NC0003417_Updated 2C Data submittal_20150316

' �•� DUKE H.F.Lee Energy Complex
ENERGY® Duke Energy Progress
PROGRESS 1199 Black Jack Church Road
Goldsboro,NC 27530
March 11,2015
Mr. Jeff Poupart
North Carolina Division of Water Resources
1617 Mail Service Center
Raleigh, NC 27699-1617
RECEIVEDIDENRJDWR
Subject: Duke Energy Progress, Inc.
H.F. Lee Energy Complex MAR 1 6 2015
Updated Form 2C data submittal
NC0003417 Water Quality
Wayne County Permitting Section
Dear Mr. Poupart:
In response to the request from the North Carolina Division of Water Resources,please find attached an
updated EPA Form 2C for the H. F. Lee Energy Complex. The pending application for renewal of the
subject permit was made on November 20, 2012. An update to that application was submitted on October
31, 2014. A check for$1,030 is also enclosed.
There has been no discharge from outfall 001 (ash basin)since October, 2012. No wastewater flows are
being sent to the ash basin. Chemical characterization of the water remaining in the ash basin previously
requested by your office is being sent under separate cover. As such no 2C sample results are included.
There has been no discharge from outfall 002(cooling pond)since 1998. The discharge from outfall 002
in 1998 was associated with a tropical system. While there has been no discharge from outfall 002 since
1998, all wastewaters generated at the facility are currently directed to the sites 550+acre wastewater
cooling pond until treatment modifications associated with outfall 003 can be completed. Therefore,a
process control sample from the sites cooling pond taken in close proximity to outfall 002 is enclosed.
There has been no discharge from outfall 003 since January 2013. Outfall 003 first discharged in January
2013 but the discharge was discontinued after one month due to operational concerns with TSS. All
wastewaters generated at the facility are currently directed to the sites 550+acre cooling pond until
additional treatment evaluation and modifications can be completed for outfall 003. Since there is no
discharge from outfall 003,no sample results are included for this outfall.
If you have any questions,please contact Mr. Shannon Langley at(919)546-2439.
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or
persons who manage the system,or those persons directly responsible for gathering the information,the information submitted is, to the best of
my knowledge and belief true,accurate,and complete. I am aware that there are significant penalties for submitting false information,including
the possibility offines and imprisonment for knowing violations.
Sincerely,
Rick Grant—Plant Manager
H. F. Lee Energy Complex
Enclosure

EPA I.D.NUMBER(copy from Item I nj1•orm I) Form Approved.
N00003417 OMB No.2040-0086.
Please print or type in the unshaded areas only. Approval expires 3-31-98.
FORM U.S.ENVIRONMENTAL PROTECTION AGENCY
2C k/EPAEXISTING MANUFWASTEWATER
ACTURING,,COMMERC APPLICATION FOR PERMIT ALO,MINI GE GRAND SILVICULTURE OPERATIONS
NPDES Consolidated Permits Program
I.OUTFALL LOCATION
For each outfall,list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A.OUTFALL NUMBER B.LATITUDE C.LONGITUDE
(list) 1.DEG 2 MIN. 3.SEC. 1.DEG 2 MIN. 3.SEC. D.RECEIVING WATER(name)
001 35.00 22.00 45.30 78.00 4.00 6.46 Neuse River
002 35.00 22.00 51.74 78.00 5.00 5.93 Neuse River
003 35.00 22.00 1.74 78.00 4.00 59.59 Neuse River
II.FLOWS,SOURCES OF POLLUTION,AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility.Indicate sources of intake water,operations contributing wastewater to the effluent,and treatment units
labeled to correspond to the more detailed descriptions in Item B.Construct a water balance on the line drawing by showing average flows between intakes,operations,
treatment units,and outfalls.If a water balance cannot be determined(e.g.,for certain mining activities),provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall,provide a description of:(1)All operations contributing wastewater to the effluent,including process wastewater,sanitary wastewater,cooling water,
and storm water runoff; (2)The average flow contributed by each operation; and(3)The treatment received by the wastewater. Continue on additional sheets if
necessary.
1 OUT- 2.OPERATION(S)CONTRIBUTING FLOW 3.TREATMENT
FALL b.AVERAGE FLOW b.LIST CODES FROM
NO.(list) a.OPERATION(list) (include units) a.DESCRIPTION TABLE 2C-1
Ash pond Discharge Neutralization, sedimentation, nitrification
001 See attachment 3 2-K 4-A
(including low volume waste, plant submitted in October 2014 discharge to surface waters
1-U
drainage systems, water treatment 3-D
wastewaters, ash sluice water and
ash pond dewatering.
