Page 13 of 51

Environmental Chemists, Inc.
p 6602 Windmill Way, Wilmington, NC. 284051 a 910.3910223 I -ab 0 910.392.4424 Fax
710 Bowser.totiln Road, N—lanteo, NC 27554 a 2a2.473.57021_ab/Fax
2-95-A VV[Imington l lif hway, Jacksonville, NC 28540 ® 910.347.55843 I..ab/Fax
ANALYTICAL & CONSULTING CHEMISTS info;, eiivironmcntatchemists,com
City of Jacksonville
Post Office Box 128
Jacksonville NC
Attention: Jill Puff
28541
Date of Report: Dec 15, 2016
Customer PO #:
Customer ID: 08110015
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
Bromochloromethane
SM 62000
< 0.50 pg/L
12/10/2016
Bromodichloromethane
SM 6200C
< 0.50 pg/L
12/10/2016
Bromoform
SM 6200C
< 0.50 pg/L
12/10/2016
Bromomethane
SM 6200CC
< 0.50 pg/L
12/10/2016
Carbon tetrachloride
SM 62000
< 0.50 pg/L
12/10/2016
Chlorobenzene
SM 62000
< 0,50 pg/L
12/10/2016
Chloroethane
SM 62000
< 0.50 pg/L
12/10/2016
Chloroform
SM 6200C
< 0.50 pg/L
12/10/2016
Chloromethane
SM 62000
< 0.50 pg/L
12110/2016
cis-1,2-Dichloroethene
SM 6200C
< 0.50 pg/L
12/10/2016
cis- 1,3-Dichloropropene
SM 62000
< 0.50 pg/L
12/10/2016
Dibromochloromethane
SM 62000
< 0.50 pg/L
12/10/2016
Dibromomethane
SM 6200C
< 0.50 pg/L
12/10/2016
Dichlorodifluoromethane
SM 6200C
< 0.50 pg/L
12/10/2016
Ethylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
Hexachlorobutadiene
SM 6200C
< 0.50 pg/L
12/10/2016
Isopropylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
M+P Xylene
SM 6200C
< 1.00 pg/L
12/10/2016
Methylene chloride
SM 62000
< 0.50 pg/L
12/10/2016
Naphthalene
SM 62000
< 0.50 pg/L
12/10/2016
n-Butylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
n-Propylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
ortho-Xylene
SM 62000
< 0.50 pg/L
12/10/2016
p-Isopropyltoluene
SM 6200C
< 0.50 pg/L
12/10/2016
sec-Butylbenzene
SM 62000
< 0,50 pg/L
12/10/2016
Styrene
SM 6200C
< 0.50 pg/L
12/10/2016
tert-Butylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Tetrachloroethene
SM 6200C
< 0.50 pg/L
12/10/2016
Toluene
SM 6200C
< 0.50 pg/L
12/10/2016
Report #:: 20.6-17367
Page 14 of 51

n., M -11
d
6602 Windmill tNby, Wilmington, NC. 28405 ® 910392.0223 1-1b ® §.10.392,44,.24 Fax
7.1{:} 13c>«sertatii°n road, Aianteo, NC 27954 252.473.57M 2Lab/Fax
235-A Wilmington Highway, Jacksonville, NC 28540 91.0.347.5843 Lab/Fax
iii Etfii�:uvlrat�nlen[<�Ic(�e�nits.cc7n�
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SN16200C
< 0.50 pg/L
12/10/2016
Trans- l,3-dichloropropene SM 6200C
< 0.50 pg/L
12/10/2016
Trichloroethene SM 6200c
< 0.50 pg/L
12/10/2016
Trichlorofluoromethane SM 62000
< 0.50 pg/L
12/10/2016
Vinyl chloride SM 6200c
< 0.50 pg/L
12/10/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12105/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/07/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2016
Retort ki 2016-17367 Page 15 of 51

Environmental iso ,
6602 Windmill Wlay. Wilinington, '4lC 21405 * 91.0.392.0223 Lab * 910,392.4424 }"ax
710 Bowsertown Read, .Manteo, itiC 27954 a 252.473.5702 Lab/Fax
2:5±-A Wilmington Highivay, Jacksonville/ NC: 28540 e 910.347.5843 Lab/I`aX
1nfc)(t,,cnvironnleiiialelieniists.c" )ql
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-41890 Site: MW -16 12/4/2016 2:26 PM Water JP
Test Method Results Date Analyzed
Sulfate
EPA 300.0
<5 mg/L
12/07/2016
Total Organic Carbon (TOC)
SM 5310 B
1.2 mg/L
12/06/2016
1,1,1, 2 -Tetrachloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
1,1,1 -Trichloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
1,1,2,2 -Tetrachloroethane
SN4 6200C
< 0.50 pg/L
12/10/2016
1,1,2 -Trichloroethane
SM 6200c
< 0.50 lag/L
12/10/2016
1,1-Dichloroethane
SM 62000
< 0.50 pg/L
12/10/2016
1,1-Dichloroethene
SM 6200c
< 0.50 pg/L
12110/2016
1,1-Dichloropropene
SM 6200c
< 0.50 pg/L
12/10/2016
1,2,3-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,3-Trichloropropane
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,4-Trimethylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2-Dibromo-3-Chloropropane
SM 6200C
< 0.50 pg/L
12/10/2016
1,2-Dibromoethane
SM 6200c
< 0.50 pg/L
12/10/2016
1,2 -Dichlorobenzene
SM 62000
< 0,50 pg/L
12/10/2016
1,2-Dichloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,2-Dichloropropane
SM 62000
< 0.50 pg/L
12/10/2016
1,3,5-Trimethylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
1,3 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
1,3-Dichloropropane
SM 6200c
< 0.50 pg/L
12/10/2016
1,4 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/1012016
2,2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/10/2016
2-Chlorotoluene
SM 6200c
< 0.50 pg/L
12/10/2016
4-Chlorotoluene
SM 6200C
< 0.50 pg/L
12/10/2016
Benzene
SM 6200c
< 0.50 pg/L
12/10/2016
Report #:: 2016-17367 Page 16 o; 51

'. j�t § »,+►r 's FIg3
6602 Windmill C' iy, Wilnaingto.n, NC 28405 m 910,392.0223 Lab - 910.392.4424 F'ax .
710 Bowsertown Road, Manteo, NC: 27954 m 252.473.5702 Lab/Fax
255-A Wilmington 1-lighway, Jacksonville, NC. 28540 • 910.347,5843 7 ab/F i.Ix
in(b(iitnvironrnentalchernist,,�.com
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 62ooc
< 0.50 pg/L
12110/2016
Bromochloromethane
SM 6200C
< 0.50 pg/L
12/10/2016
Bromodichloromethane
SM 6200c
< 0.50 pg/L
12./10/2016
Bromoform
SM 62ooc
< 0.50 pg/L
12/10/2016
Bromomethane
SM 6200c
< 0.50 pg/L
12/10/2016
Carbon tetrachloride
SM 6200c
< 0.50 pg/L
12/10/2016
Chlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
Chloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
Chloroform
SM 6200c
< 0.50 pg/L
12/10/2016
Chloromethane
SM 6200C
< 0.50 pg/L
12/10/2016 -
cis-1,2-Dichloroethene
SM 6200C
< 0.50 pg/L
12/10/2016
cis-1,3-Dichloropropene
SM 6200c
< 0.50 pg/L
12/10/2016
Dibromochloromethane
SM 6200
< 0.50 pg/L
12/10/2016
Dibromomethane
Sen 6200c
< 0.50 pg/L
12/10/2016
Dichlorodifluoromethane
SM 62000
< 0.50 pg/L
12/10/2016
Ethylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
Hexachlorobutadiene
SNI -6200C
< 0.50 pg/L
12/10/2016 .
I sop ropyl benzene
SM 6200C
< 0.50 pg/L
12/10/2016 -
M+P Xylene
SM 6200C
< 1.00 pg/L
12/10/2016
Methylene chloride
SM 6200C
< 0.50 pg/L
12/10/2016
Naphthalene
SM 6200C
< 0.50 pg/L
12/10/2016
n-Butylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
n-Propylbenzene
SM 6200c
< 0.50 pg/L
12/1012016
ortho-Xylene
SM 6200c
0.88 pg/L
12/10/2016
p-Isopropyltoluene
SM 6200c
< 0.50 pg/L
12/10/2016
sec -Butyl benzene
SM 6200c
< 0.50 pg/L
12/10/2016
Styrene
SM 6200c
< 0.50 pg/L
12/10/2016
tert-Butylbenzene
SM 6200c
< 0.50 pg/L
1211012016
Tetrachloroethene
SAA 6200c
< 0.50 pg/L
12/10/2016
Toluene
SM 6200C
< 0.50 pg/L
12/10/2016
Report #:: 2016-17367
Page 17 of 51

J
e
ANALYTICAL & CONSULTING CHEMISTS
nvir n e taChemists, Ine.,
6£502 Win(imili 41�'at, Wilm.ingtoii, I' C 28405 o 910.392.0223 Lab - 9.10.392.4:-124 .Fax
710 Bow;sertown Rona, Nianteo, NC. 27954 a 252.4:73.5702 Lab/ Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910347.5843 Lab/ Fax
inic>{aLuvironmentillClli tlliStS.CO1Tl
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200C
< 0.50 pg/L
1 211 0/2 01 6
Trans-1,3-dichloropropene SM 6200C
< 0.50 pg/L
12/10/2016
Trichloroethene SM 62000
< 0.50 pg/L
12/10/2016
Trichlorofluoromethane SM 6200C
< 0.50 pg/L
1 2/1 012 01 6
Vinyl chloride SM 6200C
< 0.50 pg/L
12/10/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0,02 mg/L 12/07/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2016
Report #:: 2016-17367 Page 18 of 51

