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HomeMy WebLinkAboutNC0005185_Application_20141124 ' NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial Minor industrial, manufacturing and commercial facilities. Mail the complete application to: ' N. C. Department of Environment and Natural Resources Division of Water Quality / NPDES Unit 1617 Mail Service Center, Raleigh, NC 27699-1617 NPDES Permit Number NC0005185 11RECEIVED/DENS DWR ' Please print or type. ' 1. Contact Information: NOv 2 4 204 P mater Quality Owner Name Magellan Midstream Partners, L.P. lttltlg Sedo0 Facility Name Charlotte II Terminal ' Mailing Address One Williams Center MD 27 City Tulsa ' State / Zip Code OK, 74172 Telephone Number 918-574-7928 ' Fax Number 918-574-7760 e-mail Address Joshua.McDorman@magellanlp.com ' 2. Location of facility producing discharge: Check here if same as above ❑ Street Address or State Road 8026 Mount Holly Road City Charlotte ' State / Zip Code North Carolina, County Mecklenburg ' 3. Operator Information: Name of the firm, consultant or other entity that operates the facility. (Note that this is not referring to the Operator in Responsible Charge or ORC) Name Magellan Midstream Partners, L.P. Mailing Address 7924 Old Mt. Holly Road ' City Charlotte State / Zip Code North Carolina Telephone Number (704) 339-6331 Fax Number ' 4. Ownership Status: ' Federal ❑ State ❑ Private ® Public ❑ Page 1 of 5 GMI 10/08 ' NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial Minor industrial,manufacturing and commercial facilities. ' S. Standard Industrial Classification(SIC) code(s): 5171 RECEIVED/DENR/DWR NOV 2 4 2014 6. Number of employees: 1 Water Quality Section ' 7. Describe the treatment system List all installed waste treatment components with capacities, describe the processes that generate wastewaters. If the space provided is not sufficient attach a separate sheet of paper with the system description. ' An air sparge/soil vapor extraction (AS/SVE) system is currently operating to remediate shallow soil and groundwater from historic petroleum releases at the Terminal. The remediation effort is regulated by the North Carolina Department of Environment and Natural Resources (NCDENR). The SVE system uses blowers to extract soil vapor and some liquids from below the ground surface. The liquids (consisting of groundwater and soil vapor moisture condensate) ' will have dissolved petroleum compounds typically present in gasoline and diesel. The current system consists of a high vacuum blower to remove vapor and liquid from extraction wells, a knockout drum to separate liquids from vapor, and an aboveground storage tank for temporary storage of the recovered groundwater. Proposed additional equipment to be installed to treat ' the groundwater prior to disposal to the NPDES discharge point include an oil/water separator, an air stripper, and up to two carbon vessels. Average flow through the system is anticipated to be approximately 5 gallons per minute (gpm), which includes instantaneous batch discharges of approximately 20 gpm. An Engineering Alternatives Analysis is provided in ' Attachment 1. S. Is facility covered under federal effluent limitation guidelines? No ® Yes ❑ ' If yes, specify the category? 9. Principal products) produced: No products are produced ' Principal raw material(s) consumed: None Briefly describe the manufacturing procces(es): ' No manufacturing occurs at the site, however, the following describes the process which generates the wastewater to be discharged: An AS/SVE system is currently operating to remediate shallow soil and groundwater from historic ' petroleum releases at the site. The SVE system uses blowers to extract soil vapor and some liquids from below the ground surface. The liquids (consisting of groundwater and soil vapor moisture condensate) will have dissolved petroleum compounds typically present in gasoline and diesel. The current system consists of a high vacuum blower to remove vapor and liquid from extraction wells, a ' knockout drum to separate liquids from vapor, and an aboveground storage tank for temporary storage of the recovered groundwater. ' Page 2 of 5 C-MI 10/08 t NPDES PERMIT APPLICATION - SHORT FORM C- Minor Industrial Minor industrial, manufacturing and commercial facilities. 10.Amount of principal product produced or raw material consumed ' specific amounts consumed and/or units of roduction over the last three ears Product Produced or Raw Material Product Produced or Raw Material ' Consumed Consumed AVERAGE PEA per Day 73 gallons 7,200 gallons per Month 2,200 gallons 216,000 gallons ' per Ye 113,000 gallons 1,000,000 gallons ' 11. Frequency of discharge: Continuous ❑ Intermittent If intermittent: Days per week discharge occurs: varies Duration: varies ' 12. Types of wastewater discharged to surface waters only ' Discharge Flow (GALLONS PER DA Sanitary - monthly average 0 Utility water, etc. -monthly average 0 Process water- monthly average 0 ' Stormwater-monthly average 0 Other-monthly average ' Explain: Proposed remediation system 73 discharge Monthly Average 73 ' total discharge (all types) ' 13. Number of separate discharge points: 1 Outfall Identification number(s) 006 14. Name of receiving stream(s) (Provide a map showing the exact location of each outfall, including ' latitude and longitudep. Unnamed tributary to Lone Creek (The proposed remediation system will discharge to the current facility's outfall via a separate pipe connected to the facility's outfall pipe.) t ' Page 3 of 5 C-MI 1 MB 1 ' NPDES PERMIT APPLICATION- SHORT FORM C - Minor Industrial Minor industrial,manufacturing and commercial facilities. ' 15. Effluent Data [for new or proposed discharges] Provide data for the parameters listed. Temperature and pH shall be grab samples,for all other parameters 24-hour composite sampling shall be used. If more than one analysis is reported, report daily maximum and monthly average. If only one analysis is reported, report as daily maximum. AV=:Permittees requesting renewal should complete the table ONLY for the parameters currently monitored. Summarize the ast 3 years of e cent data. Parameter Daily Monthly Units of Maximum Average Measurement Biochemical Oxygen Demand (BOD5) -- -- Chemical Oxygen Demand (COD) -- -- Total Organic Carbon -- -- Total Suspended Solids Ammonia as N Temperature (Summer) 76 -- degrees F ' Temperature (Winter) 75 -- degrees F pH 8.78 -- ' Fecal Coliform (If sanitary waste is N/A N/A N/A present) Total Residual Chlorine (if chlorine is N/A N/A N/A ' used) 16. List all permits,construction approvals and/or applications (check all that apply and provide permit ' numbers or check none if not applicablef. Type Permit Number Type Permit Number ' Hazardous Waste (RCRA) None NESHAPS (CAA) None UIC (SDWA) None Ocean Dumping (MPRSA) None NPDES NC0005185 Dredge or fill (Section 404 or CWA) None PSD (CAA) None Other None Non-attainment program (CAA) None 17. List any chemicals that may be discharged (Please list and explain source and potential amounts.) ' The source is a petroleum groundwater remediation system. Analytical results from a sample collected from the condensate holding tank on March 13, 2014 did not have any detections of petroleum compounds except for MTBE(6.4 ug/L) (Attachment 2). ' The following maximum concentrations have been detected in groundwater samples collected in the area where the remediation system is operating: ' Benzene (16,000 ug/L), toluene (99,000 ug/L), ethylbenzene(1,600 ug/L), Xylenes (26,000 ug/L), MTBE(44,000 ug/L), 1,2-dichloroethane (2,000 ug/L), Napthalene (1,600 ug/L). The concentrations listed above are pre-treatment concentrations and should be considered ' Page 4 of 5 C-MI 10/08 1 NPDES PERMIT APPLICATION - SHORT FORM C - Minor Industrial Minor industrial, manufacturing and commercial facilities. as worst case. The groundwater remediation system condensate will typically resemble the ' March 2014 sample from the holding tank. Groundwater analytical reports from June 2014 are provided in Attachment 3. 18. Is this facility located on Indian country? (check one) Yes ❑ No 1 ' 19. Applicant Certification I certify that I am familiar with the information contained in the application and that to the best of my knowledge and belief such information is true, complete, and accurate. ' H a01w J iC (TTL- VP -�Cyl Printed rtme of Person Signing Title ' 1 d 1 6 2/ ' Signatur of Applicant Date North Carolina General Statute 143-215.6 (b)(2) provides that: Any person who knowingly makes any false statement representation, or certification in any application, record, report, plan, or other document files or required to be maintained under Article 21 or regulations of the Environmental Management Commission implementing that Article, or who falsifies, tampers with, or knowingly renders inaccurate any recording or monitoring device or method required to be operated or maintained under Article 21 or regulations of the Environmental Management Commission implementing that Article, shall be guilty of a misdemeanor punishable by a fine not to exceed $25,000, or by imprisonment not to exceed six months, or by both. (18 U.S.C. Section 1001 provides a punishment by a fine of not more than$25,000 or imprisonment not more than 5 years,or both, for a similar offense.) r Page 5 of 5 GMI 10108 r r r r r r 1 1 r FIGURES r ' Figure 1 Site Location Map Figure 2 Process Flow Diagram i r r r r r r r owg a ' '•f♦ • ty'� • t :'A•e• . • E�4�00,6, ' Qaf1`•: Q' / °Oa P7tk Dy. � t'� ,• • •••,,>�� a'•y ��cV' . . 1, r 1,j av-eh � ^t- • _ ' °\•';BrooklalnDr �t+Z( t k'� �- 41ans P°ndL �°`,'j,• ! TY 1 y <- -a_ _'TO"�S �_�a ;�_. _.• m' i taCen-t` - / �` pl0. " t i. • 4�. •1eN...l�✓. Ims Rd. Charlotte I Terminal LIT to Long Creek ; • ti . . ( , r Outfall 001 ►:•.t �0e;::. '' t• ,-- -- •C`.. • f • (Flows South) t ` ON Approximate Property �:t•. Y, Ma�ktis° f Boundary ids- '^ ►° c\ iia eerwood!Rd' CIT -:�""•:; J,No\! ' r ' � Rd •1. _ Tild'e� -: kirb ; i • g^stead _ • st ' t 5 .�.��`• �%�- ��'r • • `4�/\� •�j « 'tom c� � • 400 0 62 • - i _ r =` Chapel Rd- Moore z• _ • •. - s� F• • Dun`leigh DrCr �� •-i ' - • f • • • • • i �.• • • •z 4 • ave Stone;;;stD :_•ti • . •�—J•.- • _ �:P� .^'-• ` .l , ! 27 / %Wesbr �_St� lads • �1 f 1 01 •`t �:;y�l ook D,. .�• S -�. t, r^ '� i gi D i• J CD V 2. 741 'r David{A oma'' > �- d Cly �•-h E � , m .*r � . NC 0 1.500 ssricige)Rd �r • y�'oi. • + •t 1 -•• �--+ #. •� N•4�.,. i • r Slate GridlOued:F15SW I MI.Island Lake,NC Latitude:35.28306 Longitude:-80.94028 ' Receiving Stream:UT to Long Creek[11-120-(2.5)) Stream Class:WSW Drainage Basin:Catawba River Basin Sub,-Basin:03-08-34 Prepared By: MAGELLAN TERMINAL HOLDINGS, L.P. LEGGETTE,BRASHEARS&GRAHAM,INC. CHARLOTTE TERMINAL I ' LB [�i Professional Groundwater and CHARLOTTE.NORTH CAROLINA£?" Environmental Engineering Services 8 Pine Tree Drive,Suite 250 SITE LOCATION G NPDES PERMIT NC0005185 St Paul,Minnesota 55112 (651)490-1405 E. g3magcharl101t.MXD DATE 1 012 312 0 1 4 FIGURE. 1 FIL �Existinq Remediation Building I Vapor Oto Air Treatment I I iqu SVE Blower I Uouids SVE I I I I Wells I Knockout Drum I Air to Atmosphere — I 1 I Oil/Water Separator I I I Transfer Pump Drum with Overpack I I Flow I ri Discharge to POTW Transfer Pump Air I Stripper Air Stripper p Blower _ Optional Carbon Vessels I Proposed Groundwater Treatment Skid Prepared By: MAGELLAN TERMINAL HOLDINGS, L.P. LEGGETTE,BRASHEARS&GRAHAM,INC. CHARLOTTE TERMINAL II Professional Groundwater and Environmental Engineering Services CHARLOTTE, NORTH CAROLINA 8 Pine Tree Drive.Suite 205 St.Paul,Minnesota 55112 PROCESS FLOW DIAGRAM (651)490-1405 FILE: Charlotte PID 021014.dw DATE: September 2014 1 FIGURE: 2 ' ATTACHMENT 1 ' Engineering Alternatives Analysis 1 1 t MAGELLAN MIDSTREAM PARTNERS,L.P. CHARLOTTE II TERMINAL ENGINEERING ALTERNATIVES ANALYSIS This Engineering Alternatives Analysis (EAA) has been prepared on behalf of Magellan ' Midstream Partners, L.P. (Magellan) in order to request permission to discharge treated groundwater from the groundwater remediation system at Magellan's Charlotte II Terminal (Terminal) to the current NPDES permit (Permit #NC0005185) held by the terminal. The Terminal is located at 7924 Mount Holly Road and the groundwater remediation system equipment building is located on the adjoining property at 8026 Mount Holly Road in Charlotte, Mecklenberg County, North Carolina. The proposed remediation system discharge will ' discharge to the existing Terminal's outfall location via a separate pipe connected to the Terminal's outfall pipe. A Site Location Map is attached as Figure 1. Remediation System Description: Magellan is currently operating an air sparge/soil vapor extraction (AS/SVE) system to remediate shallow soil and groundwater from historic petroleum releases at the Terminal. The remediation effort is regulated by the North Carolina Department of Environment and Natural Resources(NCDENR). ' The SVE system uses blowers to