WQ0005173_Monitoring - 11-2016_20170117 (2)

M w3
Facility Narpe:_
Permit Name (if
Well Location/ Site Name:
°• SUBMIT FORM ON'YELLO"W PAPER ONLY
Print Clea dy,or Type
County, '
Telephone #: `
No. of Wells to be Sampled:
Well Identification Number (from Permit): , M _2S For Groundwater Treatment Systems
Well Depth: ' cI` .( a t` - - ft. Well Diameter _&r _ In. Check One:
Screened Interval:�. ft. to ft. 11Influent (98)
Depth to Water Level- 'ft. below measuring point. p Effluent (99)
Measuring Point is Are, It. above land surface.
Gallons of water Pum ailed before sampling: -
Feld analysis: . pH , Specific Conductan uMhos
Temp. °C, Odor& Appearance
PARAMETER (Samples for metals were collected
COD
mg/l
Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
(Notes Use MPN method for highly turbid samples)
Dissolved Solids: Total 2 /
mgA
pH (when analyzed
TOC 39
units
mg/I
Chloride /
mgA
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance uMhos
Total Ammonia
mg/l
TKN as N _ -
mg/l
PF-RMff EXPIRATION DATE.,
Non-Dar9e �w 1��_t?� UIC
NPDES
IYPEOF PERMITTED OPERATION BEING MONITORED
Lagoon Remediation: Infiltration Gallery
Spray Field Remediation:
_ Rotary Distributor Land Application of Sludge
Other.
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample collected 11 -23 -IL Date� sa��mple lyzed;�--�
Laboratory Name: rnrx�r,ox�tdJL_MSI. -JIf
Certification No. _ 34j(1Z0%.__
lered OYES
NO and field acidified
Nitrite (NO2) as N
mgA
Nitrate (NO3) as N
® mg/I
Phosphorus. Total as P mg/l
Orthophosphate
mg/l
Al - Aluminum
mgA
Ba - Barium
mg/l
Ca - Calcium
mg/l
Cd - Cadmium
-_ mg/I
Chromium: Total
mg/I
Cu - Copper
>-.-�m
(ron
T m
Hg - Mercury
--JAN- 17 2017 mg/l
K - Potassium
_ mg/l
Mg - Magnesium
mg/I
Mn - Manganese
YES NO)
Ni - Nickel mg/I
Pb - Lead, - mg/I
Zn - Zinc mgA
Ammonia Nitrogen _ mg/I
Other (Specify Compounds and Concentration Units)
ORGANICS: (GC,GC/MS,HPLC)
(Specify test and method #. A 1 b report.)
Report Attached? Yes (1) No (0)
VOC . method#-SLq J9:2 0 0
method # -
method #

Environmental Chemists, Inc.
IL envirochem 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
SM
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Fortin Contract Services
Post Office Box 4188
Emerald Isle NC 28594
Attention: Dan Fortin
Date of Report: Dec 08, 2016
Customer PO #:
Customer ID: 08100061
Report #: 2016-16935
Project ID: Cape Royal Dolphin MW
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
16-40880 Site: MW -3
11/23/2016 8:35 AM Water Client
Test
Method
Results
Date Analyzed
Total Dissolved Solids (TDS)
SM 2540 C
213 mg/L
11/28/2016
Chloride
SM 4500 C1 E
14 mg/L
11/28/2016
Total Organic Carbon (TOC)
SM 5310 B
3.7 mg/L
12/05/2016
1,1,1,2 -Tetrachloroethane
SM 6200C
<0.50pg/L
11/30/2016
1,1,1 -Trichloroethane
SM 62000
< 0.50 pg/L
11/30/2016
1,1,2,2 -Tetrachloroethane
SM 62000
< 0.50 pg/L
11/30/2016
1,1,2 -Trichloroethane
SM 6200C
< 0.50 pg/L
11/30/2016
1,1-Dichloroethane
SM 62000
< 0.50 pg/L
11/30/2016
1,1-Dichloroethene
SM 62000
< 0.50 pg/L
11/30/2016
1,1-Dichloropropene
SM 62000
< 0.50 pg/L
11/30/2016
1,2,3-Trichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,2,3-Trichloropropane
SM 6200C
< 0.50 pg/L
11/30/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,2,4-Trimethylbenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,2-Dibromo-3-Chloropropane
SM 6200C
< 0.50 pg/L
11/30/2016
1,2-Dibromoethane
SM 62000
< 0.50 pg/L
11/30/2016
1,2 -Dichlorobenzene
SM 62000
< 0.50 pg/L
11/30/2016
1,2-Dichloroethane
SM 62000
< 0.50 pg/L
11/30/2016
1,2-Dichloropropane
SM 62000
< 0.50 pg/L
11/30/2016
1,3,5-Trimethylbenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,3 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1, 3-Dichloropropane.
SM 62000
< 0.50 pg/L
11/30/2016
1,4 -Dichlorobenzene
SM 62000
< 0.50 pg/L
11/30/2016
2,2-Dichloropropane
SM 62000
< 0.50 pg/L
11/30/2016
2-Chlorotoluene
SM 6200c
< 0.50 pg/L
11/30/2016
4-Chlorotoluene
SM 62000
< 0.50 pg/L
11/30/2016
Report #:: 2016-16935 Page 4 of 12