Environmental eiS s, Inc..
6602 Windmill Way VVilmin;ton, NC 28405 a 910,392.0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, 1danteo, NC 27954 a 252.473.5702 Lab; Fax
255-A VVil.mi.ngton I lighway, Jackswwiile, NC 28540 + 910.347.98,1:3 Lab/Fax
1 i1 i t)� Ctc'liYi i'O11In CTl Eil ll'll�lil I;i tS.Ci)721
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-41891 Site: MW -17 12/4/2016 4:23 PM Water JP
Test
Method
Sulfate
EPA 300,0
Total Organic Carbon (TOC)
SM 5310 e
1,1,1,2 -Tetrachloroethane
SM 6200C
1,1,1 -Trichloroethane
sra 6200C
1,1,2,2 -Tetrachloroethane
SM 6200C
1,1,2 -Trichloroethane
SM 6200c
1,1 -Dish loroethane
SM 6200c
1,1-Dich loroethene
SM 6200c
1,1-Dichloropropene
SM 6200C
1,2,3-Trichlorobenzene
SM 62000
1,2,3-Trichloropropane
SM 6200c
1,2,4-Trichlorobenzene
SM 6200C
1, 2,4-Trimethylbenzene
SM 6200C
1,2-Dibromo-3-Chloropropane
SM 6200C
1,2-Dibromoethane
SM 6200c
1, 2 -Dichlorobenzene
sM 6200C
1.2-Dichloroethane
sM 62ooc
1, 2-Dichloropropane
SM 6200c
1,3,5-Trimethylbenzene
srt 6200C
1,3 -Dichlorobenzene
SM 6200c
1, 3-Dichloropropane
SM 6200c
1,4 -Dichlorobenzene
SM 6200c
2,2-Dichloropropane
SM 6200c
2-Chlorotoluene
SM 6200C
4-Chlorotoluene
SM 6200c
Benzene
SM 6200C
Results Date Analyzed
<5 mg/L
12/07/2016 .
1.9 mg/L
12/06/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016 "
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
Report #:: 2016-17367 Page 19 of 51

Envit a fists,Inc;
6602 Windmill VV'ay, WilminL7ton, NC 284:05 d 910.392,0223 I..,ab - 10 392,4424 Fax
710 liowsertown Read, Manteo,:L\C 27954 0 252.=17 3.5702 Lab; Fiix
255-A VVilcnington Highway, Jacksonville, NC 28,540 - 910.347.5843 Lab. /Fax
in toCcr`en�•ironmerltalchenlists.conl
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
Bromochloromethane
SM 6200c
< 0.50 pg/L
12/10/2016
Bromodichloromethane
SM 6200C
< 0.50 pg/L
12/10/2016
Bromoform
SM 6200C
< 0.50 pg/L
12/10/2016
Bromomethane
SfA 132000
< 0.50 pg/L
12/10/2016
Carbon tetrachloride
SM 62000
< 0.50 pg/L
12/10/2016
Chlorobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
Chloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
Chloroform
SM 62000
< 0.50 pg/L
12/10/2016
Chloromethane
SM 62000
< 0.50 pg/L
12/10/2016
cis-1,2-Dichloroethene
SM 6200C
< 0.50 pg/L
12/10/2016
cis- 1,3-Dichloropropene
sM 6200C
< 0.50 pg/L
12/10/2016
Dibromochloromethane
SNA 6200C
< 0.50 pg/L
12/10/2016
Dibromomethane
SM 6200c
< 0.50 pg/L
12/10/2016
Dichlorodifluoromethane
SM 6200C
< 0.50 pg/L
1 211 0/201 6
Ethylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
Hexachlorobutadiene
SM 6200c
< 0.50 pg/L
12/10/2016
Isopropylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
M+P Xylene
SM 6200c
< 1.00 pg/L
12/10/2016
Methylene chloride
SM 6200C
< 0.50 pg/L
12/10/2016
Naphthalene
SM 62000
< 0.50 pg/L
12/10/2016
n-Butylbenzene
SN1 62ooc
< 0.50 pg/L
12/10/2016
n-Propylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
ortho-Xylene
SM 6200c
< 0.50 pg/L
12/10/2016
p-Isopropyltoluene
SPA 6200C
< 0.50 pg/L
12/10/2016
sec-Butylbenzene
SN16200C
< 0.50 pg/L
12/10/2016
Styrene
SM 6200C
< 0.50 pg/L
12/10/2016
tert-Butylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
Tetrachloroethene
SM 6200C
< 0,50 pg/L
12/10/2016
Toluene
SM 6200c
< 0,50 pg/L
12/10/2016
Report #:: 2016-17367
Page 20 of 51

6602 Windmill. Way, Wilmington, NC. 28405 - 910.392.0223 *LIb m 910.392.142=1 Fax
710 Bo sertown :Road, '4lanteo, NC 27954 a 252.473.5702 Lab/Fax
255-A Wilmington t lir; iwav Jacksonville, NC 28540 c 910.347.5843 Lab/Fax
i iifo (Ci/c rivi ro t)til entti lcheniist5, coin
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Trans- 1,2-Dichioroethene SM 6200C
< 0,50 pg/L
12/10/2016
Trans- l,3-dichloropropene SM 6200C
< 0.50 pg/L
12/10/2016
Trichloroethene SM 6200C
< 0.50 pg/L
12/10/2016
Trichlorofluoromethane SM 6200c
< 0.50 pg/L
12/10/2016
Vinyl chloride SM 6200c
< 0.50 pg/L
12/10/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/07/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2016
Report fi:: 2016-17367 Page 21 of 61

Environmental Chemists, 4-
6602 41"indmill kAlay, tb'ilxninlyton, NC 28405 o 9110.392.0223 Lab o 910.392.4424 Fax
710 Bowsertown Road, Manteo,.N(' 27954 + 2S2.473.57021...ab/lax
255-A Wilmington Highway, Jacksonville, NC 28540 ® 910.347.5843 Lab/Fax
in#c�ta-eni-ironine�lt4�lrllcmists.com
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
16-41893 Site: MW -1
12/4/2016 3:39 PM Water JP
Test
Method
Results Date Analyzed
Sulfate
EPA 300.0
12 mg/L
12/07/2016
Total Organic Carbon (TOC)
SM 5310 B
12.2 mg/L
12/08/2016
1,1,1,2 -Tetrachloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,1,1 -Trichloroethane
SM 6200c
< 0.50 pg/L
12110/2016
1,1,2,2 -Tetrachloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,1,2 -Trichloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
1,1-Dichloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
1,1-Dichloroethene
SM 6200c
< 0.50 pg/L
12/10/2016
1,1-Dichloropropene
SM 6200c
< 0.50 pg/L
12/10/2016
1,2,3-Trichlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
1,2,3-Trichloropropane
SM 62000
< 0.50 pg/L
12/10/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,4-Trimethylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
1,2-Dibromo-3-Chloropropane
SM 6200c
< 0.50 pg/L
12/10/2016
1,2-Dibromoethane
SM 6200c
< 0.50 pg/L
12/10/2016
1,2 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
1,2-Dichloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
1,2-Dichloropropane
SM 6200c
< 0.50 pg/L
12/10/2016
1,3,5-Trimethylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
1,3 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
1,3-Dichloropropane
SM 6200c
< 0.50 pg/L
12110/2016
1,4 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
2,2-Dichloropropane
SM 6200c
< 0.50 pg/L
12/10/2016
2-Chlorotoluene
SM 6200c
< 0.50 pg/L
12/10/2016
4-Chlorotoluene
SM 6200c
< 0.50 pg/L
12110/2016
Benzene
SM 6200c
< 0.50 pg/L
12/10/2016
Report #:. 2016-17367 Page 22 of 51

Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, N('-'28405 m 910.392.0223 Lab a 910.392.1424 Fax
710 Bowsc'Ytown Road, Manteo, NC 27954 ® 252.473.5702 Lab! Fax
2;55-A Wilmington Highway, Jacksonvi le, NC.. 28540 * 910,347.584.3 Lab/Fax
info(izenv iro.nnient<alchemists.co5n
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 6200C
< 0,50 pg/L
12/10/2016
Bromochloromethane
SM 6200C
< 0.50 pg/L
12/10/2016
Bromodichloromethane
SM 6200C
< 0.50 pg/L
12/10/2016
Bromoform
SM 6200C
< 0.50 pg/L
12/10/2016
Bromomethane
SM 6200C
< 0.50 pg/L
12/10/2016
Carbon tetrachloride
SM 6200c
< 0.50 pg/L
12/10/2016
Chlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
Chloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
Chloroform
SM 62000
< 0.50 pg/L
12/10/2016
Chloromethane
SM 6200c
< 0.50 pg/L
12/10/2016
cis-1,2-Dichloroethene
SM 62000
< 0'.50 pg/L
12/10/2016
cis-1,3-Dichloropropene
SN162000
< 0.50 pg/L
12/10/2016
Dibromochloromethane
SM 6200c
< 0.50 pg/L
12/10/2016
Dibromomethane
SM 62000
< 0.50 pg/L
12/10/2016
Dichlorodifluoromethane
SM 6200c
< 0.50 pg/L
12/10/2016
Ethylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
Hexachlorobutadiene
SN4 62000
< 0.50 pg/L
12/10/2016
Isopropylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
M+P Xylene
SM 62000
< 1.00 pg/L
12/10/2016
Methylene chloride
SM 6200c
< 0.50 pg/L
12/10/2016
Naphthalene
SN16200C
< 0.50 pg/L
12/10/2016
n-Butylbenzene
SM 6200C
< 0.50 pg/L
12/1012016
n-Propylbenzene
SM 6200c
< 0.50 pg/L
12/10/201.6
ortho-Xylene
SM 62000
< 0.50 pg/L
12/10/2016
p-isopropyltoluene
SM 62000
< 0.50 pg/L
12/10/2016
sec-Butylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
Styrene
SM 6200c
< 0.50 pg/L
12/10/2016
te rt -Bu tyl benzene
SM 6200c
< 0.50 pg/L
12/10/2016
Tetrachloroethene
SM 62000
< 0.50 pg/L
12/10/2016
Toluene
5M 6200C
< 0.50 pg/L
12/10/2016
Report #:: 2016-17367
Page 23 of -51

ANALYTICAL & CONSULTING CHEMISTS
11,1111111111 Ir ;
eJIM-
iI Is
6602 Windmill Gtiay, V%ihnington, :NC 28405 & 91.0.302.0223 Lab 9 010.312.4424 Fax
710 Bowsertown Road, Mantei), NC 27954 o 252.473.5702 Lab/1-ax
255-A V4'.ilfnin;tc)n Highway, Jacksonville, NK 28,540 » 910.347.5843 Lab/ Fax
info(ai�,envi ronnienta tchernists.com
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Trans- 1,2-Dichloroethene SM 6200C
< 0.50 pg/L
12/10/2016
Trans- 1,3-dichloropropene SM 6200c
< 0.50 pg/L
12/10/2016
Trichloroethene SM 6200c
< 0.50 pg/L
12/10/2016
Trichlorofluoromethane Sha 6200C
< 0.50 pg/L
12/10/2016
Vinyl chloride SM 6200c
< 0.50 pg/L
12/10/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016
Nitrate+Nitrite-Nitrogen EPA 3532 < 0.02 mg/L 12/0712016
Nitrate Nitrogen subtraction (Method <0.02 mg/L 12/15/2016
Report #:: 2016-17367 Page 24 of 51

