NC0004774_Request to Repurpose Outfall 001_20161110

DUKE
14 ENERGY®
November 10, 2016
Mr. Jeffrey Poupart
Water Permitting Section Chief
Division of Water Resources
North Carolina Department of Environmental Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
Subject: Request to Repurpose Outfall 001
Duke Energy Carolinas, LLC.
Buck Combined Cycle and Buck Steam Station (Buck)
Permit #: NC0004774
Rowan County
Dear Mr. Poupart,
Richard E. Baker Jr., P.E., PMP
Director, EHS CCP Environmental Programs
Mail Code: EC13K
Duke Energy
526 South Church Street
Charlotte, NC 28202
NOV 15 2016
Water Quality
Permitting Section
On August 31, 2016, Duke Energy Carolinas (Duke) submitted to NCDEQ an update to the subject NPDES permit
application. As part of that application submittal, Duke requested that flows from the combined cycle wastewater
sump be permitted to discharge through outfall 001. As discussed, in an attempt to dewater the Ash Basins as
quickly and efficiently as possible to mitigate any seepage, Duke is planning to reroute a Buck's combined cycle
wastewater sump away from the Ash Basins and to discharge this water adjacent to the existing outfall 001 (see
Attachment 1). The coordinates for this location are 35.71384, -80.37539. Wastewater handled through the
combined cycle sump includes cooling tower blowdown, treated oil/water separator effluent, reverse osmosis reject
water, and treated sanitary waste effluent. Water analysis for the Buck combined cycle wastewater sump is
available in the recently submitted NPDES permit renewal application dated February 26, 2016 and is included as
Attachment 2. Currently the cooling tower blowdown line discharging into the Buck combined cycle wastewater
sump is chlorinated. The cooling tower blowdown can be treated with a sodium bisulfite system prior to discharge of
Buck combined cycle wastewater to outfall 001.
As a result of expected NPDES permit timing and to facilitate ash basin closure activities, Duke is requesting
authorization to proceed with the relocation of the wastestream to the outfall location as described in the February
26, 2016 renewal application while the NPDES permit renewal process continues. This change would not create
any new wastestreams but would more accurately be described as a relocation of an existing wastestream already
being released to the Yadkin River.
Should you have any questions regarding this submittal or require additional information, please contact Ross
Hartfield at 980-373-6583 or at [e-mail].
Sincerely, 1f
",k
Richard E. Baker Jr.
Director, EHS-CCP Environmental Programs
Duke Energy cc: Ross Hartfield, Dale Wooten, Tom Leap
NCDEQ cc: Mike Templeton
Attachments

Attachment 1

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Attachment 2

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of
EPA 1. D. NUMBER (copy from Item 1 of Farm t)
this information on separate sheets (use the same format) instead of completing these pages.
EPA Faairty Name.
SEE INSTRUCTIONS
NC0004774
Buck SS i CC
OUTFALL NO.
V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C) CC Wastewater Sump
ART A - You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
2. EFFLUENT
3. UNITS
4. INTAKE (optional)
1. POLLUTANT
a. MAXIMUM DAILY VALUE
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVG. VALUE
a. LONG TERM AVG. VALUE
(d available)
(f ovaaable)
d. NO. OF
a Concen-
b Mass
b. NO. OF
(1) Concentration
(2) Masa
(1) concentration
(2) Mass
(1) Conc ntrauon
(2) Mass
ANALYSES
tration
(1) comentratlon
(2) Moss
ANALYSES
i. Biochemical Oxygen
4.3
c 3.1
< 46.6
3
mgA
Ib/Day
3emand (SOD)
Chemical Oxygen
_j 60
46
6910
3
mgA
Itt/Day
mend (COD)
Total Organic
1 21
1933
290 4
3
mgn
lboay
rbon (TOC)
Tolalstrspoonded
75.1
3 _
mgA
WDay
ka (ras)
Arnmonta (as N)
0.28
0.189
2.8
3
mgA
Ib/Day
Flow
VALUE
VALUE
VALUE
upper
VALUE
I 1.8
estimate
MGD
NIA
. Temporahrre
VALUE
VALUE
VALUE
VALUE
wider)
14.2
ass'=;t
7=-12,93
3
DEGREES CELSIUS
--
Temperature
VALUE
VALUE
VALUE_
VALUE
aummer)
- -
;r'w',i;"r
___--__
_
_
DEGREES CELSIUS
- -
pH
MINIMUM
MAXIMUM
MINIMUM
MAXIMUM
8.28
8;4
= "-_"
z='`
1 3
STANDARD UNITS
ART B - Mark "X" in column 2a for each pollutant you know or have reason to believe is present. Mark "X" in column 2b for each pollutant you believe to be absent. If you mark column 2a for any
pollutant which is limited either directly or indirectly but expressly In an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants
for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions
for additional details and requirements.