Environmental Chemists, Inc.
• 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Fortin Contract Services
Post Office Box 4188
Emerald Isle NC
Attention: Dan Fortin
PT
28594
Date of Report: Dec 08, 2016
Customer PO #:
Customer ID: 08100061
Report #: 2016-16935
Project ID: Cape Royal Dolphin MW
Benzene
SM 6200c
< 0.50 pg/L
11/30/2016
Bromobenzene
SM 6200c
< 0.50 pg/L
11/30/2016
Bromochloromethane
SM 6200c
< 0.50 pg/L
11/30/2016
Bromodichloromethane
SM 6200c
< 0.50 pg/L
11/30/2016
Bromoform
SM 6200c
< 0.50 pg/L
11/30/2016
Bromomethane
SM 6200c
< 0.50 pg/L
11/30/2016
Carbon tetrachloride
SM 6200c
< 0.50 pg/L
11/30/2016
Chlorobenzene
SM 6200c
<'0.50 pg/L
11/30/2016
Chloroethane
SM 6200c
< 0.50 pg/L
11/30/2016
Chloroform
sM 6200c
< 0.50 pg/L
11/30/2016
Chloromethane
SM 6200c
< 0.50 pg/L
11/30/2016
cis-1,2-Dichloroethene
SM 6200c
< 0.50 pg/L
11/30/2016
cis -1, 3-Dichloropropene
SM 6200c
< 0.50 pg/L
11/30/2016
Dibromochloromethane
SM 6200c
< 0.50 pg/L
11/30/2016
Dibromomethane
SM 6200c
< 0.50 pg/L
11/30/2016
Dichlorodifluoromethane
SM 62000
< 0.50 pg/L
11/30/2016
Ethylbenzene
SM 6200c
< 0.50 pg/L
11/30/2016
Hexachlorobutadiene
SM 6200c
< 0.50 pg/L
11/30/2016
Isopropylbenzene
SM 6200c
< 0.50 pg/L
11/30/2016
M+P Xylene
SM 6200c
< 1.00 pg/L
11/30/2016
Methylene chloride
SM 6200c
< 0.50 pg/L
11/30/2016
Naphthalene
SM 6200c
< 0.50 pg/L
11/30/2016
n-Butylbenzene
SM 6200c
< 0.50 pg/L
11/30/2016
n-Propylbenzene
SM 6200c
< 0.50 pg/L
11/30/2016
ortho-Xylene
SM 6200c
< 0.50 pg/L
11/30/2016
p-Isopropyltoluene
SM 6200c
< 0.50 pg/L
11/30/2016
sec-Butylbenzene
SM 62000
< 0.50 pg/L
11/30/2016
Styrene
SM 6200c
< 0.50 pg/L
11/30/2016
tert-Butylbenzene
SM 6200c
< 0.50 pg/L
11/30/2016
Tetrachloroethene
SM 6200c
< 0.50 pg/L
11/30/2016
Report #:: 2016-16935
Page 5 of 12

• Environmental Chemists, Inc.
enviroe-hem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Fortin Contract Services
Post Office Box 4188
Emerald Isle NC 28594
Attention: Dan Fortin
m W 3
Date of Report: Dec 08, 2016
Customer PO #:
Customer ID: 08100061
Report #: 2016-16935
Project ID: Cape Royal Dolphin MW
Toluene
SM 6200c
< 0.50 pg/L
11/30/2016
Trans-1,2-Dichloroethene
SM 6200C
< 0.50 pg/L
11/30/2016
Trans-1,3-dichloropropene
SM 6200c
< 0.50 pg/L
11/30/2016
Trichloroethene
SM 62000
< 0.50 pg/L
11/30/2016
Trichlorofluoromethane
SM 6200C
< 0.50 pg/L
11/30/2016
Vinyl chloride
SM 6200c
< 0.50 pg/L
11/30/2016
Total Coliform
SM 9222B
>8000 Colonies/100mL
11/23/2016
Fecal Coliform
SM 9222D MF
<1 Colonies/100mL
11/23/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen'
EPA 353.2
0.11 mg/L
11/23/2016
Nitrate+Nitrite-Nitrogen
EPA 353.2
< 0.02 mg/L
11/29/2016
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
12/08/2016
Report #:: 2016-16935 Page 6 of 12

Mall. original
.. _ .,,, , G„ .,,l,.c;, ,,_zIn,5 mporc«iwe, accurate, aro complete t a ta5oratory arra:yt�caP data tivas produced
�° ^� G�Nro�e�Tetrccs C! 2�a;y5s byahohh Caro'�ra A' 'A (tcrr^eriy DC i) certified lat:aratory. I am awars that there are s;gniVcart pena;;;es !or submitting false fnformstion,
iRc;L'a ^c7 fnA r+necfn7,ty of f,�ec:�nrl iirr.'ens..;�nrt�:L..:....:....,.:..�.•.....