Environmental eInc.
6602 Windmill Way, V4rilminiton, NTC: 28105 , 910.392.0223 L.ab - 910.392.4424 Fax
77.0 Bowsertown Road, Nlanteo, NC 27954 ® 252.473.5702 Lab'/Fax
255-A Wilmington Highway, Jacksonville, NC 28,540 c 910.347.584; Lab/Fax
infoizen�ironmentaichemists.com
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
16-41894 Site: MW -2
12/4/2016 9:53 AM Water JP
Test
Method
Results Date Analyzed
Sulfate
EPA 300.0
<5 mg/L
12/08/2016
Total Organic Carbon (TOC)
SM 5310 B
3.2 mg/L
12/08/2016
1,1,1,2 -Tetrachloroethane
SM 6200C
<0.50pg/L
12/10/2016
1,1,1 -Trichloroethane
SM 62000
< 0.50 pg/L
12/10/2016
1,1,2,2 -Tetrachloroethane
SM 62000
< 0.50 pg/L
12/10/2016
1,1,2 -Trichloroethane
son 6200C
< 0.50 pg/L
12/10/2016
1,1-Dichloroethane
SM 62000
< 0.50 pg/L
12/10/2016
1,1-Dichloroethene
SM 6200C
< 0.50 pg/L
12/10/2016
1,1-Dichloropropene
SM 62000
< 0.50 pg/L
12/10/2016
1,2,3-Trichlorobenzene
SM 62000
< 0.50 pg/L
12110/2016.
1,2,3-Trichloropropane
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,4-Trimethylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2-Dibromo-3-Chloropropane
SM 6200C
<0.50pg/L
12/10/2016
1,2-Dibromoethane
SM 62000
< 0.50 pg/L
12/10/2016
1,2 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/10/2016
1,2-Dichloroethane
SM 62000
< 0.50 pg/L
12/10/2016
1,2-Dichloropro pane
SM 62000
< 0.50 pg/L
12/10/2016
1,3,5-Trimethylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
1,3 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,3-Dichloro propane
SM 62000
< 0.50 pg /L
12/10/2016
1,4 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/10/2016
2,2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/10/2016
2-Chlorotoluene
SM 62000
< 0.50 pg/L
12/10/2016
4-Chlorotoluene
SM 6200C
< 0.50 pg/L
12/10/2016
Benzene
SM 62000
< 0.50 pg/L
42/10/2016
Report #:: 2016-17367 Page 25 of 51

Environmental Chemists,
6602 Windmill Way, Wiliningtcan, NC: 28405 a 910.392.0223 Lab - 910.392.4424 Fax
710 Bowserwwn Road, liantea,.NC 2795 * 252.473.3702 Lab/Fax
255-A t1'il.mington'I lighway, Jacksonville, NC 28540 * 910.347.584.31_ab,'Fax
intia��isem-ironaner�talG11c;1T1tStS.C;QIl1
City of Jacksonville
Date of Report: Dec 15. 2016
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 62000
< 0.50 pg/L
12/10/2016
Bromochloromethane
SM 6200C
< 0.50 pg1L
12/10/2016
Bromodichloromethane
SM 6200C
< 0.50 pg/L
12/10/2016
Bromoform
SM 6200C
< 0.50 pg/L
12/10/2016
Bromomethane
SPA 6200C
< 0.50 pg/L
12/10/2016
Carbon tetrachloride
SM 62000
< 0.50 pg/L
12/10/2016
Chlorobenzene
SM 62000
< 0.50 pg/L
12/10/2016
Chloroethane
SM 62000
< 0.50 pg/L
12/10/2016
Chloroform
SM 6200C
< 0.50 pg/L
12/10/2016
Chloromethane
SM 62000
< 0.50 pg/L
12/10/2016
cis-1,2-Dichloroethene
SM 62000
< 0.50 pg/L
12/10/2016
cis-1,3-Dichloropropene
SM 6200C
< 0.50 pg1L
12/10/2016
Dibromochloromethane
SM 62000
< 0.50 pg/L
12/10/2016
Dibromomethane
. SM 62000
< 0.50 pg/L
12/10/2016
Dichlorodifluoromethane
SM 62000
< 0.50 pg/L
12/10/2016
Ethylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Hexachlorobutadiene
SM 62000
< 0.50 pg/L
12/10/2016
Isopropylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
M+P Xylene
SM 62000
< 1.00 pg/L
12/10/2016
Methylene chloride
SM 6200C
< 0:50 pg/L
12/10/2016
Naphthalene
SM 62000
< 0.50 pg/L
12/10/2016
n-Butylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
n-Propylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
ortho-Xylene
SM 62000
< 0.50 pg1L
12/10/2016
p-Isopropyltoluene
SM 62000
< 0.50 pg/L
12/10/2016
sec-Butylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Styrene
SM 62000
< 0.50 pg/L
12/10/2016
tent-Butylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Tetrachloroethene
SM 62000
< 0.50 pg/L
12/10/2016
Toluene
SFVs 6200C
< 0.50 pg/L
12/10/2016
Report #:: 2016-17367
Page 26 of 51

6602 Windmill t'r`ay, Wilmington, NIC 28405 * 910.392,0223 Lab - 91.0.392.44.24 Fax
710 Bowsertotl n Road, Mlanteo, NC 27954 ® 252.473.5702 I..ab,'Fax
255-A Wilmington.Highway, Jacksonville, NC 28540 ® 91.0.347.5813 Lab; Fax
inli>�eu�; irontnerttztichemists.catn
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200c
< 0.50 tag/L
12/10/2016
Trans- l,3-dichloropropene SM 6200C
<0.50pg/L
12110/2016
Trichloroethene SM 6200C
< 0.50 pg/L
12/10/2016
Trichlorofluoromethane SM 6200C
< 0.50 pg/L
12/10/2016
Vinyl chloride SN16200C
< 0.50 pg/L
12/1012016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 0.10 mg/L 12/07/2016
Nitrate Nitrogen Subtraction Method 0.10 mg/L 12/15/2016
Report #:: 2015-17367 Page 27 of 51

ANALYTICAL & CONSULTING CHEMISTS
Environmental Che1s s, Inc. -
6602
.-6602 Windmill IN"ay, Wilrnington, NC 74405 « 910.392.0223 Lab - 910392.442.4. Fix
710 Bowsertown Road, MantCo, ti?C 2795=4 * 232.47.3.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 285,40 e 910.347.5843 Lab; Fax
info itCilviroll111entalchemists.com
City of Jacksonville Date of Report: Dec 16, 2016
Post Office Box 128 Customer PO #: 150011
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-41895 Site: MW -3 12/3/2016 - 1:06 PM Water JP
Method
Sulfate
EPA 300.0
Total Organic Carbon (TOC)
SM 5310 B
1,1,1,2 -Tetrachloroethane
SM 6200C
1,1,1 -Trichloroethane
SM 6200C
1,1,2,2 -Tetrachloroethane
SM 62000
1,1,2 -Trichloroethane
SM 6200c
1,1-Dichloroethane
SM 62000
1,1-Dichloroethene
SM 5200c
1,1-Dichloropropene
SM 6200c
1,2,3-Trichlorobenzene
SM 6200c
1,2,3-Trichloropropane
SM 6200C
1,2,4-Trichlorobenzene
SM 6200c
1,2,4-Trimethylbenzene
SM 6200c
1,2-Dibromo-3-Chloropropane
SM 6200C
1,2-Dibromoethane
SM 62000
1,2 -Dichlorobenzene
SM 6200C
1,2-Dichloroethane
SM 6200c
1,2-Dichloropropane
SM 6200C
1,3,5-Trimethylbenzene
SM 6200c
1,3 -Dichlorobenzene
SM 62ooc
1, 3-Dichloropropane
SM 6200c
1,4 -Dichlorobenzene
SM 6200c
2,2-Dichloropropane
SM 6200C
2-Chlorotoluene
SM 6200c
4-Chlorotoluene
SM 6200c
Benzene
SM 6200c
Report ft:: 2016-17367
Results Date Analyzed
9 mg/L
12/07/2016
1.7 mg/L
12/08/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/1012016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12110/2016
< 0.50 pg/L
12110/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L .
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12/10/2016
< 0.50 pg/L
12110/2016
< 0.50 pg/L
12110/2016
< 0.50 pg/L
12/1012016
Page 28 of 51

x spa. Chemists, Inc.
¢,
6602 Windmill Way, Wilmington, NC, 28405 A 910.3 ?2.0223 Lab - 91.0,391442-4 Fax
� d
'10 Bowsertoc,%.-n .Road, kianteo, NC 27954 ® 252,47.3-9702 Lab%Fax
255-A Wilmington Fli hwav, Jacksonville, NC 28540 . 91().347.5543 Lab Fax
ANALYTICAL & CONSULTING CHEMISTS info(' environmentalclietnists.com
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 62000
< 0.50 pg/L
12/10/2016
Bromochloromethane
SM 62000
< 0.50 pg/L-
12/10/2016
Bromodichloromethane
SM 62000
< 0.50 pg/L
12/10/2016
Bromoform
SM 62000
< 0.50 pg/L
12/10/2016
Bromomethane
SM 6200C
< 0,50 pg/L
12/10/2016
Carbon tetrachloride
SM 62000
< 0.50 pg/L
12/10/2016
Chlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
Chloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
Chloroform
SM 6200C
< 0.50 pg/L
12/10/2016
Chloromethane
SM 6200C
< 0.50 pg/L
12/10/2016
cis-1,2-Dichloroethene
SM 62000
< 0.50 pg/L
12/10/2016
cis- 1,3-Dichloropropene
SM 6200C
< 0.50 pg/L
12/10/2016
Dibromochloromethane
SM 62000
< 0.50 pg/L
12/1012016
Dibromomethane
SM 6200C
< 0.50 pg/L
12/i 0/2016
Dichlorodifluoromethane
SM 62000
< 0.50 pg/L
12/10/2016
Ethylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Hexachlorobutadiene
SM 62000
< 0.50 pg/L
12/10/2016
Isopropyl benzene
SM 62000
< 0.50 pg/L
12/10/2016 .
M+P Xylene
SM 6200C
< 1.00 pg/L
12/10/2016
Methylene chloride
SM 6200C
< 0.50 pg/L
12/10/2016
Naphthalene
SM 62000
< 0.50 pg/L
12/10/2016
n-Butylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
n-Propylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
ortho-Xylene
SM 62000
< 0.50 pg/L
12/10/2016
p-Isopropyltoluene
SM 62000
< 0.50 pg/L
12/10/2016
sec-Butylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Styrene
Srn 62000
< 0.50 pg/L
12/10/2016
tert-Butylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
Tetrachloroethene
SM 62000
< 0.50 pg/L
12/10/2016
Toluene
SM 6200C
< 0.50 pg/L
12/10/2016
Report #.: 2016.17367
Page 29 of 51