extract soil vapor and some liquids from below the ground surface. The liquids (consisting of groundwater and soil vapor moisture condensate) will have dissolved petroleum compounds typically present in gasoline and diesel. The current ' system consists of a high vacuum blower to remove vapor and liquid from extraction wells, a knockout drum to separate liquids from vapor, and an aboveground storage tank for temporary storage of the recovered groundwater. Proposed additional equipment to be installed to treat the groundwater prior to disposal to the NPDES discharge point includes an oil/water separator, an air stripper, and up to two carbon vessels. Figure 2 is attached to provide a process flow diagram for the existing extraction system and proposed treatment system. ' Applicant: Applicant Name: Magellan Midstream Partners, L.P. Mailing Address: One Williams Center MD 27 Tulsa, OK 74172 ' Contact Person: Joshua McDorman (918) 574-7928 1 1 t Facili : Facility Name: Magellan Charlotte II Terminal ' Facility Address: 8026 Mt. Holly Road Mecklenburg County ' Charlotte,NC 28214 Contact Person: Mark Bowen (704)339-6331 EAA Preaarer: I Preparer Name: Leggette, Brashears&Graham, Inc. Preparer Address: 8 Pine Tree Drive, Suite 250 St. Paul, MN 55112 Contact Person: Rachelle Busser(651) 558-9226 , Remediation System Flow Projections: Extraction rates may increase or decrease throughout the year due to a fluctuating groundwater ' table. Because of this variability, an estimated average design-flow rate would be approximately 5 gallons per minute (gpm), which includes instantaneous batch discharges of approximately 20 gpm, and an estimated annual discharge of 1 million gallons per year. ' Technologically Feasible Alternatives Analysis: The following alternatives have been evaluated: , • Connection to an existing wastewater treatment plant — A request to connect to the , Charlotte-Mecklenburg publicly owned treatment works (POTW) was submitted on February 11, 2014. The Charlotte-Mecklenburg POW is not currently accepting connections and the request was denied; therefore this alternative is infeasible. , • Land application—land application is infeasible based on land constraints. • Infiltration galleries — infiltration galleries were discussed as a potential alternative with the NCDENR. According to the NCDENR, infiltration galleries were used more in the ' past and/or typically more along the coast for groundwater remediation. Infiltration galleries require a separate underground injection control (UIC) permit, and are generally discouraged by the agency for remediation. The soil type at the Terminal, predominantly ' silt and clays, are less conducive to infiltration than sandy soils and would require large surface area to be effective for the proposed flow rates. For the reasons listed above, infiltration galleries are not considered further at this time. ' • In-situ groundwater remediation wells — The current remediation system utilizes air sparge (AS) technology as an in-situ groundwater remediation technology. Soil vapor extraction (SVE) and catalytic oxidation systems are used in conjunction with the AS ' system to capture and treat fugitive volatile organic carbon (VOC) emissions generated by the AS system. Occasionally moisture condensate and groundwater build-up or infiltrate the SVE system—and it is for this water that the NPDES permit modification is ' being requested. Other forms of in-situ treatments, such as in-situ chemical oxidation 2 ' 1 CISCO) and thermal treatments are not recommended due to potential risks to buried ' infrastructure such as pipelines. • Closed-loop groundwater remediation wells - These types of wells present the same issues discussed with "infiltration galleries"above. ' Economic Feasibility of Alternatives: ' Due to current existing infrastructure, land uses, limited land availability, and regulatory agency constraints, discharge options for treated moisture condensate/groundwater at the Terminal are very limited. The alternatives discussed above are not feasible at this time; therefore an ' economic feasibility evaluation of alternatives was not conducted. 1 1 1 3 1 1 1 ATTACHMENT 2 ' March 13, 2014 Condensate Tank Analytical Report 1 1 1 1 1 Pace Analytical Services,Inc. 0 9800 Kincey Ave. Suite 100 ace"IXical Huntersville,NC 28078 www.peats&CDM (704)875-9092 March 21, 2014 1 ' Mr.Thomas Garrison Excel Environmental 625 Huntsman Court ' Gastonia, NC 28054 ' RE: Project: Charlotte 11 2013068 Pace Project No.: 92193404 ' Dear Mr. Garrison: Enclosed are the analytical results for sample(s)received by the laboratory on March 14, 2014. The ' results relate only to the samples included in this report. Results reported herein conform to the most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless otherwise noted in the body of the report. Analyses were performed at the Pace Analytical Services location indicated on the sample analyte page for analysis unless otherwise footnoted. Ifou have any y questions concerning this report, please feel free to contact me. 1 Sincerely, ' Kevin Herring kevin.herring@pacelabs.com ' Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,Inc.. Page 1 of 13 Paee Analytical Services,Inc. ' aceAmlXical a 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 j wM»:pemWs.com (704)875-9092 , 1 CERTIFICATIONS ' Project: Charlotte II 2013068 Pace Project No.: 92193404 ' Charlotte Certification IDs 9800 Kincey Ave.Ste 100,Huntersville,NC 28078 Florida/NELAP Certification#:E87627 North Carolina Drinking Water Certification#:37706 Kentucky UST Certification#:84 ' North Carolina Field Services Certification#:5342 West Virginia Certification#:357 North Carolina Wastewater Certification#:12 Virginia/VELAP Certification#:460221 South Carolina Certification#:99006001 1 1 REPORT OF LABORATORY ANALYSIS ' This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,Inc.. Page 2 of 13 ' Pace Analytical Services,Inc. • 9800 Kincey Ave. Suite 100 ceAwly� '�' Huntersville,NC 28078 wwe pamlabscom (704)875-9092 ' SAMPLE SUMMARY Project: Charlotte 11 2013068 ' Pace ProjectNo.: 92193404 Lab ID Sample ID Matrix Date Collected Date Received 92193404001 C.T.-3.13.14 Water 03113/14 09:00 03114/14 13:45 t 1 REPORT OF LABORATORY ANALYSIS ' This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,Inc.. Page 3 of 13 Pace Analytical S• Ices,Inc. ' CeI`11/QlIVAf• 9800 Kincey Ave. Suite 100 f Huntersvllle,NC 28078 WWW. &c0" (704)875-9092 SAMPLE ANALYTE COUNT ' Project: Charlotte 112013068 Pace Project No.: 92193404 , Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92193404001 C.T.-3.13.14 EPA 16648 CLW 1 PASI-C ' EPA 625 RES 17 PASI-C SM 6200B CAH 10 PASI-C 1 REPORT OF LABORATORY ANALYSIS ' This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,Inc.. Page 4 of 13 ' Pace Analytical Services,Inc. • 9800 Kincey Ave. Suite 100 ace"Iytical Huntersville,NC 28078 ' s+vspecMabsoom (704)875-9092 ' ANALYTICAL RESULTS Project: Charlotte II 2013068 Pace Project No.: 92193404 Sample: C.T.-3.13.14 Lab ID: 92193404001 Collected: 03/13/14 09:00 Received: 03/14/14 13:45 Matrix:Water Report Parameters Results Units Limit MDL DF Prepared Analyzed CAS No. Qual HEM,Oil and Grease Analytical Method:EPA 1664B Oil and Grease 6.6 mg/L 5.0 1.1 1 03/18/14 11:15 ' 625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625 4-Chloro-3-methylphenol ND ug/L 5.0 3.7 1 03/17/14 13:00 03/20/14 00:47 59-50-7 2-Chlorophenol ND ug/L 5.0 1.3 1 03/17/14 13:00 03/20/14 00:47 95-57-8 ' 3,3'-Dichlorobenzidine ND ug/L 25.0 2.1 1 03/17/14 13:00 03/20/14 00:47 91-94-1 2,4-Dichlorophenol ND ug/L 5.0 1.7 1 03/17/14 13:00 03/20/14 00:47 120-83-2 2,4-Dimethylphenol ND ug/L 10.0 1.2 1 03/17/14 13:00 03/20/14 00:47 105-67-9 4,6-Dinitro-2-methylphenol ND ug/L 20.0 2.6 1 03/17/14 13:00 03/20/14 00:47 53452-1 ' 2,4-Dinitrophenol ND ug/L 50.0 9.0 1 03/17/14 13:00 03/20/14 00:47 51-28-5 2-Methylphenol(o-Cresol) ND ug/L 5.0 1.6 1 03/17/14 13:00 03/20/14 00:47 95-48-7 3&4-Methylphenol(m&p Cresol) ND ug/L 10.0 2.0 1 03/17/14 13:00 03/20/14 00:47 2-Nitrophenol ND ug/L 5.0 0.91 1 03/17/14 13:00 03/20/14 00:47 88-75-5 ' 4-Nitrophenol ND ug/L 50.0 4.1 1 03/17/14 13:00 03/20/14 00:47 100-02-7 Pentachlorophenol ND ug/L 10.0 4.6 1 03/17/14 13:00 03/20/14 00:47 87-86-5 Phenol ND ug/L 5.0 1.9 1 03/17/14 13:00 03/20/14 00:47 108-95-2 2,4,6-Trichlorophenol ND ug/L 10.0 1.3 1 03/17/14 13:00 03/20/14 00:47 88-06-2 t Surrogates Phenol-d6(S) 34 % 10-120 1 03/17/14 13:00 03/20/14 00:47 13127-88-3 2-Fluorophenol(S) 44 % 10-120 1 03/17/14 13:00 03/20/14 00:47 367-12-4 2,4,6-Tribromophenol(S) 103 % 10-137 1 03/17/14 13:00 03/20/14 00:47 118-79-6 ' 602 Volatiles by Method 6200 Analytical Method:SM 6200B Benzene ND ug/L 1.0 1.0 1 03/21/14 00:22 71-43-2 Ethylbenzene ND ug/L 1.0 1.0 1 03/21/14 00:22 100-41-4 ' Methyl-tert-butyl ether 6.4 ug/L 1.0 1.0 1 03/21/14 00:22 163404-4 Naphthalene ND ug/L 2.0 2.0 1 03/21/14 00:22 91-20-3 Toluene ND ug/L 1.0 1.0 1 03/21/14 00:22 108-88-3 m&p-Xylene ND ug/L 2.0 2.0 1 03/21/14 00:22 179601-23-1 ' o-Xylene ND ug/L 1.0 1.0 1 03/21/14 00:22 95-47-6 Surrogates 4-Bromofluorobenzene(S) 98 % 70-130 1 03/21/14 00:22 460-00-4 1,2-Dichloroethane-d4(S) 101 % 70-130 1 03/21/14 00:22 17060-07-0 ' Toluene-d8(S) 99 % 70-130 1 03/21/14 00:22 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/21/2014 04:47 PM without the written consent of Pace Analytical Services,Inc.. Page 5 of 13 Pace Analytical Services,Inc. ' aceAnalytical a 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 ' www.pacelebs.eom (704)875-9092 QUALITY CONTROL DATA , Project: Charlotte II 2013068 Pace Project No.: 92193404 QC Batch: GGSWI6980 Analysis Method: EPA 1664B QC Batch Method: EPA 1664B Analysis Description: 1664 HEM,Oil and Grease Associated Lab Samples: 92193404001 ' METHOD BLANK: 1159100 Matrix: Water Associated Lab Samples: 92193404001 Blank Reporting ' Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 03/18/14 11:14 LABORATORY CONTROL SAMPLE: 1159101 ' Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers ' Oil and Grease mg/L 40 36.7 92 78-114 MATRIX SPIKE SAMPLE: 1159102 ' 92193546001 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Oil and Grease mg/L ND 40 39.3 88 78-114 ' 1 REPORT OF LABORATORY ANALYSIS ' This report shall not be reproduced,except in full, Date:03/21/2014 04:47 PM without the written consent of Pace Analytical Services,Inc.. Page 6 of 13 ' Pace Analytical Services,Inc. e 9800 KinceyAve. Suite 100 cekdytical Huntersville,NC 28078 ' www4eoele6s com (704)875-9092 ' QUALITY CONTROL DATA Project: Charlotte II 2013068 ' Pace Project No.: 92193404 QC Batch: MSV/26160 Analysis Method: SM 62008 QC Batch Method: SM 6200B Analysis Description: 602 by 6200B ' Associated Lab Samples: 92193404001 METHOD BLANK: 1161347 Matrix: Water Associated Lab Samples: 92193404001 ' Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Benzene ug/L ND 1.0 03/20/14 21:54 Ethylbenzene ug/L ND 1.0 03/20/14 21:54 m8,p-Xylene ug/L ND 2.0 03/20114 21:54 Methyl-tert-butyl ether ug/L ND 1.0 03/20114 21:54 Naphthalene ug/L ND 2.0 03/20114 21:54 ' o-Xylene ug/L ND 1.0 03/20/14 21:54 Toluene ug/L ND 1.0 03/20/14 21:54 1,2-Dichkxoethane-d4(S) % 100 70-130 03/20/14 21:54 4-Bromofluorobenzene(S) % 99 70-130 03/20/14 21:54 Toluene-d8(S) % 99 70-130 03/20114 21:54 LABORATORY CONTROL SAMPLE: 1161348 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Benzene ug/L 50 50.8 102 60-140 Ethylbenzene ug/L 50 49.9 100 60-140 ' m&p-Xylene ug/L 100 103 103 60-140 Methyl-tert-butyl ether ug/L 50 51.9 104 60-140 Naphthalene ug/L 50 53.7 107 60-140 o-Xylene ug/L 50 51.4 103 60-140 ' Toluene ug/L 50 49.8 100 60-140 1,2-Dichloroethane-d4(S) % 97 70-130 4-Bromofluorobenzene(S) % 101 70-130 Toluene-d8(S) % 102 70-130 1 ' REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date.03/21/2014 04.47 PM without the written consent of Pace Analytical Services,Inc.. Page 7 of 13 Pace Analytical Services,Inc. ' C@ w__ �-�I• 98W Kincey Ave. Suite 100 kik Huntersvilb,NC 28078 WWW4Mee1ebse0m (704)875-9092 ' 1 QUALITY CONTROL DATA ' Project: Charlotte 112013068 Pace Project No.: 92193404 , QC Batch: OEXT/26529 Analysis Method: EPA 625 QC Batch Method: EPA 625 Analysis Description: 625 MSS Associated Lab Samples: 92193404001 ' METHOD BLANK: 1158648 Matrix: Water Associated Lab Samples: 92193404001 Blank Reporting ' Parameter Units Result Limit Analyzed Qualifiers 2,4,6-Trichlorophenol ug/L ND 10.0 03/19/14 20:05 2,4-Dichlorophenol ug/L ND 5.0 03/19/14 20:05 ' 2,4-Dimethylphenol ug/L ND 10.0 03/19/14 20:05 2,4-Dinitrophenol ug/L ND 50.0 03/19/14 20:05 2-Chlorophenol ug/L ND 5.0 03/19/14 20:05 2-Methylphenol(o-Cresol) ug/L ND 5.0 03/19/14 20:05 , 2-Nitrophenol ug/L ND 5.0 03/19/14 20:05 3&4-Methylphenol(m&p Cresol) ug/L ND 10.0 03/19/14 20:05 3,3'-Dichlorobenzidine ug/L ND 25.0 03/19/14 20:05 4,6-Dinitro-2-methylphenol ug/L ND 20.0 03119/14 20:05 ' 4-Chloro-3-methylphenol ug/L ND 5.0 03/19/14 20:05 4-Nitrophenol ug/L ND 50.0 03/19/14 20:05 Pentachlorophenol ug/L