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HomeMy WebLinkAboutWQ0034102_Monitoring - 11-2016_20170103SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENT a NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM - 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-061T Phom:919407d 06 FACILITY INFORMATION, Reese P"a fry o•7yPe PERMIT Number:W 62Expiraflon Date: Facility Name: I 111A/ G I- "✓lQ Ji711)N� Non -Discharge UIC Permit Name (if different): I NPDES Other Facility AddressTYPE OF PERMITTED OPERATION BEING MONITORED County 1 Q y %UP ❑ Lagoon m Remediation: Infiltration Gallery /(/� AR Spray Field G Remediation: Contact Person: / \C yI a r; Telephone#: 4 —' ❑ Rotary Distributor 11 Land Application of Sludge 2 Well Localic ite Name -Pak( CIV15F No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: L 10 NUMBER (from Per It): '� Dale sample Collected: Depth: : ff. Well Diameter: in. I to Water Level a2e4e: S . below measuring point Screened Interval: fl. to —ft. ;Uring Point is 'ck _R. above land surface Relative M.P. Elevation: ff. ne of water pumped bailed before sampling: S i 6 gallons )ale sample analyzed: Laboratory Name 'ARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrile (NO,) as N oosm mg/L Coliform. MF Fecal 31616 .( j, U 1100ml- Nitrate (NO3) as N oaem T mg/L Coliform: MF Total 31SW /1D0mL Phosphorus: Total as P poses mg/L ,rbL Use llPN nytlN berylr ry,rpq umpN.) Onhophosphate 70507 mg/L Dissolved Solids:Tolal 7wo0 �j,?,U mg/L AI - Aluminum oleos mg& PH (Lab) 00403 units Be - Barium 0im7 ug1L C TOC msa0 , b mg/L Ca - Calcium oo916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 uglL Arsenic oiw2 uglL Chromium: Total 01034 ug/L Grease and Oils 00s52 mg1L Cu - Copper 01042 mg/L Phenol 32730 ug/L Fe - Iron Dials ug/L Sulfate Deals mglL Hg - Mercury 71900 uglL Speafic Conductance moss -Mhos K - Potassium 00937 mg/L Total Ammonia Dodo 4 C' r yd0 mg/L Mg - Magnesium 00927 mg/L :Am,,,,ne Wbo9ea NN,ae e:Ae°eava eoogee, T." Mn - Manganese 01055 ug/L TKN as N ona2s mg/L Ni - Nickel olwl ug/L FIELD ANALYSES: WAS DRY / at time of pH 00403: �cG J units Temp. 00010. �" ` °C sampling, Spec. Cond. pm94: -Mhos check Odor moss: ti Up here: Appearance 4 `fay' Certification No. Pb - Lead otos+ ug/L Zn - Zinc 01092 mg/L Other (Specify CoMn j and ConcentrationR(F r : itil 2017 Fti i 1 _ I)WR SECTION ORGANICS: (by GC, GCIMS, HPLC) (Specify test and method N. ATTACH LAB REPORT.) Lab Report Attached? ❑ yes (1) 0 NO (0) VOC 78732 , method p method 0 method # method # for Kem6dlation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs'. Permittee (or AlAtgrired Aaent) Hama and Tek - Pkwe print "M GW -59 Rev. &2013 VOC Sgnalne or Pefmnee(or AWnp WA4ent1 (Datil UNIT SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: _ , DEPARTMENT OF ENVIRONMENT 6 NATURAL RESOURCES DIVISION OF WATER RESOURCES- INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617MAIL SERVICE CENTER, RALEIGH, NC27699.151T Phme:61941074306 FACILITY INFORMATION Please rubel Csarty a Type PERMIT Number:(y��.iOZ„Expiration Dale: Facility Name: _ 6lti It, l rr1L5lL. Non -Discharge UIC NPOES Other Permit Name (if different): F 'liry Address: .�J `� q b 1S %z7 1 TYPE ❑r OF PERMITTED OPERATION BEING MONITORED Lagoon 13 Remediation: Infiltration Gallery �) i County 4 Le44 r r�� /eR Spray Field 13 Remediation: Contact Person: �✓ &67J t �. Telephone#: QS7 .S CS t� p /Z ❑ Rotary Distributor ❑ Land Application of Sludge Well Locallon/Site Name: f 34 lew No. of wells to be sampled: Water Source Heat Pump ❑ Other: SAMPLING INFORMATION WELL ID NUMBER Permit): /4 If WELL WAS DRY (from _� Dela sample collected: FIELD AtllglyFS: CO )�O �� at time of Well Depth � P - ff. Depth to Water Level etsas rL below measuring point Well Diameter: In. Screened interval: h, to R. H 00400 units Tem 000lo: p Spec. Cond. mow: pMhos sampling, check Measuring Point is rl h. above land surfs a Relative M.P. Elevation: R. Odor Goals /L C• Iv ` here: Volume of water pumped/bailed before sampling: s 6-­� gallons Appearance Samples for metals were Collected unfiltered: ❑ YES NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Dale sample analyzed: Laboratory Name: Certification No. PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD oo33s mg/L Nitrite, (NO,) as N owls mg/L Pb - Lead D1os1 ug/L Coliform: MF Fecal 31616 /, 10 /100ml Nitrate (NO.) as N oo62D �, 0. O S 0 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 3lsw /100mL Phosphorus: Total as P costs mg/L (Hale. U. LWN meTY lw hq* r u .' Onhophosphate 7os07 mg/L Other (Specify Compounds andrCbantrallon Units): Dissolved Solids:Total 70300 mg/L Al -Aluminum oleos mg/L pH (Lab) 00403 units Ba - Barium olam uglL'- TOC oo68o �p' mg/L Ca - Calcium mete mg/L Chloride mwo mg/L Cd - Cadmium D1027 ug/L Arsenic 01002 uglL Chromium: Total wma uglL Grease and Oils mssz mg/L Cu -Copper 01042 mg/L ORGANICS: (by GC. GC/MS, HPLC) Phenol 32230 ug/L Fe - Iron olws ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00946 mg/L Hg - Mercury 719W ug/L Lab Report Attached? ❑ yes (i) 0 No (o) Specific Conductance pubes PMhos K - Potassium 00937 mg/L VOC 79732 method # Total Ammonia 0oolo <0. / 00 mg/L Mg - Magnesium men mg/L method # Ae IlMegen. NN,. N:pmunrve N".n Ttap Mn - Manganese oloss uglL ,method # THIN as N owes mglL Ni - Nickel 01047 ug/L method # For Remediallon Systems Only (Attach Lab Reports): Influent Total PeenMee (. AUUximNdA MnU Name ane Toe- Plea. pont w type GW -59 Rev. 8/2017 mg/L Effluent Total VOCs: VOC Removal% SUN10,e of Pe,.NN Uv ft enhad AWN) (Dale) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: DEPARTMENT ENVIRONMENT 6NATORAL RESOURCES INFRA IONPROCE691NO NNIT DIVISION OFWATER RESOURCES.INFORMATION COMPLIANCE REPORT FORM 1517a1NLSERVICE CENTER. "LEIGH,NC27699.1617 Phune:919d07ni305 FACILITY INFORMATION Raasa Pent Cleary wType PERMIT Number: (OZFzpiration Dale: Facility Name: -0 1�, >)/ Ct 't.6 V� Non -Discharge UIC NPDES Other Permit Name (if different):\ Facility Address: TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon m Remediation: Infiltration Gallery,7(,/� F i L County(/!*c �❑❑-t yQ Spray Field 0 Remedlation: Contact Person: 1 \Q' �/� f / C Telephone#: a 'lX+b'- ❑ Rotary Distributor ❑ Land Application of Sludge Well LocationlSite NameL4 J No. of wells to be sampled: ❑ Water Source Heat Pump 0 Other: SAMPLING INFORMATION If WELL WAS DRY WELL ID NUMBER (from Permit): T Date sample collected: FIELDANAIYSES: at time of Well Depth: fl. Well Diameter:in. pH ooeooy .�_A units Temp. 000+0: v o C sampling, Depth to Water Level 1125,16: i t [�5 _fl. below measunng point Screened Interval: 1t. to ft. Spec. Cond. 00094: ItMhos check Measuring Point is above land surface Relative M.P. Elevation: M. Odor poolhere: 11//' _ft. Volume of water pumped/bailed before sampling: S- 3 7 gallons Appearance ' El Samples for metals were collected unfiltered: 0 YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: Laboratory Name: Certification No. PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD W335 mg/L Nitrite (NOT) as N oos15 mg/L Pb - Lead 0105+ ug/L Coliform: MF Fecal 31616 /100mi- Nitrate (NOP) as N 0064 :V O l U mg/L Zn - Zinc ot092 mg/L Coliform: MF Total 3160,1 /100mL Phosphorus: Total as P 00665 mg/L ilmn Orthophosphate 70907 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total7o /(l '�f mg/L AI - Aluminum oiio5 mg/L 11 PH (Lab) omo3—�—�—units Be - Badum U1007 ug/L TOC oo6ao ✓I J mg/L Ca - Calcium 110916 mg/L Chloride oo94o .� i. 5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 uglL Chromium: Total moan uglL Grease and Oils ooss2 mg/L Cu - Copper otO42 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron aims uglL (Specify test and method If. ATTACH LAB REPORT) Sulfate M45 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) [3 No (0) Specific Conductance o009s PMhos K - Potassium 110937 mg/L VOC 76732 , method # Total Ammonia poll Gl /00 mg/L Mg - Magnesium oD927 mg/L , method # ;Am wNYo9en NH.8211:Mrt 4N&O "Tow) Mn -Manganese o+oss uglL ,method # TKN as N M25 mg/L Ni - Nickel 0+067 ug/L , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Peteeeee tw A0Nd12ed Aeent) Name.W Tee - Please pent w typo GW -59 Rev. 612013 Effluent Total VOCs: VOC Removal% Sgnalule of ParnxR6a tprauth ZWAmnU (Dote) DWATER QUALITY MONITORING: IANCE REPORT FORM Name: Name act Person: Pei y Be, S -1" P � Location/Site Name. < Ljri n t i .. SUBMIT FORM ON YELLOW PAPER ONLY T OF ENVIRONMENT d NATURAL RESOURCES WATER RESOURCES .INFORMATION PROCESSING UNIT !RVICE LEVER, RALEN3H, NC 37699.160 Phone: 9194074306 Non -Discharge UIC NPOES Other TYPE OF PERMITTED OPERATION BEING MONITORED County ) ql "' ❑ Lagoon m Remediallon: Infiltration Gallery Spray Field 0 Remediation: iphonea:el�j_ Rotary Distributor ❑ Land Application of Sludge No. of wells to be sampled: ❑ Water Source Heal Pump ❑ Other: WELL ID NUMBER (from Permit): I ) Date sample collected: I I - � /' � S- FIELD ANALYSES: o WAS DRY Well Depth C)n ry Well Diameter: in. pH Mao: � , (A units Temp. oaom: Il, / `C at lisamme g Depth to Water Level 82566: I 1 r 4 fi. below measuring point Screened Interval: ft. to _fl. Spec. Cond. 00094: IrMhos check Measuring Point is _� ft. above land surface Relative M.P. Elevation: fi. Odor moss:) A'r here: Volume of water pumped/bailed before sampling: it (/ gallons Orthophosphate 70507 Appearance[ O Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO PH (Lab) oo4w units Be - Barium o1w7 dm san7pla anaryzea: Laboratory Name: ARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD wns mg/L Nitrile (NO.) as N 008/5 mg/L Coliform: MF Fecal 31e1s �l.y /100mL Nitrate (NO,,) as N oos2o S, J mg/L Coliform: MF Total 31so4 /100ml, Phosphorus: Total as P Goess mg/L IIbU YU NPN rry6we q,nyy yryq wyer) Orthophosphate 70507 mg/L Dissolved Solids:Tolal 70ao mg/L AI - Aluminum onos mg/L PH (Lab) oo4w units Be - Barium o1w7 ug/L TOC 00660 }, /,y mglL Ca - Calcium 00916 mg/L Chloride 00940 _ //, a mglL Cd - Cadmium 01027 ug/L Arsenic 0100: ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 ng/L Phenol 3273o ug/L Fe - Iron 01045 uglL Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Specific Conductance cows lMhos K - Potassium 00937 mg/L Total Arrvnoma of slo ,[ /Mol.) mg/L Mg - Magnesium own mg/L Inmwno Non NN,n 11 Am mrce Nhc9rn To.) Mn -Manganese moss uglL TKN as N DD025 ng/L Ni - Nickel 0'067 ug/L „, ,.ov,euldnvn ayaraurs vnry fwlracn Lao He Ports): Influent Total VOCs: Pennine. (p AWgrizeV AgenU Name ane T4b - Plea6e pint a rypa GW -59 Rev. 812013 Certification No. Pb - Lead oios1 ug/L Zn - Zinc olw2 mg/L Other (Specify Compounds and Conn don Units): is ORGANICS: (by GQ GC/MS, HPLC) (Specify test and method N. ATTACH LAB REPORT.) Lab Report Attached? ❑ yes (1) 13 No (0) VOC 78732 , method N method N method M method R Effluent Total mg/L VOC SgnNure of PermNae for AulhOnzeil AyeM) (Dale) Town of Fremont Mr. Ray Bostic 532 Davis Mill Road Fremont NC, 27830 Fayetteville Division Certificate of Analysis Project: Monitoring Wells Samples (Nov) MW 1, grab K6K0936-01 Date Reported: 12/08/16 Date Received: 11/21/16 Date Sampled: 11/21/16 Sampled By: Client Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Fayetteville 4.1 gallons 11/21/16 09:20 DED Ammonia as N <0.100 mg/L 11/22/16 10:30 DSK SM 4500 NH3 C-1997 Chloride 11.5 mg/L 11/28/16 15:45 JAW EPA 300.0, Rev. 2.1 (1993) Coliform, Fecal <1.0 per 100 mL 11/21/16 16:22 JR SM 9222 D-1997 Depth of Water 20.0 feet 11/21/16 09:20 DED Field Measurement Depth to Water Surface 11.6 feet 11/21/16 09:20 DED Field Measurement Gallons purged 4.1 gallons 11/21/16 09:20 DED Field Nitrate as N 5.52 mg/L 11/28/16 15:45 JAW EPA 300.0, Rev. 2.1 (1993) pH, Field Test 3.6 pH Units 11/21/16 09:20 DED SM 4500 H+B-2000 1,1-Dichloroethane <0.125 ug/L 11/23/16 19:54 JDS (Aqueous) Total Dissolved Solids 128 mg/L 11/29/16 10:30 JR SM 2540 C-1997 H, B Temperature, field 17 °C 11/21/16 09:20 DED SM 2550 B-2000 Analyzed by: Microbac Laboratories, Inc. - Ohio Valley 1,1,1,2 -Tetrachloroethane <0.250 ug/L 11/23/16 19:54 JDS SW8260B 1,1,1 -Trichloroethane <0.250 ug/L 11/23/16 19:54 JDS SW8260B 1,1,2,2 -Tetrachloroethane <0.200 ug/L 11/23/16 19:54 JDS SW8260B 1,1,2 -Trichloroethane <0.250 ug/L 11/23/16 19:54 JDS SW8260B 1,1-Dichloroethane <0.125 ug/L 11/23/16 19:54 JDS SW8260B 1,1-Dichloroethene <0.500 ug/L 11/23/16 19:54 JDS SW8260B 1,1-Dichloropropene <0.250 ug/L 11/23/16 19:54 JDS SW8260B 1,2,3-Trichlorobenzene <0.150 ug/L 11/23/16 19:54 JDS SW8260B 1,2,3-Trichloropropane <0.500 ug/L 11/23/16 19:54 JDS SW8260B 1,2,4-Trichlorobenzene <0.200 ug/L 11/23/16 19:54 JDS SW8260B 1,2,4-Trimethylbenzene <0.250 ug/L 11/23/16 19:54 JDS SW8260B 1,2-Dibromo-3-chloropropane <1.00 ug/L 11/23/16 19:54 JDS SW8260B 1,2-Dibromoethane <0.250 ug/L 11/23/16 19:54 JDS SW8260B 1,2 -Dichlorobenzene <0.125 ug/L 11/23/16 19:54 JDS SW8260B 1,2-Dichloroethane <0.250 ug/L 11/23/16 19:54 JDS SW8260B 1,2-Dichloropropane <0.200 ug/L 11/23/16 19:54 JDS SW8260B 1,3,5-Trimethylbenzene <0.250 ug/L 11/23/16 19:54 JDS SW8260B 1,3 -Dichlorobenzene <0.250 ug/L 11/23/16 19:54 JDS SW8260B Page 1 of 16 Town of Fremont Mr. Ray Bostic 532 Davis Mill Road Fremont NC, 27830 Fayetteville Division Certificate of Analysis Project: Monitoring Wells Samples (Nov) Date Reported: 12/08/16 Date Received: 11/21/16 Date Sampled: 11/21/16 Sampled By: Client MW 1, grab K6K0936-01 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Ohio Valley 1,3-Dichloropropane <0.200 ug/L 11/23/16 19:54 JDS SW8260B 1,4 -Dichlorobenzene <0.125 ug/L 11/23/16 19:54 JDS SW8260B 2,2-Dichloropropane <0.250 ug/L 11/23/16 19:54 JDS SW8260B 2-Butanone <2.50 ug/L 11/23/16 19:54 JDS SW8260B 2-Chloroethyl vinyl ether <2.00 ug/L 11/23/16 19:54 JDS SW8260B 2-Chlorotoluene <0.125 ug/L 11/23/16 19:54 JDS SW8260B 2-Hexanone <2.50 ug/L 11/23/16 19:54 JDS SW8260B 4-Chlorotoluene <0.250 ug/L 11/23/16 19:54 JDS SW8260B 4-Methyl-2-pentanone <2.50 ug/L 11/23/16 19:54 JDS SW8260B Acetone <2.50 ug/L 11/23/16 19:54 JDS SW8260B Benzene <0.125 ug/L 11/23/16 19:54 JDS SW8260B Bromobenzene <0.125 ug/L 11/23/16 19:54 JDS SW8260B Bromochloromethane <0.200 ug/L 11/23/16 19:54 JDS SW8260B Bromodichloromethane <0.250 ug/L 11/23/16 19:54 JDS SW8260B Bromoform <0.500 ug/L 11/23/16 19:54 JDS SW8260B Bromomethane <0.500 ug/L 11/23/16 19:54 JDS