NC0005177_Renewal (Application)_20150302

■
fMC1
CERTIFIED MAIL
RETURN RECEIPT REQUESTED
February ebruary 25, 2015
Mir 0G 2015
Division of Water Quality
1617 Mail Service Center Water Quality
Raleigh,NC 27699-1617
Permitting Section
Attn: Ron Berry NPDES Unit
Re: NPDES Renewal Application—Permit No. NC0005177
Dear Mr. Berry:
FMC Corporation—Lithium Division, located in Bessemer City, Gaston County
("FMC")hereby requests renewal of NPDES Permit No. NCO005177. This renewal
application is being submitted at least 180 days prior to the expiration date of the current
permit on August 31, 2015. FMC requests that if a new permit is not issued by the
expiration date,that the current permit remain in force until superceded by a new permit.
Enclosed are three signed originals of US EPA Form 2C and attachments.
Please note the following:
• The enclosed process flow diagram has been numbered for use with the treatment
systems referenced on US EPA Form 2C.II.B, for your convenience.
• Included is the Pace Analytical Services report analytical data only.
• Also included are 3 original of the signed renewal forms for stormwater outfall
004. Forms completed are those requested by Bethany Gerogoulias along with
attachments.
Air Treatment Construction Energy Fine Chemicals Glass 8 C ramia Greoses 8 Lubricants Polymers Pool Water Treatment
PO Box 795 Phone:[phone] [e-mail]
Bessemer City,NC 28016 Fax:[phone] www.fmclithium.com
MARKETS SERVED

•
FMC looks forward to discussing the permit renewal with the Division of Water Quality.
If you have questions feel free to contact me at 704-868-7630 or by e-mail to
[e-mail].
Sincerely
Rodney S. Willis
Environmental Engineer, Site ORC
FMC Lithium Division
Bessemer City,NC
Enclosures
3-Renewal applications for outfall 001
3-Renewal applications for outfall 004(stormwater)

NPDES STORMWATER RENEWAL
FMC CORPORATION
LITHIUM DIVISION
NPDES PERMIT NC0005177
OUTFALL 004
RECEIVED/DENRIDWR
MAR 0 2 2015
Water Quality
Permitting Section

Hermit coverage
Renewal Application Form NPDES Permit Number
NCDENR National Pollutant Discharge Elimination System
Stormwater Individual Permit NC0005177
Please provide your permit number in box in the upper right hand corner, complete the information in the space provided
below and return the completed renewal form along with the required supplemental information to the address indicated.
Owner Information * Address to which permit correspondence will be mailed
Owner/ Organization Name: FMC Corporation
Owner Contact: Bruce Urban, Plant Manager
Mailing Address: PO box 795
Bessemer City, NC 28016
Phone Number: 704-868-5254
Fax Number:
E-mail address: [e-mail]
Facility Information
Facility Name: FMC Corporation— Lithium Division
Facility Physical Address: 1115 Bessemer City Kings Mtn. Highway
Bessemer City, NC
Facility Contact: Rodney Willis
Mailing Address: PO Box 795
Bessemer City, NC 28016
Phone Number: 704-868-7630
Fax Number:
E-mail address: [e-mail]
Permit Information
Permit Contact: Rodney Willis
Mailing Address: PO Box 795
Bessemer City, NC 28016
Phone Number: 704-868-7630
Fax Number:
E-mail address: [e-mail]
Discharge Information
Receiving Stream: First Creek
Stream Class: C
Basin: Catawba
Sub-Basin: 03-08-37
Number of Outfalls: 1
Facility/Activity Changes Please describe below any changes to your facility or activities since issuance of your permit. Attached a
separate sheet if necessary.
No Changes in facility or activities since last permit issuance.
CERTIFICATION
I certify that I am familiar with the information contained in the application and that to the best of my knowledge and belief
such information j true, c9mple,jeand accurate.
Signature „r, ,�/�� (�/ `'�-- Date 2.0 -F-t6 2 vl
Print or type name of person signing above Title
SW Individual Permit Coverage Renewal
Please return this completed application form Stormwater Permitting Program
and requested supplemental information to: 1612 Mail Service Center
Raleigh, North Carolina 27699-1612

SUPPLEMENTAL INFORMATION REQUIRED FOR RENEWAL OF INDIVIDUAL
NPDES STORMWATER PERMIT
Two copies of each of the following shall accompany this submittal in order for the application
to be considered complete:
(Do not submit the site Stormwater Pollution Prevention Plan)
Initials
14c) 1. A current Site Map from the Stormwater Pollution Prevention Plan. The location of
industrial activities (including storage of materials, disposal areas,process areas and
loading and unloading areas), drainage structures, drainage areas for each outfall,
building locations and impervious surfaces should be clearly noted.
' -SL.) 2. A summary of Analytical Monitoring results during the term of the existing permit
(if your permit required analytical sampling). Do not submit individual lab reports.
The summary can consist of a table including such items as outfall number,
parameters sampled, lab results, date sampled, and storm event data.
(ZSw 3. A summary of the Visual Monitoring results. Do not submit individual monitoring
reports. The summary can consist of a table including such items as outfall number,
parameters surveyed, observations, and date monitoring conducted.
(ZSc,.) 4. A summary of the Best Management Practices utilized at the permitted facility.
Summary should consist of a short narrative description of each BMP's in place at
the facility. If the implementation of any BMP's is planned,please include
information on these BMP's.
U A 5. A short narrative describing any significant changes in industrial activities at the
permitted facility. Significant changes could include the addition or deletion of
work processes, changes in material handling practices, changes in material storage
practices, and/or changes in the raw materials used by the facility.
(ZSL) 6. Certification of the development and implementation of a Stormwater Pollution
Prevention Plan for the permitted facility(Sign and return attached form).
If the final year analytical monitoring of the existing permit term has not been completed
prior to filing the renewal submittal, then the last years monitoring results should be submitted
within 30 days of receipt of the laboratory reports. (i.e. do not withhold renewal submittal
waiting on lab results)

STORMWATER POLLUTION PREVENTION PLAN
DEVELOPMENT AND IMPLEMENTATION
CERTIFICATION
North Carolina Division of Energy, Mineral, and Land Resources -Stormwater Permitting
Facility Name: FMC Corporation, Lithium Division
Permit Number. NCD0005177
Location Address: 1115 Bessemer City—Kings Mtn. Hwy.
Bessemer City, NC 28016
County: Gaston
"I certify, under penalty of law, that the Stormwater Pollution Prevention Plan (SPPP) document and all attachments were
developed and implemented under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information required by the SPPP. Based on my inquiry of the
person or persons who manage the system, or those persons directly responsible for gathering the information, the
information gathered is, to the best of my knowledge and belief, true, accurate and complete."
And
"I certify that the SPPP has been developed, signed and retained at the named facility location, and the SPPP has been
fully implemented at this facility location in accordance with the terms and conditions of the stormwater discharge
permit."
And
"I am aware that there are significant penalties for falsifying information, including the possibility of fines and
imprisonment for knowing violations."
Sign (according to permit signatory requirements) and return this Certification. DO NOT
SEND STORMWATER POLLUTION PREVENTION PLAN WITH THIS CERTIFICATION.
v[
SignatureDate
4&@ /0/(Aterk_ 2s ft-b 20ts
Print or type name of person signing above Title
SPPP Certification 10/13

NPDES regulatory sampling Notes:
2011 * First month of new permit
2011,Outfall 004
Monthly 1 Quarterly 004,2011,storm event sampling
o _o
E LL a
N N E <y `
a O O
o O -
c 'o a a c
�
c a O N O c 5 O L. C,N In C
. 15 _ ct r m m O O t < a
C 3 U T
c 3 U d U =_ z Q. c d'
2 c a ' L 12 m zc rn o 2, a z m ' ::
cI 0 VI O (n 0 o O T O O O O O
L
O. U I- I- W 2 c o. U I- m i- F- 2 I- I•- I- I- I- 0
Units MGD SU US mg/I _mg/I ug/I uglI Units MGD SU us mg/I mg/I mg/I mg/I mg/I mgll ug/I In
January 0.222 7.8 1115 <5.0 36 <5 <5 Period 1 0.115 7.3 766 <5.6 <2.0 27.2 <5.0 <0.50 <0.50 <5.0 1.24 6/5/2011
Feb* _ 2.392 7.9 1070 <2.8 J _ First month of New NPDES permit Period 2 1.703 7.6 442 53 4.9 16.0 <5.0 <0.70 0.060 <5.0 1.71 11/16/2011
T
March 0.434 8.0 1503 <2.8 _ _ Visual Monitoring
April 0.754 7.9 837 <2.5 26.8 _ ___ Color Odor Clarity Foam F.Solids S solids Oil Sheen Erosion outfall
May 0.177 7.6 905 <8.3 _ _ Period 1 Clear None Clear None None None None None
June 0.022 7.1 780 <2.6 28.6 Period 2 Lt Pink None Muddy Trace None Some silt None None
July No discharge for month
August No discharge for month _ Notes from Visual Observations
Sept. No discharge for month
Oct. 0.464 7.4 774 <2.6 32.0
Nov. 0.004 7.8 9.34 52.5 16.0
Dec. 0.406 8.0 756 <2.8

2012 Outfall 004
Monthly Quarterly 004,2012,storm event sampling
a
e
a O
a N 2
g O r Z
T. +
=
Z N
am a E Y2
o .Z. s § o m a
CI S o
r 2 42o To
c 0 c 0 0 a ii °� ce
a w Z
::
c o u)i o 2 i o u/i O o 0 0 0 0 o a
O F- I- a. o F- m F- F- H F- F- F- 0
Units MO su us mg/I mgAnits P102 su Us mgll \ mg/I _ mgll npA mg1F mg/F ' ugll In
January 0.271 8.3 803 <5.6 27.7 Period 3 0.063 6.9 892 <2.5, <2.0 30.4 <5.0 <0.70 <0.050 <0.050 0.70 5/9/2012
Feb 0.350 7.7 804 <2.8 Period 4 0.620 6.8 407 <2.5 <2.0 4.4 <5.0 0.021 <0.050 <5.0 0.10 12/10/2012
March 0.155 7.6 930 <2.5 Visual Monitoring
April 0.406 7.6 854 <2.5 32.6 Color 011or Clarity Foam F.Solids, S solids Oil Sheen Erosion outfall
May 0.012 7.1 1040 21 Period 3 Clear None Clear None None None None None
June 0 Period 4 Clear None Clear Trace None None None None
July 0.034 7.1 933 <2.7 33.3
August 0.063 7.2 788 5 31.1 Notes from Visual Qbseryati�na%
Sept. 0.323 7.3 817 <5.0
Oct. 0.079 6.9 905 5 33.0
Nov. 0
Dec. 0.620 6.8 407 <2.5 4.4

2013,Outfall 004
Monthly Quarterly 004,2013,storm event sampling
I O M
a O
m z
U +
o N
O 0 ,:, z
U. U 2 +
2 0
In N E Y 0
O a 0 a 0 I- o
c _
C P 0 ' o ra
rn
L R
0 'U ' aa 'C
iv a.C 7 U C 7 U Il
0-
m K
Pa 'O as C n A 5Z
d
N C N O N R
I O in 0 O O AC =. 0 FN 0
E O. 0 I- CO I- I- I- I- I- H 0
Units MGD su us mg/I mg/I Units MGD SU US mg/I mg/I mg/I mg/I mg/I mg/I ugh In
January 0.588 6.9 722 3.3 31.5 Period 5 0.406 7.0 832 <2.6 <2.0 26.4 <5.0 <0.12 <0.050 <1.0 0.90 4/4/2013
Feb 0.199 7.9 827 <2.5_ Period 6 1.926 7.2 629 16 13.6 17.2 <5.0 NA NA 1.41 10/7/2013
March 2.110 7.6 717 <2.5 Visual Monitoring
April 0.271 7.8 850 <2.6 26.4 Color Odor Clarity Foam F.Solids S solids Oil Sheen Erosion outfall
May 0.350 7.4 497 3.2 Period 5 Clear None Clear None None Low None None
June 0.135 7.2 763 3.1 Period 6 Lt Brown None 3 None 2 2 None None using scale of 1-5
a
July 0.620 7.4 737 <2.6 22.3
August 0.199 7.6 688 <2.5 Notes from Visual Observations
Sept. 0.034 7.8 785 <2.5
Oct. 0.034 7.6 787 <2.5 21.4
Nov. 0.004 7.2 983 <5.3
Dec. 0.406 7.1 715 <5.1

2014,Outfall 004
Monthly Quarterly 004,2014,storm event sampling
N
0 r1
.0 0
m Z
U +
O N
o Z
_O 0 >,
Z
U- LL I +
0 w 0 o E 1- O -
O -0 O �, a y r
L N
CD d 0.
c '> O c '> o O 07 0 C
:° 2 0
C V C 0 d d c cc
'0 :° c cn o m Z m z ' iii
C = o co o I 0 In 0 o o 0 0 0 0
d U F-- I- 0. 0 I- m I- I- I- I- I- F 0
Units MGD SU US mg/I mg/I Units MGD SU US mg/I mg/I mg/I mg/I mg/I mg/I ug/I in
January 1.045 7.8 810 <5.2 20.5 Period 7 0.754 7.7 642 <5.0 <20 16.5 <5.0 NA NA NA
Feb 0.686 7.9 908 <2.5 Period 8 0.155 7.0 939 18 2.5 31.0 <5.0 NA NA NA
March 0.720 7.9 870 <2.6 Visual Monitoring
April 0.525 7.5 824 <2.6 21.4 Color Odor Clarity Foam F.Solids S solids Oil Sheen Erosion outfall
May 0.271 7.8 794 <2.5 Period 7 Lt Green None 2 Trace 1 1 None None using scale of 1-5
June 0.199 7.9 790 <26 Period 8 '" None 2 None 1 2 None None using scale of 1-5
July 0.079 7.6 849 <2.7 24.4
August Notes from Visual Observations
Sept. "Clear to Grey Tan
Oct. 0.048 7.5 979 <2.6 27.6
Nov. 0.063 7.7 1004 <2.6
Dec. 0.155 8.0 897 <2.6

Pace Analytical Services,Inc.
.(le„.../a
9800 Kincey Ave. Suite 100
PeAna/ytica/®
�} Huntersville,NC 28078
www.pacelabs.com 00
�./
[phone]
ANALYTICAL RESULTS
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 004 Lab ID: 92233379002 Collected: 01/14/15 10:25 Received: 01/14/15 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua!
1664 SGT-HEM,TPH Analytical Method:EPA 1664B
Total Petroleum Hydrocarbons ND mg/L 5.0 1 01/16/15 09:53
2540D Total Suspended Solids Analytical Method:SM 2540D
Total Suspended Solids ND mg/L 2.9 1 01/21/15 03:31
5210B BOD,5 day Analytical Method:SM 5210B
BOD,5 day ND mg/L 2.0 1 01/15/15 05:57 01/20/15 06:51
4500 Chloride Analytical Method:SM 4500-CI-E
Chloride 29.0 mg/L 1.0 1 02/11/15 20:11 16887-00-6 M1,R1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full.
Date:02/13/2015 03:34 PM without the written consent of Pace Analytical Services,Inc.. Page 10 of 56

Summary of Best Management Practices (BMPs)
• Non-Structural BMPs include:
o General operating practices
• Promptly clean up any spilled material
• Tanks, piping,and dikes are frequently observed by facility personnel during
normal plant duties. Any sign of deterioration or leakage which might cause
a spill or accumulation of fluids inside diked areas is reported to the Shift
Supervisor.
• Incident reporting
• Promptly report and record spills or deficiencies in equipment or
operating practices to determine root cause and implement timely
corrective measures.
o Preventive maintenance activities:
• Regular inspections are conducted to identify visible leaks from tank seams,
gaskets, rivets,and bolts that can cause significant accumulation of liquids.
Any such leak is immediately reported for corrective action.
o Good housekeeping involves maintaining a clean and orderly work environment.
Examples of good housekeeping activities at the facility include:
• Maintaining a routine clean-up program using hand shovels, hand brooms,
or cleaning machines.
• Storing containers away from direct traffic paths and stacking containers(if
necessary) in accordance with manufacturer's instructions to avoid damage
and spills
• Labeling containers in a way that shows their contents.
Covering receptacles and drums when possible or protecting them from
storm water exposure(e.g., using indoor storage).
• Preventing potential overflow of harmful chemicals by ensuring regular pick-
up and disposal of waste material.
• Any spilled materials are promptly cleaned-up for proper disposal or
reintroduced to the process system.
• Structural BMPs
o Secondary Containment of Chemicals and oils
• Secondary containment structures generally consist of concrete floors and
walls around facility storage tanks. These containment structures are sized
large enough to contain the volume of the largest tank within the
containment area, plus the volume of a hypothetical 10-year, 24-hour
rainfall event(approximately 5.5 inches of rainfall). All materials of
construction for the storage tanks and containment areas are compatible
with the materials stored in the tanks. Each containment area is equipped
with a manually-operated drainage valve that remains locked and/or pumps
that are accessible only by authorized personnel,to prevent any
unauthorized release

o Storage of Chemicals from contamination by rain-fall
o Divert storm water away from,around (instead of across or through) regulated
"industrial activities"
o Incorporate storm water conveyances,detention basins,grading,and paving to
collect storm water runoff and minimize discharges of storm water beyond the
facility boundary.
FMC chose to combine its Stormwater Pollution Prevention Plan (SWPPP)along with the Spill
Prevention Controls and Counter(SPCC) measures plan into"ONE PLAN". The table of contents of
the"ONE PLAN" are attached.