ANALYTICAL & CONSULTING CHEMISTS
t. Chemists, q
6602- Windmill W'i , Wilmington, NC 28405 e 910.392.0223 Lab a 91.0.392.4424 Fax
710 Bowsertown Road Manteo, NC. 27994'- 252.473 ,5702 Lab/ Fax
2.i5 -A Wilmington I fig i ay, Jacksonville, NC 28540 m 91.0.347.5843 Lab; Fax
info;ii cnvironmentalchenlists.com
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200C
< 0.50 pq/L
12/10%2016
Trans- l,3-dichloropropene SM 82006
< 0.50 pg/L
12/10/2016
Trichloroethene SM 6200C
< 0.50 pg/L
12/10/2016
Trichlorofluoromethane SM 82000
< 0.50 pg/L
12/1012016
Vinyl chloride SM 6200C
< 0.50 dig/L
12/10/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/07/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2016
Report #.: 2018-17387 Page 30 of 51

6602 Windmill Way, Wilmington, NC 28405 + 910.392.0223 I.ab ® 91.0, 392.4424 Fax
710 6owsertowii.load, Ivlanteo, NC 279,54 @ 252.473.5702 Lab; Fax
255-A Wilmington Highway, Jacksonville, NC 25540 * 910.347.5843I..,abi Fax
in(�}lrierrvi rc,rtr��enta lchemists.com
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-41896 Site: MW -4 12/4/2016 8:51 AM Water JP
Test Method Results Date Analyzed
Sulfate
EPA 300.0
30 mg/L
12/08/2016
Total Organic Carbon (TOC)
SM 5310 8
1.5 mg/L
12/08/2016
1,1,1,2 -Tetrachloroethane
SM 6200C
<0.50pg/L
12/10/2016
1,1,1 -Trichloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
1,1,2,2 -Tetrachloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,1,2 -Trichloroethane
SM 62000
< 0.50 pg/L
12/10/2016
1,1-Dichloroethane
SM 62000
< 0.50 pg/L
12/10/2016
1,1-Dichloroethene
SM 6200C
< 0.50 pg/L
12/10/2016
1,1-Dichloropropene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,3-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,3-Trichloropropane
SM 6200c
< 0.50 pg/L
1211 012 0 1 6
1,2,4-Trichlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
1,2,4-Trimethylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2-Dibromo-3-Chloropropane
SM 6200C
<0,50pg/L
12/10/2016
1,2-Dibromoethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,2 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
1,2-Dichloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
1,2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/10/2016
1:3.5-Trimethylbenzene
Ski 6200C
< 0.50 pg/L
12/10/2016
1,3 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,3-Dichloropropane
SM 6200C
< 0.50 jig/L
12/10/2016
1,4 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/10/2016
2,2-Dichloropropane
SM 6200c
< 0.50 pg/L
12/10/2016
2-Chlorotoluene
SM 6200c
< 0.50 pg/L
12/10/2016'
4-Chlorotoluene
SM 6200c
< 0.50 pg/L
12/10/2016
Benzene
SM 6200c
< 0.50 pg/L
12/10/2016
Report #J:: 2016-17367 Page 31 of 51

6602 6�'inclriiiil 44-ery, 41'iltn nl;ton, NC 284:07 « 91.0.3910223 I.,ab o 91.0.392.4424 Fax
71.0 Bowsertown road,;,Mantco, NC: 279:34 ® 2.52.=173.3702 L.ab/Fax
2555-A b 'ilrninzrton Highway, iacksonville, NC 28540 s 910.347.5843 Lab' Pax
ink'c7,i,environmen taicheinists.corn
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 62000
< 0.50 pg/L
12/10/2016
Bromochloromethane
Srvi 6200c
< 0.50 pg/L
12110/2016
Bromodichloromethane
SM 6200C
< 0,50 pg/L
12/1012016
Brornoform
SM 6200C
< 0.50 pg/L
12/10/2016
Bromomethane
SM 6200C
< 0.50 pg/L
12/10/2016
Carbon tetrachloride
SM6200C
< 0.50 pg/L
12/10/2016
Chlorobenzene
SM 62000
< 0,50 pg/L
12/10/2016
Chloroethane
sin 6200c
< 0.50 pg/L
12110/2016
Chloroform
sM 62000
< 0.50 pg/L
12/10/2016
Chloromethane
sM 6200c
< 0.50 pg/L
12/10/2016
cis-1,2-Dichloroethene
SM 62000
< 0.50 pg/L
12/1012016
cis-1,3-Dichloropropene
SM 6200C
< 0.50 pg/L
12/10/2016
Dibromochloromethane
SM 6200C
< 0,50 pg/L
12/10/2016
Dibromomethane
SM 6200c
< 0,50 pg/L
12/10/2016
Dichlorodifluoromethane
SM 6200C
< 0.50 pg/L
12/10/2016
Ethylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
Hexachlorobutadiene
SM 6200c
< 0.50 pg/L
12/10/2016
Isopropylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
M+P Xylene
SM 6200C
< 1.00 pg/L
12/10/2016
Methylene chloride
SM 6200C
< 0.50 pg/L
12/10/2016
Naphthalene
SM 62000
< 0.50 pg/L
12/10/2016
n-Butylbenzene
SM 6200C
< 0.50 pg1L
12/10/2016
n-Propylbenzene
SM6200C
< 0.50 pg/L
12/10/2016
ortho-Xylene
SM 6200c
< 0.50 pg/L
12/10/2016
p-Isopropyltoluene
SM 6200C
< 0.50 pg/L
12/10/2016
sec-Butylbenzene
SM 6200C
< 0,50 pg/L
12/10/2016
Styrene
SM 62000
< 0.50 pg/L
12/10/2016
tert-Butylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
Tetrachloroethene
SM 62000
< 0.50 pg/L
12/10/2016
Toluene
SM 6200c
< 0.50 pg/L
12/10/2016
Report #:: 2016-17367
Page 32 of 51

finvironmental Chemists, Inc.
p 6602 Windrrtill Way, Willilirigt(:)n, j\1C. 28405 ® 910.3 )92.02' Lab s 910.392.=1424 Fax
/10 Bow-sertown Road, % anteo, NC: 27954 s 252.173.5702 Lab/Fax
255-A Wilmington I Iil;hway, Jacksonville, NC: 28540 o 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS inEi�<ir en ironr,zc iltalcllcnust .cont
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Trans- 1,2-Dichloroethene SM 6200C
< 0.50 pg/L
12/10/2016
Trans-1,3-dichloropropene SM 6200c
< 0.50 pg/L
12/10/2016
Trichloroethene SM 6200c
< 0.50 pg/L
12/10/2016
Trichlorofluoromethane SM,62000
< 0.50 pg/L
12/10/2016
Vinyl chloride SM 6200c
< 0.50 pg/L
12/10/2016
Nitrate Nitrogen (Cale)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/05/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/07/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2016
Report #:: 2016-17367 Page 33 of 51

ANALYTICAL & CONSULTING CHEMISTS
6602 WiTidmill Way, Wilmington, itiC 28405 e 910.392.0223 Lab e 910.3-92,44244 Fax
7.10 Boc1 serto«-n Road, Marlteo, TNC 27954 m 252.473.5702 Lab/Fax
255-At4'ilnungtinlFl:iz;hway; Jacksonville, * 910.347.5843 Lab/lax
int'o{izeuvironmentalctaemists.cona
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-41897 Site: MW -5 12/4/2016 12:51 PM Water JP
Test Method Results Date Analyzed
Sulfate
EPA 300.0
<5 mg/L
12/08/2016
Total Organic Carbon (TOC)
SM 5310 a
<0.5 mg/L
12/08/2016
1,1,1,2 -Tetrachloroethane
SM 62000
< 0.50 pg/L
12/10/2016
1,1,1 -Trichloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,1,2,2 -Tetrachloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,1,2 -Trichloroethane
SM 6200c
< 0.50 pg/L
12/10/2016
1,1-Dichloroethane
SM 62000
< 0.50 pg/L
12/10/2016
1,1-Dichloroethene
SM 6200C
< 0.50 pg/L
12/10/2016
1,1-Dichloropropene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,3-Trichlorobenzene
Stv162000
< 0.50 pg/L
12/10/2016
1,2,3-Trichloropropane
SM 6200C
< 0.50 pg/L
12/10/2016
1,2,4-Trichlorobenzene
SM 6200c
< 0.50 pg/L
12/10/2016
1,2,4-Trimethylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2-Dibromo-3-Chloropropane
SM 62000
< 0.50 pg/L
12/1012016
1,2-Dibromoethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,2 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,2-Dichloroethane
SM 6200C
< 0.50 pg/L
12/10/2016
1,2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/10/2016
1,3,5-Trimethylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
1,3 -Dichlorobenzene
SM 52000
< 0.50 pg/L
12/10/2016
1,3-Dichloropropane
SM6200C
< 0.50 pg/L
12/10/2016
1,4 -Dichlorobenzene
SM 6200C
< 0.50 pg1L
12/10/2016
2,2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/10/2016
2-Chlorotoluene
SM 6200C
< 0.50 pg/L
12/10/2016
4-Chlorotoluene
SM 6200C
< 0.50 pg/L
12/10/2016
Benzene
SM 6200C
< 0.50 pg/L
12/10/2016
Report #:: 2016-17367 Page 34 of 51