1. POLLUTANT
2 MARK'X" 3. EFFLUENT
4. UNITS
5. INTAKE (optional)
D CAS NO.
Behaved a. MAXIMUM DAILY VALUE b, MAXIMUM 30 DAY VALUE c. LONG TERM AVG. VALUE
a, LONGTERM AVG. VALUE
Ir avadable)
o.pre- b.ab- (if available) (lavoilable)
d. NO. OF
a. Concen-
b. Mass
b. NO. OF
sent
sent (1) Concentration (2)Mass (1) Concentration (2)Mass (1)Concentration
(2)Mass
(1) Ccncerdratlon
a)Mass
ANALYSES
tration
ANALYSES
a.B omWe
X
< < 0-50 < 06
--
< 7.5
3
mgA
Ib/Day
4ti58b7-9)
Ohlomro,
X
') 220 1.9
28.5
3'
mgA
Ib/Day
I
alai Residual
Color
X
15 00 N/A N/A 1333
NIA
3
Std. Units
NIA
_j
NIA
J. Focal
Xf
102.00 N/A NIA < 35.67
NIA
3
Colonies
NfA
NIA
da"
1100 ml
X
j 0,55 0.53
8.0
3
mgA
Ib1Day
- j
69a64")
l.ibiFluoride
Nitrate.
X
9.900 8.33
125.1
3
mgA
Ib/Day
j
nto (as N)
EPA Form 3510-M (Rev 2.85) PAGE V-1 CONTINUE ON PAGE V-2

EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUEDITEM V-13
POLLUTANT
2. MARK'X'
(options
D CAS NO.
Sebavved a. MAXIMUM DAILY VALUE
b. MAXIMUM 30 DAY VALUE c. LONG TERM AVG. VALUE
a. LONG TERM AVG. VALUE
favaaabla)
apre- b.ab
(danitable) (favadable)
d. NO. OF
a. Concen-
b Mass
b. NO. OF
tration
ANALYSES
seM
card (1) Concentration
(2) Mass
(1) Cowardiation
(2) Mau (1) Concertation
(2) Mass
ANALYSES
(1) Concentration
(2) Maas
. Ndfogan,
oraI Organic
X
— 2.109
2044
307
3
mgA
Ib/Day
es N)
i. W and
X
5.00
< 5
< 75.1
3
mgA
fb/Day
. Phoaphorous
as P), Total
X
^.I 3,170
2.67
40,1
3
mgA
Ib/DayKao
j
m3-u.o)
loa 1v
1) Alpha,
Total
Xa
° 5.00
WA
WA
< 5
WA
3
pClll
WA
NIA
Beta,
Total
X
— { 26.80
N/A
WA
23.47
NIA
3
PCVI
WA
N/A
3) Radium,
"Orel
X
1,00
WA
WA
< 1N/A
3
pCUi
WA
N/A
4) Radium
Total
X
1.Oo
WA
WA
< 1
WA
3
pCIA
WA
NIA
sr4 to
as SO4)
X
140.00
133.33
2002.7
3
mgA
Ib/Day-
148W78-8)
. WHO
es s)
X
1.00
< 1
< 15.0
3
mgA
Ib/Day
n. sulfas
ASS03)
X
<.; 2 DO
< 2
< 30.0
3
mgA
Ib/Day
--,1
1-32-5-5-5-5•-3)
9urfaetards
X
r, 0.140
0108
1.6
3
mgA
Ib/Day
V�
. Atumimrm,
otal
X
020
0.177
27
3
mgA
Ib/Day
7428-30-s)
. Barwm.