FMC,Inc. SPCC/SWPPP Integrated Contingency ONE PLANT"'
Bessemer City,NC Revision No.5 July 2010
Table of Contents
1.0 INTRODUCTION (SWPPP) 1
1.1 Regulatory Requirements 1
1.2 How to Use This ONE PLAN" 2
2.0 APPROVALS AND CERTIFICATIONS 4
2.1 Management Policy and Approval 4
2.2 Professional Engineer Certification 5
3.0 ORGANIZATION AND RESPONSIBILITIES 6
3.1 Spill Response Management System 6
3.2 Storm Water Pollution Prevention Team 6
3.3 Arrangements with Outside Organizations 6
4.0 FACILITY INFORMATION 7
4.1 Location and Description 7
4.2 Facility Contact and Qualified Individuals Information 7
4.3 Description of Operations 7
4.4 Description of Storm Water and Waste Water Discharge Locations 8
4.5 Security [ 10
5.0 MATERIAL STORAGE AND HANDLING INFORMATION 11
5.1 Material Storage Locations and Descriptions 11
5.2 Rail Car and Truck Loading/Unloading Areas 11
5.3 Waste Materials Storage and Disposal 11
5.4 Sewer/Impoundment Facilities 12
6.0 SPILL/RELEASE RISK AND HAZARD ASSESSMENT 13
6.1 Spill/Release Scenarios 13
6.2 Potential Sources of Storm Water Pollutants 13
6.3 Spill History 14
6.4 Existing Storm Water Monitoring Data 14
7.0 SPILL PREVENTION PROGRAM 15
7.1 Overview 15
7.2 Secondary Containment 15
7.3 Material Compatibility 15
7.4 Protection from Spills Resulting from Mechanical Failures 16
7.5 Discharge Detection Systems 17
7.6 Rail Car and Truck Loading/Unloading Operations 17
8.0 STORMWATER MANAGEMENT 18
8.1 Non-Structural BMPs 18
8.2 Visual Inspections 19
8.3 Structural BMPs 19
9.0 SPILL/RELEASE RESPONSE 21
9.1 Spill Response Process 21
9.2 Incident Classification and Response 21
9.3 Transportation-Related Spills 22
9.4 Health and Safety Considerations 22
9.5 Cleanup and Disposal 23
9.6 Documentation 23
One Plan Rev 5 July 29,2010.docx i

FMC,Inc. SPCC/SWPPP Integrated Contingency ONE PLANTM
Bessemer City,NC Revision No.5 July 2010
10.0 NOTIFICATION AND REPORTING REQUIREMENTS 24
10.1 Reporting Responsibility 24
10.2 Reportable Incidents and Requirements 24
10.3 Emergency Incident Reporting 24
10.4 Corrective Actions Reports for Incidents 25
10.5 Non-Incident or Regular Environmental Reporting 25
11.0 MAINTENANCE, INSPECTION, TESTING, AND MONITORING 26
11.1 Preventive Maintenance/Good Housekeeping of Tanks and Storage Areas 26
11.2 Integrity Testing of Bulk Oil Storage Containers 26
11.3 Inspection and Testing Programs 27
11.4 Inspection Records 28
11.5 Storm Water and Monitoring Program 28
12.0 TRAINING 31
12.1 Training Requirements 31
12.2 Training and Meeting Logs/Documentation 32
13.0 PLAN IMPLEMENTATION AND UPDATING 33
13.1 Review and Update Procedures 33
13.2 Program Review/Update Requirements 33
13.3 Revisions Pursuant to Training or Spill/Release Response 34
One Plan Rev 5 July 29,2010.docx ii

FMC,Inc. SPCC/SWPPP Integrated Contingency ONE PLAN
Bessemer City,NC Revision No.5 July 2010
LIST OF TABLES
Table No. Title
1-1 Matrix of Requirements per SPCC Plan, 40 CFR 112
1-2 Matrix of Requirements per Control of Pollution by Oil and Hazardous
Substances, SPCC Plan, 33 CFR 153
1-3 Matrix of Requirements per Determination of Reportable Quantities,
SPCC Plan,40 CFR 117, SWPPP
1-4 Matrix of Requirements per SWPPP
5-1 Inventory of Secondary Containment for Facility Storage Tanks
5-2 Chemicals Classified as SARA 313 Water Priority Pollutants and/or
Hazardous Substances
5-3 Inventory of Oil Capacities of Operational Equipment
9-1 Area Spill Kit Items
11-1 Bulk Oil Storage Container Inspections and Integrity Testing Summary
LIST OF FIGURES
Figure No. Title
1 Site Location Map(USGS Section)
2 Facility Site Plan—Secondary Containment (40-101A-5-3411, Rev. 2)
3 Site Drainage(Boundary Topo)
4 Master Site Plan—Storm and Effluent Drains(40-101A-5-3100, Rev. 7)
5 Specialty Organics, Master Site Plan, Secondary Spill Containments (40-
301-5-3009)
6 Specialty Organics, Secondary Spill Containments R&ID (40-301-5-1603)
APPENDICES
A Inspection, Incident and Emergency Call-in Forms
B Facility NPDES Permit
One Plan Rev 5 July 29,2010.docx iii

NPDES INDUSTRIAL DISCHARGE RENEWAL
FMC CORPORATION
LITHIUM DIVISION
NPDES PERMIT NC0005177
OUTFALL 001
RECEIVED/DENR/DWR
MAR 0 2 2015
Water Quality
Permitting Section

•
EPA I.D.NUMBER(cop)from Item 1 of Form 1) Form Approved.
NCD000771964 OMB No.2040-0086.
Please print or type in the unshaded areas only. Approval expires 3-31-98.
FORM(� U.S.ENVIRONMENTAL PROTECTION AGENCY
2�+ -CEPAEXISTING MANUFAAPPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
CTURING,COMMERCIAL,MINING AND SILVICULTURE OPERATIONS
NPDES Consolidated Permits Program
I.OUTFALL LOCATION
For each outfall,list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A.OUTFALL NUMBER B.LATITUDE C.LONGITUDE
(list) 1.DEG. 2.MIN. 3.SEC. 1.DEG. 2.MIN. 3.SEC. D.RECEIVING WATER(name)
001 35.00 15.00 43.00 81.00 17.00 54.00 First Creek
004 35.00 15.00 43.00 81.00 17.00 54.00 First Creek
II.FLOWS,SOURCES OF POLLUTION,AND TREATMENT TECHNOLOGIES 11111.1111111.11111
A. Attach a line drawing showing the water flow through the facility.Indicate sources of intake water,operations contributing wastewater to the effluent,and treatment units
labeled to correspond to the more detailed descriptions in Item B.Construct a water balance on the line drawing by showing average flows between intakes,operations,
treatment units,and outfalls.If a water balance cannot be determined(e.g.,for certain mining activities),provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall,provide a description of:(1)All operations contributing wastewater to the effluent,including process wastewater,sanitary wastewater,cooling water,
and storm water runoff; (2)The average flow contributed by each operation; and (3)The treatment received by the wastewater. Continue on additional sheets if
necessary.
1.OUT- 2.OPERATION(S)CONTRIBUTING FLOW 3.TREATMENT
FALL b.AVERAGE FLOW b.LIST CODES FROM
NO.(list) a.OPERATION(list) (include units) a.DESCRIPTION TABLE 2C-1
1) Misc. Salts and Cat. Phosphate -5.000 gals/mth None
001X X
2) LiOCL Air Scrubber Waste Water -100 gpm H202 Addition and Equalization 2 L
3) Boiler Blowdown None
-15 gpm x x
4)LiC1 RO permeate and condesate -9,550 GPD Reverse Osmosis 1 S
5) left blank
6) Compressor Condensate
<1
gpm x X
7) Li Hydroxide RO Reverse Osmosis
-5,000 gals/mth 1 S
8) Battery Metal Cooling Tower None
clo gpm X X
9) Combined Plant Waste Water 130 gpm pH adjustment 2 X
10) Li Hydroxide Cooling Twr. 35 None x
gpm x
11) R&D Pond stormwater management Setteling
10 gpm X X
OFFICIAL USE ONLY(effluent guidelines sub-categories)
EPA Form 3510-2C(8-90) PAGE 1 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C.Except for storm runoff,leaks,or spills,are any of the discharges described in Items II-A or B intermittent or seasonal?
©YES(complete the following table) ❑NO(go to Section Ill)
3.FREQUENCY 4.FLOW
a.DAYS PER B.TOTAL VOLUME
2.OPERATION(s) WEEK b.MONTHS a.FLOW RATE(in mg,I) (.gxcih.Hith soros)
1.OUTFALL CONTRIBUTING FLOW (.slxcii5. PER YEAR 1.LONG TERM 2.MAXIMUM 1.LONG TERM 2.MAXIMUM C.DURATION
NUMBER(list) (list) average) (speck,,,,,Age) AVERAGE DAILY AVERAGE DAILY (in das''s)
001 1) Misc. Salts and Cat. Phosphate --- 6 --- 0.005 --- 5,000 gal --
11) R&D Pond stormwater management 7 6 --- 0.015 ---- 0.010 MG 180
III.PRODUCTION
A.Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
❑YES(complete Item III-B) ®NO(go to Section IV)
B.Are the limitations in the applicable effluent guideline expressed in terms of production(or other measure of operation)?
❑YES(complete Item III-C) ❑NO(go to Section IV)
C.If you answered"yes"to Item III-B,list the quantity which represents an actual measurement of your level of production,expressed in the terms and units used in the
applicable effluent guideline,and indicate the affected outfalls.
1.AVERAGE DAILY PRODUCTION 2.AFFECTED OUTFALLS
a.QUANTITY PER DAY b.UNITS OF MEASURE C.OPERATION,PRODUCT,MATERIAL,ETC. (list outfall numbers)
(spec,fv)
IV.IMPROVEMENTS
A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application?This includes,but is not limited to,
permit conditions,administrative or enforcement orders,enforcement compliance schedule letters,stipulations,court orders,and grant or loan conditions.
❑YES(complete the following table) 0 NO(go to Item IV-B)
1.IDENTIFICATION OF CONDITION, 2.AFFECTED OUTFALLS 3.BRIEF DESCRIPTION OF PROJECT 4.FINAL COMPLIANCE DATE
AGREEMENT,ETC.
a.NO. b.SOURCE OF DISCHARGE a.REQUIRED b.PROJECTED
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges)you now have underway or which you plan.Indicate whether each program is now underway or planned,and indicate your actual or planned schedules for
construction.
p MARK"X"IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C(8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA I.D.NUMBER(copy from Item I of Form I)
CONTINUED FROM PAGE 2 NC000771964
V.INTAKE AND EFFLUENT CHARACTERISTICS
A,B,&C: See instructions before proceeding-Complete one set of tables for each outfall-Annotate the outfall number in the space provided.
NOTE:Tables V-A,V-B,and V-C are included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions,which you know or have reason to believe is discharged or may be discharged
from any outfall.For every pollutant you list,briefly describe the reasons you believe it to be present and report any analytical data in your possession.
1.POLLUTANT 2.SOURCE 1.POLLUTANT 2.SOURCE
VI.POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS
Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct?
®YES(list all such pollutants below) ❑NO(go to Item I'1-B)
EPA Form 3510-2C(8-90) PAGE 3 of 4 CONTINUE ON REVERSE

•
CONTINUED FROM THE FRONT
VII.BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
©YES(identify the test(s)and describe their purposes below) ❑NO(go to Section VIII)
Chronic Toxicity, Presently required by our NPDES discharge Permit of outfall 001.
VIII.CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
®YES(list the name,address,and telephone number of and pollutants analyzed by, ❑NO(go to Section IX)
each such laboratory or firm below)
A.NAME B.ADDRESS C.TELEPHONE D.POLLUTANTS ANALYZED
(area code&no.) (fist)
Pace Analytical Services 9800 Kincey Ave. Suite 100 704-875-9092 See page 4 of Pace
Huntersville, NC 28078 Analytical report
Pace Analytical Services 2225 Riverside Dr. See page 4 of Pace
Asheville, NC 828-254-7176 Analytical report
Pace Analytical Services 1638 Roseytown Rd. Suites 2,3&4 724-850-5600 See page 4 of Pace
Greensburg, PA 15601 Analytical report
Pace Analytical Services 8 East Tower Circle, 386-672-5668 See page 4 of Pace
Ormond Beach, FL 32174 Analytical report
Pace Analytical Services 205 East Meadow Road Suite A 336-623-8921 See page 4 of Pace
Eden, NC 27288 Analytical report
Statesville Analytical PO Box 228 704-872-4697 See page 4 of Pace
Statesville, NC 28687 Analytical report
IX.CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there
are significant penalties for submitting false information,including the possibility of fine and imprisonment for knowing violations.
A.NAME&OFFICIAL TITLE(type or print) B.PHONE NO.(area code&no.)
Bruce Urban (704) 868-7650
C.SIGNATURE D.DATE SIGNED
4,67.—....
EPA Form 3510-2C(8-90) PAGE 4 of 4

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY.You may report some or all of this information EPA I.D.NUMBER(copy from Item 1 of Form 1)
on separate sheets(use the same format)instead of completing these pages. NC000771.964 .
SEE INSTRUCTIONS.
OUTFALL NO.
V.INTAKE AND EFFLUENT CHARACTERISTICS(continued from page 3 of Form 2-C)
PART A-You must provide the results of at least one analysis for every pollutant in this table.Complete one table for each outfall.See instructions for additional details.
3.UNITS 4.INTAKE
2.EFFLUENT (.specify if blank) (optional)
b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
a.MAXIMUM DAILY VALUE (if available) (if available) AVERAGE VALUE
1.POLLUTANT (1) (1) d.NO.OF a.CONCEN- (1j b.NO.OF
CONCENTRATION (2)MASS CONCENTRATION (2)MASS (1)CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Biochemical Oxygen
11.2 mg/1 48.7 lb --- --- 1.75 mg/1 135 lbs 8 mg/1 lbs
Demand(BOD)
b.Chemical Oxygen 30 mg/1 --- --- --- --- --- 1 mg/1 lbs
Demand(COD)
c.Total Organic Carbon 3.7 mg/1 --- --- --- --- --- 1 mg/1 lbs
(TOO
d.Total Suspended 3.0 0 m 1 12.1 lb --- --- 0.19 m 1 14.4 lbs 16 m 1 lbs
Solids(TSS) 9/ 9/ 9/
e.Ammonia(asN) <0.1 mg/1 --- --- --- --- --- 1 mg/1 lbs
VALUE VALUE VALUE VALUE
f.Flow 0.537 MG 16.26 MG 9.2 MGD 1 yr --- MG
g.Temperature VALUE VALUE VALUE VALUE
h.Temperature VALUE VALUE VALUE VALUE
(summer) 27.05 --- --- °C
MINIMUM 'MAXIMUM MINIMUM (MAXIMUM
i.pH 7.6 8.3 --- 31 STANDARD UNITS
PART B- Mark"X"in column 2-a for each pollutant you know or have reason to believe is present.Mark"X"in column 2-b for each pollutant you believe to be absent.If you mark column 2a for any pollutant which is limited either
directly,or indirectly but expressly, in an effluent limitations guideline,you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a,you must provide
quantitative data or an explanation of their presence in your discharge.Complete one table for each outfall.See the instructions for additional details and requirements.
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM AVERAGE
ANDa b. a.MAXIMUM DAILY VALUE (ifavailahle) (if available) VALUE
CAS NO. BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(if available) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Bromide
(24959-67-9) X 0.81 1 mg/1
b.Chlorine,Total
Residual X <0.11 1 mg/1
c.Color X <25 1 ADMI
d.Fecal Coliform X <1.0 1 CFU/100m
e.Fluoride
(16984-48-8) X <0.50 1 mg/1
f.(as'N)te-Nitrite a <0.020 <0.10 4 mg/1
EPA Form 3510-2C(8-90) , ` PAGE V-1 CONTINUE ON REVERSE