ND 10.0 03/19/14 20:05 Phenol ug/L ND 5.0 03/19/14 20:05 ' 2,4,6-Tribromophenol(S) % 98 10-137 03/19/14 20:05 2-Fluorobiphenyl(S) % 90 15-120 03/19/14 20:05 2-Fluorophenol(S) % 48 10-120 03/19/14 20:05 Nitrobenzene-d5(S) % 82 10-120 03/19/14 20:05 ' Phenol-d6(S) % 30 10-120 03/19/14 20:05 Terphenyl-d14(S) % 90 11-131 03/19/14 20:05 LABORATORY CONTROL SAMPLE: 1158649 ' Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers 2,4,6-Trichlorophenol ug/L 50 45.6 91 37-144 ' 2,4-Dichlorophenol ug/L 50 50.0 100 1-191 2,4-Dimethylphenol ug/L 50 45.2 90 32-119 2,4-Dinitrophenol ug/L 250 247 99 1-181 2-Chlorophenol ug/L 50 44.7 89 23-134 , 2-Methylphenol(o-Cresol) ug/L 50 41.3 83 25-150 2-Nitrophenol ug/L 50 45.2 90 29-182 3&4-Methylphenol(m&p Cresol) ug/L 50 38.9 78 25-150 3,3'-Dichlorobenzidine ug/L 100 97.0 97 1-262 ' 4,6-Dinitro-2-methylphenol ug/L 100 96.8 97 1-181 4-Chloro-3-methylphenol ug/L 100 107 107 22-147 4-Nitrophenol ug/L 250 131 52 1-132 Pentachlorophenol ug/L 100 94.2 94 14-176 ' Phenol ug/L 50 22.9 46 5-112 2,4,6-Tribromophenol(S) % 118 10-137 2-Fluorobiphenyl(S) % 91 15-120 2-Fluorophenol(S) % 54 10-120 ' REPORT OF LABORATORY ANALYSIS ' This report shall not be reproduced,except in full, Date:03/21/2014 04:47 PM without the written consent of Pace Analytical Services,Inc.. Page 8 of 13 Pau Ana"al Services,Inc. q,,,,/ ^,/• 9800 Kincey Ave. SuRe 100 riPi/`11IC1/ VL1/ HuntersvUb,NC 28078 rrmpWole6acorn (704)875-9092 I QUALITY CONTROL DATA Project: Charlotte 11 2013068 ' Pace Project No.: 92193404 LABORATORY CONTROL SAMPLE: 1158649 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Nitrobenzene-d5(S) % 88 10-120 Phenol-d6(S) % 39 10-120 Terphenyl-d`14(S) % 83 11-131 ' MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 1158650 1158651 MS MSD ' 92193441001 Spike Spike MS MSD MS MSD %Rec Max Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qua[ 2,4,6-Trichlorophenol ug/L ND 100 100 46.0 41.0 46 41 37-144 12 30 2,4-Dichkxophenol ug/L ND 100 100 39.5 37.5 39 38 1-191 5 30 2,4-Dimethylphenol ug/L ND 100 100 37.0 33.5 37 33 32-119 10 30 2,4-Dinitrophenol ug/L ND 500 500 361 300 72 60 1-181 18 30 2-Chlorophenol ug/L ND 100 100 37.8 40.2 38 40 23-134 6 30 t 2-Methylphenol(o-Cresol) ug/L ND 100 100 33.2 35.7 33 36 25-150 7 30 2-Nitrophenol ug/L ND 100 100 38.4 37.0 38 37 29-182 4 30 3&4-Methylphenol(m&p ug/L ND 100 100 32.8 35.5 32 34 25-150 8 30 Cresol) 3,Y-Dichlorobenzidine ug/L ND 200 200 134 144 67 72 1-262 7 30 ' 4,6-Dinitro-2-methylphenol ug/L ND 200 200 159 128 79 64 1-181 21 30 4-Chloro-3-methylphenol ug/L ND 200 200 97.9 98.9 49 49 22-147 1 30 4-Nitrophenol ug/L ND 500 500 242 276 48 55 1-132 13 30 Pentachlorophenol ug/L ND 200 200 144 135 72 67 14-176 7 30 Phenol ug/L ND 100 100 24.2 28.9 24 29 5-112 18 30 2,4,6-Tribromophenol(S) % 81 77 10-137 2-Fluorob iphenyl(S) % 40 36 15-120 2-Fluorophenol(S) % 27 28 10-120 ' Nitrobenzene-l5(S) % 37 36 10-120 Phenol-d6(S) % 21 21 10-120 Terphenyl-d14(S) % 77 58 11-131 1 ' REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03121/2014 04:47 PM without the written consent of Pace Analytical Services,Inc.. Page 9 of 13 Pace Analytical Services,Inc. ' CI I ,le 9800 KlnceyAve. Suite 100 Q �i c Huntersville,NC 28078 ' erM:pe&ftb& M (704)875-9092 QUALIFIERS ' Project: Charlotte 11 2013068 Pace Project No.: 92193404 ' DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to changes in sample preparation,dilution of ' the sample aliquot,or moisture content. ND-Not Detected at or above adjusted reporting limit. J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. ' PRL-Pace Reporting Limit. RL-Reporting Limit. S-Surrogate ' 1,2-Diphenylhydrazine(8270 listed analyte)decomposes to Azobenzene. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) ' DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up ' U-Indicates the compound was analyzed for,but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. ' Acid preservation may not be appropriate for 2-Chloroethylvinyl ether,Styrene,and Vinyl chloride. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TNI-The NELAC Institute. LABORATORIES , PASI-C Pace Analytical Services-Charlotte 1 1 REPORT OF LABORATORY ANALYSIS ' This report shall not be reproduced,except in full, Date:03/21/2014 04:47 PM without the written consent of Pace Analytical Services,Inc.. Page 10 of 13 Pace Analytical Services,Inc. / • 9800 KinceyAve. Suite 100 C@//�`U,,,,IXicaI Huntersville,NC 28078 wwwp8w1abs.com (704)875-9092 ' QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Charlotte 11 2013068 ' Pace Project No.: 92193404 Analytical Lab ID Sample ID OC Batch Method QC Batch Analytical Method Batch 92193404001 C.T.-3.13.14 EPA 16648 GCSV/16980 92193404001 C.T.-3.13.14 EPA625 OEXT/26529 EPA625 MSSV/8889 92193404001 C.T.-3.13.14 SM 62008 MSV/26160 1 t ' REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:03/21/2014 04:47 PM without the written consent of Pace Analytical Services,Inc.. Page 11 of 13 UOCument IVame: UUGUnrGn�r�cviacu. vca cnivc� �..,.+ ' P,1eeAllalylrc��! Sam le Condition Upon Receipt SCUR Pae 1 of 2 Document Number: Issuing Authority: F-CHR-CS-03-rev.13 Pace Huntersville Quality Office Client Name: V—' x/c t I ' Courier: E] Fed Ex❑ UPS[] len USPS❑ Commercial[] Pace Other Optional ' Custody Seal on Cooler/Box Present: ❑ yes ❑ Seals intact: ❑ yes ❑ no Proj, Due Date: Proj, Name: Packing Material: ❑ Bubble Wrap ❑ Bubt"ags ❑ None ❑ Other Thermometer Used:IR Gun T1102 T601 Type of IC . WW t Blue None-----DSamples on ice,cooling process has begun ' Temp Correction Factor T1102: No Correction T1301: No Correction 7 � Biological Tissue is Frozen: Yes No N/A Date and Initi Is of person examining ' Corrected Cooler Temp.: �-+ 'C contents:� I ly Temp should be above freezing to 6'C Comments: Chain of Custody Present: --ffY-es ❑No ❑NIA 1. , Chain of Custody Filled Out: (qyos ❑No ❑N/A 2. Chain of Custodya in uis e o Sampler Name&Signature on COC: ON. 0 W 4. , Samples Arrived within Hold Time: F3 rues ❑No ❑N/A 5. Short Hold Time Analysis <72hr): Dyes Duro ❑NIA 6. ' Rush Tum Around Time Requested: Dyes Opo ❑NIA 7, Sufficient Volume: 0fe-. []No ❑N/A g. Correct Containers Used: ' ve's 11 No ❑N/A 9. ' -Pace Containers Used: es 0 N ❑NIA Containers Intact: es ❑No ❑NIA 10. Filtered volume received for Dissolved tests Oyes ❑No 11. ' Sample Labels match COC: ❑Yes jQN6"11WA 12. (Q bL 1-4 -Includes date/time/ID/Analysis Matrix: L,if All containers needing preservation have been checked. w I I All containers needing preservation are found to be in ❑Yes ONo IP1VfA ' compliance with EPA recommendation. / exceptions: VOA, coliform,TOC,O&G,WI-DRO(water) -es ❑No Sam les checked for dechlorination: Yes ❑No ❑N/A 14. ' Heads ace in VOA Vials >6mm): ❑Yes ❑N/A 15. Trip Blank Present: Ores ❑NoNIA 16. Trip Blank Custody Seals Present ❑Yes ❑No ❑N/ , Pace Trip Blank Lot#(if purchased): Client Notification/Resolution: Field Data Required? Y J N ' Person Contacted: Date/Time: Comments/Resolution: I 1 ' SCURFDte: SRF Review:Review: Date. 3 ` WO# : 92193484 WL 'Note: Whenever there is a discrepancy affecting North Carolina cimpliance samples,a copy of this form will be sent to the North Carolina DEHNR Certification Office(Le out of hold,incorrect preservative,out of temp, 92193404 incorrect containers) _ Page 12 of 13 ' CHAIN-OF-CUSTODY/Analytical Request Document Z5 ,1The Chain-o(-Custody is a LEGAL DOCUMENT.All relevant6vant fields must Ue completed accurately. M.Malees.arn en Section A Sectiont Required Client Information: R Project Inforrrtetion: Section C Pop: 1 °t t d ImglCe Iniormatlon: 1725205 Company: Report To: 'M Atlantan: Address:(n.2 Copy TO: Company Name: REGULATORY AGENCY Address. NPDES ' GROUNDWATER DRINKING WATER Emall To: Purchase Order No. au Quote _ Reference: UST RCRA OTHER Fax: Project Nemo: Pecs P r ger: ManaSite Location d � r Requested Due DetoITAT: _ Project Number:.., Pau Prom.s: STATE: Requested Analysis Filtered(YIN) Section D Matrix Codes Required Client lnlrxmation MATRIX r CODs Drinking Water DW COLLECTED Preservatives i 3 Water WT Waste WaterWW COMPOSITE COMPOSITE (- 4. Product P m START ENOIORAe w Z Sowsolid SL SAMPLE ID al OL 0 Cr rn (AZ 0.B J.-) Aires AR Cl < Z H Y Sampo IDs MUST BE UNIQUE Tissue OT Cl Wa F t (A� / ,l�(� ;�L * Odter OT X F Z Z a p U (,.l(/ _ 1 � � cOi O c a � DATE TIME DATE TIME 2 2 S Z Z S y Pace Project No./Lab I.D. 2 �� i 3 4 3 B 7 8 9 10 11 1Z ADDITIONAL COMMENTS RELINQUISHED BY l AFFILIATION DATE TIME ACCEPTED BY I AFFILIATION DATE TIME SAMPLE CONDITIONS SAMPLER NAME AND SIGNATURE U T- i ORIGINAL PRINT Name of SAMPLER: N SIGNATURE of SAMPLER. DATE Sig d(MMID /YY) L1 •Important Note'By Spning this farm you are acceptirrp Pace's NET 30 day payment term and agraeft to fete cheNea of 15%per month for any it anus rot paid within 30 days F-ALL-0-020rev.07.15-May-2007 ATTACHMENT 3 iJune 2014 Groundwater Analytical Reports 1 1 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 OESC' Fax (615) 758-5859 L•A•B S•C•1•E•N•C E•S Tax I.D. 62-0814289 Est. 1970 ' Mr. Michael Susca Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 Report Summary ' Wednesday July 02, 2014 Report Number: L706285 ' Samples Received: 06/24/14 Client Project: 2013068 ' Description: RFP #2013068 ' The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have an questions regarding this data package, please do not hesitate to caly l. Entire Report Reviewed By: Terrie Fudg , ESC Vresentative La bora tory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BIO041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02 ' Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. Page 1 of 13 t 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 0 (615) 758-5858 ESC 1-800-767-5859 Fax (615) 758-5859 , L-A B 3•C•1•E-Wc E-5 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS ' Mr. Michael Susca July 02, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ' ESC Sample # L706285-01 Date Received June 24, 2014 Description RFP #2013068 Site ID Sample ID MW-06 ' Project # 2013068 Collected By T. Garrison Collection Date 06/23/14 16:00 Parameter Result Det. Limit Units Method Date Dil. ' Nitrate 0.14 0.10 mg/1 300.0 06/24/14 1 Sulfate 38. 5.0 mg/l 300.0 06/24/14 1 Alkalinity 180 20. mg/1 2320 B-2011 06/25/14 1 ' Methane 0.49 0.010 mg/1 RSK175 06/28/14 1 Ethane BDL 0.013 mg/1 RSK175 06/28/14 1 Ethene BDL 0.013 mg/l RSK175 06/28/14 1 Volatile Organics ' Benzene 0.013 0.0010 mg/1 624 06/27/14 1 1,2-Dichloroethane BDL 0.0010 mg/1 624 06/27/14 1 Ethylbenzene BDL 0.0010 mg/1 624 06/27/14 1 Methyl tert-butyl ether BDL 0.0050 mg/1 624 06/27/14 1 Naphthalene BDL 0.0050 mg/1 624 06/27/14 1 ' Toluene BDL 0.0050 mg/1 624 06/27/14 1 Xylenes, Total BDL 0.0050 mg/1 624 06/27/14 1 Surrogate Recovery Toluene-d8 97.3 % Rec. 624 06/27/14 1 Dibromofluoromethane 100. % Rec. 624 06/27/14 1 ' a,a,a-Trifluorotoluene 98.4 % Rec. 624 06/27/14 1 4-Bromofluorobenzene 92.5 % Rec. 624 06/27/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:18 Revised: 07/02/14 14:06 Page 2 of 13 ' 1 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 *ESC 1-800-767-5859 Fax (615) 758-5859 L-A B s-C•i-E-N-C E-s Tax I.D. 62-0814289 Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca July 02, 2014 Leggette, Brashears' & Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ESC Sample # L706285-02 Date Received June 24, 2014 Description RFP #2013068 Site ID ' Sample ID MW-08 Project # 2013068 Collected By T. Garrison Collection Date 06/23/14 16:20 ' Parameter Result Det. Limit Units Method Date Dil. Volatile Organics Benzene BDL 0.025 mg/1 624 06/27/19 25 1,2-Dichloroethane BDL 0.025 mg/1 624 06/27/14 25 Ethylbenzene BDL 0.025 mg/l 624 06/27/14 25 ' Methyl tert-butyl ether 44. 