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WQ0019907_Monitoring - 11-2016_20161228 (2)
GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Facility Name: Holly Ridge WVVTP and Surface Irrigation Facility Permit Name (if different): Onslow water and Sewer Authority Facility Address: 220 Dolph Everett Rd NC 28445 SUBMIT FORM ON YELLOW PAPER ONLY County Onslow act Person: Mark C. Young Telephone#: 910-937-7570 Location/Site Name: Northside Field 1-A No. of wells to be sampled: 4 L ID NUMBER (from Permit): MW -1 Date sample collected: 2 Nov 16 Depth: 23 ft. Well Diameter: 2 in. 1 to Water Level 82646:6' 3" ft. below measuring point Screened Interval: 13 ft. to 23 ft. luring Point is 2.3 ft. above land surface Relative M.P. Elevation: ft. the of water pumped/bailed before sampling; 5 gallons Ass for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO Date sample analyzed: 2.7 Nov 16 PARAMETERS NOTE: Values should reflect dissolve COD 00335 mg/L Coliform: MF Fecal 31616 /100mL Coliform: MF Total 31504 <t /100mL (Note: Use MPN method for highly tumld samples) )issolved Solids:Total 70300 74 mg/L pH (Lab) 00403 4.66 units TOC oosso mg/L Chloride 00940 14 mg/L Arsenic 01002 ug/L Grease and Oils 00552 mg/L Phenol 3273o ug/L Sulfate 00945 mg/L Specific Conductance 0oogs pMhos Total Ammonia oo610 0.45 mg/L (Ammonia Nitrogen; NH364 N; Ammonla Nitrogen, Total) TKN as N 00625 mg/L For Remediation Systems Only (Attach Lab Reports): PARTNENT OF ENVIRONMENT b NATURAL RESOURCES 'ISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 17 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: (919)733-3221 :RMIT Number: Expiration Date: 30 Apr 16 In -Discharge W00019907 UIC )DES Other 'PE OF PERMITTED OPERATION BEING MONITORED M Lagoon ❑ Remediation: Infiltration Gallery I7 Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: WAS pH 00400: 4.68 units Temp. 000lo: 18.8 °C DRY at Spec. Cond. 00094: µMhos time of sampling, Odor 0o065: check Appearance Clear here: 11 Laboratory Name: ONWASA Laboratory / Envirochem Certification No. 539 / 94 and colloidal concentrations. Nitrite (NO,) as N 00615 mg/L Pb - Lead olos1 ug/L Nitrate (NO,) as N 00620 <0.25 - mg/L Zn - Zinc 01092 mg/L Phosphorus: Total as P 00665 <0.05 mg/L Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): AI- Aluminum otto5 mg/L Be - Barium 01007 ug/L Ca - Calcium 00916 mg/L Cd - Cadmium 01027 ug/L C Chromium: Total oto34t ug/L Cu - Copper 01042 �,o , , 'rmg/L ORGANICS: (by GC, GC/MS, HPLC) Fe - Iron 01045 Hg - Mercury 71900 K - Potassium 00937 Mg - Magnesium 00927 Mn - Manganese 01055 Ni - Nickel 01067 Influent Total ug/L (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ME Yes (1) ❑ No (0) VOC 78732: method # SM 62008 method # method # method # mg/L Effluent Total VOCs: mg/L VOC Removal% Eddie Caron, Utility and Planning Superintendent Permittee (or Authorized Agent) Name and Title- Please print or type Signature of Pennines (or Au Dale) GW -59 Rev. 2/2010 SUBMIT FORM ON YELLOW PAPER ONLY QUALITY MONITORING: rr DEPARTMENT OF ENVIRONMENT b NATURAL RESOURCES DIVISIONGROUNDWATER DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM ,, r 1617 MAIL SERVICE CENTER, RALEIGH, NC 27690.1617 Phone: 1919) 733-3221 FACILITY INFORMATION Please Print clearly or Type PERMIT Number: Expiration Date: 30Apr 16 Facility Name: Holly Ridge WVVTP and Surface Irrigation Facility Non -Discharge WQ0019907 UIC NPDES Other Permit Name (if different): Onslow water and Sewer Authority Facility Address: 220 Dolph Everett Rd TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon ❑ Remediation: Infiltration Gallery Holy Ridge """" NC 28445 County Onslow fG,tN ISmml I�pl � Spray Field ❑Remediation: Contact Person: Mark C. Young Telephone#: 910-937-7570 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Northside Field 1-A No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: hum Perm SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW -2 Date sample collected: 2 Nov 16 FIELD ANALYSES: WAS Well Depth: 23 ft. Well Diameter: 2 in. pH 00400: 4.66 units Temp. 000to: 19.4 oC DRY at Depth to Water Level x2546: 5' 1" ft. below measuring point Screened Interval: 13 ft. to 23 fL Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 2.0 ft. above land surface Relative M.P. Elevation: ft. Odor 000es: check Volume of water pumped/bailed before sampling: 5 gallons Appearance Clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 