ITEM V-B CONTINUED FROM FRONT
2.MARK'X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional) -_
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
ANDa, b. a.MAXIMUM DAILY VALUE (if available) (if available) AVERAGE VALUE
CAS NO. BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
0/available) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
g.Nitrogen,
><,
Total Organic(as c <0.5 0 1 mg/1
h.Oiand X <5.0 1 mg/1
Grease
i.Phosphorus `
(as P),Total /X\ <0.050 1 mg/1
(7723-14.0)
j.Radioactivity
(t)Alpha,Total X 7.64+-2.41 1 pCi/L
(2)Beta,Total X 6.28+-1.47 1 pCi/L
(3)Radium, X .244+-.405 1 pCi/L
Total
(4)Radium 226, X .062+-.325 1 pCi/L
Total
k.SulfateX
(°'Sa)
�•) 342 1 mg/1
(14808-79-8)
I(alS)Sulfide X <0.10 1 mg/1
m.Sulfite
(as SO,) X <2.00 1 mg/1
(14265-45-3)
n.Surfactants X 0.17 1 mg/1
o.Aluminum, X
Total <100 1 ug/1
(7429-90-5)
p.Barium,Total X 3 5.0 _ 1 ug/1
(7440-39-3)
(7440-42.8)q.Boron,Total X 74.8 1 ug/1
(7
r.Cobalt,Total
(7440-48-4) X <5.0 1 ug/1
s(7439-89-6)Total
Iron'
X <7 1.9 1 ug/1
t.Magnesium. X
TOS 45000 1 ug/1
(7439-95-4)
u.Molybdenum, X
Total <5.0 1 ug/1
(7439-98-7)
v.Manganese. X
TOS 206 1 ug/1
(7439-96-5)
w.T ,Total
(7440031 5) X <5.0 1 ug/1
(7
x.
Titanium,
T X
Total <5.0 1 ug/1
(7440-32.6)
EPA Form 3510-2C(8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D.NUMBER(copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C NC000771964 001
PART C- If you are a primary industry and this outfall contains process wastewater,refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for.Mark'X'in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals,cyanides,and total phenols.If you are not required to mark column 2-a(secondary industries,nonprocess wastewater outfalls,and nonrequired GC/MS
tractions),mark'X"in column 2-b for each pollutant you know or have reason to believe is present.Mark'X'in column 2-c for each pollutant you believe is absent.If you mark column 2a for any pollutant,you must
provide the results of at least one analysis for that pollutant.If you mark column 2b for any pollutant,you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater.If you mark column 2b for acrolein.acrylonitrile,2,4 dinitrophenol,or 2-methy1-4,6 dinitrophenol,you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater.Otherwise,for pollutants for which you mark column 2b,you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged.Note that there are 7 pages to this part;please review each carefully.Complete one table(all 7 pages)for each outfall.See instructions for
additional details and requirements.
2.MARK"X' 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
ANDa, b. c. a.MAXIMUM DAILY VALUE (ijavailable) VALUE(i(available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED d.NO.OF a.CONCEN- b.NO.OF
(if available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (1) ANALYSES TRATION b.MASS (1) ANALYSES
(2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS
METALS,CYANIDE,AND TOTAL PHENOLS
1M.Antimony.Total /�
�/ X <5.0 1 ug/1
(7440-36-0)
(7440-38 2),total X `X, <10.0 1 ug/1
(743M.0-41-7)m,Tdal X 7� <1.0 1 ug/1
(7440-41-7)
(7 44�9m,Total X X <1.0 1 ug/1
5M.Chromium, /�
Total(7440-47-3) X X <5.0 1 ug/1
6M.Copper,
(7440-50-8) Toth X X <5.0 1 ug/1
7M.Lead,Total
(7439-92-1) X X <5.0 1 ug/1
8M.Mercury,Total
(7439-97-6) X X 0.747 1 ng/1
9M.Nickel,Total
(7440-02-0) X X <5.0 1 ug/1
10M.Selenium,
Total(7782-49-2) X X <10.0 1 ug/1
11M.Silver,Total
(7440-22-4) X X <5.0 1 ug/1
12M.Thallium,
Total(7440-28-0) X X <10.0 1 ug/1
13M.Zinc,
(7440-66-6)otal X X <10.0 1 ug/1
14M.Cyanide,
Total(57-12-5) X X <0.0080 1 mg/1
i
To M.Phenols, X X <0.010 1 mg/1
DIOXIN /�
2.3,7.8-Tetra- \ / DESCRIBE RESULTS
chkwodibenzo-P- /X\
Dioxin(1764-01-6)
EPA Form 3510-2C(8-90) PAGE V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK''X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED d.NO.OF a.CONCEN- b.NO.OF
r available) REQUIRED PRESENT ABSENT CONCENTRATION(1 (2)MASS CONCENTRATION (1) ANALYSES TRATION b.MASS (1) ANALYSES
(f (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS
GC/MS FRACTION-VOLATILE COMPOUNDS
7V.Ac2-dein
(107-02-8) X X <5.0 1 ug/1
2V. trite X X <50 1 ug/1
(107-13-1)-13-1)
(71-43-2)
713V.43
p1�3 2)2) X X <2.0 1 ug/1
4V.Bis(Chloro- \ , \/
methyl)Ether X x <5.0 1 ug/1
(542-88-1) / \ , `
2nn
(7 X/ X <2.0 1 ug/1
(75-25-2)5-2) /�
6V.Carbon
Tetrachloride X X <2.0 1 ug/1
(56-23-5) .
7V. obenzene
X X <2.0 1 ug/1
(108-90-7)
8V.Chlorodi- \ / \,
bromomethane x J( <2.0 1 ug/1
(124-48-1) / ` ' `
9V. ethane X X
(75-00-3)00-3) <2.0 1 ug/1
0o.
eX X
thyivirin ryl Ether er <5.0 1 ug/1
(110-75-8)
11V.7-66-3oroform(6 ) X X <2.0 1 ug/1
12V.DichloX X
oO1nan
� 'ne <2.0 1 ug/1
(75-27-4)
13V. X X
Dichloro-
difluoromethane <2.0 1 ug/1
(75-71-8)
14Vetha a(75-4-3) X X <2.0 1 ug/1
ethane(75-34-3)
etha15Ve(1,2107- 6-o-
X X <2.0 1 ug/1
ethane(107-06-2) /�
16Vt,t(75-3-4 X X <2.0 1 ug/1
ethylene(75-35-4)
ropane(7875)
pX X <2.0 1 ug/1
propane(78 887--5) /�
18V.1,3-Dichloro-
\/
propylene
\/X J( <2.0 1 ug/1
(542-75.6)
19V.
(100-41-00-41- X X <2.0 1 ug/14) ^ `,
20V.Methyl X <2.0 1 ug/1
Bromide(74-83-9) /` `,
21V.Methyl X <2.0 1 ug/1
Chloride(74-87-3)
EPA Form 3510-2C(8-90) PAGE V4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4
2.MARK'X' 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c, a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED d.NO.OF a.CONCEN- b.NO.OF
((available) REWIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (1) ANALYSES TRATION b.MASS (1) ANALYSES
(2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS
GC/MS FRACTION-VOLATILE COMPOUNDS` (continued)(c
22V.Methylene 7� <2.0 1 ug/1
Chloride(75.09-2)
23V.1.1.2,2-
Tetrachloroethane X X <2.0 1 ug/1
(79-34-5)
24V.Tetrachloro-
ethylene(127-18.4) X X <2.0 1 ug/1
25V. X X <2.0 1 ug/1
(108-88-3) /�
26V.1,2-Trans-
Oichloroethylane X X <2.0 1 ug/1
(156-60-5)
27V.1,1,1-Trichloro-
ethane(71-55-6)
,1,1-Trkbro-
ethane(71-55-6) X X <2.0 1 ug/1
28V.1,1,2-Trichloro- X X <2.0 1 ug/1
ethane(79-00-5)
29V Trichloro-
ethyene(79-01-6) X X <2.0 1 ug/1
30V.Trichloro- ` ,
tluoromethane X X <2.0 1 ug/1
(75-69-4) , `
(7 Vinyl Chloride X X <2.0 1 ug/1
GC/MS FRACTION-ACID COMPOUNDS
1A.2-Chlor
(95-57-8) ophenol X X <5.0 1 ug/1
phenolro-
phenol(120-83-2) X X <5.0 1 ug/1
2,4-Dimethyl-
phenol
X X <10.0 1 ug/1
phenol(105 67-9)
4A.4,6-Dinitro-0-
CresolX X <20.0 1 Ug/1
(534-52-1)
5A.2,4-Dinitro-
phenol(51-28-5)
X X <50.0 1 ug/1
6A.2-Nitrophenol X X <5.0 1 ug/1
(88-75-5)
7A.4-Nitrophenol
(100-02-7) X X <50.0 1 ug/1
8A.sol(59 50-7) X X <5.0 1 ug/1
Cresol(59 50 7)
9A.Penlachloro-
X X <10.0 1 ug/1
phenol(87-86-5) _
95
(10 X X <5.0 1 ug/1
(108-95-2)2)
phenol(8-T5-2) X X <10.0 1 ug/1
phenol(88-05-2)
EPA Form 3510-20(8-90) PAGE V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK''X' 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(f available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION-BASE/NEUTRAL COMPOUNDS
18 Acenaphthene
(83-32-9) X 7� <5.0 1 ug/1
2B Ac1ene X X <5.0 1 ug/1
(208-968)6-8)
38.
(12Anthr-12-7acene X X <5.0 1 ug/1
(lzatz-7)
4B.8nzldine
(92-87-5) X X <50.0 1 ug/1
58.Benzo(a)
Anthracene X X <5.0 1 ug/1
(56-55-3) •
6B.Benzo(a) X X <5.0 1 ug/1
Pyrene(50-32-8)
73,4-Benzo-
fluoranthene
X X <5.0 1 ug/1
(205-99-2)
813.Benzo(ghi)
Perylene(191.24-2) X X <5.0 1 ug/1
98.Benzo(k)
Fhraanthene X X <5.0 1 ug/1
(207.08-9)
10B.Bis(2-Chloro-
ethoxy)Methane
2-Chloro-
ethnry)Methane X X <10.0 1 ug/1
(111-91-1)
118.Bls(2-Chloro-
ethyl)Ether
2-Chloro-
etlrv/)Ether X X <5.0 1 ug/1
(111.44.4) ,
128.Bis(2-
Chlornisapropvl) X X <5.0 1 ug/1
Ether(102-80.1)
138.Bis(2-Ethyl-
keg!)Phthalate
X X <5.0 1 ug/1
(117-81-7)
148.4-Bromophenyl
Phenyl Ether X X <5.0 1 ug/1
(101-55-3)
158.Butyl Benzyl X X <5.0 1 ug/1
Phthalate(85-68-7)
16B.2-Chloro-
naphthalene X X <5.0 1 ug/1
(91-58-7)
17B.4-Chloro-
phenyl Phenyl Ether X X <5.0 1 ug/1
(7005-72-3)
188.0ne X X <5.0 1 ug/1
(218-01-9)1-9)
19B.Dibenzo(oh)
Ane
(53-70-3) X X <5.0 1 ug/1
2013zee(95-50-1 X X <5.0 1 ug/1
benzene(95-50 1) /�
21B.1.3-01-chloro-
benzene(541-73-1) X X <5.0 1 ug/1
EPA Form 3510-2C(8-90) PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
2.MARK'X' 3.EFFLUENT 4.UNITS 5.INTAKE(optional) •
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE ((((available) VALUE(ijavailable) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
Of available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ALYSES
GC/MS FRACTION-BASE/NEUTRAL COMPOUNDS(continued)
22B.1,4-Dichloro-
benzene(106-46-7) X X <5.0 1 ug/1
23B.3,3-Dichloro-
benzidine(91-94-1) X X <25.0 1 ug/1
24B.Diethyl
Phthalate(84-66-2) X X <5.0 1 ug/1
Dimethyl
Phthalate X X
Phthalate <5.0 1 ug/1
(131-11-3)
288.Di-N-Butyl
Phthalate(84-74-2) X X <5.0 1 ug/1
27B.2,4-DinIVo-
toluene(121-14-2) X X <5.0 1 ug/1
28B.2,6-Dinitro-
toluene(606-20-2) X X <5.0 1 ug/1
29B.Di-N-Octyl
Phthalate(117-84-0) X X <5.0 1 ug/1
h0B.ydr z,2-Diphenyl-
hydrazine
ne(as Azo- X X
hydrazine(as Azo- <5.0 1 Ug/1
benzene)(122.66.7)
(31B.206-44-0)anthene X X <5.0 1 ug/1
32B.Fluorene
(86-73-7) X X <5.0 1 ug/1
33B.Hexachloro-
X <5.0 1 ug/1
benzene(118-74-1)
34B.Hexachloro-
butadiene(87-68-3) X X <5.0 1 ug/1
35Bcycl pHexadlene X X
cyclapentadiene <10.0 1 ug/1
(77-47.4)
36B Hexachloro-
ethane(67-72-1) X X <5.0 1 ug/1
372. -cd)P PX X
(1 ) yrene <5.0 1 ug/1
9
386.Isophorone
(78-59-1) X X <10.0 1 ug/1
(91-20-Naphthalene 3) X <5.0 1 ug/1
408.(98-95-3trobenzene) X X <5.0 1 ug/1
418.
sodime hyla X X
sodknethylamine <5.0 1 ug/1
(62-75-9)
428.N-Nitrosodi-
N- Nfe X X <5.0 1 ug/1
(621-64-7)
EPA Form 3510-2C(8-90) PAGE V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK'X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(f available) REQUIRED,PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION, (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(continued)
•
43B.N-Nitro-
sodiphenylamine X X <10.0 1 ug/1
(86-30-6)
( 1-8)Phenanthrene \/ X <5.0 1 ug/1
_
458.Pyrene
(129-00-0) X X <5.0 1 ug/1
46B.1,2,4-Trl-
amens X X <5.0 1 ug/1
(120-8
(120-82-1)
GC/MS FRACTION—PESTICIDES
1P.Aldrin X
(309-00-2)
2P.a-BHC X
(319-84-6)
3P.(-BHC X
(319-85-7)
_
4P.y-BHC X
(58-89-9)
5P.8-BHC X
(319-86-8)
6P.Chlordane
(57-74-9) X
7P.4,4'-DOT X
(50-29-3)
8P.4,4'-ODE X
(72-55-9)
9P.4,4'-ODD X
(72-54-8)
10P.Dieldrin X
(80-57-1)
11P.a-Enosulfan X
(115-29-7)
12P.(i-Endosulfan X
(115-29-7)
13P.Endosutfan
Sulfate X
(1031-07-8)
14P.Endrin X
(72-20-8)
15P.Endrin
Aldehyde X
(7421-93-4)
16P.Heptachlor X
(76-44-8) ,
EPA Form 3510-2C(8-90) PAGE V-8 CONTINUE ON PAGE V-9

EPA I.D.NUMBER(copy from Item I of Form I) OUTFALL NUMBER
NC000771964 001
CONTINUED FROM PAGE V-8
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(ijavailable) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED d.NO.OF a.CONCEN- b.NO.OF
( available) REQUIRED PRESENT ABSENT (1) (1) (1) ANALYSES TRATION b.MASS (1) ALYSES
Of ) � CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS
GC/MS FRACTION—PESTICIDES(continued)
17P.Heptachlor
Epoxide X
(1024-57-3)
18P.PCB-1242 �/
(53469-21-9) /�
19P.PCB-1254
(11097-69-1)
20P.PCB-1221 v
(11104-28-2)
21P.PCB-1232 X(11141-16.5)
22P.PCB-1248 X(12672-29-6)
•
23P.PCB-1260 v
(11096-82-5)
24P.PCB-1016
(12674-11-2)
25P.Toxaphene X(8001-35-2)
EPA Form 3510-2C(8-90) PAGE V-9

Pace Analytical Services,Inc.
CEAria4Itical a 9800 Kincey Ave. Suite 100
�i K! Huntersville,NC 28078
a' '•PI&com [phone]
ANALYTICAL RESULTS
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2120E Color ADMI Analytical Method:SM 2120E Color ADMI
Color,ADMI ND units 25.0 1 01/15/1513:19
Adjusted Color,ADMI ND units 25.0 1 01/15/15 13:19
pH 8.0 units 1.0 1 01/15/15 13:19
Adjusted pH,ADMI 7.6 units 1.0 1 01/15/15 13:19
HEM,Oil and Grease Analytical Method:EPA 16648
Oil and Grease ND mg/L 5.0 1 01/16/15 09:40
200.7 MET ICP Analytical Method:EPA 200.7 Preparation Method:EPA 200.7
Aluminum ND ug/L 100 1 01/16/15 18:55 01/17/15 03:31 7429-90-5
Antimony ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-36-0
Arsenic ND ug/L 10.0 1 01/16/15 18:55 01/19/15 14:16 7440-38-2
Barium 35.0 ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-39-3
Beryllium ND ug/L 1.0 1 01/16/15 18:55 01/17/15 03:31 7440-41-7
Boron 74.8 ug/L 50.0 1 01/16/15 18:55 01/17/15 03:31 7440-42-8
Cadmium ND ug/L 1.0 1 01/16/15 18:55 01/17/15 03:31 7440-43-9
Chromium ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-47-3
Cobalt ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-48-4
Copper ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-50-8
Iron 71.9 ug/L 50.0 1 01/16/15 18:55 01/17/15 03:31 7439-89-6
Lead ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7439-92-1
Magnesium 45000 ug/L 100 1 01/16/15 18:55 01/17/15 03:31 7439-95-4
Manganese 206 ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7439-96-5
Molybdenum ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7439-98-7
Nickel ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-02-0
Selenium ND ug/L 10.0 1 01/16/15 18:55 01/17/15 03:31 7782-49-2
Silver ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-22-4
Thallium ND ug/L 10.0 1 01/16/15 18:55 01/17/15 03:31 7440-28-0
Tin ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-31-5
Titanium ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-32-6
Zinc ND ug/L 10.0 1 01/16/15 18:55 01/17/15 03:31 7440-66-6
245.1 Mercury Analytical Method:EPA 245.1 Preparation Method:EPA 245.1
Mercury ND ug/L 0.20 1 01/17/15 14:15 01/20/15 16:58 7439-97-6
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
Acenaphthene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 83-32-9
Acenaphthylene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 208-96-8
Anthracene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 120-12-7
Benzidine ND ug/L 50.0 1 01/20/15 14:00 01/22/15 01:08 92-87-5
Benzo(a)anthracene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 56-55-3
Benzo(a)pyrene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 50-32-8
Benzo(b)fluoranthene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 205-99-2
Benzo(g,h,i)perylene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 191-24-2
Benzo(k)fluoranthene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 207-08-9
4-Bromophenyiphenyl ether ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 101-55-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:02/13/2015 03:34 PM without the written consent of Pace Analytical Services,Inc.. Page 6 of 56

,• ,/./
Pace Analytical Services,Inc.
aceAnalytical•
9800 Kincey Ave. Suite 100
Huntersviile,NC 28078
www.pacsiabs.com [phone]
i
ANALYTICAL RESULTS
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
Butylbenzylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 85-68-7
4-Chloro-3-methylphenol ND ug/L 5.0 1 01/20/15 14:00 01/22/1501:08 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 10.0 1 01/20/15 14:00 01/22/1501:08 111-91-1
bis(2-Chloroethyl)ether ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 111-44-4 `
bis(2-Chloroisopropyl)ether 46 ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 108-60-1 101'-
2-Chloronaphthalene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 91-58-7
2-Chlorophenol ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 95-57-8
4-Chlorophenylphenyl ether ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 7005-72-3
Chrysene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 218-01-9
Dibenz(a,h)anthracene ND ug/L 5.0 1 01/20/1514:00 01/22/15 01:08 53-70-3
1,2-Dichlorobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/1501:08 95-50-1
1,3-Dichlorobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 541-73-1
1,4-Dichlorobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/1501:08 106-46-7
3,3'-Dichlorobenzidine ND ug/L 25.0 1 01/20/15 14:00 01/22/15 01:08 91-94-1
2,4-Dichlorophenol ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 120-83-2
Diethylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 84-66-2
2,4-Dimethylphenol ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 105-67-9
Dimethylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 131-11-3
Di-n-butylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 84-74-2
4,6-Dinitro-2-methylphenol ND ug/L 20.0 1 01/20/15 14:00 01/22/15 01:08 534-52-1✓
2,4-Dinitrophenol ND ug/L 50.0 1 01/20/15 14:00 01/22/15 01:08 51-28-5
2,4-Dinitrotoluene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 121-14-2
2,6-Dinitrotoluene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 606-20-2
Di-n-octylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 117-84-0
1,2-Diphenylhydrazine ND ug/L 5.0 1 01/20/1514:00 01/22/1501:08 122-66-7
bis(2-Ethylhexyl)phthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 117-81-7
Fluoranthene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 206-44-0
Fluorene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 86-73-7
Hexachloro-1,3-butadiene ND ug/L 5.0 1 01/20/1514:00 01/22/15 01:08 87-68-3
Hexachlorobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 118-74-1
Hexachlorocyclopentadiene ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 77-47-4
Hexachloroethane ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 67-72-1
Indeno(1,2,3-cd)pyrene ND ug/L 5.0 1 01/20/1514:00 01/22/1501:08 193-39-5
Isophorone ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 78-59-1
Naphthalene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 91-20-3
Nitrobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 98-95-3
2-Nitrophenol ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 88-75-5
4-Nitrophenol ND ug/L 50.0 1 01/20/15 14:00 01/22/15 01:08 100-02-7
N-Nitrosodimethylamine ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 62-75-9
N-Nitroso-di-n-propylamine ND ug/L 5.0 1 01/20/1514:00 01/22/1501:08 621-64-7
N-Nitrosodiphenylamine ND ug/L 10.0 1 01/20/1514:00 01/22/15 01:08 86-30-6
Pentachlorophenol ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 87-86-5
Phenanthrene ND ug/L 5.0 1 01/20/1514:00 01/22/15 01:08 85-01-8
Phenol ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 108-95-2
Pyrene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 129-00-0
1,2,4-Trichlorobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 120-82-1
2,4,6-Trichlorophenol ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 88-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full.
Date:02/13/2015 03:34 PM without the written consent of Pace Analytical Services,Inc.. Page 7 of 56