City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer P© #:
Jacksonville NC
28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SPA 6200C
< 0.50 pg/L
1211012016
Bromochloromethane
SM 6200c
< 0.50 pg/L
12/10/2016
Bromodichloromethane
SM 6200c
< 0.50 pg/L
12/10/2016
Bromoform
SM 6200c
< 0.50 pg/L
12/10/2016
Bromomethane
SM 6200c
< 0.50 pg/L
12/10/2016
Carbon tetrachloride
SM 62000
< 0.50 pg/L
12/10/2016
Chlorobenzene
SM 62000
< 0.50 pg/L
12/10/2016
Chloroethane
SNI 6200c
< 0.50 pg/L
12/10/2016
Chloroform
SM 6200C
< 0.50 pg/L
12/10/2016
Chloromethane
SM 6200c
< 0.50 pg/L
1 2/1 01201 6
cis-1,2-Dichloroethene
SM 6200C
< 0.50 pg/L
12/10/2016
cis-1,3-Dichloropropene
SM 6200C
< 0.50 pg/L
12/10/2016
Dibromochloromethane
SM 62000
< 0.50 pg/L
12/10/2016
Dibromomethane
SM 6200C
< 0.50 pg/L
12/10/2016
Dichlorodifluoromethane
SM 6200C
< 0.50 pg/L
12/10/2016
Ethylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Hexachlorobutadiene
SM 6200C
< 0.50 pg/L
12/10/2016
Isopropylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
M+P Xylene
SM 6200C
< 1.00 pg/L
12/10/2016
Methylene chloride
SM 6200c
< 0.50 pg/L
12/10/2016
Naphthalene
SM 62000
< 0.50 pg/L
12/10/2016
n-Butylbenzene
SM 6200c
< 0.50 pg/L
12/10/2016
n-Propylbenzene
SM 6200C
< 0.50 pg/L
12/10/2016
ortho-Xylene
SM 6200c
< 0.50 pg/L
12/10/2016
p-Isopropyltoluene
SM 62000
< 0.50 pg/L
12/10/2016
sec-Butylbenzene
SM 62000
< 0.50 jig/L
12/10/2016
Styrene
SM 62000
< 0.50 pg/L
12/10/2016
tert-Butylbenzene
SM 62000
< 0.50 pg/L
12/10/2016
Tetrachloroethene
SM 62000
< 0.50 pg/L
12/10/2016
Toluene
SIA 62000
< 0.50 pg/L
12110/2016
Report Mt 2016-17367
Page 35 of 51

ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill t'r'ay, Wilmington, NC 28405 a 9:10.392.0223 L,ab $ 9 0.392.-1-124 11'ax
710 Bowscrtowii Road, Manteca, INC: r/951 e 252.473.5702 Lab!'RIX
255-FiWihii igtc>z1:Hi=;l";ti4ay, Jacksonville, NC 28540 + 91Q.347.5843 Lab/ Fax
info iietivironlnent:alchen-ist:s.c:om
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer P© #:
Jacksonville NC
28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene
SM 6200C
< 0.50 pg/L
12/10/2016
Trans- 1,3-dichloropropene
SM 62000
< 0,50 pg/L
12/10/2016
Trichloroethene
SM 62000
< 0.50 pg/L
12/10/2016
Trichlorofluoromethane
SM 62000
< 0.50 pg/L
12/10/2016
Vinyl chloride
Sint 6200C
< 0.50 pg/L
12/1012016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2
< 0.02 mg/L
12/05/2016
Nitrate+Nitrite-Nitrogen
EPA 353.2
< 0.02 mg/L
12/07/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2016
Report #:: 2016-17367 Page 36 of 51

Environmental fists,
6602 Windmill Way, Wilmington, NC 28405 ti 910.392.02231 -ab * 910.392.4424 Fax
710 Bow sertown Road, Manteo, .NC 27954 ® 252.=173.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.58431..ab/Fax
ir�!'�!ii�environfnent<alrhemisCs.cc�m
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-41898 Site: MW -6 12/4/2016 11:42 AM Water JP
Test Method Results Date Analyzed
Sulfate
EPA 300.0
38 mg/L
12/08/2016
Total Organic Carbon (TOC)
SM 5310 B
8.0 mg/L
12/08/2016
1,1,1,2 -Tetrachloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,1,1 -Trichloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,1,2,2 -Tetrachloroethane
SM 6200C
<0.50pg/L
12/11/2016
1,1,2 -Trichloroethane
SM 6200C
< 0.50 pg/L
12111/2016.
1,1-Dichloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,1-Dichloroethene
SM 6200C
< 0.50 pg/L
12/1 1 /2016
1,1-Dichloropropene
SM 6200C
< 0.50 pg/L
12/11/ 2016
1,2,3-Trichlorobenzene
SNI 6200C
<.0.50 pg/L
12/11/2016
1,2,3-Trichloropropane
SM 6200C
< 0.50 pg/L
12/11/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2,4-Trimethylbenzene
Sri 6200C
< 0.50 pg/L
12/11/2016
1,2-Dibromo-3-Chloropropane
SP116200C
< 0.50 pg/L
12/11/2016
1,2-Dibromoethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,2 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2-Dichloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/11/2016
1,3,5-Trimethylbenzene
SNI 6200C
< 0,50 pg/L
12/11/2016
1,3 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,3-Dichloropropane
SM 6200C
< 0.50 pg/L
12/11/2016
1,4 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
2, 2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/11/2016
2-Chlorotoluene
SM 6200C
< 0.50 pg/L
12/11/2016
4-Chlorotoluene
SM 6200C
< 0.50 pg/L
12/11/2016
Benzene
SM 6200C
< 0.50 pg/L
12/11/2016
Report k. 2016-17367 Page 37 of 51

R
1
fj-
'pis �a
ANALYTICAL & CONSULTING CHEMISTS
6602 Windmill V%Iay, Wilmington, NC: 28405 , 910.392.0223 Lab * 91.0.392,442: Fax
710 Bowsertown Road, Nlanteo, itiC 279,54 2K.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, i11t,1 C 2N5 i? 910.3 1..5843 LablE,ax
info!it cnviratment�.alchemists.ci:lm
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer 1D: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
Bromochloromethane
SM 6200c
< 0.50 jig/L
12/11/2016
Bromodichloromethane
SM 6200C
< 0.50 pg/L
12/11/2016
Bromoform
SM 6200C
< 0.50 pg/L
12/11/2016
Bromomethane
SM 6200C
< 0.50 pglL
12/11/2016
Carbon tetrachloride
SM 6200C
< 0.50 pg/L
12/11/2016
Chlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
Chloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
Chloroform
SM 6200C
< 0.50 pg/L
12/11/2016
Chloromethane
SM 62000
< 0.50 pg/L
12/11/2016
cis-1,2-Dichloroethene
SM 6200C
< 0.50 pg/L
12/11/2016
cis -1, 3-Dichloropropene
SM 62000
< 0.50 pg/L
12/11/2016
Dibromochloromethane
SM 62000
< 0.50 pg/L
12/11/2016
Dibromomethane
SM 62000
< 0.50 pg/L
12/11 /201 6
Dichlorodifluoromethane
SM 6200c
< 0.50 pg/L
12/11/2016
Ethylbenzene
SM 62000
< 0.50 pg/L
12/11/2016
Hexachlorobutadiene
SM 6200c
< 0.50 pg/L
12/11/2016
Isopropylbenzene
SM6200C
< 0.50 pg/L
12/11/2016
M+P Xylene
SM 6200C
< 1.00 pg/L
12/11/2016
Methylene chloride
SM 6200c
< 0.50 pg/L
12/11/2016
Naphthalene
SM 63200C
< 0.50 pg/L
12/11/2016
n-Butylbenzene
SM 6200c
< 0.50 pg/L
12/11/2016
n-Propylbenzene
SM 6200c
< 0.50 pg/L
12/11/2016
ortho-Xylene
SM 6200C
< 0.50 pg/L
12/11/2016
p-Isopropyltoluene
SM 6200c
< 0.50 pg/L
12/11/2016
sec-Butylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
Styrene
SM 6200C
< 0.50 pg/L
12/11/2016
tert-B utyl benzene
SM 6200c
< 0.50 pg/L
12/11/2016
Tetrachloroethene
SM 6200c
< 0.50 pg/L
12/1112016
Toluene
SM 6200c
< 0.50 pg/L
12/11/2016
Report #:: 2016-17367
Page 38 of 51

6602 Windmill IMiy, Wilmington, NC 28405 R 910.392,11223 Lab d 91.0.392.4424 Fax
710 Bowserto n Rand, Manteo, \C 27954 a 2.52.473. 702 Lab/Fax
255-A C' ilmingtcm Fligh way, Jacksonville, NC; 28540 - 91.0.3475843 I..:ab/Fax
141fa4�?'ct1Y1EC�t1tt1C11titlChc'tI11StS.Ct:)ffl
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Trans- l ,2-Dichloroethene SM 62000
< 0.50 pg/L
12/11/2016
Trans-1,3-dichloropropene SM,3200C
< 0.50 pg/L
12/11/2016
Trichloroethene SM 6200c
< 0.50 pq/L
12/11/2016
Trichlorofluoromethane SM 6200C
< 0.50 pg/L
12/11/2016
Vinyl chloride SM 6200c
< 0.50 pg/L
12/11/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 0.09 mg/L 12/05/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/07/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2016
r
Report #:: 2016-17367 Page 39 of 51