oral
X
— 0.14!3
0.141
21
3
mgA
lb/Day
1,
74-3039.3)
Born,
ofal
X
_s} 0.253
0.236
36
3
mgA
lb/Day
7440.42.8)
. COW,
"Otal
X
—<; 0.001
< 0 001
- < 0.0
3
mgA
IbfDay
7446A&4)
tmn, Total
439408)
X
i 0.334
0.307
4.6
3
mgA
Ib/Day
. Magn4alum,
atm
439.95-4)
X
1970.
18.73
281.3
3
mgA
Ib/Day
i. 0 amen,
"Olaf
X
Y) 0.00764
0.00579
0.1
3
mgA
Ib/Day
7439-90-7)
. Mangamw.
0181
X
0.005
< 0.005
< 0.1
3
mgn
Ib/Day
—`
7439.88-5)
w.'nn, Total
440-31-5)
X�<]
0.01
< 0.01
< 0.2
3
mgA
Ib/Day
Tdanntm,
Wal
Xf
0.006
< 0.005
< 01
3
mgA
Ib/Day

EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C NC0004774 CC Wastewater Sump
Suck SS / CC
PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in
column 2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries,
nonprocess wastewater outfalls, and nonrequired GC/MS fractions), mark "X" in column 2-b for each pollutant you know or have reason to behave Is present. Mark "X" in column 2-c for each
pollutant you believe is absent. If you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you
must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. If you mark column 2b for
acrolein, acrylonitrile, 2, 4 dinitrophenol, or 2-methyl-4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason to
believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the
reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions
for additional details and requirements.
1. POLLUTANT
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE o tionaq
D CAS NO.
aso eewvod
a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE c. LONG TERM AVG. VALUE
a. LONG TERM AVG. VALUE
r available)
quir- Ebro- coo-
(d available) I (d ovodablo)
d. NO. OF
a. Canton-
b Mass
d. NO. OF
ad sent Bart
(t) CarreeNraban R) Mase (1) CMaertuoUon (2) Mase (1) Coneerarabn (2) Mase
ANA'LYSES
ir0t10n
(1) Concuxtratbn (2) Mass
JANALYSES
METALS. CYANIDE,
AND TOTAL
PHENOLS
M. AManony,
X
1 10.7
1043
0.16
3
ug/l
Ib/Day
_ i
oat (744039-0)
M Arserdcjotar
X
0.02
3
ugh
Ib/Day
7440-38.2)
M. Beryllium.
X
< l 1
< 1
< 0.02
3
ugh
Ib/Day
Total (744041-7)
M. Cadmium.
X
< j 0,1
< 01
< 0.00
3
ugh
Ib/Day
Jr
sal (7440436)
M Chromium,
X
L 1.41
1.23
0.02
3
ugh
Ibn)ay
!
sal (744047.3)
Copper, Taal
X
e 0.01
0.008
0.12
3
mgA
Ib/Day
144D-50-8
M. Lead, Taal
X
< f 1
< 1
< 0.02
3
ugh
Ib/Day
_
743392-1)
. Mbrcury, Total
X
f 0.013
0.0125
0.00
3
ugh
lb/Day
7439-07-e)
M. Nkkol, TMI
X
5.18
4.73
0.07
3
ugn
Ib/Day
j
440t2-0)
em. selenium.