SW8260B Carbon disulfide <0.500 ug/L 11/23/16 19:54 JDS SW8260B Carbon tetrachloride <0.250 ug/L 11/23/16 19:54 JDS SW8260B Chlorobenzene <0.125 ug/L 11/23/16 19:54 JDS SW8260B Chlorodibromomethane <0.250 ug/L 11/23/16 19:54 JDS SW8260B Chloroethane <0.500 ug/L 11/23/16 19:54 JDS SW8260B Chloroform <0.125 ug/L 11/23/16 19:54 JDS SW8260B Chloromethane <0.500 ug/L 11/23/16 19:54 JDS SW8260B cis-1,2-Dichloroethene <0.250 ug/L 11/23/16 19:54 JDS SW8260B cis-1,3-Dichloropropene <0.250 ug/L 11/23/16 19:54 JDS SW8260B Dibromomethane <0.250 ug/L 11/23/16 19:54 JDS SW8260B Dichlorodifluoromethane <0.250 ug/L 11/23/16 19:54 JDS SW8260B Ethylbenzene <0.250 ug/L 11/23/16 19:54 JDS SW8260B Hexachlorobutadiene <0.250 ug/L 11/23/16 19:54 JDS SW8260B Isopropylbenzene <0.250 ug/L 11/23/16 19:54 JDS SW8260B Page 2 of 16 Fayetteville Division Certificate of Analysis Town of Fremont Date Reported: 12/08/16 Mr. Ray Bostic Project: Monitoring Wells Samples (Nov) Date Received: 11/21/16 532 Davis Mill Road Date Sampled: 11/21/16 Fremont NC, 27830 Sampled By: Client MW 1, grab K6K0936-01 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Ohio Valley m -,p -Xylene <0.500 ug/L 11/23/16 19:54 JDS SW8260B Methylene chloride <0.250 ug/L 11/23/16 19:54 JDS SW8260B Naphthalene <0.200 ug/L 11/23/16 19:54 JDS SW8260B n-Butylbenzene <0.250 ug/L 11/23/16 19:54 JDS SW8260B n-Propylbenzene <0.125 ug/L 11/23/16 19:54 JDS SW8260B o -Xylene <0.250 ug/L 11/23/16 19:54 JDS SW8260B p-Isopropyltoluene <0.250 ug/L 11/23/16 19:54 JDS SW8260B sec-Butylbenzene <0.250 ug/L 11/23/16 19:54 JDS SW8260B Styrene <0.125 ug/L 11/23/16 19:54 JDS SW8260B tert-Butylbenzene <0.250 ug/L 11/23/16 19:54 JDS SW8260B Tetrachloroethene <0.250 ug/L 11/23/16 19:54 JDS SW8260B Toluene <0.250 ug/L 11/23/16 19:54 JDS SW8260B trans-1,2-Dichloroethene <0.250 ug/L 11/23/16 19:54 JDS SW8260B trans-1,3-Dichloropropene <0.500 ug/L 11/23/16 19:54 JDS SW8260B Trichloroethene <0.250 ug/L 11/23/16 19:54 JDS SW8260B Trichlorofluoromethane <0.250 ug/L 11/23/16 19:54 JDS SW8260B Vinyl acetate <2.50 ug/L 11/23/16 19:54 JDS SW8260B Vinyl chloride <0.250 ug/L 11/23/16 19:54 JDS SW8260B Surrogate: 1,2-Dichloroethane-d4 103% 80%-120% 11/23/16 19:54 JDS SW8260B Surrogate: 4-Bromofluorobenzene 98.2% 86%-115% 11/23/16 19:54 JDS SW8260B Surrogate: Dibromolluoromethane 104% 86%-118% 11/23/16 19:54 JDS SW8260B Surrogate: Toluene -d8 98.7% 88%-110% 11/23/16 19:54 JDS SW8260B Total Organic Carbon 3.24 mg/L 11/29/16 14:39 EPT E415.1 MW 2, grab K6K0936-02 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Fayetteville Ammonia as N <0.100 mg/L 11/22/16 10:30 DSK SM 4500 NH3 C-1997 Chloride 19.1 mg/L 11/28/16 15:45 JAW EPA 300.0, Rev. 2.1 (1993) Page 3 of 16 Fayetteville Division Certificate of Analysis Town of Fremont <0.250 ug/L 11/23/16 20:22 JDS Date Reported: 12/08/16 Mr. Ray Bostic <0.250 Project: Monitoring Wells Samples (Nov) 11/23/16 20:22 Date Received: 11/21/16 532 Davis Mill Road 1,1,2,2 -Tetrachloroethane <0.200 ug/L 11/23/16 20:22 Date Sampled: 11/21/16 Fremont NC, 27830 1,1,2 -Trichloroethane <0.250 ug/L 11/23/16 20:22 Sampled By: Client SW8260B 1,1-Dichloroethane <0.125 MW 2, grab 11/23/16 20:22 JDS SW8260B 1,1-Dichloroethene <0.500 K6K0936-02 11/23/16 20:22 JDS Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Miaobac Laboratories, Inc. - Fayetteville 1,2,3-Trichlorobenzene <0.150 ug/L 11/23/16 20:22 Coliform, Fecal <1.0 per 100 mL 11/21/16 16:22 JR SM 9222 D-1997 Depth of Water 20.0 feet 11/21/16 09:30 DED Field Measurement Depth to Water Surface 8.00 feet 11/21/16 09:30 DED Field Measurement Gallons purged 5.9 gallons 11/21/16 09:30 JGP Field Nitrate as N 0.419 mg/L 11/28/16 15:45 JAW EPA 300.0, Rev. 2.1 (1993) pH, Field Test 6.6 pH Units 11/21/16 09:30 JGP SM 4500 H+B-2000 JDS SW8260B 1,2-Dichloroethane <0.250 ug/L (Aqueous) Total Dissolved Solids 220 mg/L 11/29/16 10:30 JR SM 2540 C-1997 H, B Temperature, field 16 °C 11/21/16 09:30 JGP SM 2550 B-2000 Analyzed by: Miaobac Laboratories, Inc. - Ohio Valley 1,1,1,2 -Tetrachloroethane <0.250 ug/L 11/23/16 20:22 JDS SW8260B 1,1,1 -Trichloroethane <0.250 ug/L 11/23/16 20:22 JDS SW8260B 1,1,2,2 -Tetrachloroethane <0.200 ug/L 11/23/16 20:22 JDS SW8260B 1,1,2 -Trichloroethane <0.250 ug/L 11/23/16 20:22 JDS SW8260B 1,1-Dichloroethane <0.125 ug/L 11/23/16 20:22 JDS SW8260B 1,1-Dichloroethene <0.500 ug/L 11/23/16 20:22 JDS SW8260B 1,1-Dichloropropene <0.250 ug/L 11/23/16 20:22 JDS SW8260B 1,2,3-Trichlorobenzene <0.150 ug/L 11/23/16 20:22 JDS SW8260B 1,2,3-Trichloropropane <0.500 ug/L 11/23/16 20:22 JDS SW8260B 1,2,4-Trichlorobenzene <0.200 ug/L 11/23/16 20:22 JDS SW8260B 1,2,4-Trimethylbenzene <0.250 ug/L 11/23/16 20:22 JDS SW8260B 1,2-Dibromo-3-chloropropane <1.00 ug/L 11/23/16 20:22 JDS SW8260B 1,2-Dibromoethane <0.250 ug/L 