Environmental
Chemists,
Q 6 q 66t12 Windt -hill Way, Wilmin ton, NC 910.392,0223 Lab a 910.392.4424 Fax
710 Bowsertown Road, iMantec), NC 27954 e 252.4:73.5702 Lab/ Fax
255 -A Wilmington I fighway, Jacksonville, NC 2854:0 o 910.:x-47.1. 43 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS inik7.a enviroametitztlc:llemists.c(:)n1
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-41899 Site: MW -7 12/4/2016 10:50 AM Water JP
Test Method - Results Date Analyzed
Sulfate
EPA 300.0
26 mg/L
12/08/2016
Total Organic Carbon (TOC)
SM 5310 B
4.6 mg/L
12108/2016
1,1,1,2 -Tetrachloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,1,1 -Trichloroethane
SM 62000
< 0.50 pg/L
12/11/2016
1,1,2,2 -Tetrachloroethane
SM 52000
< 0.50 pg/L
12/11/2016
1,1,2 -Trichloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,1-Dichloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1, 1 -Dichloroethene
SM 6200C
< 0.50 pg/L
12111/2016
1, 1 -Dichloropropene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2,3-Trichlorobenzene
SM (3200C
< 0.50 pg/L
12/11/2016
1,2,3-Trichloropropane
SM 6200c
< 0.50 pg/L
12/11/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2,4-Trimethylbenzene
SM 6200c
< 0.50 pg/L
12/11/2016
1,2-Dibromo-3-Chloropropane
SM 6200c
<0.50pg/L
12/11/2016
1,2-Dibromoethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,2 -Dichlorobenzene
SM 62000
< 0.50 pg/L
12/11/2016
1,2-Dichloroethane
SM 6200c
< 0.50 pg/L
12/11/2016
1,2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/11/2016
1,3,5-Trimethylbenzene
SM 6200c
< 0.50 pg/L
12/11/2016
1,3 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/11/2016
1,3-Dichloropropane
SM 6200c
< 0.50 pg/L
12/11/2016
1,4 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12111/2016
2,2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/11/2016
2-Chlorotoluene
SM 6200C
< 0.50 pg/L
12/11/2016
4-Chlorotoluene
SM 6200C
< 0.50 pg/L
12/11/2016
Benzene
SM 6200C
< 0.50 pg/L
12/11/2016
Report #:: 2016-17367 Page 40 of 51

Envffi
ronmental Chemists, Inc.
6602 Windmill V%Iay, Wilmington, NC 28405 - 9:10.392.0223 Lab a 9.10.392.4=124 Fax
710 Bowserwwn Road, Ma.nteo, NC:. 27954 - 252.4,73.5702 Lab/Fax
2;:15-A Wilmington Highway, Jacksonville, NC, 28540 4 91.0 ,347" 5843 Lab/ :F Fax
itil'o,, l»nvii•onmeiitalclaernists.c�:)saI
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention:. Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 62000
< 0.50 pg/L
12/11/2016
Bromochloromethane
SM 62000
< 0.50 pg/L
12/11/2016
Bromodichloromethane
SM 62000
< 0.50 pg/L
12/11/2016
Bromoform
SM 62000
< 0.50 pg/L
12/11/2016
Bromomethane
SM 62000
< 0.50 pg/L
12/11/2016
Carbon tetrachloride
Sri 62000
< 0.50 pg/L
12/11/2016
Chlorobenzene
SM 62000
< 0.50 pg/L
12/11/2016
Chloroethane
SM 62000
< 0.50 pg/L
12/1112016
Chloroform
SM 6200C
< 0,50 pg/L
12/11/2016
Chloromethane
SM 62000
< 0.50 pg/L
12/11/2016
cis-1,2-Dichloroethene
SM 62000
< 0.50 pg/L
12/11/2016
cis-1,3-Dichloropropene
SM 62000
<-0.50 pg/L
12/11/2016
Dibromochloromethane
SM 6200C
< 0.50 pg/L
12/11/2016
Dibromomethane
SM 6200C
< 0.50 pg/L
12/11/2016
Dichlorodifluoromethane
SM 62000
< 0.50 pg/L
12/11/2016
Ethylbenzene
SAA 6200C
< 0.50 pg/L
12/11/2016
Nexachlorobutadiene
SM 62000
< 0.50 pg/L
12/11/2016. .
Isopropylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
M+P Xylene
SM 6200C
< 1.00 pg/L
12/1.1/2016
Methylene chloride
SM 6200C
< 0.50 pg1L
12/11/2016
Naphthalene
SM 62000
< 0,50 pg/L
12/11/2016
n-Butylbenzene
SM 62000
< 0.50 pg/L
12/11/2016
n-Propylbenzene
SM 62000
< 0.50 pg/L
12111/2016
ortho-Xylene
SM 6200C
< 0.50 pg/L
12/11/2016
p-Isopropyltoluene
SM 62000
< 0.50 pg/L
12/11/2016
sec-Butylbenzene
SM 62000
< 0.50 pg/L
12/11/2016
Styrene
SM 62000
< 0.50 pg/L
12/11/2016
tert-Butylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
Tetrachloroethene
SM 6200C
< 0.50 pg/L
12/11/2016
Toluene
SM 6200C
< 0.50 pg/L
12/11/2016
Report i;:: 2016-17367
Page 41 of 51

City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Trans- l ,2-Dichloroethene SM 6200c
< 0.50 pg/L
12111/2016
Trans-1,3-dichloropropene SM 62000
< 0.50 pg/L
1.2/11/2016
Trichloroethene Sri 62000
< 0.50 pg/L
12/11/2016
Trichlorofluoromethane SM 6200C
< 0.50 pg/L
12/11/2016
Vinyl chloride SM 6200C
< 0.50 pg/L
12/11/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 363.2 < 0.02 mg/L 12/05/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/07/2016
Nitrate Nitrogen subtraction Method <0.02 mg/L 12115/2016
Report #:: 2016.17367 Page 42 of 51

Environmental
Chemists,
6602 Windmill tVa , Wilmington, NC 28 405 e 9.10.392.0223 Lab w 910.392.4424 Fax
7.10 Bowsertown Road, Mwiteo, NC.. 27954 e 252.473.5702 Lab 1"ax
255-A Wilmington f-h-liway, Jacksonville, xIC:: 28540 o 91.0.3,17.5843 Lab/Fax
irllbt ellviroll rnentalchefnists.com
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-41900 Site: MW -11 12/4/2016 2:45 PM Water JP
Test Method Results Date Analyzed
Sulfate
EPA 300.0
<5 mg/L
12/08/2016
Total Organic Carbon (TOC)
SM 5310 B
1.3 mg/L
12/08/2016
1,1,1,2 -Tetrachloroethane
SM 6200C
<0.50pg/L
12/11/2016
1,1,1 -Trichloroethane
SM 62000
< 0.50 pg/L
12/11/2016
1,1,2,2 -Tetrachloroethane
SM 6200C
<0.50pg/L
12/11/2016
1,1, 2 -Trichloroethane
SM 6200c
< 0.50 pg/L
12111/2016
1,1-Dichloroethane
SM 6200c
< 0.50 pg/L
12/11/2016
1,1-Dichloroethene
sttA6200C
< 0.50 pg/L
12/11/2016
1,1-Dichloropropene
SM 62000
< 0.50 pg/L
12/11/2016
1.2,3-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2,3-Trichloropropane
srn 6200c
< 0.50 pg/L
12/11/2016
1,2.4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2,4-Trimethylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2-Dibromo-3-Chloropropane
SPA6200C
< 0.50 pg/L
12/11/2016
1,2-Dibromoethane
S%16200c
< 0.50 pg/L
12/11/2016
1,2 -Dichlorobenzene
SM 62400
< 0.50 pg/L
12/11/2016
1,2-Dichloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1, 2-Dichloropropane
SN4 6200C
< 0.50 pg/L
12/11/2016
1,3,5-Trimethylbenzene
SM 6200C
< 0.50 pg/L
12111/2016
1,3 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,3-Dichloropropane
SM 6200C
< 0.50 pg/L
12/11/2016
1,4 -Dichlorobenzene
SM 0200C
< 0.50 pg/L
12/11/2016
2,2-Dichloropropane
SM 62000
< 0.50 pg/L
12/11/2016
2-Chlorotoluene
SM 6200C
< 0.50 pg/L
12/11/2016
4-Chlorotoluene
Ski 6200C
< 0.50 pg/L
12/11/2016
Benzene
SM 6200c
< 0.50 pg/L
12/11/2016
Report #:: 2015-17367 Page 43 of 51

City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 6200C
< 0.50 pglL
12/11/2016
Bromochloromethane
SM 62000
< 0,.50 pg/L
12/11/2016
Bromodichloromethane
SM 6200c
< 0.50 pg/L
12/11/2016
Bromoform
SM 6200c
<-0.50 pg/L
12111/2016
Bromomethane
SM 6200C
< 0.50 pg/L
12/11/2016
Carbon tetrachloride
SM 62000
< 0.50 pg/L
12/11/2016
Chlorobenzene
SM 6200c
< 0.50 pg/L
12/11/2016
Chloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
Chloroform
SM 62000
< 0.50 pg/L
12/11/2016
Chloromethane
SM 6200c
< 0.50 pg/L
12/11/2016
cis-1,2-Dichloroethene
SM 6200c
< 0.50 pg/L
12/11/2016
cis-1,3-Dichloropropene
SM 6,2000
< 0.50 pg/L
12/11/2016
Dibromochloromethane
SM 6200c_
< 0.50 pg/L
12/11/2016
Dibromomethane
SM 6200c
< 0.50 pg/L
12/11/2016
Dichlorodifluoromethane
SM 6200c
< 0.50 pg/L
12/11/2016
Ethylbenzene
SM 6200c
< 0.50 pg/L
12/11/2016
Hexachlorobutadiene
SM6200C
< 0.50 pg/L
12/1112016
Isopropylbenzene
SM 6200c
< 0.50 pg/L
12/11/2016
M+P Xylene
SM 6200c
< 1.00 pg/L
12/11/2016
Methylene chloride
SM 6200c
< 0.50 pg/L
12/11/2016
Naphthalene
SM 6200C
< 0.50 pg/L
12/11/2016
n-Butylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
n-Propylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
ortho-Xylene
SM 6200C
< 0.50 pg/L
12/11/2016
p-Isopropyltoluene
6,M 6200c
1.74 pg/L
12/11/2016
sec -B utyl benzene
SM 6200C
< 0.50 pg/L
12/11/2016
Styrene
SM 6200C
< 0.50 pg/L
12/11/2016
tert-Butylbenzene
SM 6200c
< 0.50 pg/L
12/1112016
Tetrachloroethene
SM 6200c
< 0.50 pg/L
12/11/2016
Toluene
SM 6200c
< 0.50 pg/L
12/11/2016
Report #:: 2016-17367
Page 44 of 51