�jf� Pace Analytical Sonde**,Inc.
ac
a e A-_t,1�� 9800 Kincey Ave. Suite 100
1J Huntersville,NC 28078
inew.pacelabacom [phone]
ANALYTICAL RESULTS
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
Surrogates
Nitrobenzene-d5(S) 52 % 10-120 1 01/20/15 14:00 01/22/15 01:08 4165-60-0
2-Fluorobiphenyl(S) 47 % 15-120 1 01/20/15 14:00 01/22/15 01:08 321-60-8
Terphenyl-d14(S) 60 % 11-131 1 01/20/15 14:00 01/22/15 01:08 1718-51-0
Phenol-d6(S) 10 % 10-120 1 01/20/15 14:00 01/22/15 01:08 13127-88-3
2-Fluorophenol(S) 15 % 10-120 1 01/20/15 14:00 01/22/15 01:08 367-12-4
2,4,6-Tribromophenol(S) 32 % 10-137 1 01/20/15 14:00 01/22/15 01:08 118-79-6
624 Volatile Organics Analytical Method:EPA 624
Acrolein ND ug/L 5.0 1 01/17/15 08:15 107-02-8
Acrylonitrile ND ug/L 50.0 1 01/17/15 08:15 107-13-1
Benzene ND ug/L 2.0 1 01/17/15 08:15 71-43-2
Bromodichloromethane ND ug/L 2.0 1 01/17/15 08:15 75-27-4
Bromoform ND ug/L 2.0 1 01/17/15 08:15 75-25-2
Bromomethane ND ug/L 2.0 1 01/17/15 08:15 74-83-9
Carbon tetrachloride ND ug/L 2.0 1 01/17/15 08:15 56-23-5
Chlorobenzene ND ug/L 2.0 1 01/17/15 08:15 108-90-7
Chloroethane ND ug/L 2.0 1 01/17/15 08:15 75-00-3
2-Chloroethylvinyl ether ND ug/L 5.0 1 01/17/15 08:15 110-75-8
Chloroform ND ug/L 2.0 1 01/17/15 08:15 67-66-3
Chloromethane ND ug/L 2.0 1 01/17/15 08:15 74-87-3
%Dibromochloromethane ND ug/L 2.0 1 01/17/15 08:15 124-48-1
Dichlorodifluoromethane ND ug/L 2.0 1 01/17/15 08:15 75-71-8
1,1-Dichioroethane ND ug/L 2.0 1 01/17/15 08:15 75-34-3
1,2-Dichloroethane ND ug/L 2.0 1 01/17/15 08:15 107-06-2
1,1-Dichloroethene ND ug/L 2.0 1 01/17/15 08:15 75-35-4
trans-1,2-Dichloroethene ND ug/L 2.0 1 01/17/15 08:15 156-60-5
1,2-Dichloropropane ND ug/L 2.0 1 01/17/15 08:15 78-87-5
cis-1,3-Dichloropropene ND ug/L 2.0 1 01/17/15 08:15 10061-01-5
Ethylbenzene ND ug/L 2.0 1 01/17/15 08:15 100-41-4
Methylene Chloride ND ug/L 2.0 1 01/17/15 08:15 75-09-2
1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 01/17/15 08:15 79-34-5
Tetrachloroethene ND ug/L 2.0 1 01/17/15 08:15 127-18-4
Toluene ND ug/L 2.0 1 01/17/15 08:15 108-88-3
1,1,1-Trichloroethane ND ug/L 2.0 1 01/17/15 08:15 71-55-6
1,1,2-Trichloroethane ND ug/L 2.0 1 01/17/15 08:15 79-00-5
Trichloroethene ND ug/L 2.0 1 01/17/15 08:15 79-01-6
Trichlorofluoromethane ND ug/L 2.0 1 01/17/15 08:15 75-69-4
Vinyl chloride ND ug/L 2.0 1 01/17/15 08:15 75-01-4
Surrogates
4-Bromofluorobenzene(S) 97 % 70-130 1 01/17/15 08:15 460-00-4
Toluene-d8(S) 92 % 70-130 1 01/17/15 08:15 2037-26-5
1,2-Dichloroethane-d4(S) 101 % 70-130 1 01/17/15 08:15 17060-07-0
MBIO 9222D Fecal Coliform CHT Analytical Method:SM 9222D
Fecal Coliforms ND CFU/100 mL 1.0 1 01/14/15 14:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:02/13/2015 03:34 PM without the written consent of Pace Analytical Services,Inc.. Page 8 of 56

Pace Analytical Services,Inc.
Ce 11na�• 9800 Kinsey Ave. Suite 100
�f7/`T IJC Huntersville,NC 28078
wwwpacetabs.com [phone]
ANALYTICAL RESULTS
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method:SM 2540D
Total Suspended Solids ND mg/L 2.9 1 01/21/15 03:31
4500CL G Chlorine,Residual Analytical Method:SM 4500-Cl G
Chlorine,Total Residual 0.11 mg/L 0.024 1 01/16/15 11:00 7782-50-5 H1
4500S2D Sulfide Water Analytical Method:SM 4500-S2D
Sulfide ND mg/L 0.10 1 01/15/15 10:30 18496-25-8
5210B BOO,5 day Analytical Method:SM 5210B
BOD,5 day ND mg/L 2.0 1 01/15/15 05:57 01/20/15 06:51
Total Organic Nitrogen Calc. Analytical Method:TKN-NH3 Calculation
Total Organic Nitrogen ND mg/L 0.50 1 02/04/15 17:36
300.0 IC Anions 28 Days Analytical Method:EPA 300.0
Bromide 0.81 mg/L 0.20 2 01/21/15 04:36 24959-67-9
Fluoride ND mg/L 0.50 1 01/17/15 05:37 16984-48-8
Sulfate 342 mg/L 20.0 10 01/17/15 11:49 14808-79-8
350.1 Ammonia Analytical Method:EPA 350.1
Nitrogen,Ammonia ND mg/L 0.10 1 01/27/15 20:08 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method:EPA 351.2
Nitrogen,Kjeldahl,Total ND mg/L 0.50 1 01/30/15 15:05 7727-37-9 M1
353.2 Nitrogen,NO2/NO3 pres. Analytical Method:EPA 353.2
Nitrogen,NO2 plus NO3 ND mg/L 0.020 1 01/30/15 18:31
365.1 Phosphorus,Total Analytical Method:EPA 365.1
Phosphorus ND mg/L 0.050 1 01/28/15 17:02 7723-14-0
420.4 Phenolics,Total Analytical Method:EPA 420.4 Ati145 11"
Phenol ND mg/L 0.010 1 A0.W415 L 01/29/15 15:48 108-95 2
4500CNE Cyanide,Total Analytical Method:SM 4500-CN-E
Cyanide ND mg/L 0.0080 1 01/26/15 14:48 57-12-5
5220D COD Analytical Method:SM 5220D
Chemical Oxygen Demand 30.0 mg/L 25.0 1 01/15/15 14:20
5310B TOC Analytical Method:SM 5310B
Total Organic Carbon 3.7 mg/L 1.0 1 01/16/15 13:57 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:02/13/2015 03:34 PM without the written consent of Pace Analytical Services.Inc.. Page 9 of 56

, Pace Analytical Services,Inc.
e
aceAnalytical 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
ss00m [phone]
ANALYTICAL RESULTS-RADIOCHEMISTRY
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix:Water
PWS: Site ID: Sample Type:
Parameters Method Act t Unc(MDC)Carr Trac Units Analyzed CAS No. Qual
Gross Alpha EPA 900.0 7.64 t 2.41 (2.69) pCi/L 01/27/15 21:32 12587-46-1
C:NA T:NA
Gross Beta EPA 900.0 6.28 t 1.47 (1.29) pCi/L 01/27/15 21:32 12587-47-2
C:NA T:NA
Radium-226 EPA 903.1 0.0627 t 0.325 (0.675) pCi/L 02/03/15 11:18 13982-63-3
C:NA T:86%
Radium-228 EPA 904.0 0.244 t 0.405 (0.882) pCi/L 01/30/15 16:07 15262-20-1
C:89%7:61%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.. Page 43 of 56

Analytical Results
Pace Analytical
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date: 01/15/2015
Reported: 02/04/2015 STATESVILLE
For: 9223379 ANALYTICAL
Comments:
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
150115-12-01 MBAS 001 0.17 mg/L SM5540C-2000 01/15/2015 MD
Respectfully submitted,
NP -V✓i..j711A,
Dena Myers
NC Cert#440,
NCDW Cert#37755,
EPA#NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 rage 55 of 56

Analytical Environmental Services,Inc Date: 19-Feb-15
Client: Pace Analytical Services,Inc. Client Sample ID: 001
Project Name: 92238054 Collection Date: 2/18/2015 9:02:00 AM
Lab ID: 1502G20-001 Matrix: Aqueous
Reporting Dilution
Analyses Result Limit Qual Units BatchlD Factor Date Analyzed Analyst
Sulfite by SM4500-S03-B
Sulfite BRL 2.00 H mg/L R286188 1 02/19/2015 15:30 OM
Qualifiers: ' Value exceeds maximum contaminant level E Estimated(value above quantitation range)
BRL Below reporting limit S Spike Recovery outside limits due to matrix
II holding times for preparation or analysis exceeded Nan See case narrative
N Analytc not NELAC certified NC Not confirmed
B Analyte detected in the associated method blank < Less than Result value
> Greater than Result value .1 Estimated value detected below Reporting Limit
Page 13 of 15
4 of 6

Condition of Receipt
Sample Number 150115-12-01 Temp on Arrival: 2
Parameter Schedule: MBAS
Received on Ice
Chemicals in containers, lab
PO Box 228 •Statesville, NC 28687• 704/872/4697
Page 2 tae 56 of 56

I.
ROOF DRAINS:
J -50%OF MANF.BLDG.62.500 SF
FLOWS TO PLANT PROCESS SEWER
0- VIA.NORTH AND SOUTH DRAINS
0-
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PI
1 R
WATER TANK PUMP(-100
QSTORMWATER FROM CHL
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NON-CONTACT COOLING WATER HYDROXIDE SCRUBBER
HYDROXIDE CENTRIFUGES VIA I ROOF DRAIN
ROOF DRAINS
© -1 GPM(I)COMPRESSO
I
t WEST PLANT SITE SURFACE r, O LITHIUM HYDROXIDE C
AND ROOF DRAINAGE 7 PERMtATE UNIT 0.701
STORM WATERS FROM PERIMETER FLOWS
OF RED POND AND SOUTHERN
PORTION OF KILO LAB
S WASTE WATER FLOWS
::LiEiC:fsCERNITA0NOCRmETRTTSTIDBEORMN:AWATER
T FLOW
ANHOLE OR
ININLETTEMCING
TYPICALLY TYPICALLY FLOW ID
CLOSED (OPEN
_ DIVERSION NCY SPILLWAY OVER FLOW
DIVERSION GATE
ID GATE
1 `OVERFLOW(I) V NOTCH il
T WIER BOX O FLOW,0.0.615 MGD
\�I I
_ POINT
GROUNDWATER R&D SURFACE AND STORM WATERS SOURCE
CHARGE MANUF.PARKING LOT,AND -. cc,_
NG TOWER PURGE q OUTFALL 001
POND S.0.BOOILLEIR BLOW DOWN -'r
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t
UNNAMED TRIBUTARY
TO ABERNETHY CREEK
14 I.....o.. ..... 2120/14 RSW
3 WARR,SW SIMA.rre 10/14/10 RSW
2 R&D TO POTW 2122/10 RSW I
1 :ADDED FLOW#10 8/2/05 I RSV/ I
REV., DESCRIPTION DATE Or (FBC
f M CFIAC Cerperetion
Lithium Division
Benemer City, NC
xrT.or.7s.w5 - NPOES Renewal 2010
POINT AND STORMWATER i
DISCHARGE FLOW SHEET
I I I.R V auwl_NAME >.ff_JAiE
A....-AEE
n - — sc.-SCALE. OC'.0051W,D6.
ramie DRAWING 50 REV.
- 15 s s saran . •

NPDES INDUSTRIAL DISCHARGE RENEWAL
FMC CORPORATION
LITHIUM DIVISION
NPDES PERMIT NC0005177
OUTFALL 001

EPA I.D.NUMBER(copy from Item I of Form I) Form Approved.
NCDO00771964 OMB No.2040-0086.
Please print or type in the unshaded areas only. Approval expires 3-31-98.
FORM U.S.ENVIRONMENTAL PROTECTION AGENCY
2C ,EPA TO
DISCHARGE WASTEWATER
EXISTING MANUFACTURING,COMMERCIAL,MINING AND SILVICULTURE OPERATIONS
NPDES Consolidated Permits Program
I.OUTFALL LOCATION
For each outfall,list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A.OUTFALL NUMBER B.LATITUDE C.LONGITUDE
(list) 1.DEG. 2.MIN. 3.SEC. 1.DEG. 2.MIN. 3.SEC. D.RECEIVING WATER(name)
001 35.00 15.00 43.00 81.00 17.00 54.00 First Creek
004 35.00 15.00 43.00 81.00 17.00 54.00 First Creek
II.FLOWS,SOURCES OF POLLUTION,AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility.Indicate sources of intake water,operations contributing wastewater to the effluent,and treatment units
labeled to correspond to the more detailed descriptions in Item B.Construct a water balance on the line drawing by showing average flows between intakes,operations,
treatment units,and outfalls.If a water balance cannot be determined(e.g.,for certain mining activities),provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall,provide a description of:(1)All operations contributing wastewater to the effluent,including process wastewater,sanitary wastewater,cooling water,
and storm water runoff; (2)The average flow contributed by each operation; and (3)The treatment received by the wastewater. Continue on additional sheets if
necessary.
1.OUT- 2.OPERATION(S)CONTRIBUTING FLOW 3.TREATMENT
FALL b.AVERAGE FLOW b.LIST CODES FROM
NO.(list) a.OPERATION(list) (include units) a.DESCRIPTION TABLE 2C-1
1) Misc. Salts and Cat. Phosphate None
001 -5,000 gals/mth X X
2) LiOCL Air Scrubber waste water _100 gpm H202 Addition and Equalization 2
3)Boiler Blowdown None
-15 gpm X X
4)LiCl RO permeate and condesate -9 550 GPD Reverse Osmosis 1
5) left blank
6) Compressor CondensateNone
1 gpm % x
7) Li Hydroxide RO Reverse Osmosis
-5,000 gals/mth 1
6) Battery Metal Cooling Tower 10 None % %
gpm
9) Combined Plant waste water 130 gpm pH adjustment 2 X
101 Li Hydroxide Cooling Twr. None
35 gpm X X
11) R&D Pond stormwater management Setteling
10 gpm X X
OFFICIAL USE ONLY(effluent guidelines sub-categories)
EPA Form 3510-2C(8-90) PAGE 1 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C.Except for storm runoff,leaks,or spills,are any of the discharges described in Items II-A or B intermittent or seasonal?
YES(complete the following table) El NO(go to Section III)
3.FREQUENCY 4.FLOW
a.DAYS PER 8.TOTAL VOLUME
2.OPERATION(s) WEEK b.MONTHS a.FLOW RATE(in mgd) (specify with,.Wins)
1.OUTFALL CONTRIBUTING FLOW (specifi• PER YEAR 1.LONG TERM 2.MAXIMUM 1.LONG TERM 2.MAXIMUM C.DURATION
NUMBER(lisr) (list) average) (.strectb'o' age) AVERAGE DAILY AVERAGE DAILY (in dap)
001 1) Misc. Salts and Cat. Phosphate --- 6 --- 0.005 --- 5,000 gal ---
11) R&D Pond stormwater management 7 6 --- 0.015 ---- 0.010 MG 180
III.PRODUCTION
A.Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
El YES(complete Item ill-B) NO(go to Section IV)
B.Are the limitations in the applicable effluent guideline expressed in terms of production(or other measure of operation)?
El YES(complete Item Ill-C) El NO(go to Section IV)
C.If you answered"yes"to Item III-B,list the quantity which represents an actual measurement of your level of production,expressed in the terms and units used in the
applicable effluent guideline,and indicate the affected outfalls.
1.AVERAGE DAILY PRODUCTION
2.AFFECTED OUTFALLS
c.OPERATION,PRODUCT,MATERIAL,ETC. list an{
a.QUANTITY PER DAY b.UNITS OF MEASURE ( >all numbers)
(.specO)
IV.IMPROVEMENTS
A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application?This includes,but is not limited to,
permit conditions,administrative or enforcement orders,enforcement compliance schedule letters,stipulations,court orders,and grant or loan conditions.
El YES(complete the following table) NO(go to Item IV-B)
1.IDENTIFICATION OF CONDITION, 2.AFFECTED OUTFALLS 3.BRIEF DESCRIPTION OF PROJECT 4.FINAL COMPLIANCE DATE
AGREEMENT,ETC.
a.NO. b.SOURCE OF DISCHARGE a.REQUIRED b.PROJECTED
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges)you now have underway or which you plan.Indicate whether each program is now underway or planned,and indicate your actual or planned schedules for
construction.
El MARK"X"IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C(8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA I.D.NUMBER(copy from hem I of Form I)
CONTINUED FROM PAGE 2 NC000771964
V.INTAKE AND EFFLUENT CHARACTERISTICS
A,B,&C: See instructions before proceeding-Complete one set of tables for each outfall-Annotate the outfall number in the space provided.
NOTE:Tables V-A,V-B,and V-C are included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions,which you know or have reason to believe is discharged or may be discharged
from any outfall.For every pollutant you list,briefly describe the reasons you believe it to be present and report any analytical data in your possession.
1.POLLUTANT 2.SOURCE 1.POLLUTANT 2.SOURCE
•
VI.POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS
Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct?
YES(list all such pollutants below) ❑NO(go to Item f7-B)
EPA Form 3510-2C(8-90) PAGE 3 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
VII.BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
©YES(identify the test(s)and describe their purposes below) ❑NO(go to Section VIII)
Chronic Toxicity, Presently required by our NPDES discharge Permit of outfall 001.
VIII.CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
®YES(list the name,address,and telephone number of and pollutants analyzed hr. ❑NO(go to Section IX)
each such laboratory or firm helms.)
A.NAME B.ADDRESS C.TELEPHONE D.POLLUTANTS ANALYZED
(area code&no.) (list)
Pace Analytical Services 9800 Kincey Ave. Suite 100 704-875-9092 See page 4 of Pace
Huntersville, NC 28078 Analytical report
Pace Analytical Services 2225 Riverside Dr. See page 4 of Pace
Asheville, NC 828-254-7176 Analytical report
Pace Analytical Services 1638 Roseytown Rd. Suites 2,354 724-850-5600 See page 4 of Pace
Greensburg, PA 15601 Analytical report
Pace Analytical Services 8 East Tower Circle, 386-672-5668 See page 4 of Pace
Ormond Beach, FL 32174 Analytical report
Pace Analytical Services 205 East Meadow Road Suite A 336-623-8921 See page 4 of Pace
Eden, NC 27288 Analytical report
Statesville Analytical PO Box 228 704-872-4697 See page 4 of Pace
Statesville, NC 28687 Analytical report
IX CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there
are significant penalties for submitting false information,including the possibility of fine and imprisonment for knowing violations.
A.NAME&OFFICIAL TITLE(type or print) B.PHONE NO.(area code&no.)
Bruce Urban (704) 868-7650
6
C.SIGNATURE ,..,,...41AZ4A_____ D.DATE SIGNED
Z.6 F-f_f (s
EPA Form 3510-2C(8-90) PAGE 4 of 4