5.0 mg/l 624 06/30/14 1000 Naphthalene BDL 0.12 mg/l 624 06/27/14 25 Toluene BDL 0.12 mg/l 624 06/27/14 25 Xylenes, Total BDL 0.12 mg/l 624 06/27/14 25 Surrogate Recovery ' Toluene-d8 99.4 8 Rec. 624 06/27/14 25 Dibromofluoromethane 99.0 8 Rec. 624 06/27/14 25 a,a,a-Trifluorotoluene 96.7 8 Rec. 624 06/27/14 25 4-Bromofluorobenzene 95.9 % Rec. 624 06/27/14 25 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:18 Revised: 07/02/14 14:06 ' Page 3 of 13 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 *ESC Fax (615) 758-5859 L A B 5•C-I-E-N C E-S Tax I.D. 62-0819289 Est. 1970 REPORT OF ANALYSIS Mr. Michael Susca July 02, 2014 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 'Date Received June 24, 2014 ESC Sample # L706285-03 Description RFP #2013068 Site ID Sample ID MW-13R ' Project # 2013068 Collected By T. Garrison Collection Date 06/23/14 14:45 Parameter Result Det. Limit Units Method Date Dil. ' Volatile Organics Benzene BDL 0.0010 mg/1 624 06/27/14 1 1,2-Dichloroethane BDL 0.0010 mg/l 624 06/27/14 1 Ethylbenzene BDL 0.0010 mg/1 624 06/27/14 1 ' Methyl tert-butyl ether BDL 0.0050 mg/1 624 06/30/14 1 Naphthalene BDL 0.0050 mg/1 624 06/27/14 1 Toluene BDL 0.0050 mg/l 624 06/27/14 1 Xylenes, Total BDL 0.0050 mg/1 624 06/27/14 1 Surrogate Recovery Toluene-d8 98.2 8 Rec. 624 06/27/14 1 , Dibromofluoromethane 100. % Rec. 624 06/27/14 1 a,a,a-Trifluorotoluene 99.1 8 Rec. 624 06/27/14 1 4-Bromofluorobenzene 95.8 % Rec. 624 06/27/14 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) , Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:18 Revised: 07/02/14 14:06 Page 4 of 13 ' 1 1 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 *ESC' Fax (615) 758-5859 L-A B S•C-I-E-N-C E-S Tax I.D. 62-0819289 Est. 1970 REPORT OF ANALYSIS Mr. Michael Susca July 02, 2014 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ESC Sample # L706285-04 Date Received June 24, 2014 Description RFP #2013068 Site ID ' Sample ID OW-35 Project # 2013068 Collected By T. Garrison Collection Date 06/23/14 16:30 ' Parameter Result Det. Limit Units Method Date Dil. Volatile Organics Benzene BDL 0.0010 mg/1 624 06/27/14 1 1,2-Dichloroethane BDL 0.0010 mg/l 624 06/27/14 1 Ethylbenzene BDL 0.0010 mg/l 624 06/27/14 1 ' Methyl tert-butyl ether BDL 0.0050 mg/1 624 06/30/14 1 Naphthalene HDL 0.0050 mg/l 624 06/27/14 1 Toluene BDL 0.0050 mg/1 624 06/27/14 1 Xylenes, Total BDL 0.0050 mg/1 624 06/27/14 1 Surrogate Recovery ' Toluene-dB 98.6 % Rec. 624 06/27/14 1 Dibromofluoromethane 98.3 8 Rec. 624 06/27/14 1 a,a,a-Trifluorotoluene 99.1 % Rec. 624 06/27/14 1 4-Bromofluorobenzene 92.4 % Rec. 624 06/27/14 1 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:18 Revised: 07/02/14 14:06 ' Page 5 of 13 1 1 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 (615) 758-5658 1-800-767-5859 *ESC Fax (615) 758-5859 , L�A B S-C•I-E•N,C E-S Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS , Mr. Michael Susca July 02, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 'Date Received June 24, 2019 ESC Sample # L706285-05 Description RFP #2013068 Site ID Sample ID OW-37 ' Project # 2013068 Collected By T. Garrison Collection Date 06/23/14 15:45 Parameter Result Det. Limit Units Method Date Dil. ' Benzene 1.3 0.020 mg/1 624 06/28/14 20 Ethylbenzene BDL 0.020 mg/1 624 06/28/14 20 Toluene BDL 0.10 mg/1 624 06/28/14 20 Xylenes, Total BDL 0.060 mg/1 624 06/28/14 20 Methyl tert-butyl ether 0.024 0.020 mg/1 624 06/28/14 20 Naphthalene BDL 0.10 mg/1 624 06/28/14 20 Surrogate Recovery Toluene-d8 99.1 8 Rec. 624 06/28/14 20 Dibromofluoromethane 94.2 % Rec. 624 06/28/14 20 a,a,a-Trifluorotoluene 100. % Rec. 624 06/28/14 20 ' 4-Bromofluorobenzene 94.9 % Rec. 624 06/28/14 20 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:18 Revised: 07/02/14 14:06 Page 6 of 13 , 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 *ESC Fax (615) 758-5859 ' L-A B S.C•1•E•N-C E•E Tax I.D. 62-0814289 • - Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca July 02, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ' ESC Sample 8 : L706285-06 Date Received June 24, 2014 Description RFP $2013068 Site ID ' Sample ID OW-49 Project N 2013068 Collected By T. Garrison Collection Date 06/23/14 12:15 ' Parameter Result Det. Limit Units Method Date Dil. Volatile Organics Benzene BDL 0.0010 mg/l 624 06/27/14 1 1,2-Dichloroethane BDL 0.0010 mg/l 624 06/27/14 1 Ethylbenzene BDL 0.0010 mg/1 624 06/27/14 1 ' Methyl tert-butyl ether BDL 0.0050 mg/1 624 06/30/14 1 Naphthalene BDL 0.0050 mg/l 624 06/27/14 1 Toluene BDL 0.0050 mg/1 624 06/27/14 1 Xylenes, Total BDL 0.0050 mg/1 624 06/27/14 1 Surrogate Recovery ' Toluene-d8 99.9 % Rec. 624 06/27/14 1 Dibromofluoromethane 101. 8 Rec. 624 06/27/14 1 a,a,a-Trifluorotoluene 99.0 8 Rec. 624 06/27/14 1 4-Bromofluorobenzene 96.0 % Rec. 624 06/27/14 1 1 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:18 Revised: 07/02/14 14:06 ' Page 7 of 13 1 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 *ESC (615) 758-5658 1-800-767-5859 Fax (615) 758-5859 ' L-A B S•C-1•E•N•C-E•S Tax I.D. 62-0819289 Est. 1970 REPORT OF ANALYSIS ' Mr. Michael Susca July 02, 2014 Leggette, Brashears S Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ' ESC Sample # L706285-07 Date Received June 29, 2014 Description RFP #2013068 Site ID Sample ID OW-48R , Project # 2013068 Collected By T. Garrison Collection Date 06/23/14 15:15 Parameter Result Det. Limit Units Method Date Dil. ' Nitrate 0.12 0.10 mg/l 300.0 06/24/14 1 Sulfate 21. 5.0 mg/l 300.0 06/24/14 1 Alkalinity 24. 20. mg/1 2320 B-2011 06/25/14 1 ' Methane BDL 0.010 mg/1 RSK175 06/28/14 1 Ethane BDL 0.013 mg/1 RSK175 06/28/14 1 Ethene BDL 0.013 mg/l RSK175 06/28/14 1 Volatile Organics , Benzene BDL 0.0010 mg/1 624 06/27/14 1 1,2-Dichloroethane BDL 0.0010 mg/l 624 06/27/14 1 Ethylbenzene BDL 0.0010 mg/1 624 06/27/14 1 Methyl tert-butyl ether BDL 0.0050 mg/l 624 06/27/14 1 Naphthalene BDL 0.0050 mg/l 624 06/27/14 1 Toluene BDL 0.0050 mg/l 624 06/27/14 1 ' Xylenes, Total BDL 0.0050 mg/l 624 06/27/14 1 Surrogate Recovery Toluene-d8 100. 8 Rec. 624 06/27/14 1 Dibromofluoromethane 100. % Rec. 624 06/27/14 1 ' a,a,a-Trifluorotoluene 97.8 % Rec. 624 06/27/14 1 4-Bromofluorobenzene 93.3 8 Rec. 624 06/27/14 1 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:18 Revised: 07/02/14 14:06 Page 8 of 13 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 *ESC1-800-767-5859 ' Fax (615) 758-5859 L-A-8 S•C•I•E•N-c E•8 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Mr. Michael Susca July 02, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample # L706285-08 Date Received June 24, 2014 Description RFP #2013068 Site ID ' Sample ID OW-JOR Project # 2013068 Collected By T. Garrison Collection Date 06/23/14 11:15 ' Parameter Result Det. Limit Units Method Date Dil. Volatile Organics Benzene BDL 0.0010 mg/1 624 06/27/14 1 1,2-Dichloroethane BDL 0.0010 mg/1 624 06/27/14 1 Ethylbenzene BDL 0.0010 mg/1 624 06/27/14 1 ' Methyl tert-butyl ether BDL 0.0050 mg/1 624 06/27/14 1 Naphthalene BDL 0.0050 mg/1 624 06/27/14 1 Toluene BDL 0.0050 mg/1 624 06/27/14 1 Xylenes, Total BDL 0.0050 mg/1 624 06/27/14 1 Surrogate Recovery ' Toluene-d8 98.3 % Rec. 624 06/27/14 1 Dibromofluoromethane 99.3 % Rec. 624 06/27/14 1 a,a,a-Trifluorotoluene 97.2 % Rec. 624 06/27/14 1 4-Bromofluorobenzene 94.8 S Rec. 624 06/27/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:18 Revised: 07/02/14 14:06 ' Page 9 of 13 1 1 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 E S C Fax (615) 758-5859 ' L•A-B 5•C•1•E•N-CE•S Tax I.D. 62-0814289 MEWMIM Est, 1970 REPORT OF ANALYSIS ' Mr. Michael Susca July 02, 2014 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ' Date Received June 29, 2014 ESC Sample # L706285-09 Description RFP #2013068 Site ID Sample ID OW-55 ' Project # 2013068 Collected By T. Garrison Collection Date 06/23/14 15:30 Parameter Result Det. Limit Units Method Date Dil. , volatile Organics Benzene BDL 0.010 mg/1 624 06/27/14 10 1,2-Dichloroethane BDL 0.010 mg/l 624 06/27/14 10 Ethylbenzene BDL 0.010 mg/1 624 06/27/14 10 Methyl tert-butyl ether 11. 2.5 mg/1 624 06/30/14 500 Naphthalene BDL 0.050 mg/1 624 06/27/14 10 Toluene BDL 0.050 mg/1 624 06/27/14 10 Xylenes, Total BDL 0.050 mg/1 624 06/27/14 10 Surrogate Recovery Toluene-d8 99.5 % Rec. 624 06/27/14 10 , Dibromofluoromethane 100. % Rec. 624 06/27/14 10 a,a,a-Trifluorotoluene 96.6 % Rec. 624 06/27/14 10 4-Bromofluorobenzene 94.4 % Rec. 624 06/27/14 10 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:18 Revised: 07/02/14 14:06 Page 10 of 13 ' 1 t ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615} 758-5858 1-800-767-5859 *ESC Fax (615) 758-5859 ' L-AB S•C•I•E•NCE•S Tax I.D. 62-0814289 • Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca July 02, 2014 Leggette, Brashears 6 Graham - ET 6 Executive Drive; Ste 109 t Farmington, CT 06032 ESC Sample # L706285-10 Date Received June 24, 2014 Description RFP #2013068 Site ID ' Sample ID OW-57 Project # 2013068 Collected By T. Garrison Collection Date 06/23/14 11:30 Parameter Result Det. Limit Units Method Date Dil. Nitrate 0.20 0.10 mg/l 300.0 06/24/14 1 Sulfate BDL 5.0 mg/1 300.0 06/24/14 1 Alkalinity 150 20. mg/1 2320 B-2011 06/25/14 1 ' Methane BDL 0.010 mg/l RSK175 06/28/14 1 Ethane BDL 0.013 mg/l RSK175 06/28/14 1 Ethene BDL 0.013 mg/1 RSK175 06/28/14 1 ' Volatile Organics Benzene 0.010 0.010 mg/l 624 06/27/14 10 1,2-Dichloroethane BDL 0.010 mg/l 624 06/27/14 10 Ethylbenzene BDL 0.010 mg/l 624 06/27/14 10 Methyl tert-butyl ether 6.5 1.2 mg/l 624 06/30/14 250 ' Naphthalene BDL 0.050 mg/l 624 06/27/14 10 Toluene BDL 0.050 mg/l 624 06/27/14 10 Xylenes, Total BDL 0.050 mg/l 624 06/27/14 10 Surrogate Recovery Toluene-d8 98.3 % Rec. 624 06/27/14 10 Dibromofluoromethane 98.5 % Rec. 624 06/27/14 10 ' a,a,a-Trifluorotoluene 98.0 % Rec. 624 06/27/14 10 4-Bromofluorobenzene 93.8 % Rec. 624 06/27/14 10 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:18 Revised: 07/02/14 14:06 ' Page 11 of 13 12065Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 *ESC Fax (615) 758-5859 t L,A B B•C•1•E•N-C E-5 Tax I.D. 62-0819289 Est. 1970 Mr. Michael Susca REPORT OF ANALYSIS ' July 02, 2019 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ' ESC Sample # L706285-11 Date Received June 29, 2014 Description RFP #2013068 Site ID Sample ID Ow-58 ' Project # 2013068 Collected By T. Garrison Collection Date 06/23/14 14:40 Parameter Result Det. Limit Units Method Date Dil. Volatile Organics Benzene BDL 0.0010 mg/l 624 06/28/14 1 1,2-Dichloroethane BDL 0.0010 mg/l 624 06/28/14 1 Ethylbenzene BDL 0.0010 mg/1 624 06/28/14 1 ' Methyl tert-butyl ether BDL 0.0050 mg/l 624 06/28/14 1 Naphthalene BDL 0.0050 mg/1 624 06/28/14 1 Toluene BDL 0.0050 mg/l 624 06/28/14 1 Xylenes, Total BDL 0.0050 mg/l 624 06/28/14 1 Surrogate Recovery Toluene-d8 98.1 % Rec. 624 06/28/14 1 ' Dibromofluoromethane 99.9 % Rec. 624 06/28/14 1 a,a,a-Trifluorotoluene 98.6 8 Rec. 624 06/28/14 1 4-Bromofluorobenzene 96.2 % Rec. 624 06/28/14 1 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:18 Revised: 07/02/14 14:06 Page 12 of 13 ' 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 *ESC 1-800-767-5859 Fax (615) 758-5859 L•A-B 5-C•1•E•N•C E•S Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Mr. Michael Susca July 02, 2014 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample N L706285-12 Date Received June 24, 2014 Description RFP 1)2013068 Site ID Sample ID DOP-1 Project M 2013068 Collected By T. Garrison Collection Date 06/23/14 11:45 Parameter Result Det. Limit Units Method Date Dil. Volatile Organics Benzene 0.010 0.010 mg/1 624 06/28/19 10 1,2-Dichloroethane BDL 0.010 mg/l 624 06/28/14 10 ' Ethylbenzene BDL 0.010 mg/1 624 06/28/14 10 Methyl tert-butyl ether 5.9 0.50 mg/1 624 06/29/14 100 Naphthalene BDL 0.050 mg/1 624 06/28/14 10 Toluene BDL 0.050 mg/1 624 06/28/14 10 Xylenes, Total BDL 0.050 mg/l 624 06/28/14 10 Surrogate Recovery ' Toluene-d8 97.2 % Rec. 624 06/28/14 10 Dibromofluoromethane 101. 8 Rec. 624 06/28/14 10 a,a,a-Trifluorotoluene 97.6 8 Rec. 624 06/28/14 10 4-Bromofluorobenzene 95.1 8 Rec. 624 06/28/14 10 1 1 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:18 Revised: 07/02/14 14:06 ' Page 13 of 13 1 Summary of Remarks For Samples Printed ' 07/02/14 at 14:06:30 TSR Signing Reports: 064 ' Sample: L706285-01 Account: LEGBGFCT Received: 06/24/14 09:00 Due Date: 07/02/14 00:00 RPT Date: 06/30/14 15:18 ' Sample: L706285-02 Account: LEGBGFCT Received: 06/24/14 09:00 Due Date: 07/02/14 00:00 RPT Date: 06/30/14 15:18 Sample: 1706285-03 Account: LEGBGFCT Received: 06/24/14 09:00 Due Date: 07/02/14 00:00 RPT Date: 06/30/14 15:18 ' Sample: L706285-04 Account: LEGBGFCT Received: 06/24/14 09:00 Due Date: 07/02/14 00:00 RPT Date: 06/30/14 15:18 Sample: L706285-05 Account: LEGBGFCT Received: 06/24/14 09:00 Due Date: 07/02/14 00:00 RPT Date: 06/30/14 15:18 Sample: L706285-06 Account: LEGBGFCT Received: 06/24/14 09:00 Due Date: 07/02/14 00:00 RPT Date: 06/30/14 15:18 ' Sample: L706285-07 Account: LEGBGFCT Received: 06/24/14 09:00 Due Date: 07/02/14 00:00 RPT Date: 06/30/14 15:18 Sample: L706285-08 Account: LEGBGFCT Received: 06/24/14 09:00 Due Date: 07/02/14 00:00 RPT Date: 06/30/14 15:18 Sample: L706285-09 Account: LEGBGFCT Received: 06/24/14 09:00 Due Date: 07/02/14 00:00 RPT Date: 06/30/14 15:18 ' Sample: L706285-10 Account: LEGBGFCT Received: 06/24/14 09:00 Due Date: 07/02/14 00:00 RPT Date: 06/30/14 15:18 Received one RSR vial empty Sample: L706285-11 Account: LEGBGFCT Received: 06/24/14 09:00 Due Date: 07/02/14 00:00 RPT Date: 06/30/14 15:18 ' Sample: L706285-12 Account: LEGBGFCT Received: 06/24/14 09:00 Due Date: 07/02/14 00:00 RPT Date: 06/30/14 15:18 1 1 1 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 E S C1-B00-767-5859 ' Fax (615) 758-5859 L-A B B•C-I•E-N-C E-3 Tax I.D. 62-0814289 Est. 1970 ' Mr. Michael Susca Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 Report Summary ' Friday August 22, 2014 Report Number: L706716 ' Samples Received: 06/25/14 Client Project: ' Description: RFP #2013068 ' The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. 1 Entire Report Reviewed By: Terrie Fudg , ESC I resentative Laboratory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, ' FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BIO041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, NII - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02 ' Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided ' in laboratory standard operating procedures: 060302, 060303, and 060304. 