enyirochem
SM
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab . 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax
[e-mail]
Fortin Contract Services
Date of Report:
Dec 08, 2016
Post Office Box 4188
Customer PO #:
SM 4500 CI E
Emerald Isle NC 28594
Customer ID:
08100061
Attention: Dan Fortin
Report #:
2016-16935
1,1,1,2 -Tetrachloroethane
Project ID: Cape Royal Dolphin MW
Lab ID Sample ID:
Collect Date/Time Matrix
Sampled by
16-40877 Site: MW -5
11/23/2016 8:21 AM Water
Client
Test Method Results Date Analyzed
Total Dissolved Solids (TDS)
SM 2540 C
264 mg/L
11/28/2016
Chloride
SM 4500 CI E
31 mg/L
11/28/2016
Total Organic Carbon (TOC)
SM 5310 B
56.5 mg/L
12/05/2016
1,1,1,2 -Tetrachloroethane
SM 62000
< 0.50 pg/L
11/30/2016
1,1,1 -Trichloroethane
SM 6200c
< 0.50 pg/L
11/30/2016
1,1,2,2 -Tetrachloroethane
SM 6200C
< 0.50 pg/L
11/30/2016
1,1,2 -Trichloroethane
SM 62000
< 0.50 pg/L
11/30/2016
1,1-Dichloroethane
SM 62000
< 0.50 pg/L
11/30/2016
1,1-Dichloroethene
SM 6200C
< 0.50 pg/L
11/30/2016
1, 1 -Dichloropropene
SM 62000
< 0.50 pg/L
11/30/2016
1,2,3-Trichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,2,3-Trichloropropane
SM 6200c
< 0.50 pg/L
11/30/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,2,4-Trimethylbenzene
SM 62000
< 0.50 pg/L
11/30/2016
1,2-Dibromo-3-Chloropropane
SM 62000
< 0.50 pg/L
11/30/2016
1,2-Dibromoethane
SM 6200c
< 0.50 pg/L
11/30/2016
1,2 -Dichlorobenzene
SM 6200c
< 0.50 pg/L
11/30/2016
1,2-Dichloroethane
SM 6200c
< 0.50 pg/L
11/30/2016
1,2-Dichloropropane
SM 62000
< 0.50 pg/L
11/30/2016
1,3,5 -Trim ethyl benzene
SM 6200c
< 0.50 pg/L
11/30/2016
1,3 -Dichlorobenzene
SM 62000
< 0.50 pg/L
11/30/2016
1,3-Dichloropropane
SM 62000
< 0.50 pg/L
11/30/2016
1,4 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
2,2-Dichloropropane
SM 6200c
< 0.50 pg/L
11/30/2016
2-Chlorotoluene
SM 6200c
< 0.50 pg/L
11/30/2016
4-Chlorotoluene
SM 62000
< 0.50 pg/L
11/30/2016
Report #:: 2016-16935
Page 1 of 12

envirochem
SM
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax
[e-mail]
Fortin Contract Services
Date of Report: Dec 08, 2016
Post Office Box 4188
Customer PO M
Emerald Isle NC
28594
Customer ID: 08100061
Attention: Dan Fortin
Report M 2016-16935
K U✓5
Project ID: Cape Royal Dolphin MW
Benzene
SM 62000
< 0.50 pg/L
11/30/2016
Bromobenzene
SM 62000
< 0.50 pg/L
11/30/2016
Bromochloromethane
SM 62000
< 0.50 pg/L
11/30/2016
Bromodichloromethane
SM 62000
< 0.50 pg/L
11/30/2016
Bromoform
SM 62000
< 0.50 pg/L
11/30/2016
Bromomethane
SM 62000
< 0.50 pg/L
11/30/2016
Carbon tetrachloride
SM 62000
< 0.50 pg/L
11/30/2016
Chlorobenzene
W 62000
< 0.50 pg/L
11/30/2016
Chloroethane
SM 62000
< 0.50 pg/L
11/30/2016
Chloroform
SM 62000
< 0.50 pg/L
11/30/2016
Chlorbmethane
SM 62000
< 0.50 pg/L
11/30/2016
cis-1,2-Dichloroethene
SM 62000
< 0.50 pg/L
11/30/2016
cis- 1,3-Dichloropropene
SM 6200C
< 0.50 pg/L
11/30/2016
Dibromochloromethane
SM 62000
< 0.50 pg/L
11/30/2016
Dibromomethane
SM 62000
< 0.50 pg/L
11/30/2016
Dichlorodifluoromethane
SM 6200C
< 0.50 pg/L
11/30/2016
Ethylbenzene
SM 62000
< 0.50 pg/L
11/30/2016
Hexachlorobutadiene
SM 62000
< 0.50 pg/L
11/30/2016
Isopropylbenzene
SM 62000
< 0.50 pg/L
11/30/2016
M+P Xylene
SM 62000
< 1.00 pg/L
11/30/2016
Methylene chloride
SM 62000
< 0.50 pg/L
11/30/2016
Naphthalene
SM 62000
< 0.50 pg/L
11/30/2016
n-Butylbenzene
SM 62000
< 0.50 pg/L
11/30/2016
n-Propylbenzene
SM 62000
< 0.50 pg/L
11/30/2016
ortho-Xylene
SM 62000
< 0.50 pg/L
11/30/2016
p-Isopropyltoluene
SM 62000
< 0.50 pg/L
11/30/2016
sec-Butylbenzene
SM 62000
< 0.50 pg/L
11/30/2016
Styrene
SM 62000
< 0.50 pg/L
11/30/2016
tert-Butylbenzene
SM 62000
< 0.50 pg/L
11/30/2016
Tetrachloroethene
SM 6200C
< 0.50 pg/L
11/30/2016
Report #:: 2016-16935 Page 2 of 12