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY.You may report some or all of this information EPA I.D.NUMBER(copyfrom hem I of Form I)
on separate sheets(use the same format)instead of completing these pages. NC000771964
SEE INSTRUCTIONS.
OUTFALL NO.
V.INTAKE AND EFFLUENT CHARACTERISTICS(continued from page 3 of Form 2-C)
PART A-You must provide the results of at least one analysis for every pollutant in this table.Complete one table for each outfall.See instructions for additional details.
3.UNITS 4.INTAKE
2.EFFLUENT (specify if blank) (optional)
1 b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
a.MAXIMUM DAILY VALUE (if available) (if available) AVERAGE VALUE
(1) (1) d.NO.OF a.CONCEN- (II b.NO.OF
1.POLLUTANT CONCENTRATION (2)MASS CONCENTRATION (2)MASS (1)CONCENTRATION (21 MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Biochemical Oxygen 11.2 mg/1 48.7 lb --- --- 1.75 mg/1 135 lbs 8 mg/1 lbs
Demand(BOD)
b.Chemical Oxygen 30 mg/1 --- --- --- --- --- 1 mg/1 lbs
Demand(COD)
c.Total Organic Carbon 3.7 mg/1 --- --- --- --- 1 mg/1 lbs
(TOC)
-
d.Total Suspended
Solids(TSS) 3.0 mg/1 12.1 lb --- --- 0.19 mg/1 14.4 lbs 16 mg/1 lbs
e.Ammonia(as N) <0.1 mg/1 --- --- --- --- --- 1 mg/1 lbs
VALUE VALUE VALUE VALUE
f.Flow 0.537 MG 16.26 MG 9.2 MGD 1 yr --- MG
g.Temperature VALUE VALUE VALUE VALUE
(winter) 8.1 --- --- °C
h.Temperature VALUE VALUE VALUE VALUE
(summer) 27.05 --- --- °C
MINIMUM MINIMUM MAXIMUM
I.pH 7.6 !MAXIMUM
8.3 --- --- 31 STANDARD UNITS
PART B- Mark"X"in column 2-a for each pollutant you know or have reason to believe is present.Mark"X"in column 2-b for each pollutant you believe to be absent.If you mark column 2a for any pollutant which is limited either
directly,or indirectly but expressly, in an effluent limitations guideline,you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a,you must provide
quantitative data or an explanation of their presence in your discharge.Complete one table for each outfall.See the instructions for additional details and requirements.
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM AVERAGE
ANDa.MAXIMUM DAILY VALUE a. b.
CAS NO. (ifavailable)) (ifavailahle) VALUE
BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(if available) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Bromide
(24959-67-9) X 0.81 1 mg/1
b.Chlorine,Total
Residual X <0.11 1 mg/1
c.Color X <2 5 1 ADM I
•
d.Fecal Coliform X <1.0 1 CFU/100m
e.Fluoride
(16984-48-8) X <0.50 1 mg/1
f.(asiN)te-Nitrite X <0.020 <0.10 4 mg/1 '
EPA Form 3510-2C(8-90) PAGE V-1 CONTINUE ON REVERSE

ITEM V-B CONTINUED FROM FRONT -
2.MARK'X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional) ,
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
ANDa b, a.MAXIMUM DAILY VALUE (Pfavailable) (ijavailable) AVERAGE VALUE
CAS NO. BELIEVED BELIEVED (1) (1) CO d.NO.OF a.CONCEN- (1) b.NO.OF
(ifavailable) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
g.Nitrogen, \ ,
Total Organic(m ><
m X <0.50 1 mg/1
N)
h.Oil and X <5.0 1 mg/1
Grease
i.Phosphorus ` ,
(as P),Taal X <0.050 1 mg/1
(7723-14.0) , `
J.Radioactivity
(t)Alpha,Total X 7.64+-2.41 1 pCi/L
(2)Beta,Total X 6.28+-1.47 1 pCi/L
(3)Radium, X .244+-.405 1 pCi/L
Total
(4)Radium 226, X ,062+-.325 1 pCi/L
Total
k.Sulfate
(arm') X 342 1 tog/1
(14808-79-8)
I(aSS)Sulfide X <0.10 1 tog/1
ar S)
m.Sulfite
(arSO,) X <2.00 1 mg/1
(14265-45-3)
n.Surfactants X 0.17 1 mg/1
a.Aluminum,
TOS X <100 1 ug/1
(7429-90-5)
p.Barium,Total X 35.0 1 ug/1
(7440-39-3)
q.Baron,Total X 74.8 1 ug/1
(7440-42-8)
(.Cobalt,Total
(7440-48-4) X <5.0 1 ug/1
a.Iron,Total
Total
(7439 X <71.9 1 ug/1
L Magnesium,
TX
Total
45000 1 ug/1
(7439-95-4)
u.Molybdenum, X
TOS <5.0 1 ug/1
(7439-98-7)
v.Manganese,
TOS X 206 1 ug/1
(7439-96-5)
w.Tin,Total
(7440-31-5) X <5.0 1 ug/1
x.Titanium,
X
Total <5.0 1 ug/1
(7440-32-6)
EPA Form 3510-2C(8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D.NUMBER(copy from hem I of Form I) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C NC000771964 001
PART C- If you are a primary industry and this outfall contains process wastewater,refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for.Mark'X"in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals,cyanides,and total phenols.If you are not required to mark column 2-a(secondary industries,nonprocess wastewater outfalls,and nonrequired GC/MS
fractions),mark'X'in column 2-b for each pollutant you know or have reason to believe is present.Mark"X"in column 2-c for each pollutant you believe is absent.If you mark column 2a for any pollutant,you must
provide the results of at least one analysis for that pollutant.If you mark column 2b for any pollutant,you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater.If you mark column 2b for acrolein,acrylonitrile,2,4 dinitrophenol,or 2-methyl-4,6 dinitrophenol,you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater.Otherwise,for pollutants for which you mark column 2b,you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged.Note that there are 7 pages to this part;please review each carefully.Complete one table(all 7 pages)for each outfall.See instructions for
additional details and requirements.
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
ANDa. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(if available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
METALS,CYANIDE,AND TOTAL PHENOLS
1M.antimony,Total X u <5.0 1 ug/1
(7440-36-0) /� , `
2M.
444038-2)'TOS X X <10.0 1 ug/1
3M.Beryllium,Total X X <1.0 1 ug/1
(7440-41-7)
4M.(744043-9)m,Total X X <1.0 1 ug/1
5M.Chromium.
Total(7440-47-3) X X <5.0 1 Ug/1
4(7740 filo B)'Total /��/ X <5.0 1 ug/1
7M.Lead,Total
(7439-92-1) X X <5.0 1 ug/1
8M.Mercury,Total
(7439-97-6) X X 0.747 1 ng/1
9M.Nickel,Total
<
(7440-02-0) 5.0 1 ug/1
10M.Selenium,
Total(7782-49-2) X X <10.0 1 ug/1
11M.Silver,Total
(7440-22-4) X X <5.0 1 ug/1
12M.Thallium, �/
Total(7440-28-0) X X <10.0 1 ug/1
13M(744 6--,)Total X X <10.0 1 ug/1
14M.Cyanide, /�
Total(57-12-5) X X <0.0080 1 mg/1
Total Phenols X X <0.010 1 mg/1
DIOXIN
2,3,7,8-Tetra- \ / DESCRIBE RESULTS
chkxodibenzo-P- /X\
Dioxin(1764-01-6)
EPA Form 3510-2C(8-90) PAGE V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional) �•
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
ANDa. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED d.NO.OF a.CONCEN- b.NO.OF
(if available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—VOLATILE COMPOUNDS
1V.
(1007-0-02 8)) /�X X <5.0 1 ug/1
2V.Acrylonitrile
(107-13-1) X X <50 1 ug/1
3V.(7143-2)Benzene X X <2 0 1 ug/1
(7143-2)
4V.Bis(Chloro- ` / \/
methyl)Ether x x <5.0 1 ug/1
(542-88-1)
5V.2-mofonn
(75-25-2) X X <2 0 1 ug/1
6V.Carbon
Tetrachloride X X <2.0 1 ug/1
(56-23-5)
7V. obenzene
X X <2 0 1 ug/1
(108-90-7)
8V.Chlorodi- \ / `/
bromomethane x J� <2.0 1 ug/1
(12448-1) , ` , `
9V.Chloroethane X X
(75-00-3) <2.0 1 ug/1
10V.2 X X
ethylvintl nylEther <5.0 1 ug/1
(110-75-8)
Chloroform
(67-66-3) X X
<2.0 1 ug/1
12V.DtchloX X
bromomethanane <2.0 1 ug/1
(75-27-4)
13V. X X
Dichloro-
difluoromethane <2.0 1 ug/1
(75-71-8)
14Vetha e(75-o4-3) X X <2 0 1 ug/1
ethane(75-34-3)
tha15V.a(107-06-2) X X
ethane(107-06-2) <2•0 1 ug/1
eth
16V. ne 5 -o-
X X <2.0 1 ug/1
ethylene(75-35-4)
ropane 7-o-
p
propane(78-87-5) X X <2.0 1 ug/1
18V.1,3-Dichloro- \ / \ ,
propylene X X <2.0 1 ug/1
(542-75.6)
19V.414)41-4)amens
(100 X X <2 0 1 ug/1
20V.Methyl �/ �/ <2 0 1 ug/1
Bromide(74-83-9) `X `X
•
21V.Methyl y X <2.0 1 ug/1
Chloride(74-87-3) /\
EPA Form 3510-2C(8-90) PAGE V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4
2.MARK°X° 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
Of available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION-VOLATILE COMPOUNDS(continued)
22V.Methylene X X <2.0 1 ug/1
Chloride(75-09-2)
23V.1,1,2,2-
Tetrachloroethane X X <2.0 1 ug/1
(79-34-5) ,
24V.Tetrachloro X X <2.0 1 ug/1
ethylene(127-18-4)
25V.Toluene X X <2.0 1 ug/1
(108-08-3)
26V.1.2-Trans-
Dichioroethylene X X <2.0 1 ug/1
(156-60-5)
e7V.than (71-55-8)
1-55-8) X X <2.0 1 ug/1
eUiane(71-55.8)
28V.1,1.2-Trichloro X X <2.0 1 ug/1
ethane(79-00-5)
29V ee(79- X X <2.0 1 ug/1
eth8,ylan (79-0
e t�)
30V.Trichloro-
fluoromethane X X <2.0 1 ug/1
(75-69-4)
31V.Vinyl Chloride X X <2.0 1 ug/1
(75-01-4) j
GC/MS FRACTION-ACID COMPOUNDS
IA.2Chlorophenol
(95-57-8) X X <5.0 1 ug/1
phenol(120-8ro- X X <5.0 1 ug/1
phenol(120 83 2)
3A.2•a-ameth1- X X <10.0 1 ug/1
phenol( 05.67-9)
4k a, 3O X X <20.0 1 ug/1
Cresol(55344-552-1)
5A.2,4(51-no-
phenol(51-28-5) X X <50.0 1 ug/1
6A.2-NNrophenol X X <5.0 1 ug/1
(88-75-5)
7h 4-Nltropnenol
(100-02-7) X X <50.0 1 ug/1
8A.P-Chloro-M-
Cresol(59-50-7) X X <5.0 1 ug/1
9A.Pentathlon, X X <10.0 1 ug/1
phenol(87-88-5) .
10A.PX X <5.0 1 ug/1
(108-955-2)2)
phenol(88-0 -2) X X <10.0 1 ug/1
phenol(88-05-2)
EPA Form 3510-2C(8-90) PAGE V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK'W 3.EFFLUENT 4.UNITS 5.INTAKE(optional) •
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c, a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED d.NO.OF a.CONCEN- b.NO.OF
Of available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION ANALYSES TRATION b.MASS (1) ALYSES
(2)MASS CONCENTRATION (2)MASS
GC/MS FRACTION-BASE/NEUTRAL COMPOUNDS
1B.Acenaphthene X X <5.0 1 ug/1
(83-32-9)
28. X X <5.0 1 ug/1
(208.96-08.96-8)
3B.Anthracene
(120.12-7) X X <5.0 1 ug/1
( 2-887-5) X X <50.0 1 ug/1
Benzo(a)
An X X
Anthracene <5.0 1 ug/1
(56-55-3)
68 SCHIZO(a) X X <5.0 1 ug/1
Pyrene(50-32.8)
78.3, Benzo-
twarantnthene
X X <5.0 1 ug/1
(205-99-2)
88.Benzo(ghi)
Perylene(191-24-2) X X <5.0 1 ug/1
9B.Benzo(k)
Fk'Omn81ene X X <5.0 1 ug/1
(207-08-9)
108.Bis(2-Chloro-
ethoxy)Methane X X <10.0 1 ug/1
(111-91-1)
118.Bis(2-Chloro-
ethyl)Ether
2-Chloro-
erhyl)Ether X X <5.0 1 ug/1
(111-44-4)
12B.Bis(2-
Chloraisapropvl) X X <5.0 1 ug/1
Ether(102-80-1)
138hexy Bis el-
hexyn Phthalate <5.0 1 ug/1
(11781-7)
14B.4-Bromophenyl
Phenyl Ether X X <5.0 1 ug/1
(101-55-3)
15B. Benzyl X X <5.0 1 ug/1
Phthalate(85-68-7)
16B.2-Chloro-
naphthalene X X <5.0 1 ug/1
(91-58-7)
17B.4-Chloro-
phenyl Phenyl Ether X X <5.0 1 ug/1
(7005-72-3) `,
1813. ysene X 7� <5.0 1 ug/1
(218-01-9)
198.Dibenzo(ah)
Anthracene
(53-70-3) X X <5.0 1 ug/1
208.1,2-Dichloro-
benzene(95-50-1) X X <5.0 1 ug/1
21B.1,3-Di-chloro-
benzene(541-73-1)
.3-Di-chloro-
benzene(541-73-1) X X <5.0 1 ug/1
EPA Form 3510-2C(8-90) PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional) -
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
al available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION-BASE/NEUTRAL COMPOUNDS(continued)
228.1,4-Dichloro-
X X <5.0 1 ug/1
benzene(106-46-7)
238.3.3-Dichloro-
benzidine(91-94-1) X X <25.0 1 ug/1
248.Diethyl
Phthalate(84.66-2) X <5.0 1 ug/1
Phthalate
hth la eelhyl
-1 - <5.0 1 ug/1
(131
(131-11-3)
268.Di-N-Butyl
Phthalate(84-74-2) X X <5.0 1 ug/1
278.2,4-Dinftro-
toluene(121-14-2) X X <5.0 1 ug/1
288.2,6-Dinkro-
toluene(606-20-2) X X <5.0 1 ug/1
296.Di-N-Octyl
Phthalate(117-84-0) X X <5.0 1 ug/1
hy8.dr 1.2-Diphenyl-
hydrazine
X X
hydrazkre(as Azo- <5.0 1 ug/1
benzene)(122-66-7)
(1 N-0)antlrene X X <5.0 1 ug/1
328.Fluorene
(86-73-7) X X <5.0 1 ug/1
338.Hexachloro-
benzene(118-74-1) X X <5.0 1 ug/1
348.Hexachloro-
butadIene(87-68-3) X X <5.0 1 ug/1
Hexachloro-
cyclopentadiene
X
<10.0 1 ug/1
(7747-4)
36B Hexachloro-
ethane(67-72-1) X X <5.0 1 ug/1
378.Indeno
(193395)3-cd)Pyrene
X X <5.0 1 ug/1
(7&59-1one X X <10.0 1 ug/1
398.Naphthalene
(91-20-3) <5.0 1 ug/1
408.Nitrobenzene
(98-95-3) X X <5.0 1 ug/1
418.N-NitroX X
sodimethylemine <5.0 1 ug/1
(62-75-9)
428.N-Nitrosodf-
NPrOp ne X X <5.0 1 ug/1
(621-64-7)
EPA Form 3510-2C(8-90) PAGE V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (If available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED d.NO.OF a.CONCEN- LNALYSES
.NO.OF
(ijilable) REQUIRED PRESENT ABSENT CONCENNATN (2)MASS CONCENTRATION) (1) ANALYSES TRATION b.MASS (1)
(2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(continued)
43B.N-Nitro-
sodiphenylamine X X <10.0 1 ug/1
(86-30-6) _
( 1$44B.PhenanCnene xX <5.0 1 ug/1
)
-
458.Pyrene
(129.00.0) X X <5.0 1 ug/1
468.1,2,4-Tri-
chlone X X <5.0 1 ug/1
(120-82-1)-82-1)
GC/MS FRACTION—PESTICIDES
1P.Aldrin I
X
(309-00-2)
2P.a-BHC X
(319-84-6)
3P.AHC X
(319-85-7)
4P.T-BHC X
(58-89-9)
5P.S-BHC X
(319-86-8)
6P.Chlordane X
(57-74-9)
7P.4,4'-DOT X
(50-29-3)
8P.4,4'-DDE X
(72-55-9)
9P.4,4'-DDD X
(72-54-8)
10P.Dieldrin X
(60-57-1)
11P.a-Enosulfan X
(115-29-7)
12P.r,-Endosulfan X
(115-29-7)
13P.Endoaulfan
Sulfate X
(1031-07-8)
14P.Endrin X
(72-20-8)
15P.Endrin
Aldehyde(7421-93-4)
X
16P.Heptachlor iX
(76-44-8) I
EPA Form 3510-2C(8-90) PAGE V-8 CONTINUE ON PAGE V-9

EPA I.D.NUMBER(copy from Item 1 of Form 1) OUTFALL NUMBER
NC000771964 001
CONTINUED FROM PAGE V-8
2.MARK 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) - (1) (1) \d.NO.OF a.CONCEN- (1) b.NO.OF
Of available) REQUIRED PRESENT ABSENT CONCENTRATION_ (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—PESTICIDES(continued)
17P.Heptachlor
Epoxide X
(1024-57-3)
18P.PCB-1242
(53469-21-9)
19P.PCB-1254 �/
(11097-69-1) /�
20P.PCB-1221 X(11104-28-2)
21P.PCB-1232 v
(11141-16-5)
22P.PCB-1248 X(12672-29-6)
23P.PCB-1260
(11096-82-5)
24P.PCB-1016
(12674-11-2)
25P.Toxaphene v
(8001-35-2)
EPA Form 3510-2C(8-90) PAGE V-9

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IL VIA.NORTH AND SOUTH DRAINS
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AIMS6616631 MXNII Mt rt 610E1 AL:n A