1 ' Page 1 of 17 1 1 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 OESC Fax (615) 758-5859 ' L-A B S-C•I•E•N C E•S Tax I.D. 62-0819289 Est. 1970 Mr. Michael Susca REPORT OF ANALYSIS ' August 22, 2019 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ' ESC Sample # L706716-01 Date Received June 25, 2019 Description RFP #2013068 Site ID Sample ID MW-2 ' Project # Collected By Brady Glover Collection Date 06/24/14 08:50 Parameter Result Det. Limit Units Method Date Dil. ' Benzene 2.6 0.025 mg/l 624 06/26/14 25 Ethylbenzene 0.84 0.025 mg/l 624 06/26/14 25 Toluene 0.14 0.12 mg/l 624 06/26/14 25 Xylenes, Total 1.6 0.075 mg/l 624 06/26/14 25 ' Methyl tert-butyl ether 0.031 0.025 mg/l 624 06/26/14 25 Naphthalene 0.38 0.12 mg/l 624 06/26/14 25 Surrogate Recovery Toluene-d8 101. % Rec. 624 06/26/14 25 Dibromofluoromethane 94.4 % Rec. 624 06/26/14 25 a,a,a-Trifluorotoluene 105. 8 Rec. 624 06/26/14 25 , 4-Bromofluorobenzene 94.4 8 Rec. 624 06/26/14 25 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/22/14 15:36 Printed: 08/22/14 15:36 Page 2 of 17 ' 1 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-B00-767-5859 *ESC' Fax (615) 758-5859 L-A-8 8•0•1•E•N-C E•5 Tax I.D. 62-0819289 Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca August 22, 2014 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ESC Sample # L706716-02 Date Received June 25, 2014 Description RFP #2013068 Site ID ' Sample ID OW-1 Project # Collected By Brady Glover Collection Date 06/24/14 09:15 ' Parameter Result Det. Limit Units Method Date Dil. Free Carbon Dioxide 51. 20. mg/1 4500002 D-201 06/28/14 1 Benzene BDL 0.0033 mg/1 624 06/26/14 10 Ethylbenzene BDL 0.010 mg/1 624 06/26/14 10 Toluene BDL 0.050 mg/l 624 06/26/14 10 Xylenes, Total BDL 0.030 mg/l 624 06/26/14 10 Methyl tert-butyl ether 0.24 0.010 mg/1 624 06/26/14 10 Naphthalene BDL 0.050 mg/1 624 06/26/14 10 Surrogate Recovery ' Toluene-d8 103. % Rec. 624 06/26/14 10 Dibromofluoromethane 96.3 8 Rec. 624 06/26/14 10 a,a,a-Trifluorotoluene 103. 8 Rec. 624 06/26/14 10 4-Bromofluorobenzene 98.4 % Rec. 624 06/26/14 10 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/22/14 15:36 Printed,: 08/22/14 15:36 Page 3 of 17 1 1 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 4VESC Fax (615) 758-5859 ' L-A 9 9•C•1-E-N C E•3 Tax I.D. 62-0814289 Est. 1970 Mr. Michael Susca REPORT OF ANALYSIS ' August 22, 2019 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 , ESC Sample # : L706716-03 Date Received June 25, 2014 Description RFP #2013068 Site ID . Sample ID OW-15 ' Project # Collected By Brady Glover Collection Date 06/24/14 09:30 Parameter Result Det. Limit Units Method Date Dil. ' Free Carbon Dioxide 160 100 mg/1 4500002 D-201 06/28/14 5 Benzene 4.5 0.25 mg/1 624 06/28/14 250 Ethylbenzene 1.1 0.25 mg/l 624 06/28/14 250 Toluene 15. 1.2 mg/l 624 06/28/14 250 ' Xylenes, Total 14. 0.75 mg/l 624 06/28/14 250 Methyl tert-butyl ether BDL 0.25 mg/l 624 06/28/14 250 Naphthalene 1.6 1.2 mg/1 624 06/28/14 250 Surrogate Recovery Toluene-d8 99.3 8 Rec. 624 06/28/14 250 ' Dibromofluoromethane 97.0 8 Rec. 624 06/28/14 250 a,a,a-Trifluorotoluene 104. % Rec. 624 06/28/14 250 4-Bromofluorobenzene 95.4 % Rec. 624 06/28/14 250 1 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) , Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/22/14 15:36 Printed: 08/22/14 15:36 Page 4 of 17 ' 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 *ESC Fax (615) 758-5859 L-A B 5•C•I•E•N-C E•5 Tax I.D. 62-0814289 Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca August 22, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ESC Sample # L706716-04 DateReceived June 25, 2014 Description RFP #2013068 Site ZD ' Sample ID OW-16 Project # Collected By Brady Glover Collection Date 06/24/14 10:40 ' Parameter Result Det. Limit Units Method Date Dil. Free Carbon Dioxide 51. 20. mg/l 4500002 D-201 06/28/14 1 Benzene BDL 5.0 mg/1 624 06/28/14 5000 Ethylbenzene BDL 5.0 mg/1 624 06/28/14 5000 ' Toluene 52. 25. mg/1 624 06/28/14 5000 Xylenes, Total 26. 15. mg/1 624 06/28/14 5000 Methyl tert-butyl ether BDL 5.0 mg/l 624 06/28/14 5000 Naphthalene BDL 25. mg/1 624 06/28/14 5000 Surrogate Recovery Toluene-d8 103. % Rec. 624 06/28/14 5000 Dibromofluoromethane 104. 8 Rec. 624 06/28/14 5000 a,a,a-Trifluorotoluene 99.4 8 Rec. 624 06/28/14 5000 4-Bromofluorobenzene 94.9 8 Rec. 624 06/28/14 5000 1 1 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) : Note The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/22/14 15:36 Printed: 08/22/14 15:36 ' Page 5 of 17 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 E S C Fax (615) 758-5859 ' L•A-B S.C.i•E•N•C.E•5 Tax I.D. 62-0819289 Est. 1970 Mr. Michael Susca REPORT OF ANALYSIS ' August 22, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 , ESC Sample # L706716-05 Date Received June 25, 2019 Description RFP #2013068 Site ID Sample ID OW-10 ' Project # Collected By Brady Glover Collection Date 06/24/14 10:50 Parameter Result Det. Limit Units Method Date Dil. ' Free Carbon Dioxide 76. 20. mg/l 4500002 D-201 06/28/14 1 Benzene 16. 5.0 mg/l 624 06/28/14 5000 Ethylbenzene BDL 5.0 mg/l 624 06/28/14 5000 ' Toluene 82. 25. mg/l 624 06/28/14 5000 Xylenes, Total BDL 15. mg/l 624 06/28/14 5000 Methyl tert-butyl ether 34. 5.0 mg/l 624 06/28/14 5000 Naphthalene BDL 25. mg/l 624 06/28/14 5000 Surrogate Recovery Toluene-d8 105. 8 Rec. 624 06/28/14 5000 , Dibromofluoromethane 107. 8 Rec. 624 06/28/14 5000 a,a,a-Trifluorotoluene 102. % Rec. 624 06/28/14 5000 4-Bromofluorobenzene 96.3 % Rec. 624 06/28/14 5000 1 1 t 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/22/14 15:36 Printed: 08/22/14 15:36 Page 6 of 17 ' 1 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 *ESC1-800-767-5859 ' Fax (615) 758-5859 L-A B 5•C-1•E-N-C E'S Tax I.D. 62-0814289 Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca August 22, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ESC Sample # L706716-06 Date Received June 25, 2014 Description RFP #2013068 Site ID ' Sample ID OW-14 Project # Collected By Brady Glover Collection Date 06/24/14 11:20 ' Parameter Result Det. Limit Units Method Date Dil. Free Carbon Dioxide 150 100 mg/l 4500002 D-201 06/28/14 5 Benzene 2.6 2.5 mg/l 624 06/28/14 2500 Ethylbenzene BDL 2.5 mg/l 624 06/28/14 2500 ' Toluene 48. 12. mg/l 624 06/28/14 2500 Xylenes, Total BDL 7.5 mg/l 624 06/28/14 2500 Methyl tert-butyl ether BDL 2.5 mg/l 624 06/28/14 2500 Naphthalene BDL 12. mg/l 624 06/28/14 2500 Surrogate Recovery ' Toluene-d8 104. 8 Rec. 624 06/28/14 2500 Dibromofluoromethane 107. 8 Rec. 624 06/28/14 2500 a,a,a-Trifluorotoluene 101. % Rec. 624 06/28/14 2500 4-Bromofluorobenzene 98.1 % Rec. 624 06/28/14 2500 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/22/14 15:36 Printed: 08/22/14 15:36 Page 7 of 17 1 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 *ESC Fax (615) 758-5859 ' L-A�B S•C•I•E•N�C E-S Tax I.D. 62-0814289 LVVVV� • Est. 1970 Mr. Michael Susca REPORT OF ANALYSIS ' August 22, 2019 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ' ESC Sample # L706716-07 Date Received June 25, 2019 Description RFP #2013066 Site ID Sample ID OW-11R ' Project # Collected By Brady Glover Collection Date 06/24/14 11:00 Parameter Result Det. Limit Units Method Date Dil. ' Nitrate HDL 0.10 mg/l 300.0 06/26/14 1 Sulfate BDL 5.0 mg/l 300.0 06/26/14 1 Alkalinity BDL 20. mg/l 2320 B-2011 06/28/14 1 ' Free Carbon Dioxide 140 20. mg/l 4500002 D-201 06/28/14 1 Methane BDL 0.010 mg/l RSK175 06/28/14 1 Ethane BDL 0.013 mg/l RSK175 06/28/14 1 Ethene BDL 0.013 mg/l RSK175 06/28/14 1 ' Benzene 7.8 1.0 mg/1 624 06/28/14 1000 Ethylbenzene 1.4 1.0 mg/l 624 06/28/14 1000 Toluene 99. 5.0 mg/l 624 06/28/14 1000 Xylenes, Total 7.5 3.0 mg/l 624 06/28/14 1000 ' Methyl tert-butyl ether BDL 1.0 mg/l 624 06/28/14 1000 Naphthalene BDL 5.0 mg/l 624 06/28/14 1000 Surrogate Recovery Toluene-d8 103. 8 Rec. 624 06/28/14 1000 Dibromofluoromethane 104. 8 Rec. 624 06/28/14 1000 ' a,a,a-Trifluorotoluene 103. 8 Rec. 624 06/28/14 1000 4-Bromofluorobenzene 98.4 % Rec. 624 06/28/14 1000 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/22/14 15:36 Printed: 08/22/14 15:36 Page 8 of 17 ' 1 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 *ESC 1-800-767-5859 Fax (615) 758-5859 L-A-8 8•C-I•E•N,C E•B Tax I.D. 62-0814289 + Est. 1970 REPORT OF ANALYSIS Mr. Michael Susca August 22, 2019 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample # L706716-08 Date Received June 25, 2019 Description RFP #2013068 Site ID Sample ID OW-7AR Project # Collected By Brady Glover Collection Date 06/24/14 13:20 ' Parameter Result Det. Limit Units Method Date Dil. Free Carbon Dioxide 160 20. mg/l 4500002 D-201 06/28/14 1 Benzene 2.5 0.050 mg/l 624 06/28/14 50 Ethylbenzene 1.6 0.050 mg/l 624 06/28/14 50 Toluene 0.85 0.25 mg/l 624 06/28/14 50 Xylenes, Total 3.5 0.15 mg/l 624 06/28/14 50 Methyl tert-butyl ether 2.7 0.050 mg/l 624 06/28/14 50 Naphthalene 0.53 0.25 mg/l 624 06/28/14 50 Surrogate Recovery Toluene-d8 104. % Rec. 624 06/28/14 50 Dibromofluoromethane 101. % Rec. 624 06/28/14 50 a,a,a-Trifluorotoluene 100. % Rec. 624 06/28/14 50 4-Bromofluorobenzene 100. 8 Rec. 624 06/28/14 50 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/22/14 15:36 Printed: 08/22/14 15:36 ' Page 9 of 17 1 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859*ESC ' Fax (615)5) 758 758-5859 L•A-B 5•C•I•E•N-C E•S Tax I.D. 62-0814289 Est. 1970 Mr. Michael Susca REPORT OF ANALYSIS ' August 22, 2019 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 , ESC Sample # L706716-09 Date Received June 25, 2019 Description RFP #2013068 Site ID Sample ID Ow-12 ' Project # Collected By Brady Glover Collection Date 06/24/14 13:15 Parameter Result Det. Limit Units Method Date Dil. ' Free Carbon Dioxide 110 20. mg/l 4500002 D-201 06/28/14 1 Benzene 1.4 0.050 mg/l 624 06/28/14 50 Ethylbenzene 1.0 0.050 mg/l 624 06/28/14 50 ' Toluene BDL 0.25 mg/l 624 06/28/14 50 Xylenes, Total 1.4 0.15 mg/l 624 06/28/14 50 Methyl tert-butyl ether 7.8 0.050 mg/l 624 06/28/14 50 Naphthalene 0.46 0.25 mg/l 624 06/28/14 50 Surrogate Recovery Toluene-d8 104. % Rec. 624 06/28/14 50 ' Dibromofluoromethane 102. % Rec. 624 06/28/14 50 a,a,a-Trifluorotoluene 101. % Rec. 624 06/28/14 50 4-Bromofluorobenzene 97.3 8 Rec. 624 06/28/14 50 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/22/14 15:36 Printed: 08/22/14 15:36 Page 10 of 17 ' 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 OESC Fax (615) 758-5859 L-A-8 S•C•1•E•N•C E•S Tax I.D. 62-0814289 Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca August 22, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample # L706716-10 Date Received June 25, 2014 Description RFP #2013068 Site ID Sample ID OW-45 Project # Collected By Brady Glover Collection Date 06/24/14 14:45 ' Parameter Result Det. Limit Units Method Date Dil. Volatile Organics Benzene BDL 0.0050 mg/l 624 06/29/14 5 1,2-Dichloroethane BDL 0.0050 mg/l 624 06/29/14 5 ' Ethylbenzene BDL 0.0050 mg/l 624 06/29/14 5 Methyl tert-butyl ether 6.4 1.0 mg/l 624 07/01/14 200 Naphthalene BDL 0.025 mg/l 624 06/29/14 5 Toluene BDL 0.025 mg/l 624 06/29/14 5 Xylenes, Total BDL 0.025 mg/l 624 06/29/14 5 ' Surrogate Recovery Toluene-d8 96.0 % Rec. 624 06/29/14 5 Dibromofluoromethane 94.7 8 Rec. 624 06/29/14 5 a,a,a-Trifluorotoluene 97.9 % Rec. 624 06/29/14 5 4-Bromofluorobenzene 89.3 8 Rec. 624 06/29/14 5 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) . Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/22/14 15:36 Printed: 08/22/14 15:36 tPage 11 of 17 1 12065 Lebanon Rd. , Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859*ELSC ' Fax (615) 758-5859 L•A-B S•C•I•E•N•C E•S Tax I.D. 62-0819289 z Est. 1970 REPORT OF ANALYSIS ' Mr. Michael Susca August 22, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ' ESC Sample # : L706716-11 Date Received June 25, 2019 Description RFP #2013068 Site ID Sample ID OW-8 Project # Collected By Brady Glover Collection Date 06/24/14 13:45 Parameter Result Det. Limit Units Method Date Dil. Free Carbon Dioxide 86. 20. mg/l 45000O2 D-201 06/28/14 1 Benzene 9.6 0.25 mg/l 624 06/28/14 250 Ethylbenzene 0.98 0.25 mg/1 624 06/28/14 250 ' Toluene 68. 5.0 mg/l 624 07/03/14 1000 Xylenes, Total 6.8 0.75 mg/l 624 06/28/14 250 Methyl tent-butyl ether 9.3 0.25 mg/l 624 06/28/14 250 Naphthalene BDL 1.2 mg/l 624 06/28/14 250 Surrogate Recovery Toluene-d8 104. % Rec. 624 06/28/14 250 ' Dibromofluoromethane 100. 