r
viro(+em
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Fortin Contract Services
Date of Report: Dec 08, 2016
Post Office Box 4188
Customer PO #:
Emerald Isle NC
28594
Customer ID: 08100061
Attention: Dan Fortin
Report #: 2016-16935
AT LV5
Project ID: Cape Royal Dolphin MW
Toluene
SM 62000
< 0.50 pg/L
11/30/2016
Trans- 1,2-Dichloroethene
SM 62000
< 0.50 pg/L
11/30/2016
Trans- 1,3-dichloropropene
SM 6200C
<0.50pg/L
11/30/2016
Trichloroethene
SM 62000
< 0.50 pg/L
11/30/2016
Trichlorofluoromethane
SM 62000
< 0.50 pg/L
11/30/2016
Vinyl chloride
SM 62000
< 0.50 pg/L
11/30/2016
Total Coliform
SM 9222s
>8000 Colonies/100mL
11/23/2016
Fecal Coliform
SM 9222D MF
<1 Colonies/100mL
11/23/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 0.02 mg/L 11/23/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 11/29/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/08/2016
Report #:: 2016-16935 Page 3 of 12

r1w
to
Bal -=gal liiii7 _
Itign
SUBMIT FORM ON YELLOW PAPER ONLY
.xz ter.:,.,....ra._.r..:.,..
,,.. , ..-.:. ,.-s^z7.r.�;.. �.:. y. a. .%_..e�,..a ;."� ..: �o.� ....
,-•�-
.. - _ , ... - _.. x _ _.�
i'AC �NFOF MATtON Please Print Clearly or Type
J.F illt)r lie' CA PZ P Q YA t C !) h PIW h<
Permit Name (if 4flerent):
iFacifity Address:_ Pb_ _
MW - -
PERMIT f EXPIRATION DATE
icor►-GiliSe_f i �/i;iC
NPDES _
T YRE.OF.PERMOED OPERATION BEING MONITORED
Lagoon Remec+iation: !nk1katlon Gallery
P Remedlatiorx ,. _ -
_ _- rotary Distr�utor- —rand bion of S' e -
APFca . lug
%r 0i& r Tremont Systera±s - Other. _
_ _ ' .o - o = NOTE ilafues s(�oufrl:geiiect t(issoived anti:. -
Scxeensd_Intsrval, ft. 3o ft- L !t(8..,.:t$ t98);
Depth tawater- Level: ft: below measuring point, - -- ,colloidal: concet�trattons -
Measun rig Poinf is 7 ` k._afaove land surface. ®Ef#luent (99j - _ -
Galicns_diwater.pu�pe,.d +ed izefore sampling�- Date sample coltected�?, D e sample,analyied
i=iaid pnaly�is:
_Sp sV _Dor ;etarlc -- umbos 1 1n _B�ar^s: - �' t i P*rG`r�c r l
-- - - - -
Odr .-Appearance-co
-- pARAMffgS (Samples, for metals_ were-coiideted unfiltered_- Yid _ - - AiO and field acidified= -YES - NO) - _
COD .--_mg/i Ntiite (NO2)_as. N.,. a. 3 mg/iNt _ _-Ni_ . ckel- = - mg/i
^"
..nli` - ttal— tj `
Coliform -MF Total - J100mi
Dissolved -Solids: -Total _- _ 2'1. _ mg/t
Tvv
-7T,7
mgJl
Bal -=gal liiii7 _
Itign
Ca - caicium "r
_ _ lilg/`i.
Arsenic -
mtgLi
Grease and Oils
tigfl
Phgnoi
AN t82
rpg/i
Sulfate -
- ng/l
♦.7t:ICrW IIV" VVII{JY�dQ1:aVG_ -
urYllrus
Total' Arnernor ild r
mgri
TKN as -N
mg/1
Phosphorus _Total=as P _ =_ =,- mgA
Al - Aluminum
mgJl
Bal -=gal liiii7 _
--
Ca - caicium "r
_ _ lilg/`i.
Cd - Cadmium
Chromium -Total
- mgA
Qu -(hopper
AN t82
rpg/i
F4-1ron
VME
Hg = Mercury
_ mgA
T% - r-uidssrurn
mg/1
Mg - Magnesium
mgr!
Mn - Manganese
mgA
Zn - Zinc,-
Amanda -,Nitrogen,_- - gig
Other (Specify CompoundsatrdConcentratiori Units
' ORGANCCS: (GC=aaCr'MS.,HKq)
(Specify test anis-method #. Att- Iab 'repo_ rt.)
Heport Attached? Yes (t) No - (U
VOC : method #ash �200C
method # a
method #
lIWAQ Paw A1QA