Condenser cooling water, septic tank Evaporation
002 See attachment 3 1-F 4-A
sand filter domestic wastewater submitted in October 2014 Discharge to surface waters
}LRSG Slowdown, combined cycle plant
wastewaters (including wastewaters
that can be directed to outfall 003)
Water purification process Gravity thickening, Filter press
003 See attachment 3 5-L 4-A
wastewaters, sump drainage, Neutralization 5-R S-q
submitted in October 2014
Wet surface air cooler blowdown
2-K
OFFICIAL USE ONLY(effluent guidelines sub-categories)
EPA Form 3510-2C(8-90) PAGE 1 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C.Except for storm runoff,leaks,or spills,are any of the discharges described in Items II-A or B intermittent or seasonal?
❑YES(complete the following table) ®NO(go to Section III)
3.FREQUENCY 4 FLOW
a DAYS PER B TOTAL VOLUME
2.OPERATION(s) WEEK b MONTHS a FLOW RATE(in mgd) (spec*wish wuo)
1 OUTFALL CONTRIBUTING FLOW (spear/t. PER YEAR 1 LONG TERM 2 MAXIMUM 1 LONG TERM 2 MAXIMUM C DURATION
NUMBER(lnt) (Mr) average) (spectry average) AVERAGE DAILY AVERAGE DAILY (`n T)
111.PRODUCTION
A.Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
❑YES(complete Item 111-B) ❑NO(go to Section 11)
B.Are the limitations in the applicable effluent guideline expressed in terms of production(or other measure of operation)?
❑YES(complete Item lII-(') ❑NO(go to Section IV)
C.If you answered"yes'to Item III-B,list the quantity which represents an actual measurement of your level of production,expressed in the terms and units used in the
applicable effluent guideline,and indicate the affected outfalls.
1.AVERAGE DAILY PRODUCTION 2.AFFECTED OUTFALLS
a.QUANTITY PER DAY b.UNITS OF MEASURE C.OPERATION,PRODUCT,MATERIAL,ETC. (list outfall numbers)
(spectfi)
RECEIVED/DENRIDWR
MAR 16 2015
Water Quality
Permitting Section
IV.IMPROVEMENTS
A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application?This includes,but is not limited to,
permit conditions,administrative or enforcement orders,enforcement compliance schedule letters,stipulations,court orders,and grant or loan conditions.
YES(complete the following table) ❑NO(go to Item 1V-B)
1 IDENTIFICATION OF CONDITION, 2.AFFECTED OUTFALLS 3.BRIEF DESCRIPTION OF PROJECT 4.FINAL COMPLIANCE DATE
AGREEMENT,ETC.
a.NO b.SOURCE OF DISCHARGE a.REQUIRED b.PROJECTED
North Carolina Coal Ash 001 ash sluice prohibition of CCR's in ash basin 10/1/2014 10/1/2014
Management Act of 2014
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs(or other environmental projects which may affect your
discharges)you now have underway or which you plan.Indicate whether each program is now underway or planned,and indicate your actual or planned schedules for
construction.
❑MARK'X"IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C(8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA I.D.NUMBER(copy from Item 1 of Form 1)
CONTINUED FROM PAGE 2 NC0003417
V INTAKE AND EFFLUENT CHARACTERISTICS
A,B.8 C See instructions before proceeding—Complete one set of tables for each outfall—Annotate the outfall number in the space provided
NOTE Tables V-A,V-B,and V-C are included on separate sheets numbered V-1 through V-9
D Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions.which you know or have reason to believe is discharged or may be discharged
from any outfall.For every pollutant you list,briefly describe the reasons you believe it to be present and report any analytical data in your possession.
1.POLLUTANT 2.SOURCE 1.POLLUTANT 2 SOURCE
Asbestos Used in insulation. Trace
amounts may be washed down
drains in plant areas during
maintenance.
Uranium Trace elements potentially
Vanadium present in coal
Zirconiuim -
Strontium
VI.POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS
Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct?
YES(list all such pollutants below) El NO(go to Item 17-B)
The following substances may be present in coal or coal ash:
Antimony, Arsenic, Beryllium, Cadmium, Chromium, Copper, Lead, Mercury, Nickel, Selenium, Silver, Thallium,
Zinc.
See updated attachment 5 submitted in October 2014 for potential discharges not covered by analysis.