11/23/16 20:22 JDS SW8260B 1,2 -Dichlorobenzene <0.125 ug/L 11/23/16 20:22 JDS SW8260B 1,2-Dichloroethane <0.250 ug/L 11/23/16 20:22 JDS SW8260B 1,2-Dichloropropane <0.200 ug/L 11/23/16 20:22 JDS SW8260B 1,3,5-Trimethylbenzene <0.250 ug/L 11/23/16 20:22 JDS SW8260B 1,3 -Dichlorobenzene <0.250 ug/L 11/23/16 20:22 JDS SW8260B 1,3-Dichloropropane <0.200 ug/L 11/23/16 20:22 JDS SW8260B 1,4 -Dichlorobenzene <0.125 ug/L 11/23/16 20:22 JDS SW8260B Page 4 of 16 Fayetteville Division Certificate of Analysis Town of Fremont Date Reported: 12/08/16 Mr. Ray Bostic Project: Monitoring Wells Samples (Nov) Date Received: 11/21/16 532 Davis Mill Road Date Sampled: 11/21/16 Fremont NC, 27830 Sampled By: Client Page 5 of 16 MW 2, grab K6K0936-02 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Ohio Valley 2,2-Dichloropropane <0.250 ug/L 11/23/16 20:22 JDS SW8260B 2-Butanone <2.50 ug/L 11/23/16 20:22 JDS SW8260B 2-Chloroethyl vinyl ether <2.00 ug/L 11/23/16 20:22 JDS SW8260B 2-Chlorotoluene <0.125 ug/L 11/23/16 20:22 JDS SW8260B 2-Hexanone <2.50 ug/L 11/23/16 20:22 JDS SW8260B 4-Chlorotoluene <0.250 ug/L 11/23/16 20:22 JDS SW8260B 4-Methyl-2-pentanone <2.50 ug/L 11/23/16 20:22 JDS SW8260B Acetone <2.50 ug/L 11/23/16 20:22 JDS SW8260B Benzene <0.125 ug/L 11/23/16 20:22 JDS SW8260B Bromobenzene <0.125 ug/L 11/23/16 20:22 JDS SW8260B Bromochloromethane <0.200 ug/L 11/23/16 20:22 JDS SW8260B Bromodichloromethane <0.250 ug/L 11/23/16 20:22 JDS SW8260B Bromoform <0.500 ug/L 11/23/16 20:22 JDS SW8260B Bromomethane <0.500 ug/L 11/23/16 20:22 JDS SW8260B Carbon disulfide <0.500 ug/L 11/23/16 20:22 JDS SW8260B Carbon tetrachloride <0.250 ug/L 11/23/16 20:22 JDS SW8260B Chlorobenzene <0.125 ug/L 11/23/16 20:22 JDS SW8260B Chlorodibromomethane <0.250 ug/L 11/23/16 20:22 JDS SW8260B Chloroethane <0.500 ug/L 11/23/16 20:22 JDS SW8260B Chloroform <0.125 ug/L 11/23/16 20:22 JDS SW8260B Chloromethane <0.500 ug/L 11/23/16 20:22 JDS SW8260B cis-1,2-Dichloroethene <0.250 ug/L 11/23/16 20:22 JDS SW8260B cis-1,3-Dichloropropene <0.250 ug/L 11/23/16 20:22 JDS SW8260B Dibromomethane <0.250 ug/L 11/23/16 20:22 JDS SW8260B Dichlorodifluoromethane <0.250 ug/L 11/23/16 20:22 JDS SW8260B Ethylbenzene <0.250 ug/L 11/23/16 20:22 JDS SW8260B Hexachlorobutadiene <0.250 ug/L 11/23/16 20:22 JDS SW8260B Isopropylbenzene <0.250 ug/L 11/23/16 20:22 JDS SW8260B m -,p -Xylene <0.500 ug/L 11/23/16 20:22 JDS SW8260B Methylene chloride <0.250 ug/L 11/23/16 20:22 JDS SW8260B Page 5 of 16 Fayetteville Division Certificate of Analysis Town of Fremont Date Reported: 12/08/16 Mr. Ray Bostic Project: Monitoring Wells Samples (Nov) Date Received: 11/21/16 532 Davis Mill Road Date Sampled: 11/21/16 Fremont NC, 27830 Sampled By: Client MW 2, grab K6K0936-02 Analyte Result Units Analyzed Analyzed By Method Quali£er Analyzed by: Microbac Laboratories, Inc. - Ohio Valley Naphthalene <0.200 ug/L 11/23/16 20:22 JDS SW8260B n-Butylbenzene <0.250 ug/L 11/23/16 20:22 JDS SW8260B n-Propylbenzene <0.125 ug/L 11/23/16 20:22 JDS SW8260B o -Xylene <0.250 ug/L 11/23/16 20:22 JDS SW8260B p-Isopropyltoluene <0.250 ug/L 11/23/16 20:22 JDS SW8260B sec-Butylbenzene <0.250 ug/L 11/23/16 20:22 JDS SW8260B Styrene <0.125 ug/L 11/23/16 20:22 JDS SW8260B tert-Butylbenzene <0.250 ug/L 11/23/16 20:22 JDS SW8260B Tetrachloroethene <0.250 ug/L 11/23/16 20:22 JDS SW8260B Toluene <0.250 ug/L 11/23/16 20:22 JDS SW8260B trans-l,2-Dichloroethene <0.250 ug/L 11/23/16 20:22 JDS SW8260B trans-l,3-Dichloropropene <0.500 ug/L 11/23/16 20:22 JDS SW8260B Trichloroethene <0.250 ug/L 11/23/16 20:22 JDS SW8260B Trichlorofluoromethane <0.250 ug/L 11/23/16 20:22 JDS SW8260B Vinyl acetate <2.50 ug/L 11/23/16 20:22 JDS SW8260B Vinyl chloride <0.250 ug/L 11/23/16 20:22 JDS SW8260B Surrogate: 1,2-Dichloroethane-d4 102% 80%-120% 11/23/16 20:22 JDS SW8260B Surrogate: 4-Bromofluorobenzene 101% 86%-115% 11/23/16 20:22 JDS SW8260B Surrogate: Dibromofluoromethane 102% 86%-118% 11/23/16 20:22 JDS SW8260B Surrogate: Toluene -d8 99.4% 88%-110% 11/23/16 20:22 JDS SW8260B Total Organic Carbon 8.05 mg/L 11/29/16 15:15 EPT E415.1 MW 3, grab K6K0936-03 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Fayetteville Ammonia as N <0.100 mg/L 11/22/16 10:30 DSK SM 4500 NH3 C-1997 Chloride 12.0 mg/L 11/28/16 15:45 JAW EPA 300.0, Rev. 2.1 (1993) Coliform, Fecal <1.0 per 100 mL 11/21/16 16:22 JR SM 9222 D-1997 Depth of Water 15.0 feet 11/21/16 09:51 JGP Field Measurement Page 6 of 16 Fayetteville Division Certificate of Analysis Town of Fremont Date Reported: 12/08/16 Mr. Ray Bostic Project: Monitoring Wells Samples (Nov) Date Received: 11/21/16 532 Davis Mill Road Date Sampled: 11/21/16 Fremont NC, 27830 Sampled By: Client MW 3, grab K6K0936-03 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Fayetteville Depth to