PP , * FPO--
envirochem
sm
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Fortin Contract Services
Date of Report:
Dec 08, 2016
Post Office Box 4188
Customer PO #:
SM 4500 CI E
Emerald Isle NC 28594
Customer ID:
08100061
Attention: Dan Fortin
Report #:
2016-16935
1,1,1,2 -Tetrachloroethane
Project ID: Cape Royal Dolphin MW
Lab ID Sample ID:
Collect Date/Time Matrix
Sampled by
16-40882 Site: MW -6
11/23/2016 8:10 AM Water
Client
Test Method Results Date Analyzed
Total Dissolved Solids (TDS)
SM 2540 C
278 mg/L
11/28/2016
Chloride
SM 4500 CI E
52 mg/L
11/28/2016
Total Organic Carbon (TOC)
SM 5310 B
21.1 mg/L
12/05/2016
1,1,1,2 -Tetrachloroethane
SM 6200C
< 0.50 pg/L
11/30/2016
1,1,1 -Trichloroethane
SM 62000
< 0.50 pg/L
11/30/2016
1,1,2,2 -Tetrachloroethane
SM 62000
< 0.50 pg/L
11/30/2016
1,1,2 -Trichloroethane
SM 62000
< 0.50 pg/L
11/30/2016
1,1-Dichloroethane
SM 6200C
< 0.50 pg/L
11/30/2016
1,1-Dichloroethene
SM 6200C
< 0.50 pg/L
11/30/2016
1,1-Dichloropropene
SM 62000
< 0.50 pg/L
11/30/2016
1,2,3-Trichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,2,3-Trichloropropane
SM 6200C
< 0.50 pg/L
11/30/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,2,4-Trimethylbenzene
SM 62000
< 0.50 pg/L
11/30/2016
1,2-Dibromo-3-Chloropropane
SM 6200C
< 0.50 pg/L
11/30/2016
1,2-Dibromoethane
SM 62000
< 0.50 pg/L
11/30/2016
1,2 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,2-Dichloroethane
SM 6200C
< 0.50 pg/L
11/30/2016
1,2-Dichloropro pane
SM 6200C
< 0.50 pg/L
11/30/2016
1,3,5-Trimethylbenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,3 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,3-Dichloropropane
SM 6200C
< 0.50 pg/L
11/30/2016
1,4 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
2,2-Dichloro propane
SM 62000
< 0.50 pg/L
11/30/2016
2-Chlorotoluene
SM 6200C
< 0.50 pg/L
11/30/2016
4-Chlorotoluene
SM 6200C
< 0.50 pg/L
11/30/2016
Report #:: 2016-16935 Page 10 of 12

Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Fortin Contract Services
Post Office Box 4188
Emerald Isle NC
Attention: Dan Fortin
jam[ W
28594
Date of Report: Dec 08, 2016
Customer PO M
Customer ID: 08100061
Report M 2016-16935
Project ID: Cape Royal Dolphin MW
Benzene
SM 6200C
< 0.50 pg/L
11/30/2016
Bromobenzene
SM 6200c
< 0.50 pg/L
11/30/2016
Bromochloromethane
SM 6200C
< 0.50 pg/L
11/30/2016
Bromodichloromethane
SM 6200C
< 0.50 pg/L
11/30/2016
Bromoform
SM 6200C
< 0.50 pg/L
11/30/2016
Bromomethane
SM 62000
< 0.50 pg/L
11/30/2016
Carbon tetrachloride
SM 6200C
< 0.50 pg/L
11/30/2016
Chlorobenzene
SM 62000
< 0.50 pg/L
11/30/2016
Chloroethane
SM 62000
< 0.50 pg/L
11/30/2016
Chloroform
SM 6200C
< 0.50 pg/L
11/30/2016
Chloromethane
SM 6200C
< 0.50 pg/L
11/30/2016
cis-1,2-Dichloroethene
SM 6200C
< 0.50 pg/L
11/30/2016
cis-1,3-Dichloropropene
SM 62000
< 0.50 pg/L
11/30/2016
Dibromochloromethane
SM 6200c
< 0.50 pg/L
11/30/2016
Dibromomethane
SM 6200C
< 0.50 pg/L
11/30/2016
Dichlorodifluoromethane
SM 6200c
< 0.50 pg/L
11/30/2016
Ethylbenzene
SM 6200c
< 0.50 pg/L
11/30/2016
Hexachlorobutadiene
SM 6200C
< 0.50 pg/L
11/30/2016
Isopropylbenzene
SM 6200C
< 0.50 pg/L
11/30/2016
M+P Xylene
SM 6200c
< 1.00 pg/L
11/30/2016
Methylene chloride
SM 6200C
< 0.50 pg/L
11/30/2016
Naphthalene
SM 62000
< 0.50 pg/L
11/30/2016
n-Butylbenzene
SM 6200C
< 0.50 pg/L
11/30/2016
n-Propylbenzene
SM 62000
< 0.50 pg/L
11/30/2016
ortho-Xylene
SM 6200C
< 0.50 pg/L
11/30/2016
p-Isopropyltoluene
SM 6200c
< 0.50 pg/L
11/30/2016
sec-Butylbenzene
SM 6200C
< 0.50 pg/L
11/30/2016
Styrene
SM 6200c
< 0.50 pg/L
11/30/2016
tert-Butylbenzene
SM 6200c
< 0.50 pg/L
11/30/2016
Tetrachloroethene
SM 6200C
< 0.50 pg/L
11/30/2016
Report #:: 2016-16935
Page 11 of 12