X
1
< 1
< 0-02
3
ugh
ib/Day
Total (7782-49.2)
1M slim, Taal
X
f 1
< t
< 0.02
3
ugh
Ib/Day
{
7440.224)
2M. Thstilurn.
Xc
1 0.0002
< 0.0002
< 0.0
3
mgA
ItifDay
_
Total (7440.28-0)
3M. Zinc. Taal
X
yj 0,014
0 013
0.20
3
mgA
Ib/Day
7440886)
4M. Cyanide.
X
) 0.083
< 0 029
< 0.44
3
mgA
Iti/Day
r f
Total (57.125)
5M. Phar$,
X
_ _ i 0.083
0 043
0.6
3
mgA
Ib/Day
- f
aal
I
IOXIN
,3,7,6 TetraDESCRIBE RESULTS
hbrod6enza P X
' xin (1784-01.8)
EPA Form 351044 (Rev. 265) PAGE V-3 - _-- - _ CONTINUE ON PAGE V4

NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-3 NCOM4774 CC Wastewater Sump
r7-
Buck SS I CC
1. POLLUTANT
2 MARK"X" 3. EFFLUENT
4. UNITS
5. INTAKE option
D CAS NO.
a.re•
Believed a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE c. LONG TERM AVG. VALUE
a. LONG TERM AVG. VALUE
auva@ab$e)
quir.
b pro- cxtb- (davallable) (tavaaable)
Id. NO. OF
Ia. Conten-
lb. Mass
I
d. NO. OF
sera
surd (1)Concardratlon 1(2) mass (t)concergreuon 1(2) mass Imconcerdratim (2)Me--
(1)Caneerdrotion (27".
ed
ANALYSES
tration
ANALYSES
CIMS FRACTION - VOLATILE
COMPOUNDS
V Acrotein
X
�); 5
c 5
< 0.08
3
ugA
Ib/Day
___;
10702-0)
. Acrylonnr e
X
<• 5
< 5
< 0.08
3
ugn
IbfDay
I
107.13.7)
'
. Bereene
X
` 2
< 2
< 0.03
3
ugn
Ib/Day
71.43-2)
V. &e (Chloro.
ethyl) Ether
X
542-000-t
eramf=
X
< j 2
< 2
< 0.03
:3
ugn
lb/Day
5.25-2)
.carbon
etradaoride
X
2
< 2
< 003
3
ugA
Ib/Day
5&2361
Chsomberaeno
X
< j 2
< 2
< 0.03
3
ugn
Ib/Day
105.WT)
W. Chbrod4
momethane
X
e_i 2
< 2
c 0.03
3
ugn
Ib/Day
7
124-48-1)
Chloroethane
75-003)
X
c 5- 2
c 2
< 0.03
3
Ugn
Ib/Day
^f
OV. 2-Chloro-
tryyvinyt Ether
X
c l 5
e 5
< 0.08
3
ugA
Ib/Day
tto•75-8)
1V. Chlorol6rnr
X
_i, 35
19 223
0.29
3
ugA
IblDay
1
87.88.3)
2V. Dieldo
romemethane
X
.. 2
< 2
c 0.03
3
ugn
Ib/Day
7527-0)
3V. Nchloro
atuoromettane
X
2
< 2
< 0.03
3
ugn
Ib/Day
571-0)
4V.tA-DzWoro-
X
cj 2
< 2
< 0.03
3
ugA
lb/Day
Kano (7534.3)
SV 1,24)zh4oro-
X
Yj 2 -
< 2
< 0.03
3
ugn
Ibn)ay
+
barn (107-0&2
ev. t,t•otchloro.