Water Surface 6.80 feet 11/21/16 09:51 JGP Field Measurement Gallons purged 4.0 gallons 11/21/16 09:51 JGP Field Nitrate as N <0.0500 mg/L 11/28/16 15:45 JAW EPA 300.0, Rev. 2.1 (1993) Al2 pH, Field Test 5.9 pH Units 11/21/16 09:51 JGP SM 4500 H+B-2000 (Aqueous) Total Dissolved Solids 188 mg/L 11/29/16 10:30 JR SM 2540 C-1997 H, B Temperature, field 10 °C 11/21/16 09:51 JGP SM 2550 B-2000 Analyzed by: Microbac Laboratories, Inc. - Ohio Valley 1,1,1,2 -Tetrachloroethane <0.250 ug/L 11/23/16 20:51 JDS SW8260B 1,1,1 -Trichloroethane <0.250 ug/L 11/23/16 20:51 JDS SW8260B 1,1,2,2 -Tetrachloroethane <0.200 ug/L 11/23/16 20:51 JDS SW8260B 1,1,2 -Trichloroethane <0.250 ug/L 11/23/16 20:51 JDS SW8260B 1,1-Dichloroethane <0.125 ug/L 11/23/16 20:51 JDS SW8260B 1,1-Dichloroethene <0.500 ug/L 11/23/16 20:51 JDS SW8260B 1,1-Dichloropropene <0.250 ug/L 11/23/16 20:51 JDS SW8260B 1,2,3-Trichlorobenzene <0.150 ug/L 11/23/16 20:51 JDS SW8260B 1,2,3-Trichloropropane <0.500 ug/L 11/23/16 20:51 JDS SW8260B 1,2,4-Trichlorobenzene <0.200 ug/L 11/23/16 20:51 JDS SW8260B 1,2,4-Trimethylbenzene <0.250 ug/L 11/23/16 20:51 JDS SW8260B 1,2-Dibromo-3-chloropropane <1.00 ug/L 11/23/16 20:51 JDS SW8260B 1,2-Dibromoethane <0.250 ug/L 11/23/16 20:51 JDS SW8260B 1,2 -Dichlorobenzene <0.125 ug/L 11/23/16 20:51 JDS SW8260B 1,2-Dichloroethane <0.250 ug/L 11/23/16 20:51 JDS SW8260B 1,2-Dichloropropane <0.200 ug/L 11/23/16 20:51 JDS SW8260B 1,3,5-Trimethylbenzene <0.250 ug/L 11/23/16 20:51 JDS SW8260B 1,3 -Dichlorobenzene <0.250 ug/L 11/23/16 20:51 JDS SW8260B 1,3-Dichloropropane <0.200 ug/L 11/23/16 20:51 JDS SW8260B 1,4 -Dichlorobenzene <0.125 ug/L 11/23/16 20:51 JDS SW8260B 2,2-Dichloropropane <0.250 ug/L 11/23/16 20:51 JDS SW8260B 2-Butanone <2.50 ug/L 11/23/16 20:51 JDS SW8260B Page 7 of 16 Town of Fremont Mr. Ray Bostic 532 Davis Mill Road Fremont NC, 27830 Fayetteville Division Certificate of Analysis Project: Monitoring Wells Samples (Nov) Date Reported: 12/08/16 Date Received: 11/21/16 Date Sampled: 11/21/16 Sampled By: Client MW 3, grab K6K0936-03 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Ohio Valley 2-Chloroethyl vinyl ether <2.00 ug/L 11/23/16 20:51 JDS SW8260B 2-Chlorotoluene <0.125 ug/L 11/23/16 20:51 JDS SW8260B 2-Hexanone <2.50 ug/L 11/23/16 20:51 JDS SW8260B 4-Chlorotoluene <0.250 ug/L 11/23/16 20:51 JDS SW8260B 4-Methyl-2-pentanone <2.50 ug/L 11/23/16 20:51 JDS SW8260B Acetone <2.50 ug/L 11/23/16 20:51 JDS SW8260B Benzene <0.125 ug/L 11/23/16 20:51 JDS SW8260B Bromobenzene <0.125 ug/L 11/23/16 20:51 JDS SW8260B Bromochloromethane <0.200 ug/L 11/23/16 20:51 JDS SW8260B Bromodichloromethane <0.250 ug/L 11/23/16 20:51 JDS SW8260B Bromoform <0.500 ug/L 11/23/16 20:51 JDS SW8260B Bromomethane <0.500 ug/L 11/23/16 20:51 JDS SW8260B Carbon disulfide <0.500 ug/L 11/23/16 20:51 JDS SW8260B Carbon tetrachloride <0.250 ug/L 11/23/16 20:51 JDS SW8260B Chlorobenzene <0.125 ug/L 11/23/16 20:51 JDS SW8260B Chlorodibromomethane <0.250 ug/L 11/23/16 20:51 JDS SW8260B Chloroethane <0.500 ug/L 11/23/16 20:51 JDS SW8260B Chloroform <0.125 ug/L 11/23/16 20:51 JDS SW8260B Chloromethane <0.500 ug/L 11/23/16 20:51 JDS SW8260B cis-1,2-Dichloroethene <0.250 ug/L 11/23/16 20:51 JDS SW8260B cis-1,3-Dichloropropene <0.250 ug/L 11/23/16 20:51 JDS SW8260B Dibromomethane <0.250 ug/L 11/23/16 20:51 JDS SW8260B Dichlorodifluoromethane <0.250 ug/L 11/23/16 20:51 JDS SW8260B Ethylbenzene <0.250 ug/L 11/23/16 20:51 JDS SW8260B Hexachlorobutadiene <0.250 ug/L 11/23/16 20:51 JDS SW8260B Isopropylbenzene <0.250 ug/L 11/23/16 20:51 JDS SW8260B m -,p -Xylene <0.500 ug/L 11/23/16 20:51 JDS SW8260B Methylene chloride <0.250 ug/L 11/23/16 20:51 JDS SW8260B Naphthalene <0.200 ug/L 11/23/16 20:51 JDS SW8260B n-Butylbenzene <0.250 ug/L 11/23/16 20:51 JDS SW8260B Page 8 of 16 Fayetteville Division Certificate of Analysis Town of Fremont Date Reported: 12/08/16 Mr. Ray Bostic Project: Monitoring Wells Samples (Nov) Date Received: 11/21/16 532 Davis Mill Road Date Sampled: 11/21/16 Fremont NC, 27830 Sampled By: Client MW 3, grab K6K0936-03 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Ohio Valley n-Propylbenzene <0.125 ug/L 11/23/16 20:51 JDS SW8260B o -Xylene <0.250 ug/L 11/23/16 20:51 JDS SW8260B p-Isopropyltoluene <0.250 ug/L 11/23/16 20:51 JDS SW8260B sec-Butylbenzene <0.250 ug/L 11/23/16 20:51 JDS SW8260B Styrene <0.125 ug/L 11/23/16 20:51 JDS SW8260B tert-Butylbenzene <0.250 ug/L 11/23/16 20:51 JDS SW8260B Tetrachloroethene <0.250 ug/L 11/23/16 20:51 JDS SW8260B Toluene <0.250 ug/L 11/23/16 20:51 JDS SW8260B trans-1,2-Dichloroethene <0.250 ug/L 11/23/16 20:51 JDS SW8260B trans-1,3-Dichloropropene <0.500 ug/L 11/23/16 20:51 JDS SW8260B Trichloroethene <0.250 ug/L 11/23/16 20:51 JDS SW8260B Trichlorofluoromethane <0.250 ug/L 11/23/16 20:51 