6602 Windmill Way, Wilmington, NC. 9-8405 o 910.302.022.3 Lab « 910.392.4424: Fax
710 TRo sertown Road, klanteo, :NC 27954 a 252.473.5702 Lab/1-ax
255-A Wilmington Highway, Jacksonville, NC 28540 e 9.10.347.5843 Lab/Fax
iitfo!aenvironn7eut<t(eltcmists.conr
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC 28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Trans-1,2-Dichloroethene SM 6200C
< 0.50 pg/L
12/11/2016
Trans-1,3-dichloropropene SM 6200C
< 0.50 pg/L
12/11/2016
Trichloroethene San 6200c
< 0.50 pg/L
12/11/2016
Trichlorofluoromethane San 6200c
< 0.50 pg/L
12/11/2016
Vinyl chloride SM 6200C
< 0.50 pg/L
12/11/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 12/05/20.16
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 12/07/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/15/2016
Report #:: 2016-17367 Page 45 of 51

0
ANALYTICAL & CONSULTING CHEMISTS
t '@ ',� �� . F Chemists,
f i5 x tom..
a" Y.l A � g t
6602 Windmill VVay, Wilmington, NC. 28405 $ 910.392.0223 Lab a 910,392.4424 Fax
T10 Bowsertown Road, Manteo, N -C 279.,54 a 252.473.570'_ Lab/ Fax
255-A VVilminnton Highway Jacksonville, NC 2854:0 s 910.347.5843 Lab/ Fax
in f'i)ti��c^nvirun ixieu t,ticlienr ists.con1
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-41901 Site: MW -12 12/4/2016 12:00 PM Water JP
Test Method Results Date Analyzed
Sulfate
EPA 300.0
15 mg/L
12/08/2016
Total Organic Carbon (TOC)
SM 5310 B
44.3 mg/L
12/08/2016
1,1,1, 2 -Tetrachloroethane
SM 62000
< 0.50 tag/L
12/11/2016
1,1,1 -Trichloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,1,2,2 -Tetrachloroethane
SM 6200C
< 0.50 fag/L
12/11/2016
1,1,2 -Trichloroethane
SM 6200C
< 0.50 tag/L
12/11/2016
1,1-Dichloroethane
SM 6200C
< 0.50 tag/L
12/11/2016
1, 1 -Dichloroethene
SM 62000
< 0.50 tag/L
12/11/2016
1,1-Dichloropropene
SM 62000
< 0.50 tag/L
12/11/2016
1,2,3-Trichlorobenzene
SM 6200C
< 0.50 tag/L
12/11/2016
1;2,3-Trichloropropane
SPA 6200C
< 0.50 tag/L
12/11/2016
1,2,4-Trichlorobenzene
SM 62000
< 0.50 lag/L
12/11/2016
1,2,4-Trimethylbenzene
SM 6200C
< 0.50 tag/L
12/11/2016
1,2-Dibromo-3-Chloropropane
SM 6200C
< 0.50 tag/L
12111/2016
1,2-Dibromoethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,2 -Dichlorobenzene
SM 6200C
< 0.50 tag/L
12/11/2016
1, 2-Dichloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,2-Dichloropropane
SM 62000
< 0.50 tag/L
12/11/2016
1,3,5-Trimethylbenzene
SM 6200C
< 0.50 tag/L
12/11/2016
1,3 -Dichlorobenzene
SM 6200C
< 0.50 tag/L
12/11/2016
1,3-Dichloropropane
SM C200C
< 0.50 tag/L
12/11/2016
1,4 -Dichlorobenzene
SM 6200C
< 0.50 tag/L
12/11/2016
2,2-Dichloropropane
SM 62000
< 0.50 tag/L
12/11/2016
2-Chlorotoluene
SM 62000
< 0.50 tag/L
12/11/2016
4-Chlorotoluene
Srv16200C
< 0.50 tag/L
12/11/2016
Benzene
SM 6200c
< 0.50 tag/L
12/11/2016
Report #:: 2016-17367 Page 46 of 51

I
Environmental a ig I.
6602 t1 hidnlill VVay, Wilmin. ton, NC 28405 , 910.392.0223 Lab & 911).392.4424 Pax
710 Bowsertoti4•n Road, Manteo, NC 27954 9 152.43.5702 Lab/ Fax
255-A Wilmington Highway, jacksonville, NC.. 28540 o 91.0.347.5843 Lab/Fax
it1f0�CtCtlYtCt)k1TilCtlfe11i;11C1T11St5.COn1
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 62000
< 0.50 pg/L
12/11/2016
Bromochloromethane
SM 6200C
< 0.50 pg/L
12/11/2016
Bromodichloromethane
SM 62000
< 0.50 pg/L
12/11/2016
Bromoform
SM 62000
< 0.50 pg/L
12/11/2016
Bromomethane
SM 6200C
< 0.50 pg/L
12/11/2016
Carbon tetrachloride
SM 62000
< 0.50 pg/L
12/11/2016
Chlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
Chloroethane
SM 620000
< 0.50 pg/L
12/11/2016
Chloroform
SM 62000
< 0.50 pg/L
12/11/2016
Chloromethane
SM 6200C
< 0.50 pg/L
12/11/2016
cis-1,2-Dichloroethene
SM 62000
< 0.50 pg/L
12/11/2016
cis-1,3-Dichloropropene
SM 62000
< 0.50 pg/L
12/11/2016..
Dibromochloromethane
SM 6200C
< 0.50 pg/L
12/11/2016
Dibromomethane
SM 6200C
< 0.50 pg/L
12/11/2016
Dichlorodifluoromethane
SM 62000
< 0.50 pg/L
12/11/2016
Ethylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
Hexachlorobutadiene
SM 62000
< 0.50 pg/L
12/11/2016
Isopropylbenzene
SM 62000
< 0.50 pg/L
12/11/2016
M+P Xylene
SM 62000
< 1.00 pg/L
12/11/2016
Methylene chloride
SM 62000
< 0.50 pg/L
12/11/2016
Naphthalene
SM 62000
< 0.50 pg/L
12/11/2016
n-Butylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
n-Propylbenzene
SM 62000
< 0.50 pg/L
12/11/2016
ortho-Xylene
SM 62000
< 0.50 pg/L
12/11/2016
p-Isopropyltoluene
SM 6200C
< 0.50 pg/L
12/11/2016
sec-Butylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
Styrene
SM 62000
< 0.50 pg/L
12/11/2016
te rt -B utyl benzene
SM 6200C
< 0.50 pg/L
12111/2016
Tetrachloroethene
SM 62000
< 0.50 pg/L
12/11/2016
Toluene
SM 62000
< 0.50 pg/L
12/11/2016
Repert #:; 2016-17367
Page 47 of 51

nviron.me tal Chemists, Inc. -
660,2
c:660,2 Windmill V 'ay, VVilntington, IAC 28 05 s 910.392.0223 Lab o 910.392.4424 Fax
710 Bowsertown Road, llanteo, NC. 27954 a 252.473.5702 Lab; Fax
255-A VVilminntc>n 1-lighway, Jacksonville, NC 28540 ® 91.0.347.5843 Lab/Fax.
info i%em irc:mnlentatellenlists.com
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Trans- 1,2-Dichloroethene
SM 6200C
< 0.50 pg/L
12/1112016
Trans- 1,3-dichloropropene
SM 6200C
< 0.50 pg/L
12/11/2016
Trichloroethene
SM 6200C
< 0.50 pg/L
12/11/2016
Trichlorofluoromethane
SM 6200C
< 0.50 pg/L
12/11/2016
Vinyl chloride
SM 6200C
< 0.50 pg/L
12/11/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2
0.08 mg/L
12/05/2016
Nitrate+Nitrite-Nitrogen
EPA 353.2
< 0.02 mg/L
12/07/2016
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
- 12115/2016
Report #:: 2016-17367 Page 48 of 51

Environmental
Chemists,
6602 Windmill k;Vay, Wilmington, vC. 2840i o 910.392,0223 Lab * 910.392.4424 F,,ax
710 BoLtisertown Road, Nla.n.teo, NC 27954 - 252.=173.5702 Lab/Fax
255,A Wilmington Highway, Jackso.1 ville, `,iC:28540 * 51.0.347.5843 l..:ab/Fax
inlor�i'et vironmen talcllernists.com
City of Jacksonville Date of Report: Dec 15, 2016
Post Office Box 128 Customer PO #:
Jacksonville NC 28541 Customer ID: 08110015
Attention: Jill Puff Report #: 2016-17367
Project ID: Monitoring Wells
Lab ID Sample ID: Collect DatetTime Matrix Sampled by
16-41902 Site: MW -15 12/4/2016 9:37 AM Water JP
Test Method Results Date Analyzed
Sulfate
EPA 300.0
<5 mg/L
12/08/2016
Total Organic Carbon (TOC)
SM 5310 B
0.7 mg/L
12108/2016
1,1,1,2 -Tetrachloroethane
StA6200c
<0.50pg/L
12/11/2016
1,1,1 -Trichloroethane
SM 62000
< 0.50 pg/L
12/11/2016
1,1,2,2 -Tetrachloroethane
SM 6200C
<0.50pg/L
12/11/2016
1,1,2 -Trichloroethane
SM 62000
< 0.50 pg/L
12/11/2016
1,1-Dichloroethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,1-Dichloroethene
SM 6200c
< 0.50 pg/L
12/11/2016
1,1-Dichloropropene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2,3-Trichlorobenzene
SM 6200c
< 0.50 pg/L
12/11/2016
1,2,3-1-richloropropane
SM 6200C
< 0.50 pg/L
12/11/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2,4-Trimethylbenzene
SM 6200C
< 0.50 pg/L
12/11/2016
1,2-Dibromo-3-Chloropropane
SN46200C
< 0.50 pg/L
12/1112016
1,2-Dibromoethane
SM 6200C
< 0.50 pg/L
12/11/2016
1,2 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/11/2016
1,2-Dichloroethane
SM 6200c
< 0.50 pg/L
12/11/2016
1,2-Dichloropropane
SM 6200C
< 0.50 pg/L
12/11/2016
1, 3, 5-Trimethylbenzene
SM 62000
< 0.50 pg/L
12/11/2016
1,3 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/11/2016
1,3-Dichloropropane
SrA 62000
< 0.50 pg/L
12/11/2016
1,4 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
12/11/2016
2,2-Dichloropropane
SM6200C
< 0.50 pg/L
12/11/2016
2-Chlorotoluene
SM 6200c
< 0.50 pg/L
12/11/2016
4-Chlorotoluene
sM 62ooc
< 0.50 pg/L
12/11/2016
Benzene
SM 6200c
< 0,50 pg/L
12/11/2016
Report #:: 2016-17367 Page 49 of 51