X
�< 2
< 2
< 0.03
3
ugn
IblDay
lhylone (75354)
7V. 1,24DRxtdoro-
X<„�
2
< 2
< 0.03
3
ugn
Ib/Day
Dana (7"75)
r
SV. i,3•DWc1ftro-
X
a 2
c 2
< 0.03
3
ugn
Ib/Day
T
42.75 9)
ereene
X
2
< 2
< 0.03
3
ugA
WDay
j
F(74-87-3)
X
� 2
c 2
< 0.03
3
ugn
IbyDay.83.9)l
X
< 2
< 2
< 0.03
3-073)
ug4
ItuDay
_J
LPA Fane 3blWC (RSV. Z-05) PAGE V4 CONTINUE ON PAGE V•5

EPA Forth 351620 (Rev, 265) PAGE V-5 CONTINUE ON PAGE V-6
EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-4
NC0004774 CC Wastewater Sump
Buck SS / CC
1. POLLUTANT
2. MARK X & EFFLUENT
4. UNITS
INTAKE (options
D CAS NO.
e.roBeloved
Ia. MAXIMUM DAILY VALUE lb. MAXIMUM 30 DAY VALUE c. LONG TERM AVG. VALUE
a. LONG TERM AVG. VALUE
devabW)
rruu•
bpro- c.etr (II.Mebls) 0favaDahla)
d, NO. OF
a Concen-
lb. Mass
d. NO. OF
ed
ANALYSES
tration
ANALYSES
send
sent (7) concemmuon
(2) Maws (1) Concordrawn (2) mass (1) comentrauon (2) Mass
1) Comardraton (2) Mass
GCIMS FRACTION
- VOLATILE
COMPOUNDS continue
Mathyora
X
< j 2
< 2
c 0.03
3
ugn
IbMay
_a
roe (7549.2)
1,1,2.2-Tetre-
Woroeurene
79345)
X
j 2
< 2
< 003
3
ugA
IWDay
4V. Teaaddoro-
X
< J 2
< 2
< 0.03
3
ugA
Ib/Day
hybne (127-18-4)
.Toluene
X
c j 2
< 2
< 0,03
3
ugA
Ib/Day
10&883)
1,2-Trans.
Iryone
X
2
< 2
< 003
3
ugA
ItVDay
156665)
7V, 1,1,1 Td-
hbrootham
X<
2
< 2
< 0.03
3
ugA
ID/Day
71558)
. 1,1,2-Td-
hloroethsne
78-0651
X
2
2
c 0.03
3
ugA
0)/Day
Tmhoro-
X
<; 2
< 2
c 0.03
3
ugA
Ib/Day
j
hyom 170-016)
Tnchbro-
mnxthano
7589-{)
X
< } 2
< 2
< 0.03
3
ugA
Ib/Day
j
IV. viv
X
c�j 2
< 2
< 0.03
3
ugA
Ib/Day
'de (75414)
CIMS FRACTION - ACID COMPOUNDS
A.2•Chloropheno!
X<
[ 10
< 10
< 0.15
3
ugA
IbMay—
76)
2,4.Dchicro.
X
10
< 10
a 0.15
3
ugA
Ib/Day
henol(120.63.2)
. 2.4-0MVIlryl-
x
_ <j 10
< 10
< 015
3
ugA
Ib/Day
(10587.9)
.4,64)htro-0
X
< j 10
< 10
< 015
3
ugA
lb/Day
1(53482-1)
2,4-Dntre-
X
50
< 50
< 0.75
3 _
ugA
Ib/Day
nal (51.285)
2-N"henot
X
E 10
< 10
< 0.15
3_
ugA
Ib/Day
6&755)
A. 4Nftpheml
X
c;j 10
< 10
< 0.15
3
ugA
Ib/Day-
10602-7)
P-cftru-•
X
i 10
< 10
< 015
3
ugA
Ib/Day
I (59567)
Pem eddoro-
X
< 1 10
< 10
< 0.15
3
ugA
Ib/Day
banW (67-0&5)
OA. Phonal
X
_< 10
< 10
< 0.15
3
ugA
IbMay
L!