8 Rec. 624 06/28/14 250 a,a,a-Trifluorotoluene 101. % Rec. 624 06/28/14 250 4-Bromofluorobenzene 101. % Rec. 624 06/28/14 250 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/22/14 15:36 Printed: 08/22/14 15:36 Page 12 of 17 ' 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 *ESC 1-800-767-5859 Fax (615) 758-5859 L-A B 3•C•1•E•N-C E•5 Tax I.D. 62-0814289 Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca August 22, 2019 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample # L706716-12 Date Received June 25, 2014 Description RFP #2013068 Site ID ' Sample ID OW-33 Project # Collected By Brady Glover Collection Date 06/24/14 15:35 ' Parameter Result Det. Limit Units Method Date Dil. Nitrate BDL 0.10 mg/1 300.0 06/26/14 1 Sulfate BDL 5.0 mg/1 300.0 06/26/14 1 Alkalinity 280 20. mg/1 2320 B-2011 06/28/14 1 ' Methane 0.10 0.010 mg/l RSK175 06/28/14 1 Ethane BDL 0.013 mg/l RSK175 06/28/14 1 Ethene BDL 0.013 mg/1 RSK175 06/28/14 1 ' volatile Organics Benzene BDL 0.0010 mg/1 624 06/29/14 1 1,2-Dichloroethane BDL 0.0010 mg/l 624 06/29/14 1 Ethylbenzene BDL 0.0010 mg/1 624 06/29/14 1 Methyl tert-butyl ether BDL 0.0050 mg/1 624 07/01/14 1 ' Naphthalene BDL 0.0050 mg/1 624 06/29/14 1 Toluene BDL 0.0050 mg/l 624 06/29/14 1 Xylenes, Total BDL 0.0050 mg/1 624 06/29/14 1 Surrogate Recovery Toluene-d8 97.2 % Rec. 624 06/29/14 1 Dibromofluoromethane 98.5 % Rec. 624 06/29/14 1 ' a,a,a-Trifluorotoluene 96.9 % Rec. 624 06/29/14 1 4-Bromofluorobenzene 87.8 % Rec. 624 06/29/14 1 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/22/14 15:36 Printed: 08/22/14 15:36 ' Page 13 of 17 1 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 OESC Fax (615) 758-5859 ' L•A,B S•C-1•E•N-C E•5 Tax I.D. 62-0814289 • Est. 1970 REPORT OF ANALYSIS , Mr. Michael Susca August 22, 2014 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ' ESC Sample # L706716-13 Date Received June 25, 2014 Description RFP #2013068 Site ID Sample ID OW-19 ' Project # Collected By Brady Glover Collection Date 06/24/14 15:40 Parameter Result Det. Limit Units Method Date Dil. , Free Carbon Dioxide BDL 20. mg/l 4500002 D-201 06/28/14 1 Benzene 0.0032 0.0010 mg/1 624 07/03/14 1 Ethylbenzene 0.0023 0.0010 mg/l 624 07/03/14 1 ' Toluene BDL 0.0050 mg/l 624 07/03/14 1 Xylenes, Total 0.023 0.0030 mg/1 624 07/03/14 1 Methyl tert-butyl ether 0.0035 0.0010 mg/l 624 07/03/14 1 Naphthalene BDL 0.0050 mg/l 624 07/03/14 1 Surrogate Recovery Toluene-d8 93.7 % Rec. 624 07/03/14 1 ' Dibromofluoromethane 91.4 % Rec. 624 07/03/14 1 a,a,a-Trifluorotoluene 96.0 % Rec. 624 07/03/14 1 4-Bromofluorobenzene 99.6 8 Rec. 624 07/03/14 1 1 1 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/22/14 15:36 Printed: 08/22/14 15:36 Page 14 of 17 , 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 OESC1-800-767-5859 ' Fax (615) 758-5859 L-A B S•C•1•E•N C E•S Tax I.D. 62-0819289 Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca August 22, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample # L706716-19 Date Received June 25, 2014 Description RFP #2013068 Site ID ' Sample ID OW-18 Project # Collected By Brady Glover Collection Date 06/24/14 14:35 ' Parameter Result Det. Limit Units Method Date Dil. Benzene BDL 0.0010 mg/1 624 07/02/14 1 Ethylbenzene BDL 0.0010 mg/1 624 07/02/14 1 Toluene BDL 0.0050 mg/l 624 07/02/14 1 Xylenes, Total BDL 0.0030 mg/1 624 07/02/14 1 ' Methyl tert-butyl ether 0.0015 0.0010 mg/1 624 07/02/14 1 Naphthalene BDL 0.0050 mg/l 624 07/02/14 1 Surrogate Recovery Toluene-d8 98.2 % Rec. 624 07/02/14 1 Dibromofluoromethane 95.8 % Rec. 624 07/02/14 1 ' a,a,a-Trifluorotoluene 99.2 % Rec. 624 07/02/14 1 4-Bromofluorobenzene 94.1 8 Rec. 624 07/02/14 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 08/22/14 15:36 Printed: 08/22/14 15:36 ' Page 15 of 17 Attachment A ' List of Analytes with QC Qualifiers Sample Work Sample Run ' Number Group Type Analyte ID Qualifier L706716-02 WG728672 SAMP Benzene R2950185 D WG729026 SAMP Free Carbon Dioxide 82952489 T8 ' L706716-03 WG729026 SAMP Free Carbon Dioxide R2952489 T8 L706716-04 WG729026 SAMP Free Carbon Dioxide R2952489 T8 L706716-05 NG729026 SAMP Free Carbon Dioxide 82952489 T8 L706716-06 WG729026 SAMP Free Carbon Dioxide 82952489 T8 L706716-07 WG729026 SAMP Free Carbon Dioxide R2952489 T8 ' L706716-08 WG729026 SAMP Free Carbon Dioxide R2952489 T8 L706716-09 WG729026 SAMP Free Carbon Dioxide R2952489 T8 L706716-11 WG728678 SAMP Benzene R2952205 ** WG729026 SAMP Free Carbon Dioxide R2952489 T8 L706716-13 WG729026 SAMP Free Carbon Dioxide R2952489 T8 1 1 1 1 Page 16 of 17 ' 1 ' Attachment B Explanation of QC Qualifier Codes ' Qualifier Meaning TB (ESC) - Additional method/sample information: Sample(s) received past/too close to holding time expiration. ' U BDL (EPA) - Below Detectable Limits: Indicates that the compound was analyzed but not detected. ' Qualifier Report Information ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical ' results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all reported data is valid and useable ' "unless qualified as 'R' (Rejected) ." Definitions ' Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Precision - The agreement between a set of samples or between duplicate samples. ' Relates to how close together the results are and is represented by Relative Percent Differrence. Surrogate - Organic compounds that are similar in chemical composition, extraction, and chromotography to analytes of interest. The surrogates are used to ' determine the probable response of the group of analytes that are chem- ically related to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. TIC - Tentatively Identified Compound: Compounds detected in samples that are ' not target compounds, internal standards, system monitoring compounds, or surrogates. 1 ' Page 17 of 17 12065 Lebanon Rd. , Mt. Juliet, TN 37122 (615) 758-5858 l67-5859OESC ' Faxax (61(615) 758-5859 L•A•B S•C•1•E•N-C E•3 Tax I.D. 62-0814289 Est. 1970 Mr. Michael Susca Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 Report Summary Wednesday July 02, 2014 ' Report Number: L706818 Samples Received: 06/26/14 , Client Project: RFP 2013068 Description: RFP #2013068 ' The analytical results in this report are based upon information supplied ' by you, the client, and are for your exclusive use. If you have an questions regarding this data package, please do not hesitate to caly l. Entire Report Reviewed By: Terrie Fu 79 ESC resentative ' Laboratory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, , NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02 Accreditation is only applicable to the test methods specified on each scope of accreditation held ' by ESC Lab Sciences. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided , in laboratory standard operating procedures: 060302, 060303, and 060304. 1 Page 1 of 8 ' 1 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 OESC1-800-767-5859 ' Fax (615) 758-5859 L-A B s•C-I•E•N-c-E•s Tax I.D. 62-0814289 • Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca July 02, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample # L706818-01 Date Received June 26, 2014 Description RFP #2013068 Site ID ' Sample ID OW-56 Project # RFP 2013068 Collected By Brady Glover Collection Date 06/25/14 13:15 ' Parameter Result Det. Limit Units Method Date Dil. Nitrate BDL 0.10 mg/l 300.0 06/26/14 1 Sulfate BDL 5.0 mg/l 300.0 06/26/14 1 Alkalinity 240 20. mg/l 2320 B-2011 06/29/14 1 ' Methane 0.045 0.010 mg/1 RSK175 06/28/14 1 Ethane BDL 0.013 mg/l RSK175 06/28/14 1 Ethene BDL 0.013 mg/l RSK175 06/28/14 1 ' Volatile Organics Benzene BDL 0.020 mg/l 624 06/28/14 20 1,2-Dichloroethane BDL 0.020 mg/l 624 06/28/14 20 Ethylbenzene BDL 0.020 mg/l 624 06/28/14 20 Methyl tert-butyl ether 14. 1.2 mg/l 624 06/29/14 250 ' Naphthalene BDL 0.10 mg/l 624 06/28/14 20 Toluene BDL 0.10 mg/l 624 06/28/14 20 Xylenes, Total BDL 0.10 mg/l 624 06/28/14 20 Surrogate Recovery Toluene-d8 99.3 8 Rec. 624 06/28/14 20 Dibromofluoromethane 102. 8 Rec. 624 06/28/14 20 ' a,a,a-Trifluorotoluene 99.7 8 Rec. 624 06/28/14 20 4-Bromofluorobenzene 96.2 8 Rec. 624 06/28/14 20 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:20 Revised: 07/02/14 14:06 ' Page 2 of 8 1 12065 Lebanon Rd. , Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859OESC ' Fax (615) 758-5859 L•A,8 B-C•1•E•N-C E•5 Tax I.D. 62-0819289 WWMZ • �� Est. 1970 REPORT OF ANALYSIS ' Mr. Michael Susca July 02, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 , ESC Sample # L706818-02 Date Received June 26, 2014 Description RFP #2013068 Site ID Sample ID OW-51 ' Project # RFP 2013068 Collected By Brady Glover Collection Date 06/25/14 11:10 Parameter Result Det. Limit Units Method Date Dil. ' Nitrate BDL 0.10 mg/l 300.0 06/26/14 1 Sulfate BDL 5.0 mg/1 300.0 06/26/14 1 Alkalinity 130 20. mg/1 2320 B-2011 06/29/14 1 ' Methane 0.014 0.010 mg/1 RSK175 06/28/14 1 Ethane BDL 0.013 mg/l RSK175 06/28/14 1 Ethene BDL 0.013 mg/1 RSK175 06/28/14 1 volatile Organics ' Benzene BDL 0.010 mg/1 624 06/28/14 10 1,2-Dichloroethane BDL 0.010 mg/1 624 06/28/14 10 Ethylbenzene BDL 0.010 mg/1 624 06/28/14 10 Methyl tert-butyl ether 12. 1.0 mg/l 624 06/29/14 200 Naphthalene BDL 0.050 mg/l 624 06/28/14 10 ' Toluene BDL 0.050 mg/l 624 06/28/14 10 Xylenes, Total BDL 0.050 mg/l 624 06/28/14 10 Surrogate Recovery Toluene-d8 99.9 % Rec. 624 06/28/14 10 Dibromofluoromethane 102. % Rec. 624 06/28/14 10 ' a,a,a-Trifluorotoluene 99.4 8 Rec. 624 06/28/14 10 4-Bromofluorobenzene 97.9 % Rec. 624 06/28/14 10 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:20 Revised: 07/02/14 14:06 Page 3 of 8 ' 1 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 *ESC1-800-767-5859 ' Fax (615) 758-5859 L B S•C•i-E-N•C-E•B Tax I.D. 62-0814289 Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca July 02, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample # L706818-03 Date Received June 26, 2014 Description RFP #2013068 Site ID Sample ID OW-60 Project # REP 2013068 Collected By Brady Glover Collection Date 06/25/14 12:30 ' Parameter Result Det. Limit Units Method Date Dil. Nitrate BDL 0.10 mg/1 300.0 06/26/14 1 Sulfate 10. 5.0 mg/l 300.0 06/26/14 1 Alkalinity 130 20. mg/1 2320 B-2011 06/29/14 1 ' Methane BDL 0.010 mg/1 RSK175 06/28/14 1 Ethane BDL 0.013 mg/1 RSK175 06/28/14 1 Ethene BDL 0.013 mg/l RSK175 06/28/14 1 ' Volatile Organics Benzene BDL 0.0010 mg/1 624 06/28/14 1 1,2-Dichloroethane BDL 0.0010 mg/1 624 06/28/14 1 Ethylbenzene BDL 0.0010 mg/l 624 06/28/14 1 Methyl tert-butyl ether 0.014 0.0050 mg/l 624 06/29/14 1 ' Naphthalene BDL 0.0050 mg/l 624 06/28/14 1 Toluene BDL 0.0050 mg/1 624 06/28/14 1 Xylenes, Total BDL 0.0050 mg/l 624 06/28/14 1 Surrogate Recovery Toluene-d8 99.1 9 Rec. 624 06/28/14 1 Dibromofluoromethane 101. 8 Rec. 624 06/28/14 1 ' a,a,a-Trifluorotoluene 101. 8 Rec. 624 06/28/14 1 4-Bromofluorobenzene 95.2 % Rec. 624 06/28/14 1 1 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:20 Revised: 07/02/14 14:06 Page 4 of 8 1 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 (615) 758-5858 1-800-79E S C ' Fax (615)5) 758 758-5859 L-A B 5•C•1•E•N-C E•S Tax I.D. 62-0614289 Est. 1970 • Mr. Michael Susca REPORT OF ANALYSIS ' July 02, 2019 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ' ESC Sample # L706818-04 Date Received June 26, 2014 Description RFP #2013068 Site ID Sample ID OW-59 ' Project # RFP 2013068 Collected By Brady Glover Collection Date 06/25/14 12:15 Parameter Result Det. Limit Units Method Date Dil. ' Volatile Organics Benzene BDL 0.0010 mg/l 624 06/28/14 1 1,2-Dichloroethane BDL 0.0010 mg/l 624 06/28/14 1 Ethylbenzene BDL 0.0010 mg/l 624 06/28/14 1 ' Methyl tert-butyl ether BDL 0.0050 mg/l 624 06/29/14 1 Naphthalene BDL 0.0050 mg/l 624 06/28/14 1 Toluene BDL 0.0050 mg/l 624 06/28/14 1 Xylenes, Total BDL 0.0050 mg/l 624 06/28/14 1 Surrogate Recovery Toluene-d8 98.9 % Rec. 624 06/28/14 1 ' Dibromofluoromethane 99.7 % Rec. 624 06/28/14 1 a,a,a-Trifluorotoluene 98.6 % Rec. 624 06/28/14 1 4-Bromofluorobenzene 92.5 8 Rec. 624 06/28/14 1 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:20 Revised: 07/02/14 14:06 Page 5 of 8 ' ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 OESC' Fax (615) 758-5859 L-A-B 8•C•I•E•N•C-E•3 Tax I.D. 62-0819289 Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca July 02, 2019 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample # L706818-05 Date Received June 26, 2014 Description RFP #2013068 Site ID ' Sample ID SW-1 Project # RFP 2013068 Collected By Brady Glover Collection Date 06/25/14 13:25 Parameter Result Det. Limit Units Method Date Dil. Benzene BDL 0.0010 mg/1 624 06/28/14 1 Ethylbenzene BDL 0.0010 mg/1 624 06/28/14 1 Toluene BDL 0.0050 mg/1 624 06/28/14 1 ' Xylenes, Total BDL 0.0030 mg/1 629 06/28/19 1 Methyl tent-butyl ether 0.062 0.0010 mg/1 624 06/28/14 1 Naphthalene BDL 0.0050 mg/l 624 06/28/14 1 Surrogate Recovery Toluene-d8 101. 9 Rec. 624 06/28/14 1 Dibromofluoromethane 98.8 % Rec. 624 06/28/14 1 ' a,a,a-Trifluorotoluene 103. % Rec. 624 06/28/14 1 4-Bromofluorobenzene 90.4 8 Rec. 624 06/28/14 1 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:20 Revised: 07/02/14 14:06 ' Page 6 of 8 1 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 (615) 758-5858 1-800-79*ESC ' Fax (61515) 758 758-5859 L-A B S-C•1-E-N-C E-5 Tax I.D. 62-0814269 Est. 1970 Mr. Michael Susca REPORT OF ANALYSIS ' July 02, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ' ESC Sample # L706818-06 Date Received June 26, 2014 Description RFP #2013068 Site ID Sample ID DUP 2 ' Project # RFP 2013068 Collected By Brady Glover Collection Date 06/25/14 13:20 Parameter Result Det. Limit Units Method Date Dil. ' Benzene BDL 0.010 mg/l 624 06/28/14 10 Ethylbenzene BDL 0.010 mg/l 624 06/28/14 10 Toluene BDL 0.050 mg/l 624 06/28/14 10 Xylenes, Total BDL 0.030 mg/l 624 06/28/14 10 ' Methyl tert-butyl ether 13. 