NC0000752_Renewal Application_20160927

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KAPSTONE
September 23, 2016
Ms. Wren Thedford
NC DENR / SWR / NPDES Unit
1617 Mail Service
Raleigh, NC 27699-1617
Re: Renewal Notice
NPDES Permit No. NC0000752
Roanoke Rapids Mill
Halifax County
Dear Ms. Thedford
KAPSTONE
KRAFT PAPER CORPORATION
ADhAslonofKAPSTONE PAPER AND PACKAGING CORPORATION
100 Gaston Road Roanoke Rapids, NC 27870
kapstonepaper.com
r-tiw d ENE YNC,DEQ/DVVR
SFP 27 2096
'Offal ' a aaiift/
Pcfniii,,'in Seciion
Pursuant to Federal (40 CFR 122.4 Appendices A -D and North Carolina (15A NCAC 2H)
regulations NPDES permit renewal application must be submitted at least 180 days prior to the
expiration of the existing permit. The purpose of this correspondence is to request renewal of
NPDES Permit No. 0000752 for the Kapstone Kraft Paper mill located in Roanoke Rapids, North
Carolina. Enclosed you will find the following information (one original and two copies):
• EPA Form 3510-1 (General Information Form)
• Topographic Map of Mill Site and Discharge Points
• Application Form 2C- Wastewater Discharge Information
• Mill Water Balance Diagram
• Wastewater Treatment System Diagram
• Wastewater Treatment System Narrative Description
• Sludge Management Plan Narrative Description
• Results of Analysis Required under Part V -B and V -C of Form 2 C
• Priority Pollutant Analysis Results
Since the last renewal of the NPDES there have been minor changes to the wastewater treatment
system. A new top was installed on our Wastewater Lift Station, the Primary Clarifier launder
trough was lined, and the Clarifier Effluent line that crosses over the Roanoke River to the Aeration
Pond was replaced.
If you have any questions please don't hesitate to call Neal Davis at 252-533-6295 or Chris
Williams at 252-533-6237.

Sincerely,
Wilbur G. Kessinger
Vice President Mill Operation
xc: Neal Davis
Mike Knudson
Chris Williams
Paul Kinnin
Ben White

EPA FORM 3510
GENERAL INFORMATION FORM
RECEIVEDINCDEQIDVVR
SEP 2 7 2016
Water Quality
Permitting Section

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�XII�NATURE�OF�B.USINE_ S,'kSr"�(providera�`tirietdescript(on` ��
~ The Kapstone Paper Corporation, Roanoke Rapids mill produces high quality unbleached Kraft paper and
paperboard. The mill is integrated including power generation, chemical recovery, pulp production and final
paper and paperboard manufacture.
ERTIFIGT
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Wilbur G 'Kessinger Jr. VP Mill Operations
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EPA FORM 3510-1(8-90)

TOPOGRAPHIC MAP OF
.MILL SITE AND-DISCHAG E POINTS

Data use subject to license. #TN Scale 1 : 25,000
© 2006 DeLorme. Topo USA® 6.0. MN ce.rvvj 0 2
0 300 1W 600 800 1000
m
www.delorme.com 1" = 2,083.3 ft Data Zoom 13-0

APPLICATION FORM 2C
WASTEWATER DISCHARGE INFORMATION

EPA I.D. NUMBER (copy from Item I of Form 1) Form Approved.
NCD044737807 OMB No. 2040-0086
Please print or type in the unshaded areas only. Annan 1 — i- q q4 00
FORM
2C
NPDES
I. OUTFALL LOCATION
U.S.
U.S. ENVIRONMENTAL PROTECTION AGENCY
���EPA CATION FOR PERMIT TO DISCHARGE WASTEWATER
EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURE OPERATIONS
Consolidated Permits Program
For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A. OUTFALL NUMBER
(list)
B. LATITUDE C. LONGITUDE
D. RECEIVING WATER (name)
1. DEG.
1 2. MIN.
3. SEC. 1. DEG. 2. MIN.
3. SEC.
001
N36
- 28
18.6 W77 38
12.8
Roanoke River
002
N36
28
18.8 W77 38
20.5
Roanoke River
II. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units
labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations,
treatment units, and outfalls. If a water balance cannot be determined (e.g., for certain mining activities), provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall, ptovide a description of. (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water,
and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets if
necessary.
1. OUT-
2. OPERATION(S) CONTRIBUTING FLOW 3. TREATMENT
FALL
NO. (list)
b. AVERAGE FLOW b. LIST CODES FROM
a. OPERATION (list) (include units) a. DESCRIPTION TABLE 2C-1
0 01
Condensate Collection .56 MGD Ear Screen
1-T
Pulp Mill Area 2.6 MGD Primary Clarification
1-U
Paper Mill Area 10.2 MGD Aeration Pond
3-B
Utilities Area 3.5 MGD Stabilization Ponds
3-G
Defoamer Addition
XX
Discharge to River
4-A '
Sludge neutralization
S -E
Chemical Conditioning
5-E
Rotary Screen Thickner
2-D
Srew Presses
5-R
• Sludge Lagoon
S -T
Landfill
5-Q
- Diversion Pond
XX
002
B&C Evaporator Cooling Water 3.14 MGD Single pass non -contact, no treatment
XX
OFFICIAL USE ONLY (effluentguidelinessub-categories)
EPA Form 3510-2C (8-90) -PAGE 1 of 4 CONTINUE ON REVERSE

\0,
CONTINUED FROM THE FRONT
C. Except for storm runoff, leaks, or spills; are any of the discharges described in Items II -A or B intermittent or seasonal?
❑ YES (complete thefollowing table) Z NO (go to Section 111)
3. FREQUENCY
4. FLOW
a. DAYS PER
B. TOTAL VOLUME
2. OPERATION(s)
WEEK
b. MONTHS
a. FLOW RATE (in mgd)
(specify with units)
1. OUTFALL
CONTRIBUTING FLOW
- W -0y
PER YEAR
1, LONG TERM
2. MAXIMUM
1. LONG TERM
2. MAXIMUM
C. DURATION
NUMBER (list)
(list)
average)
(spec average)
AVERAGE
DAILY
AVERAGE
DAILY
(in days)
III. PRODUCTION
A. Does an effluent guideline limitation promulgated by EPA under Section
304 of the
Clean Water
Act apply to your
facility?
YES (complete Item III -B)
❑
NO (go to Section
IV)
B. Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure of operation)?
❑✓ YES (complete Item 111-0 ❑ NO (go to Section IV)
C. If you answered "yes" to Item III -B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used in the
applicable effluent guideline, and indicate the affected outfalls.
1. AVERAGE DAILY PRODUCTION
2. AFFECTED OUTFALLS
(list outfall numbers)
a. QUANTITY PER DAY
b. UNITS OF MEASURE
c. OPERATION, PRODUCT, MATERIAL, ETC.
(spec)
1384
Tons
Unbleached Kraft Paper
001, 002
IV. IMPROVEMENTS
A. Are you now required
by any Federal, State or local
authority to meet any implementation schedule for the construction,
upgrading or operations of wastewater
treatment equipment or
practices or any other environmental
programs which may affect the discharges described in this application?
This includes, but is not limited to,
permit conditions, administrative
or enforcement orders,
enforcement compliance schedule letters, stipulations, court orders, and
grant or loan conditions.
❑ YES (complete
the following table)
© NO (go to Item X -B)
1. IDENTIFICATION OF CONDITION,
2. AFFECTED OUTFALLS
3. BRIEF DESCRIPTION OF PROJECT
4. FINAL COMPLIANCE DATE
AGREEMENT, ETC.
a. NO,
b. SOURCE OF DISCHARGE
a. REQUIRED
b. PROJECTED
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned, and indicate your actual or planned schedules for
construction.
❑ MARK "X" IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
.EPA Form 3510-2C (8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA Form 3510-2C (8-90) PAGE 3 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
VII. QIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
© YES (,dent fy the tests) and describe their purposes below) NO (go to Sagion Vlll)
The North Carolia Ceriodaphnia Chronic effluent bioassay procedure is performed on effluent dischage 001 on a
quarterly basis (March, June, September and December)
VIII, CONTRACT ANALYSIS INFORMA71ON
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
® YES (list the name, address, and telephone number of, andpollutants analyzed by, NO (go to Section LY)
each such laboratory or firm below)
A. NAME
B. ADDRESS
C. TELEPHONE
D. POLLUTANTS ANALYZED
(area code & no.)
(list)
Meritech, Inc,
642 Tamcc Road
336-342-4748
Priority Pollutants
Reidsville, NC 27320
Purgeable Organics
Acid / Base Neutral
Extractable
Pesticides
'
Semi- volatiles
Volatile organics
Florida Radiochemistry Services
5456 Hoffner Ave. Suite 201
407-382-7733
Radiological Analysis
Inc.
Orlando FL. 32812
IX. CERTIFICATION
I certify under penalty of law that this document
and all attachments were prepared under my direction
or supervision in accordance
with a system designed to assure that
qualffled personnel properly gather and evaluate
the information submitted. Based on my inquiry
of the person or persons who
manage the system or those persons
directly responsible for gathering the information,
the information submitted is, to the best of my knowledge
and belief, true, accurate,
and complete. I am aware that there
are significant penalties for submitting false
information, including the possibility of fine and imprisonment
for knowing violations.
A. NAME & OFFICIAL TITLE (type or print)
B. PHONE NO. (area code & no.)
Wilbur G. Kessinger Jr. Vice President Mill Operations
[phone]
C. SIGNATURE
D. DATE SIGNED
EPA Form 35104C (8-90) V V PAGE 4 of 4

MILL WATER BALANCE DIAGRAM

Mill Water Balance
Paper Mill Effluent ** 10.2 MGD
Pulpmill Effluent ** 2.60
Condensate Collection Effluent## 0.86
Utility Effluent ** 3.5
C7
Roanoke Rapids Mill
August 2015 - July 2016
Rain Runoff and Landfill Leachate
Main Sewer Flow, Waste Flow to River
o Water -�
## 1
-MGD T�o,tn,o„ ## 20.3 MGD
Recycle ®®oae.•®s.
Recycle .
Estimated Flow From- Enai r Studue
## Flowmeter,
Non Contact to River ** 3.14 MGD
Paper Mill Influent
10
Paper Mill
.... �Ia
•
Cold Water Tank
Pulpmill
Secondary Blow Heat
®®®du
Primary Turp Cond
o
Sec. Reflux Condensor
Pulpmill Influent
rdu
�1
Flow from River
•
a
I
Condensate Collection
## 20.03 MGD
•
®
�.I
HPFT
�I
Ou
Utility
a
B Evaps Surface Cond
•
C Evaps Surface Cond
v. ®..I
Boiler Water Makeup
Utility Influent
Slaker Stacks
Ash Pond
Ir
Non Contact Water
Non Contact
®• a
Surface Condensor Overflow
Sec. Turp Cond
Paper Mill Effluent ** 10.2 MGD
Pulpmill Effluent ** 2.60
Condensate Collection Effluent## 0.86
Utility Effluent ** 3.5
C7
Roanoke Rapids Mill
August 2015 - July 2016
Rain Runoff and Landfill Leachate
Main Sewer Flow, Waste Flow to River
o Water -�
## 1
-MGD T�o,tn,o„ ## 20.3 MGD
Recycle ®®oae.•®s.
Recycle .
Estimated Flow From- Enai r Studue
## Flowmeter,
Non Contact to River ** 3.14 MGD

WASTEWATER TREATMENT SYSTEM
DIAGRAM

Paper Mill
Roanoke River..W,11�
Stormwater Ditch
Site Plan - Roanoke Rapids
Roanoke Rapids
Wastewater Treatment Plant
Aerators:
4 - 50 hp Aero 2 Aerators
3- 75 hp Aero 2 Aerators
18 - 75 hp Aerators
�6 - 60 hp Aerators
2135 hp Total
Landfill Leachate

WASTEWATER TREATMENT SYSTEM
NARRATIVE DESCRIPTION

Wastewater Treatment System Description
The main sewer brings wastewater into the facility and is a concrete lined open channel.
There is a Main Sewer sampler, pH, conductivity probes, and a flow meter in the Main
Sewer. The instruments have local readouts at the channel and in the Sludge Press / Lime
Kiln operator control room. The sludge press / lime kiln operator monitors the operation
of the sludge press and the wastewater facility from this control room.
The flow goes through a mechanical bar screen, into a wet well where three lift pumps
carry the flow to a 200 ft. diameter primary clarifier. The primary clarifier has a capacity
of 3.8 million gallons. In the event of a power failure, mechanical problems, or high
strength waste the Sludge press / Lime kiln operator can divert the main sewer by gravity
to the Diversion Pond. The pond is 20.4 acres and holds 28 million gallons of wastewater
or about two days of wastewater flow. The water from the diversion pond is then
pumped to the head of the wastewater plant at a rate of approximately 1500 gallons per
minute.
The flow from the Primary Clarifier is then gravity fed to the Aeration Pond. Nutrients
are added -to the clarified effluent. The aeration pond covers 21.5 acres and has a
retention time of approximately four days. There are 31 aerators with a total rated
horsepower of 2,135. The aeration pond also receives approximately 0.8 -MGD from the
condensate collection system Hard Pipe Feed Tank. This is a method of condensate
collection and treatment in the Maximum Achievable Control Technology rules for the
Pulp and Paper Industry. We also have the capability of adding defoamer to the aeration
pond influent flow to prevent excessive foam. The water then cascades down to the
stabilization ponds or settling ponds. There are.370 acres of stabilization ponds with' a
retention time of approximately 30 — 35 days. The ponds and dikes are clay lined and
have a capacity of approximately 482 million gallons.
The final stabilization pond discharge has a bar screen, a composite sampler and A
butterfly valve at the discharge to the river. This allows us to control the amount of
discharge flow. There is also a multi sensor velocity flow meter in the discharge line.
We have equipment to feed defoamer to the effluent for foam control. The defoamer is
NALCO 7507 Plus, a water based defoamer to suppress foam, just after the discharge
valve to the river at. the discharge.
Sludge from the primary clarifier is pumped to a blend tank where sulfuric acid is added
for pH control. Polymer is added to the sludge pumped from the blend tank to one of two
Rotary Screen Thickeners and gravity fed to one of two Dupps Andritz screw presses. A
sludge cake of 40 % solids or greater is produced. These solids are deposited in one of
four Ravens 28 foot Dump Trailers and hauled to the permitted landfill (#WQ0000436).
During the treatment process solids accumulate in the first stabilization pond. To assure
optimum treatment efficiency, this pond is periodically dredged to remove those solids.
Dredging spoils from the Stabilization ponds or Diversion pond are pumped by way of
fused 8 —10 inch plastic pipe to the back of the old sludge pond where it is allowed to

decant. Leachate from the old sludge pond and the onsite landfill flows by gravity into
the aeration pond and is treated along with the other wastewater.

SLUDGE MANAGEMENT PLAN
NARRATIVE DESCRIPTION

Kapstone Kraft Paper Corporation
Roanoke Rapids Mill
Sludge Management Plan
The solids that settle to the bottom of the Primary Clarifier are pumped from the center of
the clarifier.to a blend tank where Sulfuric Acid is added to lower the pH and did the
flocking of the sludge. The sludge is then pumped from the Blend tank to one of two
Rotary Screen Thickeners. While in route to the Rotary Screen Thickener polymer is
added to thicken the sludge. Filtrate is released through the screen of the Rotary Screen
Thickener and the solids remain inside and are dumped into a hopper. One of two, thirty
eight foot Screw Presses compresses the solids and pushes the filtrate through the
screens. The solids are then dumped in the screw conveyors and into one of four sealed
sludge hauling trailers. The sludge is about 40% sludge solids. Sludge is then taken to
the mills Landfill by way of the mill's privately owned roads (Permit Number
WQ0000436). All filtrate from the sludge press is returned to the head of the wastewater
plant for treatment. All leachate from the Landfill is fed by gravity to the Aeration Pond
of the Wastewater Treatment Plant
The mill has a Distribution of Residuals permit acquired February of 2009, and renewed
in June of 2015 for the beneficial use of Flyash and Primary Clarifier Residuals (Permit
Number WQ0021577).
To periodically clear ponds of accumulated solids, dredging through 8-10 inch fused
plastic pipe to what is referred to as the Old Sludge Pond is contracted. The solids decant
in the sludge pond and the filtrate returns to the Aeration Pond for treatment.
July 12, 2011
Revised: September 20, 2016

RESULTS OF ANALYSIS
PART V -B of FORM 2C
FLOW TO RIVER
001

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information EPA I.D. NUMBER (copyfrom Item 1 of Form 1)
on separate sheets (use the same format) instead of completing these pages. NCD044737807 001
SEE INSTRUCTIONS.
OUTFALL NO.
V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C)
001
PART A You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
3. UNITS
4. INTAKE
2. EFFLUENT
(specifyifblank)
(optional)
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
a. MAXIMUM DAILY VALUE
(ifavailable)
(ifavailable)
AVERAGE VALUE
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
1. POLLUTANT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
(1) CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
a. Biochemical Oxygen
32.6
5,690
13.91
2356
249
mg/1
lbs.
Demand (BOD)
b. Chemical Oxygen
144
19,456
1
m9/1
lbs.
Demand(COD)
c. Total Organic Carbon
14.5
1,959
1
m /1
g
lbs.
(TOC)
d. Total Suspended
Solids(TSS)
37.89
7428
21.85
3700
249
mg/1
lbs.
e. Ammonia (as N)
6.30 -
904
2.57
435
12
mg/1
lbs.
VALUE
VALUE
VALUE
VALUE
f. Flow
23.5
20.3
365
MGD
g. Temperature
VALUE
VALUE
VALUE
°C
VALUE
(winter)
5.2 C
17
h. Temperature
VALUE
VALUE
VALUE
°C
VALUE
(summer)
29.3 C
54
MINIMUM
MAXIMUM
MINIMUM
MAXIMUM
i. pH
6.7
7.9
249
STANDARD UNITS
PART B — Mark "X" in column 2-a for each pollutant you know or have'reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either
directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide
quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements.
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG. VALUE
a. LONG TERM AVERAGE
AND
a
b,
a. MAXIMUM DAILY VALUE
(ifavailable)
(ifavailable)
VALUE
CAS NO.
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
- (1)
(1)
(1)
(ifavailable)
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
a. Bromide
0.092
12 .43
1
mg/1
lbs
(24959-67-9)
b. Chlorine, Total
X
0
Residual
Residual
C. Color
X
336 C.U.
1
d. Fecal Coliform
X
2Col/100m1
1
e. Fluoride
(16984-48-5) 1
.182 mg/1
24.6
1
mg/1
lbs.
f.
\/
.37
49.9
1
mg/1
lbs.
(asi/V)teNitrite
EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE

ITEM V -B CONTINUED FROM FRONT
EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG. VALUE
a. LONG TERM
AND
a
b.
a. MAXIMUM DAILY VALUE
(ifavailable)
(ifavailable)
AVERAGE VALUE
CAS NO.
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(E
(ifavailable)
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
g. Nitrogen,
` /
Total Organic (as
X
10.4
1492
6.63
1122
13
mg/1
lbs.
N)
h. Oil and
Grease
l
I. Phosphorus
(as P), Totalu
965
168
.518
87.6
13
mg/1
lbs.
(7723-14-0)
j. Radioactivity
(1) Alpha, Total
x
1.1
1
pCi/L
(2) Beta, Total
x
1.3
1
pCi/L
(3) Radium,
X
0.3
1
pCi/L
Total
Radium 226,
X
0.2
1
pCi/L
To)t
Sulfate
(-SO4)X
(
1860
251,301
1
mg/1
lbs.
(14808-79-8)
I. Sulfide
X
1
(ass)
-
m. Sulfite
(as S03)
X.
1
(142651;5-3)
n. Surfactants
x
1.98
267. 5
1
mg/1
-lbs.
o. Aluminum,
TotalX
. 411
55.5
1
mg/1
lbs.
(7429-90-5)
p. Barium, Total
(7440-39-3)
X.106
14.3
1
mg/1
lbs.
q. Boron, Total
(7440-42-8)
x
083
11.2
1
mg/1
lbs.
r. Cobalt, Total
\/
x
1
(7440-48-4)
s.Iron, Total\/
x
.177
23.9
1
m 1
g/
lbs.
(7439-89-5)
t. Magnesium,
Total
X
6.24
843
1
mg/1
lbs.
(7439-9513)
u. Molybdenum,
Total
X
1
(7439-98-7)
v. Manganese,
TotalX
387
52.3
1
mg/1
lbs.
(7439-96-5)
w. Tin, Total
X
1
(7440-31-5)
x. Titanium,
Total
x
1
(7440-32-6)
EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D. NUMBER (copyfiomItem I offonn 1) JOUTFALLNUMBER
r.r)NTINI IFr1 FRr)M PAr:F -q r)F r=nRM 9-r. I NCDO4473707 1001
PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and nonrequired GC/MS
fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must
provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2 -methyl -4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for
additional details and requirements.
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG.
a. LONG TERM
.AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
OF
(1j
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION (2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION (2) MASS
ANALYSES
METALS, CYANIDE, AND TOTAL PHENOLS
1M. Antimony, Total
1
(7440-36-0)
2M. Arsenic, Total�.
1
(7440-38-2)
3M. Beryllium, Total
1
(7440-41-7)
Total.
4M. Cadmium, Total�/
X
u
004
.54
1
Mg/1
lbs.
(7440-43-9)
5M. Chromium,
1
Total (7440-47-3)
6M. Copper, Total
05
8.7
. O5
8.5
5
mg/1
lbs.
(7440-50-8)
7M. Lead, Total�/
X
�/
X
1
(7439-92-1)
8M. Mercury, Total�/
X
u
15.1
2.0
1
ng/ 1
lbs.
(7439-97-6)
9M. Nickel, Totalu
u
012
1.6
1
mg/1
lbs.
(7440-02-0)
/ `
10M. Selenium,
�/
1
Total (7782-49-2)
X\
11 M. Silver, Total
\/
X
�/
X
1
(7440-22-4)
12M. Thallium,
\/
X
�/
X
1
Total (7440-28-0)
13M. Zinc, Total
X
1
(7440-66-6)
14M. Cyanide,
X
1
Total (57-12-5)
15M. Phenols,u
. 039
5.3
1
mg/1
lbs.
Total
DIOXIN
2,3,7,8 -Tetra-
DESCRIBE RESULTS Not Detected
chlorodibenza-P-
X
X
Dioxin (1764-01-6)
EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
1. POLLUTANT
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
AND
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
CAS NUMBER
a.
'TESTING
b.
c.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
(ifavailable)
REQUIRED
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)(I
(1)
(1)
PRESENT
ABSENT
CONCENTRATION
' (2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
6. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —VOLATILE COMPOUNDS '
IV. Accrolein
x
X
1
(107-02-8)
2V. Acrylonitrile
X
X
(107-13-1)
1
3V. Benzene
x
X
(71-43-2)
i
4V. Bis (Chloro-
n7ethyl) Ether
\ /
\
(542-88-1)
/X\
X
1
5V. Bromoform
(75-25-2)
x
X
1
Carbon
Tetrachloride
X
X
1
(56-23-5)
7V. Chlorobenzene
\\//
(108-90-7)
x
1
8V. Chlofodi-
bromomethane
\ /
X
\ /
X
1
(124-48-1)
W. Chloroethane ,
x
X
1
(75-00-3)
10V2-Chloro-
ethylvinyl Ether
x
1
(110-75-8)
11 V. Chloroform
x
X
(67-66-3)
1
12V. Dichloro-
bromomethane
u
1
(75-27-4)
/ \
13V. rometro-
difluoomethane
X
X
1
(75-71-8)
14V. 1,1-Dichloro-
ethane (75-34-3)
X
X
1
15V. 1,2-Dichloro-
x
%<
ethane (107-06-2)
1
16V. 1,1-Dichloro-
ethylene (75-35.4)
X
x\/
1
17V.1,2-Dichloro-
propane (78-87-5)
x\/
X
1
18V.1,3-Dichloro-
propylene
\ /
`
X
(542-75-6)
/X\
1
19V. Ethylbenzene
\/
(100-41-4)
x
X
1
20V. Methyl
X
x
1
Bromide (74-83-9)
21V. Methyl
Chloride (74-87-3)
EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V-5

CCINTINI IFr1 FRr1M PAt;F V-A
EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b,
c.,
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION—VOLATILE COMPOUNDS (continued)
22V. Methylene
1
Chloride (75-09-2)
23V.1,1,2,2-
Tetrachloroethane
` ,
X
X
1
79-34-5
' `
24V. Tetrachloro-
ethylene (127-18-4)
25V. Toluene
1
(108-88-3)
26V. 1,2-Trans-
Dichloroethylene
X
X
1
(156-60-5)
27V.1,1,1-Trichloro-
Xx1
ethane (71-55-6)
28V.1,1,2-Trichloro-
1
ethane (79-00-5)
29V Trichloro-
x
1
ethylene (79-01-6)
30V. Trichloro-
fluoromethane
X
X
1
75-69-4
31V. Vinyl Chloride
1
(75-01-4)
GC/MS FRACTION —ACID COMPOUNDS
1A.2 -Chlorophenol
1
(95-57-8)
2A. 2,4-Dichloro-
1
phenol(120-83-2)
3A.2,4 -Dimethyl-
1
phenol(105-67-9)
4A.4,6-Dinitro-0-
1
Cresol (534-52-1)
5A.2,4-Dinitro-
1
phenol(51-28-5)
GA. 2-Nitrophenol
1
(88-75-5)
7A.4-Nitrophenol
1
(100-02-7)
BA. P -Chloro -M-
1
Cresol (59-50-7)
9A. Pentachloro-
phenol (87-86-5)
10A. Phenol
x
u
1
(108-95-2)
/\
11A.2,4,6-Trichloro-
X
1
phenol (88-05-2)
/�
EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE

EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7
2. MARK "X" 3. EFFLUENT
4. UNITS
5. INTAKE (optionan
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG.
a. LONG TERM
AND
a.
b.
C. a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED (1)
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
1
()
r )
(favailable
REQUIRED
PRESENT
ABSENT CONCENTRATION (2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASElNEUTRAL COMPOUNDS
1 B. Acenaphthene
1
(83-32-9)
2B. Acenaphtylene
1
(208-96-8)
3B. Anthracene
�/
x
�/
x
1
(120-12-7)
4B. Benzidine
�/
x
1
(92-87-5)
5B. Benzo (a)
Anthracene
X
1
(56-55-3)
6B. Benzo (a)
�/
x
�/
x
1
Pyrene (50-32-8)
7B. 3,4-Benzo-
fluoranthene
X
1
(205-99-2)
8B. Benzo (ghi)
�/
x
�/
x
1
Perylene (191-24-2)
9B. Benzo (k)
Fluoranthene
X
1
(207-08-9)
10B. Bis (2-Chlora-
ethoxy) Methane
1
(111-91-1)
11 B. Bis (2-Chloro-
ethyl) Ether
�/
x
�/
x
1
(111-44-4)
12B. Bis (2-
Chloroisopropyn
1
Ether(102-80-1)
13B. Bis (2-Ethyl-
hexyl) Phthalate
X
j
(117-81-7)
14B. 4-Bromophenyl
Phenyl Ether
1
(101-55-3)
15B. Butyl Benzyl
�/
x
�/
x
1
Phthalate (85-68-7)
16B. 2-Chloro-
naphthalene
X
X
1
(91-58-7)
17B. 4-Chloro-
phenyl Phenyl Ether
X
1
(7005-72-3)
16B. Chrysene
�/
x
1
(218-01-9)
19B. Dibenzo (oh)
Anthracene
�/
1
(53-70-3)
/�
20B.1,2-Dichloro-
�/
x
1
benzene (95-50-1)
,3-DI-chloro-
21B.1,3-Di-chloro-
x
1
benzene(541-73-1)
benzene (541-73-1)
EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7

(Y)NITIKII RM FRrIM DArAP v -R
EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
CAS NUMBER
a.
TESTING
b.
BELIEVED
C.
BELIEVED
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
d. NO. OF
a: CONCEN-
AVERAGE VALUE
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued)
226.1,4-Dichloro-
1
benzene (10646-7)
238.3,3-Dlchloro-
1
benzidine (91-94-1)
246. Diethyl
Phthalate (84-66-2)
X
X
1
25B. Dimethyl
Phthalate
X
\ ,
X
1
(131-11-3)
26B. Di -N -Butyl
1
Phthalate (84-74-2)
27B.2,4-Dinitro-
1
toluene (121-14-2)
28B.2,6-Dinitro-
1
toluene (606-20-2)
29B. Di-N-Octyl
\/
1
Phthalate (117-84-0)
x\
30B.1,2 -Diphenyl -
zo-
hydrazine (as Azo-
X
1
benzene)
benzene)(122-66-7)
31B. Fluoranthene
1
(206-44-0)
32B. Fluorene
1
(86-73-7)
33B. Hexachloro-
X
1
benzene (118-74-1)
34B. Hexachloro-
1
butadiene (87-68-3)
35B. Hexachloro-
cyclopentadiene
` ,
X
\ ,
X
1
(77-47-4)
36B Hexachloro-
x
x�\
1
ethane (67-72-1)
378
(1,2,3 -c -cd) � Pyrene
1
(193-39-5)
38B.Isophorone
1
(78-59-1)
39B. Naphthalene
1
(91-20-3)
40B. Nitrobenzene
X1
(98-95-3)
41B. N -Nitro-
sodimethylamine
\ /
X
` /
X
1
(62-75-9)
/ \
42B. N-Nitrosodi-
N-Propylamine
1
(621-64-7)
EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9
2. MARK W'
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
((/available)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION (2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued)
43B. N-Nitro-
sodiphenylamine
X
X
1
(86-30-6)
44B. Phenanthrene
\/
x
X
1
(85-01-8)
45B. Pyrene
29 -OG -0)
(1s-oo-o>
X
X
1
46B. 1,2,4-Tri-
chlorobenzene
X
X
1
(120-82-1)
GC/MS FRACTION — PESTICIDES
1 P.Alddn
X
X
1
(300 9-00-2)
-BHC
x
X
1
(319-84-6)
(31
�\
3P.
x
X
1
(319--85-7)85-7)
/�
BHC
x
X
1
(58-89-9)
(58-8
�\
BHC
X
X
1
(319--86-8)
(31
6P. Chlordane
X
X
1
(57-74-9)
7P.4,4' -DDT
X
X
1
(50-29-3)
8P.4,4' -DDE
X
X
1
(72-55-9)
9P. -DDD
x
X
1
(72-54-2-54-8)
�\
Dieldrin
X
X
1
(60-57-1)
(60-
11 P. a-Enosulfan
X
X
1
(115-29-7)
12P. (i-Endosulfan
\�
x
X
1
(115-29-7)
Endosulfan
Sulfate
Sulfate
X
X
1
(1031-07-8)
14 ) n
X
X
1
(72-20-8-20-8)
Endrin
Aldehyde
X
X
1
(7421-93-4)
16P. Heptachlor
X
X
1
(761{4-8)
EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9

EPA I.D. NUMBER (copyfrom Item I of Form 1) OUTFALL NUMBER
NCD044737BO7 001
rntiTiw ir=n c=anon enr_r= v_a
EPA Form 3510-2C (8-90) PAGE V-9
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
C. LONG TERM AVRG.
a. LONG TERM
AND
a,
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
d. NO. OF
a. CON CEN-
AVERAGE VALUE
b. NO. OF
(1)
CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS
CAS NUMBER
(ifavailable)
TESTING
REQUIRED
BELIEVED
PRESENT
BELIEVED
ABSENT
ANALYSES
TRATION
b. MASS
ANALYSES
GC/MS FRACTION — PESTICIDES (continued)
17P. Heptachlor
Epoxide
\ /
�(
\ /
X
1
(1024-57-3)
/ \
/ \
18P. PCB -1242
1
(53469-21-9)
19P. PCB -1254
\/
x
�/
x
1
(11097-69-1)
20P. PCB -1221
\/
x
\/
1
(11104-28-2)
�\
21 P. PCB -1232
(11141-16-5)
\/
x\
1
22P. PCB -1248
(12672-29-6)
\/
x
1
23P. PCB -1260
(11096-82-5)
x
1
242. PCB -1016
(12674-11-2)1-2)
X
1
25P.Toxaphene
\/
x
�/
1
(8001-35-2)
^
EPA Form 3510-2C (8-90) PAGE V-9

RESULTS OF ANALYSIS
PART V -B of FORM 2C
NON CONTACT COOLING WATER
002

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information EPA I.D. NUMBER (copyfromJtem I of Form 1)
on separate sheets (use the same format) instead of completing these pages. IN.CDO44737807 002
&FF IMCTRI ICTlnkr4
OUTFALL NO.
V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C) 002
PART A—You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
3. UNITS
4. INTAKE'
2. EFFLUENT
(specify if blank)
(optional
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
a. MAXIMUM DAILY VALUE
(ifavailable)
(ifavailable)
d. NO. OF
a. CONCEN-
AVERAGE VALUE
b. NO. OF
CONCENTRATION
(2) MASS
1
CONCENTRATION
(2) MASS
(1) CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS
1. POLLUTANT
ANALYSES
TRATION
b. MASS
ANALYSES
a. Biochemical Oxygen
0.48
12.6
1
mg/1
lbs.
Demand (BOD)
b. Chemical Oxygen
48
1257
1
mg/1
lbs.
Demand (COD)
c. Total Organic Carbon
3.93
102.9
1
mg/1
lbs.
(TOC)
d: Total Suspended
4
105
1
mg/1
lbs.
Solids (TSS)
e. Ammonia (as IV)
VALUE
VALUE
VALUE
VALUE
f. Flow
3.14 avg .
MGD.
g. Temperature
VALUE
VALUE
VALUEC
1
°
VALUE
(winter)
33.G
h. Temperature
V(%LUE
VALUE
VALUEC
1
°
VALUE
(summer)
48.G
i. pH
MINIMUM
G.8
MAXIMUM
7.3
MINIMUM
MAXIMUM
3
STANDARD UNITS
PART B — Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent If you mark column 2a for any pollutant which Is limited either
directly, or indirectly but expressly, in an effluent limitations guideline, you•must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide
quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. '
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG. VALUE
a. LONG TERM AVERAGE
AND
a
b_
a. MAXIMUM DAILY VALUE
(ifavailable)
(ifavailable)
d. NO. OF
a. CONCEN-
VALUE
b. NO. OF
(1)
CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS-
(1)
CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS
CAS NO.
(ifavailable)
BELIEVED
PRESENT
BELIEVED
ABSENT
ANALYSES
TRATION
b. MASS
ANALYSES
a. Bromide
0.046
1.2
1
mg/1
lbs.
(24959-67-9)
b. Chlorine, Total
0
Residual
c. Color
X
58 C.U.
1
d. Fecal Coliform
x
2col/100ml
1
e. Fluoride
X
1.05
1
mg/1
lbs.
(16984-48-8)
.040
f. Nitrate -Nitrite
2.6
1
mg/1
lbs.
(as M
.10
EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE

ITFIIA %/-R r`r\AITIAII Mn PPMA CRr1AIT
EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optionai)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG. VALUE
a. LONG TERM
AND
a
b,
a. MAXIMUM DAILY VALUE
(ifavailable)
(1favailable)
d. NO. OF
CONCEN-
AVERAGE VALUE
b. NO. OF
(1)
CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS
(1)
CONCENTRATION
(2) MASS
CAS NO.
(ifavailable)
BELIEVED
PRESENT
BELIEVED
ABSENT
ANALYSES
a.
TRATION
b. MASS
ANALYSES
g. Nitrogen,
Total Organic (as
\ /
X
.39
10 .2
1
mg/ 1
lbs.
M
h. Oil and
1
Grease
I. Phosphorus
(as P), Total
u
.107
2.8
1
mg/1
lbs.
(7723-14-0)
j. Radioactivity
(1) Alpha, Total
X
.60
1
pCi/L
(2) Beta, Total
X
1.2
1
pCi/L
(3) Radium,
0.2
1
pCi/L
Total
(4) Radium 226,
0.1
1
pCi/L
Total
k. Sulfate
(asSOa)X
11
288
1
mg/1
lbs.
(14808-79-8)
' `
I. Sulfide
�/
x
1
(ass)
m. Sulfite
u
(as SOi)
1
(14265-45-3)
n. Surfactants
X
.129
3.4
1
mg/1
lbs.
o. Aluminum,
Total
.210
5.5
1
mg/1
lbs.
(7429-90-5)
p. Barium, Total
x
1
mg/1
lbs.
(7440-39-3)
.024
.63
q. Boron, Total
1
(7440-42-8)
r. Cobalt, Total
(7440-4813)
S. Iron, Total
320
8.4
1
mg/1
lbs.
(7439-89-6)
t. Magnesium,
Total
3.04
79.6
1
mg/1
lbs.
(7439-9513)
u. Molybdenum,
Total
u
1
(7439-98-7)
v. Manganese,
Total
.091
2.4
1
mg/1
lbs.
(7439-96-5)
w. Tin, Total
1
(7440-31-5)
x. Titanium,
Total
X
1
(7440-32-6)
EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D. NUMBER (copyfiom Item 1 of Form I) JOUTFALLNUMBER
MWINIIFII.FRnM PAr;F 3 nF FnRM 9-C I NCDO44737807 I 002
PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and nonrequired GC/MS
fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must
provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2 -methyl -4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you. discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for
additional details and requirements.
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1: POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONGTERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
b. NO. OF
(1)
CONCENTRATION
(2) MASS
(�)
CONCENTRATION
(2) MASS
(1)
CONCENTRATION (2) MASS
(1)
CONCENTRATION
(2) MASS
CAS NUMBERTESTING
(ifavailable)
REQUIRED
BELIEVED
PRESENT
BELIEVED
ABSENT
d. NO. OF
ANALYSES
a. CONCEN-
TRATION
b. MASS
ANALYSES
METALS, CYANIDE, AND TOTAL PHENOLS
1M. Antimony, Total
1
(7440-36-0)
2M. Arsenic, Total
1
(7440-38-2)
3M. Beryllium, Total
1
(7440-41-7)
4M. Cadmium, Total�/
X
u
003
.008
1
mg/1
lbs.
(7440113-9)
5M. Chromium,
\/
X
�/
X
1
Total (7440-47-3)
6M. Copper, Total\/
X
�/
.003
.008
1
mg/1
lbs.
(7440-50-8)
7M. Lead, Total
�/
1
(7439-92-1)
X\
8M. Mercury, Total
2.52
66
1
rig/1
lbs.
(7439-97-8)
9M. Nickel, Total
�/
X
u
1
(7440-02-0)
10M. Selenium,
�/
X
1
Total (7782119-2)
11 M. Silver, Total
1
(7440-22-4)
12M. Thallium,
�/
X
�/
X
1
Total (7440-28-0)
13M. Zinc, Total
1
(7440-66-6)
14M. Cyanide,
1
Total (57-12-5)
15M. Phenols,v
, 046
1.2
1
mg/1
lbs.
Total
DIOXIN
2,3,7,8 -Tetra-
[DESCRIBE RESULTS Non Detected
-
chlorodibenzo-PX
X
Dioxin (1764-01-6)
EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE

we] 04Ifrtalll0.l:1Kelky,arlala:Z.kill
EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V-5
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (oprionan
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE I
(ifavailable)
I
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
1
1
1
1
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION (2) MASS
CONCENTRATION (2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATI IN
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —VOLATILE COMPOUNDS
1V.Accrolein
1
(107-02-8)
2V. Acrylonitrile
\/
x
�/
x
1
(107-13-1)
Benzene
X
X
1
(71
(71.43-2)
4V. Bis (Chloro-
methyl) Ether
X
X
1
(542-88-1)
5V. Bromoform
1
(75-25-2)
6V. Carbon
Tetrachloride
X
x
1
(56-23-5)
7V. Chlorobenzene
�/
x
1
(108-90-7)
8V. Chlorodi-
bromomethane
x1
(124-48-1)
/X\
9V. Chloroethane
�/
1
(75-00-3)
^
10V. 2-Chloro-
ethylvinyl Ether
x
X
1
(110-75-8)
11 V. Chloroform
\/
1
(67-66-3)
x\
12V. Dichloro-
bromomethane
1
(75-27-4)
\
13V. Dichloro-
difluoromethane
X
x
1
(75-71-8)
14V.1,1-Dichloro-
1
ethane (75-34-3)
15V.1,2-Dichloro-
1
ethane (107-06-2)
16V.1,1-Dichloro-
\/
1
ethylene (75-354)
x\
17V.1,2-Dichloro-
x
x
1
propane (78-87-5)
18V.1,3-Dichloro-
propylene
\ /
X
\ /
X
1
(542-75-6)
19V. Ethylbenzene
1
(100=41-4)
20V. Methyl
\/
x
�/
x
1
Bromide (74-83-9)
_T
21V. Methyl
u
u
1
Chloride (74-87-3)
EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V-5

CC)NTINt1Ft7 FROM PAC F: V.4
EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional) '
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION—VOLATILE COMPOUNDS (continued)
22V. Methylene
1
Chloride (75-09-2)
23V. 1,1,2,2-
Tetrachloroethane
X
X
-
1
79-345
24V. Tetrachloro-
ethylene (127-18-4)
25V. Toluene
1
(108-88-3)
26V.Moro thylen
Dichloroethylene
` '
X
` /
X
1
156-60-5
27V.1,1,1-Trichloro-
X
x\/
1
ethane (71-55-6)
�\
28V.1,1,2-Trichloro-
X
1
ethane (79-00-5)
/�
29V Trichloro-
ethylene (79-01-6)
30V. Trichloro-
`\fluoromethane X
-
1
75-69�
/X\
31V. Vinyl Chloride
x1
(75-01-4)
GC/MS FRACTION —ACID COMPOUNDS
1A.2 -Chlorophenol
x1
(95-57-8)
2A 2,4-Dichloro-
�/
1
phenol(120-83-2)
x\
3A.2,4 -Dimethyl-
,4-Dimethyl-phenol(105-67-9)
phenol (105-67-9)
4A.4,6-Dinitro-0-
1
Cresol (53452-1)
5A.2,4-Dinitro-
�/
x
�/
x
1
phenol (51-28-5)
6A.2-Nitrophenol
1
(88-75-5)
7A.4-Nitrophenoi
�/
1
(100-02-7)
x\
8A. P -Chloro -M-
�/
1
Cresol (59-50-7)
x\
9A. Pentachloro-
phenol (87-86-5)
/�
10A. Phenol
1
(108-95-2)
1IA. 2,4,6-Trichloro-
X
1
phenol (88-05-2)
EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optionan
1. POLLUTANT
b. MAXIMUM 30 DAY'VALUE
c. LONG TERM AVRG.
a. LONGTERM
AND
a.
a. MAXIMUM DAILY VALUE
(ifavallable)
VALUE (favailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(i)
(1)
available
Cf )
REQUIRED
PRESENT
ABSENT
CONCENTRATION (2) MASS
CONCENTRATION (2) MASS
CONCENTRATION (2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASEINEUTRAL COMPOUNDS
I B. Acenaphthene
x
1
(83-32=9)
2B. Acenaphtylene
1
(208-96-8)
3B. Anthracene
x
1
(120-12-7)
4B. Benzidine
v
x
�/
x
1
(92-87-5)
5B. Benzo (a)
Anthracene
�/
x
X x
1
(56-55-3)
6B. Benzo (a)
�/
x
�/
x
1
Pyrene (50-32-8)
7B. 3,4-Benzo-
fluoranthene
X
1
(205-99-2)
8B. Benzo (ghi)
�/
x
1
Perylene (191-24-2)
9B. Benzo (k)
Fluoranthene
X
1
(207 -OB -9)
10B. Bis (2 -Chloro -
ethoxy) Methane
x
1
(111-91-1)
11 B. Bis (2 -Chloro -
ethyl) Ether
x
1
(111-44-4)
12B. Bis (2-
Chloroisopropyo
1
Ether (102-80-1)
13B. Bis (2 -Ethyl -
hexyl) Phthalate
1
(117-81-7)
14B. 4-Bromophenyl
Phenyl Ether
X x
1
(101-55-3)
'15B. Butyl Benzyl�/
x
1
Phthalate (85-68-7)
16B. 2 -Chloro -
naphthalene
x
1
(91-58-7)
17B. 4 -Chloro -
phenyl Phenyl Ether
�/
x
�/
x
1
(7005-72-3)
18B. Chrysene
�/
x
�/
x
1
(218-01-9)
19B. Dibenzo (ah)
Anthracene
�/
x
�/
x
1
(53-70-3)
POB. 1,2-Dichloro-
�/
x
1
benzene (95-50-1)
216.1,3 -Di -chloro-
�/
x
�/
x
1
benzene (541-73-1)
EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
AND
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
CAS NUMBER
a.
TESTING
b.
BELIEVED
C.
BELIEVED
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
d. NO. OF
a. aONCEN-
AVERAGE VALUE
b. NO. OF
(1)
(1)
(1)
(ijava!lable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
T
MASS
(1)
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued)
22B. 1,4-Dichloro-
x
1
benzene(106-46-7)
23B.3,3-Dichloro-
�/
1
benzidine (91-94-1)
^
24B. Diethyl
x
x
Phthalate (84-66-2)
1
25B. Dimethyl
Phthalate
x
x
1
(131-11-3)
Butyl
x
x
Z
Phth26B.alate
Phthalate (84-74-2)
late
276.2,4-Dinitro-
x
x
1
toluene (121-14-2)
x
x
1
toluene (606-20-2)
toluen (606 20-
�\
296. actyl
x
x
1
Phthalate (I (117 -84Q)
30B. 1,2 -Diphenyl -
zo-
hydrazine (as Azo-
x
x
1
benzene)
benzene)(122-66-7)
31B. Fluoranthene
x
1
(206114-0)
3287 Fuorene
x
x
1
(86-73--7)
33B. Hexachloro-
x
x
1
benzene'(118-74-1)
34B. Hexachloro-
x
x
1
butadiene (87-68-3)
Hexachloro-
cyclopentadiene
cycl
x
x
1
(77117-4)
36B Hexachloro-
x
x
1
ethane (67-72-1)
37B.Indeno
(1,2,3 -cd) Pyrene
x
x
1
(193-39-5)
38B. Isophorone •
x
x
1
(78-59-1)
39B. Naphthalene
x
1
(91-20-3)
40B. Nitrobenzene
x
1
(98-95-3)
41 B. N-Nitro-
sodimethylamine
x
x
1
(62-75-9)
42B. N-Nitrosodi-
N-Propylamine
x
x
1
(621-64-7)
EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optionan
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
c
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
available .
if )
REQUIRED
PRESENT
ABSENT
CONCENTRATION (2) MASS
CONCENTRATION (2) MASS
CONCENTRATION (2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued)
43B. N-Nitro-
sodiphenylamine
1
(86-30-6)
44B. Phenanthrene
\/
x
1
(85-01-8)
45B.Pyrene
X
X
1
(129
(129-00-0)
46B. 1,2,4-Tri-
chlorobenzene
�/
x
1
(120-82-1)
GC/MS FRACTION — PESTICIDES
Aldrin
X
1
(30
(309-00-2)
BHC
x4-6)
X
1
(319-8-8
(31
/\
3P. D -BHC
x
x
1
(319-85-7)
4P.y-BHC
X
X
1
(58-89-9) 9-9)
I
5P. S -BHC
X
X
1
.
(319-86-8)
6P. Chlordane
\/
x
1
(57-74-9)
7P.4,4' -DDT
X
X
1
(50-29-3)
x
x
1
(72-55-9)
9P.4,4' -DDD
1
(72-54-8)
Dieldrin
x
x
_
1
(60-
(60-57-1)
�\
�\
11 P. a-Enosulfan
\/
x
�/
x
1
(115-29-7)
12P. p-Endosulfan
�/
x
1
(115-29-7)
Endosulfan
Sulfate
X
1
(1031-07-8)
Endrin
x
x
1
(72-
(72_20.8)
^
yndrin
Aldeldeh de
1
(7421-93-4)
16P. Heptachlor
�/
x
�/
x
1
(76-04-8)
EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9

EPA I.D. NUMBER (copyfi•omItem 1 of Form 1) OUTFALL NUMBER
NCD044737807 001
CONTINUED FROM PAGE V-8
EPA Form 3510-2C (8-90) PAGE V-9
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (if'available)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — PESTICIDES (continued)
17P. Heptachlor
E oxide
` ,
X
` ,
X
1
(1024-57-3)
18P. PCB -1242
1
(53469-21-9)
19P. PCB -1254
\/
x
x\/
1
(11097-69-1)
20P. PCB -1221
x
1
(11104-28-2)
21 PCB -1232
X
1
(11141-16-5)
2226 PCB -1248
x
X
1
'
(12672-29-6)
/�
23P.PCB
X
\�
1
(110
(11096-82-5)-5)
�\
2426 PCB -1016
1
(12674-11-2)1-2)
2001-35-2)
X
-
1
(8001-35-2)
EPA Form 3510-2C (8-90) PAGE V-9

PRIORITY POLLUTANT RESULTS
FLOW TO RIVER
001

Meritech, Inc.
Environmental Laboratory
N t Laboratory Certification No, 165
�^ ='•'fes" -
?'r
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd,
Roanoke Rapids, NC 27870
Report Date:
Date Sample Rcvd:
.
Page 1
7/11/16
6/21/16
Meritech Work Order #
06211693 Sample: Flow to River Composite
6/20-21/16
Parameters
Result
Analysis Date Reporting Limit
Metho
COD
144 ing/L
6/24/16
15 mg/L
EPA 410.4
Chloride
16.0 nig/L
.6/22/16
0.10 ing/L
SM 4500 Cl B
Fluoride
0,182 mg/L
6/22/16
0.1 mg/L
SM 4500FC
Color
336 C.U.
6/22/16
-
SM 2120E
Ml BAS
1.98 mg/L
6/22/16
0,10 nig/L
SM 5540C
Ammonia, Nitrogen
1.3 ing/L
7/5/16
0,1 mg/L
EPA 350.1
TKN
2.73 mg/L
6/24/16
0,20 nig/L
EPA 351.1
Nitrate/Nitrite Nitrogen
0,37 nig/L
6/22/16
0.10 mg/L
EPA 353.2
Nitrogen, total
3.10 nig/L
7/5/16
0.20 mg/L
EPA 353.2
Sulfate
1,860 mg/L
6/22/16
5 nig/L
SM 426C
Sulfite
<10 mg/L
6/22/16
10 nig/L
SM 450OS03B
Aluminum, total
0.411 mg/L
6/24/16
0.010 nig/L
EPA 200.7
Antimony, total
<0,025 mg/L
6/24/16
0.025 ing/L
EPA 200.7
-Arsenic, total
<0,010 mg/L
6/24/16
0.010 ing/L
EPA 200.7
Barium, total
0,106 nig/L
6/24/16
0.005 mg/L
EPA 200.7
Beryllium, total
<0,005 nig/L
6/24/16
0,005 ing/L
EPA 200.7
Boron, total
0.083 mg/L
6/24/16
0.050 nig/L
EPA 200,7
Cadmium, total
0.004 nig/L
6/24/16
0.002 mg/L
EPA 200.7
Chromium, total
<0,005 nig/L
6/24/16
0,005 nig/L
EPA 200.7
Cobalt, total
<0.005 nig/L
6/24/16
0.005 mg/L
EPA 200.7
Copper, total
0.011 mg/L
6/24/16
0,002 mg/L
EPA 200.7
11-011, total
0,177 nig/L
6/24/16
0,025 nig/L
EPA 200.7
Lead, total
<0,010 mg/L
6/24/16
0.010 ing/L
EPA 200.7
Magnesium, total
6.24 nig/L
7/7/16
0,100 nig/L
EPA 200.7
Manganese, total
0,548 mg/L
6/24/16
0.005 mg/L
EPA 200,7
Mercury, total
<0.0002 nig/L
6/23/16
0.0002 nig/L
EPA 245.1
Molybdenum, total
<0,005 nig/L
6/24/16
0.005 nig/L
EPA 200.7,
Nickel, total
0,012 mg/L
6/24/16
0,010 nig/L
EPA 200.7
Phosphorous, total
0,228 mg/l,
6/24/16
0,020 nig/L
EPA 200,7
Selenium, total
<0,010 ing/L
6/24/16
0.010 mg/L
EPA 200.7
Silver, total .
<0,005 ing/L
6/24/16
0.005 nig/L
EPA 200.7
Thallium, total
<0,020 mg/L .
6/24/16
0,020 nig/L
EPA 200.7
Tin, total
<0.025 mg/L
6/24/16
0,025 nig/L
EPA 200.7
Titanium, total
<0,005 mg/L
6/24/16
0.005 nig/L
EPA 200.7
Zinc, total
<0.010 nig/l,
6/24/16
0.010 mg/L'
EPA 200.7
TOC
14.5 mg/L
6/23/16
2 nig/L
SM 5310C
Sulfide
<0,10 nig/L
6/22/16
0,10 ing/L
SM 4500 SD
EPA 625 BNA
Attached
7/5/16
642 Tamco Road, Reidsville, North Carolina 27320
teI.[phone] fm(336)342-1522

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
im
Page 2
Contact: Neal Davis Report Date: 7/11/16
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870 Date Sample Rcvd: 6/21/16
Meritech Work Order # 06211694 Sample: Flow to River Grab 6/21/16
Parameters,
Result
Analysis Date
,Reporting Limit Method
Cyanide, total
<0.005 mg/L'
6/24/16
0.005 mg/L. EPA 335.4
Oil & Grease (HEM)
<5 nig/L
6/23/16
5 mg/L EPA 1664A
Phenols, total
0.039 mg/L
6/22/16.
0.010 mg/L EPA 420.1
EPA 608
Attached
6/25/16
- -
EPA 624
Attached
6/22/16
- -
* Fecal Coliform was resampled on 6/23/16
1 hereby certify that 1 have reviewed and approve these data.
f.
. I ve d1l
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

MERITECH,
INC,
Environmental Laboratories
1 Laboratory Certificate ##165
Client:
Kapstone Kraft Paper Co.
Meriteclt ID#:
-06211693
Project:
625
Analysis:
07/05/16
Client Santple ID:
Flow to River
Extraction:
06/21/16
Sample Collection:
06/21/16
Analyst:
PM
Benzidine
< 50 ug/L
Dilution Factor.:
I
LPA 625 SLMI'VOLATILL ORGANICS
Parameter
Result
Parameter
Result
Acenaplithene
< 10 ug/L
Fluoranthene
< 10 ug/L.
Acenaphthylene
< 10 ug/L
Fhtorene
< 10 ug/L
Anthracene
< 10 ug/L
Hexachlorobenzene
< 10 ug/L
Benzidine
< 50 ug/L
Hexachlorobutadiene
< 10 ug/L
Benzo(a)atitbracene
< 10 ug/L
1•lexachlorocyclopentadiene
< 50 ug/L
Beilzo(a)pyrene
< 10 ug/L
Hexachloroethane
< 10 ug/L
Benzo(b)fluoranthene
< 10 ug/L
lndeno(1,2,3-cd)pyrene
< 10 ug/L
Benzo(k)fluoranthene
< 10 ug/L
Isophorone
< 10 ug/L
Benzo(g,h,i)perylene
< 10 ug/L
2-tNethy1naphthalene
< 10 ug/L
Benzyl butyl plithalate
< 10 ug/L
Naphthalene
< 10 ug/L
Bis(2-chloroetltoxy)methane
< 10 ug/L
Nitrobenzene
< 10 ug/L
Bis(2-clrloroethyl)ether
< 10 ugiL
\i-Nitrosodimethylatnine
< 10 ug/L
Bis(2-chloroisopropyl)ether
< 10 ug/L
N-Nitrosodi-n-propylamitie
< 10 ug/L
Bis(2-ethylhexyl)phthalate
< 10 ug/L
\r-Nitrosodiphenylan lne
< 10 ug/L
4-13romoplienyl phenyl ether
< 10 ug/L
Phenanthrene
< 10 ug/L
2-Cliloronaphtlialene
< 10 ug/L
Pyrene
< 10 ug/L
4-Chlorophenylphenylether
< 10 ug/L
1,2,4-Trichlorobenzene
< 10 ug/L
Chrysene
< 10 ug/L
Dibenzo(a,h)atithracene
< 10 ugiL
4-Chloro-3•anethylphenol
< 10 ug/L
1,2 -Dichlorobenzene
< 10 ug/L
2 -Chlorophenol
< 10 lig/1'
1,3 -Dichlorobenzene
< 10 ug/L,
2,4-Dichloroplhenol
< 10 ug/L
1,4 -Dichlorobenzene
< 10 ug/L
2,4 -Dimethylphenol
< 10 ug/L
3,T-Dichlorobenzidine
< 50 ug/L
2,4-Dinitrophenol
< 50 ug/L
Diethyl phthalate
< 10 ug/L
4,6-Dinitro-2-rnethylphenol
< 50 ug/L
Dimethyl phthalate
< 10 ug/L
2-Nitrophenol
< 10 ag/L
Di -n -butyl phthalate
< 10 ug/L
4-Nitroplletlol
< 50 Ug/l.,
2,4-Dinitrotoluene
< 10 ug/L
Pentachlorophenol,
< 50 ug/L
2,6-Dinitrotoluene
< 10 ug/L
Plienol
< 10 ug/L
Di-n-octyl phthalate
< 10 ug/L
2,4,6 -Trichlorophenol
< 10 ug/L
1,2-Diplienyilrydrazine
< 10 ug/L
1 hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 T'amco Road * Reidsville, NC 27320
[phone] Ph * [phone] Fax

r
MERITECIt INC.
ENVIRONMENTAL LABORATORIES
- Laboratory Certification No. 165
. Ff
Client: Kapstone Paper & Packaging Merl -tech Work Order #:
Project: 608 / PCB
Client Sample: ' Flow to River Grab Analysis:
Sample Collection; 06/21/2016 Analyst:
EPA 608 e Organochlorine Pesticides
Parameter
Result
Delta - BHC
< 0.001 mg/L
4,4' --DDE
< 0.001 mg/L
4,4' -DDT
< 0.001 mg/L
Aldrin
< 0.001 mg/L
Alpha - BHC
.< 0.001 mg/L
Alpha Endosulfan I
< 0.001 mg/L
Beta - BHC
< 0.001 mg/L
4,4' -DDD
< 0.001 mg/L
Chlordane
< 0.010 mg/L
Toxaphene
< 0.020 mg/L
Dieldrin
< 0.001 mg/L
Endosulfan Sulfate
< 0.001 mg/L
Endrin
< 0.001 mg/L
Endrin Aldehyde
< .0.001 mg/L
Gamma - BHC.
< 0.001 mg/L
Heptachlor
< 0.001 mg/L
Heptachlor Epoxide
< 0.001 mg/L
Beta - Endosulfan II
< 0.001 mg/L
Methoxychlor
< 0.001 mg/L
PCB — 1016
< 0.005 mg/L
PCB — 1221
< 0.005 mg/L
PCB —1232
< 0.005 mg/L
PCB — 1242
< 0.005 mg/L
PCB —1254
< 0.005 mg/L
PCB =1260
< 0.005 mg/L
06211693
06/25/2016
R&A
J
I hereby certify that I have revimed and approve these data. fit
Laboratory Representative
642 Tamco- Road * Reidsville, NC 27320
[phone] Ph * [phone] Fax

Report Date: 06/23/16
EPA 624 VOLATILE ORGANICS
Parameter
Benzene
Dichlorobromomethane
Bromoform
Methyl Bromide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
2-Cliloroethyl vinyl ether.
Chloroform
Methyl Chloride
Chlorodi bromornethane
1,2-Dibromoethane
1,1-Dichloroetliane
1,2-Dichloroethane
1,4 -Dichlorobenzene .
1,2 -Dichlorobenzene
1,3 -Dichlorobenzene
1,1 -Diehl oroethylene
trans-1,2-Dichloroethylene
1,2-Dichloropropane
cis-1,3-Dichloropropylene
trans- l,3-Dich loropropylene
Ethyl benzene
Methylene chloride
1,1,2,2 -Tetrachloroethane
Tetrachloroethylene
Toluene
1,1,1 -Trichloroethane
1,1,2 -Trichloroethane
Trichloroethylene
Trichlorofluoromethane
Vinyl chloride
Additional Comuounds
Acrolein
Acrylonitrile
1 hereby certify that 1 have reviewed and approve these data.
Result
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 50.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 50.0 ug/L
< 50.0 ug/L
< 10.0 ug/L
< 50.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10,0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10,0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10,0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 50.0 ug/L
< 50.0 ug/L
< 500 ug/L
< 100 ug/L
Laboratory Representative
642 Tamco Road * Reidsville', NC 27320
[phone] Ph * [phone] Fax
MERITECH, INC.
Environmental Laboratories
{
Laboratory Certification #165
Client:
Kapstone Kraft Paper Co. Meritech ID#: 0621 1694
Project:
Priority Pollutant Analysis Analysis: 06/22/16
Client Sample ID:
Flow to River Analyst: V W`V
Sample Collection:
06/21/16 Dilution Factor: 10
Report Date: 06/23/16
EPA 624 VOLATILE ORGANICS
Parameter
Benzene
Dichlorobromomethane
Bromoform
Methyl Bromide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
2-Cliloroethyl vinyl ether.
Chloroform
Methyl Chloride
Chlorodi bromornethane
1,2-Dibromoethane
1,1-Dichloroetliane
1,2-Dichloroethane
1,4 -Dichlorobenzene .
1,2 -Dichlorobenzene
1,3 -Dichlorobenzene
1,1 -Diehl oroethylene
trans-1,2-Dichloroethylene
1,2-Dichloropropane
cis-1,3-Dichloropropylene
trans- l,3-Dich loropropylene
Ethyl benzene
Methylene chloride
1,1,2,2 -Tetrachloroethane
Tetrachloroethylene
Toluene
1,1,1 -Trichloroethane
1,1,2 -Trichloroethane
Trichloroethylene
Trichlorofluoromethane
Vinyl chloride
Additional Comuounds
Acrolein
Acrylonitrile
1 hereby certify that 1 have reviewed and approve these data.
Result
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 50.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 50.0 ug/L
< 50.0 ug/L
< 10.0 ug/L
< 50.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10,0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10,0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10,0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 10.0 ug/L
< 50.0 ug/L
< 50.0 ug/L
< 500 ug/L
< 100 ug/L
Laboratory Representative
642 Tamco Road * Reidsville', NC 27320
[phone] Ph * [phone] Fax

3-:0-2033
Chain of Custody Record (COC)
NPDES#: Alc* coo '? 5a
Client: AIAZ722-6-r- °cA1= int /�_� Phone:0•jo?-S'23 -40C?��
F"ITEC � ��
�
Address: Fax: o d -' _
.33 — 6/ SL( S
"�
ENVIRONMENTAL LABORATORIES
,, /
o�}�y(�/lE=,alb t , 9l� Email:
— tit_
/�r�i�
:~
642TamcoRd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
Attention: /Zz 01;tv; t
Turn Around Time*
www.merltech-labs.com
How would you like your report sent? "RUSH work needs prior approval.
Circle all that apply. Email Std 2
(preferred), Fax, ail
s) 3-5 Das 24-48Hrs
Sampling Dates & Times
Person T kings ple (Sign/Print):'•""
:Use.-Oril'
Sample Location
and/or ID #
Comp?
#of
Test(s) Required
-
OnJce?.
<pH'-O:IC?;
start End
Date Time Date Time
J •' -'/', � �i
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' ec
Method of
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
_
Shipment:
Comments:
2r, r
-
S ��[ �JtC•� u-=
Os U PS
i
t'
Fed EX
Are these results for regulatory purposes? Yes
Al No Qx Report results in: Q
mg/t mg/kg u L
` g/ g g/
Hand Delivery
Relinquisheds.! G/ .`Jf,
R ivy.� ' Date:,
ime1:)Z
Time:
L Other
Re[ ui e y 6n pate
Time: i Received by: Date:
1641
Time -
Relinquished by: Date:
Time: Re ived by ofine�
i
J;-- v

Client:
Attention
MERITECH,
INC.
ENVIRONMENTAL LABORATORIES
Laboratory Certification No. 165
Kapstone Kraft Paper Corp,
100 Gaston Road
Roanoke Rapids, NC 27870
Neal Davis
Date Sampled 06/21/16
Digested 06/22/16
Analysis 07/01/16
Analyst: CWL
EPA 1631 Low Level Mercury Anal
Meritech 1D # Sample 1D ReSUlt Reporting Limit
MBLK0517BB Method Blank < 0.5 ng/L 0.5 ng/L
M06221603
Field Blank 2.09 ng/L 1.0 ng/L
11.206221604 Flow / River 15.1 ng/L 1.0 ng/L
I hereby certifj, that 1 have reviewed and approve these data.
0.41
Laboratory Representative
642 Tamco Rd - PO Box 27 - Reidsville, NC 27320
[phone] Ph - [phone] Fax
E -Mail: [e-mail]-

DA
3-20-2013 Chain of Custody -Record (COC)
J
Client:
NPDES#: 11:_
Phone: L-": X
/2
Address:-
Fax:ys /� 4,
MER1TE(.,4H. INC.
ENVIRONMENTAL LABORATORIES
Erna il:
642 Tamco Rd. Phone: [phone]
Project- Z'
P.O.#:
Reidsville NC 27320 Fax: [phone]
How would you like your Report sent? ­
Email: info@ meritech-labs.comAttention:
Circle all that apply: ,/6;`aiI'(preferred), FaX/'Maif
WWW.ME)ritech-labs.comerson
Taking Sample (Sign/Print); 1 /.1 e�z AZ 5
EPA 1631
Sample Location /!D#
Date
Time
Sampling Site Description
1-56ttfei
JTubing
Lot:'#
Field Blank
0,
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":X
:.J "J
'N
J I+."'
:R:!
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..... ..... .. .
V
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Method of
Comments:
Shipment:
Q. UPS
Fed Ex
Are these results for regulatory purposes? Yes No El.
Hand DeliveryJz-
Relinquished b Da.�e: Time;
R eiy 'by: Date: Time:
Other
R:l ;e. Time:
Received by; Date; Time:
16Y.
Relinquished by: Date: Time:
Received by Lab;_1Dat Time:
ReGiWed trom Lab Secure Area
0601

°Radlologrcal Analysts,
- None,Ey,�flimcritegcnmusY6asiiyplfeafaampIIanxeeatf : _
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4006
456
6.67 pCi/L.
20.1 PCf/L
4010
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— _ —
4026
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448
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AN DrMi
LaboratoryLog#: _ r 0 t oZ —Iir. Cerbfted by: iN9ke Naumann J
Cornments:
j.aboratarv.�rEw 2� � .
vublic WaterSu" s6cuon, Attm.Da4a 6istry;1634 Nlml SetvEt 6w tar, Raloigb;Nc t?699-1634'
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Cornments:
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5.9401fi Chain of Custody Record (COC)
NPDES#•�
Tient: APSOV��r ,Yc2-�,le2 �� Phone: c?�S� 5.3.E
MERITECH INC.
Address: 'Izo L�a4<7?-W- A) Fax: — S32 '• �& S
ENVIRONMENTAL LABORATORIES
Email:/..., o/$al
i; 642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention:_ �` r ,/'gU/S Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
WWW.Meritechlabs.coi1i
s �2448Hrsa(preferred), m
Sampling Dates & Times
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Lab Use Only
Sample Location and/or ID #
Start
End
comp?
Grab?
#ofon
Cont.
Test(s) Required ')
Ice?.Yes
pH OK?
Date
Time
Date
Time
iU
/ No
Cl OK?
�- io
Temperature Upon Receipt:
Method Of
*** Dechlorination (<0.5 ppm) of Ammonia, cyanide, Phenol and TKN samples must be done in the field prior to preservation. ***
Comments: —
Compositor #
Shipment:
UPS
Jug #
til
tel; d Ex
Are these results or regulatory purposes? Yes ONo
Report results in: m L m k ' u L
p g/ g
g/ g/
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Relinquished by: . D te:/ Time:
Received a • Time:
_• �. Y_
Other
Relinqui d by: ate Time: /
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Received Y Date: Time:
Relinquished Date: Time:
Rec L D TlmerLt T��A,
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Meritech; Inc.
:.4 Environmental Laboratory
Laboratory Certification No. 165
8
Contact: Neal Davis Report Date: 6/30/2016
Client: Kapstone Paper & Packaging NPDES#:. WQ0O21577
100 Gaston Rd. WQ0O00436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 6/23/2016
Meritech Work Order # 062316104 Sample: WW Flow/River Grab 6/23/16
Parameters Results Analysis Date Reporting Limit Method
Fecal Coliform 2 col/100 ml 6/23/16 1 col/100 ml' SM 9222 D
Meritech Work Order # 062316105 Sample: B&C Colling Water Grab 6/23/16
Parameters Results Analysis Date Reporting Limit Method
Fecal Coliform 2 col/100 ml 6/23/16 1 col/100 ml SM 9222 D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3-:0-20Chain of Custody Record (COC)
NPDES#: &-c- 00r)n ?52
Client: �� .sr,,;•� �P�GI'%•�ncz �o% Phone:� �d%s
Address: /GC 4r/�ie � -) Fax: �?� �' Ch
l�G.9�U0/Yc� � �/r✓s Al Email: lllxY . 1�.4ii�s Cd ig04'70W-L.4SO,
?�7d Project:
Attention:Al[ nc ,4, Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Hrs
Circle all that apply: mai,(preferred), Fax, Mail•: Std 0 a s) 33 S Days 214-4 1
��
•E�.�T'EC� INC.
•
ENVIRONMENTAL LABORATORIES
" 642 TamcoRd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritech=labs.com
Sample Location and/or ID #
Sampling Dates &Times
Person Taking Sample ign/Pr t):
�,7
Lab Use Only
Start
End
comp?
Grab?
#ofOn
cont.
Test(s) Req U 0 red
ice?
es No
pH OK?
CI OK?
Date
Time
Date
Time
-
Temperature Upon
Receipt—
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be -done in the field prior to preservation. ***
Comments:
Compositor #
Jug #
UPS
Fed EX
Are these restil for regulatory purposes? Yes r N Ck
Report results in: mg/Lmg/kg, ug/L-
•Hand Delivery
Relinquished Da : Ti
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R DateTirge:
•� ' ' �+
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Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Neal Davis Report Date: 8/24/2016
Client: Kapstone Paper & Packaging NPDES#: NCSO00106
100 Gaston Rd.
Roanoke Rapids, NC 27870 Date Sample Rcvd: 8/3/2016
Meritech Work Order # 080316143 Sample: Flow to River Grab 8/3/16
Parameters Results Analysis Date Reporting Limit Method
Bromidejotal 0.092 mg/L 8/12/16 0.020 mg/L EPA 200.7
Dioxin, 2378- TCDD Not Detected 8/18/16 1.01 pg/L EPA 1613B
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco-Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

1`�
Chain of Custody Record (COC)
NPDES#:
Client: s3�%F�� "�.�f�r'.�'� Lo�1 Phone: 07<�2
Address, 110 4oM- / �J� Fax:_ )r5-,2 — :r3g
lr
.��/.�'df�N /��i�S. � Email:�l�
Project:
P.O.#:
Turn Around Time*
Attention: �
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: Emaill(pret�arredl ax, Nlai�l � Std a s) Davs 24
a AYi ITEC C
ENVIRONMENTAL LABORATORIES
�
i, 642 Tamco Rd. Phone: [phone]
` Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
i/VWW.Meritechiabs.corrl
Sample Location and/or ID #
Sampling Dates $c Times
Person Taking Sample (Sign/Print):
Lab Use Only
Start
End
Comp?
Grab?
# of
Cont.
Test(s) Required ;�
On Ice? Yes
/ No
pH OK?
Cl OK?
Date
Time
Date
Time
/e, J r` Li
ew
Awl
LA
A6 Z1V'
Temperature Upon Receipt:
Method of
Shipment:
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol
and TKN samples must be done in the field priorto preservation-
Comments:
'
Compositor #
Jug #
UPS
• d Ex
Are these results for regulatory purposes? Yes 0 No
Report results in: mg/L mg/k u L
g g/
Hand Delivery
Relinquished by: D te: Time:
iG
Received a Time:
^ r
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to
Received Y= Date: Time:
Relinquished Da—tile: Time:
Rec ' L �D f Time:15
1`�

PRIORITY POLLUTANT RESULTS
NON CONTACT COOLING WATER
��IIN

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Neal Davis
Client: Kapstone Paper & Packaging
100 Gaston Rd.
Roanoke Rapids, NC 27870.
Report Date:
Date Sample Rcvd:
7/11/16
-
6/21/16
Meritech Work Order #
06211692 Sample:
Cooling Water Grab
6/21/16
Parameters
Res ul
Analysis Date
Reporting Limit
Method
COD
48 mg/L
6/24/16
15 mg/L
EPA 410.4
Chloride
8.0 mg/l,
6/22/16
0.10 mg/L
SM 4500 Cl B
Fluoride
0.040 ing/L
6/22/16
0.1 mg/L
SM 4500FC
Color
58 C.U.
6/22/16
-
SM 2120E
MBAS
0.129 mg/L
6/22/16
0.10 mg/L
SM 5540C
Ammonia, Nitrogen
<0.1 mg/L
6/27/16
0.1 mg/L
EPA 350.1
TKN
0.29 mg/L
6/24/16
0.20 mg/L
EPA 351.1
Nitrate/Nitrite Nitrogen
0.10 mg/L
6/23/16
0.10 mg/L
EPA 353.2
Nitrogen, total
0.39 mg/L
6/27/16
0.20 mg/L
EPA 353.2
Sulfate
11 mg/L
6/22/16
5 mg/L
SM 426C
Sulfite
<10 mg/L
6/22/16
10 mg/L
SM 4500S03B
Aluminum, total
0.210 mg/L
6/24/16
0.010 mg/L
EPA 200.7
Antimony, total
<0.025 mg/L
6/24/16
0.025 mg/L
EPA 200.7
Arsenic, total
<0.010 mg/L
6/24/16
0.010 mg/L
EPA 200.7
Barium, total
0.024 mg/L
6/24/16
0.005 ung/L
EPA 200.7
Beryllium, total
<0.005 mg/L
6/24/16
0.005 mg/L
EPA 200.7
Boron, total
<0.050 mg/L
6/24/16
0.050 mg/L
EPA 200.7
Cadmium, total
0.003 mg/L
6/24%16
0.002 mg/L
EPA 200.7
Chromium, total
<0.005 mg/L
6/24/16
0.005 mg/L
EPA 200.7
Cobalt, total
<0.005 mg/L
6/24/16
0.005 mg/L
EPA 200.7
Copper, total
0.003 mg/L
6/24/16
0.002 mg/L
EPA 200.7
Iron, total
0.320 mg/L
6/24/16
0.025 mg/L
EPA 200.7
Lead, total
<0.010 mg/L
6/24/16
0.010 mg/L
EPA 200.7
Magnesium, total
3.04 mg/L
7/7/16
0.100 mg/L
EPA 200.7
Manganese, total
0.091 mg/L
6/24/16
0.005 mg/L
EPA 200.7
Mercury, total
<0.0002 mg/L
6/23/16
0.0002 mg/L
EPA 245.1
Molybdenum, total
<0.005 tng/L
6/24/16
0.005 mg/L
EPA 200.7
Nickel, total
<0.010 mg/L
6/24/16
0.010 rng/L
EPA 200.7
Phosphorous, total
0.107 mg/L
6/24/16
0.020 mg/1,
EPA 200.7
Selenium, total
<0.010 mg/L.
6/24/16
0.010 mg/L
EPA 200.7
Silver, total
<0.005 mg/L
6/24/16
0.005 mg/L
EPA 200.7
Thallium, total
<0.020 mg/L
6/24/16
0.020 mg/L
EPA 200.7
Tin, total
<0.025 mg/L
6/24/16
0.025 mg/L
EPA 200.7
Titanium, total
<0.005 mg/L
6/24/16
0.005 mg/L
EPA 200.7
Zinc, total
<0.010 mg/L
6/24/16
0.010 mg/L
EPA 200.7
Cyanide, total
<0.005 mg/L
6/24/16
0.005 mg/L
EPA 335.4
Oil & Grease (HEM)
<5 mg/L
6/23/16
5 mg/L
EPA 1664A
Phenols, total
0.046 mg/L
6/22/16
0.010 mg/L
EPA 420.1
TOC
3.93 mg/l,
6/23/16
2 nig/l,
SM 5310C
Sulfide
<0.10 mg/L
6/22/16
0.10 mg/L
SM 4500 SD
EPA 608
Attached
6/25/16
-
EPA 624
Attached
6/22/16
-
EPA 625 SNA
Attached
7/5/16
-
-
Fecal Coliform was resaunpled on 6/23/16
1 hereby certify that I have reviewed and approve these data.
LaboratoryRepresen ative
642 Tainco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

MERITECH, INC.,
ENVIRONMENTAL LABORATORIES
Laboratory Certification No. 165
Client: Kapstone Paper & Packaging. Meritech Work Order #: 06211692.
Project: 608 / PCB
Client Sample: Cooling Water Grab Analysis: 06/25/2016
Sample Collection: 06/21/2016 Analyst: R & A
EPA 608 o Ort4anoehlorine Pesticides
Parameter
Result
Delta - BHC
< 0.001 mg/L
4,4' -DDE .
< 0,001 mg/L
4,4' -DDT
< 0.001 mg/L
Aldrin
< 0.001 mg/L
Alpha - BHC
< 0.001 mg/L
Alpha Endosulfan I
< 0.001 mg/L
Beta- BHC
< 0.001 mg/L
4,4' -DDD
< 0.001.mg/L
Chlordane
< 0.010 mg/L
Toxaphene
< 0.020 mg/L
Dieldrin
< 0.001 mg/L
Endosulfan Sulfate
< 0.001 mg/L
Endrin
< 0.001 mg/L
Endrin Aldehyde
< 0,001 mg/L
Gamma - BHC
< 0.001 mg/L
Heptachlor -
< 0.001 mg/L
Heptachlor Epoxide
< 0.001 mg/L
Beta - Endosulfan II
< 0.001 mg/L
Methoxychlor
< 0.001 mg/L
PCB —1016
< 0.005 m,g/L
PCB —1221.
< 0.005 mg/L
PCR —1232
< 0.005 mg/L
PCB —1242
< 0.005 mg/L
PCB —1254
< 0.005 mg/L
PCB —1260
< 0.005 mg/L
11
I hereby certify that I have reviewed and approve these data, .
Laboratory Representative
642 Tamco Road * Reidsville, NC 27320
[phone] Ph.* [phone] Fax

642 Tameo Road * Reidsville, NC 27320
[phone] Ph * [phone] Fax
IRUTIEwCHON INC,
Environmental Laboratories
Laboratory Certification #165
Client:
Kapstone Kraft Paper Co.
Merite.ch ID#: 06211692
Project:
Priority Pollutant Analysis
Analysis: 06/22/16
Client Sample ID:
Cooling Water
Analyst: VWV
Sample Collection:
06/21/16
Dilution Factor: 1
Report Date: 06/23/16
EPA 624 VOLATILE
ORGANICS
Parameter
Result
Benzene
< 1.00 ug/L
Dichlorobromomethane
< 1.00 ug/L
Bromoform
< 1.00 ug/L
Methyl Bromide
< 5.00 ug/L
Carbon Tetrachloride
< 1.00 ug/L
Chlorobenzene
< 1.00 ug/L
Chloroethane
< 5.00 ug/L
2-Chloroethyl vinyl ether
< 5.00 ug/L
Chloroform
< 1.00 ug/L
Methyl Chloride
< 5.00 ug/L
Chi orodibromomethane
< 1.00 ug/L
1,2-Dibromoethane
< 1.00 ug/L
1, 1 -Dichloroethane
< 1.00 ug/L
1,2-Dichloroethane
< 1.00 ug/L
1,4 -Dichlorobenzene
< 1.00 ug/L,
1,2 -Dichlorobenzene
< 1.00 ug/L
1,3 -Dichlorobenzene
< 1.00 ug/L
1,1-Dichloroethylene
< 1.00 ug/L
trans-1,2-Dichloroethylene
< 1.00 ug/L
1,2-Dichloropropane
< 1.00 ug/L,
cis-1,3-Dichloropropylene
< 1.00 ug/L
trans-1,3-Dichloropropylene
< 1.00 ug/L
Ethyl benzene
< 1.00 ug/l,
Methylene chloride
< 1.00 ag/L
1,1,2,2 -Tetrachloroethane
< 1.00 ug/L
Tetrachloroethylene
< 1.00 ug/L
Toluene
< 1.00 ug/L
1,1,1 -Trichloroethane
< 1.00 ug/L
1,1,2 -Trichloroethane
< 1.00 ug/L
Trichloroethylene
< 1.00 ug/L
Trichlorofluoromethane
< 5.00 ug/L
Vinyl chloride
< 5,00 ug/L
Additional Compounds
Acrolein
<50.0 ug/L
Acrylonitrile
<10.0 ug/L
1 hereby certify that
1 have reviewed and approve these data. c/fGrE%�
Laboratory Representative
642 Tameo Road * Reidsville, NC 27320
[phone] Ph * [phone] Fax

MERITECH, INC.
Environmental Laboratories
Laboratory Certificate #165
Client:
Kapstone Kraft Paper Co.
Meritech iD#:
06211692
Project:
625
Analysis:
07/05/16
Client Sample ID:
Cooling Water
Extraction:
06/21/16
Sample Collection:
06/21/16
Analyst:
PM
Benzidine
< 50 ug/L
Dilation Factor:
1
EPA 625 SEMIVOLATILE ORGANICS
Parameter
Result
Parameter
Result
Acenaphthene
< 10 ug/L
Fluoranthene
< 10 ug/L
Acenaphthylene
< 10 ug/L
Fluorene
< 10 ug/L
Anthracene
< 10 ug/L
Hexachlorobenzene
< 10 ug/L
Benzidine
< 50 ug/L
Hexachlorobutadiene
< 10 ug/L
Benzo(a)anthracene
< 10 -ug/L
Hexachlorocyclopentadiene
< 50 ug/L
Benzo(a)pyreue
< 10 ug/L
Hexachloroethane
< 10 ug/L
Benzo(b)fluoranthene
< 10 ug/L
Indeno(1,2,3-cd)pyrene
< 10 ug/L
Benzo(k)tluornnthene
< 10 ug/L
Isophorone
< 10 ug/L
Benzo(g,h,i)perylene
< 10 ug/L
2 -Methylnaphthalene
< 10 ug/L
Benzyl butyl phthalate
< 10 ug/L
Naphthalene
< 10 ug/L
Bis(2-cliloroetltox),)methane
< 10 ug/L
Nitrobenzene
< 10 ug/L
Bis(2-chloraethyl)ether
< 10 ug/L
N-Nitrosodimethylamine
< 10 ug/L
Bis(2-chloroisopropyl)ether
< 10 ug/L
N-Nitrosodi-n-propylamine
< 10 ug/L
B is(2-ethyl hexyl)phth al ate
< 10 ug/L
N-Nitrosodiphenylamine
< 10 ug/L.
4-Bromophenyl plienyl ether
< 10 ug/L
Phenanthrene
< 10 ug/L
2-Chloronaphtltalene
< 10 ug/L
Pyrene
< 10 ug/L
4-Chlorophenyl phenyl ether
< 10 ug/L
1,2,4-Trichlorobenzene
< 10 ug/L
Chrysene
< 10 ug/L
Dibenzo(a,h)aathracene
< 10 ug/L
4-Chloro-3-methylphenol
< 10 ugiL
1,2 -Dichlorobenzene
< 10 ug/L
2 -Chlorophenol
< 10 ug/L
1,3 -Dichlorobenzene
< 10 ug/L
2,4-Dichlorophenol
< 10 ug/L
1,4 -Dichlorobenzene
< 10 ug/L
2,4 -Dimethylphenol
< 10 ug/L
3,T-Dichlorobenzidine
< 50 ug/L
2,4-Dinitrophenol
< 50 ug/L
Diethyl phthalate
< 10 ug/L
4,6-Dinitro-2-methylphenol
< 50 ug/L
Dimethyl phthalate
< 10 ug/L
2-Nitrophenol
< 10 ug/L
Di -n -butyl phthalate
< 10 ug/L
4-Nitrophenol
< 50 ug/L
2,4-Dinitrotoluene
< 10 ug/L
Pentachlorophenol
< 50 ug/L
2,6-Dinitrotoluene
< 10 ug/L
Phenol
< 10 ug/L
Dkn-octyl plithalate
< 10 ug/L
2,4,6-TrMilorophenot
< 10 ug/L
1,2-Diphenylhydrazine
< 10 ug/L
I hereby certify that I have reviewed
and approve these data,
Laboratory Representative
642 Tamco Road * Reidsville, NC 27320
[phone] Ph * [phone] Fax

3-20-2013 Chain of Custody Record (COC)
�/. //
Client:_/_ .p�iarG~A411 ��z>��
NPDES#:_-J/(' G'XQ, ?5'2
Phone:
ERITEC INC.'
Address: 1-14
�,,��
Fax: .
"s v
ENVIRONMENTAL LABORATORIES
�
��i4�;/ �>r�J/J S
Email: �lle1ge—o /) � 1v (`,./ siZii•=.d4
*
r. 642 TamcoRd. Phone: [phone]
62 70
Project:
Reidsville NC 27320 Fax: [phone]
P O #:
Email: [e-mail]
Attention. �� , • t
Turn Around Time*
www.meritech—lL bas
How would you like your report sent? *RUSH work needs prior approval.
I o
Circle all that apply: Email(preferred), Fax, ail , Std 1 s) 3.5 Days 24--48-1-I�rs
-Sampling Dates & Times
PersonT kings pie (sign/Print
-i: - r . ,.
Lab Use Only:
Sample Location and/or ID #
...,
-`" �''
Comp?
Grab?
# of
Test (s) Required �•a
On Ice?
•-
'.pH O•K?
Start End
Date Time Date Time
cont.
Yes / No
CI.OK?
7-
6/1,
Z11
6W
Temperature Upon
y�
Method Of *** Dechlorination (10.5 ppm)•of Ammonia,'Cyanide, Phenol and TKN samples must be done in the field prior to preservation.*** Y
�
Comments: 1-71-) Shipment: ;�•
"Compositor # -
_
5e
[]: UPS ��
-e-
-
- Jug #
Fed Ex Are these results fgir regulatory purposes? Yes
No ,.i Report results in:
mg/L [, mg/kg. ug/L
Relinquished by: Da
Hand Delivery.�'•
Time ' ✓ R t�ei by.
Date: time:
/
Other Relinquis b - 1' gate:
/ .a r^ -d r_; %,,�
Time: Received by: s
~�~
Date: Time:
Relinquished by: • Date: '
Time: Re by b:
e:

Client:
Attention
MERITECH, INC.
ENVIRONMENTAL LABORATORIES
Laboratory Certification No. 165
Kapstone Kraft Paper Corp.
100 Gaston Road
Roanoke Rapids, NC 27870
Neal Davis
Date Sampled
06/21/16
Digested
06/22/16
Analysis
07/01/16
Analyst:
CWL
EPA 1631 Low bevel Mercury Anal s0
1\4critech ID #
Sample ID
Result
ReportingLimit
imit
MBLK0517AA
Method Blank
< 0.5 ng/L
0.5 ng/L
M06221601
Field Blank
< 1.0 ng/L
1.0 ng/L
M06221602
B&C Cooling
2.52 ng/L
1.0 ng/L
I hereby certify that I have reviewed and approve these data.
Laboratory epresentativc
642*Tamco Rd - PO Box 27 - Reidsville, NC 27320
(336)3 42-4748 Ph - [phone] Fax
E -Mail: [e-mail]

1
a
oa
3.20.2013" Chain of Custody Record (COC)
Client: � ✓ ' „t�,a�=' 'r? � "=T // �r �r //k /'"'
NPDES#: �`i' •?
Phone: :Y'•1 - {3,:3 y ,? S' .>;'
� � WC
Address: / �?C">,.ry•,_..r �:�
Fax: ;,.f> -• - f,;.; %' .
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. i�. ENVIRONMENTAL LABORATORIES
f
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642
w Tamco Rd. Phone: [phone]
Project: �l�i ! C'�'Itirrc'
p•O•#:
Reidsville NC 27320 Fax: [phone]
Email• [e-mail]
Attention: ' �
How would you like your Report sent?
WWW.meritech-labs.com
Circle all that app ly:6MaU,(preferred), Fax,' Mai!+
Person Taking Sample (Sign/Print) ) //' �,.
.�
EPA 1631
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Date
Time
Site Description„I
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l�l� `il'syiarllc lf�a, C'!
Comments:
Shipment:
UPS
„Fed Ex
Are these results for regulatory purposes? Yes r: No []
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Hand Delivery
Relinquished I > , ro y -
r" Dote: Time•
R iv"' b y: / Date: Time:
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Received by Lab: / ��- D t Time:G/a, 7/6 o,?7-;
Received from Lab Secure Area
0 601

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Neal Davis Report Date: 8/24/2016
Client: Kapstone Paper & Packaging NPDES#: NCS000106
100 Gaston Rd. .
Roanoke Rapids, NC 27870 Date Sample Rcvd: 8/3/2016
Meritech Work Order # 080316142 Sample: Cooling Water Grab 8/3/16
Parameters Results Analysis Date Reporting Limit Method
Bromide, Total
0.046 mg/L
8/12/16.
0.020 mg/L
EPA 200.7
Dioxin, 2378- TCDD
Not Detected
8/18/16
1.06 pg/L
EPA 1613B
�I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Ta nco Road, Reidsville, North Carolina 27320
tel.[phone] £ax.[phone]

5-9-2016 Chain of Custody Record (COC)
NPDES#: -'4WIIOen�
MER ITECKINC
Client: Phone: o?5,:2
R
Address: '17614"'7 Fax: -�
ENVIRONMENTAL LABORATORIES
_,U_a2
♦Email: /461z'
41
642 Tamco Rd. Phone: [phone]
Project:
Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: Turn Around Time
How would you like your report sent? *RUSH work needs prior approval.
www.meritechlabs.com
1­76� (d - 48 Hrs
Circle all that apply: CEmaNq* (preferred), Fax, Q�allStd 1da _) F-7-1 = 241
Sampling Dates & Times
Person Taking Sample (Sign/Print):
Lab Use Only
Sample Location and/or ID #
start
End
Comp?
# of
Test(s)
Required
on ice? Yes
pH OK?
Date
Time
Date
Time
Grab?
Cont.
No
C1 OK?
'16;�T 76 z7w
fA IJ6
'A
Temperature Upon Receipt:
Method of
Dechlorination (<0-5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation..
Comments:
Compositor #
Jug #
Shipment:
UPS
Fed Ex.
Are theser9gults for regulatory purposes? -Yes _4��N4�'Q
Report results in: mg/L mg/kg U ug/L /Z
E—qT'Delivery
Relinquish 4'. DateTime:
Race
nme:Hand
Other
Reli=. '.2—DAe Time:
Recehied byvl Date: 'nme:
Relinquish y- Date: Time:
R,66eiv d Laf-,

In/ Nair $t1L�utomtaUursmesi tiewpplletlforeomplfatlte trtCfi
WATER SYSTEM:ID•##: '1,_ Cou L- •� .
Me a of VR hf--Sjrstesn: � �iGz� �� �AQ L �� C ilY�G1/iil `-
Sampleiype: ❑•S-MefeSwMAe•-e*y.Pvint [iCoinpoaite
Samgie — Fsxtiy Point• `. •:.. •
Facility ID Yo. &E� 7S
Sample Point: '3 •'
Mail Resohs to (sy4o= reptesaitavve):
Telephone4:
Fax #: (� S�6 `�`?� _ J_. l� - . ' I
Responsible Nxwa's email:
LA$ORAt•ORY tD *. 1?= 7 q 9 ❑ SAMPLE UNSATtSFAC bRY ` :-.O..RESAMifP ikE, Ugn tED .
drrn • •: � � i
safes «.
�eciaZjltitonto�rii,
- IYVtG: ii resuu CAVtN:s35 aiiowap►e- umrtr the ranoratory must tax artalytiCai resuitsto.tha State wFtht64S hotrs.
**Note: Not applicable if using ICp=MS
0
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L-,{?fr,
nst�' �
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456
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N/A
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4020
Fiadiursa 226
445
1
403Q
Radium 228
452
1PCI/t
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4100
Gross Seta
43S
4 PCVL
50 PWL '
PCI/L
- IYVtG: ii resuu CAVtN:s35 aiiowap►e- umrtr the ranoratory must tax artalytiCai resuitsto.tha State wFtht64S hotrs.
**Note: Not applicable if using ICp=MS
0
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L-,{?fr,
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Laboratory Lag #: ^.• l a �. CeTtrfed by: nfii se r laranann f

5.9.2016 Chain of Custody Record (COC)
NPDES#r:�®C?iWS 0Q 7,
�Jrl�2
Client; Phone:MERITECK.INC.
a
Address: �� /If 17.001,0 Fax: �U� -15,3
ENVIRONMENTAL LABORATORIES
Email:/U�
'!, . 642 Tamco Rd. Phone: [phone]
Project:
' a Reidsville NC 27320 Fax: [phone]
P.O.#:
Email: [e-mail]
Attention: �' / _'®/� Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
www.meritechiabs.comCircle
pply: Ema (preferred), Fax, Mail std 1 d s) s 24-4sH
all that apply:(
Sampling Dates & Times
Person Taking Sample (Sign/Print):
Lab Use Only
Sample- Location and/or ID #
Start
End
comp?
4 o
Test (s) Required
On Ice? Yes
pH OK
Date
Time
Date
Time
Grab?
cont.
/ No
C1 OK'-.
' P3
r
7 S? ZCfi "r
/
Temperature Upon Receip
Method of
*** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.
Shipment:
Comments:
/
Compositor#
.. UPS
Jug#
} Fed Ex
Are thes r ults for regulatory purposes? Yes N C
Report results in: mg/L mg/kg- ug/L
Hand Delivery
Rellnquis y: „ Datar Time:
5�/�fra �v
Recel; y; cData;� Time: /�/�
A 5S lv
Q% Other
Relin ed � DVtpl Time:--Q
Received by' Date: Time:
Relinquish y. Date: Time:
R celved La

r Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Neal Davis Report Date: 6/30/2016
Client: Kapstone Paper & Packaging NPDES#: WQ0021577
100 Gaston Rd. WQ0000436
Roanoke Rapids, NC 27870 Date Sample Rcvd: 6/23/2016
Meritech Work Order # 062316104 Sample: WW Flow/River Grab 6/23/16
Parameters Results Analysis Date Reporting Limit Method
Fecal Coliform 2 col/100 ml 6/23/16 1 col/100 ml SM 9222 D
Meritech Work Order # 062316105 Sample: B&C Colling Water Grab 6/23/16
Parameters Results Analysis Date Reporting Limit Method
Fecal Coliform 2 col/100 ml 6/23/16 1 col/100 ml SM 9222 D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tainco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

3.20.2013 -
Chain of Custody Record (COC)
NPDES#:1YC Ooel)n ?�L2
Client: Phone: dZp 5'3.3 —o`?��%
S.5RITE
Address: Fax: r3a_
XoAyohc� IZ eui✓s Aq Email: /1/,.44, Cd
_ ci 797, Project:
_ P.O.#:
Att-,ntion: <� .� Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply:EmaR(preferred), Fax Mail : Std 0 a s) 3-S Days 24-48Krs-
P INC.l
''
'. ENVIRONMENTAL LABORATORIES
642TamcoRd_ Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: info@meritech-[abs.com
www.meritech-labs.com 1
Sample Location and/or ID #
-
Sampling Dates & Times
Person Taking Sample ign/Pr-'t): //
//
L,ab Use Only
Start
End
Comp.
?
Grab?
#of
cont.
Test(s)
Required
on Ice?
es No
pH OK?
Cl OK?
Date
Time
Date
Time
n
i
o! �z
/vsoS
Temperature Upon Receipt-
Method of
Shipment:
""* Dechlorination (<0.S ppm) of Ammonia, cyanide, Phenol
and TKN samples must be done in the field prior to preservation. ***
Comments:
Compositor #
[ UPS
Jug#
Fed Ex
Are these resul for regulatory purposes? Yes
Nc;
Report results in: mg/L [° mg/kg ug/L
(Hand Delivery
Relinquished by: Da Time:-
z Qr
RenLqve Date: Tirge:
�1�u Lu '! �f / �j
Other
R quis ed by: ,Date: tme: y
Received by: // Date: Time:
Relinquished by: Date: Time:
U
_1Da2e;_ i 4 ime:'
Red)L
layU ) l

WaterResources
ENVIRONMENTAL QUALITY
PAT MCCRORY
Governor
DONALD R. VAN DER VAART
Secretaii
S. JAY ZIMMERMAN
Director
September 28, 2016
Mr. Wilbur G. Kessinger, Jr., VP
Kapstone Kraft Paper Corporation
100 Gaston Road
Roanoke Rapids, NC 27870
Subject: Permit Renewal
Application No. NC00000752
Kapstone Kraft Paper Corporation WWTP
Northampton County
Dear Mr. Kessinger:
The Water Quality Permitting Section acknowledges receipt of your permit application and
supporting documentation received on September 27, 2016. The primary reviewer for this renewal
application is Sergei Chernikov.
The primary reviewer will review your application, and he will contact you if additional information
is required to complete your permit renewal. Per G.S. 150B-3 your current permit does not expire until
permit decision on the application is made. Continuation of the current permit is contingent on timely and
sufficient application for renewal of the current permit.
Please respond in a timely manner to requests for additional information necessary to complete the
permit application. If you have any additional questions concerning renewal of the subject permit, please
contact Sergei Chernikov at 919-807-6398 or [e-mail].'
cc: Central Files
NPDES
Raleigh Regional Office
Sincerely,
Wren Thedford
Wastewater Branch
State of North Carolina I Environmental Quality I Water Resources
1617 Mail Service Center I -Raleigh, North Carolina 27699-1617
919-807-6300