10885.2)
2,4,64d-
1A,2.4,64d,
tmwheml
topheml
X
J 10
< 10
< 015
3
ugA
Ib/Day
6&0&2)
EPA Forth 351620 (Rev, 265) PAGE V-5 CONTINUE ON PAGE V-6

EPA I.D. NUMBER (copy from Item 1 of Form 1)OUTFALL NUMBER
CONTINUED FROM PAGE V-5 I NC0004774 C Wastewater Sum Buck SS I CC
1. POLLUTANT
2.M ARK
"X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
AND S NO.
a.re-
ae9Oved
a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVG. VALUE
a. LONG TERM AVG. VALUE
la
�(,f�aaio.tA)
prcr-
(d rmlilablo)
(f available)
d. NO. OF
a. Concert-
b. Mass
�d.
NO. OF
b pre-
e.eb
ee
sem
sem
ANALYSES
trebon
ANALYSES
(1)lconcrmhation R)Maao (1)Cwxemration (2)Masa
(I)COncentrauon (2)Ma5a
o)Comenhetion (2)Mass
GC/MS FRACTION
- BASE
NEUTRAL
COMPOUNDS
e. neonepmhane
X
.4isi
ugn
IwDay
e3a2s
B 'Awneptoylene
X
ugn
IwDay
8. Arahrecerre
X
" "
ugn
Ib/Day
-
-
12a12-7)
B. Berkidhw
X
;� ,
ugn
IblDay
; _
-
$7-5)
a. BMW (a)
races
)
x
�'"-.` _
ugn
It1/oay
-
H. Berko (a)
X
ug/I
Ib/Day
B. 3,4-Bomo-
ranarene
X`._
`
-
ugA
Ib/Day
- }
-
2)
a. aanto (glu)
x
ug/I
Ib/Day
eryrerm (101.242)
B. Berko (1)
ntheno
X
_
ugn
Ib/Day
7 0B 9)
-
OB. Bis (2{Mem•
hoayl) Methane
X
ugA
Ib/Day
111.01-1)
-
IB. We (2-Chlom-
h)A) Ether
X
k
ug/l
lb/Day
"
111444)
28 am (2LhWmeo-
pyo Ether
X
�•'�'�
%c R
ug/I
(b/Day
1081)
3B. 5,3 (Z•Etlo
xyq Phthalate
xd
; ,€.
ug/I
M/Day
1-7)
4aromO-
PharrA
x
ugA
Ib/Day
(101-55.3)ButA
L
Bent9A
x
r,,-, .
ugn
Ib/Daylate
(RFS -7)
.2Ltdom-
phumlaw
x
ug/I
Ib/Day
$
91.sa.n
78.4Chbto-
hergt Phanyl
X
ug/I
1b/Day
then (7005-72J)
88. Chtysene
X
"ca_ -
ugll
lb/Day
218-01-8)
08. DWnto (ash)
re
X
U911Ib/Day
53-7b3)
8.1,2-C(ohloro-
are
X
ugA
lb/Day-
-
m (9550-a
d
1e.1.3.OxMo+o-
X
ugA
Ib/Day-
mana (541-731)
I
EPA Form 3510.20 (Rev. 245) PAGE V-6 CONTINUE ON PAGE V•7

EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-6 I INt;0004 / /4 GL: Wastewater Sumo tfUCK US / GG
1. POLLUTANT
2. MARK W
3. EFFLUENT 4. UNITS
5. INTAKE options
D CAS NO.
ZZBe
wed
a. Y 30
c. R
a. L G.
III)
d avedable)
qUk•
(Mavailabte)
(f ava'dabte) _
d. NO. OF a. Concen-
b. Mass
d. NO. OF
b.pre-
c.ob-
od
sent '
sent
ANALYSES tre(ron
ANALYSES
(1) ConceMraron
R) Maas (1)Conwrdnl on (2) Masa
(1)CanaeFmaaon (2) Masa
Concenvet on (2) Maas
CIMS FRACTION - BASEINEUTRAL
COMPOUNDS
continued
B. 1.4.Oton)mo.
x
ugn
Ib/Day-
nzene (10640.7)
B. 3.3-MMoro-
rKidlne
X
`,` - , -
- -, _
UgA
Ib/Day
t84 -t)
48, Do"
'
taro
x
ugA
IbMay
B, o(matrM
We
X
p
tea,
ugA
Ib/Day
131.11.3)
. D4N-em)9
tate
x
:.,
Ugn
III/Day
84.74.2)
7B.2.4-DNbo-
X
tom' 1--: - -
, ' -.
ugA
M/Day
stuene(121.14.2)
88.2,60Hra.