Environmental Chemists, Inc.
envirochem6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Fortin Contract Services
Date of Report: Dec 08, 2016
Post Office Box 4188
Customer PO M
Emerald Isle NC 28594
Customer ID: 08100061
Attention: Dan Fortin
Report M 2016-16935
rfW d
Project ID: Cape Royal Dolphin MW
Toluene
SM 6200C
< 0.50 pg/L
11/30/2016
Trans- 1,2-Dichloroethene
SM 6200C
< 0.50 pg/L
11/30/2016
Trans-1,3-dichloropropene
SM 62000
< 0.50 pg/L
11/30/2016
Trichloroethene
SM 62000
< 0.50 pg/L
11/30/2016
Trichlorofluoromethane
SM 6200c
< 0.50 pg/L
11/30/2016
Vinyl chloride
SM 6200C
< 0.50 pg/L
11/30/2016
Total Coliform
SM 92226
>8000 Colonies/100ml-
11/23/2016
Fecal Coliform
SM 9222D MF
<1 Colonies/100ml-
11/23/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 0.03 mg/L 11/23/2016
Nitrate+ N itrite-N itrogen EPA 353.2 < 0.02 mg/L 11/29/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/08/2016
Comment:
Reviewed by:
Report #:: 2016-16935 Page 12 of 12

a
Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Fortin Contract Services
PROJECT NAME: Cape Royal Dolphin- MW's
REPORT NO: 10 — t 1.6-3
ADDRESS: Post Office Box 4188
CONTACT NAME: Dan Fortin
PO NO:
Emerald Isle, NC 28594
REPORT TO:
PHONE/FAX:
Date Time
COPY TO:
email:
Sampled By: SAMPLE TYPE: I = Influent, E = Effluent, W = Well, ST = Stream, SO = Soil, SL = Sludge, Other:
Sample Identification
Collection
T
"
E
�
D
a o o
0 v a
e a
E
m
J Z
PRESERVATION
ANALYSIS REQUESTED
Date Time
Temp
W
Z
J
=
o
_
�,
=
=
z
o
=
w
o
MW#
P
Nitrate, TDS, Chloride
Gf)
Depth
P
TOC
G
pH
P
Total Coliform, Fecal Coliform
G
G P
G G
VOC (NOV.)
P
G
MW#
P
��
Nitrate, TDS, Chloride
G
Depth
P
TOC
G G
pH
C P
G G
Total Coliform, Fecal Coliform
P
G G
Transfer
elinqui hed y:
Date/Time
R4beived By:
Date/Time
1.
P/
1 'Q y 10.gg
2.
Temperature eivq�
Delivered By:
Coinments:_Due Vrch, July, Nov.
Accepted: V
ived By:
Rejec Resample Re/ est d:
Date: G 7-� 11P Time: r
TURNAROUND:

Analytical & Consulting Chemists
ENVIRONMENTAL CHEMISTS, INC
NCDENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
[e-mail]
Client: Fortin Contract Services
PROJECT NAME: Cape Royal Dolphin- MW's
REPORT NO:
ADDRESS: Post Office Box 4188
CONTACT NAME: Dan Fortin
PO NO:
Emerald Isle, NC 28594
REPORT TO:
PHONE/FAX:
Date Time
COPY TO:
email:
Sampled Bv: SAMPLE TYPE: I = Influent_ E = Effluent_ W = Well_ ST = Stream_ SO = Snil SI = Rlnrina C1+har-
Sample Identification
Collectiona
F
°'
E
�n
N
°o `o
o
�
_
C 0
'.� o
o a
"`
�,
c `
`o m
t E
"
e W
m 00
J
z
PRESERVATION
ANALYSIS REQUESTED
Date Time
Temp
w
o
z
o
�,
i
x
x
a
z
o
=
w
x
o
MW# 'T
P
Nitrate, TDS, Chloride
G
// I✓1
Depth b
G
P
TOC
G
PH ° cc-:�)
Total Coliform, Fecal Coliform
G
GI
G
P
G
VOC (NOV.)
P
G
G
MW#
_
G
Nitrate, TDS, Chloride
�r 1 �!
Depth
G
P
TOC
G
p
pH o
C
P
Total Coliform, Fecal Coliform
G
G
C
P
G
G
Transfer
Relinqui h d By:
Date/Time
ceived By:
Date/Time
2.
I emperature W nj Ike ero
Delivered By: /
Cornme1nts:_D a rch, July, Nov.
Received By:

W InSUBMIT FORM ON YELLOW PAPER ONLY
Please Print Clearly or Type
/ �LAL—L � L PHI r�
fit)r (carp
Fade. `° E—.. -
Permit Name (if different):
ty Address: C � � � G � A %3 0 � R Q
Facili
95 9 LlCounty C 4 A T E (<" � t
VM Contact Person: "4 Telephone #: 9 52- - 5 ` 3 -X7/2 C?
Weil Location/ Site, Name: No. of Wells to be Sampled:
Well identification Number (from Permit): For Gioundwater Trealment Systems
Well Depth: ft. Well Diameter. in. Check One -
Screened Interval. ft. to _ fL ❑ Influent (98)
Depth to Water level: 17�� ft. below measuring point. ❑ Effluent (99)
Measuring Point is _, fL above land surface.
Gallons of water pumpedlbailed before sampling:
Field analysis: pH r . Specific Conductan6e uMhos
Temp. 'C, Odor W&Z-2, . Appearance I �'
,PARAMf_TE$g (Samples for metals_ were collected
COD
mg/l
Coliform: MF Fecal
/100ml
Coliform: MF Total
/100ml
(Note: Use MPH rpethod for highly WrM samples)
Al - Aluminum
Dissolved Solids: Total mgA
pH (when analyzed)
units
TOC n
mg/l
Chloride /
mgA
Arsenic
mg/I
Grease and Oils
mgA
Phenol
mg/l
Sulfate
mgA
Specific Conductance
uMhos
Total Ammonia
rng/l
TKN as N
- mg/l
YES - NO
PERMIT
DATE:
NPDES
TYPE OF PERMITTED OPERATION BEING MONITORED
Lagoon - - - Remediation: Infiltration Gallery
Spray Field Remedatim
Rotary Distributor Land Application of Sludge
Other. - -
NOTE: Values should reflect dissolved and
colloidal concentrations.
Date sample collected: 1=��—=L Date sample analyzed: -
Laboratory Name: e Cf fC &1 I S _T S /Arc
Certification No. - 2 27
and field acidified
Nitrite (NO2) as N O 2
mgA
Nitrate (NO3) as N n 2
mgA
Phosphorus: Total as P
mgA
Orthophosphate
mgA
Al - Aluminum
mgA
Ba - Barium
mgA
Ca - Calcium
mg/l
Cd - Cadmium .IAN 1 A 2017
mgA
Chromium: Total_.
mgA
Cu - Copper
mg/l
Fe- Iron -
mg/I
Hg - Mercury
mgA
K - Potassium
mg/l
Mg - Magnesium
mgn
Mn - Manganese -
mgA
YES L' NO)
Ni - Nickel mg/1
Pb - Lead MO
Zn - Zinc-- mgn
Ammonia Nitrogen mg/l
Other (Specify Compounds and Concentration Units)
ORGANICS: (GC,GCIMS,HPLC)
(Specify test and method #. Att ab report.)
Report Attached? Yes 1) No (0)
VOC method # - 51742600
method # =
method # =

Report #:: 2016-16935 Page 7 of 12
Environmental Chemists,
Inc.
envirochem6602
Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
sM
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS
[e-mail]
Fortin Contract Services
Date of Report: Dec 08, 2016
Post Office Box 4188
Customer PO #:
Emerald Isle NC 28594
Customer ID: 08100061
Attention: Dan Fortin
Report #: 2016-16935
Project ID: Cape Royal Dolphin MW
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
16-40881 Site: MW -7
11/23/2016 8:00 AM Water Client
Test
Method Results Date Analyzed
Total Dissolved Solids (TDS)
SM 2540 C
145 mg/L
11/28/2016
Chloride
SM 4500 CI
E 16 mg/L
11/28/2016
Total Organic Carbon (TOC)
SM 5310 B
20.3 mg/L
12/05/2016
1,1,1,2 -Tetrachloroethane
sM 62000
< 0.50 pg/L
11/30/2016
1,1,1 -Trichloroethane
SM 6200C
< 0.50 pg/L
11/30/2016
1,1,2,2 -Tetrachloroethane
SM 6200C
< 0.50 pg/L
11/30/2016
1,1,2 -Trichloroethane
SM 62000
< 0.50 pg/L
11/30/2016
1,1-Dichloroethane
SM 6200C
< 0.50 pg/L
11/30/2016
1,1-Dichloroethene
SM 6200C
< 0.50 pg/L
11/30/2016
1,1-Dichloropropene
SM 62000
< 0.50 pg/L
11/30/2016
1,2,3-Trichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,2,3-Trichloropropane
SM 62000
< 0.50 pg/L
11/30/2016
1,2,4-Trichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,2,4 -Trim ethyl benzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,2-Dibromo-3-Chloropropane
SM 6200C
< 0.50 pg/L
11/30/2016
1,2-Dibromoethane
SM 6200C
< 0.50 pg/L
11/30/2016
1,2 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
1,2-Dichloroethane
SM 62000
< 0.50 pg/L
11/30/2016
1,2-Dichloropropane
SM 6200C
< 0.50 pg/L
11/30/2016
1,3,5 -Trim ethyl benzene
SM 62000
< 0.50 pg/L
11/30/2016
1,3 -Dichlorobenzene
SM 62000
< 0.50 pg/L
11/30/2016
1,3-Dichloropropane
SM 62000
< 0.50 pg/L
11/30/2016
1,4 -Dichlorobenzene
SM 6200C
< 0.50 pg/L
11/30/2016
2,2-Dichloropropane
SM 62000
< 0.50 pg/L
11/30/2016
2-Chlorotoluene
SM 62000
< 0.50 pg/L
11/30/2016
4-Chlorotoluene
SM 62000
< 0.50 pg/L
11/30/2016
Report #:: 2016-16935 Page 7 of 12