JDS SW8260B Vinyl acetate <2.50 ug/L 11/23/16 20:51 JDS SW8260B Vinyl chloride <0.250 ug/L 11/23/16 20:51 JDS SW8260B Surrogate:1,2-Dichloroethane-d4 101% 80%-120% 11/23/16 20:51 JDS SW8260B Surrogate: 4-Bromofluorobenzene 96.4% 86%-115% 11/23/16 20:51 JDS SW8260B Surrogate: Dibromofluoromethane 103% 86%-118% 11/23/16 20:51 JDS SW8260B Surrogate: Toluene -d8 97.1% 88%-110% 11/23/16 20:51 JDS SW8260B Total Organic Carbon 3.01 mg/L 11/29/16 15:42 EPT E415.1 MW 4, grab K6K0936-04 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Fayetteville Ammonia as N <0.100 mg/L 11/22/16 10:30 DSK SM 4500 NH3 C-1997 Chloride 24.5 mg/L 11/28/16 15:45 JAW EPA 300.0, Rev. 2.1 (1993) Coliform, Fecal <1.0 per 100 mL 11/21/16 16:22 JR SM 9222 D-1997 Depth of Water 18.0 feet 11/21/16 10:15 JGP Field Measurement Depth to Water Surface 7.00 feet 11/21/16 10:15 JGP Field Measurement Gallons purged 5.4 gallons 11/21/16 10:15 JGP Field Page 9 of 16 Town of Fremont Mr. Ray Bostic 532 Davis Mill Road Fremont NC, 27830 Fayetteville Division Certificate of Analysis Project: Monitoring Wells Samples (Nov) Date Reported: 12/08/16 Date Received: 11/21/16 Date Sampled: 11/21/16 Sampled By: Client MW 4, grab K6K0936-04 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Fayetteville Nitrate as N <0.0500 mg/L 11/28/16 15:45 JAW EPA 300.0, Rev. 2.1 (1993) pH, Field Test 5.3 pH Units 11/21/16 10:15 JGP SM 4500 H+B-2000 (Aqueous) Total Dissolved Solids 194 mg/L 11/29/16 10:30 JR SM 2540 C-1997 H, B Temperature, field 15 °C 11/21/16 10:15 JGP SM 2550 B-2000 Analyzed by: Microbac Laboratories, Inc. - Ohio Valley 1,1,1,2 -Tetrachloroethane <0.250 ug/L 11/23/16 21:20 JDS SW8260B 1,1,1 -Trichloroethane <0.250 ug/L 11/23/16 21:20 JDS SW8260B 1,1,2,2 -Tetrachloroethane <0.200 ug/L 11/23/16 21:20 JDS SW8260B 1,1,2 -Trichloroethane <0.250 ug/L 11/23/16 21:20 JDS SW8260B 1,1-Dichloroethane <0.125 ug/L 11/23/16 21:20 JDS SW8260B 1,1-Dichloroethene <0.500 ug/L 11/23/16 21:20 JDS SW8260B 1,1-Dichloropropene <0.250 ug/L 11/23/16 21:20 JDS SW8260B 1,2,3-Trichlorobenzene <0.150 ug/L 11/23/16 21:20 JDS SW8260B 1,2,3-Trichloropropane <0.500 ug/L 11/23/16 21:20 JDS SW8260B 1,2,4-Trichlorobenzene <0.200 ug/L 11/23/16 21:20 JDS SW8260B 1,2,4-Trimethylbenzene <0.250 ug/L 11/23/16 21:20 JDS SW8260B 1,2-Dibromo-3-chloropropane <1.00 ug/L 11/23/16 21:20 JDS SW8260B 1,2-Dibromoethane <0.250 ug/L 11/23/16 21:20 JDS SW8260B 1,2 -Dichlorobenzene <0.125 ug/L 11/23/16 21:20 JDS SW8260B 1,2-Dichloroethane <0.250 ug/L 11/23/16 21:20 JDS SW8260B 1,2-Dichloropropane <0.200 ug/L 11/23/16 21:20 JDS SW8260B 1,3,5-Trimethylbenzene <0.250 ug/L 11/23/16 21:20 JDS SW8260B 1,3 -Dichlorobenzene <0.250 ug/L 11/23/16 21:20 JDS SW8260B 1,3-Dichloropropane <0.200 ug/L 11/23/16 21:20 JDS SW8260B 1,4 -Dichlorobenzene <0.125 ug/L 11/23/16 21:20 JDS SW8260B 2,2-Dichloropropane <0.250 ug/L 11/23/16 21:20 JDS SW8260B 2-Butanone <2.50 ug/L 11/23/16 21:20 JDS SW8260B 2-Chloroethyl vinyl ether <2.00 ug/L 11/23/16 21:20 JDS SW8260B 2-Chlorotoluene <0.125 ug/L 11/23/16 21:20 JDS SW8260B Page 10 of 16 Town of Fremont Mr. Ray Bostic 532 Davis Mill Road Fremont NC, 27830 Fayetteville Division Certificate of Analysis Project: Monitoring Wells Samples (Nov) Date Reported: 12/08/16 Date Received: 11/21/16 Date Sampled: 11/21/16 Sampled By: Client MW 4, grab K6K0936-04 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Ohio Valley 2-Hexanone <2.50 ug/L 11/23/16 21:20 JDS SW8260B 4-Chlorotoluene <0.250 ug/L 11/23/16 21:20 JDS SW8260B 4-Methyl-2-pentanone <2.50 ug/L 11/23/16 21:20 JDS SW8260B Acetone <2.50 ug/L 11/23/16 21:20 JDS SW8260B Benzene <0.125 ug/L 11/23/16 21:20 JDS SW8260B Bromobenzene <0.125 ug/L 11/23/16 21:20 JDS SW8260B Bromochloromethane <0.200 ug/L 11/23/16 21:20 JDS SW8260B Bromodichloromethane <0.250 ug/L 11/23/16 21:20 JDS SW8260B Bromoform <0.500 ug/L 11/23/16 21:20 JDS SW8260B Bromomethane <0.500 ug/L 11/23/16 21:20 JDS SW8260B Carbon disulfide <0.500 ug/L 11/23/16 21:20 JDS SW8260B Carbon tetrachloride <0.250 ug/L 11/23/16 21:20 JDS SW8260B Chlorobenzene <0.125 ug/L 11/23/16 21:20 JDS SW8260B Chlorodibromomethane <0.250 ug/L 11/23/16 21:20 JDS SW8260B Chloroethane <0.500 ug/L 11/23/16 21:20 JDS SW8260B Chloroform <0.125 ug/L 11/23/16 21:20 JDS SW8260B Chloromethane <0.500 ug/L 11/23/16 21:20 JDS SW8260B cis-1,2-Dichloroethene <0.250 ug/L 11/23/16 21:20 JDS SW8260B cis-1,3-Dichloropropene <0.250 ug/L 11/23/16 21:20 JDS SW8260B Dibromomethane <0.250 ug/L 11/23/16 21:20 JDS SW8260B Dichlorodifluoromethane <0.250 ug/L 11/23/16 21:20 JDS SW8260B Ethylbenzene <0.250 ug/L 11/23/16 21:20 JDS SW8260B Hexachlorobutadiene <0.250 ug/L 11/23/16 21:20 JDS SW8260B Isopropylbenzene <0.250 ug/L 11/23/16 21:20 JDS SW8260B m -,p -Xylene <0.500 ug/L 11/23/16 21:20 JDS SW8260B Methylene