X
_
ugA
9A)ay--
auene (696-202)
B. MN•Octyl
"
tan
X
ugA
Ib/Day
-
41784-0) -
. 1.2-aPbanyt-
rezlne (es Ileo-
X7
-
Ugh
IbMay
- -
- -
eno) (122-0¢.7)
18. FkWardheno
X
-
ugA
IbMay
8. Fwans
X
,_ .
ugA
@/Day
' s
0&73•
e Hexeddoro•
X
ugn
Ib/Day
(. ;
neat (118-74.1)
_
S. Man.
bbrabutedlene
X
U901Ib/Day
—
—
67-wa)
8. Hexaddaro•
-
- -
pmaadtena
X
8 ,
ugA
Ib/Day-
77.47.4)
. Hex"Horo•
-
X°_
e
"
_ _
_
ugn
Ib/Day
_
no (e7-72.1)
-.
78. Warta
.
d) P
1.2.3-cd)yrone
X
,',a' °1. '- - .
_
ugA
Ib/Day
- - - -
-
19388.5)
e.lscowane
X°-
. ".,
ugn
III/Day
1)
S. Naphomlene
X
,) % -_ -
_ ..' _
UgA
IbA)ay"
-.
91.26-3)
Ndrobenzene
80.err3)
X
. .., .^�_-.
-
- . ,
Ugn
IWDay
,-_
-
19. N-Ndm-
o wdyarnme
X
ug/1
Ib/Day
82-759)
28. NAftosodl•
•Propytamina
X
, ` _
ugA
Ib1Day
-
62184.7y
EPA farm 3S10 -2C (Rev. 285) PAGE V-7 CONTINUE ON PAGE V8

EPA I.D. NUMBER (copy from item I of Form 1) OUTFALL NUMBER
1117INTIll FRnm PAGE V-7 NC0004774 CC Wastewater Sumo Buck SS I CC
1. POLLUTANT 2. MARK "X" 3. EFFLUENT
4. U FrS S. INTAKE (optional
ANDCAS NO. a.re- I
ll a. MAXIMUM DAILY VALUE b. MAXIMUM 30 -DAY VALUE LONG TERM AVG. VALUE
I
Ia. LONG TERM AVG. VALUE
(if avalaw) q*-
]c.
(if evagam) (it evagable) Id.
NO. OF
a. Conten-
'n
1). Mass
I
d, NO. OF
Isent lbent
Imcoricertl
(2) Masa lo) cor"Mingon 1(2) M053 I(I)CoMeMration 1(2) Ill
"ll
ANAL—RES
tration
j(1)C0W0rMMn j(2)ll
ANALYSE S
GC/MS FRACTION
- BASEINEUTRAL
COMPOUNDS(continued)
B. M-Nftra.
tpherrytemins
X
U911
Ill
B. Pill
X
U911
IbIll
8501.81
Pyrene
X
u9A
Ib/Day
I
.1.2,446.