0.50 mg/l 624 06/30/14 500 Naphthalene BDL 0.050 mg/l 624 06/28/14 10 Surrogate Recovery Toluene-d8 98.8 % Rec. 624 06/28/14 10 Dibromofluoromethane 99.2 % Rec. 624 06/28/14 10 a,a,a-Trifluorotoluene 101. % Rec. 624 06/28/14 10 ' 4-Bromofluorobenzene 92.5 % Rec. 624 06/28/14 10 1 1 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:20 Revised: 07/02/14 14:06 Page 7 of 8 ' 1 12065 Lebanon Rd. Mt. Juliet, TN 37122 1615) 758-5858 *ESC1-800-767-5859 ' Fax (615) 758-5859 L•A-B S•C•1•E•N-C E•S Tax I.D. 62-0814289 _ . Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca July 02, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample # L706818-07 Date Received June 26, 2014 Description RFP #2013068 Site ID ' Sample ID SW-2 Project # RFP 2013068 Collected By Brady Glover Collection Date 06/25/14 10:45 ' Parameter Result Det. Limit Units Method Date Dil. Benzene BDL 0.0010 mg/l 624 06/28/14 1 Ethylbenzene BDL 0.0010 mg/1 624 06/28/14 1 Toluene BDL 0.0050 mg/l 624 06/28/14 1 Xylenes, Total BDL 0.0030 mg/l 624 06/28/14 1 ' Methyl tert-butyl ether 0.31 0.010 mg/1 624 06/30/14 10 Naphthalene BDL 0.0050 mg/1 624 06/28/14 1 Surrogate Recovery Toluene-d8 98.7 8 Rec. 624 06/28/14 1 Dibromofluoromethane 100. % Rec. 624 06/28/14 1 ' a,a,a-Trifluorotoluene 101. % Rec. 624 06/28/14 1 4-Bromofluorobenzene 92.6 % Rec. 624 06/28/14 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 06/30/14 15:20 Revised: 07/02/14 14:06 Page 8 of 8 1 Summary of Remarks For Samples Printed , 07/02/14 at 14:06:44 TSR Signing Reports: 064 ' Sample: L706818-01 Account: LEGBGFCT Received: 06/26/14 09:00 Due Date: 07/03/14 00:00 RPT Date: 06/30/14 15:20 ' Sample: L706818-02 Account: LEGBGFCT Received: 06/26/14 09:00 Due Date: 07/03/14 00:00 RPT Date: 06/30/14 15:20 Sample: L706818-03 Account: LEGBGFCT Received: 06/26/14 09:00 Due Date: 07/03/14 00:00 RPT Date: 06/30/14 15:20 , Sample: L706818-04 Account: LEGBGFCT Received: 06/26/14 09:00 Due Date: 07/03/14 00:00 RPT Date: 06/30/14 15:20 Sample: L706818-05 Account: LEGBGFCT Received: 06/26/14 09:00 Due Date: 07/03/14 00:00 RPT Date: 06/30/14 15:20 Sample: L706818-06 Account: LEGBGFCT Received: 06/26/14 09:00 Due Date: 07/03/14 00:00 RPT Date: 06/30/14 15:20 ' Sample: L706818-07 Account: LEGBGFCT Received: 06/26/14 09:00 Due Date: 07/03/14 00:00 RPT Date: 06/30/14 15:20 1 1 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 75B-5858 *ESC 1-800-767-5859 Fax (615) 758-5859 L•A B 5•c•1•E•W-C E-B Tax I.D. 62-0614289 Est. 1970 ' Mr. Michael Susca Leggette, Srashears & Graham - CT ' 6 Executive Drive; Ste 109 Farmington, CT 0602 Report Summary ' Monday July 07, 2014 Report Number: L707152 ' Samples Received: 06/27/14 Client Project: ' Description: RFP #2013068 ' The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. t Entire Report Reviewed By: ' Terrie Fudg ESCresentative Laboratory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02 ' Accreditation is only applicable to the test methods specified on each scope of accreditation held by ESC Lab Sciences. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided ' in laboratory standard operating procedures: 060302, 060303, and 060304. ' Page 1 of 14 t 12065 Lebanon Rd. , Mt. Juliet, TN 37122 (615) 758-5856 1-800-767-5859 OESC Fax (615) 758-5859 ' L-A�B S-C•I•E•N•CGE•8 Tax I.D. 62-0819289 ' Est. 1970 Mr. Michael Susca REPORT OF ANALYSIS ' July 07, 2014 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ' ESC Sample # L707152-01 Date Received June 27, 2019 Description RFP #2013068 Site ID Sample ID DW-1 ' Project # Collected By Brady Glover Collection Date 06/26/14 09:40 Parameter Result Det. Limit Units Method Date Dil. ' Volatile Organics Benzene BDL 0.0010 mg/l 624 07/02/14 1 1,2-Dichloroethane 0.018 0.0010 mg/l 624 07/02/14 1 Ethylbenzene BDL 0.0010 mg/l 624 07/02/14 1 ' Methyl tert-butyl ether 0.76 0.10 mg/l 624 07/05/14 20 Naphthalene BDL 0.0050 mg/l 624 07/02/14 1 Toluene BDL 0.0050 mg/l 624 07/02/14 1 Xylenes, Total BDL 0.0050 mg/1 624 07/02/14 1 Surrogate Recovery Toluene-d8 97.8 % Rec. 624 07/02/14 1 t Dibromofluoromethane 98.1 8 Rec. 624 07/02/14 1 a,a,a-Trifluorotoluene 99.5 8 Rec. 624 07/02/14 1 4-Bromofluorobenzene 97.0 % Rec. 624 07/02/14 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) t Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 11:20 Printed: 07/07/14 11:21 Page 2 of 14 ' 1 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 *ESC 1-800-767-5859 Fax (615) 758-5859 ' L-A B S•C•1•E•N•C-E•S Tax I.D. 62-0814289 Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca July 07, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample # L707152-02 Date Received June 27, 2014 Description RFP #2013068 Site ID Sample ID W-2 Project # Collected By Brady Glover Collection Date 06/26/14 09:30 ' Parameter Result Det. Limit Units Method Date Dil. Benzene 0.52 0.010 mg/1 624 07/04/14 10 Ethylbenzene 0.22 0.010 mg/1 624 07/04/14 10 Toluene BDL 0.050 mg/1 624 07/04/14 10 Xylenes, Total 0.96 0.030 mg/1 624 07/04/14 10 Methyl tert-butyl ether 0.99 0.010 mg/1 624 07/04/14 10 Naphthalene 0.12 0.050 mg/1 624 07/04/14 10 Surrogate Recovery Toluene-d8 97.1 % Rec. 624 07/04/14 10 Dibromofluoromethane 95.6 8 Rec. 624 07/04/14 10 a,a,a-Trifluorotoluene 98.9 % Rec. 624 07/04/14 10 4-Bromofluorobenzene 104. 8 Rec. 624 07/04/14 10 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. a Reported: 07/07/14 11:20 Printed: 07/07/14 11:21 Page 3 of 14 1 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 *ESC Fax (615) 758-5859 ' L•A B 8•C•I•E-W C E•3 Tax I.D. 62-0814289 ' Est. 1970 Mr. Michael Susca REPORT OF ANALYSIS ' July 07, 2014 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ' ESC Sample # L707152-03 Date Received June 27, 2014 Description RFP #2013068 Site ID Sample ID OW-33 t Project # Collected By Brady Glover Collection Date 06/26/14 11:15 Parameter Result Det. Limit Units Method Date Dil. , Free Carbon Dioxide 120 20. mg/1 4500002 D-201 07/02/14 1 Benzene 1.2 0.010 mg/l 624 07/01/14 10 Ethylbenzene 0.021 0.010 mg/l 624 07/01/14 10 ' Toluene BDL 0.050 mg/l 624 07/01/14 10 Xylenes, Total 0.25 0.030 mg/l 624 07/01/14 10 Methyl tert-butyl ether BDL 0.010 mg/l 624 07/01/14 10 Naphthalene 0.13 0.050 mg/l 624 07/01/14 10 Surrogate Recovery Toluene-d8 100. 8 Rec. 624 07/01/14 10 ' Dibromofluoromethane 96.1 8 Rec. 624 07/01/14 10 a,a,a-Trifluorotoluene 103. % Rec. 624 07/01/14 10 4-Bromofluorobenzene 100. 8 Rec. 624 07/01/14 10 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 11:20 Printed: 07/07/14 11:21 Page 4 of 14 ' 1 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 0 E S C1-800-767-5859 ' Fax (615) 758-5859 L•A 8 8•C-1•E•N-c E•S Tax I.D. 62-0814289 Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca July 07, 2014 Leggette, Brashears b Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample # L707152-09 Date Received June 27, 2014 Description RFP #2013068 Site ID ' Sample ID OW-59 Project # Collected By Brady Glover Collection Date 06/26/14 11:20 ' Parameter Result Det. Limit Units Method Date Dil. Free Carbon Dioxide 100 20. mg/1 4500002 D-201 07/02/14 1 Benzene 0.0016 0.0010 mg/1 624 07/01/14 1 Ethylbenzene BDL 0.0010 mg/1 624 07/01/14 1 Toluene BDL 0.0050 mg/l 624 07/01/14 1 Xylenes, Total BDL 0.0030 mg/1 624 07/01/14 1 Methyl tert-butyl ether BDL 0.0010 mg/1 624 07/01/14 1 Naphthalene BDL 0.0050 mg/1 624 07/01/14 1 Surrogate Recovery ' Toluene-d8 100. 8 Rec. 624 07/01/14 1 Dibromofluoromethane 99.9 8 Rec. 624 07/01/14 1 a,a,a-Trifluorotoluene 104. % Rec. 624 07/01/14 1 4-Bromofluorobenzene 103. % Rec. 624 07/01/14 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 11:20 Printed: 07/07/14 11:21 ' Page 5 of 14 1 12065 Lebanon Rd. 1 Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 OESC Fax (615) 758-5859 1 L-A B B•C•I•E•N•C E•S Tax I.D. 62-0814289 Est. 1970 Mr. Michael Susca REPORT OF ANALYSIS 1 July 07, 2019 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 1 ESC Sample # L707152-05 Date Received June 27, 2014 Description RFP #2013068 Site ID Sample ID OW-62 1 Project # Collected By Brady Glover Collection Date 06/26/14 10:40 Parameter Result Det. Limit Units Method Date Dil. 1 Nitrate BDL 0.10 mg/1 300.0 06/27/14 1 Sulfate BDL 5.0 mg/1 300.0 01/03/14 1 Alkalinity 320 20. mg/1 2320 B-2011 06/29/14 1 1 Methane BDL 0.010 mg/1 RSK175 07/02/14 1 Ethane BDL 0.013 mg/1 RSK175 07/02/14 1 Ethene BDL 0.013 mg/1 RSK175 07/02/14 1 Volatile Organics 1 Benzene 0.0012 0.0010 mg/1 624 07/02/14 1 1,2-Dichloroethane BDL 0.0010 mg/1 624 07/02/14 1 Ethylbenzene BDL 0.0010 mg/1 624 07/02/14 1 Methyl tert-butyl ether 0.024 0.0050 mg/1 624 07/02/14 1 Naphthalene BDL 0.0050 mg/l 624 07/02/14 1 1 Toluene BDL 0.0050 mg/1 624 07/02/14 1 Xylenes, Total BDL 0.0050 mg/1 624 07/02/14 1 Surrogate Recovery Toluene-d8 96.8 % Rec. 624 07/02/14 1 Dibromofluoromethane 99.5 8 Rec. 624 07/02/14 1 1 a,a,a-Trifluorotoluene 99.3 % Rec. 624 07/02/14 1 4-Bromofluorobenzene 96.1 % Rec. 624 07/02/14 1 i 1 1 I BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 11:20 Printed: 07/07/14 11:21 Page 6 of 14 1 1 i ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 OESC1-800-767-5859 ' Fax (615) 758-5859 L•A-B S•C•I•E•N•C E'S Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS Mr. Michael Susca July 07, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample # L707152-06 Date Received June 27, 2014 Description RFP #2013068 Site ID ' Sample ID OW-6 Project # Collected By Brady Glover Collection Date 06/26/14 10:25 Parameter Result Det. Limit Units Method Date Dil. Nitrate 0.35 0.10 mg/l 300.0 06/27/14 1 Sulfate BDL 5.0 mg/l 300.0 07/03/14 1 Alkalinity 37. 20. mg/1 2320 B-2011 06/29/14 1 ' Methane BDL 0.010 mg/1 RSK175 07/02/14 1 Ethane BDL 0.013 mg/1 RSK175 07/02/14 1 Ethene HDL 0.013 mg/1 RSK175 07/02/14 1 ' Volatile Organics Benzene BDL 0.0010 mg/l 624 07/02/14 1 1,2-Dichloroethane BDL 0.0010 mg/l 624 07/02/14 1 Ethylbenzene BDL 0.0010 mg/1 624 07/02/14 1 Methyl tert-butyl ether BDL 0.0050 mg/l 624 07/02/14 1 ' Naphthalene BDL 0.0050 mg/1 624 07/02/14 1 Toluene BDL 0.0050 mg/1 624 07/02/14 1 Xylenes, Total BDL 0.0050 mg/l 624 07/02/14 1 Surrogate Recovery Toluene-d8 96.6 % Rec. 624 07/02/14 1 Dibromofluoromethane 97.2 8 Rec. 624 07/02/14 1 ' a,a,a-Trifluorotoluene 99.5 8 Rec. 624 07/02/19 1 4-Bromofluorobenzene 96.1 % Rec. 624 07/02/14 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 11:20 Printed: 07/07/14 11:21 Page 7 of 14 1 12065 Lebanon Rd. ' Mt. Juliet, TN 371.22 (615) 758-5858 1-800-767-5859 OESC Fax (615) 758-5859 ' L-A B S•C•1•E•N-C E•S Tax I.D. 62-0814289 Est. 1970 Mr. Michael Susca REPORT OF ANALYSIS ' July 07, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 , ESC Sample # L707152-07 Date Received June 27, 2019 Description RFP #2013068 Site ID Sample ID OW-23 ' Project # Collected By Brady Glover Collection Date 06/26/14 14:15 Parameter Result Det. Limit Units Method Date Dil. ' Benzene BDL 0.025 mg/l 624 07/01/14 25 Ethylbenzene BDL 0.025 mg/l 624 07/01/14 25 Toluene BDL 0.12 mg/l 624 07/01/14 25 Xylenes, Total BDL 0.075 mg/l 624 07/01/14 25 ' Methyl tert-butyl ether 23. 0.50 mg/l 624 07/04/14 500 Naphthalene BDL 0.12 mg/l 624 07/01/14 25 Surrogate Recovery Toluene-d8 101. % Rec. 624 07/01/14 25 Dibromofluoromethane 98.1 % Rec. 624 07/01/14 25 a,a,a-Trifluorotoluene 106. 