EPA Form 3510-2C(8-90) PAGE 3 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
VII.BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
©YES(idents i the test(s)and describe their purposes below) ❑NO(go to Section VIII)
Quarterly toxicity testing on outfall 001 was conducted while the outfall was discharging in accordance with
the requirements of the existing NPDES permit. All tests performed by the facility have "passed".
Toxicity testing is required to be performed on outfall 002. There has been no discharge from outfall 002
during this permit cycle so no tests have been performed.
Toxicity testing is required to be performed on outfall 003 upon startup of the combined cycle unit. Startup
of the combined cycle unit occurred in early 2013 but no toxicity tests have been performed as the discharge
to the river was ceased in February 2013. Upon completion of modifications and commencement of discharge to
the river, toxicity tests will be conducted as required.
VIII.CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
®YES(list the name,address,and telephone number of and pollutants analyzed by, 0 NO(go to Section LY)
each such laboratory or firm below)
A.NAME B.ADDRESS C.TELEPHONE D.POLLUTANTS ANALYZED
(area code&no.) (list)
Duke Energy Analytical Lab 13339 Hagers Ferry Road 980-875-5245 Metals, COD, TKN, NO2/NO3,
NC # 248 Huntersville, NC 28078 Total Phosphorus, Oil and
Grease, TSS, TOC, Bromide,
Sulfate, Fluoride
Shealy Lab 106 Vantage Point Drive 803-791-9700 BOD, Color, Sulfide,
NC # 329 West Columbia, SC 29172 Sulfite, Fecal,
Surfactants, Cyanide,
Phenol, Volatiles,
Semi-volatile acid
compounds, PCB's, Mercury
GEL Lab 2040 Savage Road 843-556-8171 Radiological
NC # 233 Charleston, SC 29417
IX.CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information,the infomnation submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there
are significant penalties for submitting false information,inducing the possibility of fine and imprisonment for knowing violations.
A.NAME&OFFICIAL TITLE(ripe or print) B.PHONE NO.(area code&no.)
Rick Grant, Plant Manager [phone]
C.SIGNATURE D.DATE SIGNED
SAD 031 fzois
EPA Form 3510-2C(8-90) PAGE 4 of 4

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of EPA I.D.NUMBER(copy from Item 1 of Form 1)
this information on separate sheets(use the same format)instead of completing these pages. EPA Facility Name
SEE INSTRUCTIONS NC0003417 H.F. Lee Energy Complex
OUTFALL NO. •
V. INTAKE AND EFFLUENT CHARACTERISTICS(continued from page 3 of Form 2-C) 002
PART A-You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
2.EFFLUENT 3.UNITS 4. INTAKE(optional)
1. POLLUTANT a. MAXIMUM DAILY VALUE b.MAXIMUM 30 DAY VALUE c.LONG TERM AVG.VALUE a.LONG TERM AVG.VALUE
((f available) (it available) d. NO.OF a Concen- b Mass b NO.OF
(1)Concentration (2)Mass (1)Concentration (2)Mass (1)Concentration (2)Mass ANALYSES tration (1)concentration I21 Mass ANALYSES
a Biochemical Oxygen 2 mg/I Ib/Day
Demand(BOD(
b Chemical Oxygen 31 mg/I lb/Day
Demand(COD)
c Total Organic - 8.6 mg/I Ib/Day
Carbon(TOC)
a.Total Suspended 12 mg/I lb/Day
Solids(TSS)
e.Ammonia(as N) 0.08 mg/I lb/Day
f Flow VALUE N/A VALUE VALUE VALUE
MGD N/A
g.Temperature VALUE VALUE VALUE VALUE
(winter) DEGREES CELSIUS
h.Temperature VALUE VALUE VALUE VALUE
(summer) DEGREES CELSIUS
r phi MINIMUM MAXIMUM MINIMUM MAXIMUM
STANDARD UNITS
PART B-Mark"X"in column 2a for each pollutant you know or have reason to believe is present.Mark"X"in column 2b for each pollutant you believe to be absent.If you mark column 2a tor any
pollutant which is limited either directly or indirectly but expressly in an effluent limitations guideline,you must provide the results of at least one analysis for that pollutant.For other pollutants
for which you mark column 2a,you must provide quantitative data or an explanation of their presence in your discharge.Complete one table for each outfall.See the instructions
for additional details and requirements.
1. POLLUTANT 2.MARK"X" 3.EFFLUENT 4.UNITS 5. INTAKE(optional)
AND CAS NO. Believed a. MAXIMUM DAILY VALUE b.MAXIMUM 30 DAY VALUE c.LONG TERM AVG.VALUE a.LONG TERM AVG.VALUE
(if available) a.pre- b ab- (if available) ((f available) d. NO.OF a.Concen- b Mass b NO.OF
sent sent (1)Concentration (2)Mass (1)Concentration (2)Mass (1)Concentration (2)Mass ANALYSES tration t1)Concentration (2)Mass ANALYSES
a.Bromide X 0.38 mg/I lb/Day
24959-67-91
b.Chlorine. X mg/I lb/Day
Total Residual
C.Color X 15.00 N/A N/A N/A Std Units N/A N/A
d.Fecal X N/A N/A N/A Colonies N/A N/A
Coldorm /100 ml
e Fluoride X 0.20 mg/I Itb/Day
(16984-48-8) - -
f.Nitrate- X < 0.01 < mg/I Ib/Day
Nitrite(as NI _
EPA Form 3510.2C(Rev.2-85) PAGE--V-1 CONTINUE ON PAGE V-2

EPA I.D.NUMBER(copy from Item 1 of Form 1) OUTFALL NUMBER
ITEM V-B CONTINUED FROM FRONTNC0003417 002 H.F. Lee Enerav Comolex
1.POLLUTANT 2.MARK"X" 3.EI-1-LUENT 4.UNITS . INTAKE(optional)
•ND CAS NO. Believed a. MAXIMUM DAILY VALUE b.MAXIMUM 30 DAY VALUE c.LONG TERM AVG.VALUE a.LONG TERM AVG.VALUE
if available) a.pre- b.ab- (if available) (d available) d.NO.OF a Concert- b.Mass b.NO.OF
sent sent (1)Concentration 12)Mass (1)Concentration (2)Mass (1)Concentration (2)Mass ANALYSES tration 1)Concentration
(2)Mass ANALYSES
• Nitrogen,
otal Organic A 0.95 mg/I lb/Day '
as N)
.Oil and l - -
rease A < 5.00 < mg/l lb/Day
.Phosphorous
as P).Total X 0.052 mg/I lb/Day
7723-14-0)
.KaalOaCOVlly
1)Alpha,
otal X < 5.00 N/A N/A N/A phi/I N/A
N/A
2)Beta.
otal A 10.70 N/A N/A N/A pCi/I N/A N/A
3)Radium.
<
otal A 1.00 N/A N/A N/A pCdl N/A
N/A
4)Radium
26.Total X < 1.00 N/A N/A N/A pCi/l N/A '
N/A
.Sulfate
as SO4) A 35.00 mg/I lb/Day '
14808-79-8)
Sulfide
as S) X C 1.00 < mg/I lb/Day '
Sulfite
as S03) A C 2.00 < mg/I lb/Day
14265-45-3)
Surfactants
X 0.05 mg/I lb/Day
..Aluminum,
otal A 0.185 mg/I lb/Day
7429-90-5)
r.Barium.
OLEO A 0.055 mg/I lb/Day
7440-39-3)
• Boron,
oral A NM "6 mg/I lb/Day
7440-42-8) -
.Cobalt,
Mal A ' 'I 1.00 < mg/I lb/Day
7440.48.4)
-.Iron.Total
7439-89-6) A iii 0.217 mg/I lb/Day
Magnesium.
oral A ® 4.28 mg/I lb/Day
7439-95-4) •
.Molybdenum,
otal A "1 3.87 mg/I lb/Day
7439-98-7)
.Manganese.
otal X 1 0.025 mg/I lb/Day
7439-96-5)
Tin,Total
7440-31.5) A < 0.01 < mg/I lb/Day
Titanium,
otal X < 0.005 < mg/I lb/Day
/440-34-b)
EPA Form 3510.20(Rev.2-85) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D.NUMBER(copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C NC0003417 002 H.F. Lee Energy Complex -
PART C-If you are a primary industry and this outfall contains process wastewater,refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for.Mark"X"in
column 2-a for all such GC/MS fractions that apply to your industry and for ALL toxic metals,cyanides,and total phenols.If you are not required to mark column 2-a(secondary industries,
nonprocess wastewater outfalls,and nonrequired GC/MS fractions),mark"X"in column 2-b for each pollutant you know or have reason to believe is present.Mark"X"in column 2-c for each
pollutant you believe is absent.If you mark column 2a for any pollutant,you must provide the results of at least one analysis for that pollutant.If you mark column 2b for any pollutant,you
must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater.If you mark column 2b for
acrolein,acrylonitrile,2,4 dinitrophenol,or 2-methyl-4,6 dinitrophenol,you must provide the results of at least one analysis for each of these pollutants which you know or have reason to
believe that you discharge in concentrations of 100 ppb or greater.Otherwise,for pollutants for which you mark column 2b,you must either submit at least one analysis or briefly describe the
reasons the pollutant is expected to be discharged.Note that there are 7 pages to this part;please review each carefully.Complete one table(all 7 pages)for each outfall.See instructions
for additional details and requirements.
1.POLLUTANT 2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
AND CAS NO. a.re- Believed a.MAXIMUM DAILY VALUE b.MAXIMUM 30 DAY VALUE c.LONG TERM AVG.VALUE a.LONG TERM AVG.VALUE
(if available) quir- b.pre- c.ab- (if available) (if available) d.NO.OF a.Concen- b.Mass d.NO.OF
ed sent sent (1)Concentration 12)Mass (1)Concentration 1(21 Mass (1)Concentration I(2)Mass ANALYSES tration (1)Concentration I(2)Mass ANALYSES
METALS,CYANIDE,AND TOTAL PHENOLS
1M.Antimony, X < 1 < ugh lb/Day
Total(7440-36-0)
2M.Arsenic.Total X 1.06 ug/1 lb/Day
(7440-38-2)
8M.Beryllium, X < 1 < ug/l lb/Day
Total(7440-41-7)
AM.Cadmium. X < 0 1 < ug/1 lb/Day
Total(7440.43-9)
5M.Chromium. X < 1 < ug/1 lb/Day
Total(7440-47-3)
EM.Copper.Total X < 0.005 < mg/I Ib/Day
(7440-50-8)
7M.Lead,Total X < 1 < ug/1 IblDay
(7439.92.1)
8M.Mercury,Total X 0.000847 ug/1 lb/Day
(7439.97.61
9M.Nickel,Total X 1.01 ug/1 lb/Day
(7440-02-0)
10M.Selenium. X < 1 < ug/I Ib/Day
Total(7782-49-2)
11M.Silver,Total X < 1 < ug/I Ib/Day
(7440.22-4)
12M.Thallium. X < 0.0002 < mg/I lb/Day
Total(7440-28-0)
13M.Zinc,Total X 0.008 mg/I lb/Day
(7440.66-6)
14M.Cyanide. X < 0.010 < mg/I Ib/Day
Total(57-12-5)
15M.Phenols. X 0.0079 mg/I lb/Day
Total
DIOXIN
2,3.7.8 Tetra DESCRIBE RESULTS
chlorodibenzo P X
Dioxin(1764.01.6)
EPA Form 3510-2C(Rev.2-851 PAGE V-3 CONTINUE ON PAGE V-4

EPA I.D.NUMBER(copy from Item 1 of Form 1) 'OUTFALL NUMBER
CONTINUED FROM PAGE V-3 N00003417 002 H.F. Lee Energy Complex •
1.POLLUTANT 2.MARK•X• 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
AND CAS NO. a.re- _Believed a.MAXIMUM DAILY VALUE b.MAXIMUM 30 DAY VALUE c.LONG TERM AVG.VALUE a,LONG TERM AVG.VALUE
(it available) quir- b.pre- c.ab- (if available) (if available) d.NO.OF a.Concen- b.Mass d.NO.OF
ed sent sent (1)Concentration I(2)Mass (1)Concentration I(2)Mass (1)Concentration 1(2)Mass ANALYSES tration (1)Concentration I(2)Mass ANALYSES
GC/MS FRACTION-VOLATILE COMPOUNDS
1v.Acrolern X A' ` 5 < ug/I lb/Day " `
(107-02-8)
2V.Acrylonttrde X t1x 5 < ug/l IWDay
(107.13.1)
3V.Benzene X '"' 2 < ughIb/Day
(71-43-2) _
4V.Bis(Chloro-
methyl)Ether X
(542-88-1)
5V.Bromoform X p_.i._ 2 < ugh lb/Day
(75-25.2)
6V.Carbon
Tetrachloride X '''< . 2 < ugh lb/Day
(56.23-5)
7V.Chlorobenzene X r< 2 < ugh Ib/Day I
(108.90.7)
8V.Chlorodi-
bromomethane X "< 2 < ugh lb/Day _
_.
(124-48-1)
9V.Chloroethane X +� 2 < ugh lb/Day r
i
(75-00-3)
10V.2-Chloro-
ethylvinyl Ether X `< 5 < ugh lb/Day
(110-75-8)
11v.Chloroform X p*-- 2 < ugh lb/Day
(67.66.3) _
12V.Dichloro-
brornomethane X # 2 < ug/I lb/Day .
(75.27-4)
13V.Dichloro-
_
dlltuoromethane X i' 2 < ug/l lb/Day _
(75-71-8)
14V.1,1-Dichloro- X 2'd'� 2 < tgll lb/Day p
ethane(75-34-3)
15v.1,2-Dichloro- X ' ' 2 < ugh lb/Day ',
ethane(107.06-2)
16V.1,1-Dichloro- X t ' 2 < ugh '' _..
ethylene(75.35-4) .._ ..
17v.1,2-Dichloro- X '-„ci"i 2 < wail ‘. ,
lb/Day -__I
propane(78.87.5)
18V.1,3 - X 2 < ugh lb/Day °""�'•
propylene(542-75-6)
19V.Ethylbenzene X r.----, 2 < ughIWDay '
(100-41-4) _
20V.Methyl X "III2 < ugh lb/Day
Bromide(74-83-9) _
21V.Methyl X S 2 < ugh lb/Day
Chloride(74-87-3)
EPA Form 3510-2C(Rev.2-85) PAGE V-4 CONTINUE ON PAGE V-5

EPA I.D.NUMBER(copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-4 NC0003417 002 H.F. Lee Energy Complex -
1.POLLUTANT 2.MARK"X" 3.EFFLUENT 4.UNITS 5. INTAKE(optional)
•ND CAS NO. a.re- Believed a.MAXIMUM DAILY VALUE b.MAXIMUM 30 DAY VALUE c.LONG TERM AVG.VALUE a.LONG TERM AVG.VALUE
if available) qua- b.pre- c.ab- (if available) (8 available) d.NO.OF a.Concert- b Mass d.NO.OF
ed sent sent (1)Concentration 1(2)Mass (1)Concentration 1(2)Mass (1)Concentration 1(2)Mass ANALYSES (ration (1)Concentration 1121 Mass ANALYSES
GC/MS FRACTION-VOLATILE COMPOUNDS(continued)
'2V.Methylene X < 2 < ugll lb/Day
hlonde(75-09-2)
3V.1,1,2,2-Tetra-
hloroethane X < 2 < ugil lb/Day
79-34-5)
—
4V.Tetrachloro- X < 2 < ug/I lb/Day
-thylene(127-18-4)
'5V.Toluene X < 2 a ug/I Ib/Day
108-88-3)
•6V.1.2-Trans-
9ichloroethylene X < 2 < ug/I lb/Day
156.60-5)
7V.1.1.1.Tn-
hloroethane X < 2 < ug/I lb/Day
71-55-6)
8V 1,1,2-T n-
hloroethene X < 2 < ug/I Ib/Day
79-00-5)
9V.Tnchloro- X < 2 < ug/I Ib/Day
-thylene(79-01-6) _
30V.Tnchloro-
luoromethane X < 2 < ug/I lb/Day
75-69-4) _
1v.Vinyl X < 2 < ugil lb/Day
blonde(75-01-4)
GC/MS FRACTION-ACID COMPOUNDS
1A.2-Chlorophenol X < 10 < ugil lb/Day
95-57-8)
A.2,4-Dichloro- X < 10 < ugil lb/Day '
•hend(120-83-2)
A.2,4-Dimethyl- X < 10 < ug/I lb/Day
•hend(105-67-9)
-A.4,6-Dinitro-0- X < 10 < ugll lb/Day '
resol(534-52-1)
•.2.4-Dinitro- X < 50 < ug/I lb/Day
•hend(51-28-5)
A.2-N,Vophenol X < 10 < ugii lb/Day
88-75-5)
A.4-Nitrophenol X < 10 < ugil lb/Day
100-02-7)
A.P-Chloro-M- X a 10 a ug/I lb/Day
resd(59-50-7) ,
A.Pentachloro- X < 10 a ug/I lb/Day
•henol(87-86-5) ,
10A.Phenol X < 10 < ug/l lb/Day
108-95-2)
11A.2,4.6-Tn-
hlorophenol X < 10 < ug/I lb/Day
88-06-2)
EPA Form 3510-2C(Rev.2-85) PAGE V-5 CONTINUE ON PAGE V-6

EPA I.D.NUMBER(copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-5 N00003417 002 H.F.Lee Energy Complex ,
1.POLLUTANT 2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
AND CAS NO. a.re- Believed a.MAXIMUM DAILY VALUE b.MAXIMUM 30 DAY VALUE c.LONG TERM AVG.VALUE a.LONG TERM AVG.VALUE
(If available) Cul-- b.pre- cab- (d available) (If available) d.NO.OF a.Conten- b.Mass d.NO.OF
ed sent sent (1)Cancentratlon 1(2)Mass J1)Concentration 1(2)Mass (1)Concentration 1(2)Mass ANALYSES(ration (1)concentration 1(2)Mass ANALYSES
GC/MS FRACTION-BASE NEUTRAL COMPOUNDS
18.Acenaphthene X IIIIIIugh lb/Day 777
(83-32-9) �.-
2B.Aceaptntytene X ugh lb/Day trt�.3
(208.98.8)
38.Anthracene X .. ugh ib/Day
(120-12-7) _ r
�
4B.Benzidine X ugh lb/Day -).
(92-87-5)
58.Benzo(a)
Anthracene X IIIugh lb/Day el
(56.55.3)
68.Benzo(a) X 1 ugh - lb/Day
Pyrene(50-32-8) _
78.3.4-Benzo-
nuoranaMne X IIIugh lb/Day nil
(205-99-2)
88.Benzo(9111) X 1111 ugh lb/Day n
Perytene(191-24-2)
9B.Benzo(k)
Fluoranthene x ® ugh lb/Day
(207-08-9) _
10B.Bb(2-Chloro
ethoxyl)Methane X I. ugh lb/Day -
011-91-1)
11B.BIB(2-Chloro-
ethyl)
2-Chloroethyl)Ether X Mugh lb/Day -
(111-44-4)
+
12B.BIs(2-Chlorois
o
propyl)Ether X M MR lb/Day M
(108-60-1)
138.Bis(2-Ethyl-
hexyl)Phthalate X I. .. Ugh lb/Day -
(117-81.7) - ,
-
14B.4-Brorno-
phenyl Phenyl X ugh lb/Day III'
Ether(101-55-3) _
158.Baty)Benzyl X ugh lb/Day -. h
Phthalate(85.68-7)
168.2-Chloro
naphthalene X I ugh lb/Day .
(91-58-7)
178.4-Choro- �sa.�1
phenyl Phenyl X 11111 ugh lb/Day El
Ether(7005-72-3)
18B.Chrysene X ugh lb/Day �'..
�.
(21801.9) ,
198.Dbenzo(ch)
Anthracene X II. ugh lb/Day ..
(5370.3) ,
208.1,2-Dkhloro- X ugh Ib/Day in ...
benzene(95.50-1) _
218.1,3-Dlchlaro- X ugh lb/Day --.
benzene(541-73.1) _ _ _
EPA Form 3510-2C(Rev.2-85) PAGE V-6 CONTINUE ON PAGE V-7

EPA I.D.NUMBER(copy from Item 1 of Form 1) OUTFALL NUMBER
CON 1 INUEO FROM PAGE V46 IN UUU 54-1/ UUL mr. Lee tnergy(.omp(ex
1.POLLUTANT 2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
AND CAS NO. are- Believed 'a.MAXIMUM DAILY VALUE b.MAXIMUM 30 DAY VALUE c.LONG TERM AVG.VALUE a.LONG TERM AVG.VALUE
(If available) puir- b.pre- c.ab- (if available) (If available) d.NO.OF a.Concert- b.Mass d.NO.OF
ed sent sent (1)Concentration 1(2)Mass (1)Concentration 1(2)Mass (1)Concentration 1(2)Mass ANALYSES tration (1)Concentration I(2)Mass ANALYSES
GC/MS FRACTION-BASE/NEUTRAL COMPOUNDS(continued)
22B.1.4-Dichtoro- X . .... ugh lb/Day
benzene(106-46-7) I
23B.3,3-Oichloro- I
benzidine X _ ! ug/I lb/Day .".,-.7
(91_94-1)
24B.Diethyl 1
Phthalate X ug/1 Ib/Day
(84-66-2)
25B.Dimethyl
Phthalate X ug/I lb/Day F
iLs
(131-11-3)
266.Di-N-Butyl
Phthalate X I ug/I lb/Day
(84-74-2)
278.2,4-Dlnitro- X ug/I lb/Day ,
toluene(121-14-2) _
28B.2,6-Dinitro- X lelug/I lb/Day r` 7
toluene(606-20-2)
29B.Di-N-Octyl
Phthalate X ug/I lb/Day
(117-84-0)
308.1,2-Dlphenyl-
hydrazine(as Azo- Xi = ug/I lb/Day
benzene)(122-66-7) _
316.Fluoranthene X r..._4 ug/I lb/Day I: - '
(206.44-0)
32B.Fluorene Xj ug/I Ib/Day
(86-73-7) �
338.Hexachloro- X v - ug/1 lb/Day L.
.
benzene(118-74.1) _
34B.Hexa-
-
chlorobutadiene X _.' ug/1 lb/Day
(87.68-3)
.
35B.Hexachloro-
cyclopentadiene X MI ug/1 lb/Day
(77-47-41
36B.Hexachloro- X a ug/I lb/Day
ethane(67-72-1)
37B.Indero �!��; •
(1,2,3-cd)Pyrene X iE.+: ughl lb/Day t
(193.39.5)
38B.Isophorone X ® ug/I lb/Day Ir"-
_
(78-59-1)
398.Naphthalene X ® ug/I lb/Day
(91-20-3) _
406.Nitrobenzene X ® ugA lb/Day T'
(98-95-3)
416.N-Nitro-
ir.. a
sodimethylamine XIL ug/l lb/Day 1.
(62-75-9) . .
42B.N-Nitrosodi-
N-Propylamine X III
ug/I IblDay _ _
(621-64-7) -
EPA Form 3510-2C(Rev.2-85) PAGE V-7 CONTINUE ON PAGE V-8

EPA I.D.NUMBER(copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-7 _ NC0003417 002 H.F. Lee Energy Complex •
1.POLLUTANT 2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
•ND CAS NO. ase- Believed a.MAXIMUM DAILY VALUE b.MAXIMUM 30 DAY VALUE c.LONG TERM AVG.VALUE a.LONG TERM AVG.VALUE
if available) ow- b.pre- cab- (8 available) (if available) d.NO.OF a.Concen- b.Mass d.NO.OF
ed sent sent (1)Concentration I(2)Mass (1)Concentration 1(2)Mass (1)Concentration 1(2)Mass ANALYSES tration (1)Concentration 1(2)Mass ANALYSES
GC/MS FRACTION-BASE/NEUTRAL COMPOUNDS(continued)
3B.N-Nitro- p
odlphenylamine X ug/I Ib/Day E
86-30-6)
4B.Phenanthrene X ug/) lb/Day r:77,
85-01-8)
5B.Pyrene X ug/I lb/Day -
12300-0)
66.1,2,4-Tn-
hlorobenzene X ug/I lb/Day !:::1„.
120-82-1)
GC/MS FRACTION-PESTICIDES
1P.Aldrin X
309-00-2)
'P.alpha-BHC X
319-84-6)
P.beta-BHC X
315-85-7)
P.gamma-BHC X
58.89.9)
••.delta-BHC X
319-86-8)
•-.Chlordane X
57-74-9)
P.4,4'-DDT X
50-29-3)
.P.4,4'-1)DE X
72.55-9)
•P.4.4'-DDD X
72-54-8) _ _
10P.Dieldnn X
60-57-1)
11P.alpha-Endosulfan X
115-29-7)
12P.beta-Endosulfan X
115-29-7)
13P.Endosulan
ulfele X
1031-07-8)
14P.Endnn X
72-20-8)
t5P.Endrin
•ehyde X
7421-93-4)
16P.Heptachlor X
76-44-8)
EPA Form 3510-2C(Rev.2-85) PAGE V-8 CONTINUE ON PAGE V-9

EPA I.D.NUMBER(copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-8 NC0003417 002 H.F. Lee Energy Complex •
1.POLLUTANT 2.MARK'X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
AND CAS NO. a.re- _Believed a.MAXIMUM DAILY VALUE b.MAXIMUM 30 DAY VALUE c.LONG TERM AVG.VALUE a.LONG TERM AVG.VALUE
(If available) quip- b.p e- c.ab- (If available) Of available) d.NO.OF a.Concern b.Mass d.NO.OF
ed sent sant (1)Concentration 1(2)Mass (1)Concentration j(2)Mass (1)Concentration 1(2)Mass ANALYSES tuition (1)Concentration 1(2)Mass ANALYSES
GC/MS FRACTION-PESTICIDES(continued)
17P.HaptadNor
Epoxide X
(1024.67.3)
18P.PCB-1242 X < 0.25 <
(53469.21.9)
19P.PCB-1254 X < 0.25 <
(11097-6x9-1)
20P.PCB-1221 X < 0.25 <
(11104-28.2)
21P.PCB-1232 X < 0.25 <
(11141.16-5)
22P.PCB-1248 X < 0.25 <
(12672-29-6)
23P.PCB-1260 X < 0.25 <
(11096-82-5)
24P.PCB-1016 X < 0.25 <
(12674-11-2)
25P.Toxaphene X
(8001-35.2)
EPA Form 3510-2C(Rev.2-85) PAGE V-9