0
SM
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Fortin Contract Services
Date of Report: Dec 08, 2016
Post Office Box 4188
Customer PO #:
Emerald Isle NC
28594
Customer ID: 08100061
Attention: Dan Fortin
Report #: 2016-16935
Mty °�
Project ID: Cape Royal Dolphin MW
Benzene
SM 6200c
< 0.50 pg/L
11/30/2016
Bromobenzene
SM 6200c
< 0.50 pg/L
11/30/2016
Bromochloromethane
SM 6200c
< 0.50 pg/L
11/30/2016
Bromodichloromethane
SM 6200c
< 0.50 pg/L
11/30/2016
Bromoform
SM 6200c
< 0.50 pg/L
11/30/2016
Bromomethane
SM 6200c
< 0.50 pg/L
11/30/2016
Carbon tetrachloride
SM 62000
< 0.50 pg/L
11/30/2016
Chlorobenzene
SM 62000
< 0.50 pg/L
11/30/2016
Chloroethane
SM 6200c
< 0.50 pg/L
11/30/2016
Chloroform
SM 62000
< 0.50 pg/L
11/30/2016
Chloromethane
SM 6200c
< 0.50 pg/L
11/30/2016
cis-1,2-Dichloroethene
SM 62000
< 0.50 pg/L
11/30/2016
cis- 1,3-Dichloropropene
SM 62000
< 0.50 pg/L
11/30/2016
Dibromochloromethane
SM 62000
< 0.50 pg/L
11/30/2016
Dibromomethane
SM 62000
< 0.50 pg/L
11/30/2016
Dichlorodifluoromethane
SM 62000
< 0.50 pg/L
11/30/2016
Ethylbenzene
SM 62000
< 0.50 pg/L
11/30/2016
Hexachlorobutadiene
SM 6200C
< 0.50 pg/L
11/30/2016
Isopropylbenzene
SM 6200c
< 0.50 pg/L
11/30/2016
M+P Xylene
SM 6200c
< 1.00 pg/L
11/30/2016
Methylene chloride
SM 6200c
< 0.50 pg/L
11/30/2016
Naphthalene
SM 6200c
< 0.50 pg/L
11/30/2016
n-Butylbenzene
SM 6200c
< 0.50 pg/L
11/30/2016
n-Propylbenzene
SM 62000
< 0.50 pg/L
11/30/2016
ortho-Xylene
SM 6200c
< 0.50 pg/L
11/30/2016
p-Isopropyltoluene
SM 6200c
< 0.50 pg/L
11/30/2016
sec -Butyl benzene
SM 6200c
< 0.50 pg/L
11/30/2016
Styrene
SM 6200c
< 0.50 pg/L
11/30/2016
tert-Butylbenzene
SM 6200c
< 0.50 pg/L
11/30/2016
Tetrachloroethene
SM 62000
< 0.50 pg/L
11/30/2016
Report #:: 2016-16935
Page 8 of 12

Irenvirochem
ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Fortin Contract Services
Date of Report: Dec 08, 2016
Post Office Box 4188
Customer PO #:
Emerald Isle NC 28594
Customer ID: 08100061
Attention: Dan Fortin
Report #: 2016-16935
7
Project ID: Cape Royal Dolphin MW
Toluene
SM 62000
< 0.50 pg/L
11/30/2016
Trans-1,2-Dichloroethene
SM 5200C
< 0.50 pg/L
11/30/2016
Trans-1,3-dichloropropene
SM 6200C
< 0.50 pg/L
11/30/2016
Trichloroethene
SM 62000
< 0.50 pg/L
11/30/2016
Trichlorofluoromethane
SM 62000
< 0.50 pg/L
11/30/2016
Vinyl chloride
SM 6200C
< 0.50 pg/L
11/30/2016
Total Coliform
SM 9222B
>8000 Colonies/100ml-
11/23/2016
Fecal Coliform
SM 9222D MF
<1 Colonies/100ml-
11/23/2016
Nitrate Nitrogen (Calc)
Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 11/23/2016
Nitrate+Nitrite-Nitrogen EPA 353.2 < 0.02 mg/L 11/29/2016
Nitrate Nitrogen Subtraction Method <0.02 mg/L 12/08/2016
Report #:: 2016-16935 Page 9 of 12