mbenrane
X
u 9A
lb/Day
1)
S FRACTION - PESTICIDES
Aldrin
x
30&00.2)
P. aWw4BHC
X
31904 0)
. beta -BHC
X
1585-7)
P.gamma-0Hc
X
deft -Ill
X
31908.0)
-
Chill
X
57-748)
X
89293)
4,W430E
X
.4.N -DDD
X
72,14-8)
OP. ll
X
lRelptia-Erdasullan
_X
!15-20-7)
:2P. beta-EndoWfar,
x
KIIS-2D-7)
3P. Endosuffen
Wars
X
1031.07-8)
4P. Endrin
X
SP. Endrin
Well
7121934)
lop. HaphWiftr
X
704")
EPA ram 3510-2C Ill 245) PAGE V-8 CONTINUE ON PAGE V9

EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
MnRITrr n ren conga oer:e v -a I NCrKW77A CC Wastewater Sumn Buck SS f CC
t. POLLUTANT Z MARK "X" 3. EFFLUENT
4. UNITS 5. INTAKE (optional)
AND CAS NO. am-
Bmekved a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE c. LONG TERM AVG. VALUE
a. LONG TERM AVG. VALUE
eve8aw) quu.
ed
b pro• a ea (if availow) Qt available)
d. NO. OF
JANALYSES
a. Cancan.
tration
b. Mass
(1)Corrrararetbn (;)Masa
d. NO. OF
ANALYSES
soot send (I)ConoewreWn R)Van (1)Cw=rdm6orr R1 Mass (t)coneer"Uan (2)Mass
CIMS FRACTION - PESTICIDES
continued
7P. xeptesldor
_
poxide
X
1024$73)
6P. PCB•1242
x
< 0.4
<
c 0.4
3
ago
Ib/Day
WS -21.a)
6P. PCB -1254
X
< 0.4
<
< 0.4
3
ugli
Ib/Day
1109740-1)
-1221
X
< 0.4
<
< 0.4
3
UgA
INDay
042&2)
PCB•1232
X
< 0.4
<
< 0.4
3
ugA
Ib/Day
PCB•1246
X
< 0.4
<
< 0A
3
ugn
Ib/Day
[12M4PCB
72-2BA)
PCB -126n
X
c 0.4
<
< OA
:3_
ugll
b0ay
am -S)
PC13
X
0.4
<
0.4
3
ugA
(b/Day
.11-2)
Toxephane
X
1352)
EPA form 3510.20 (Ref. 245) PAGE VA

EPA I.D. NUMBER (COPY from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-7 NC0004774 CC Wastewater Sump
Buck SS / CC
1. POLLUTANTL2.MARK
"X" 3. EFFLUENT
4. UNITS 5. INTAKE o 'one
D CAS N0.
eerbved a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE c. LONG TERM AVG. VALUEa.
LONG TERM AVG. VALUE
d evellable)
bpro- c.eb• Vavadaw) (favailable)
d. NO. OF
a. Concen.
b. Mass
d. NO. OF
sent
sem (1) CortceMration
) Masa (1) ComrftWn (2) Mass (1) Concenbetion (2) Masa
ANALYSES
tration
0) COMOntOlOn (2) Maas
ANALYSES
GC/MS FRACTION
- BASE/NEUTRAL
COMPOUNDS
continued
e. N•Nf ro-
owrrytemm
8830
X -(
_ _
ugA
IblDay
B Pha o d nro
X _
ugA
lb/Day
18)
Pyrene
X „� j -
-
ugA
Ib/Day
_
129000)
1,2,4Td-
lombenxene
X
ugA
lb/Day
12092-1)
CIMS FRACTION
- PESTICIDES
P. Alddn
X
30900-2)
P. etphe-BHC
X
tli84A)
P. bete -BHC
X
'
15-06-7)
P. gamma-0HC
X
56a99)
P. detto.BHC
X
31&0&8)
W. ChloWane
X
87-748)
P. 4.N-ODT
50.293)
X
_
4,4'-0DE
X
56-9)
.4.,V -DDD
. X
,
•5")
OP. Dieldrin
X
6037-1)
/PA%4w-Endosuffen
-X
11529.7)
2P. beta-ErMaaWfan
X
116-29.7)
3P.EndosuNen
-
-
Wtate
x
1031-07-8)
IP. Endrin
X
208)
SP. Endrin
enyds
X
4214)3 4)
OF. Ffaptectdor
X
-
EPA Form 351020 (Rev. 235) PAGE VA CONTINUE ON PAGE V•9