8 Rec. 624 07/01/14 25 ' 4-Bromofluorobenzene 96.7 % Rec. 624 07/01/14 25 1 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 11:20 Printed: 07/07/14 11:21 Page 8 of 14 ' 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 *ESC' Fax (615) 758-5859 L-A-B 8•C•I•E-N C E•S Tax I.D. 62-0814289 Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca July 07, 2014 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 t Farmington, CT 06032 ESC Sample # L707152-08 Date Received June 27, 2014 Description RFP #2013068 Site ID ' Sample ID OW-63 Project # Collected By Brady Glover Collection Date 06/26/14 14:50 ' Parameter Result Det. Limit Units Method Date Dil. Volatile Organics Benzene BDL 0.0010 mg/l 624 07/02/14 1 1,2-Dichloroethane BDL 0.0010 mg/1 624 07/02/14 1 Ethylbenzene BDL 0.0010 mg/l 624 07/02/14 1 ' Methyl tert-butyl ether 1.2 0.25 mg/1 624 07/05/14 50 Naphthalene BDL 0.0050 mg/l 624 07/02/14 1 Toluene BDL 0.0050 mg/1 624 07/02/14 1 Xylenes, Total BDL 0.0050 mg/1 624 07/02/14 1 Surrogate Recovery ' Toluene-d8 98.5 8 Rec. 624 07/02/14 1 Dibromofluoromethane 97.4 8 Rec. 624 07/02/14 1 a,a,a-Trifluorotoluene 99.4 % Rec. 624 07/02/14 1 4-Bromofluorobenzene 94.4 % Rec. 624 07/02/14 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 11:20 Printed: 07/07/14 11:21 ' Page 9 of 14 1 12065 Lebanon Rd. 1 Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 *ESC Fax (615) 758-5859 L•A-B S•C•1•E•N-C-E•S Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS 1 Mr. Michael Susca July 07, 2014 Leggette, Brashears S Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 1 ESC Sample # L707152-09 Date Received June 27, 2014 Description RFP #2013068 Site ID Sample ID W-4 1 Project # Collected By Brady Glover Collection Date 06/26/14 15:50 Parameter Result Det. Limit Units Method Date Dil. 1 Volatile Organics Benzene BDL 0.0010 mg/1 624 07/02/14 1 1,2-Dichloroethane BDL 0.0010 mg/1 624 07/02/14 1 Ethylbenzene BDL 0.0010 mg/1 624 07/02/14 1 Methyl tert-butyl ether BDL 0.0050 mg/l 624 07/05/14 1 1 Naphthalene BDL 0.0050 mg/l 624 07/02/14 1 Toluene BDL 0.0050 mg/1 624 07/02/14 1 Xylenes, Total BDL 0.0050 mg/l 624 07/02/14 1 Surrogate Recovery Toluene-d8 98.3 % Rec. 624 07/02/14 1 1 Dibromofluoromethane 96.0 8 Rec. 624 07/02/14 1 a,a,a-Trifluorotoluene 100. % Rec. 624 07/02/14 1 4-Bromofluorobenzene 97.3 % Rec. 624 07/02/14 1 i 1 1 1 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 11:20 Printed: 07/07/14 11:21 Page 10 of 14 1 1 1 1 t 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5658 *ESC1-800-767-5859 ' Fax (615) 758-5859 L-A-8 S•C•1•E•N-C-E•S Tax I.D. 62-0814289 Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca July 07, 2014 Leggette, Brashears & Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample # L707152-10 Date Received June 27, 2014 Description RFP #2013068 Site ID ' Sample ID OW-61 Project # Collected By Brady Glover Collection Date 06/26/14 14:30 ' Parameter Result Det. Limit Units Method Date Dil. Volatile Organics Benzene 1.0 0.010 mg/1 629 07/02/19 10 1,2-Dichloroethane BDL 0.010 mg/l 624 07/02/14 10 Ethylbenzene BDL 0.010 mg/l 624 07/02/14 10 Methyl tert-butyl ether 2.6 0.50 mg/l 624 07/05/14 100 Naphthalene BDL 0.050 mg/l 624 07/02/14 10 Toluene BDL 0.050 mg/l 624 07/02/14 10 Xylenes, Total BDL 0.050 mg/l 624 07/02/14 10 Surrogate Recovery Toluene-d8 98.4 % Rec. 624 07/02/14 10 Dibromofluoromethane 96.7 % Rec. 624 07/02/14 10 a,a,a-Trifluorotoluene 99.0 8 Rec. 624 07/02/14 10 4-Bromofluorobenzene 99.0 % Rec. 624 07/02/14 10 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 11:20 Printed: 07/07/14 11:21 ' Page 11 of 14 1 1 1 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859E S C ' Fax (615) 758-5859 L-A-B 9•C•1•E•N•C E•3 Tax I.D. 62-0814289 Est. 1970 REPORT OF ANALYSIS ' Mr. Michael Susca July 07, 2014 Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 Farmington, CT 06032 ' ESC Sample # L707152-11 Date Received June 27, 2014 Description RFP #2013068 Site ZD ' Sample ID OW-9 Project # Collected By Brady Glover Collection Date 06/26/14 00:00 Parameter Result Det. Limit Units Method Date Dil. ' Free Carbon Dioxide 94. 20. mg/l 4500002 D-201 07/02/14 1 volatile Organics Benzene 3.1 2.0 mg/1 624 07/04/14 2000 ' 1,2-Dichloroethane BDL 2.0 mg/l 624 07/04/14 2000 Ethylbenzene BDL 2.0 mg/1 624 07/04/14 2000 Methyl tert-butyl ether BDL 10. mg/1 624 07/04/14 2000 Naphthalene BDL 10. mg/l 624 07/04/14 2000 Toluene 91. 10. mg/1 624 07/04/14 2000 Xylenes, Total BDL 10. mg/l 624 07/04/14 2000 ' Surrogate Recovery Toluene-d8 99.9 8 Rec. 624 07/04/14 2000 Dibromofluoromethane 109. % Rec. 624 07/04/14 2000 a,a,a-Trifluorotoluene 106. % Rec. 624 07/04/14 2000 4-Bromofluorobenzene 99.6 8 Rec. 624 07/04/14 2000 ' 1 BDL - Below Detection Limit Det. Limit - Practical Quantitation Limit(PQL) ' Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 11:20 Printed: 07/07/14 11:21 ' Page 12 of 14 1 1 ' Attachment A List of Analytes with QC Qualifiers ' Sample Work Sample Run Number Group Type Analyte ID Qualifier L707152-03 WG729269 SAMP Free Carbon Dioxide 82954248 T8 L707152-04 WG729269 SAMP Free Carbon Dioxide 82954248 T8 L707152-11 WG729269 SAMP Free Carbon Dioxide 82954248 T8 ' Page 13 of 14 Attachment B ' Explanation of QC Qualifier Codes Qualifier Meaning ' T8 (ESC) - Additional method/sample information: Sample(s) received past/too close to holding time expiration. Qualifier Report Information ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and ' as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of ' matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all reported data is valid and useable "unless qualified as 'R' (Rejected)." Definitions , Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. ' Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence. Surrogate - Organic compounds that are similar in chemical composition, extraction, ' and chromotography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem- ically related to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. TIC - Tentatively Identified Compound: Compounds detected in samples that are ' not target compounds, internal standards, system monitoring compounds, or surrogates. 1 1 Page 14 of 14 1 Summary of Remarks For Samples Printed 07/07/14 at 11:21:28 TSR Signing Reports: 064 ' Sample: L707152-01 Account: LEGBGFCT Received: 06/27/14 09:00 Due Date: 07/07/14 00:00 RPT Date: 07/07/14 11:20 Sample: L707152-02 Account: LEGBGFCT Received: 06/27/14 09:00 Due Date: 07/07/14 00:00 RPT Date: 07/07/14 11:20 ' Sample: L707152-03 Account: LEGBGFCT Received: 06/27/14 09:00 Due Date: 07/07/14 00:00 RPT Date: 07/07/14 11:20 Sample: L707152-04 Account: LEGBGFCT Received: 06/27/14 09:00 Due Date: 07/07/14 00:00 RPT Date: 07/07/14 11:20 Sample: L707152-05 Account: LEGBGFCT Received: 06/27/14 09:00 Due Date: 07/07/14 00:00 RPT Date: 07/07/14 11:20 all analyses logged from template (COC lists NO2, but is supposed to be NITRATE - template ' fixed) JCR Sample: L707152-06 Account: LEGBGFCT Received: 06/27/14 09:00 Due Date: 07/07/19 00:00 RPT Date: 07/07/19 11:20 all analyses logged from template (COC lists NO2, but is supposed to be NITRATE - template fixed) JCR Sample: L707152-07 Account: LEGBGFCT Received: 06/27/14 09:00 Due Date: 07/07/14 00:00 RPT Date: 07/07/14 11:20 ' Sample: L707152-08 Account: LEGBGFCT Received: 06/27/14 09:00 Due Date: 07/07/14 00:00 RPT Date: 07/07/14 11:20 Sample: L707152-09 Account: LEGBGFCT Received: 06/27/14 09:00 Due Date: 07/07/14 00:00 RPT Date: 07/07/14 11:20 Sample: L707152-10 Account: LEGBGFCT Received: 06/27/14 09:00 Due Date: 07/07/14 00:00 RPT Date: 07/07/14 11:20 Sample: L707152-11 Account: LEGBGFCT Received: 06/27/14 09:00 Due Date: 07/07/14 00:00 RPT Date: 07/07/14 11:20 1 1 1 1 12065 Lebanon Rd. ' Mt. Juliet, TN 37122 *ESC (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 L-A-8 S-C-I-E-N•C E•S Tax I.D. 62-0814289 - Est. 1970 Mr. Michael Susca Leggette, Brashears 6 Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 Report Summary Monday July 07, 2014 ' Report Number: L707990 Samples Received: 07/02/14 ' Client Project: 2013068 Description: RFP #2013068 ' The analytical results in this report are based upon information supplied ' by you, the client, and are for your exclusive use. If you have an questions regarding this data package, please do not hesitate to caly l. 1 Entire Report Reviewed By: Terrie Fudg ESC resentative ' Laboratory Certification Numbers A2LA - 1461-01, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, ' NC - ENV375/DW21704/BI0041, ND - R-140. NJ - TN002, NJ NELAP - TN002, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02 Accreditation is only applicable to the test methods specified on each scope of accreditation held ' by ESC Lab Sciences. This report may not be reproduced, except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided ' in laboratory standard operating procedures: 060302, 060303, and 060304. 1 Page 1 of 4 ' 1 1 1 ' 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 *ESC1-800-767-5859 ' Fax (615) 758-5859 L-A B S•C•i-E•w•C•E-5 Tax I.D. 62-0814289 Est. 1970 ' REPORT OF ANALYSIS Mr. Michael Susca July 07, 2014 Leggette, Brashears s Graham - CT 6 Executive Drive; Ste 109 ' Farmington, CT 06032 ESC Sample M L707990-01 Date Received July 02, 2014 Description RFP $2013068 Site ID ' Sample ID OW-22 Project # 2013068 Collected By Brady Glover Collection Date 07/01/14 15:00 ' Parameter Result Det. Limit Units Method Date Dil. Benzene 0.0024 0.0010 mg/l 8260B 07/06/14 1 Toluene BDL 0.0050 mg/l 8260B 07/06/14 1 Ethylbenzene BDL 0.0010 mg/l 8260B 07/06/14 1 Total Xylenes BDL 0.0030 mg/1 8260B 07/06/14 1 ' Methyl tert-butyl ether 0.026 0.0010 mg/1 8260B 07/06/14 1 1,2-Dichloroethane BDL 0.0010 mg/l 8260B 07/06/14 1 Naphthalene BDL 0.0050 mg/l 8260B 07/06/14 1 Surrogate Recovery Toluene-d8 101. % Rec. 8260B 07/06/14 1 ' Dibromofluoromethane 94.9 % Rec. 8260B 07/06/14 1 a,a,a-Trifluorotoluene 103. % Rec. 8260B 07/06/14 1 4-Bromofluorobenzene 88.0 % Rec. 8260B 07/06/14 1 1 1 1 BDL - Below Detection Limit ' Det. Limit - Practical Quantitation Limit(PQL) Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from ESC. Reported: 07/07/14 10:52 Revised: 07/07/14 16:18 Page 2 of 4 1 I� Attachment A ' List of Analytes with QC Qualifiers Sample Work Sample Run ' Number Group Type Analyte ID Qualifier L707990-01 UG729987 SAMP Naphthalene R2956349 J3 I 1 . 1 Page 3 of 4 ' ' Attachment B Explanation of QC Qualifier Codes Qualifier Meaning J3 The associated batch QC was outside the established quality control range for precision. Qualifier Report Information ' ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NELAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of ' matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These exceptions are evaluated and all reported data is valid and useable "unless qualified as 'R' (Rejected)." t Definitions Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence. ' Surrogate - Organic compounds that are similar in chemical composition, extraction, and chromotography to analytes of interest. The surrogates are used to determine the probable response of the group of analytes that are chem- ically related to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. ' TIC - Tentatively identified Compound: Compounds detected in samples that are not target compounds, internal standards, system monitoring compounds, or surrogates. t Page 4 of 4 1 1 1 1 ' ATTACHMENT 4 Local Government Review Documents 1 1 1 ' LEGGETTE BRASHEARS & GRAHAM INC. ' PROFESSIONAL GROUNDWATER AND ENVIRONMENTAL ENGINEERING SERVICES ' 8 PINE TREE DRIVE SUITE 250 ST.PAUL,MN 55112 (651)490-1405 ' FAX(651)490-1006 www.lbgweb.com November 17,2014 1 NCDENR/DWR/NPDES Complex Permitting Unit ' 1617 Mail Service Center Raleigh,NC 27699-1617 ' Re: Local Government Review Form Magellan Charlotte II Terminal Charlotte,Mecklenburg County,North Carolina ' NPDES Permit NC0005185 ' To Whom it May Concern: In accordance with the Engineering Alternative Analysis Guidance Document for a new wastewater treatment system discharge, a written request to complete the Local Government Review Form was sent to the Charlotte- Mecklenburg Clerk's office along with a copy of the NPDES permit application. The request was sent via certified mail with return receipt and was received by the Clerk's office on October 31,2014. A completed copy of the Local Government Review Form has not been received from the local government as of the date of this letter. A copy of the certified mail card is attached. If you have any questions or concerns,please do not hesitate to call me at(651)558-9226. ' Sincerely, LEGGETTE,BRASHEARS&GRAHAM, INC. ' (--j7r4.ejLtA, *-V — Rachelle A.Busser ' Environmental Engineer 11 ' State of i '1111n PAy+CJ`. ,County of 7Z"M et j On this ? � day of N WVMW ,aO K personally appeared before me,the said ' name 5 SP II' to me known and known to me to be the person described in and who executed the foregoing document and he(or she)acknowledged that he(or she)executed the ' same and being duly sworn by me,made oath that the statements in the foregoing docume a tr�a. My Commission expires .(Signature of Notary Public) ' N SARAH RAE JAPPE is(Official Seal) NOTARY PUBLIC MINNESOTA MY COMMISSION lie EXPIRES ' JANUARY 31,2017 ILLIN CONNECTICUT•FLORIDA• • A U • C G • SOTA•NUSSOURI NEW JERSEY•NEW YORK•NORTH DAKOTA•OHIO•PENNSYLVANIA•SOUTH DAKOTA•TEXAS•WISCONSIN ' •ER: COMPLETE THIS SECTION • • ON DELIVERY ■ Complete items 1,2,and 3.Also complete A. Sign item 4 if Restricted Delivery is desired. X , C ❑Agent ■ Print your name and address on the reverse (1 ❑Address ' so that we can return the card to you. B. Red b Tint N -e) D to o I've ■ Attach this card to the back of the mailpiece, C or on the front if space permits. D. Is delivery address different from item 17 Yes 1. Article Addressed to: If YES,enter delivery address below: ❑ No s +p ►e, G Ke 11 G CWL -I— oma C, WA Cln�f l a-�c_ N C. Zg 3. Service Type Certified Mail ❑Express Mail ' Registered ❑ Return Receipt for Merchandi ❑ Insured Mail ❑C.O.D. 4. Restricted Delivery?(Extra Fee) ❑Yes ' 2. Article Number 7011 0470 0000 2216 4285 � (Transfer from service label) PS Form 3811, February 2004 Domestic Return Receipt 102595-02-M-1! 1 1 1 1 1 1