n
66021, ,,indmill V ay, Wilmington, NC 28405 - 91(1.392.0223 Lab a 910.392.44-24 Fax
71.0 Bowsertown Road.. Nianteo, NIC27954 m 252.473.5702 I..ab/ Fax
255-A VNrilmingft)n Highway, Jacksonville, NC 28540 * 910.347.5843 Lab; l pix
inCniu environmentalchemists.com
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO ##:
Jacksonville NC
28541
Customer ID: 08110015
Attention: Jill Puff
Report #: 2016-17367
Project ID: Monitoring Wells
Bromobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
Bromochloromethane
sfvt 62000
< 0.50 pg/L
12/11/2016
Bromodichloromethane
SM 6200C
< 0.50 pg/L
12/11/2016
Bromoform
SM 6200c
< 0.50 pg/L
12111/2016
Bromomethane
SM 6200C
< 0:50 pg/L
12/11/2016
Carbon tetrachloride
SM 6200C
< 0.50 pg/L
12/11/2016
Chlorobenzene
SM 6200C
< 0.50 pg/L
12/11/2016
Chloroethane
SM 6200C
< 0.50 pg/L
12111/2016
Chloroform
SM 6200C
< 0.50 pg/L
12/11/2016
Chloromethane
SM 6200C
< 0.50 pg/L
12/11/2016
cis-1,2-Dichloroethene
SNA 6200C
< 0.50 pg/L
12/11/2016
cis-1,3-Dichloropropene
SM 620oc
< 0.50 pg/L
12/11/2016
Dibromochloromethane
SM 6200c
< 0.50 pg/L
12/1112016
Dibromomethane
SM 6200C
< 0.50 pg/L
12/11/2016
Dichlorodifluoromethane
SM 6200C
< 0.50 pg/L
12/11/2016
Ethylbenzene
SM 6200c
< 0,50 pg/L
12/11/2016
Hexachlorobutadiene
SM 6200c
< 0.50 pg/L
12/11/2016
I sopropyl benzene
SM 6200c
< 0.50 pg/L
12/11/2016
M+P Xylene
SM6200C
< 1.00 pg/L
12/11/2016
Methylene chloride
SM 6200C
< 0.50 pg/L
12/11/2016
Naphthalene-
SM 6200C
< 0.50 pg/L
12/1112016
n-Butylbenzene
SM 6200c
< 0.50 pg/L
12/11/2016
n-Propylbenzene
SM 6200c
< 0.50 pg/L
12/11/2016
ortho-Xylene
SM 62000
< 0.50 pg/L
12/11/2016
p-Isopropyltoiuene
SM 6200C
< 0.50 pg/L
12/11/2016
sec -B utyl benzene
SM 6200C
< 0.50 pg/L
12/11/2016
Styrene
SM 6200c
< 0.50 pg/L
12/11/2016
tert-Butylbenzene
SM 6200c
< 0.50 pg/L
12/11/2016
Tetrachloroethene
SM 6200c
< 0.50 pg/L
12/11/2016
Toluene
SM 6200C
< 0.50 pg/L
12/11/2016
Report #:: 2416-17367
Page 60 of 51

6602 GVIndmill Way, Wilrningtorl, UC 28105 o 910.392.0223' Lab o 910.392,4424 Fax
710 Bowsertown Road, Manteo, N('27954 ® 252.413.: 702 Lab; Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.:14".5343 Lab%Fax
i nforri,,envimrimen ta(chemists,coin
City of Jacksonville
Date of Report: Dec 15, 2016
Post Office Box 128
Customer PO #:
Jacksonville NC
28541
Customer ID: 08110015
Attention: Jill Puff
-
Report #: 2016-17367
Project ID: Monitoring Wells
Trans-l,2-Dichloroethene
SM 62000
< 0.50 pg/L
12/11/2016
Trans- 1,3-dichloropropene
SM 62000
< 0.50 pg/L
12/11/2016
Trichloroethene
SM 6200C
< 0.50 pg/L
12/11/2016
Trichlorofluoromethane
SM 62000
< 0.50 pg/L
12/11/2016
Vinyl chloride
SM 6200C
< 0.50 pg/L
12/11/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2
< 0.02 mg/L
12/05/2016
Nitrate+Nitrite-Nitrogen
EPA 353.2
0.14 mg/L
12/07/2016
Nitrate Nitrogen Subtraction Method 0.14 mg/L 12/15/2016
Comment:
Reviewed by: ka 1 f
Raeort #:: 2016-17367 Page 51 of 51

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
CLIENT: City of Jacksonville
PROJECT NAME:
REPORT NO: -
ADDRESS: PO Box 128
CONTACT NAME:
PO NO: 150011
Jacksonville, NC 28540
REPORT TO: Jill 'Puff
PHONE/FAX:
ANALYSIS REQUESTED
COPY TO:
E-MAIL: "puff: ci.'acksonville.nc.us
Sampled By: .IP SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collectiony
E a
o- `o L'
o
w
.6
a `o
o n
" `
_o` 6
E
mLu
�
z
PRESERVATION
ANALYSIS REQUESTED
Date Time
Temp
w
o
Z
�
=
o
N
M
z
=
°¢
z
o
W
°
MW 8
12/5/2016 9:48
15.3
W
P
I
X
X
TOC, Sulfate, Nitrate, VOC( SM 6200 C)
G
G
MW 9
12/5/2016 9:24
17.7
W
P
>X
X
t
TOC, Sulfate, Nitrate, VOC SM 6200 C
G
G
MW10
12/5/2016 9:35
17.1
W
P
X
X
G
TOC, Sulfate, Nitrate, VOC( SM 6200 C)
G
G
MW13
12/5/2016 10:24
17.1
W
P
X
X
L
TOC, Sulfate, Nitrate, VOC( SM 6200 C
G
G
MW14
12/5/2016 10:14
15.5
W
P
X
X
TOC. Sulfate, Nitrate, VOC( SM 6200 C)
G
G�
P
G
G
P
G
G
P
G
I G
NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.2 ppm or loss) In the field at the timil of collection. See reverse for Instructions
Transfer
Roncgfthed By:
Date/Time
ffieceived By:
Date/Time
1.
2.
Temperature W R _ �r //Accepted:_ cted: Resample Re ue ted:__
Delivered By: Received By:-� Date: Time:
Comments: TURNAROUND:

Gamp • m
Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
CLIENT: City of Jacksonville
PROJECT NAME:
REPORT NO: NO
ADDRESS: PO Box 128
CONTACT NAME:
PO NO: 160011
Jacksonville, NC 28540
REPORT TO: Jill Puff
PHONE/FAX:
Date Time
COPY TO:
E-MAIL: 'puff: ci.'acksonville.nc.us
Sampled By: AP/JP
SAMPLE TYPE: I = Influent. E = Effluent. W = Well. ST = Stream. SO = Soil. SL = Sludae. Other:
Sample Identification
Collection
Q m
E F
�n
c a
E `o
d ig
C
c `o
0 a
�=
o am
c� E
O w
m M
J z
PRESERVATION
v
ANALYSIS REQUESTED
Date Time
Temp
-0-d-
T
'o
_
o
=
xo
z
o
W
o
MW 16
12/4/2016 14:26
13.6
W
P
Asho
X
X
TOC, Sulfate, Nitrate, VOC(SM 6200 C)
G
G
MW17
12/4/2016 16:23
16
W
P
i
t
X
X
z,
TOC, Sulfate, Nitrate, VOC(SM 6200 C)
G
G
P
G
G
P
G
G
P
G
G
NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.2 ppm or less) in the Feld at the time ofLqgllectlon. See reverse for instructions
Transfer
ReIi ished By: Date/Time a ived By: Date/Time
2.,
Tem w 7e - ed• d •,,� Accepted: V ed: Resample Re ue ted:
Delivered By• Received B Date: Time:
Comments: TUR A OUND:

° ENVIRONMENTAL CHEMISTS, INC 6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
Analytical & Consulting Chemists NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
CLIENT: City of Jacksonville
PROJECT NAME:
REPORT NO:�b 7
ADDRESS: PO Box 128
CONTACT NAME:
PO NO: 150011
Jacksonville, NC 28540
REPORT TO: Jill Puff
PHONE/FAX:
ANALYSIS REQUESTEDSample
COPY TO:
E-MAIL: 'puff: ci.'acksonville.nc.us
Samnlarl Rv- APLIP SAMPLE TYPE: I = Influent. E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Identification
Collection
m N•y
�E
un
o (D
o
U_'
CG0
o
C `
n
Jp
E
W
Z
PRESERVATION
ANALYSIS REQUESTEDSample
Date Time
Tem
=z
p
MW 1
12/4/2016 15:39
19.6
W
P
X
TOC, Sulfate, Nitrate, VOC( SM 6200 C)
G
G
MW2
12/4/2016 9:53
15.9
W
P
��
X
X
TOC, Sulfate, Nitrate, VOC( SM 6200C)
G
G
MW3
12/3/2014 13:06
15.5
W
P
X
X
4
TOC, Sulfate, Nitrate, VOC( SM 6200 C)
G
G
MW4
12/4/2016 8:51
15.8
W
P
�
X
X
TOC, Sulfate, Nitrate, VOC SM 6200 C)
G
G
MW5
12/4/2016 12:51
17.1
W
P
�+
X
X
(
TOC, Sulfate, Nitrate, VOC SM 6200 C
G
G
MW6
12/4/2016 11:42
15.9
W
P
460
X
X
`
TOC, Sulfate, Nitrate, VOC( SM 6200 C)
G
G
MW7
12/4/2016 10:50
16.5
W
P
X
X
�
TOC, Sulfate, Nitrate, VOC( SM 6200 C)
-G.
G
MW11
12/4/2016 14:45
20.2
W
P
���
X
X
Z
TOC, Sulfate, Nitrate, VOC( SM 6200 C)
G
G
MW12
12/4/2016 12:00
21.9
W
P
��d j
X
X
TOC, Sulfate, Nitrate, VOC(SM 6200 C)
G
G
MW15
12/4/2016 9:37
20.8
W
P
114
X
X
TOC, Sulfate, Nitrate, VOC( SM 6200 C)
G
G
NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.2 ppm or less) in the field at the Urge of collection. See reverse for instructions
Transfer
R I nquished By: te/Time
Received By:
Date/Time
LiU
ttry
It V1
2.
Temperatt
Delivered
Comment:
Re a ed:
Time:
JRNA OUND: