WQ0001492_Monitoring - 11-2016_20161222

hart ; hickman
SMARTER ENVIRONMENTAL SOLUTIONS
Via FedEx
December 19, 2016
NC Department of Environmental Quality
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: November 2016 Groundwater Monitoring Compliance Report FoRFrF:I\/ED
SDIBR Permit No. WQ0001492 OFf' 2 L
Former Occidental Chemical Corporation Facility Z�16
Castle Hayne, North Carolina DWRSECTION
H&H Job No. OXY -003 I,NFORAOTIONPROCESSING WTI`
Dear Sir or Madam:
In accordance with Sections IV.7 and IV.9 of Surface Disposal of Industrial Byproducts
Residuals (SDIBR) Permit No. WQ0001492, Hart & Hickman, PC (H&H), on behalf of Glenn
Springs Holdings, Inc./Occidental Chemical Corporation, is submitting the enclosed
Groundwater Quality Monitoring: Compliance Reports Forms (GW -59A and GW -59) and
laboratory analytical reports for groundwater samples collected in accordance with the SDIBR
permit during the month of November 2016. One original and one copy of the report package
are enclosed.
If you have any questions or need additional information, please do not hesitate to contact me at
[phone].
Sincerely,
Hart & Hickman, PC
Scott Drury, PE
Project Manager
Enclosures
Steve Hart, PG
Principal
cc: Mr. David Guier — Glenn Springs Holdings (via email)
2923 South Tryon Street, Suite 100 3334 Hillsborough Street
Charlotte, NC 28203 Raleigh, NC 27607 www.harthickman.com
704.586.0007 main 919.847.4241 main

U W -PYA L0MYL1AIV0.,r. KLrk)KI rIJKM rermft n wyuuul4w
(Submit one each monitoring period with GW -59 forms.)
]
Enter date monitoring results were due.( 12130116 ) Will this monitoring report (GW -59 and GW -59A)
YES
NO
be submitted after the established due date?
X
2
Was any required information missing on the GW -59 report forms?
YES
N O
X
IF the answer to question 1 or 2 is "YES'; list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap,
YES
NO
missing identification plate, area overgrown, etc.)? If the answer is "Yes', contact the Regional Office for
guidance.
X
4
Are any monitored constituents equal to or above the established standards?
YES
NO
X
If the answer to question 4 is "NO'; skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
See enclosed Summary of Affected Wells
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
X
If the answer to question 5 is "NO" skip to section 8.
N the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
See enclosed Summary of Affected Wells
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
X
If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly
located; contact the Regional Office.
Immediate notification of elevated iron, chloride, and TDS concentrations and pH levels outside the
2L standard range was not made since these conditions were already known to DWR (see the attached
email). Immediate notification of elevated chromium in MW -24 (CPW-4D) was not made since this
condition is attributable to the Plant Process Area (PPA) of the site and was already known to DEQ.
Chromium impacts associated with the PPA are being managed under an Administrative Agreement (AA)
for Voluntary Assessment and Remedial Action under the Inactive Hazardous Sites Branch (IHSB)
Registered Environmental Consultant (REC) Program, DEQ ID NCD057454670.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
X
If the answer to question 7 is "YES'; describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 9D days: an evaluation may be
reetrired to determine the impaet the waste dispose/system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subiect the permittee to a Notice of Violation,
fines. and/or eena/ties.
The facility is currently operating under a Corrective Action Plan for ground water remediation by natural
attenuation under the provisions outlined in 15A NCAC 2L.0106(I).
8
The person completing this portion (GW -59A) of the monitoring report should sign below and submit this
form with GW -59 forms for required wells to the address provided at the top of the current GW -59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report (Compliance Repo GW -59A) is true and complete to the best of my knowledge.
Ca IZ 1`1114
Signature of Permittee (or Authorized gent) Date
GW -59A 12/812003

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: Occidental Chemical Corporation
Permit Name (if different):
Facility Address: 5408 Holly Shelter Rd
Castle Hayne NC 28249 County New Hanover
1-.1
Contact Person: David Guier Telephone#: [phone]
Well Location/Site Name: 34°21'46.2200", -077°52'12.3200" No. of wells to be sampled:
L ID NUMBER (from Permit): MW -1 (CPW-13S) Date sample collected: 11/3/2016
Depth: 38 ft. Well Diameter: 4 in.
1 to Water Level 82546: 7.28 ft, below measuring point Screened Interval: 28 ft. to 38 ft.
,uring Point is 2.65 ft. above land surface Relative M.P. Elevation: 14.95 ft.
ne of water pumped/bailed before sampling: 0.75 gallons
)les for metals were collected unfiltered: ® YES ❑ NO and field acidified: ® YES ❑ NO
PARTMENTOF ENVIRONMENT &-NATURAL RESOURCES' -
tSION OFWATER RESOURCES -INFORMATION PROCESSING UNIT
7 MAILSERYICELENTER, RALEIGN�,N( 37699-1617 Phone:[phone]
:RMIT Number:
Expiration Date. 8/31/2021
n -Discharge
UIC
'DES
Other W00001492
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump ® Other: SDIBR Permit
FIELD ANALYSES:
pH o0400: 6.31 units Temp. 000t0: 0C
Spec. Cond.00094 µMhos
Odor oo0e5:
Appearance
Date sample analyzed: 11/08/2016 - 11/12/2016
Laboratory Name: ALS Environmental
Certification No. 676
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616
/100mL
Nitrate (NO3) as N 00620
mg/L
Zn -Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
n I
(Note: Use MPN method for highly IUNitl samples)
Orthophosphate 70507
mg/L
Other (Specify l rlls6unds and Concentration Units):
)issolved Solids:Total 70300 940
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium otoo7
ug/L
TOC ooeao
mg/L
Ca - Calcium 00916
mg/L
Chloride oos4o 8.4
mg/L
Cd - Cadmium 01027
ug/L
Arsenic o1oo2
ug/L
Chromium: Total oto34
<10
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
19,300
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate oo945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
-YAG-7473 , method #
Total Ammonia 00610
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn -Manganese 01055
ug/L
,method #
TKN as N 00625
mg/L
Ni - Nickel 01067
<40
ug/L
, method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOIDS:
mg/L
Effluent Total VOCs: mg/L VOC Removal%
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent) C
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permi ee (or Authonz Apert (pate)
GW -59 Rev. 8/2013
at
of

ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
Name: Occidental Chemical
Name (if different):
Address: 5408 Holly Shelter R
VC 28249
i
SUBMIT FORM ON YELLOW PAPER ONLY
County New Hanover
act Person: David Guitar Telephone#: [phone]
Location/Site Name: 34°21'51.6400", -077°52'30.2400" No. of wells to be sampled: 24
L ID NUMBER (from Permit): MW -2 (CPW-14S)
Depth: 28 ft.
1 to Water Level 82546: 7.02 ft. below measuring point
luring Point is 2.73 ft. above land surface
ne of water pumped/bailed before sampling: 0.75
)lea for metals were collected unfiltered: ® YES F1
Date sample collected: 11/1/2016
Well Diameter:
4 in.
Screened Interval:
18 ft.
Relative M.P. Elevation:
12.53
gallons
NO
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOURCES =INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
PERMIT Number:
Expiration Date: 8/31/2021
Non -Discharge
UIC
NPDES
Other WQ0001492
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
to 28 ft,
ft,
ate sample analyzed: 11/08/2016 - 11/12/2016 Laboratory Name: ALS Environmental
4RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N oo615
mg/L
Coliform: MF Fecal 31616
/100mL
Nitrate (NO3) as N 00620
mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P oo66s
mg/L
(Note: Use MPN methoti for highly turf ld samples)
Orthophosphate 70507
mg/L
;solved Solids:Total 70300 700
mg/L
Al -Aluminum ol1o5
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride oog4o 147
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
<10 ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
Phenol 32730
ug/L
Fe - Iron 01045
3,760 ug/L
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
tecific Conductance Doom
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610
mg/L
Mg - Magnesium 00927
mg/L
(Ammonia Nitrogen', NH3asN; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
TKN as N 00625
mg/L
Ni - Nickel 01067
<40 ug/L
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
❑ Water Source Heat Pump ® Other: SDIBR Permit
FIELD ANALYSES:
pH oo400: 6_90 units
Spec. Cond.00094:
Odor 000es: _
Appearance
Temp. Doom eC DRY at
µMhos time of
Certification No. 676
Pb - Lead olo51 ug/L
Zn -Zinc 01092 mg/L
Other (Specify Cows and Concentration Units):
UEC 2 8 2016
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes (1) ❑ No (0)
_V , method #
method #
method #
method #
mg/L Effluent Total VOCs.
mg/L VOC Removal°/
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent) e-/
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permmee (or AutItonzed nt) (Dale)
GW -59 Rev. 812013
C

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: Occidental Chemical Corporation
Permit Name (if different):
Facility Address: 5408 Holly Shelter Rd
Castle
act Person: David Guier
Location/Site Name: 34022'04.7700". -077°52'2
SUBMIT FORM ON YELLOW PAPER ONLY
County New Hanover
Telephone#: [phone]
No. of wells to be sampled: 24
L ID NUMBER (from Permit): MW -3 (CPW-15S) Date sample collected: 11/2/2016
Depth: 40 ft. Well Diameter: 4 in.
i to Water Level 82546: 7.61 ft. below measuring point Screened Interval: 25 ft. to 40 ft.
,uring Point is 3.56 ft. above land surface Relative M.P. Elevation: 13.76 ft.
ne of water pumped/bailed before sampling: 0.75 gallons
)les for metals were collected unfiltered: © YES ❑ NO and field acidified: ® YES n NO
ate sample analyzed: 11/08/2016 -11/11/2016 Laboratory Name: ALS Environmental
I RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD oo33s
mg/L
Nitrite (NO2) as N omi5
mg/L
Coliform: MF Fecal 316le
/100mL
Nitrate (NO3) as N 00620
mg/L
Coliform: MF Total 315o4
/10OmL
Phosphorus: Total as P ooe65
mg/L
(NoteUse MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
:solved Solids:Total 70300 546
mg/L
Al -Aluminum a11os
mg/L
pH (Lab) oo4o3
units
Ba - Barium 01007
ug/L
TOC oo6eo
mg/L
Ca - Calcium oog16
mg/L
Chloride oo940 194
mg/L
Cd - Cadmium 01027
ug/L
Arsenic olooz
ug/L
Chromium: Total 01034
<10 ug/L
Grease and Oils 00552
mg/L
Cu -Copper 01042
mg/L
Phenol 32730
ug/L
Fe - Iron oio45
<100 ug/L
Sulfate o0945
mg/L
Hg - Mercury 71900
ug/L
ecific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia omio
mg/L
Mg - Magnesium 00927
mg/L
(Ammonia Nitrogen; NHs as N', Ammonia Nitrogen. Total)
Mn - Manganese oloss
ug/L
TKN as N 00625
mg/L
Ni - Nickel 01067
<40 ug/L
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
PARTMENT OF ENVIRONMENT &.NATURAL RESOURCES
rSION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
17 MAIL SERVICE CENTER, RALEIGH,.,NCA6699=1617 Phone:[phone]
:RMIT Number:
Expiration Date: 8/31/2021
in -Discharge
UIC
)DES
Other W00001492
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ft Other: SDIBR Permit
FIELD ANALYSES:
pH 00400: 7.77 units
Spec. Cord. 00094:
Odor 000ae: _
Appearance
Temp. 000lo: °C DRY at
µMhos time of
Certification No. 676
Pb - Lead o1o51 ug/L
Zn - Zinc 01092 mg/L
Other (Specify CompgitOdg and Concentration Units):
DEC 2
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes (1) ❑ No (0)
-V96 Faia method #
method #
method #
method #
mg/L Effluent Total VOCs:
VOC Removal%
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent) C e 1 ! / 9��
Permittee (or Authorized Agent) Name and Tele - Please pant or type Signature of Penin a (or Authorized en0 (a9//4")
GW -59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
UNDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
OF ENVIRONMENT 8 NATURAL RESOURCES
ATER RESOURCES -INFORMATION PROCESSING UNIT
VICE. CENTER, RALEIGH; NC 27699-1617 Phone:[phone]
FACILITY INFORMATION i-teaseenntCteanyor type PERMIT Number: Expiration Date 8/31/2021
Facility Name: Occidental Chemical Corporation Non -Discharge UIC
Permit Name (if different): NPDES Other W00001492
Facility Address: 5408 Holly Shelter Rd TYPE OF PERMITTED OPERATION BEING MONITORED
Castle Hayne NC 28249 County New Hanover ❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
Contact Person: David Guier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°22'25.7100", -077'51'58.5900" No. of wells to be sampled: 24 ❑ Water Source Heat Pump ® Other: SDIBR Permit
WELL ID NUMBER (from Permit): MW -8 (CPW-8DR) Date sample collected: 11/4/2016
Well Depth: 87 ft. Well Diameter: 4 in.
Depth to Water Level 82546: 4.02 ft. below measuring point Screened Interval: 67 ft. to 87 ft.
Measuring Point is 3.15 ft. above land surface Relative M.P. Elevation: 8.35 ft.
Volume of water pumped/bailed before sampling: 0.75 gallons
acidified: ® YES ❑ NO
FIELD ANALYSES:
pH 0o4o0: 7_18 units
Spec. Cond. 00094:
Odor oaoe5: _
Appearance
Date sample analyzed: 11/08/2016 - 11/12/2016 Laboratory Name: ALS Environmental
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N oo615 mg/L Pb - Lead o1o51
Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092
Coliform: MF Total 31504
/100ml-
(Note: Use MPN method far highly turbid samples)
mg/L
solved Solids:Total 70300 688
mg/L
pH (Lab) oo4o3
units
TOC ooeso
mg/L
Chloride 00940 257
mg/L
Arsenic 01002
ug/L
Grease and Oils 00552
mg/L
Phenol 32730
ug/L
Sulfate 00945
mg/L
scific Conductance 00095
µMhos
Total Ammonia oo610
mg/L
(Ammonia Nitrogen: NHsas N: Ammonia Nitrogen, Total)
uglL
TKN as N 00625
mg/L
For Remediation Systems Only (Attach Lab Reports):
Phosphorus: Total as P 00665
mg/L
Orthophosphate 70507
mg/L
AI -Aluminum 01105
mg/L
Ba - Barium 01007
ugli-
Ca - Calcium 00916
mg/L
Cd - Cadmium 01027
ug/L
Chromium: Total 01034
<10 ug/L
Cu - Copper 01042
mg/L
Fe - Iron 01045
720 ug/L
Hg - Mercury 71900
ug/L
K - Potassium 00937
mg/L
Mg - Magnesium 00927
mg/L
Mn - Manganese 01055
uglL
Ni - Nickel 01067
<40 ug/L
Influent Total VOCs
Temp. otio10: °C DRY at
µMhos time of
Certification No. 676
ug/L
mg/L
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes (1) ❑ No (0)
method #
method #
method #
method #
mg/L Effluent Total VOCs:
mg/L
VOC Removal%
GW -59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW -59 Rev. 8/2013
mg/L Effluent Total VOCs
.
Signature
mg/L VOC Removal%
/s
DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES- +
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES- INFORMATION PROCESSING UNIT.
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone:[phone]
FACILITY INFORMATION Pease Print Clearly or Type
PERMIT Number: Expiration Date: 8/31/2021
Facility Name: Occidental Chemical Corporation
Non -Discharge UIC
NPDES Other W00001492
Permit Name (if different):
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Hayne NC 28249 County New Hanover
-' '-�-" -"
EJ Spray Field El Remediation:
Contact Person: David Guier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°22'21.7300", -077°52'11.7100"
No. of wells to be sampled: 24
❑ Water Source Heat Pump ® Other: SDIBR Permit
(hpm PermiO
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW -9 (CPW-9D)
Date sample collected: 11/2/2016
FIELD ANALYSES:
WAS
Well Depth: 108 ft.
Well Diameter: 4 in.
pH 00400: 7.36 units Temp. 000lo: oC
DRY at
Depth to Water Level 82546: 3.42 ft. below measuring point
Screened Interval: 88 ft. to
—
108 ft. Spec. Cond. 00094: µMhos
time of
sampling,
Measuring Point is 2.57 ft. above land surface
Relative M.P. Elevation: 8.37 ft.
Odor 0ooa5:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: © YES
❑ NO and field acidified: © YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 11/08/2016 - 11/12/2016
Laboratory Name: ALS Environmental
Certification No. 676
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N 00615
mg/L
Pb - Lead oio51 ug/L
Coliform: MF Fecal 31616 /100ml-
Nitrate (1,103) as N 00620
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
ri
Other (Speciflpounds and Concentration Units) -
issolved SOIIdS:TOtal 70300 1,810 mg/L
At -Aluminum o11o5
mg/L
pH (Lab) 00403 units
Be - Barium 01007
ug/L 0E
TOC oo6ao mg/L
Ca - Calcium oo915
I
Chloride 00940 200 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total olo34 <10
ug/L
Grease and Oils 0o5s2 ril
Cu - Copper o1o42
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 <100
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate oo945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0)
pecific Conductance 00095 µMhos
K - Potassium 00937
mg/L _VoC = u;T method #
Total Ammonia oosio mg/L
Mg - Magnesium oog27
mg/L
, method #
(Ammonia Nitrogen', NH3as N. Ammonia Nitrogen, Total)
Mn - Manganese om55
ug/L , method #
TKN as N 00625 mg/L
Ni - Nickel 01067 <40
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW -59 Rev. 8/2013
mg/L Effluent Total VOCs
.
Signature
mg/L VOC Removal%
/s

UNDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
Name: Occidental Chemical
Name (if different):
SUBMIT FORM ON YELLOW PAPER ONLY
or
28249 County New Hanover
act Person: David Guitar Telephone#: [phone]
Location/Site Name: 34°22'13.9300", -077°52'19.0700" No. of wells to be sampled: 24
L ID NUMBER (from Permit): MW -10 (CPW-10D)
Depth: 100 ft.
1 to Water Level 62546: 5.45 ft. below measuring point
curing Point is 3.38 ft. above land surface
ne of water pumped/bailed before sampling. 0.75
)les for metals were collected unfiltered: ® YES ❑
Date sample collected:
Well Diameter:
11/2/2016
4 in.
Screened Interval: 60 ft. to 100 ft.
Relative M.P. Elevation: 10.38 ft.
gallons
NO and field acidified: [EYES ❑ NO
Date sample analyzed: 11/09/2016 - 11/12/2016 Laboratory Name: ALS Environmental
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N oasis
mg/L
Coliform: MF Fecal 31616
11 00m
Nitrate (NO3) as N 00620
mg/L
Coliform: MF Total 31504
/100ml-
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Assolved Solids:Total 70300 1,230
mg/L
AI -Aluminum o1105
mg/L
pH (Lab) 00403
units
Be - Barium 01007
ug/L
TOC o066o
mg/L
Ca - Calcium oog16
mg/L
Chloride oog4o 120
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total oio34
<10 ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
Phenol 32730
ug/L
Fe - Iron 01045
<100 ug/L
Sulfate 00945
Ill
Hg.- Mercury 71900
ug/L
3pecif c Conductance oo095
µMhos
K - Potassium 00937
mg/L
Total Ammonia oosl o
mg/L
Mg - Magnesium 00927
mg/L
(Ammonia Nitrogen. NH3 as N. Ammonia Nitrogen. Total)
Mn - Manganese 01055
ug/L
TKN as N 00625
mg/L
Ni - Nickel 01067
<40 ug/L
�ARTMENT OF ENVIRONMENT & NATURAL RESOURCES
ISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
7 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
RMIT Number:
Expiration Date: 8/31/2021
n -Discharge
UIC
'DES
Other WQ0001492
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump © Other: SDIBR Permit
FIELD ANALYSES: I WAS
pH 00400: 9.57 units Temp. 000to: 0C DRY at
Spec. COnd. oo: µMhos time
094
sampling,
Odor000s5: check
Appearance here: El
Certification No. 676
Pb - Lead 01051 ug/L
Zn - Zinc 01092 mg/L
Othel03cify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes (1) ❑ No (0)
-4QC_Zsz3_ method #
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs. Ill VOC Removal
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or tale
GW -59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
MELMOM DEPARTMENT OF ENVIRONMENT a- NATURAL RESOURCES
UNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES- INFORMATION PROCESSING UNIT
PLIANCE REPORT FORM 617 MAIL: SERVICE'CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
Name: Occidental Chemical
Name (if different):
Castle
INC 28249
or
County New Hanover
act Person: David Guier Telephone#: [phone]
Location/Site Name: 34°22'09.7700", -077°51'39.4400" No. of wells to be sampled:
24
PERMIT Number:
Expiration Date'. 8/31/2021
Non -Discharge
UIC
NPDES
Other W00001492
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
L ID NUMBER (from Permit): MW -11 (CPW-1S) Date sample collected: 1112/2016
Depth: 32 ft. Well Diameter: 2 in,
i to Water Level 82546: 4_84 ft. below measuring point Screened Interval: 17 ft. to 32 ft.
luring Point is 2 ft. above land surface Relative M.P. Elevation: 26.40 ft.
ne of water pumped/balled before sampling: 0.75 gallons
)lea for metals were collected unfiltered: © YES ❑ NO and field acidified: ® YES ❑ NO
❑ Water Source Heat Pump ® Other. SDIBR Permit
FIELD ANALYSES: I WAS
pH 00400: 6.73 units Temp. 000lo: °C DRY at
Spec. Cond. 00094: µMhos time of
samplir
Odor 000a5: check
Appearance
Date sample analyzed:
11/09/2016 - 11/11/2016
Laboratory Name: ALS Environmental
mg/L
PARAMETERS NOTE: Values
should reflect dissolved and colloidal concentrations.
)issolved Solids:Total 70300 327
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead oto51
Coliform: MF Fecal 31616
/100ml-
Nitrate (NO3) as N 00620
mg/L Zn -Zinc 01092
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P00665
mg/L
Certification No. 676
ug/L
mg/L
(Note'. Use MPN matlwd for highlylureid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds
and Concentration Units):
)issolved Solids:Total 70300 327
mg/L
At - Aluminum oil s
mg/L
6.1
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC oo68o
mg/L
Ca - Calcium 00916
mg/L
I ) E L 2 8 2010
Chloride 00940 5.0
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
uglL
Chromium: Total olo34
<10 ug1L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
7,860 ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate oog4s
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
-VOG-zam" , method #
Total Ammonia 00610
mg/L
Mg - Magnesium 00927
mg/L
, method #
(Amman(. Nitrogen: NH,, as N, Ammonia Nitrogen, Total)
Mn - Manganese gloss
ug/L
method #
TKN as N 00625
mg/L
Ni - Nickel 01067
<40 ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs. mg/L Effluent Total VOCs:
mg/L VOC Removal%
Steve HartPG Principal Hart & Hickman, PC (Authorized Agent) C /;Z//.
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Pe"Iflee (or Autholizedgen (Date)
GW -59 Rev. 8/2013

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Name: Occidental Chemical
Name (if different):
NC 28249
or Type
SUBMIT FORM ON YELLOW PAPER ONLY
County New Hanover
act Person: David Guier Telephone#: [phone]
Location/Site Name: 34'22'03.3000", -077'51'56.8900" No. of wells to be sampled: 24
L ID NUMBER (from Permit): MW -12 (CPW-12D) Date sample collected: 11/1/2016
Depth: 98 ft. Well Diameter: 4 in.
1 to Water Level 62546: 4.59 ft. below measuring point Screened Interval: 58 ft.
wring Point is 0.80 ft. above land surface Relative M.P. Elevation: 14.1
ne of water pumped/bailed before sampling: 0.75 gallons
)les for metals were collected unfiltered: © YES ❑ NO and field acidified: IN YES
to 98 ft.
ft.
I:Ce7
Date sample analyzed: 11/08/2016 - 11/12/2016 Laboratory Name: ALS Environmental
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N o0615
mg/L
Coliform: MF Fecal 31616
11 00m
Nitrate (NO3) as N oo6zo
mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P00665
mg/L
(Nota, Use MPN method for highly lurbtd samples).
Orthophosphate 70507
mg/L
Assolved Solids:Total 70300 1,000
mg/L
Al -Aluminum ollo5
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC oo600
mg/L
Ca - Calcium 00916
ni
Chloride 00940 6.2
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
<10 uglL
Grease and Oils 00552
mg/L
Cu - Copper 01 D42
ni
Phenol 32730
ug/L
Fe - Iron 01045
12,300 ug/L
Sulfate 00945
mg/L
Hg - Mercury 71goa
ug/L
Specific Conductance 00095
pMhos
K - Potassium oo937
mg/L
Total Ammonia oo6m
mg/L
Mg - Magnesium 00927
mg/L
(Ammonia Nitrogen, NH,asN: Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
TKN as N 00625
mg/L
Ni - Nickel 01067
<40 ug/L
PARTMENT OF ENVIRONMENT& NATURAL RESOURCES
1SION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
17 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
IRMIT Number:
Expiration Date. 8/31/2021
In -Discharge
UIC
)DES
Other WQ0001492
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump ® Other: SDIBR Permit
FIELD ANALYSES: 1 WAS
pH 00400_ 6.25 units Temp. 000lo: oC DRY at
Spec. Cond. 00094: µMhos time of
samplin
Odor 000m- check
Appearance here:r
Certification No. 676
Pb - Lead olos1 ug/L
Zn - Zinc 01092 mg/L
Other (Specifybppunds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes (1) ❑ No (0)
-VG -3°'3 method #
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs:
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW -59 Rev. 8/2013
mg/L VOC Removal%

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: Occidental Chemical
Permit Name (if different):
Print Clearly or
NC 28249
SUBMIT FORM ON YELLOW PAPER ONLY
County New Hanover
3d Person: David Guier Telephone#: [phone]
Location/Site Name: 34`21'46.2200", -077"52'12.3200" No. of wells to be sampled: 24
PARTMENT OF ENVIRONMENT B NATURAL RESOURCES'
1SION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
17 MAIL SERVICE CENTERS RALEIGH, NC 27699-1617 Phone: [phone]
!RMIT Number:
Expiration Date: 8/31/2021
,n -Discharge
UIC
'DES
Other W00001492
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump ® Other: SDIBR Permit
ELL ID NUMBER (from Permit): MW -13 (CPW-13D)
ell Depth: 80 ft.
apth to Water Level 82546: 8.16 ft. below measuring point
easuring Point is 2.53 ft. above land surface
flume of water pumped/bailed before sampling: 0.75
imples for metals were collected unfiltered: IN YES
Date sample collected: 11/3/2016
Well Diameter: 4 in.
Screened Interval: 70 fL to
Relative M.P. Elevation: 15.13 ft.
gallons
El NO and field acidified: ® YES El NO
80 ft.
FIELD ANALYSES:
pH 00400: 6.61 units Temp. 000lo: °C
Spec. Cond. 00094: µMhos
Odor 000m:
Appearance
WAS
DRY at
time
samplilin
check
here: r
L
\BORATORY INFORMATION
ug/L
Fe - Iron 01045
1,540 ug/L
(Specify test and method #. ATTACH LAB REPORT.)
ate sample analyzed: 11/08/2016 - 11/12/2016
Laboratory Name: ALS Environmental
Hg - Mercury 71900
Certification No. 676
Lab Report Attached? ❑ Yes (1) ❑ No (0)
4RAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
K - Potassium 00937
mg/L
-VA6vZasa_ method At
COD 00335 mg/L
Nitrite (NO2) as N oo615
mg/L
Pb - Lead oio51 ug/L
, method #
Coliform: MF Fecal 31618 /100mi-
Nitrate (NO3) as N 00620
mg/L
Zn - Zinc 01092 mg/L
, method #
Coliform: MF Total 31504 /100ml.
Phosphorus: Total as P oo665
mg/L
<40 ug/L
, method #
t Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compo and Concentration Units):
tsolved Solids:Total 70300 1,060 mg/L
AI -Aluminum o11o5
mg/L
pH (Lab) 00403 units
Ba - Barium 01007
ug/L
DEC 2 S 0%
TOC oo68o mg/L
Ca - Calcium 00,916
mg/L
Chloride 00940 166 mg/L
Cd - Cadmium 01027
ug/L
Arsenic oloo2 ug/L
Chromium: Total 01034 <10
ug/L
Grease and Oils 00552
mg/L
Cu - Copper o1o42
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
1,540 ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
ifc Conductance 00095
µMhos
K - Potassium 00937
mg/L
-VA6vZasa_ method At
Total Ammonia 00610
mg/L
Mg - Magnesium 00927
mg/L
, method #
(Ammonia Nitrogen; NH, as N', Ammonia Nitrogen, Total)
Mn - Manganese oio55
ug/L
, method #
TKN as N 00625
mg/L
Ni - Nickel 01067
<40 ug/L
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
mg/L Effluent Total VOCs
:
mg/L VOC Removal°/
Steve Hart, PG,. Principal, Hart 8 Hickman, PC (Authorized Agent) L [. Z//
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee io1 Authon d Age t) (Date)
GW -59 Rev. 8/2013

UNDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
Name: Occidental Chemical Corporation
Name (if different):
Castle
SUBMIT FORM ON YELLOW PAPER ONLY
or
NC 28249 County New Hanover
act Person: David Guier Telephone#: [phone]
Location/Site Name: 34"21'51.6400", -077'52'30.2400" No. of wells to be sampled: 24
DEPARTMENT OF ENVIRONMENT &.NATURAL RESOURCES
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
PERMIT Number:
Expiration Date: 8/31/2021
Non -Discharge
UIC
NPDES
Other W00001492
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
WELL ID NUMBER (from Permit): MW -14 (CPW-14D) Date sample collected: 11/1/2016
Well Depth: 80 ft. Well Diameter: 4 in.
Depth to Water Level 82546: 7_36 ft. below measuring point Screened Interval: 75 ft. to 85 ft.
Measuring Point is 3.44 ft. above land surface Relative M.P. Elevation: 12.94 it
Volume of water pumped/bailed before sampling: 0.75 gallons
Samples for metals were collected unfiltered: ® YES ❑ NO and field acidified: ® YES ❑ NO
❑ Water Source Heat Pump ❑ft Other: SDI BR Permit
FIELD ANALYSES:
pH 00400: 6_66 units
Spec. Cond. 00094:
Odor 00065:
Appearance
Date sample analyzed: 11/08/2016 - 11/12/2016
rbd1
Laboratory Name: ALS Environmental
Orthophosphate 70507
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
Other (Specify Compounds and Concentration Units):
COD 00335 mg/L
Nitrite (NO,) as N 00615
mg/L Pb - Lead o1o51
Coliform: MF Fecal 31616 /100mL
Nitrate (NO3) as N 00620
ni Zn - Zinc 01092
Coliform: MF Total 31504 /100mL
Note Use MPN method for hi hl t
Phosphorus: Total as Foams
mg/L
If WELL
Temp. otlom °C DRY at
µMhos time of
Certification No. 676
ug/L
mg/L
9 y e samPa.)
Orthophosphate 70507
ni
Other (Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 888
mg/L
Al -Aluminum o11o5
mg/L
n_ j
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC oo6ao
ni
Ca - Calcium oo916
mg/L
DEC 2 R 2016
Chloride 00940 160
ni
Cd - Cadmium o1o27
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
<10 ug/L
Grease and Oils 00552
ni
Cu - Copper 01o42
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
3,250 ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 000g5
µMhos.
K - Potassium 00937
mg/L
'GC < , method #
Total Ammonia oo610
mg/L
Mg - Magnesium 00927
mg/L
, method #
(Ammonia Nitrogen: NH�as N', Ammonia Nitrogen, Total)
Mn - Manganese o1o55
ug/L
, method #
TKN as N 00625
mg/L
Ni - Nickel 01067
<40 ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs.
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent) CA, ir
Permittee (or Authorized Agent) Name and Title- Please print or type Signature of Permittee (or (or Authorizer
GW -59 Rev. 812013
mg/L VOC Removal%

ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
or
SUBMIT FORM ON YELLOW PAPER ONLY
Facility Name: Occidental Chemical Corporation
Permit Name (if different):
Facility Address: 5408 Holly Shelter Rd
Castle Hayne NC 28249 County New Hanover
act Person: David Guier Telephone#: [phone]
Location/Site Name: 34°22'04.7700", -077°52'21.5000" No. of wells to be sampled:
L ID NUMBER (from Permit): MW -15 (CPW-15D)
Depth: 74 ft.
i to Water Level 82546: 7.62 ft. below measuring point
wring Point is 3.64 ft. above land surface
ne of water pumped/bailed before sampling: 0.75
Date sample collected:
11/2/2016
Well Diameter:
4 in.
Screened Interval:
64 ft. to 74 ft.
Relative M.P. Elevation:
13.64 ft.
gallons
NO and field acidified: ® YES ❑
3ARTMENT OF ENVIRONMENT 8 NATURAL RESOURCES
ISION OF. WATER RESOURCES -INFORMATION PROCESSING UNIT
7 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 'Phone: [phone]
RMIT Number:
Expiration Date. 8/31/2021
n -Discharge
UIC
'DES
Other W00001492
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump ® Other: SDIBR Permit
FIELD ANALYSES:
pH 00400: 7_06 units
Spec. Cond. 00094:
Odor 000es:
Appearance
Date sample analyzed:
11/08/2016 - 11/11/2016
Laboratory Name: ALS Environmental
mg/L
PARAMETERS NOTE: Values
should reflect dissolved and colloidal concentrations.
mg/L
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead. oio51
Coliform: MF Fecal 31616
/100mL
Nitrate (NO3) as N 00620
mg/L Zn -Zinc 01092
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
Temp. 000lo. °C DRY at
µMhos time of
Certification No. 676
ug/L
mg/L
(Note: Use MPN method far highly tumid samples)
Orthophosphate 70507
mg/L
Other (SMifj Compounds and Concentration Units):
)issolved Solids:Total 70300 604
mg/L
Al -Aluminum o11o5
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC oo6eo
mg/L
Ca - Calcium 00518
mg/L
Chloride oos4o 146
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
<10 ug/L
Grease and Oils 00552
nri
Cu -Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
980 ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate oos4s
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium oo937
mg/L
vee-Te , method #
Total Ammonia 00610
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen, NH3as N: Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
method #
TKN as N oo625
mg/L
Ni - Nickel 01067
<40 ug/L
, method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs:
mg/L
Effluent Total VOCs:
mg/L VOC Removal%
here:❑
UvV-3w Kev. oILU 13

NATER QUALITY MONITORING:
NCE REPORT FORM
or
SUBMIT FORM ON YELLOW PAPER ONLY
Name: Occidental Chemical Corporation
Name (if different):
Address: 5408 Holly Shelter Rd
Castle Hayne NC 28249 County New Hanover
act Person: David Guier Telephone#: [phone]
Location/Site Name: 34°22'34.0100", -077'51'43.9000" No. of wells to be sampled: 24
L ID NUMBER (from Permit): MW -16 (CPW-6S) Date sample collected: 11/3/2016
Depth: 42 ft. Well Diameter: 4 in.
h to Water Level 82546:12.66 ft. below measuring point Screened Interval: 27 ft. to 42 ft.
:wring Point is 3.59 ft. above land surface Relative M.P. Elevation: 15.79 ft.
ne of water pumped/bailed before sampling: 0.75 gallons
PARTMENT:OF ENVIRONMENT 8 NATURAL RESOURCES
'ISIONbF WATER RESOURCES - INFORMATION PROCESSING UNIT
7 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617. Phone: [phone].
IRMIT Number:
Expiration Date: 8/31/2021
n -Discharge
UIC
'DES
Other W00001492
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump X Other: SDIBR Permit
FIELD ANALYSES:
pH 00400: 7_50 units
Spec. Cond. 00094:
Odor 000s5: _
Appearance
Date sample analyzed:
rbtl
11/09/2016 -11/15/2016
Laboratory Name: ALS Environmental
ni
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
mg/L
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead oto51
Coliform: MF Fecal 31616
/100mi-
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092
Coliform: MF Total 31504
NU MPN hodt Is
/100mL
hl I
Phosphorus: Total as P 00665
mg/L
Temp. 000lo: °C
µMhos
Certification No. 676
ug/L
mg/L
( ele. se mer or �g y lu i sampas)
Orthophosphate 70507
ni
Other ($y#cyjy Compounds and Concentration Units):
)issolved Solids:Total 70300 2,000
mg/L
Al - Aluminum 01105
mg/L
DJ
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC oo6ao
mg/L
Ca - Calcium oogte
ri
Chloride 00940 107
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total o1om
<10 ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron oto45
6,040 ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
- IPA tali method #
Total Ammonia oo61a
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen: NH3as N, Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625
ri
Ni - Nickel 01067
<40 ug/L
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs:
mg/L VOC Removal%
Steve Hart, PG, Principal, Hart &Hickman, PC (Authorized Agent) �
✓� /
Permittee (or Authorized Agent). Name and Title- Please print or type Signature of Perniltee (( Authorized Agn
GW -59 Rev. 8/2013
If WELL
DRY at
time of
sampling,
check
here: F-1

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: Occidental Chemical Corporation
Permit Name (if different):
Facility, Address: 5408 Holly Shelter Rd
SUBMIT FORM ON YELLOW PAPER ONLY
County New Hanover
act Person: David Guier Telephone#: [phone]
Location/Site Name: 34'22'18.4900", -077'51'46.3100" No. of wells to be sampled:
24
iEPARTMENT OF ENVIRONMENT 8. NATURAL RESOURCES
iMSION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
817 MAIL SERVICE CENTER, RALEIGH,.NC27699-1817. Phone: [phone]
ERMIT Number:
Expiration Date: 8/31/2021
on -Discharge
UIC
PDES
Other W00001492
YPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
L ID NUMBER (from Permit): MW -17 (CPW-7S) Date sample collected: 11/1/2016
Depth: 28 ft. Well Diameter: 4 in.
i to Water Level 82546: 6.03 ft. below measuring point Screened Interval: 12 ft. to 28 ft.
luring Point is 0.94 ft. above land surface Relative M.P. Elevation: 15.14 ft.
ne of water pumped/bailed before sampling: 0.75 gallons
11es for metals were collected unfiltered: ® YES ❑ NO and field acidified: ® YES ❑ NO
ate sample analyzed: 11/08/2016 - 11/12/2016 Laboratory Name: ALS Environmental
4RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N ooa15
mg/L
Coliform: MF Fecal 31616
/100ml-
Nitrate (NO3) as N 00620
mg/L
Coliform: MF Total 31504
/100ml-
Phosphorus: Total as P 00665
mg/L
(Note: Use MPNmethotltor highly turbid samples)
Orthophosphate 70507
mg/L
;solved Solids:Total 70300 1,620
mg/L
At -Aluminum o11o5
mg/L
pH (Lab) 00403
units
Ba - Barium oloo7
ug/L
TOC oo66o
mg/L
Ca - Calcium oo91e
mg/L
Chloride 00940 4.6
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
uglL
Chromium: Total 01034
<10 ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
Phenol 32730
ug/L
Fe - Iran 01045
6,870 ug/L
Sulfate oog45
mg/L
Hg - Mercury 71900
ug/L
lecific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610
mg/L
Mg - Magnesium 00927
mg/L
(Ammonia Nitrogen: NH3asN. Ammonia Nitrogen, Totso
Mn - Manganese 01055
ug/L
TKN as N 00625
mg/L
Ni - Nickel 01067
<40 ug/L
❑ Water Source Heat Pump ® Other: SDIBR Permit
FIELD ANALYSES:
pH 00400: 6_86 units Temp. 000lo.
Spec. Cond. oo094: µMhos
Odor 00085:
Appearance _
Pb - Lead olos1
Zn - Zinc 01092
Certification No. 676
ug/L
mg/L
oC DRY at
time of
Other (Specify jompounds and Concentration Units):
D
JE(
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes (1) ❑ No (0)
'd667a7a- , method #
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs:
mg/L VOC Removal%
GW -59 Rev. 812013

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
DEPARTMENT OF ENVIRONMENT$. NATURAL RESOURCES
DIVISION OF WATER RESOURCES- INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617Phone: [phone]
FACILITY INFORMATION Pease Print Clearly or Type
PERMIT Number: Expiration Date: 8/31/2021
Facility Name: Occidental Chemical Corporation
Non -Discharge UIC
NPDES Other W00001492
Permit Name (if different):
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Hayne NC 28249 County New Hanover
- '11� -'
❑ Spray Field ❑ Remediation:
Contact Person: David Guier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°22'25.7100", -077°51'58.5900"
No. of wells to be sampled: 24
❑ Water Source Heat Pump © Other: SDIBR Permit
(from Pem n
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW -18 (CPW-8S)
Date sample collected: 11/4/2016
FIELD ANALYSES:
WAS
Well Depth: 36 ft.
Well Diameter: 4 in.
pH 00400: 7_30 units Temp. 000to: °C
DRY at
Depth to Water Level 82546: 3.17 ft. below measuring point
Screened Interval: 21 ft. to
36 ft. Spec. Cond. 00094: pMhos
time of
sampling,
Measuring Point is 2.85 ft. above land surface
Relative M.P. Elevation: 7.95 ft.
Odor 00085:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here'.
Samples for metals were collected unfiltered: © YES
❑ NO and field acidified: 0 YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 11/09/2016 - 11/12/2016
Laboratory Name: ALS Environmental
Certification No. 676
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO2) as N oo61 s
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 /1 OOmL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092 ni
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P00665
mg/L
(Note: Use MEN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 407 mg/L
Al -Aluminum 01105
mg/L-'
pH (Lab) 00403 units
Be - Barium 01007
ug/L
TOC ooaao mg/L
Ca - Calcium 00916
mg/L UEC 2 8 9 G 16
Chloride 00940 109 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034 <10
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 <100
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/Lveli , method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L , method #
(Ammonia Nit ogan, NH3 as N. Ammonia Nitrogen, Total)
Mn -Manganese 01055
ug/L ,method #
TKN as N 00625 mg/L
Ni - Nickel 01067 <40
ug/L method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs:
mg/L
Effluent Total VOCs.
mg/L
VOC Removal%
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW -59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW -59 Rev. 812013
Effluent Total VOCs:
Signature at Permittee (or Authorized /
mg/L VOC Removal%
DEPARTMENT OF ENVIRONMENT&NATURAL RESOURCES -
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER RESOURCES 21INFORMATION-PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NO 27699-1617 'Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 8/31/2021
Facility Name: Occidental Chemical Corporation
Non -Discharge UIC
NPDES Other W00001492
Permit Name (if different):
Facility Address: 5408 Holly Shelter Rd
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Castle Hayne NC 28249 County New Hanover
"Al -"'
❑ Spray Field ❑ Remediation:
Contact Person: David Guier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34'22'21.7300", -077°5211.7100"
No. of wells to be sampled: 24
❑ Water Source Heat Pump ® Other: SDIBR Permit
(fmm Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW -19 (CPW-9S)
Date sample collected: 11/4/2016
FIELD ANALYSES:
WAS
Well Depth: 38 ft.
Well Diameter: 4 in,
pH 00400: 7.97 units Temp. 0001or 0C
DRY at
Depth to Water Level 82546: 2.85 ft, below measuring point
Screened Interval: 23 ft. to
38 ft. Spec. Cond. 00094: µMhos
time
sampling,
Measuring Point is 2.58 ft. above land surface
Relative M.P. Elevation: 8.28 ft.
Odor 000s5:
check
Volume of water pumped/bailed before sampling: 0.75
gallons
Appearance
here:❑
Samples for metals were collected unfiltered: © YES
❑ NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 11/09/2016 - 11/11/2016
Laboratory Name: ALS Environmental
Certification No. 676
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD oo335 mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead oio51 ug/L
Coliform: MF Fecal 31616 /100ml-
Nitrate (NO3) as N 00620
mg/L Zn -Zinc oio92 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P00665
mg/L
(Note. Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compylnjs and Concentration Units):
yj
issolved Solids:Total 70300 463 mg/L
AI - Alumin um of1os
mg/L
pH (Lab) 00403 units
Be - Barium 01007
ug/L
TOC o068o mg/L
Ca - Calcium costs
mg/L
Chloride 00940 99.5 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total olom <10
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug/L
Fe - Iron 01045 <100
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate oo945 mg/L
Hg - Mercury 71900
uglL Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L-4F96_e74- , method #
Total Ammonia oo6m mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen, NH, as N. Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 mg/L
Ni - Nickel 01067 <40
ug/L , method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW -59 Rev. 812013
Effluent Total VOCs:
Signature at Permittee (or Authorized /
mg/L VOC Removal%

TER QUALITY MONITORING:
E REPORT FORM
Facility Name: Occidental Chemical
Permit Name (if different):
NC 28249
SUBMIT FORM ON YELLOW PAPER ONLY
County New Hanover
act Person: David Guier Telephone#: [phone]
Location/Site Name: 34"22'13.9300", -077°52'19.0700" No. of wells to be sampled: 24
L ID NUMBER (from Permit): MW -20 (CPW-10S)
Depth: 35 ft.
i to Water Level 62546: 4.88 ft. below measuring point
.uring Point is 3.43 ft. above land surface
ne of water pumped/bailed before sampling: 0.75
Date sample collected: 11/2/2016
Well Diameter:
4 in.
Screened Interval:
20 ft.
Relative M.P. Elevation:
10.33
to 35 ft.
ft.
'ARTMENT OF ENVIRONMENT & NATURAL RESOURCES
)SION OF WATER RESOURCES INFORMATION PROCESSING UNIT
7 -MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
RMIT Number:
Expiration Date: 8/31/2021
n -Discharge
UIC
'DES
Other W00001492
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump ® Other: SDIBR Permit
WELL
FIELD ANALYSES: I WAS
pH 00400: 6.91 units Temp. 000to: °C DRY at
Spec. Cord. 00094: µMhos time of
samplin
Odor 000a5: check
Appearance here:F—
ate sample analyzed: 11/09/2016 - 11/11/2016 Laboratory Name: ALS Environmental
kRAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO3) as N 00615 mg/L Pb - Lead 01051
Coliform: MF Fecal 31616 /100ml- Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092
Coliform: MF Total 31504
/100mL
(Note: Use MPN method for highly turbid samples)
ml
solved Solids:Total 70300 498
mg/L
pH (Lab) 00403
units
TOC ooe80
mg/1-
g/LChloride
Chloride00940 92.8
mg/L
Arsenic 01002
ug/L
Grease and Oils 00552
mg/L
Phenol 32730
ug/L
Sulfate 00945
mg/L
ecific Conductance 00095
µMhos
Total Ammonia oo6lo
mg/L
(Ammonia Nitrogen', NH3as N; Ammonia Nitrogen, Total)
ug/L
TKN as N 00625
mg/L
Phosphorus: Total as P o06e5
mg/L
Orthophosphate 70507
ml
AI - Aluminum 01 los
mg/L
Be - Bar um 01007
ug/L
Ca - Calcium oo916
mg/L
Cd - Cadmium 01027
ug/L
Chromium: Total olo34
<10 ug/L
Cu - Copper 01042
mg/L
Fe - Iron 01045
<100 ug/L
Hg - Mercury 71900
ug/L
K - Potassium 00937
mg/L
Mg - Magnesium 00927
mg/L
Mn - Manganese o1o55
ug/L
Ni - Nickel 01067
<40 ug/L
Certification No. 676
ug/L
mg/L
Other (Specify Compounds and Concentration Units):
p
w
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes (1) ❑ No (0)
method #
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal
Steve Hart, PG Principal, Hart & Hickman, PC (Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW -59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING: .,
;
DEPARTMENT OF ENVIRONMENT. & NATURAL RESOURCES
DIVISION OF WATER RESOURCES -.INFORMATION-PROCESSING UNIT
,.
COMPLIANCE REPORT FORM
LABORATORY INFORMATION
1617 MAIL SERVICE CENTER, RALEIGH, NC 27 699-1 617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: 8/31/2021
Facility Name: Occidental Chemical Corporation
Date sample analyzed: 11/09/2016 - 11/14/2016
Non -Discharge UIC
Permit Name (if different):
Certification No. 676
NPDES Other WQ0001492
Facility Address: 5408 Holly Shelter Rd
and colloidal concentrations.
TYPE OF PERMITTED OPERATION BEING MONITORED
Castle Hayne NC 28249 County New Hanover
ElLagoon LlRemediation: Infiltration Gallery
-- 1u -.p
Nitrite (NO,) as N 00615
❑ Spray Field ❑ Remediation:
Contact Person: David Guier Telephone#: [phone]
Pb - Lead oio51 ug/L
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°22'31.7100", -077°51'38.6900" No. of wells to be sampled: 24
Nitrate (NO,) as N 00620
❑ Water Source Heat Pump ❑x Other: SDIBR Permit
WELL ID NUMBER (from Permit): MW -21 (CPW-5S)
Well Depth: 34 ft.
Depth to Water Level 82546: 6.78 ft. below measuring point
Measuring Point is 2.48 ft. above land surface
Volume of water pumped/bailed before sampling: 0.75
Samples for metals were collected unfiltered: © YES
Date sample collected: 11/3/2016
Well Diameter: 4 in.
Screened Interval: 19 ft. to 34 ft.
Relative M.P. Elevation: 9.88 ft.
gallons
❑ NO and field acidified: IN YES ❑ NO
FIELD ANALYSES:
pH 00400: 7.25 units Temp. 000lo: °C
Spec. Cord. 00094: µMhos
Odor 00085:
Appearance
WAS
DRY at
time of
sampling,
check
here: ❑
LABORATORY INFORMATION
Date sample analyzed: 11/09/2016 - 11/14/2016
Laboratory Name: ALS Environmental
Certification No. 676
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD 00335 mg/L
Nitrite (NO,) as N 00615
mg/L
Pb - Lead oio51 ug/L
Coliform: MF Fecal 31616 /100mL
Nitrate (NO,) as N 00620
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504 /100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Coa and Concentration Units):
31rjl
ninum
)issolved Solids:Total 70300 1,400 mg/L
Al - Alumo11o5
mg/L
pH (Lab) 00403 units
Be - Barium 01007
ug/L
€� 2 tr
TOC oo6eo mg/L
Ca - Calcium oo916
mg/L
Chloride 00940 286 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002 ug/L
Chromium: Total 01034
<10
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 uglL
Fe - Iron 01045
4,820
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095 µMhos
K - Potassium 00937
mg/L
vee -b-&— method #
Total Ammonia 00610 mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen, NH3asN; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug1L
method #
TKN as N 00625 mg/L
Ni - Nickel 01067
<40
ug/L
method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs:
mg/L
Effluent Total VOCs: mg/L VOC Removal%
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent) C, 1 Z
Permittee (or Authorized Agent) Name and Title - Please pant at type Signature of Perm) ee (or Authoriz Agen (Da
(Da
Rev. 8/2013

NDWATER QUALITY MONITORING:
LIANCE REPORT FORM
Name: Occidental Chemical Corporation
Name (if different):
Castle
SUBMIT FORM ON YELLOW PAPER ONLY
or
NC 28249 County New Hanover
act Person: David Guier Telephone#: [phone]
Location/Site Name: 34°22'14.4900", -077'51'31.0900" No. of wells to be sampled: 24
\RTMENTOF ENVIRONMENT & NATURAL RESOURCES
iION OF WATER RESOURCES - INFORMATION PROCESSING UNIT
MAICSERVICE CENTER, RALEIGH, NC 27669-1617 Phone: [phone]
PERMIT Number:
Expiration Date. 8/31/2021
Non -Discharge
UIC
NPDES
Other W00001492
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump ® Other: SDIBR Permit
WELL ID NUMBER (from Permit): MW -22 (CPW-2D)
Well Depth: 75 ft.
Depth to Water Level 82546: 14_30 ft. below measuring point
Measuring Point is 3 ft. above land surface
Volume of water pumped/bailed before sampling: 0.75
Samples for metals were collected unfiltered: ® YES
Date sample collected: 11/2/2016
Well Diameter: 4 in.
Screened Interval: 45 ft. to
Relative M.P. Elevation: 25.36 ft.
gallons
❑ NO and field acidified: IN YES ❑ NO
60 ft.
—
FIELD ANALYSES:
pH 004o0: 6.78 units Temp. 000to: °C
Spec. Cond. 00094: µMhos
Odor 00065:
Appearance
WAS
DRY at
time sampling,
ng,
check
here:❑
LABORATORY INFORMATION
Date sample analyzed: 11/09/2016 - 11/1112016
Laboratory Name: ALS Environmental
Certification No. 676
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L
Pb - Lead o1051 ug/L
Coliform: MF Fecal 31616
/100mL
Nitrate (NO3) as N ooszo
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Comper)n4s and Concentration Units):
DJ
issolved Solids:Total 70300 387
mg/L
Al - Aluminum olto5
mg/L
pH (Lab) 00403
units
Be - Barium 01007
ug/L
PEG c o
TOC 00660
mg/L
Ca - Calcium coats
ni
nt
Chloride oo940 10.4
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
uglL
Chromium: Total 01034
<10
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
uglL
Fe - Iron 01045
52160
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate ca945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
pecifc Conductance 00095
µMhos
K - Potassium 00937
mg/L
AQG48z method #
Total Ammonia oo610
mg/L
Mg - Magnesium 00927
mg/L
, method #
(Ammonia Nitrogen; NH�as N; Ammonia Ntlrogen. Total)
Mn - Manganese 01055
uglL
method #
TKN as N 00625
mg/L
Ni - Nickel 01067
<40
ug/L
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please pnnt or type
GW -59 Rev. 8/2013

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Name: Occidental Chemical Corporation
Name (if different):
Castle
act Person: David Guier
NC
,,
Location/Site Name: 34'22'19.9800". -077°51'25.3900"
L ID NUMBER (from Permit): MW -23 (CPW-3D)
Depth: 105 ft.
n to Water Level 82546: 21_86 ft. below measuring point
luring Point is 3 ft. above land surface
SUBMIT FORM ON YELLOW PAPER ONLY
County New Hanover
Telephone#: [phone]
No. of wells to be sampled: 24
'ARTMENT OF ENVIRONMENT & NATURAL RESOURCES
?SION`OF WATER RESOURCES -'INFORMATION PROCESSING UNIT
7 MAIL.SERVICE CENTER; RALEIGH; NC 27699-1617 Phone: [phone]
RMIT Number:
Expiration Date: 8/31/2021
n -Discharge
UIC
'DES
Other W00001492
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump ® Other: SDIBR Permit
Date sample collected: 11/2/2016 FIELD ANALYSES:
Well Diameter: 4 in. pH 004oa: 6.99 units Temp. 000lo: eC
Screened Interval: 57 ft. to 97 ft. Spec. Cond. 000g4: µMhos
Relative M.P. Elevation: 27.42 ft. Odor 00085:
ne of water pumped/bailed before sampling: 0.75 gallons
Appearance
Ile sample analyzed:
thod rb'E
11/09/2016 - 11/14/2016
Laboratory Name: ALS Environmental
mg/L
\RAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
mg/L
COD oo335
mg/L
Nitrite (NO2) as N om15
mg/L Pb - Lead a1o51
Coliform: MF Fecal 31616
/100ml-
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092
Coliform: MF Total 31504
N PN h hl
/100ml-
Phosphorus: Total as P00665
mg/L
Certification No. 676
ug/L
mg/L
( oto. uIAme for is y to i samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
;solved Solids:Total 70300 572
mg/L
Al -Aluminum 01105
mg/L
61
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC oo68o
mg/L
Ca - Calcium 0o916
mg/L
iDU 2 8.2016
Chloride 00940 41.0
mg/L
Cd - Cadmium cio27
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
<10 ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron oio4s
3,820 ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
,ecific Conductance 000ss
µMhos
K - Potassium 00937
mg/L
-VJDG-7e7e- , method #
Total Ammonia o06lo
mg/L
Mg - Magnesium 00927
mg/L
, method #
(Ammonia Nitrogen, NH3as N, Ammons Nitrogen, Total)
Mn - Manganese 01055
ug/L
method #
TKN as N 00625
mg/L
Ni - Nickel 01067
<40 ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs'. mg/L VOC Removal%
at
of
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW -59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
11/2/2016
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM s r
s
1617 MAIL SERVICE CENTER, RALEIGH,
NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Pease Print Clearly or Type
Nitrite (NO2) as N 00615
PERMIT Number:
Expiration Date: 8/31/2021
Facility Name: Occidental Chemical Corporation
Nitrate (NO3) as N 00620
Non -Discharge
UIC
Permit Name (if different):
mg/L
NPDES
Other WQ0001492
Facility Address: 5408 Holly Shelter Rd
Chloride oog4o 11.7
TYPE OF PERMITTED OPERATION BEING MONITORED
Castle Hayne NC 28249County New Hanover
ug/L
El Lagoon
El Remediation: Infiltration Gallery
',... -`
Chromium: Total 01034
❑ Spray Field
❑ Remediation:
Contact Person: David Guier Telephone#: [phone]
mg/L
❑ Rotary Distributor
❑ Land Application of Sludge
Well Location/Site Name: 34°22'24.6800", -077°51'25.8700" No. of wells to be sampled: 24
Phenol 32730
❑ Water Source Heat Pump
M Other: SDIBR Permit
L ID NUMBER (from Permit): MW -24 (CPW-4D)
Depth: 75 ft.
i to Water Level 82546: 22_31 ft. below measuring point
luring Point is 3 ft. above land surface
ne of water pumped/bailed before sampling: 0.75 gall
Aes for metals were collected unfiltered: M YES ❑ NO
Date sample collected:
11/2/2016
Well Diameter:
4 in.
Screened Interval:
60 k. to 75 ft.
Relative M.P. Elevation:
26.99 ft.
FIELD ANALYSES:
pH 00400: 7_08 units Temp. 000lo:
Spec. Cond. oao94: µMhos
Odor 000m:
Appearance
As sample analyzed:
11/09/2016 - 11/11/2016
Laboratory Name: ALS Environmental
mg/L
!I RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
isolved Solids:Total 70300 402
COD 00335
mg/L
Nitrite (NO2) as N 00615
mg/L Pb - Lead o1o51
Coliform: MF Fecal 31616
/100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc o1o92
Coliform: MF Total 315o4 /100mL
(Note- Use MPN method for hi hl turbid sem les)
Phosphorus: Total as P oo66s
mg/L
Certification No. 676
ug/L
mg/L
aC DRY at
time of
9 y p
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
isolved Solids:Total 70300 402
mg/L
Al -Aluminum 01105
mg/L
n j
—�
pH (Lab) OD403
units
Ba - Barium 01007
ug/L
TOC oD68o
mg/L
Ca - Calcium oosle
ni
A 2016
Chloride oog4o 11.7
mg/L
Cd - Cadmium o1D27
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
5,260 ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
<100 ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
ecific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VQG 7a7a , method #
Total Ammonia oo6lo
mg/L
Mg - Magnesium oo927
mg/L
, method #
(Ammonia Nitrogen, NHsas N, Ammonia Nitrogen. Total)
Mn - Manganese 01055
ug/L
, method It
TKN as N 00625
mg/L
Ni - Nickel 01067
<40 ug/L
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Steve Hart, PG, Principal, Hart & Hickman, PC (Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW -59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER RESOURCES INFORMATION. PROCESSING UNIT
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617. 'Phone: [phone]
FACILITY INFORMATION vfeasePrint clearly orType PERMIT Number: Expiration Date: 8/31/2021
Facility Name: Occidental Chemical Corporation Non -Discharge UIC
Permit Name (if different): NPDES Other WQ0001492
Facility Address: 5408 Holly Shelter Rd TYPE OF PERMITTED OPERATION BEING MONITORED
Castle Hayne NC 28249 County New Hanover ❑ Lagoon ❑ Remediation: Infiltration Gallery
_ 1 ❑ Spray Field ❑ Remediation:
Contact Person: David Guier Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: 34°22'31.7100", -077"51'38.6900" No. of wells to be sampled: 24 ❑ Water Source Heat Pump ® Other: SDIBR Permit
L ID NUMBER (from Permit): MW -25 (CPW-5D) Date sample collected: 11/3/2016
Depth. 99 ft. Well Diameter: 4 in.
1 to Water Level 82546: 5.83 ft. below measuring point Screened Interval: 59 ft. to 99 ft.
,uring Point is 2.61 ft, above land surface Relative M.P. Elevation: 10.01 ft.
ne of water pumped/bailed before sampling: 0.75 gallons
)les for metals were collected unfiltered: ❑77 YES ❑ NO and field acidified: 1717 YES rl NO
FIELD ANALYSES:
pH 00400; 7.68 units Temp. 000lo:
Spec. Cond.00094 µMhos
Odor 00085:
Appearance
aC IDRYat
time of
Date sample analyzed: 11/09/2016 - 11/17/2016
Laboratory Name: ALS Environmental
Certification No. 676
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N oo615
ni
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616
/100ml-
Nitrate (NO,) as N 00620
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100ml-
Phosphorus: Total as P 00665
mg/L
(Note: Use MPN method for highly turbid samples)
q Orthophosphate 70507
p (i 8 2()(fi
mg/L
Other (Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 2,230
mg/L
AI - Aluminumoilm
mg/L
pH (Lab) oo4os
units
Ba - Barium 01007
ug/L
TOC 00680
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 1,010
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034 <10
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045 <100
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
ipecific Conductance 00095
µMhos
K - Potassium 00937
mg/L
V4DL -fs7s- method #
Total Ammonia 00610
mg/L
Mg - Magnesium oo927
mg/L
method #
(Ammonia Nitrogen, NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01088
ug/L
,method #
TKN as N 00625
mg/L.
Ni - Nickel 01067 <40
ug/L
, method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs: mg/L
Effluent Total VOCs: mg/L VOC Removal%
_Steve Hart, PG, Principal, Hart 8 Hickman, PC (Authorized Agent)
Permittee (or Authorized Agent) Name and Title - Please print or type
GW -59 Rev. 8/2013
4
here: El

UNDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
or
Name: Occidental Chemical Corporation
Name (if different):
Address: 5408 Hollv Shelter Rd
SUBMIT FORM ON YELLOW PAPER ONLY
County New Hanover
act Person: David Guitar Telephone#: [phone]
Location/Site Name: 34°22'34.0100", -077'51'43.9000" No. of wells to be sampled: 24
DEPARTMENT OF ENVIRONMENT 8 NATURAL RESOURCES
DIVISION OF WATER RESOURCES- INFORMATION PROCESSING UNIT
1617 MAIL'. SERVICE CENTER; RALEIGH, NC 27699-1617 Phone: [phone]
PERMIT Number:
Expiration Date: 8/31/2021
Non -Discharge
UIC
NPDES
Other W00001492
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
L ID NUMBER (from Permit): MW -26 (CPW-6D) Date sample collected: 11/3/2016
Depth: 101 ft. Well Diameter: 4 in.
It to Water Level 82546:12.00 ft. below measuring point Screened Interval: 61 ft. to 101 ft.
:wring Point is 327 ft. above land surface Relative M.P. Elevation: 15.77 ft.
ne of water pumped/bailed before sampling: 0.75 gallons
Dles for metals were collected unfiltered: ® YES ❑ NO and field acidified: ON YES ❑ NO
❑ Water Source Heat Pump ® Other: SDIBR Permit
FIELD ANALYSES:
WAS
pH 00400: 11.10 units Temp. 000lo: °C
DRY at
Spec. Cond. oo094: µMhos
time of
sampling,
Odor 00085:
check
Appearance
here: ❑
ate sample analyzed: 11/09/2016 - 11/15/2016 Laboratory Name: ALS Environmental
I RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N 00615 Di mg/L Pb - Lead o1o51
Coliform: MF Fecal 31616 MOOT!- Nitrate (NO3) as N 00620 _ mg/L Zn - Zinc 01092"
Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 ""U G 6.1016mg/L
Certification No. 676
ug/L
mg/L
(Note. Use MPN method far highly tumid samples)
mg/L
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
naolved Solids:Total 70300 942
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC oo6eo
mg/L
Ca - Calcium oog16
mg/L
Chloride oo94o 233
mg/L
Cd - Cadmium 01027
ug1L
Arsenic 01002
ug/L
Chromium: Total 01034
<10 ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron o1o45
<100 ug/L
(Specify test and method #. ATTACH IAB REPORT.)
Sulfate oo945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
tecific Conductance 000gs
µMhos
K - Potassium 00937
mg/L
Y136 -aa? -9_ , method #
Total Ammonia oo610
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen. NH3 as N: Ammonia Nitrogen, Tata?)
Mn - Manganese 01055
ug/L
method #
TKN as N 00625
mg/L
Ni - Nickel 01067
<40 ug/L
method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs
mg/L
Effluent Total VOCs.
mg/L
VOC Removal%
lJvv-oe Rev. erzurl

ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
Name: Occidental Chemical Corporation
Name (if different):
Address: 5408 Holly Shelter Rd
SUBMIT FORM ON YELLOW PAPER ONLY
28249 County New Hanover
act Person: David Guier Telephone#: [phone]D4
Location/Site Name: 34°22'18.4900", -077"51'46.3100" No. of wells to be sampled: 24
WELL ID NUMBER (from Permit): MW -27 (CPW-7D)
Well Depth: 98 ft.
Depth to Water Level 82546: 6_04 ft. below measuring point
Measuring Point is 0.09 ft. above land surface
Volume of water pumped/bailed before sampling: 0.75
Samples for metals were collected unfiltered: ® YES ❑
1ENT OF ENVIRONMENT 8
OFWATERRESOURCES-
:RMIT Number:
Expiration Date. 8/31/2021
m -Discharge
UIC
'DES
Other W00001492
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump ® Other: SDIBR Permit
Date sample collected: 11/1/2016 FIELD ANALYSES:
Well Diameter: 4 in. pH oo400: 7.14 units Temp. 000to_
Screened Interval: 58 ft. to 98 ft. Spec. Cord. 00694: I
Relative M.P. Elevation: 14.59 ft. Odor 00085:
gallons
NO
Appearance
Date sample analyzed: 11/08/2016 - 11/14/2016 Laboratory Name: ALS Environmental
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051
Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092
Coliform: MF Total 31504 /100mL
(Note Use Ml method for highly turbid Moroea)
Ived Solids:Total 70300 704
mg/L
pH (Lab) 00403
units
TOC omen
mg/L
Chloride oo940 33.7
mg/L
Arsenic 01002
ug/L
Grease and Oils 00552
mg/L
Phenol 32730
ug/L
Sulfate oti
mg/L
ific Conductance 000g5
µMhos
Total Ammonia 00610
mg/L
(Ammonia Nitrogen; NH, as N, Ammonia Nitrogen, Total)
mg/L
TKN as N 00625 mg/L
For Remediation Systems Only (Attach Lab Reports):
Phosphorus: Total as P 00665
mg/L
Orthophosphate 70507
mg/L
AI-Aluminumolim
mg/L
Be - Barium 01007
ug/L
Ca - Calcium oog16
mg/L
Cd - Cadmium 01027
ug/L
Chromium: Total 01034
<10 uglL
Cu - Copper 01042
mg/L
Fe - Iron 01045
3,190 ug/L
Hg - Mercury 71900
ug/L
K - Potassium 00937
mg/L
Mg - Magnesium 00927
mg/L
Mn - Manganese 01055
ug/L
Ni - Nickel 01067
<40 ug/L
Certification No. 676
ug/L
ri
WELL
eC DRY at
time of
Other (Specify Compounds and Concentration Units):
1),1
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ❑ Yes (1) ❑ No (0)
-V96-seaa , method #
method #
method #
method #
Influent Total VOCs: mg/L Effluent Total VOCs
mg/L VOC Removal%
Steve Hart, PG,. Principal, Hart & Hickman, PC (Authorized Agent) `� C / �� t
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee or Authorized Agent)
GW -59 Rev. 8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: Occidental Chemical Corporation
Permit Name (if different):
Facility Address: 5408 Holly Shelter Rd
Castle Hayne NC 28249 County New Hanover
Contact Person: David Guier Telephone#: [phone]
Well Location/Site Name: 34`22'03.3000", -077°51'56.8900" No. of wells to be sampled: 24
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
DIVISION OF WATER. RESOURCES -INFORMATION PROCESSING UNIT
1617'MAIL.sERVICE CENTER,: RALEIGH, NC27699-1617 Phone: [phone]
PERMIT Number:
Expiration Date. 8/31/2021
Non -Discharge
UIC
NPDES
Other W00001492
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
L ID NUMBER (from Permit): MW -28 (CPW-12S) Date sample collected: 11/1/2016
Depth: 34 ft. Well Diameter: 4 in.
h to Water Level 82546: 4_30 ft. below measuring point Screened Interval: 19 ft. to 34 ft.
wring Point is 0.81 ft. above land surface Relative M.P. Elevation: 14.11 ft.
ne of water pumped/bailed before sampling: 0.75 gallons
ples for metals were collected unfiltered: ® YES ❑ NO and field acidified: ® YES ❑ NO
❑ Water Source Heat Pump © Other: SDIBR Permit
FIELD ANALYSES:
pH 00400: 6_85 units
Spec. Cond. 000g4:
Odor 00085- _
Appearance
Ae sample analyzed:
11/08/2016 - 11/12/2016
Laboratory Name: ALS Environmental
mg/L
1RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
;solved Solids:Total 70300 1,690
COD 00335
mg/L
Nitrite (NO2) as N oo615
mg/L Pb - Lead olos1
Coliform: MF Fecal 31616
/100mL
Nitrate (NO3) as N 00620
mg/L Zn - Zinc 01092
Coliform: MF Total 31504
Nis U MPN hod f h'
/100mL
ht t b d I
Phosphorus: Total as P 00665
mg/L
Temp. 000io: eC
µMhos
Certification No. 676
ug/L
mg/L
( oe. se met or ig y ur i sari
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
;solved Solids:Total 70300 1,690
mg/L
AI -Aluminum o11o5
mg/L
QJ
pH (Lab) 00403_units
Ba - Barium 01007
ug/L
TOCoo68o
mg/L
Ca- Calcium 00916
mg/L
DEC 28 2016
Chloride 00940 7.1
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 0100
ug/L
Chromium: Total 01034
<10 ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
29,200 uglL
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
,ecific Conductance 00095
µMhos
K - Potassium 00937
mg/L
_Vol , method #
Total Ammonia oo610
mg/L
Mg - Magnesium oo927
mg/L
method #
(Ammonia Nitrogen. NH, as N, Ammonia Nitrogen, Total)
Mn - Manganese oloss
ug/L
, method #
TKN as N 00625
mg/L
Ni- Nickel 01067
<40 ull
method #
For Remediation Systems Only (Attach Lab Reports)
Influent Total VOCs-
mg/L
Effluent Total VOCs:
mg/L
VOC Removal%
DRY at
time of
sampling,
check
here: E]
wv-o9 Rev. arzula

Summary of Affected Wells (Page 1 of 2)
Former Occidental Chemical Corporation Facility
Castle Hayne, NC
H&H Job No. OXY -003
Well ID
Sample Date
TDS
(mg/L)
Chloride
(mg/L)
Iron
(Ng/L)
Chromium
(Ng/L)
pH
(s.u.)
15A NCAC 2L Standard
500
250
300
10
6.5-8.5
MW -1 (CPW-13S)
03/11/15
950
10
25,000
5.0 U
6.44
07/16/15 1,000 9.7 21,000 5.0 U
6.28
11/12/15 900 8.7 19,000 5.0 U
6.59
03/14/16 1,010 8.3 24,400 IOU
6.09
07/12/16
928
8.2
19,300
20
6.01
08/09/16*
NA
NA
NA
IOU
6.37
11103/16
940
8.4
19,300
IOU
6.31
03/12/15
630
97
3,200
5.0 U
7.04
07/14/15 640 110 3,600 5.0 U
7.02
11/10/15 650 110 4,100 5.0 U
7.21
MW -2 (CPW-14S)
03/15/16
704
127
3,820
IOU
7.13
07/13/16 723 120 3,290 IOU
6.60
11/01/16 700 14.7 3,760 IOU
6.90
.-03/13/15
540
170
100 U
5.0 U
8.04
MW -3 (CPW-15S)
07/15/15
550
180
100 U
5.0 U
7.95
11/10/15 590 190 100 U 5.0 U
8.18
03/15/16 389 192 280 IOU
9.11
07/13/16 647 191 100 U IOU
7.53
11/02/16 546 194 100 U IOU
7.77
MW -8 (CPW-8DR)
03/13/15
460
110
2,100
5.0 U
7.54
07/15/15 730 230 1 400 5.0 U
7.52
11/11/15 710 220 1,300 5.0 U
7.53
03/16/16 634 198 100 U IOU
8.21
07/14/16 656 202 100 U IOU
7.59
11/04/16 688 257 720 IOU
7.18
MW -9 (CPW-9D)
03/13/15
2,200
170
100 U
5.0 U
7.24
07/15/15 2,000 170 170 5.0 U
7.26
11/11/15 2,000 180 230 5.0 U
7.41
03/16/16 1,930 198 380 IOU
7.38
07/14/16 1,830 178 100 U IOU
7.17
11/02/16 1 810 200 100 U IOU
7.36
MW
03/13/15
1,400
130
100 U
5.0 U
9.91
07/15/15 1,400 140 100 U 5.0 U
9.68
11/12/15 1,300 130 110 5.0 U
9.92
-10 (CPW-10D)
03/15/16
1,310
162
100 U
IOU
9.29
07/14/16 1,170 158 100 U IOU
7.83
11/02/16 1,230 120 100 U IOU
9.57
MW -11 (CPW-1 S)
02/17/15
350
4.4
11,000
5.8
6.67
08/31/15 350 4.7 9,700 2.8
6.82
03/24/16 320 4.1 5,900 IOU
7.07
11/02/16 327 5.0 7,860 IOU
6.73
MW -12 (CPW-12D)
03/12/15
1,000
IOU
13,000
5.0 U
7.04
07/14/15 1,100 7.0 13,000 5.0 U
6.88
11/09/15 1,000 6.8 12,000 5.0 U
7.21
03/14/16 1,060 6.2 13,200 IOU
7.09
07/13/16 1,030 6.1 10,400 IOU
6.55
11/01/16 1 000 6.2 12,300 IOU
6.25
03/11/15
1,100
140
2,000
5.0 U
6.88
07/16/15
1,200
140
1,900
5.0 U
6.87
11/12/15 840 100 130 5.0 U
7.75
MW -13 (CPW-13D)
03/14/16
1,130
150
1,200
IOU
7.03
07/12/16 822 101 100 U 152
7.47
08/09/16* NA NA NA IOU
6.92
11/03/16 1,060 166 1,540 IOU
6.61
MW -14 (CPW-14D)
03/12/15
730
120
3,400
5.0 U
6.96
07/14/15 730 140 3,600 5.0 U
6.92
11/10/15 790 140 3,600 5.0 U
7.10
03/15/16 762 128 3,150 IOU
7.08
07/13/16 566 82.6 100 U IOU
7.37
11/01/16 888 160 3,250 IOU
6.66
MW -15 (CPW-15D)
03/13/15
690
170
180
5.0 U
7.44
07/15/15 700 170 390 5.0 U
7.57
11/09/15 680 170 1,300 5.0 U
7.59
03/15/16 668 185 220 IOU
7.52
07/13/16 648 181 500 IOU
7.00
11102/16 604 146 980 IOU
7.06
_MW-1.6-(CPW,6S)-
03/11/15
1,100
110
490
7.4
6.72'
07/16/15 1,200 97 330 5.9
6.71
11/12/15 690 47 890 5.0 U
6.71
--03/_15/16-_ _.-- _ 2,130 - - --- ---- -. 522 _ 6,410 _ 10-U
7.33
07/12/16 760 56.8 370 11
6.09
08/10/16* NA NA NA IOU
6.72
11/03/16 2 000 107 6,040 IOU
7.50
MW -17 (CPW-7S)
03/12/15
1,400
IOU
4,000
5.0 U
7.12
07/14/15 2,000 5.0 U 9,500 5.0 U
6.86
11/10/15 1,400 5.0 U 7,900 5.0 U
7.14
03/16/16 1,460 3.7 100 U IOU
7.36
07/13/16 1,720 2.9 3,750 IOU
6.61
11/01/16
1,620
4.6
6,870
IOU
6.86
MW -18 (CPW-8S)
03/13/15
710
230
150
5.0 U
7.61
07/15/15 410 88 170 5.0 U
7.62
11/11/15 430 99 130 5.0 U
7.63
03/16/16 446 92.8 120 IOU
7.48
07/14/16 429 94.7 100 U IOU
7.00
11/04/16 407 109 100 U IOU
7.30
MW -19 (CPW-9S)
03/13/15
530
91
100 U
5.0 U
8.06
07/15/15 480 91 150.00 5.0 U
7.50
11/11/15 440 89 100 U 5.0 U
7.95
03/16/16 2,420 91.0 100 U IOU
8.05
07/14/16 495 94.6 180 IOU
7.13
11/04/16 1 463 1 99.5 100 U IOU
7.97
Attachment A (Page 1 of 2)
S2016AAR ster Projects\Oxychem\Quarry\Quarry L -Cap Sampling\2016W ovember 2016\Summary of Affected Wells Hart &Hickman, PC

Summary of Affected Wells (Page 2 of 2)
Former Occidental Chemical Corporation Facility
Castle Hayne, NC
H&H Job No. OXY -003
Well ID
Sample Date
TDS
(mg/L)
Chloride
(mg/L)
Iron
(Ng/L)
Chromium
(Ng/L)
pH
(s.u.)
15A NCAC 2L Standard
500
250
300
10
6.5-8.5
MW -20 (CPW-10S)
03/13/15
580
85
450
5.0 U
6.98
07/15/15 450 88 100 U 5.0 U
7.34
11/11/15 460 89 350 5.0 U
7.26
03/15/16 557 91.4 410 lou
7.13
07/14/16 519 87.1 130 10 U
6.63
11/02/16 498 92.8 100 U lou
6.91
MW -21 (CPW-5S)
03/11/15
1,300
230
230
8.0
7.49
07/16/15 1,300 220 2,800 8.5
7.43
11/12/15 1,300 230 3,400 8.7
7.43
03/14/16 1,440 285 1,010 IOU
7.66
07/12/16 1,330 227 2,960 18
7.01
08/10/16* NA NA NA 101-1
7.34
11/03/16 1 400 286 4,820 IOU
7.25
MW -22 (CPW-2D)
02/17/15
800
16.0
13,000
3.7
6.74
08/31/15 530 13.0 6,800 5 U
7.01
03/23/16 553 12.3 5,170 lou
6.84
11/02/16 387 10.4 5,160 lou
6.78
MW -23 (CPW-3D)
02/17/15
610
25.0
9,000
3.3
6.78
09/01/15 620 27.0 3,400 5 U
7.17
03/23/16 633 24.1 3,860 lou
7.26
11/02/16 572 41.0 3,820 lou
6.99
MW -24 (CPW-4D)
02/18/15
390
13.0
4,000
5,400
6.65
08/31/15 390 13.0 930 5,700
7.07
03/24/16 412 12.2 130 5,110
7.33
09/14/16 408 12.2 130 6,840
7.13
11/02/16 402 11.7 100 U 5,260
7.08
MW -25 (CPW-5D)
03/11/15
2,800
1,100
100 U
5.0 U
7.12
07/16/15 2,900 1,100 140 5.0 U
7.15
11/12/15 2,800 1,100 100 U 5.0 U
7.52
03/14/16 2,520 1,000 100 U 10 U
7.33
07/12/16 2,340 1,000 100 U 101-1
7.43
11/03/16 2,230 1,010 100 U 10 U
7.68
MW -26 (CPW-6D)
03/11/15
1,500
450
1,300
5.0 U
7.19
07/16/15 2,600 550 8,300 5.0 U
7.24
11/12/15 2,000 490 3,100 5.0 U
7.35
03/15/16 1,430 434 800 lou
7.40
07/12/16 779 209 100 U 11
11.41
08/10/16* NA NA NA lou
7.06
11/03/16 942 233 100 U lou
11.10
MW -27 (CPW-7D)
03/11/15
740
57
2,200
5.0 U
7.46
07/14/15 700 18 3,200 5.0 U
7.20
11/10/15 770 55 3,100 5.0 U
7.58
03/14/16 5,270 51.0 2,330 lou
7.37
07/13/16 661 30.1 100 U 11
7.54
08/10/16* NA NA NA lou
7.18
11/01/16 704 33.7 3,190 lou
7.14
MW -28 (CPW-12S)
03/12/15
1,000
12
16 000
5.0 U
7.06
07/14/15 980 6.2 21,000 5.0 U
6.94
11/09/15 950 7.2 20,000 5.0 U
7.24
03/14/16 1,200 8.8 19,900 lou
7.14
07/13/16 1,300 1 5.7 27,600 IOU
6.55
11/01/16 1 690 7.1 29,200 lou
6.85
15A NCAC 2L Standard
500
250
300
10
6.5-8.5
Note
Bold concentration exceeds the 2L standard
*well resampled in August 2016 for analysis of total chromium due to anomalous chromium detection in July 2016 sample
Attachment A (Page 2 of 2)
SAAAA-Master Projects\Oxychem\Quarry\Quarry L -Cap Sampling\2016W ovember 2016\Summary of Affected Wells Hart & HickmanPC
12/13/2016 f

Lavender, Charles
Ftrims • I Nam - L eaekamy oom •
Sent: Wednesday, AptN 14, 2010 8:67 AM . .
To: Lavender,GWee -
Matey -mb
Subject FM QW qually monkodng talmd of Penh# WQGW1402
Good Morning Cherles,
Bee Dr. StehmanIs reply. .
In the GGT 99A question #6, say 01madiate notification wan not made since these elevated
cossdit'OnV were already 7mawa to the agency (see the enclosed mail). 9f
Nam'J'm&, ph.])., P.H.
Oleua Springs Holdings, Ina.
[phone] (p)
Imam h. baeR®oasy. com
-.. -Original ldessage----- ,
fronts 8tebmea, Charles(mailto:charles.stebmatt�gncdenr.gatrI
Beats Wednesday,, Aps:il 14, 2020 9:40 AM
Tos Sagk,. Nam H.
Subjects no, Gff Vality monitoring report of PG=dt: # WQ0002.02
Naas,
Ragazdizg YCFUr inquiry about truthfully answering the gmaticar on the GPP59A, I• believe
YOU should masher questions 4, 5, & 6 as yes. This office was notified in this past about
elw mted =0 aondit3,c=, . especially at well # i7, so you do stat need to notify this office
immediately. a However, when we regeive your report, we win be sending mm a letter of
aasusera about the sitaatioa. We letter rill request that you ltfrovido an e2ggaaatioa for
Me cosidition and a discussion of ghat is P=Poaed to aarract the problem.
ChaVISs f. Stebsesta, Ph.D.,P.G. '
mo�tal zogrem Baperpisor xxx
D`F
tlUaltiy, Aquifer Px+otec -Acs: Bectian tPiWIIgtast Regipual Office, 127
OLUUMd Drive► Ssttesseian VIUdngt=,MMtb Cd=11na 28403
Acnes [phone], £exs [phone]
DrBQa s Per MMM*ive Order no. 1S0, all a -mails seat to and fsnm this account are
smubject to tbs north Carolina Public Records Law wad may be disclosed to third parties.
------Origin=al isessags-----
From: Nam a. ZmL%m=r.c= rmailtogmm a. BAL%m=W.aamj
Bents - ZhteedaY, 4rJ.2 13, 2010 12:31, PH
To: Beohman; Charles
Subjects OR quality monitoritsg report of Permit # WQ0001492
Dr..etebman, -
X am praparL29 for a groundwater quality moaitoxiug report is eccozdaace with the Non-
Disctsarge Pertsit . (0000014.92). Ttsis is my f3 ret: time preparing this zeport:. r, isave one
question ort GN -5-9A' Bums sa dt:oring wells located beyond the xaviev boUndary Mme exceeded
the• established standards over several yams. Therafore, I win say Yes to Question ##B.
The GN-S9A Porm says, 61f the ensurer to Questicn :#6 is YBB, aoatact the ragiassal office
l meediately for guidaace.0 Please advice as haw to xespand to this statement. Cb=mium
bas always been iu ooptpliaaca but other peratnetere such as TDS and chloride have sometimes
shown exoeadance.

Your respanse to"this email, is greatly appreciated. i will document your response on the
tai-S9A Form. Then Z' will sign and submit it to the NCMI NR. '
Shm'eaek, Ph.D.s P.S.
ace - GW* .
(979) 687-7tO9 (p)
nam h. baekomy. com .
.

A
November 21, 2016
Ms. Sheri Finn
GHD Services Inc.
2055 Niagara Falls Blvd., Suite 3
Niagara Falls, NY 14304
Laboratory Results for: Castle Hayne 258-402-D02-3100
Dear Ms.Finn,
Service Request No:R1611784
Enclosed are the results of the sample(s) submitted to our laboratory November 07, 2016
For your reference, these analyses have been assigned our service request number R1611784.
All analyses were performed according to our laboratory's quality assurance program. The test
results meet requirements of the NELAP standards except as noted in the case narrative report. All
results are intended to be considered in their entirety, and ALS Environmental is not responsible for
use of less than the complete report. Results apply only to the items submitted to the laboratory for
analysis and individual items (samples) analyzed, as listed in the report. The measurement
uncertainty of the results included in this report is within that expected when using the prescribed
method(s) for analysis of these samples, and represented by Laboratory Control Sample control
limits. Any events, such as QC failures, which may add to the uncertainty are explained in the report
narrative.
Respectfully submitted,
ALS Group USA, Corp. dba ALS Environmental
Brady Kalkman
Project Manager
ADDRESS 1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
PHONE [phone] FAX [phone]
ALS Group USA, Corp.
dba ALS Environmental
1 of 102

ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsgiobal.com
RIGHT SOL -U -TIONS RIGI-IT PARTNER
2 of 102

AEriulronmental 1565 Jefferson Rd, Building 300, Rochester, NY 14623 1585-288-5380 I www.alsglobal.com
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.) Service Request: R1611784
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap Date Received: 11/7/16
Sample Matrix: Water
CASE NARRATIVE
All analyses were performed consistent with the quality assurance program of ALS Environmental. This report contains analytical
results for samples designated for Tier II data deliverables, including results of QC samples analyzed from this delivery group.
Analytical procedures performed by the lab are validated in accordance with NELAC standards. Any parameters that are not
included in the lab's NELAC accreditation are identified on a "Non -Certified Analytes" report in the Miscellaneous Forms Section of
this report. Individual analytical results requiring' further explanation are flagged with qualifiers and/or discussed below. The flags
are explained in the Report Qualifiers and Definitions page in the Miscellaneous Forms section of this report.
Sample Receipt
Twenty nine water samples were received for analysis at ALS Environmental on.11/07/2016. Any discrepancies noted upon initial
sample inspection are noted on the cooler receipt and preservation form included in this data package. The samples were
received in good condition and consistent with the accompanying chain of custody form. Samples are refrigerated at <6°C upon
receipt at the lab except for aqueous samples designated for metals analyses, which are stored at room temperature.
Metals Analyses:
No significant anomalies were noted with this analysis.
General Chemistry Analyses:
No significant anomalies were noted with this analysis.
Approved by ���� /�� Date 11/21/2016
3 of 102

SAMPLE DETECTION SUMMARY
LIEN'T'ID::"MW-1 (CPW13$) "`
; ' ", Lab,ID: 81611784-006
MDL
PQL
Units
Analyte
Results Flag MDL
-----------
PQL
--------------------
Units
Method
------- -----------------------------
Chloride
8.4 1.0
2.0
mg/L
300.0
Solids, Total Dissolved (TDS)
940 8
20
mg/L
SM 2540 C -
Iron, Total
19.3 0.02
0.10
mg/L
200.7
AnalyteResults
Flag
MDL
PQL
Units
Method
---------------------------------------------------------------------------------------------------------------------------------------------------------------------
Chloride
166
4.0
8.0
mg/L
300.0
Solids, Total Dissolved (TDS)
1060
8
20
mg/L
SM 2540 C -
Iron, Total
1.54
0.02
0.10
mg/L
200.7
LIENT ID rMW 2 (CPW 14S) ,L ab ID 81611784-008
,
Analyte
Results Flag
MDL
-----------------
PQL
Units
Method
-Method-
----------------------------------
Chloride
Chloride
-- --
147
4.0
8.0
mg/L
300.0
Solids, Total Dissolved (TDS)
700
8
20
mg/L
SM 2540 C -
Iron, Total
3.76
0.02
0.10
mg/L
200.7
LIENT'SID`f�MIN-14"'(CPW=`14D), _,� , x x r x ✓.; �/,,��
s-,
Analyte
Results Flag
MDL
PQL
Units
Method --
Chloride
160
4.0
8.0
mg/L
300.0
Solids, Total Dissolved (TDS)
888
8
20
mg/L
SM 2540 C -
Iron, Total
3.25
0.02
0.10
mg/L
200.7
s,o-,� 5�,�ry ..+, "m, w's �vl.r,. .( ?i� rvY.r,✓:�✓Y rHwS✓nr, va d.ezv i�xa�[r'u ��✓tF,.,
..N :, uX"'¢: v,ro.'v.sr_'�.f '7.. ✓$.LXd✓. ,'X, Y+, -u. a .�. aa�
.z+"5, x�a'x
.XNR eS
v. SXx �.
X..,u .�
Analyte
Results Flag
MDL
PQL
Units
Method
------------------------------------------------------------------------------------------------------------------------------
Chloride
194
4.0
8.0
mg/L
300.0
Solids, Total Dissolved (TDS)
546
4
11
mg/L
SM 2540 C-
IQ 16 1 ,84 0 1
Analyte
Results Flag
MDL
PQL
Units
Method
Chloride
146
4.0
8.0
mg/L
300.0
Solids, Total Dissolved (TDS)
604
8
20
mg/L
SM 2540 C -
Iron, Total
0.98
0.02
0.10
mg/L
200.7
Analyte
Results Flag
MDL
PQL
Units
Method
Chloride
257
4.0
8.0
mg/L
300.0
Solids, Total Dissolved (TDS)
688
8
20
mg/L
SM 2540 C -
Iron, Total
0.72
0.02
0.10
mg/L
200.7
Analyte
Results
- -
Flag MDL
-- - - - ----
PQL
-- -------------------------------------------
Units
Method
-- - - - -----------------------------------------------------------------------------------------------------
Chloride
109
2.0
4.0
mg/L
300.0
Solids, Total Dissolved (TDS)
407
4
10
mg/L
SM 2540 C-
4 of 102

SAMPLE DETECTION SUMMARY
Chloride
Analyte
Results. Flag MDL
PQL
Units
Method_
Chloride
---
200 4.0
8.0
mg/L
-
300.0
Solids, Total Dissolved (TDS)
1810 11
30
nno0-
8K8254OC'
GK8254OC-
A]
am1oo
Analyte
Results Flag MDL
PQL
Chloride
88.5 1.0
2.0
mg/L
300.0
Solids, Total Dissolved [7OG)
463 4
10
mg/L
GK02G4OC-
Analyte
Results Flag MDL
PQL
Units
Method
Chloride
120 4.0
8.0
mg/L
300.0
Solids, Total Dissolved /TO8\
1230 8
20
mg/L
8K8254OC-
PL
Analyte
Results Flag MDL
PQL
Units
Method
Chloride
92.8 1.0
2.0
mg/L
300.0
Solids, Total Dissolved (TOS)
498 4
10
mg/L
SKA354OC-
LIENT
Analyte
EkemmUtm Flag MDL
PQL
Method
Chloride
6.3 1.0
---Units
2.0
mg/L
300.0
8o|ido, Total Dissolved (TDS)
1000 0
20
mg/L
SM 3540 C -
|non, Total
13.3 0.02
0.10
mg/L
200.7
Analyte
ykmsmUte Flag MDL
PQL
Units
Method
Chloride
7.1 1.0
2.0
mg/L
300.0
Solids, Total Dissolved (TOS)
1890 8
20
mg/L
8K8254OC'
Iron. Total
29.2 0.02
0.10
mg/L
200.7
Analyte
Results Flag MDL
PQL
Units
Method
Chloride
107 2.0
4.0
mg/L
300.0
Solids, Total Dissolved (TO8)
2000 15
40
mg/L
8K8254OC'
|non.Toto|
8.04 0.02
010
mg/L
2007
30 mg/L
GK8254OC-
am1oo
Analyte
Results Flag MDL
PQL
Units
Method
Chloride 233 4.0 8.0 mg/L 300.0
Solids, Total Dissolved (TDG) 942 8 20 mg/L SK8254OC-
Analyte - --- -
Results
Flag MDL
PQL Units
Method_
---
Chloride
---
4.8
1.0
2.0 nnz8-
-
300.0
Solids, Total Dissolved (TDS)
1620
11
30 mg/L
GK8254OC-
am1oo

AALSEnUiff'ou-Melitag
SAMPLE DETECTION SUMMARY
LIENT81611784
«„
Analyte
--Flag--MDL--PQL---Units
--Method
----
---------------------------------------------
Iron, Total
----Results
6.87 0.02
0.10
mg/L
200.7
lab I 6117 23
Analyte
- ---- ---Results -Flag - MDL-
PQL
------------------
Units
Method
-----------------------------------------------------------------------------
Chloride
33.7 1.0
2.0
mg/L
300.0
Solids, Total Dissolved (TDS)
704 4
10
mg/L
SM 2540 C -
Iron, Total
3.19 0.02
0.10
mg/L
200.7
LIENT*ID�'` MW 27 (CPW 5S) "' �� Lab ID 81611784-024
Analyte
Results Flag MDL
PQL
Units
--Units ---
Method
--------------------------------------------------------------------------------------------------------------
Chloride
286 10
20
mg/L
300.0
Solids, Total Dissolved (TDS)
1400 8
20
mg/L
SM 2540 C -
Iron, Total
4.82 0.02
0.10
mg/L
200.7
Analyte
- Results Flag MDL
PQL
Units
Method
Chloride
1010 20
40
m /L
300.0
Solids, Total Dissolved (TDS)
2230 18
50
mg/L
SM 2540 C-
,,..,". ,. �"'", "' + f!'; +y J rv, ; i :✓ +-Y" ✓ dh.Y 5l fi d 4 .� Fd Y [" 4 k "�, p �.
LIENT (DNfW 11`ACPW 1`S�` � �� � Lab ID `81611784 026
a,
Analyte
Results Flag MDL
PQL
Units
Method
Chloride
5.0 1.0
2.0
mg/L
300.0
Solids, Total Dissolved (TDS)
327 4
10
mg/L
SM 2540 C -
Iron, Total
7.86 0.02
0.10
mg/L
200.7
LIEN7'(D "MW"22`"(CPWLab ID: R1611784 027
AnalyteResults
Flag MDL
PQL
Units
Method
-----------------------------------------------------------------------------------------------------------------------------------------------------------
Chloride
10.4 1.0
-2.0
mg/L
300.0
Solids, Total Dissolved (TDS)
387 4
10
mg/L
SM 2540 C -
Iron, Total
5.16 0.02
0.10
mg/L
200.7
Analyte
- --- - --- - - - - --- -- - -- - -- -
Results Flag MDL
- - - -- --- - - - --- -- - -- -- ---------
PQL
-------- ----
Units
- -
Method
- ---- -- -- -
- -- -- - --
Chloride
41.0 1.0
2.0
m /L
g
300.0
Solids, Total Dissolved (TDS)
572 4
10
mg/L
SM 2540 C -
Iron, Total
3.82 0.02
0.10
mg/L
200.7
N
ENTIDJ
LI BMW 24 (CPW 4D) ' '' ` '`' Lab ID 87611784-029
Analyte
Results Flag MDL
PQL ----------
Units
-----------d
Metho
------------------------------------------------------------------------------------------------------------------------------------------------------
Chloride
11.7 1.0
2.0
mg/L
300.0
Solids, Total Dissolved (TDS)
Chromium, Total
6of102
402 4 10 mg/L SM 2540 C-
5.26 0.0009 0.010 mg/L 200.7

ALS Environmental—Rochester Laboratory
1 565 ,Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS RIGHT PARTNE=R
7 of 102

Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.) Service Request: R1611784
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
SAMPLE CROSS-REFERENCE
SAMPLE #
CLIENT SAMPLE ID
DATE
TIME
R1611784-006
MW -1 (CPW 13S)
11/3/2016
0925
R1611784-007
MW -13 (CPW-13D)
11/3/2016
0835
R1611784-008
MW -2 (CPW-14S)
11/1/2016
1700
R1611784-009
MW -14 (CPW-14D)
11/1/2016
1540
R1611784-010
MW -3 (CPW-15S)
11/2/2016
1000
R1611784-011
MW -15 (CPW-15D)
11/2/2016
0835
R1611784-012
MW -8 (CPW-8DR)
11/4/2016
0910
R1611784-013
MW -18 (CPW-8S)
11/4/2016
1020
R1611784-014
MW -9 (CPW-9D)
11/4/2016
1145
R1611784-015
MW -19 (CPW-9S)
11/4/2016
1240
R1611784-016
MW -10 (CPW-10D)
11/2/2016
1245
R1611784-017
MW -20 (CPW-10S)
11/2/2016
1120
R1611784-018
MW -12 (CPW-12D) ,
11/1/2016
0930
R1611784-019
MW -28 (CPW-12S)
11/1/2016
1100
R1611784-020
MW -16 (CPW-6S)
11/3/2016
1325
R1611784-021
MW -26 (CPW-6D)
11/3/2016
1215
R1611784-022
MW -17 (CPW-7S)
11/1/2016
1420
R1611784-023
MW -27 (CPW-7D)
11/1/2016
1300
R1611784-024
MW -21 (CPW-5S)
11/3/2016
1545
R1611784-025
MW -25 (CPW-5D)
11/3/2016
1425
R1611784-026
MW -11 (CPW-1 S)
11/3/2016
1040
R1611784-027
MW -22 (CPW-2D)
11/2/2016
1640
R1611784-028
MW -23 (CPW-3D)
11/2/2016
1525
R1611784-029
MW -24 (CPW-4D)
11/4/2016
1525
8 of 102
Printed 11/21/2016 9:19:33 AM Sample Summary

\LS SRO
565 Jefferson Rd Bldg 300, Suite 360 Rochester, NY 14623 585-288-5380 FAX [phone] PAGE 1 OF
be64
*•
'i- �•�
I
e
t2)?, ' a'`'
roject Name: Castle Hayne - TA ual SDRS
Monitoring rt 1\ u 8DMG`+
'roject Manager: Sheri Finn Company: GHD
:ompany/Address: 2055 Niagara Falls Blvd
Phone: [phone]
b
:ity, State, Zip' Niagara Falls, NY 14304 Email: [e-mail]
e
*Also report to Scott Drury(Hart&oHickmafn) via ail: [e-mail]**
4-E
"o
o
R
5e
.am ler s Signature:U.W
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z
n
T
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M
Sample I.D..
Date
Time
LAB 1D
Matrix
E~ N,
I.A.,
IRENURKS
MW -1• (CPW-13S)
GW
2
X
X
X
1%1W-13•(CPW-13D)
GW
2
X
X
X
MW -2 (CPW-14S)
GW
2
X
X
X
MW -14 (Cl -W -14D)
GW
2
X
X
X
]%IW-3-(CPW-15S)
GW
2
X
X
X
MW -15 (CPW-15D) '
GW
2
X
X
X
MW -8 (CP'W-8DR)
GW
2
X
X
X
MW -18 (CPW-8S)
GW
2
X
X
X
MW -9 (CPW-9D)
GW
2
X
X
X
MW -19 (CPW-9S)
GW
2
X
X
X
JRNAROUND REQUIREMENTS
REPORT REQUIREMENTS'
Comments/Special Instructions:
24 hr 48 hr 5 BD
X I. Routine Report: Results and Method Blank
_
X Standard (15 BD)
(Surrogate, as required)
Provide FAX Preliminary Results
tequested Report Date:
H. Results w/ QC (Dup., MS, MSD
III. Results (with QC and Calibration
Summaries)
as req)
t J I lei ✓,l` O J��
K7 d I '11014 .7
nvoice Information
'.O. # 4502201560
IV. ASP -B
GHQ Services Inc.
Castle Hayne 268402-oo2-3200
till to: GSHI
V. CLP
111111111111111111111 HE IN 11111111111111111
" EDD?:
RECEIVED BY:
RELINQUISHED BY:
RECEIVED BY:
ML INQUIS BY::
;ignature:,�f?�/l� ��5
Signature:
Signature:
Signature:
Tinted Name: Mike Edmonds
Printed Name:
Printed Nane:
Printed Name: n
Firm:cz-
Mundy
Firm: ,b �%� `
Firm:
Firm: /7
)ate/Time: ��' �6 "oa
Date/Time:
Date/Time:
Date/Time: r�^�
9 of 102

ALS SR#
1565 Jefferson Rd Bldg 300, Suite 360 Rochester, NY 14623 585-288-:5380 FAX [phone] PAGE 2` OF
P UU �(//��}}6
e-�s-:s€
Name: Castle Hayne TrrAl S135
nne�aR-Monitoring,
•
Project Number:: 6448DMProJect
Project Manager: Sheri Finn Company: GAD
H
Q
y
Company/Address: 2055 Niagara Falls Blvd
Phone: [phone]
fl
City, State, Zip: Niagara Falls, NY 14304 Email:
[e-mail]
**Also report to Scott Drury (Hart & Hickman) via email: [e-mail]**Rn
o
o
oo
fq
Sampler's Signature:
la
U $
9
o
z
oS
T
Z
..
a
Sample I.D.
Date
Time
LAB ID
Matrix
F.
U
F
REMARKS
MW -10 (CPW-1013)
GW
2
X
Jt
X
MW -20 (CPW-10S)
GW
2
X
X
X
MW -12 (CPW-12D)
GW
2
X
X
X
!�
MW -28 (CPW-12SD)
GW
2
X
X
X
MW -16 (CPW-6S)
GW
2
X
X
X
MW -26 (CPW-6D)
GW
2
X
X
X
MW -17 (CPW-7S)
GW
2
X
X
X
MW -27 (CPW-7D)
GW
2
X
X
X
MW-21(CPW-5S)
GW
2
X
X
X
MW -25 (CPW-5D)
GW
2
X
X
X
URNAROUND REQUIREMENTS
REPORT REQUIREMENTS
Comments/Special Instructions:
24 hr 48 hr 5 BD
X' I. Routine Report: Results and Method Blank
c h,'b m %
X Standard (15 BD)
(Surrogate, as required)
Provide FAX Preliminary Results
II. Results w/ QC (Dup., MS, MSD as req)
R equested Report Date:
III. Results (with QC and Calibration
Summaries)
81611784 5
Invoice Information
P.O. # 4502201560
IV. ASI'_B
o 00
castle Hayne �6a.�vic
Bill to: GSHI
V. CLP
IIIIIIIII111111111111111 III VIII VIII IIIA IIII IIII
EDD?:
RECEIVED BY:
Signature: —_
RELINQUISHED BY:
Signature:
RECEIVED BY:
Signature-
RELINQUISHED BY:
Signature: 21
Printed Name: Mike Edmonds
Printed Name:
Printed Name:
Printed Name. -
Firm: Mundy
Firm:
Firm:
Firm:
---
Date/Time:? _ I7
, II �0
Date!Time: // /f/-ilnyy l ;��
Date/Time:
Date/Time: J�ris;
10 of 102

Aenuironme-ntall
CHAIN OF CUSTODY/LARORATORY ANALYSIS REQUEST- FORM
• Rochester, NY -14623 [phone] [phone] (fax). PAGE OF
1565 Jefferson Road, Buildi g 300 Suite 360 Ro h 1
P IeoI Na e `(„A I (.,
.� ,,.
Pro)ecl Number
ANALYSIS REQUESTEp (include Method Number and Container Preservative)
j
M�
Projectonager
Repr4cc R(f�'t(�iFr••'�"
larr2
PRESERVATIVE
6 0 :: I
A t.{C
�i
Preservative Key '
0. NONE
1. HCL
Company/Address i
w
Z
y
2. HNO3
3. H2SO4�1
i
Iy��
�y �r
�+A - t
PKI
Z
V
� v ,�
'�
4. NaOH
5., Zn. Acetate i
( d,/��.�,��
N rGi'Tn
`�LL
U
C .o o
U e S �� c •
C
6. McOH
7. NaHSOq I'
sv� —
Phone 0
19 f I/A J
a
WID
j
zSampler's
a U0 e
`C
ALTERNATE
8. Other
REMARKS/
DESCRIPTION TION Ii
Sarrplees Prints Name
Signature
0 0 0
JI, FOR OFFICE USE SAMPLING
IU ONLY LAB ID DATE TIME! MATRIX
CLIENT SAMPLE
(CAW
Nffi
t✓ SC tr
n
SPECIAL INSTRUCTIONS/COMMENTS r
Metais �I
c.17ro011 tY41
i
See QAPP O
STATE WHERE SAMPLES WERE COLLECTED
RELINQUISHED BY i RECEIVED BY
Signa I y Signature
nted Name
Printed
Flnn Firm
�,�
Dateliime t tn 6 Date/time/� r 4. /� 171'
Distribution: White - Lab Copy, Yellow, - Return to Originator
RELINQUISHED BY
TURNAROUND REQUIREMENTS REPORT REQUIREMENTS
INVOICE INFORMATION
RUSH (SURCHARGES APPLY) I. Results Only
II. Results + QC Summaries Po sn
7 day -2 day —a day — (LCS. DUP. MS/MSD as required) LL' tV
4day .--5 day B1LLT ��
III. Results+ OC and Calibration
Summaries
REQUES' ED REPOR� DATE
d _ IV. Data Validation Report with Raw Data
r
Edata —Yes —No
RECEIVED BY RELINQUISHED BY RECEIVED BY
i
Signature Signature
Si a
P. me
Printed Name i
Printed Name
Firm
FFirm R1611784
[weTme GHD Services Inc.
Date/Time t tSJ� Castle H
G� ayne 268.102_1)023100
I llllllll
11 of 102 1111111111111111111111111111111111111 IN
1

R1611784 5
GHD Services Inc.
Castle Hayne 268-002-D023100
Q. I Illlllll III IIIII IIIII HE 1111111111111111111 IN..
�(��� (C®®➢err Receipt and Preservation Check Form
Project/Client Folder Number
Cooler received on d- S' "/ by: t COURIER: ALS UPSFED$X VELOCITY CLIENT
1
I Were Custody seals on outside of cooler?
N
2
Custody papers properly completed (ink, signed)?
'
3
Did all bottles arrive in good condition (unbroken)?
Ti N
4
Circle: et: ce IIDry Ice Cel packs present
Y' N
5a
]Perchlorate samples have required headspace?
Y N
5b
Did VOA vials, Alk,or Sulfide have sig* bubbles?
Y
6
Where did the bottles originate? i ALS/ROC CLIENT
7
Soil VOA received as: Bulls Encore 5035set A.
8. Temperature Readings Date: fl-�- l Time: C'qGO ID: R# IR#8 From: f e6pAank Sample Bottle
Observed Temp (°C) .
Correction Factor (°C)
Corrected Temp (°C) , .Z
Within 0-6°C? N Y N Y N Y N Y N Y N Y N
If <0°C, were samples frozen? Y N 1 Y N Y N Y N Y N I Y N I Y rj
If out of Temperature, note packing/ice condition: Ice melted Poorly Packed same uay ltule
&Client Approval to Run Samples: Standing Approva! Client aware at drop-off .^Client notified :
All samples held in storage location:
by
oil - �'- �%
at
-�
5035 samples placed in storage location:
by
on
at
>12
Cooler Breakdown: Date: Time: 13.16 by:
1. Were all bottle labels complete (i. e. analysis, preservation, etc.)?
2. Did all bottle labels and tags agree with custody papers? N�
3. Were correct containers used for the tests indicated? • YDS NO
4. Were 5035 vials acceptable (no extra labels, not leaking)? YES NO
5. Air Samples: Cassettes / Tubes Intact Canisters Pressurized Tedlar(R Rags Inflated
pH
Reagent Yes No Lot Received Exp
Sample ID
Vol.Lot Added Fina]
HPROD
1.1GFB
HTR
Added I pH
>12
NaOH
S03
I MARRS
<2
HN01 aW 26d 56
<2
H2SO4
<4
NaHSO4
Residual
For CN If+, contact PM to
Chlorine
Phenol add Na2S203 (CN),
(-
and 522 ` ascorbic (phenol).
Na2S203 -
ZnAcetate - - **Not to be tested before analysis - pH tested and
HCl ** ** recorded by VOAs on a separate worksheet
Bottle lot numbers:
Other Comments:
PC Secondary Review:
Yes=A I1
samples OK
No=Sampics
were
preserved at
The lab as
listed
PM OK to
Adjust:
CLRES
BULK
DO
FLDT
HPROD
1.1GFB
HTR
LL3541
PH
SUB
S03
I MARRS
ALSREV
*significant air bubbles: VOA > 5-6 mm : WC >1 in. diameter
P:\INTRANET\QAQC\Fornis Controlled\Cooler Receipt rl2.doc 12 of 102 8/11/16

ALS Environmental—Rochester Laboratory
1565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsgiobal.com
RIGHT SOLUTIONS ' RIGHT PARTNER
13 of 102

REPORT QUALIFIERS AND DEFINITIONS
U Analyte was analyzed for but not detected.
The sample quantitation limit has been
corrected for dilution and for percent
moisture, unless otherwise noted in the case
narrative.
Estimated value due to either being a
Tentatively Identified Compound (TIC) or
that the concentration is between the MRL
and the MDL. Concentrations are not verified
within the linear range of the calibration. For
Dol): concentration >40% difference between
two GC columns (pesticides/Arclors).
B Analyte was also detected in the associated
method blank at a concentration that may
have contributed to the sample result.
E Inorganics- Concentration is estimated due to
the serial dilution was outside control limits.
E Organics- Concentration has exceeded the
calibration range for that specific analysis.
D Concentration is a result of a dilution,
typically a secondary analysis of the sample
due to exceeding the calibration range or that
a surrogate has been diluted out of the sample
and cannot be assessed.
* Indicates that a quality control parameter has
exceeded laboratory limits. Under the
"Notes" column of the Form I, this qualifier
denotes analysis was performed out of
Holding Time.
+ Correlation coefficient for MSA is <0.995.
N Inorganics- Matrix spike recovery was outside
laboratory limits.
N Organics- Presumptive evidence of a compound
(reported as a TIC) based on the MS library search.
S Concentration has been determined using Method
of Standard Additions (MSA).
W Post -Digestion Spike recovery is outside control
limits and the sample absorbance is <50% of the
spike absorbance.
P Concentration >40% (25% for CLP) difference
between the two GC columns.
C Confirmed by GC/MS
Q DoD reports: indicates a pesticide/Aroclor is not
confirmed (>100% Difference between two GC
columns).
X See Case Narrative for discussion.
MRL Method Reporting Limit. Also known as:
LOQ Limit of Quantitation (LOQ)
The lowest concentration at which the method
analyte may be reliably quantified under the
method conditions.
MDL Method Detection Limit. A statistical value
derived from a study designed to provide the lowest
concentration that will be detected 99% of the
time. Values between the MDL and MRL are
estimated (see J qualifier).
H Analysis was performed out of hold time for LOD Limit of Detection. A value at or above the MDL
tests that have an "immediate" hold time which has been verified to be detectable.
criteria. ND Non -Detect. Analyte was not detected at the
# Spike was diluted out. concentration listed. Same as U qualifier.
e _15L
d =
Rochester Lab ID # for State Certifications'
Connecticut ID # PHO556
Delaware Accredited
Maine ID #NY0032
Nebraska Accredited
New Hampshire ID #
294100 A/B
DoD ELAP #65817
New Jersey ID # NY004
Pennsylvania ID# 68-786
Florida ID # E87674
New York ID # 10145
Rhode Island ID # 158
Illinois ID #200047
North Carolina #676
Virginia #460167
' Analyses were performed according to our laboratory's NELAP-approved quality assurance program and any applicable state or agency
requirements. The test results meet requirements of the current NELAWIM standards or state or agency requirements, where applicable, except as
noted in the case narrative. Since not all analyte/method/matrix combinations are offered for state/NELAC accreditation, this report may contain
results which are not accredited. For a specific list of accredited analytes, contact the laboratory or go to httn://www.alsglobal.com/en/Our-
Services/Life-Sciences/Environmental/Do�-,mloads/North-America-Downloads
1 X :.i U 1, 0 "i' 10 t S 14 of 102 11 T i I Alk T N l R

ALS Laboratory Group
15 of 102
Acronyms
ASTM
American Society for Testing and Materials
A2LA
American Association for Laboratory Accreditation
CARB
California Air Resources Board
CAS Number
Chemical Abstract Service registry Number
CFC
Chlorofluorocarbon
CFU
Colony -Forming Unit
DEC
Department of Environmental Conservation
DEQ
Department of Environmental Quality
DHS
Department of Health Services
DOE
Department of Ecology
DOH
Department of Health
EPA
U. S. Environmental Protection Agency
ELAP
Environmental Laboratory Accreditation Program
GC
Gas Chromatography
GC/MS
Gas Chromatography/Mass Spectrometry
LUFT
Leaking Underground Fuel Tank
M
Modified
MCL
Maximum Contaminant Level is the highest permissible concentration of a
substance allowed in drinking water as established by the USEPA.
MDL
Method Detection Limit
MPN
Most Probable Number
MRL
Method Reporting Limit
NA
Not Applicable
NC
Not Calculated
NCASI
National Council of the Paper Industry for Air and Stream Improvement
ND
Not Detected
NIOSH
National Institute for Occupational Safety and Health
PQL
Practical Quantitation Limit
RCRA
Resource Conservation and Recovery Act
SIM
Selected Ion Monitoring
TPH
Total Petroleum Hydrocarbons
tr
Trace level is the concentration of an analyte that is less than the PQL but
greater than or equal to the MDL.
15 of 102

ALn.J V. V.F ---, < V. F.
dba ALS Environmental
Analyst Summary report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Service Request: R1611784
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Name: MW -1 (CPW-13S) Date Collected: 11/3/16
Lab Code: R1611784-006 Date Received: 11/7/16
Sample Matrix: Water
Analysis Method Extracted/Digested By Analyzed By
200.7 CBURLESON NMANSEN
300.0 CWOODS
SM 2540 C-1997(2011) KWONG
Sample Name: MW -13 (CPW-13D) Date Collected: 11/3/16
Lab Code: R1611784-007 Date Received: 11/7/16
Sample Matrix: Water
Analysis Method Extracted/Digested By Analyzed By
200.7 CBURLESON NMANSEN
300.0 CWOODS
SM 2540 C-1997(2011) KWONG
Sample Name: MW -2 (CPW-14S) Date Collected: 11/1/16
Lab Code: R1611784-008 Date Received: 11/7/16
Sample Matrix: Water
Analysis Method Extracted/Digested By Analyzed By
200.7 CBURLESON NMANSEN
300.0 CWOODS
SM 2540 C-1997(2011) KWONG
Sample Name: MW -14 (CPW-14D) Date Collected: 11/1/16
Lab Code: R1611784-009 Date Received: 11/7/16
Sample Matrix: Water
Analysis Method Extracted/Digested By Analyzed By
200.7 CBURLESON NMANSEN
300.0 CWOODS
SM 2540 C-1997(2011) KWONG
Printed 11/21/2016 9:19:36 AM Superset Reference: 16-000040023 0 rev 00
16 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analyst Summary report
Client:
GHD Services Inc. (Formerly
Conestoga -Rovers & Associates,
Service Request: R1611784
Project:
Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Name:
MW -3 (CPW-15S)
Date Collected: 11/2/16
Lab Code:
R1611784-010
Date Received: 11/7/16
Sample Matrix:
Water
Analysis Method
Extracted/Digested By
Analyzed By
200.7
CBURLESON
NMANSEN
300.0
CWOODS
SM 2540 C-1997(2011)
KWONG
Sample Name:
MW -15 (CPW-15D)
Date Collected: 11/2/16
Lab Code:
R1611784-011
Date Received: 11/7/16
Sample Matrix:
Water
Analysis Method
Extracted/Digested By
Analyzed By
200.7
CBURLESON
NMANSEN
300.0
CWOODS
SM 2540 C-1997(2011)
KWONG
Sample Name:
MW -8 (CPW-8DR)
Date Collected: 11/4/16
Lab Code:
R1611784-012
Date Received: 11/7/16
Sample Matrix:
Water
Analysis Method
Extracted/Digested By
Analyzed By
200.7
CBURLESON
NMANSEN
300.0
CWOODS
SM 2540 C-1997(2011)
KWONG
Sample Name:
MW -18 (CPW-8S)
Date Collected: 11/4/16
Lab Code:
R1611784-013
Date Received: 11/7/16
Sample Matrix:
Water
Analysis Method
Extracted/Digested By
Analyzed By
200.7
CBURLESON
NMANSEN
300.0
CWOODS
SM 2540 C-1997(2011)
KWONG
Printed 11/21/2016 9:19:36
AM
Superset Reference: 16-0000400230 rev 00
17 of 102

ALU V ■ -V V --, l..Vl F.
dba ALS Environmental
Analyst Summary report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Service Request: R1611784
Project: Castle Hayne 258-402-DO2-3100/6448 - L -Cap
Sample Name: MW -9 (CPW-9D) Date Collected: 11/4/16
Lab Code: R1611784-014 Date Received: 11/7/16
Sample Matrix: Water
Analysis Method Extracted/Digested By Analyzed By
200.7 CBURLESON NMANSEN
300.0 CWOODS
SM 2540 C-1997(2011) KWONG
Sample Name: MW -19 (CPW-9S) Date Collected: 11/4/16
Lab Code: R1611784-015 Date Received: 11/7/16
Sample Matrix: Water
Analysis Method Extracted/Digested By Analyzed By
200.7 CBURLESON NMANSEN
300.0 CWOODS
SM 2540 C-1997(2011) KWONG
Sample Name: MW -10 (CPW-IOD) Date Collected: 11/2/16
Lab Code: R1611784-016 Date Received: 11/7/16
Sample Matrix: Water
Analysis Method Extracted/Digested By Analyzed By
200.7 CBURLESON NMANSEN
300.0 CWOODS
SM 2540 C-1997(2011) KWONG
Sample Name: MW -20 (CPW-10S) Date Collected: 11/2/16
Lab Code: R1611784-017 Date Received: 11/7/16
Sample Matrix: Water
Analysis Method Extracted/Digested By Analyzed By
200.7 CBURLESON NMANSEN
300.0 CWOODS
SM 2540 C-1997(2011) KWONG
Printed 11/21/2016 9:19:36 AM Superset Reference: 16-0000400230 rev 00
18 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analyst Summary report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Service Request: R1611784
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Name: MW -12 (CPW-12D) Date Collected: 11/1/16
Lab Code: R1611784-018 Date Received: 11/7/16
Sample Matrix: Water
Analysis Method Extracted/Digested By Analyzed By
200.7 CBURLESON NMANSEN
300.0 CWOODS
SM 2540 C-1997(2011) KWONG
Sample Name: MW -28 (CPW-12S) Date Collected: 11/1/16
Lab Code: R1611784-019 Date Received: 11/7/16
Sample Matrix: Water
Analysis Method Extracted/Digested By Analyzed By
200.7 CBURLESON NMANSEN
300.0 CWOODS
SM 2540 C-1997(2011) KWONG
Sample Name: MW -16 (CPW-6S) Date Collected: 11/3/16
Lab Code: R1611784-020 Date Received: 11/7/16
Sample Matrix: Water
Analysis Method Extracted/Digested By Analyzed By
200.7 CBURLESON NMANSEN
300.0 CWOODS
SM 2540 C-1997(2011) KWONG
Sample Name: MW -26 (CPW-6D) Date Collected: 11/3/16
Lab Code: R1611784-021 Date Received: 11/7/16
Sample Matrix: Water
Analysis Method Extracted/Digested By Analyzed By
200.7 CBURLESON NMANSEN
300.0 CWOODS
SM 2540 C-1997(2011) KWONG
Printed 11/21/2016 9:19:36 AM Superset Reference: 16-0000400230 rev 00
19 of 102

--- -V_F VUA't. Vl F.
dba ALS Environmental
Analyst Summary report
Client:
GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Service Request: R1611784
Project:
Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Name:
MW -17 (CPW-7S)
Date Collected: 11/1/16
Lab Code:
R1611784-022
Date Received: 11/7/16
Sample Matrix:
Water
Analysis Method
Extracted/Digested By
Analyzed By
200.7
CBURLESON
NMANSEN
300.0
CWOODS
SM 2540 C-1997(2011)
KWONG
Sample Name:
MW -27 (CPW-7D)
Date Collected: 11/1/16
Lab Code:
R1611784-023
Date Received: 11/7/16
Sample Matrix:
Water
Analysis Method
Extracted/Digested By
Analyzed By
200.7
CBURLESON
NMANSEN
300.0
CWOODS
SM 2540 C-1997(2011)
KWONG
Sample Name:
MW -21 (CPW-5S)
Date Collected: 11/3/16
Lab Code:
R1611784-024
Date Received: 11/7/16
Sample Matrix:
Water
Analysis Method
Extracted/Digested By
Analyzed By
200.7
CBURLESON
NMANSEN
300.0
CWOODS
SM 2540 C-1997(2011)
KWONG
Sample Name:
MW -25 (CPW-5D)
Date Collected: 11/3/16
Lab Code:
R1611784-025
Date Received: 11/7/16
Sample Matrix:
Water
Analysis Method
Extracted/Digested By
Analyzed By
200.7
CBURLESON
NMANSEN
300.0
GNITAJOUPPI
SM 2540 C-1997(2011)
KWONG
Printed 11/21/2016 9:19:36
AM
Superset Reference: 16-0000400230 rev 00
20 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analyst Summary report
Client:
GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Service Request: R1611784
Project:
Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Name:
MW -11 (CPW-1S)
Date Collected: 11/3/16
Lab Code:
R1611784-026
Date Received: 11/7/16
Sample Matrix:
Water
Analysis Method
Extracted/Digested By
Analyzed By
200.7
CBURLESON
NMANSEN
300.0
CWOODS
SM 2540 C-1997(2011)
KWONG
Sample Name:
MW -22 (CPW-2D)
Date Collected: 11/2/16
Lab Code:
R1611784-027
Date Received: 11/7/16
Sample Matrix:
Water
Analysis Method
Extracted/Digested By
Analyzed By
200.7
CBURLESON
NMANSEN
300.0
CWOODS
SM 2540 C-1997(2011)
KWONG
Sample Name:
MW -23 (CPW-3D)
Date Collected: 11/2/16
Lab Code:
R1611784-028
Date Received: 11/7/16
Sample Matrix:
Water
Analysis Method
Extracted/Digested By
Analyzed By
200.7
CBURLESON
NMANSEN
300.0
CWOODS
SM 2540 C-1997(2011)
KWONG
Sample Name:
MW -24 (CPW-4D)
Date Collected: 11/4/16
Lab Code:
R1611784-029
Date Received: 11/7/16
Sample Matrix:
Water
Analysis Method
Extracted/Digested By
Analyzed By
200.7
CBURLESON
NMANSEN
300.0
CWOODS
SM 2540 C-1997(2011)
KWONG
Printed 11/21/2016 9:19:36
AM
Superset Reference: 16-0000400230 rev 00
21 of 102

INORGANIC PREPARATION METHODS
The preparation methods associated with this report are found in these tables unless discussed in the case narrative.
Water/Liquid Matrix
Analytical Method
Preparation Method
200.7
200.2
200.8
200.2
6010C
3005A/3010A
6020A
ILM05.3
9014 Cyanide Reactivity
SW846 Ch7, 7.3.4.2
9034 Sulfide Reactivity
SW846 CV, 7.3.4.2
9034 Sulfide Acid
Soluble
9030B
9056A Bomb (Halogens)
5050A
9066 Manual Distillation
9065
SM 4500 -CN -E Residual
Cyanide
SM 4500 -CN -G
SM 4500 -CN -E WAD
Cyanide
SM 4500 -CN -1
Solid/Soil/Non-Aqueous Matrix
Analytical Method
Preparation
Method
6010C
3050B
6020A
3050B
6010C TCLP (131 1)
extract
3005A/3010A
6010 SPLP (1312) extract
3005A/3010A
7196A
3060A
7199
3060A
9056A Halogens/Halides
5050
300.0 Anions/ 350.1/
353.2/ SM 232013/ SM
5210B/ 9056A Anions
DI extraction
For analytical methods not listed, the preparation
method is the same as the analytical method
reference.
..a-a...a91-114..... ou-1 . ,.._-='.,,....,rzg ,,�Z....MM:.',x,w=
P:\INTRANET\QAQC\Forms Controlled\Prep Methods Inorganic rev l.doc 1/19/15
22 of 102

ALS EnvUmonnmemtal--Roch ester Laboratory
1565 Jefferson Road. Building 300. Suite 360' Rochester. NY 14623
Phone (S0S)Z88'S30OFax (S85)Z00'B475
RIGHT SOLUTIONS RIGHT PAR -1 NERI
000f102

ALS Environmental—Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS fUGHT"PARTNER
24 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -1 (CPW-13S)
Lab Code: R1611784-006
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/03/16 09:25
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:37 AM Superset Reference: 16-0000400230 rev 00
25 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 11:15
11/08/16
Iron, Total
200.7
19.3
mg/L
0.10 1
11/10/16 11:15
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 11:15
11/08/16
Printed 11/21/2016 9:19:37 AM Superset Reference: 16-0000400230 rev 00
25 of 102

HLA %31 Uup UAt&, l.Vl P.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -13 (CPW-13D)
Lab Code: R1611784-007
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/03/16 08:35
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/20169:19:37 AM Superset Reference: 16-0000400230 rev 00
26 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 11:45
11/08/16
Iron, Total
200.7
1.54
mg/L
0.10 1
11/10/16 11:45
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 11:45
11/08/16
Printed 11/21/20169:19:37 AM Superset Reference: 16-0000400230 rev 00
26 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -2 (CPW-14S)
Lab Code: R1611784-008
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/01/16 17:00
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:38 AM Superset Reference: 16-0000400230 rev 00
27 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 12:28
11/08/16
Iron, Total
200.7
3.76
mg/L
0.10 1
11/10/16 12:28
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 12:28
11/08/16
Printed 11/21/2016 9:19:38 AM Superset Reference: 16-0000400230 rev 00
27 of 102

ALU ".-F
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -14 (CPW-14D)
Lab Code: R1611784-009
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/01/16 15:40
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:38 AM Superset Reference:16-0000400230 rev 00
28 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 12:34
11/08/16
Iron, Total
200.7
3.25
mg/L
0.10 1
11/10/16 12:34
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 12:34
11/08/16
Printed 11/21/2016 9:19:38 AM Superset Reference:16-0000400230 rev 00
28 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -3 (CPW-15S)
Lab Code: R1611784-010
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/02/16 10:00
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:38 AM Superset Reference: 16-0000400230 rev 00
29 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 12:40
11/08/16
Iron, Total
200.7
0.10 U
mg/L
0.10 1
11/10/16 12:40
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 12:40
11/08/16
Printed 11/21/2016 9:19:38 AM Superset Reference: 16-0000400230 rev 00
29 of 102

ALU Vl V V--, t.Vl F.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -15 (CPW-151))
Lab Code: R1611784-011
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/02/16 08:35
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:38 AM Superset Reference: 16-0000400230 rev 00
30 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 12:46
11/08/16
Iron, Total
200.7
0.98
mg/L
0.10 1
11/10/16 12:46
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 12:46
11/08/16
Printed 11/21/2016 9:19:38 AM Superset Reference: 16-0000400230 rev 00
30 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -8 (CPW-8DR)
Lab Code: R1611784-012
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/04/1609:10
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:38 AM Superset Reference: 16-0000400230 rev 00
31 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 12:52
11/08/16
Iron, Total
200.7
0.72
mg/L
0.10 1
11/10/16 12:52
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 12:52
11/08/16
Printed 11/21/2016 9:19:38 AM Superset Reference: 16-0000400230 rev 00
31 of 102

PWIUO 1J1 UUP V U '' Uz F.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -18 (CPW-8S)
Lab Code: R1611784-013
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/04/16 10:20
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:38 AM Superset Reference: 16-0000400230 rev 00
32 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 12:58
11/08/16
Iron, Total
200.7
0.10 U
mg/L
0.10 1
11/10/16 12:58
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 12:58
11/08/16
Printed 11/21/2016 9:19:38 AM Superset Reference: 16-0000400230 rev 00
32 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -9 (CPW-9D)
Lab Code: R1611784-014
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/04/16 11:45
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/20169:19:38 AM Superset Reference: 16-0000400230 rev 00
33 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 13:16
11/08/16
Iron, Total
200.7
0.10 U
mg/L
0.10 1
11/10/16 13:16
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 13:16
11/08/16
Printed 11/21/20169:19:38 AM Superset Reference: 16-0000400230 rev 00
33 of 102

dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -19 (CPW-9S)
Lab Code: R1611784-015
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/04/16 12:40
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:38 AM Superset Reference: 16-0000400230 rev 00
34 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil. Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1 11/10/16 13:22
11/08/16.
Iron, Total
200.7
0.10 U
mg/L
0.10 1 11/10/16 13:22
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1 11/10/16 13:22
11/08/16
Printed 11/21/2016 9:19:38 AM Superset Reference: 16-0000400230 rev 00
34 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-DO2-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -10 (CPW-IOD)
Lab Code: R1611784-016
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/02/16 12:45
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:38 AM Superset Reference: 16-0000400230 rev 00
35 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil. Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1 11/10/16 13:28
11/08/16
Iron, Total
200.7
0.10 U
mg/L
0.10 1 11/10/16 13:28
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1 11/10/16 13:28
11/08/16
Printed 11/21/2016 9:19:38 AM Superset Reference: 16-0000400230 rev 00
35 of 102

dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -20 (CPW-10S)
Lab Code: R1611784-017
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/02/16 11:20
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:38 AM Superset Reference: rev 00
36 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 13:34
11/08/16
Iron, Total
200.7
0.10 U
mg/L
0.10 1
11/10/16 13:34
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 13:34
11/08/16
Printed 11/21/2016 9:19:38 AM Superset Reference: rev 00
36 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-1302-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -12 (CPW-12D)
Lab Code: R1611784-018
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/01/1609:30
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/20169:19:38 AM Superset Reference: 16-0000400230 rev 00
37 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 13:40
11/08/16
Iron, Total
200.7
12.3
mg/L
0.10 1
11/10/16 13:40
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 13:40
11/08/16
Printed 11/21/20169:19:38 AM Superset Reference: 16-0000400230 rev 00
37 of 102

dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -28 (CPW-12S)
Lab Code: R1611784-019
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/01/16 11:00
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
38 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 13:46
11/08/16
Iron, Total
200.7
29.2
mg/L
0.10 1
11/10/16 13:46
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 13:46
11/08/16
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
38 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -16 (CPW-6S)
Lab Code: R1611784-020
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/03/16 13:25
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
39 of 102
Analysis
Analyte Name
Method
Result
Units
MRL
Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7.
0.010 U
mg/L
0.010
1
11/10/16 13:52
11/08/16
Iron, Total
200.7
6.04
mg/L
0.10
1
11/10/16 13:52
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040
1
11/10/16 13:52
11/08/16
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
39 of 102

dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -26 (CPW-6D)
Lab Code: R1611784-021
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/03/16 12:15
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/20169:19:39 AM Superset Reference: 16-0000400230 rev 00
40 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 13:58
11/08/16
Iron, Total
200.7
0.10 U
mg/L
0.10 1
11/10/16 13:58
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 13:58
11/08/16
Printed 11/21/20169:19:39 AM Superset Reference: 16-0000400230 rev 00
40 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -17 (CPW-7S)
Lab Code: R1611784-022
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/01/16 14:20
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/20169:19:39 AM Superset Reference: 16-0000400230 rev 00
41 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 14:04
11/08/16
Iron, Total
200.7
6.87
mg/L
0.10 1
11/10/16 14:04
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 14:04
11/08/16
Printed 11/21/20169:19:39 AM Superset Reference: 16-0000400230 rev 00
41 of 102

dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -27 (CPW-7D)
Lab Code: R1611784-023
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/01/16 13:00
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
42 of 102
Analysis
Analyte Name
Method
Result
Units
MRL
Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010
1
11/10/16 14:22
11/08/16
Iron, Total
200.7
3.19
mg/L
0.10
1
11/10/16 14:22
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040
1
11/10/16 14:22
11/08/16
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
42 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -21 (CPW-5S)
Lab Code: R1611784-024
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/03/16 15:45
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
43 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 14:28
11/08/16
Iron, Total
200.7
4.82
mg/L
0.10 1
11/10/16 14:28
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 14:28
11/08/16
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
43 of 102

dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -25 (CPW-5D)
Lab Code: R1611784-025
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/03/16 14:25
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
44 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/10/16 14:34
11/08/16
Iron, Total
200.7
0.10 U
mg/L
0.10 1
11/10/16 14:34
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/10/16 14:34
11/08/16
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
44 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -11 (CPW-1S)
Lab Code: R1611784-026
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/03/16 10:40
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
45 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/09/16 16:51
11/08/16
Iron, Total
200.7
7.86
mg/L
0.10 1
11/09/16 16:51
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/09/16 16:51
11/08/16
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
45 of 102

dba ALS Environmental
Analytical Report
Client: GILD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -22 (CPW-2D)
Lab Code: R1611784-027
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/02/16 16:40
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
46 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1
11/09/16 17:00
11/08/16
Iron, Total
200.7
5.16
mg/L
0.10 1
11/09/16 17:00
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/09/16 17:00
11/08/16
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
46 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -23 (CPW-3D)
Lab Code: R1611784-028
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/02/16 15:25
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:40 AM Superset Reference: 16-0000400230 rev 00
47 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil. Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010 1 11/09/16 17:16
11/08/16
Iron, Total
200.7
3.82
mg/L
0.10 1 11/09/16 17:16
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1 11/09/16 17:16
11/08/16
Printed 11/21/2016 9:19:40 AM Superset Reference: 16-0000400230 rev 00
47 of 102

� V' V uF V , l uz F'
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -24 (CPW-4D)
Lab Code: R1611784-029
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/04/16 15:25
Date Received: 11/07/16 08:50
Basis: NA
Printed 11/21/2016 9:19:40 AM Superset Reference: 16-0000400230 rev 00
48 of 102
Analysis
Analyte Name
Method
Result
Units
MRL Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
5.26
mg/L
0.010 1
11/09/16 17:19
11/08/16
Iron, Total
200.7
0.10 U
mg/L
0.10 1
11/09/16 17:19
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040 1
11/09/16 17:19
11/08/16
Printed 11/21/2016 9:19:40 AM Superset Reference: 16-0000400230 rev 00
48 of 102

ALS Environmental—Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsglobal.com
RIGHT SOLUTIONS RIGHT PARTNER
49 of 102

�vA Vup vU�, � UxF.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -1 (CPW-13S)
Lab Code: R1611784-006
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/03/16 09:25
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 8.4 mg/L 2.0 10 11/12/16 01:42
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 940 mg/L 20 1 11/08/16 12:00
Printed 11/21/2016 9:19:41 AM Superset Reference: 16-0000400230 rev 00
50 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project:. Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -13 (CPW-13D)
Lab Code: R1611784-007
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/03/16 08:35
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 166 mg/L 8.0 40 11/12/16 01:55
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 1060 mg/L 20 1 11/08/16 12:00
Printed 11/21/2016 9:19:42 AM Superset Reference: 16-0000400230 rev 00
51 of 102

ALV V. V.v -U. P.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -2 (CPW-14S)
Lab Code: R1611784-008
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/01/16 17:00
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 147 mg/L 8.0 40 11/12/16 02:09
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 700 mg/L 20 1 11/08/16 12:00
Printed 11/21/2016 9:19:42 AM Superset Reference: 16-0000400230 rev 00
52 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -14 (CPW-14D)
Lab Code: R1611784-009
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/01/16 15:40
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 160 mg/L 8.0 40 11/12/16 02:22
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 888 mg/L 20 1 11/08/16 12:00
Printed 11/21/2016 9:19:42 AM Superset Reference: 16-0000400230 rev 00
53 of 102

--- < . V.F V IJ ' l V. F.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -3 (CPW-15S)
Lab Code: R1611784-010
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/02/16 10:00
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 194 mg/L 8.0 40 11/11/16 02:29
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 546 mg/L 11 1 11/08/16 12:00
Printed 11/21/2016 9:19:42 AM Superset Reference: 16-0000400230 rev 00
54 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -15 (CPW-15D)
Lab Code: R1611784-011
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/02/16 08:35
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 146 mg/L 8.0 40 11/11/16 21:15
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 604 mg/L 20 1 11/08/16 12:00
Printed 11/21/2016 9:19:42 AM Superset Reference: 16-0000400230 rev 00
55 of 102

ai,3 "ruup U311, wrp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -8 (CPW-8DR)
Lab Code: R1611784-012
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/04/1609:10
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 257 mg/L 8.0 40 11/12/16 01:20
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 688 mg/L 20 1 11/08/16 12:00
Printed 11/21/2016 9:19:42 AM Superset Reference: 16-0000400230 rev 00
56 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -18 (CPW-8S)
Lab Code: R1611784-013
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/04/16 10:20
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 109 mg/L 4.0 20 11/12/16 01:34
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 407 mg/L 10 1 11/09/16 13:00
Printed 11/21/2016 9:19:42 AM Superset Reference: 16-0000400230 rev 00
57 of 102

ALA] V ■ -F V __' - F.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -9 (CPW-9D)
Lab Code: R1611784-014
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/04/16 11:45
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 200 mg/L 8.0 40 11/12/16 03:38
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 1810 mg/L 30 1 11/09/16 13:00
Printed 11/21/2016 9:19:42 AM Superset Reference: 16-0000400230 rev 00
58 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -19 (CPW-9S)
Lab Code: R1611784-015
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/04/16 12:40
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed
Chloride 300.0 99.5 mg/L 2.0 10 11/11/16 03:31
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 463 mg/L 10 1 11/09/16 13:00
Printed 11/21/2016 9:19:42 AM Superset Reference: 16-0000400230 rev 00
59 of 102

moi.., v..,..t, ......��� ..,.,,t..
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -10 (CPW-10D)
Lab Code: R1611784-016
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/02/16 12:45
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 120 mg/L 8.0 40 11/12/16 03:52
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 1230 mg/L 20 1 11/09/16 13:00
Printed 11/21/2016 9:19:42 AM Superset Reference: 16-0000400230 rev 00
60 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -20 (CPW-10S)
Lab Code: R1611784-017
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/02/16 11:20
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 92.8 mg/L 2.0 10 11/11/16 03:56
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 498 mg/L 10 1 11/09/16 13:00
Printed 11/21/2016 9:19:42 AM Superset Reference: 16-0000400230 rev 00
61 of 102

ALa uruup Dari, wrp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -12 (CPW-12D)
Lab Code: R1611784-018
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/01/1609:30
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 6.2 mg/L 2.0 10 11/12/16 04:03
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 1000 mg/L 20 1 11/08/16 12:00
Printed 11/21/2016 9:19:43 AM Superset Reference: 16-0000400230 rev 00
62 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -28 (CPW-12S)
Lab Code: R1611784-019
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/01/16 11:00
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 7.1 mg/L 2.0 10 11/12/16 04:16
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 1690 mg/L 20 1 11/08/16 12:00
Printed 11/21/2016 9:19:43 AM Superset Reference: 16-0000400230 rev 00
63 of 102

L'1LU \71 V UV VILA' l UA F.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -16 (CPW-6S)
Lab Code: R1611784-020
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/03/16 13:25
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result _ Units MRL Dil. Date Analyzed Q
Chloride 300.0 107 mg/L 4.0 20 11/15/16 03:39
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 2000 mg/L 40 1 11/09/16 13:00
Printed 11/21/2016 9:19:43 AM Superset Reference: 16-0000400230 rev 00
64 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -26 (CPW-6D)
Lab Code: R1611784-021
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/03/16 12:15
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 233 mg/L 8.0 40 11/15/16 03:53
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 942 mg/L 20 1 .11/09/16 13:00
Printed 11/21/2016 9:19:43 AM Superset Reference: 16-0000400230 rev 00
65 of 102

tiva uruup uari9 %_U1 P.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -17 (CPW-7S)
Lab Code: R1611784-022
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/01/16 14:20
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 4.6 mg/L 2.0 10 11/14/1613:50
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 1620 mg/L 30 1 11/08/16 12:00
Printed 11/21/2016 9:19:43 AM Superset Reference: 16-0000400230 rev 00
66 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -27 (CPW-7D)
Lab Code: R1611784-023
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/01/16 13:00
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 33.7 mg/L 2.0 10 11/14/1613:22
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 704 mg/L 10 1 11/08/16 12:00
Printed 11/21/2016 9:19:43 AM Superset Reference: 16-0000400230 rev 00
67 of 102

Ai.a croup UOA, %.orp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -21 (CPW-5S)
Lab Code: R1611784-024
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/03/16 15:45
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 286 mg/L 20 100 11/14/1613:36
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 1400 mg/L 20 1 11/09/16 13:00
Printed 11/21/2016 9:19:43 AM Superset Reference: 16-0000400230 rev 00
68 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -25 (CPW-5D)
Lab Code: R1611784-025
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/03/16 14:25
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 1010 mg/L 40 200 11/17/16 00:23
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 2230 mg/L 50 1 11/09/16 13:00
Printed 11/21/2016 9:19:43 AM Superset Reference: 16-0000400230 rev 00
69 of 102

A til V.F VII_, t.Vl F.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -11 (CPW-1S)
Lab Code: R1611784-026
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/03/16 10:40
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 5.0 mg/L 2.0 10 11/11/16 06:28
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 327 mg/L 10 1 11/09/16 13:00
Printed 11/21/2016 9:19:43 AM Superset Reference: 16-0000400230 rev 00
70 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -22 (CPW-2D)
Lab Code: R1611784-027
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/02/16 16:40
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 10.4 mg/L 2.0 10 11/11/16 06:43
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 387 mg/L 10 1 11/09/16 13:00
Printed 11/21/2016 9:19:43 AM Superset Reference: 16-0000400230 rev 00
71 of 102

I&Jua 111 UUP V OtI, \..Ul P.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -23 (CPW-3D)
Lab Code: R1611784-028
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/02/16 15:25
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 41.0 mg/L 2.0 10 11/14/1613:09
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 572 mg/L 10 1 11/09/16 13:00
Printed 11/21/2016 9:19:43 AM Superset Reference: 16-0000400230 rev 00
72 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: MW -24 (CPW-4D)
Lab Code: R1611784-029
Inorganic Parameters
Service Request: R1611784
Date Collected: 11/04/16 15:25
Date Received: 11/07/16 08:50
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed
Chloride 300.0 11.7 mg/L 2.0 10 11/11/16 09:29
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 402 mg/L 10 1 11/09/16 13:00
Printed 11/21/2016 9:19:43 AM Superset Reference: 16-0000400230 rev 00
73 of 102

AALS Eroulircromeentad
ALS Environmental—Rochester Laboratory
1 565 Jefferson Road, Building 300, Suite 360, Rochester, NY 14623
Phone [phone] Fax [phone]
www.alsgiobal.com
RIGH i Ili €..U.7...14.1NS i" IGH 9 P/"iR~$ NER
74 of 102

ALS Envimmnmmental--Rochester Laboratory
1565 Jefferson Road. Building 300. Suite ]GO. Rochester. NY 14623
Phone (S8S)2Q0'538OFax (S8S)280'0475
xmwm/.a|sg|obaicorn
R|CHTSOLUTIONS | RIGHT PARTNER
7aof102

HLJ hl -UUP lJat%l %-Ul-Y.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: Method Blank
Lab Code: R1611784 -MBI
Inorganic Parameters
Service Request: R1611784
Date Collected: NA
Date Received: NA
Basis: NA
Printed 11/21/2016 9:19:40 AM Superset Reference: 16-0000400230 rev 00
76 of 102
Analysis
Analyte Name
Method
Result
Units
MRL
Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010
1
11/09/16 16:22
11/08/16
Iron, Total
200.7
0.10 U
mg/L
0.10'
1
11/09/16 16:22
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040
1
11/09/16 16:22
11/08/16
Printed 11/21/2016 9:19:40 AM Superset Reference: 16-0000400230 rev 00
76 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: Method Blank
Lab Code: R1611784-MB2
Inorganic Parameters
Service Request: R1611784
Date Collected: NA
Date Received: NA
Basis: NA
Printed 11/21/2016 9:19:40 AM Superset Reference: 16-0000400230 rev 00
77 of 102
Analysis
Analyte Name
Method
Result
Units
MRL
Dil.
Date Analyzed
Date Extracted Q
Chromium, Total
200.7
0.010 U
mg/L
0.010
1
11/10/16 11:03
11/08/16
Iron, Total
200.7
0.10 U
mg/L
0.10
1
11/10/16 11:03
11/08/16
Nickel, Total
200.7
0.040 U
mg/L
0.040
1
11/10/16 11:03
11/08/16
Printed 11/21/2016 9:19:40 AM Superset Reference: 16-0000400230 rev 00
77 of 102

ALS kiroup USA, Uorp.
dba ALS Environmental
QA/QC Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Matrix Spike Summary
Inorganic Parameters
Sample Name: MW -1 (CPW-13S)
Lab Code: R1611784-006
Matrix Spike
R1611784-006MS
Service Request:R1611784
Date Collected: 1 1/03/16
Date Received: 11/07/16
Date Analyzed: 11/10/16
Units:mg/L
Basis:NA
Analyte Name
Method
Sample Result
Result
Spike Amount
% Rec
% Rec Limits
Chromium, Total
200.7
0.010 U
0.192
0.200
96
70-130
Iron, Total
200.7
19.3
20.3
1.00
105 #
70-130
Nickel, Total
200.7
0.040 U
0.497
0.500
99
70-130
Results flagged with an asterisk (°) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 11/21/2016 9:19:37 AM Superset Reference: 16-0000400230 rev 00
78 of 102

Matrix Spike
R1611784-007MS
Service Request:R1611784
Date Collected: 11/03/16
Date Received: 1 1/07/16
Date Analyzed: 1 l/ 10/16
Units:mg/L
Basis:NA
Analyte Name
ALS Group USA, Corp.
Sample Result
dba ALS Environmental
Spike Amount
QA/QC Report
Client:
GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Project:
Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix:
Water
97
Matrix Spike Summary
Iron, Total
Inorganic Parameters
Sample Name:
MW -13 (CPW-13D)
Lab Code:
R1611784-007
Matrix Spike
R1611784-007MS
Service Request:R1611784
Date Collected: 11/03/16
Date Received: 1 1/07/16
Date Analyzed: 1 l/ 10/16
Units:mg/L
Basis:NA
Analyte Name
Method
Sample Result
Result
Spike Amount
% Ree
% Rec Limits
Chromium, Total
200.7
0.010 U
0.194
0.200
97
70-130
Iron, Total
200.7
1.54
2.48
1.00
94
70-130
Nickel, Total
200.7
0.040 U
0.490
0.500
98
70-130
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 11/21/2016 9:19:37 AM Superset Reference: 16-0000400230 rev 00
79 of 102

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Matrix Spike Summary
Inorganic Parameters
Sample Name: MW -22 (CPW-2D)
Lab Code: R1611784-027
Matrix Spike
R1611784-027MS
Service Request:R1611784
Date Collected: 1 1/02/16
Date Received: 1 1/07/16
Date Analyzed: 1 1/9/16
Units:mg/L
Basis:NA
Analyte Name
Method
Sample Result
Result
Spike Amount
% Ree
% Rec Limits
Chromium, Total
200.7
0.010 U
0.193
0.200
96
70-130
Iron, Total
200.7
5.16
5.92
1.00
75 #
70-130
Nickel, Total
200.7
0.040 U
0.480
0.500
96
70-130
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 11/21/2016 9:19:39 AM Superset Reference: 16-0000400230 rev 00
80 of 102

Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 11/21/2016 9:19:37 AM 81 of 102 Superset Reference: 16-0000400230 rev 00
ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client:
GHD Services Inc. (Formerly
Conestoga -Rovers & Associates, Inc.)
Service Request: R1611784
Project
Castle Hayne 258-402-D02-3100/6448 - L -Cap
Date Collected: 11/03/16
Sample Matrix:
Water
Date Received: 11/07/16
Date Analyzed: 11/10/16
Replicate Sample Summary
Inorganic Parameters
Sample Name:
MW -1 (CPW-13S)
Units: mg/L
Lab Code:
R1611784-006
Basis: NA
Duplicate Sample
R1611784 -
Analysis
Sample 006DUP
Analyte Name
Method
MRL Result Result
Average RPD RPD Limit
Chromium, Total
200.7
0.010 0.010 U 0.010 U
NC NC 20
Iron, Total
200.7
0.10 19.3 19.1
19.2 <1 20
Nickel, Total
200.7
0.040 0.040 U 0.040 U
NC NC 20
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 11/21/2016 9:19:37 AM 81 of 102 Superset Reference: 16-0000400230 rev 00

Results flagged with an asterisk (") indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 11/21/2016 9:19:37 AM 82 of 102 Superset Reference: 16-0000400230 rev 00
ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client:
GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Service Request: R1611784
Project
Castle Hayne 258-402-1302-3100/6448 - L -Cap
Date Collected: 11/03/16
Sample Matrix:
Water
Date Received: 11/07/16
Date Analyzed: 11/10/16
Replicate Sample Summary
Inorganic Parameters
Sample Name:
MW -13 (CPW-13D)
Units: mg/L
Lab Code:
R1611784-007
Basis: NA
Duplicate Sample
R1611784 -
Analysis
Sample 007DUP
Analyte Name
Method
MRL Result Result
Average RPD RPD Limit
Chromium, Total
200.7
0.010 0.010 U 0.010 U
NC NC 20
Iron, Total
200.7
0.10 1.54 1.55
1.54 <1 20
Nickel, Total
200.7
0.040 0.040 U 0.040 U
NC NC 20
Results flagged with an asterisk (") indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 11/21/2016 9:19:37 AM 82 of 102 Superset Reference: 16-0000400230 rev 00

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Project Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Replicate Sample Summary
Inorganic Parameters
Sample Name: MW -22 (CPW-2D)
Lab Code: R1611784-027
Service Request:
R1611784
Date Collected:
11/02/16
Date Received:
11/07/16
Date Analyzed:
11/09/16
Units: mg/L
Basis: NA
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 11/21/2016 9:19:39 AM 83 of 102 Superset Reference: 16-0000400230 rev 00
Duplicate Sample
R1611784 -
Analysis
Sample
027DUP
Analyte Name
Method
MRL
Result
Result
Average
RPD
RPD Limit
Chromium, Total
200.7
0.010
0.010 U
0.010 U
NC
NC
20
Iron, Total
200.7
0.10
5.16
5.35
5.26
4
20
Nickel, Total
200.7
0.040
0.040 U
0.040 U
NC
NC
20
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 11/21/2016 9:19:39 AM 83 of 102 Superset Reference: 16-0000400230 rev 00

ALS l roup IDSA, Uorp.
dba ALS Environmental
QA/QC Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.) Service Request: R1611784
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap Date Analyzed: 11/09/16
Sample Matrix: Water
Lab Control Sample Summary
Inorganic Parameters
Units:mg/L
Basis:NA
Lab Control Sample
R1611784-LCS1
Analyte Name
Analytical Method
Result
Spike Amount
% Ree
% Rec Limits
Chromium, Total
200.7
0.193
0.200
97
85-115
Iron, Total
200.7
0.957
1.00
96
85-115
Nickel, Total
200.7
0.499
0.500
100
85-115
Printed 11/21/2016 9:19:40 AM
84 of 102
Superset Reference: 16-0000400230 rev 00

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Lab Control Sample Summary
Inorganic Parameters
Lab Control Sample
R1611784-LCS2
Service Request: R1611784
Date Analyzed: 11/10/16
Units:mg/L
Basis:NA
Analyte Name
Analytical Method
Result
Spike Amount
% Ree
% Ree Limits
Chromium, Total
200.7
0.205
0.200
102
85-115
Iron, Total
200.7
0.99
1.00
99
85-115
Nickel, Total
200.7
0.527
0.500
105
85-115
Printed 11/21/2016 9:19:40 AM
85 of 102
Superset Reference: 16-0000400230 rev 00

ALS Env! nmnmmenta]--Roch ester Laboratory
1565 Jefferson Road. Building ]OD. Suite 360. Rochester' NY 14623
Phone (SQS)200'S38UFax (585)280'047S
RIGHT SOLUTON5! RIGHT PARTNER
86 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: Method Blank
Lab Code: R1611784 -MBI
Inorganic Parameters
Service Request: R1611784
Date Collected: NA
Date Received: NA
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 0.20 U mg/L 0.20 1 11/10/16 23:41
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 10 U mg/L 10 1 11/08/16 12:00
Printed 11/21/2016 9:19:44 AM Superset Reference: 16-0000400230 rev 00
87 of 102

tiL'3 111 UUP VOt%, \_Vl P.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: Method Blank
Lab Code: R1611784-MB2
Inorganic Parameters
Service Request: R1611784
Date Collected: NA
Date Received: NA
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 0.20 U mg/L 0.20 1 11/11/16 04:47
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 10 U mg/L 10 1 11/08/16 12:00
Printed 11/21/2016 9:19:44 AM Superset Reference: 16-0000400230 rev 00
88 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: Method Blank
Lab Code: R1611784-MB3
Inorganic Parameters
Service Request: R1611784
Date Collected: NA
Date Received: NA
Basis: NA
Analyte Name Analysis Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 0.20 U mg/L 0.20 1 11/11/16 16:28
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 10 U mg/L 10 1 11/09/16 13:00
Printed 11/21/2016 9:19:44 AM Superset Reference: 16-0000400230 rev 00
89 of 102

t&JUO vivuP %JOZX, %,V■Y.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: Method Blank
Lab Code: R1611784-MB4
Inorganic Parameters
Service Request: R1611784
Date Collected: NA
Date Received: NA
Basis: NA
Analysis
Analyte Name Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 0.20 U mg/L 0.20 1 11/12/16 00:14
Printed 11/21/2016 9:19:44 AM Superset Reference: 16-0000400230 rev 00
90 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: Method Blank
Lab Code: R1611784-MB5
Inorganic Parameters
Service Request: R1611784
Date Collected: NA
Date Received: NA
Basis: NA
Analysis
Analyte Name Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 0.20 U mg/L 0.20 1 11/14/16 09:03
Printed 11/21/2016 9:19:44 AM Superset Reference: 16-0000400230 rev 00
91 of 102

ALU VX VV I V--, VI F.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: Method Blank
Lab Code: R1611784-MB6
Inorganic Parameters
Service Request: R1611784
Date Collected: NA
Date Received: NA
Basis: NA
Analysis
Analyte Name Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 0.20 U mg/L 0.20 1 11/14/16 22:07
Printed 11/21/2016 9:19:44 AM Superset Reference: 16-0000400230 rev 00
92 of 102

ALS Group USA, Corp.
dba ALS Environmental
Analytical Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates,
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Sample Name: Method Blank
Lab Code: R1611784-MB7
Inorganic Parameters
Service Request: R1611784
Date Collected: NA
Date Received: NA
Basis: NA
Analysis
Analyte Name Method Result Units MRL Dil. Date Analyzed Q
Chloride 300.0 0.20 U mg/L 0.20 1 11/16/16 22:15
Printed 11/21/2016 9:19:44 AM Superset Reference: 16-0000400230 rev 00
93 of 102

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Project Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Replicate Sample Summary
General Chemistry Parameters
Sample Name: MW -8 (CPW-8DR)
Lab Code: R1611784-012
Service Request:
R1611784
Date Collected:
11/04/16
Date Received:
11/07/16
Date Analyzed:
11/08/16
Units: mg/L
Basis: NA
Duplicate
Sample
R1611784 -
Sample 012DUP
Analyte Name Analysis Method MRL Result Result Average RPD RPD Limit
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 20 688 692 690 <1 10
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 11/21/2016 9:19:45 AM 94 of 102 Superset Reference: 16-0000400230 rev 00

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Project Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Replicate Sample Summary
General Chemistry Parameters
Sample Name: MW -26 (CPW-6D)
Lab Code: R1611784-021
Service Request:
R1611784
Date Collected:
11/03/16
Date Received:
11/07/16
Date Analyzed:
11/09/16
Units: mg/L
Basis: NA
Duplicate
Sample
R1611784 -
Sample 021DUP
Analyte Name Analysis Method MRL Result Result Average RPD RPD Limit
Solids, Total Dissolved (TDS) SM 2540 C-1997(2011) 20 942 946 944 <1 10
Results flagged with an asterisk (*) indicate values outside control criteria.
Results flagged with a pound (#) indicate the control criteria is not applicable.
Percent recoveries and relative percent differences (RPD) are determined by the software using values in the calculation which have not been rounded.
Printed 11/21/20169:19:45 AM 95 of 102 Superset Reference: 16-0000400230 rev 00

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Lab Control Sample Summary
General Chemistry Parameters
Lab Control Sample
R1611784-LCS1
Service Request: R1611784
Date Analyzed: 11/08/16 - 11/10/16
Units:mg/L
Basis:NA
Analyte Name
Analytical Method
Result
Spike Amount
% Ree
% Rec Limits
Chloride
300.0
1.95
2.00
98
90-110
Solids, Total Dissolved (TDS)
SM 2540 C-1997(2011)
904
914
99
90-110
Printed 11/21/2016 9:19:43 AM
96 of 102
Superset Reference: 16-0000400230 rev 00

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Lab Control Sample Summary
General Chemistry Parameters
Lab Control Sample
R1611784-LCS2
Service Request: R1611784
Date Analyzed: 11/08/16 - 11/11/16
Units:mg/L
Basis:NA
Analyte Name
Analytical Method
Result
Spike Amount
% Rec
% Rec Limits
Chloride
300.0
1.98
2.00
99
90-110
Solids, Total Dissolved (TDS)
SM 2540 C-1997(2011)
882
914
97
90-110
Printed 11/21/2016 9:19:44 AM
97 of 102
Superset Reference: 16-0000400230 rev 00

ALS Group USA, Uorp.
dba ALS Environmental
QA/QC Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Lab Control Sample Summary
General Chemistry Parameters
Lab Control Sample
R1611784-LCS3
Service Request: R1611784
Date Analyzed: 11/09/16 - 11/11/16
Units:mg/L
Basis:NA
Analyte Name
Analytical Method
Result
Spike Amount
% Ree
% Rec Limits
Chloride
300.0
2.03
2.00
101
90-110
Solids, Total Dissolved (TDS)
SM 2540 C-1997(2011)
876
914
96
90-110
Printed 11/21/2016 9:19:44 AM
98 of 102
Superset Reference: 16-0000400230 rev 00

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Lab Control Sample Summary
General Chemistry Parameters
Lab Control Sample
R1611784-LCS4
Service Request: R1611784
Date Analyzed: 11/12/16
Units:mg/L
Basis:NA
Analyte Name Analytical Method Result Spike Amount % Rec % Rec Limits
Chloride 300.0 2.04 2.00 102 90-110
Printed 11/21/2016 9:19:44 AM
99 of 102
Superset Reference: 16-0000400230 rev 00

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Lab Control Sample Summary
General Chemistry Parameters
Lab Control Sample
R1611784-LCS5
Service Request: R1611784
Date Analyzed: 11/14/16
Units:mg/L
Basis:NA
Analyte Name Analytical Method Result Spike Amount % Ree % Rec Limits
Chloride 300.0 2.05 2.00 103 90-110
Printed 11/21/2016 9:19:44 AM
100 of 102
Superset Reference: 16-0000400230 rev 00

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Lab Control Sample Summary
General Chemistry Parameters
Lab Control Sample
R1611784-LCS6
Service Request: R1611784
Date Analyzed: 11/14/16
Units:mg/L
Basis:NA
Analyte Name Analytical Method Result Spike Amount % Rec % Rec Limits
Chloride 300.0 2.00 2.00 100 90-110
Printed 11/21/2016 9:19:44 AM
101 of 102
Superset Reference: 16-0000400230 rev 00

ALS Group USA, Corp.
dba ALS Environmental
QA/QC Report
Client: GHD Services Inc. (Formerly Conestoga -Rovers & Associates, Inc.)
Project: Castle Hayne 258-402-D02-3100/6448 - L -Cap
Sample Matrix: Water
Lab Control Sample Summary
General Chemistry Parameters
Lab Control Sample
R1611784-LCS7
Service Request: R1611784
Date Analyzed: 11/16/16
Units:mg/L
Basis:NA
Analyte Name Analytical Method Result Spike Amount % Rec % Rec Limits
Chloride 300.0 1.99 2.00 100 90-110
Printed 11/21/2016 9:19:44 AM
102 of 102
Superset Reference: 16-0000400230 rev 00