Pace Analytical Services,Inc.
C@Ay 9800 Kincey Ave. Suite 100
�i '�( Huntersville,NC 28078
/ [phone]
ANALYTICAL RESULTS
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2120E Color ADMI Analytical Method:SM 2120E Color ADMI
Color,ADMI ND units 25.0 1 01/15/15 13:19
Adjusted Color,ADMI ND units 25.0 1 01/15/15 13:19
pH 8.0 units 1.0 1 01/15/15 13:19
Adjusted pH,ADMI 7.6 units 1.0 1 01/15/15 13:19
HEM,Oil and Grease Analytical Method:EPA 1664B
Oil and Grease ND mg/L 5.0 1 01/16/15 09:40
200.7 MET ICP Analytical Method:EPA 200.7 Preparation Method:EPA 200.7
Aluminum ND ug/L 100 1 01/16/15 18:55 01/17/15 03:31 7429-90-5
Antimony ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-36-0
Arsenic ND ug/L 10.0 1 01/16/15 18:55 01/19/15 14:16 7440-38-2
Barium 35.0 ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-39-3
Beryllium ND ug/L 1.0 1 01/16/15 18:55 01/17/15 03:31 7440-41-7
Boron 74.8 ug/L 50.0 1 01/16/15 18:55 01/17/15 03:31 7440-42-8
Cadmium ND ug/L 1.0 1 01/16/15 18:55 01/17/15 03:31 7440-43-9
Chromium ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-47-3
Cobalt ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-48-4
Copper ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-50-8
Iron 71.9 ug/L 50.0 1 01/16/15 18:55 01/17/15 03:31 7439-89-6
Lead ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7439-92-1
Magnesium 45000 ug/L 100 1 01/16/15 18:55 01/17/15 03:31 7439-95-4
Manganese 206 ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7439-96-5
Molybdenum ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7439-98-7
Nickel ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-02-0
Selenium ND ug/L 10.0 1 01/16/15 18:55 01/17/15 03:31 7782-49-2
Silver ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-22-4
Thallium ND ug/L 10.0 1 01/16/15 18:55 01/17/15 03:31 7440-28-0
Tin ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-31-5
Titanium ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-32-6
Zinc ND ug/L 10.0 1 01/16/15 18:55 01/17/15 03:31 7440-66-6
245.1 Mercury Analytical Method:EPA 245.1 Preparation Method:EPA 245.1
Mercury ND ug/L 0.20 1 01/17/15 14:15 01/20/15 16:58 7439-97-6
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
Acenaphthene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 83-32-9
Acenaphthylene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 208-96-8
Anthracene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 120-12-7
Benzidine ND ug/L 50.0 1 01/20/15 14:00 01/22/15 01:08 92-87-5
Benzo(a)anthracene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 56-55-3
Benzo(a)pyrene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 50-32-8
Benzo(b)fluoranthene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 205-99-2
Benzo(g,h,i)perylene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 191-24-2
Benzo(k)fluoranthene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 207-08-9
4-Bromophenylphenyl ether ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 101-55-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:02/13/2015 03:34 PM without the written consent of Pace Analytical Services,Inc.. Page 6 of 56

q,,,�J �+ Pace Analytical Services,Inc.
Ce/`V Kl/ lc al a 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
[phone]
ANALYTICAL RESULTS
Project NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Dual
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
Butylbenzylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 85-68-7
4-Chloro-3-methylphenol ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 59-50-7
bis(2-Chloroethoxy)methane ND ugh 10.0 1 01/20/15 14:00 01/22/15 01:08 111-91-1
bis(2-Chloroethyl)ether ND ugh 5.0 1 01/20/15 14:00 01/22/15 01:08 111-44-4
bis(2-Chloroisopropyl)ether SLB ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 108-60-1 -'' IOZ'-Co•
2-Chloronaphthalene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 91-58-7
2-Chlorophenol ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 95-57-8
4-Chlorophenylphenyl ether ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 7005-72-3
Chrysene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 218-01-9
Dibenz(a,h)anthracene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 53-70-3
1,2-Dichlorobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 95-50-1
1,3-Dichlorobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 541-73-1
1,4-Dichlorobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/1501:08 106-46-7
3,3'-Dichlorobenzidine ND ug/L 25.0 1 01/20/15 14:00 01/22/15 01:08 91-94-1
2,4-Dichlorophenol ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 120-83-2
Diethylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 84-66-2
2,4-Dimethylphenol ND ugh 10.0 1 01/20/15 14:00 01/22/15 01:08 105-67-9
Dimethylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 131-11-3
Di-n-butylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 84-74-2
4,6-Dinitro-2-methylphenol ND ug/L 20.0 1 01/20/15 14:00 01/22/15 01:08 534-52-1✓
2,4-Dinitrophenol ND ug/L 50.0 1 01/20/1514:00 01/22/15 01:08 51-28-5
2,4-Dinitrotoluene ND ug/L 5.0 1 01/20/1514:00 01/22/15 01:08 121-14-2
2,6-Dinitrotoluene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 606-20-2
Di-n-octylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 117-84-0
1,2-Diphenylhydrazine ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 122-66-7
bis(2-Ethylhexyl)phthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 117-81-7
Fluoranthene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 206-44-0
Fluorene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 86-73-7
Hexachloro-1,3-butadiene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 87-68-3
Hexachlorobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 118-74-1
Hexachlorocyclopentadiene ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 77-47-4
Hexachloroethane ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 67-72-1
Indeno(1,2,3-cd)pyrene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 193-39-5
Isophorone ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 78-59-1
Naphthalene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 91-20-3
Nitrobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 98-95-3
2-Nitrophenol ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 88-75-5
4-Nitrophenol ND ug/L 50.0 1 01/20/15 14:00 01/22/15 01:08 100-02-7
N-Nitrosodimethylamine ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 62-75-9
N-Nitroso-di-n-propylamine ND ugh 5.0 1 01/20/1514:00 01/22/15 01:08 621-64-7
N-Nitrosodiphenylamine ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 86-30-6
Pentachlorophenol ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 87-86-5
Phenanthrene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 85-01-8
Phenol ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 108-95-2
Pyrene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 129-00-0
1,2,4-Trichlorobenzene ND ugh 5.0 1 01/20/15 14:00 01/22/15 01:08 120-82-1
2,4,6-Trichlorophenol ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 88-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:02/13/2015 03:34 PM without the written consent of Pace Analytical Services,Inc.. Page 7 of 56

Pace Analytical Services,Inc.
A cer_L yr iI• 9800 Kincey Ave. Suite 100
��f��/LIL. Huntersville,NC 28078
wwwp'cMb onm [phone]
I
ANALYTICAL RESULTS
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
Surrogates
Nitrobenzene-d5(S) 52 % 10-120 1 01/20/15 14:00 01/22/15 01:08 4165-60-0
2-Fluorobiphenyl(S) 47 % 15-120 1 01/20/15 14:00 01/22/15 01:08 321-60-8
Terphenyl-d14(S) 60 % 11-131 1 01/20/15 14:00 01/22/15 01:08 1718-51-0
Phenol-d6(S) 10 % 10-120 1 01/20/15 14:00 01/22/15 01:08 13127-88-3
2-Fluorophenol(S) 15 % 10-120 1 01/20/15 14:00 01/22/15 01:08 367-12-4
2,4,6-Tribromophenol(S) 32 % 10-137 1 01/20/15 14:00 01/22/15 01:08 118-79-6
624 Volatile Organics Analytical Method:EPA 624
Acrolein ND ug/L 5.0 1 01/17/15 08:15 107-02-8
Acrylonitrile ND ug/L 50.0 1 01/17/15 08:15 107-13-1
Benzene ND ug/L 2.0 1 01/17/15 08:15 71-43-2
Bromodichloromethane ND ug/L 2.0 1 01/17/15 08:15 75-27-4
Bromoform ND ug/L 2.0 1 01/17/15 08:15 75-25-2
Bromomethane ND ug/L 2.0 1 01/17/15 08:15 74-83-9
Carbon tetrachloride ND ug/L 2.0 1 01/17/15 08:15 56-23-5
Chlorobenzene ND ug/L 2.0 1 01/17/15 08:15 108-90-7
Chloroethane ND ug/L 2.0 1 01/17/15 08:15 75-00-3
2-Chloroethylvinyl ether ND ug/L 5.0 1 01/17/15 08:15 110-75-8
Chloroform ND ug/L 2.0 1 01/17/15 08:15 67-66-3
Chloromethane ND ug/L 2.0 1 01/17/15 08:15 74-87-3
o Dibromochloromethane ND ug/L 2.0 1 01/17/15 08:15 124-48-1
Dichlorodifluoromethane ND ug/L 2.0 1 01/17/15 08:15 75-71-8
1,1-Dichloroethane ND ug/L 2.0 1 01/17/15 08:15 75-34-3
1,2-Dichloroethane ND ug/L 2.0 1 01/17/15 08:15 107-06-2
1,1-Dichioroethene ND ug/L 2.0 1 01/17/15 08:15 75-35-4
trans-1,2-Dichloroethene ND ug/L 2.0 1 01/17/15 08:15 156-60-5
1,2-Dichloropropane ND ug/L 2.0 1 01/17/15 08:15 78-87-5
cis-1,3-Dichloropropene ND ug/L 2.0 1 01/17/15 08:15 10061-01-5
Ethylbenzene ND ug/L 2.0 1 01/17/15 08:15 100-41-4
Methylene Chloride ND ug/L 2.0 1 01/17/15 08:15 75-09-2
1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 01/17/15 08:15 79-34-5
Tetrachloroethene ND ug/L 2.0 1 01/17/15 08:15 127-18-4
Toluene ND ug/L 2.0 1 01/17/15 08:15 108-88-3
1,1,1-Trichloroethane ND ug/L 2.0 1 01/17/15 08:15 71-55-6
1,1,2-Trichloroethane ND ug/L 2.0 1 01/17/15 08:15 79-00-5
Trichloroethene ND ug/L 2.0 1 01/17/15 08:15 79-01-6
Trichlorofluoromethane ND ug/L 2.0 1 01/17/15 08:15 75-69-4
Vinyl chloride ND ug/L 2.0 1 01/17/15 08:15 75-01-4
Surrogates
4-Bromofluorobenzene(S) 97 % 70-130 1 01/17/15 08:15 460-00-4
Toluene-d8(S) 92 % 70-130 1 01/17/15 08:15 2037-26-5
1,2-Dichloroethane-d4(S) 101 % 70-130 1 01/17/15 08:15 17060-07-0
MBIO 9222D Fecal Coliform CHT Analytical Method:SM 9222D
Fecal Coliforms ND CFU/100 mL 1.0 1 01/14/15 14:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:02/13/2015 03:34 PM without the written consent of Pace Analytical Services,Inc.. Page 8 of 56

Pace Analytical Services,Inc.
Q/��,, /sem •wim9800 Kincey Ave. Suite 100
C8Alk11ybC21 Huntersville,NC 28078
D [phone]
ANALYTICAL RESULTS
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method:SM 2540D
Total Suspended Solids ND mg/L 2.9 1 01/21/15 03:31
4500CL G Chlorine,Residual Analytical Method:SM 4500-CI G
Chlorine,Total Residual 0.11 mg/L 0.024 1 01/16/15 11:00 7782-50-5 H1
4500S2D Sulfide Water Analytical Method:SM 4500-S2D
Sulfide ND mg/L 0.10 1 01/15/15 10:30 18496-25-8
5210B BOD,5 day Analytical Method:SM 5210B
BOD,5 day ND mg/L 2.0 1 01/15/15 05:57 01/20/15 06:51
Total Organic Nitrogen Calc. Analytical Method:TKN-NH3 Calculation
Total Organic Nitrogen ND mg/L 0.50 1 02/04/15 17:36
300.0 IC Anions 28 Days Analytical Method:EPA 300.0
Bromide 0.81 mg/L 0.20 2 01/21/15 04:36 24959-67-9
Fluoride ND mg/L 0.50 1 01/17/15 05:37 16984-48-8
Sulfate 342 mg/L 20.0 10 01/17/15 11:49 14808-79-8
350.1 Ammonia Analytical Method:EPA 350.1
Nitrogen,Ammonia ND mg/L 0.10 1 01/27/15 20:08 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method:EPA 351.2
Nitrogen,Kjeldahl,Total ND mg/L 0.50 1 01/30/15 15:05 7727-37-9 M1
353.2 Nitrogen,NO2/NO3 pres. Analytical Method:EPA 353.2
Nitrogen,NO2 plus NO3 ND mg/L 0.020 1 01/30/15 18:31
365.1 Phosphorus,Total Analytical Method:EPA 365.1
Phosphorus ND mg/L 0.050 1 01/28/15 17:02 7723-14-0
420.4 Phenolics,Total Analytical Method:EPA 420.4 1°5 .,iSI7
Phenol ND mg/L 0.010 1 �o.`p.P4J' 01/29/15 15:48 108-95-2
4500CNE Cyanide,Total Analytical Method:SM 4500-CN-E
Cyanide ND mg/L 0.0080 1 01/26/15 14:48 57-12-5
5220D COD Analytical Method:SM 5220D
Chemical Oxygen Demand 30.0 mg/L 25.0 1 01/15/15 14:20
5310B TOC Analytical Method:SM 53108
Total Organic Carbon 3.7 mg/L 1.0 1 01/16/15 13:57 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:02/13/2015 03:34 PM without the written consent of Pace Analytical Services,Inc.. Page 9 of 56

Pace Analytical Services,Inc.
aceAnalytical a 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS-RADIOCHEMISTRY
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix:Water
PWS: Site ID: Sample Type:
Parameters Method Act±Unc(MDC)Carr Trac Units Analyzed CAS No. Qual
Gross Alpha EPA 900.0 7.64±2.41 (2.69) pCi/L 01/27/15 21:32 12587-46-1
C:NA TTNA
Gross Beta EPA 900.0 6.28±1.47 (1.29) pCi/L 01/27/15 21:32 12587-47-2
C:NA T:NA
Radium-226 EPA 903.1 0.0627±0.325 (0.675) pCi/L 02/03/15 11:18 13982-63-3
C:NA T:86%
Radium-228 EPA 904.0 0.244±0.405 (0.882) pCi/L 01/30/15 16:07 15262-20-1
C:89%T:61%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.. Page 43 of 56

Analytical Results
Pace Analytical �?0114
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date: 01/15/2015 STATESVILLE
Reported: 02/04/2015
For: 9223379 ANALYTICAL L j rAL
Comments:
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
150115-12-01 MBAS 001 0.17 mg/L SM5540C-2000 01/15/2015 MD
Respectfully submitted,
Dena Myers
NC Cert#440,
NCDW Cert#37755,
EPA#NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 rage 55 of 56

s
Analytical Environmental Services,Inc Date: 19-Feb-15
Client: Pace Analytical Services,Inc. Client Sample ID: 001
Project Name: 92238054 Collection Date: 2/18/2015 9:02:00 AM
Lab ID: I 502G20-001 Matrix: Aqueous
Reporting Dilution
Analyses Result Qual Units BatchlD Date Analyzed Analyst
Limit Factor
Sulfite by SM4500-S03-B
Sulfite BRL 2.00 H mg/L R286188 1 02/19/2015 15:30 OM
Qualifiers: • Value exceeds maximum contaminant level E Estimated(value above quantitation range)
BRL Below reporting limit S Spike Recovery outside limits due to matrix
11 Holding times for preparation or analysis exceeded Narr Sec case narrative
N Analytc not NELAC certified NC Not confirmed
B Analyte detected in the associated method blank < Less than Result value
> Greater than Result value 1 Estimated value detected below Reporting Limit
Page 13 of 15
4 of 6

+ •F
Condition of Receipt
Sample Number 150115-12-01 Temp on Arrival: 2
Parameter Schedule: MBAS
Received on Ice
Chemicals in containers, lab
PO Box 228 •Statesville, NC 28687 • 704/872/4697
Page 2 of 56 of 56

NPDES INDUSTRIAL DISCHARGE RENEWAL
FMC CORPORATION
LITHIUM DIVISION
NPDES PERMIT NC0005177
OUTFALL 001

4
EPA I.D.NUMBER(copy from Item 1 of Form I) Form Approved.
NCD 000771964 OMB No.2040-0086.
Please print or type in the unshaded areas only. Approval expires 3-31-98.
FORM U.S.ENVIRONMENTAL PROTECTION AGENCY
APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
2C -TEPAEXISTING MANUFACTURING,,COMMERCIAL,MINING AND SILVICULTURE OPERATIONS
NPDES Consolidated Permits Program
I.OUTFALL LOCATION
For each outfall,list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A.OUTFALL NUMBER B.LATITUDE C.LONGITUDE
(list) 1.DEG. 2.MIN. 3.SEC. t DEG. 2.MIN. 3.SEC. D.RECEIVING WATER(name)
001 35.00 15.00 43.00 81.00 17.00 54.00 First Creek
004 35.00 15.00 43.00 81.00 17.00 54.00 First Creek
II.FLOWS,SOURCES OF POLLUTION,AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility.Indicate sources of intake water,operations contributing wastewater to the effluent,and treatment units
labeled to correspond to the more detailed descriptions in Item B.Construct a water balance on the line drawing by showing average flows between intakes,operations,
treatment units,and outfalls.If a water balance cannot be determined(e.g.,for certain mining activities),provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall,provide a description of:(1)All operations contributing wastewater to the effluent,including process wastewater,sanitary wastewater,cooling water,
and storm water runoff; (2)The average flow contributed by each operation; and (3)The treatment received by the wastewater. Continue on additional sheets if
necessary.
1.OUT- 2.OPERATION(S)CONTRIBUTING FLOW 3.TREATMENT
FALL b.AVERAGE FLOW b.LIST CODES FROM
NO.(list) a.OPERATION(list) (include units) a.DESCRIPTION TABLE 2C-1
1) Misc. Salts and Cat. Phosphate _5,000 gals/mth None
001 X x
2) LiOCL Air Scrubber Waste WaterH202 Addition and Equalization
-100 2 L
4Pm
3) Boiler slowdown 'None
-15 gpm x x
4)LiCl RO permeate and condesate _9,550 GPD Reverse Osmosis 1 S
5) left blank
6) Compressor Condensatec1 None X
gpm X
7) Li Hydroxide RO Reverse Osmosis
-5,000 gals/mth 1 S
B) Battery Metal Cooling Tower None
<10 gpm X X
9) Combined Plant Waste Water 130 m pH adjustment 2 x
gP
10) Li Hydroxide Cooling Twr. None
35 gpm x x
11) R&D Pond stormwater management 10 m Setteling X x
gP
OFFICIAL USE ONLY(effluent guidelines sub-categories)
EPA Form 3510-2C(8-90) PAGE 1 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C.Except for storm runoff,leaks,or spills,are any of the discharges described in Items II-A or B intermittent or seasonal?
©YES(complete the following table) ❑NO(go to Section III)
3.FREQUENCY 4.FLOW
a.DAYS PER B.TOTAL VOLUME
2.OPERATION(s) WEEK b.MONTHS a.FLOW RATE(in mgd) (sperih.edrh emhs)
1.OUTFALL CONTRIBUTING FLOW (sperifj• PER YEAR 1.LONG TERM 2.MAXIMUM 1.LONG TERM 2.MAXIMUM C.DURATION
NUMBER(list) (iist) average) (saec,t'overage) AVERAGE DAILY AVERAGE DAILY (in dap)
001 1) Misc. Salts and Cat. Phosphate --- 6 --- 0.005 --- 5,000 gal ---
11) R&D Pond stormwater management 7 6 --- 0.015 ---- 0.010 MG 180
III.PRODUCTION
A.Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
0 YES(complete Item Ill-B) NO(go to Section IV)
B.Are the limitations in the applicable effluent guideline expressed in terms of production(or other measure of operation)?
❑YES(complete Item Ill-C) ❑NO(go to Section IV)
C.If you answered"yes"to Item III-B,list the quantity which represents an actual measurement of your level of production,expressed in the terms and units used in the
applicable effluent guideline,and indicate the affected outfalls.
1.AVERAGE DAILY PRODUCTION
C.OPERATION,PRODUCT,MATERIAL,ETC. 2.AFFECTED OUTFALLS
a.QUANTITY PER DAY b.UNITS OF MEASURE (list outfall numbers)
(specify)
IV.IMPROVEMENTS
A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application?This includes,but is not limited to,
permit conditions,administrative or enforcement orders,enforcement compliance schedule letters,stipulations,court orders,and grant or loan conditions.
❑YES(complete the f011owing table) NO(go to Item IV-B)
1.IDENTIFICATION OF CONDITION, 2.AFFECTED OUTFALLS 3.BRIEF DESCRIPTION OF PROJECT 4.FINAL COMPLIANCE DATE
AGREEMENT,ETC.
a.NO. b.SOURCE OF DISCHARGE a.REQUIRED b.PROJECTED
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges)you now have underway or which you plan.Indicate whether each program is now underway or planned,and indicate your actual or planned schedules for
construction.
❑MARK"X"IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C(8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA I.D.NUMBER(copy from Item 1 of Form 1)
CONTINUED FROM PAGE 2 NC000771964
V.INTAKE AND EFFLUENT CHARACTERISTICS
A,B,&C: See instructions before proceeding-Complete one set of tables for each outfall-Annotate the outfall number in the space provided.
NOTE:Tables V-A,V-B,and V-C are included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions,which you know or have reason to believe is discharged or may be discharged
from any outfall.For every pollutant you list,briefly describe the reasons you believe it to be present and report any analytical data in your possession.
1.POLLUTANT 2.SOURCE 1.POLLUTANT 2.SOURCE
VI.POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS
Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct?
®YES(list all such pollutants below) ❑NO(go to Item V7-B)
EPA Form 3510-2C(8-90) PAGE 3 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
VII.BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
171 YES(ident Jv the test(s)and describe their purposes below) ❑NO(go to Section VIII)
Chronic Toxicity, Presently required by our NPDES discharge Permit of outfall 001.
VIII.CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
®YES(list the name,address,and telephone number of and pollutants analyzed by, ❑NO(go to Section IX)
each such laboratory or firm below)
A.NAME B.ADDRESS C.TELEPHONE D.POLLUTANTS ANALYZED
(area code&no.) (list)
Pace Analytical Services 9800 Kincey Ave. Suite 100 704-875-9092 See page 4 of Pace
Huntersville, NC 28078 Analytical report
Pace Analytical Services 2225 Riverside Dr. See page 4 of Pace
Asheville, NC 828-254-7176 Analytical report
Pace Analytical Services 1638 Roseytown Rd. Suites 2,3&4 724-850-5600 See page 4 of Pace
Greensburg, PA 15601 Analytical report
Pace Analytical Services 8 East Tower Circle, 386-672-5668 See page 4 of Pace
Ormond Beach, FL 32174 Analytical report
Pace Analytical Services 205 East Meadow Road Suite A 336-623-8921 See page 4 of Pace
Eden, NC 27288 Analytical report
Statesville Analytical PO Box 228 704-872-4697 See page 4 of Pace
Statesville, NC 28687 Analytical report
IX.CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there
are significant penalties for submitting false information,including the possibility of fine and imprisonment for knowing violations.
A.NAME&OFFICIAL TITLE(type or print) B.PHONE NO.(area code&no.)
Bruce Urban (704) 868-7650
C.SIGNATU E �J D.DATE SIGNED
EPA Form 3510-2C(8-90) PAGE 4 of 4

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY.You may report some or all of this information EPA I.D.NUMBER(copy from Item I of Form!)
on separate sheets(use the same format)instead of completing these pages.
NC 000771964
SEE INSTRUCTIONS.
OUTFALL NO.
V.INTAKE AND EFFLUENT CHARACTERISTICS(continued from page 3 of Form 2-C)
PART A-You must provide the results of at least one analysis for every pollutant in this table.Complete one table for each outfall.See instructions for additional details.
3.UNITS 4.INTAKE
2.EFFLUENT (speciifyifblank) (optional)
b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
a.MAXIMUM DAILY VALUE (if available) (if available) AVERAGE VALUE
d.1.POLLUTANT (1) (�) ANALOYSES.OF aTRATION b.MASS (�) ANALYSES
CONCENTRATION (2)MASS CONCENTRATION (2)MASS (1)CONCENTRATION (2)MASS CONCENTRATION (2)MASS
a.Biochemical Oxygen 11.2 mg/1 48.7 lb --- --- 1.75 mg/1 135 lbs 8 mg/1 lbs
Demand(BOD)
b.Chemical Oxygen 30 mg/1 --- --- --- --- --- 1 mg/1 lbs
Demand(COD)
c.Total Organic Carbon
(TOC) 3.7 mg/1 --- --- --- --- --- 1 mg/1 lbs
d.Total Suspended
Solids(TSS) 3.0 mg/1 12.1 lb --- --- 0.19 mg/1 14.4 lbs 16 mg/1 lbs
e.Ammonia(as N) <0.1 mg/1 --- --- --- --- --- 1 mg/1 lbs
VALUE VALUE VALUE VALUE
f.Flow 0.537 MG 16.26 MG 9.2 MGD 1 yr --- MG
g.Temperature VALUE VALUE VALUE VALUE
(winter) 8.1 --- --- °C
h.Temperature VALUE VALUE VALUE VALUE
(summer) 27.05 --- --- °C
MINIMUM MAXIMUM MINIMUM MAXIMUM
i.pH 7.6 8.3 31 STANDARD UNITS
PART B- Mark"X"in column 2-a for each pollutant you know or have reason to believe is present.Mark"X"in column 2-b for each pollutant you believe to be absent.If you mark column 2a for any pollutant which is limited either
directly,or indirectly but expressly,in an effluent limitations guideline,you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a,you must provide
quantitative data or an explanation of their presence in your discharge.Complete one table for each outfall.See the instructions for additional details and requirements.
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM AVERAGE
ANDa b. a.MAXIMUM DAILY VALUE (if available) (if available) VALUE
CAS NO. BELIEVED BELIEVED (1) (i) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(if available) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Bromide
(24959-67-9) X 0.81 1 mg/1
b.Chlorine.Total
Residual <0.11 1 mg/1
c.Color X <25 1 ADM I
d Fecal Coliform X <1.0 1 CFU/100m
e.Fluoride
(16984.48-8) <0.50 1 mg/1
(asitv)te-Nitrite X <0.020 <0.10 4 mg/1
EPA Form 3510-2C(8-90) PAGE V-1 CONTINUE ON REVERSE

ITEM V-B CONTINUED FROM FRONT
2.MARK'X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional) `
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
ANDe, b. a.MAXIMUM DAILY VALUE (if available) (if available) AVERAGE VALUE
CAS NO. BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(ifavailable) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
g.Nitrogen, \ /
Total Organic(as X <0.50 1 mg/1
N)
h.oil and X <5.0 1 mg/1
Grease
i.Phosphorus X
` ,
(as P),Total <0.050 1 mg/1
(7723-14-0) -
j.Radioactivity
(t)Alpha,Total X 7.64+-2.41 1 pCi/L
(2)Beta,Total X 6.28+-1.47 1 pCi/L
(3)Radium, X .244+-.405 1 pCi/L
Total
(4)Radium 226, X ,062+-.325 1 pCi/L
Total
k.Sulfate
(also,) X 342 1 mg/1
(14808-79-8)
I. e
( X <0.10 1 mg/1
(ash
m.Sulfite
(arSO,) X <2.00 1 mg/1
(14265.45-3)
n.Surfactants X 0.17 1 mg/1
o.Aluminum,
Total X <100 1 ug/1
(7429-90-5)
p.(7440-39-3)Barium,Total X 35.0 1 ug/1
(
q.Boron,Total
X 74.8 1 ug/1
(7440-42-8))
r.Cobalt Total
(7440-48-4) X <5.0 1 ug/1
s.Iron,Total
(7439$9.6) X <71.9 1 ug/1
(
t.Magnesium, X
Total 45000 1 ug/1
(7439-95-4)
u.Molybdenum, X
TOtaI <5.0 1 ug/1
(7439-98-7)
v.Manganese, X
Total 206 1 ug/1
(7439-96-5)
w.40'Total
(7440-31-5) X <5.0 1 ug/1
a
Titanium.
X
Total <5.0 1 ug/1
(7440-32-6)
EPA Form 3510-2C(8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D.NUMBER(copy from Item I of Form I) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C NC000771964 001
PART C- If you are a primary industry and this outfall contains process wastewater,refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for.Mark'X'in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals,cyanides,and total phenols.If you are not required to mark column 2-a(secondary industries,nonprocess wastewater outfalls,and nonrequired GC/MS
fractions),mark°X"in column 2-b for each pollutant you know or have reason to believe is present.Mark"X"in column 2-c for each pollutant you believe Is absent.If you mark column 2a for any pollutant,you must
provide the results of at least one analysis for that pollutant.If you mark column 2b for any pollutant,you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater.If you mark column 2b for acrolein,acrylonitrile,2,4 dinitrophenol,or 2-methyl-4,6 dinitrophenol,you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater.Otherwise,for pollutants for which you mark column 2b,you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged.Note that there are 7 pages to this part;please review each carefully.Complete one table(all 7 pages)for each outfall.See instructions for
additional details and requirements.
2.MARK"X° 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
ANDa. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) d.NO.OF a.CONCEN- b.NO.OF
(if available) REQUIRED PRESENT ABSENT (1) (1)
(1)
CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ALYSES
METALS,CYANIDE,AND TOTAL PHENOLS
1M(7440-36.0)y TotalX X <5.0 1 ug/1
Arsenic.Total
(7440-38-2) X X <10.0 1 ug/1
/�
3M.Beryllium,Total
(7440-41-7) /�>( X <1.0 1 ug/1
4M.Cadmium,Total
(7440.43-9) X X <1.0 1 ug/1
5M.Chromium,
Total(7440-47-3) X X <5.0 1 ug/1
44
6M. tal X X <5.0 1 ug/1
7M.Lead,Total
(7439-92-1) X X <5.0 1 ug/1
8M.Mercury,Total
(7439-97-6) X X 0.747 1 ng/1
9M.Nickel,Total X X <5.0 1 ug/1
(7440-02-0)
10M.Selenium,
Total(7782-49-2) X X <10.0 1 ug/1
11M.Silver,Total
(7440-22-4) X X <5.0 1 ug/1
12M.Thallium,
Total(7440-28-0) X X <10.0 1 ug/1
(74MOZinc,)otal X X <10.0 1 ug/1
14M.Cyanide, /�
Total(57-12-5) X X <0.0080 1 mg/1
15M.
Total Phenols, X X <0.01 0 1 mg/1
DIOXIN
2,3,7,8-Tetra- X DESCRIBE RESULTS
chlorodibenzo-P-
Dioxin(1764-01-6)
EPA Form 3510-2C(8-90) PAGE V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK'X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BEUEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
Of available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ,ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION-VOLATILE COMPOUNDS
2-8
(10 X X <5.0 1 ug/1
(107.0-02-a))
2
Ai<rWe
(1 X X <50 1 ug/1
(107-13-1)13-1)
3V.BX X <2 0 1 ug/1
(71-43-2) /�
4V.Bis(Odom- ` , \ ,
methyl)Ether X JX <5.0 1 ug/1
(542-88-1)
orm
(7 X X <2.0 1 ug/1
(75.25-2)25-2)
6V.Carbon
Tetrachloride X X <2.0 1 ug/1
(56-23-5)
7V.Chlorobenzene X X <2.0 1 ug/1
(106-90--90-7)
8V.Chlorodi- \ , \/
bromomethane J� x <2.0 1 ug/1
(124.48-1) , ` ' `
3)oethane
(75-00-3) /�X/ X <2 0 1 ug/1
loro-
ethylvinyl Ether X X
<5.0 1 ug/1
(110-75-8)
11V.Chloroform X X <2.0 1 ug/1
(67-66-3)
bro12V.Dichloro-
b'Of1X X
OA11B <2.0 1 ug/1
(75-27.4)
13V.Dichloro-
difluoromethane <2.0 1 ug/1
(75-71.8)
14Vetha a(75-1,1-Di4-3) X X <2.0 1 ug/1
ethane(75-34-3)
etha15V.a(107-06-2) X X <2.0 1 ug/1
etliane(107-06-2)
eth leve(75-5-4) X X <2.0 1 ug/1
ethylene(75-35-4)
7V.1.2-Dichlaro• X X
propane(78-87-5) <2.0 1 ug/1
18V.1.3-Dichloro-
ProPY X X <2.0 1 ug/1
(542-75-6)
190.Ethylbenzene
(100.41.4) X X <2.0 1 Ug/1
^ `,
20V.Methyl Bromide
7( <2.0 1 ug/1
Bromide(74-83-9) ` , ,``,
21V.Methyl y X <2.0 1 ug/1
Chloride(74-87-3) /\
EPA Form 3510-2C(8-90) PAGE V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c, a.MAXIMUM DAILY VALUE Of available) VALUE(f available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED d.NO.OF a.CONCEN- LNALYSES
.NO.OF
CONCE(1RATION (2)MASS CONCETRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS( available REQUIRED PRESENT ABSENT ANALYSES TRATION b.MASS
GC/MS FRACTION-VOLATILE COMPOUNDS(continued)
22V.Methylene
CX X <2.0 1 ug/1Chloride(75 09-2)
23V.1,1.22-
Tetrachloroethane X X <2.0 1 ug/1
(79-34-5)
24V.Tetrachloro-
ethylene
�/ <2.0 1 ug/1
ethylene ne((1227-18-4) X X
25V.
Toluene
X X <2.0 1 ug/1
(108-88-3)
26V.1,2-Trans-
Dichbroe6,ylene X X <2.0 1 ug/1
(15650-5)
27V.1,1,1-Trichloro-
ethane(71-55-6)
1-Trichloro-
ethane(71-55-6) X X <2.0 1 ug/1
28V.1, ichbro-
X X <2.0 1 ug/1
(79-0
ethane(79-00-5)
29V Trichloro-
ethylene(79-01-6) X X <2.0 1 ug/1
30V.Trichloro-
fluoromethane X X <2.0 1 ug/1
(75-69-4)
5(7.01.4)l Chloride X X <2.0 1 ug/1
GC/MS FRACTION-ACID COMPOUNDS
1A.2-Chlorophenol
(95-57-8) X X <5.0 1 ug/1
_
2A.2,4-Dichloro X X <5.0 1 ug/1
phenol(120-83-2)
3A.2,4-Dinlethyl X X <10.0 1 ug/1
phenol(105-67-9)
4A.4,6-Dinitro-O-
X X <20.0 1 ug/1
Cresol(534-52-1)
ph n lrX X <50.0 1 ug/1
phenol(51-28-5)
6A.2-Nitrophend X X <5.0 1 ug/1
(88-75-5)
7A. -02-7) nmol X X <50.0 1 ug/1
(10002-7)
8A
Cr ofP-(59 50-7 X X <5.0 1 ug/1
Creed(59-50 7)
9A.Pentachloro-
X X <10.0 1 ug/1
phenol(87-86-5)
10A.Phenol
(108-95-2) X X <5.0 1 ug/1
phenol(88-0 -2) X X <10.0 1 ug/1
phenol(88-05-2)
EPA Form 3510-2C(8-90) PAGE V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK'X' 3.EFFLUENT _ 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. a a.MAXIMUM DAILY VALUE (if-available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(if available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ALYSES
GC/MS FRACTION-BASE/NEUTRAL COMPOUNDS
8.3Acenaphthene
( X X <5.0 1 ug/1
(83-32-9)2-9) /�
28.Acenaphtylene �/ X <5.0 1 ug/1
X
(208.96-8)
3B.Anthracene
(120-12-7) X X <5.0 1 ug/1 •_
48.Benzidine
(92 87 X X <50.0 1 ug/1
(97-5)5)
5B.Benzo(a)
Anthracene X X <5.0 1 ug/1
(58-55-3) ,
6B.Benzo(a) X X <5.0 1 ug/1
Pyrene(50-32-8)
7B. I X
Iluorantuoranthene
X <5.0 1 ug/1
(205-99-2)
8B.Benzo(girl)
Perylene(191-24-2) X X <5.0 1 ug/1
98.Benzo(k)
Fluorantherre X X <5.0 1 ug/1
(207.08-9) _
10B.Bis(2-Chloro-
erhosy)Methane X X <10.0 1 ug/1
(111-91-1)
11B.Bis(2-Chloro-
ethyl)Ether X X <5.0 1 ug/1
(111-44-4)
12B.BIs(2-
Chlorobopropy!) X X <5.0 1 ug/1
Ether(102-80.1)
13B.Bis(2-Erhpl-
hery!)Phthalate X X <5.0 1 ug/1
(117431-7)
148.4-Bromophenyl
Phenyl Ether X X <5.0 1 ug/1
(101-55-3) _
158.Butyl Benzyl X X <5.0 1 ug/1
Phthalate(85-68-7)
16B.2-Chloro-
naphthalene X X <5.0 1 ug/1
(91-58-7)
178.4-Chloro-
phenyl Phenyl Ether X X <5.0
1 ug/1
(7005-72-3) _
Chrysene X X <5.0 1 ug/1
(218-01218-01-9)
19B.Dibenzo(air)
Anthracene(53-70-3) X X <5.0 1 ug/1
beB.ne e(95-50-I X X <5.0 1 ug/1
benzene(95-50-1)
21B.1.3-01-chloro-
benzene
.3-Di-chloro- �/
benzene(541-73-1) X X <5.0 1 ug/1
EPA Form 3510-2C(8-90) PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
2.MARK'X' 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c, a.MAXIMUM DAILY VALUE (if available) VALUE(ifavailable) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(ifavailable) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ALYSES
GC/MS FRACTION-BASE/NEUTRAL COMPOUNDS(continued)
benzene X06 46 7) X X <5.0 1 ug/1
23B.3,3-Dichloro-
benzidine(91-94-1) X X <25.0 1 ug/1
248.Diethyl
Phthalate(84-66-2) X X <5.0 1 ug/1
258.Dimethyl X X
Phthalate alate <5.0 1 ug/1
(131-11-3)
26B.Di-N-Butyl
Phthalate(84-74-2) X X <5.0 1 ug/1
27B.2,4-Dinitro-
toluene(121-14-2) X X <5.0 1 ug/1
28B.2,6-Dinitro-
toluene(606-20-2) X X <5.0 1 ug/1
29B.Di-N-Octyl
Phthalate(117-84-0) X X <5.0 1 ug/1
h1,2-Diphenyl-
hydrazine
ias - X X
hydrydr azzinee Azo
(as Am <5.0 1 ug/1
benzene)(122-66-7)
(144-0) e X X <5.0 1 ug/1
(86-73-77) X X <5.0 1 ug/1
33B.Hexachloro-
benzene(118-74-1) X X <5.0 1 ug/1
34B.Hexachloro-
butadiene(87-68-3) X X <5.0 1 ug/1
35B.Hexachlaro-
(cyc
77 lopentadiene
X X <10.0 1 ug/1
36B Hexachloro-
ethane(67-72-1) X X <5.0 1 ug/1
372.-cd) X X
(1Pyrene <5.0 1 ug/1
(1993-39-3.39.5)
3813.Isophorone
(78-59-1) X X <10.0 1 ug/1
398.Naphthalene
(91-20-3) X <5.0 1 ug/1
40(98-95-3)o<xer'Zer�e X X <5.0 1 ug/1
41B.N-Nitro-
BOdiAeBiylar"ine <5.0 1 ug/1
(62-75-9) X X
42B.N-Nitroaodi-
N-Propylarrine X X <5.0 1 ug/1
(621.64-7)
EPA Form 3510-2C(3-90) PAGE V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK"X' 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(if available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(continued)
43B.N-Nitro- `,
sodiphenylamine X X <10.0 1 ug/1
(86-30-6) ' ` _
44B.Phenanthrene
(85-01-8) X X <5.0 1 ug/1
45B.Pyrene
(129-00-0) X X <5.0 1 ug/1
46B.1.2,4-Tri- .
chloro(120-8 -1) X X <5.0 1 ug/1
(120-82-1)
GC/MS FRACTION—PESTICIDES
1P.Aldrin X
(309-00-2)
2P.a-BHC X
(319.84-6)
3P.(S-BHC X
(319-85-7)
4P.y-BHC \/
(58-89-9) X
5P.5-BHC X
(319-86-8)
6P.Chlordane X
(57-74-9)
7P.4,4'-DOT \/
(50-29-3) X
8P.4,4'-DDE X
(72-55-9)
9P.4,4'-DDD \/
(72-54-8) X
10P.Dieldrin X
(60-57-1)
11P.a-Enosulfan X
(115-29-7)
12P.(-Endosulfan
(115-29-7)
13P.Endosulfan
Sulfate X
(1031-07-8)
14P.Endrin X
(72-20-8)
15P.Endrin
Aldehyde X
(7421-93-4)
16P.Heptachlor �/
(76-44-8) X
EPA Form 3510-2C(8-90) PAGE V-8 CONTINUE ON PAGE V-9

EPA I.D.NUMBER(copy from Item/of Form l) OUTFALL NUMBER
NC000771964 001
CONTINUED FROM PAGE V-8
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED d.NO.OF a.CONCEN- b.NO.OF
(if available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATIONIANALYSES TRATION b.MASS (1) ANALYSES
(2)MASS CONCENTRATION (2)MASS
GC/MS FRACTION—PESTICIDES(continued)
o.Heptachlor
E
Epoxide
(1024-57-3)
18P.PCB-1242 �/
(53469-21-9) /�
19P.PCB-1254 v
(11097-69-1)
20P.PCB-1221 �/
(11104-28-2) /�
2W.PCB-1232 v
(11141-16-5)
22P.PCB-1248 v
(12672-29-6)
23P.PC8-1260
(11096-82-5)
24P.PCB-1016
(12674-11-2)
25P.Toxaphene v
(8001-35-2) /X
EPA Form 3510-2C(8-90) PAGE V-9

ac
` Pace Analytical Services,Inc.
eAnalyt�cal• 9800 Kincey Ave. Suite 100
G Huntersville,NC 28078
' viviwpacalabacom [phone]
ANALYTICAL RESULTS
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2120E Color ADMI Analytical Method:SM 2120E Color ADMI
Color,ADMI ND units 25.0 1 01/15/15 13:19
Adjusted Color,ADMI ND units 25.0 1 01/15/15 13:19
pH 8.0 units 1.0 1 01/15/15 13:19
Adjusted pH,ADMI 7.6 units 1.0 1 01/15/15 13:19
HEM,Oil and Grease Analytical Method:EPA 1664B
Oil and Grease ND mg/L 5.0 1 01/16/15 09:40
200.7 MET ICP Analytical Method:EPA 200.7 Preparation Method:EPA 200.7
Aluminum ND ug/L 100 1 01/16/15 18:55 01/17/15 03:31 7429-90-5
Antimony ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-36-0
Arsenic ND ug/L 10.0 1 01/16/15 18:55 01/19/15 14:16 7440-38-2
Barium 35.0 ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-39-3
Beryllium ND ug/L 1.0 1 01/16/15 18:55 01/17/15 03:31 7440-41-7
Boron 74.8 ug/L 50.0 1 01/16/15 18:55 01/17/15 03:31 7440-42-8
Cadmium ND ug/L 1.0 1 01/16/15 18:55 01/17/15 03:31 7440-43-9
Chromium ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-47-3
Cobalt ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-48-4
Copper ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-50-8
Iron 71.9 ug/L 50.0 1 01/16/15 18:55 01/17/15 03:31 7439-89-6
Lead ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7439-92-1
Magnesium 45000 ug/L 100 1 01/16/15 18:55. 01/17/15 03:31 7439-95-4
Manganese 206 ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7439-96-5
Molybdenum ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7439-98-7
Nickel ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-02-0
Selenium ND ug/L 10.0 1 01/16/15 18:55 01/17/15 03:31 7782-49-2
Silver ND ugh 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-22-4
Thallium ND ugh 10.0 1 01/16/15 18:55 01/17/15 03:31 7440-28-0
Tin ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-31-5
Titanium ND ug/L 5.0 1 01/16/15 18:55 01/17/15 03:31 7440-32-6
Zinc ND ug/L 10.0 1 01/16/15 18:55 01/17/15 03:31 7440-66-6
245.1 Mercury Analytical Method:EPA 245.1 Preparation Method:EPA 245.1
Mercury ND ug/L 0.20 1 01/17/15 14:15 01/20/15 16:58 7439-97-6
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
Acenaphthene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 83-32-9
Acenaphthylene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 208-96-8
Anthracene ND ugh 5.0 1 01/20/15 14:00 01/22/15 01:08 120-12-7
Benzidine ND ugh 50.0 1 01/20/15 14:00 01/22/1501:08 92-87-5
Benzo(a)anthracene ND ugh 5.0 1 01/20/15 14:00 01/22/15 01:08 56-55-3
Benzo(a)pyrene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 50-32-8
Benzo(b)fluoranthene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 205-99-2
Benzo(g,h,l)perylene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 191-24-2
Benzo(k)fluoranthene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 207-08-9
4-Bromophenylphenyl ether ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 101-55-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:02/13/2015 03:34 PM without the written consent of Pace Analytical Services,Inc.. Page 6 of 56

Pace Analytical Services,Inc.
Cn y^'l• 9800 Kincey Ave. Suite 100
G IJ'LIJJ 1 Huntersville,NC 28078
wevapaceiebscom [phone]
ANALYTICAL RESULTS
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
Butylbenzylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 85-68-7
4-Chloro-3-methylphenol ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 59-50-7
bis(2-Chloroethoxy)methane ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 111-91-1
bis(2-Chloroethyl)ether ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 111-44-4 ,
bis(2-Chloroisopropyl)ether SLB ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 108-60-1 KA,'w�
2-Chloronaphthalene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 91-58-7
2-Chlorophenol ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 95-57-8
4-Chlorophenylphenyl ether ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 7005-72-3
Chrysene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 218-01-9
Dibenz(a,h)anthracene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 53-70-3
1,2-Dichlorobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 95-50-1
1,3-Dichlorobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 541-73-1
1,4-Dichlorobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/1501:08 106-46-7
3,3'-Dichlorobenzidine ND ug/L 25.0 1 01/20/15 14:00 01/22/15 01:08 91-94-1
2,4-Dichiorophenol ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 120-83-2
Diethylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 84-66-2
2,4-Dimethylphenol ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 105-67-9
Dimethylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 131-11-3
Di-n-butylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 84-74-2
4,6-Dinitro-2-methylphenol ND ug/L 20.0 1 01/20/15 14:00 01/22/15 01:08 534-52-1✓
2,4-Dinitrophenol ND ug/L 50.0 1 01/20/15 14:00 01/22/15 01:08 51-28-5
2,4-Dinitrotoluene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 121-14-2
2,6-Dinitrotoluene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 606-20-2
Di-n-octylphthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 117-84-0
1,2-Diphenylhydrazine ND ug/L 5.0 1 01/20/15 14:00 01/22/1501:08 122-66-7
bis(2-Ethylhexyl)phthalate ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 117-81-7
Fluoranthene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 206-44-0
Fluorene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 86-73-7
Hexachloro-1,3-butadiene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 87-68-3
Hexachlorobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 118-74-1
Hexachlorocyclopentadiene ND ug/L 10.0 1 01/20/15 14:00 01/22/1501:08 77-47-4
Hexachloroethane ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 67-72-1
Indeno(1,2,3-cd)pyrene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 193-39-5
Isophorone ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 78-59-1
Naphthalene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 91-20-3
Nitrobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 98-95-3
2-Nitrophenol ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 88-75-5
4-Nitrophenol ND ug/L 50.0 1 01/20/15 14:00 01/22/15 01:08 100-02-7
N-Nitrosodimethylamine ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 62-75-9
N-Nitroso-di-n-propylamine ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 621-64-7
N-Nitrosodiphenylamine ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 86-30-6
Pentachlorophenol ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 87-86-5
Phenanthrene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 85-01-8
Phenol ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 108-95-2
Pyrene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 129-00-0
1,2,4-Trichlorobenzene ND ug/L 5.0 1 01/20/15 14:00 01/22/15 01:08 120-82-1
2,4,6-Trichlorophenol ND ug/L 10.0 1 01/20/15 14:00 01/22/15 01:08 88-06-2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full.
Date:02/13/2015 03:34 PM without the written consent of Pace Analytical Services,Inc.. Page 7 of 56

, . .4
Pace Analytical Services,Inc.
•n�snp�/�� r�r 9800 Kinney Ave. Suite 100
aL PV KING/ Huntersville,NC 28078
[phone]
I
ANALYTICAL RESULTS
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method:EPA 625 Preparation Method:EPA 625
Surrogates
Nitrobenzene-d5(S) 52 % 10-120 1 01/20/15 14:00 01/22/15 01:08 4165-60-0
2-Fluorobiphenyl(S) 47 % 15-120 1 01/20/15 14:00 01/22/15 01:08 321-60-8
Terphenyl-d14(S) 60 % 11-131 1 01/20/15 14:00 01/22/15 01:08 1718-51-0
Phenol-d6(S) 10 % 10-120 1 01/20/15 14:00 01/22/15 01:08 13127-88-3
2-Fluorophenol(S) 15 % 10-120 1 01/20/15 14:00 01/22/15 01:08 367-12-4
2,4,6-Tribromophenol(S) 32 % 10-137 1 01/20/15 14:00 01/22/15 01:08 118-79-6
624 Volatile Organics Analytical Method:EPA 624
Acrolein ND ug/L 5.0 1 01/17/15 08:15 107-02-8
Acrylonitrile ND ug/L 50.0 1 01/17/15 08:15 107-13-1
Benzene ND ug/L 2.0 1 01/17/15 08:15 71-43-2
Bromodichloromethane ND ug/L 2.0 1 01/17/15 08:15 75-27-4
Bromoforrn ND ug/L 2.0 1 01/17/15 08:15 75-25-2
Bromomethane ND ug/L 2.0 1 01/17/15 08:15 74-83-9
Carbon tetrachbride ND ug/L 2.0 1 01/17/15 08:15 56-23-5
Chlorobenzene ND ug/L 2.0 1 01/17/15 08:15 108-90-7
Chloroethane ND ug/L 2.0 1 01/17/15 08:15 75-00-3
2-Chloroethylvinyl ether ND ug/L 5.0 1 01/17/15 08:15 110-75-8
Chloroform ND ug/L 2.0 1 01/17/15 08:15 67-66-3
Chloromethane ND ug/L 2.0 1 01/17/15 08:15 74-87-3
o Dibromochloromethane ND ug/L 2.0 1 01/17/15 08:15 124-48-1
Dichlorodifluoromethane ND ug/L 2.0 1 01/17/15 08:15 75-71-8
1,1-Dichloroethane ND ug/L 2.0 1 01/17/15 08:15 75-34-3
1,2-Dichloroethane ND ug/L 2.0 1 01/17/15 08:15 107-06-2
1,1-Dichloroethene ND ug/L 2.0 1 01/17/15 08:15 75-35-4
trans-1,2-Dichloroethene ND ug/L 2.0 1 01/17/15 08:15 156-60-5
1,2-Dichloropropane ND ug/L 2.0 1 01/17/15 08:15 78-87-5
cis-1,3-Dichloropropene ND ug/L 2.0 1 01/17/15 08:15 10061-01-5
Ethylbenzene ND ug/L 2.0 1 01/17/15 08:15 100-41-4
Methylene Chloride ND ug/L 2.0 1 01/17/15 08:15 75-09-2
1,1,2,2-Tetrachloroethane ND ug/L 2.0 1 01/17/15 08:15 79-34-5
Tetrachloroethene ND ug/L 2.0 1 01/17/15 08:15 127-18-4
Toluene ND ug/L 2.0 1 01/17/15 08:15 108-88-3
1,1,1-Trichloroethane ND ug/L 2.0 1 01/17/15 08:15 71-55-6
1,1,2-Trichloroethane ND ug/L 2.0 1 01/17/15 08:15 79-00-5
Trichloroethene ND ug/L 2.0 1 01/17/15 08:15 79-01-6
Trichlorofluoromethane ND ug/L 2.0 1 01/17/15 08:15 75-69-4
Vinyl chloride ND ug/L 2.0 1 01/17/15 08:15 75-01-4
Surrogates
4-Bromofluorobenzene(S) 97 % 70-130 1 01/17/15 08:15 460-00-4
Toluene-d8(S) 92 % 70-130 1 01/17/15 08:15 2037-26-5
1,2-Dichloroethane-d4(S) 101 % 70-130 1 01/17/15 08:15 17060-07-0
MBIO 9222D Fecal Coliform CHT Analytical Method:SM 9222D
Fecal Coliforms ND CFU/100 mL 1.0 1 01/14/15 14:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:02/13/2015 03:34 PM without the written consent of Pace Analytical Services,Inc.. Page 8 of 56

Pace Analytical Services,Inc.
•
CeAnalybcal 9800 KinceyAve. Suite 100
Huntersville,NC 28078
mowpocalabs.com [phone]
ANALYTICAL RESULTS
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method:SM 2540D
Total Suspended Solids ND mg/L 2.9 1 01/21/15 03:31
4500CL G Chlorine,Residual Analytical Method:SM 4500-Cl G
Chlorine,Total Residual 0.11 mg/L 0.024 1 01/16/15 11:00 7782-50-5 H1
4500S2D Sulfide Water Analytical Method:SM 4500-S2D
Sulfide ND mg/L 0.10 1 01/15/15 10:30 18496-25-8
52108 BOD,5 day Analytical Method:SM 5210B
BOD,5 day ND mg/L 2.0 1 01/15/15 05:57 01/20/15 06:51
Total Organic Nitrogen Calc. Analytical Method:TKN-NH3 Calculation
Total Organic Nitrogen ND mg/L 0.50 1 02/04/15 17:36
300.0 IC Anions 28 Days Analytical Method:EPA 300.0
Bromide 0.81 mg/L 0.20 2 01/21/15 04:36 24959-67-9
Fluoride ND mg/L 0.50 1 01/17/15 05:37 16984-48-8
Sulfate 342 mg/L 20.0 10 01/17/15 11:49 14808-79-8
350.1 Ammonia Analytical Method:EPA 350.1
Nitrogen,Ammonia ND mg/L 0.10 1 01/27/15 20:08 7664-41-7
351.2 Total Kjeldahl Nitrogen Analytical Method:EPA 351.2
Nitrogen,Kjeldahl,Total ND mg/L 0.50 1 01/30/15 15:05 7727-37-9 M1
353.2 Nitrogen,NO2/NO3 pres. Analytical Method:EPA 353.2
Nitrogen,NO2 plus NO3 ND mg/L 0.020 1 01/30/15 18:31
365.1 Phosphorus,Total Analytical Method:EPA 365.1
Phosphorus ND mg/L 0.050 1 01/28/15 17:02 7723-14-0
420.4 Phenolics,Total Analytical Method:EPA 420.4 5 AVOW
Phenol ND mg/L 0.010 1 .w.n3lar 01/29/15 15:48 108-95-2
4500CNE Cyanide,Total Analytical Method:SM 4500-CN-E
Cyanide ND mg/L 0.0080 1 01/26/15 14:48 57-12-5
5220D COD Analytical Method:SM 5220D
Chemical Oxygen Demand 30.0 mg/L 25.0 1 01/15/15 14:20
5310B TOC Analytical Method:SM 5310B
Total Organic Carbon 3.7 mg/L 1.0 1 01/16/15 13:57 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:02/13/2015 03:34 PM without the written consent of Pace Analytical Services,Inc.. Page 9 of 56

Pace Analytical Services,Inc.
• 9800 Kincey Ave. Suite 100
aceAnalytical Huntersville,NC 28078
sww.pacxlabs.twm [phone]
ANALYTICAL RESULTS-RADIOCHEMISTRY
Project: NPDES Renew 2015
Pace Project No.: 92233379
Sample: 001 Lab ID: 92233379001 Collected: 01/14/15 10:00 Received: 01/14/15 13:25 Matrix:Water
PWS: Site ID: Sample Type:
Parameters Method Act±Unc(MDC)Carr Trac Units Analyzed CAS No. Qual
Gross Alpha EPA 900.0 7.64 t 2.41 (2.69) pCi/L 01/27/15 21:32 12587-46-1
C:NA T:NA
Gross Beta EPA 900.0 628 t 1.47 (1.29) pCi/L 01/27/15 21:32 12587-47-2
C:NA TTNA
Radium-226 EPA 903.1 0.0627 t 0.325 (0.675) pCi/L 02/03/15 11:18 13982-63-3
C:NA 7:86%
Radium-228 EPA 904.0 0.244 t 0.405 (0.882) pCi/L 01/30/15 16:07 15262-20-1
C:89%T:61%
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,Inc.. Page 43 of 56

Analytical Results
—1411111-
Pace Analytical 1
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date: 01/15/2015 STATESVILLE
Reported: 02/04/2015 1 N i` TIC A T
For: 9223379 A Aj.,T 1 AL
Comments:
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
150115-12-01 MBAS 001 0.17 mg/L SM5540C-2000 01/15/2015 MD
Respectfully submitted,
v`✓ZA.JTh4,
Dena Myers
NC Cert#440,
NCDW Cert#37755,
EPA#NC00909
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 rage 55 of 56

Analytical Environmental Services,Inc Date: 19-Feb-15
Client: Pace Analytical Services,Inc. Client Sample ID: 001
Project Name: 92238054 Collection Date: 2/18/2015 9:02:00 AM
Lab ID: 1502G20-001 Matrix: Aqueous
Analyses Result Reporting Dilution
Qual Units BatchlD Date Analyzed Analyst
Limit Factor
Sulfite by SM4500-S03-B
Sulfite BRL 2.00 H mg/L R286188 1 02/19/2015 15:30 OM
Qualifiers: • Value exceeds maximum contaminant level E Estimated(value above quantitation range)
BRL Below reporting limit S Spike Recovery outside limits due to matnx
H l folding times for preparation or analysis exceeded Nan- See case narrative
N Analyte not NELAC certified NC Not confirmed
B Analyte detected in the associated method blank < Less than Result value
> Greater than Result value .1 Estimated value detected below Reporting Limit
Page 13 of 15
4 of 6

Condition of Receipt
Sample Number 150115-12-01 Temp on Arrival: 2
Parameter Schedule: MBAS
Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 rage 56 of 56

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