chloride <0.250 ug/L 11/23/16 21:20 JDS SW8260B Naphthalene <0.200 ug/L 11/23/16 21:20 JDS SW8260B n-Butylbenzene <0.250 ug/L 11/23/16 21:20 JDS SW8260B n-Propylbenzene <0.125 ug/L 11/23/16 21:20 JDS SW8260B o -Xylene <0.250 ug/L 11/23/16 21:20 JDS SW8260B Page 11 of 16 Fayetteville Division Certificate of Analysis Town of Fremont Date Reported: 12/08/16 Mr. Ray Bostic Project: Monitoring Wells Samples (Nov) Date Received: 11/21/16 532 Davis Mill Road Date Sampled: 11/21/16 Fremont NC, 27830 Sampled By: Client MW 4, grab K6K0936-04 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Ohio Valley p-Isopropyltoluene <0.250 ug/L 11/23/16 21:20 JDS SW8260B sec-Butylbenzene <0.250 ug/L 11/23/16 21:20 JDS SW8260B Styrene <0.125 ug/L 11/23/16 21:20 JDS SW8260B tert-Butylbenzene <0.250 ug/L 11/23/16 21:20 JDS SW8260B Tetrachloroethene <0.250 ug/L 11/23/16 21:20 JDS SW8260B Toluene <0.250 ug/L 11/23/16 21:20 JDS SW8260B trans-l,2-Dichloroethene <0.250 ug/L 11/23/16 21:20 JDS SW8260B trans-l,3-Dichloropropene <0.500 ug/L 11/23/16 21:20 JDS SW8260B Trichloroethene <0.250 ug/L 11/23/16 21:20 JDS SW8260B Trichlorofluoromethane <0.250 ug/L 11/23/16 21:20 JDS SW8260B Vinyl acetate <2.50 ug/L 11/23/16 21:20 JDS SW8260B Vinyl chloride <0.250 ug/L 11/23/16 21:20 JDS SW8260B Surrogate: 1,2-Dichloroethane-d4 103% 80%-120% 11/23/16 21:20 JDS SW8260B Surrogate: 4-Bromofluorobenzene 97.3% 86%-115% 11/23/16 21:20 JDS SW8260B Surrogate: Dibromofluoromethane 103% 86%-118% 11/23/16 21:20 JDS SW8260B Surrogate: Toluene -d8 98.1% 88%-110% 11/23/16 21:20 JDS SW8260B Total Organic Carbon 2.84 mg/L 11/29/16 15:54 EPT E415.1 QC Batch Run - (Microbac Laboratories, Inc. - Fayetteville) Analyte Result Units Source RPD Limit Chloride 12.3 mg/L K6K0936 2 10 Nitrate as N 0.223 mg/L K6K1031 200 Nitrate as N 3.57 mg/L K6K1003 11 200 Nitrate as N 0.109 mg/L K6K0992 106 200 Total Dissolved Solids 114 mg/L K6K0943 5 5 Nitrate as N 0.430 mg/L K6K0936 200 Ammonia as N ND mg/L K6K0875 20 Ammonia as N ND mg/L K6K0944 20 Chloride 23.1 mg/L K6K0992 2 10 Page 12 of 16 Town of Fremont Mr. Ray Bostic 532 Davis Mill Road Fremont NC, 27830 Fayetteville Division Certificate of Analysis Project: Monitoring Wells Samples (Nov) Date Reported: 12/08/16 Date Received: 11/21/16 Date Sampled: 11/21/16 Sampled By: Client QC Batch Run - (Microbac Laboratories, Inc. -Fayetteville) Analyte Result Units Source RPD Limit Chloride 102 mg/L K6K1031 0.8 10 Chloride 5.92 mg/L K6K1003 6 10 QC Batch Run - (Microbac Laboratories, Inc. - 01do Dalley) Analyte Result Units Source RPD Limit Notes and Definitions U Not detected at or above adjusted sample detection limit H Analyte was prepared and/or analyzed outside of the analytical method holding time B Detected in the associated Method Blank Al2 MS/MSD fail recovery, but the LCS passes criteria. * [Undefined) State Certifications: NCDNR #I I NCDOH #37714 Respectfully Submitted �.e21uLL ��cpiGa-fit e� Jeanne Overstreet, Project Manages Thank you for your business. We invite yourfeedback on our level ofservice to you. Please contact the Division Manager, Rob Dermer at 910-864-1920 with any questions. You may also contact J. Trevor Boyce, President alpresident@microbac.com Page 13 of 16 LAS ID# SAMPLE TYPE DATE �TIME COMP GRAB 1 _ ,L 1-. 4 i. 30 m'AdoOOMMNNIN11 ph Fleld: ph Flela: Temp Field 1• Tamp Fleld 2: Water Level 92 Initials-->~ Turnaround time: REGULAR RUSH Comments or Special Hazards: , (� 6 LEC IS DATA FOR REG. COMPLIANCE PURE SEN NO YES WHICH: r 9 Page 14 of 16 I Fayetteville Division 2592 Hope Mills Road — Fayetteville, NC 28306 (910) 864-1920 1864-87 *K6KO936* I C R O VI CHAIN OF CUSTODY RECORD III�� I�III�III�III�UIV�I�I PAGE TYPE OF ANALYSIS PRESERVATION (CODE) :LiEN7 NAME SAODRE55:PON PROJECT! LOCATION! r 4, pp�^n CODE: A =None W !' B = HNO3 (pH 2) • -.a trema irrllk5. CONTACT N: G+z, 5�' o " = H2SO4 (pH<2) + <6°C 1p <6°C D = NaOH + C PHONE: V ai� l/ E = ZN Acetate + <6°C SAMPLED 6Y: e S% 5 — DATE! METHOD OF SHIPMENT: O v -v �. F =HCI G = Sodium Thlo pH PLOW TEMP •C RES. SUL'FIOE r.H��RWE LAS ID# SAMPLE TYPE DATE �TIME COMP GRAB 1 _ ,L 1-. 4 i. 30 m'AdoOOMMNNIN11 ph Fleld: ph Flela: Temp Field 1• Tamp Fleld 2: Water Level 92 Initials-->~ Turnaround time: REGULAR RUSH Comments or Special Hazards: , (� 6 LEC IS DATA FOR REG. COMPLIANCE PURE SEN NO YES WHICH: r 9 Page 14 of 16 I Fayetteville Division 2592 Hope Mills Road - Fayetteville, NC 28306 (910) 864-19201864-8- CHAIN 64-1920!864-8" CHAIN OF CUSTODY RECORD ph Field: ph Field: Temp Field 1: Temp Field 2: Water Level #2 PAGE Comments or Special Hazards: &,, IS DATA FOR REG. COMPLIANCE PURPOSE? NO YES WHICH: Page 15 of 16 a Microbac Laboratories, ,Inc. —Fayetteville Z Monitoring Well Field Sheet .P.V Sampling date: Client: f' Sampled by: Purged by: -A '"��