2 - 7 Nov 16 Laboratory Name: ONWASA Laboratory l Envirachem Certification No. 539194 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 0os15 mg/L Pb - Lead oio51 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 <0.25 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 <1 /100mL Phosphorus: Total as P oo665 <0.05 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 703ao 74 mg/L At - Aluminum o11o5 mg/L pH (Lab) 0o4o3 4.66 units Be - Barium 01007 ug/L _ yip TOC oosso mg/L Ca -Calcium 00916 mg/L Chloride 00940 45.5 mg/L Cd - Cadmium oio27 ug/L Arsenic o1om ug/L Chromium: Total 91934 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method M ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 719oo ug/L Lab Report Attached? N Yes (1) ❑ No (0) Specific Conductance 000es µMhos K - Potassium 00937 mg/L VOC 78732: , method # SM 62008 Total Ammonia ooslo .47 mg/L Mg - Magnesium 00927 mg/L , method # (Ammonia Nitrogen: N%as N: Ammonia Nlirogern Total) Mn - Manganese oloss ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Eddie Caron, Utility and Planning Superintendent Permittee (or Authorized Agent) Name and Title- Please pnnt or type GW -59 Rev. 2/2010 SUBMIT FORM ON YELLOW PAPER ONLY TER QUALITY MONITORING: E REPORT FORM TY INFORMATION Please Pdnf Clearly or Type Name: Holly Ridge W WiP and Surface Irrigation Facility Name (if different): Onslow water and Sewer Authority Address: 220 Dolph Everett Rd idge '6"°e" NC 28445 County Onslow act Person: Mark C. Young Telephone#: 910-937-7570 Location/Site Name: Northside Field 1-A No. of wells to be sampled: 4 L ID NUMBER (from Permit): MW -3 Date sample collected: 2 Nov 16 Depth: 22 ft. Well Diameter: 2 in. h to Water Level 82546: a. 1'. ft. below measuring point Screened Interval: 12 ft. to 22 ft. luring Point is 3.3 ft. above land surface Relative M.P. Elevation: ft. ne of water pumped/bailed before sampling: 5 gallons oles for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO ISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 7 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: (919) 723.322 !RMIT Number: Expiration Date: 30 Apr 16 n -Discharge W00019907 UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑� Lagoon ❑ Remediation: Infiltration Gallery ❑� Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: pH 00400: 5.28 units Spec. Cond. 00094: Odor 000ss: _ Appearance cloud) Temp. coclo: 19.3 °C DRY at µMhos time of Date sample analyzed: 2.7 Nov 16 Laboratory Name: ONWASA Laboratory / Envirochem Certification No. 539 / 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 mg/L Pb - Lead oias1 uglL Coliform: MF Fecal 31s1s /100mL Nitrate (NOa) as N 00620 <0.25 mg/L Zn -Zinc oto92 mg/L Coliform: MF Total 31504 <1 (Note: Use MPN method for highly turbid as les) /100mL Phosphorus: Total as P ooss5 <0.05 mg/L nip Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 98 mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 5.28 units Be - Barium 01007 ug/L TOC ooeso mg/L Ca - Calcium 00916 mg/L _ Chloride 0094o 27.5 mg/L Cd -Cadmium alo27 ug/L Arsenic 01002 ug/L Chromium: Total 01030 ug/L Grease and Oils 00552 mg/L Cu - Copper o1o42mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron oto45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? X Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: , method # SM 62008 Total Ammonia ooslo <0.2 mg/L Mg - Magnesium 00927 mg/L , method # (Amnnnla Nitrogen; 1,11-13aa N; Ammonia Nitrogen, Total) Mn - Manganese o1o5s ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Eddie Caron, Utility and Planning Superintendent/ z 1G /G Permiftee (or Authorized Agent) Name and Title- Please print or type Signature o Permittee (or genu (Date) GW -59 Rev. 212010 Eddie Caron, Utility and Planning Superintendent/ z 1G /G Permiftee (or Authorized Agent) Name and Title- Please print or type Signature o Permittee (or genu (Date) GW -59 Rev. 212010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: Date sample collected: 2 Nov 16 DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM Depth: 23 ft. 1517 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 1919) 7333221 FACILITY INFORMATION Please Print Clearly or Type DRY at PERMIT Number: Expiration Dale: 30 Apr 16 Facility Name: Holly Ridge WWTP and Surface Irrigation Facility time sampling, Non -Discharge W00019907 UIC Permit Name (if different): Onslow water and Sewer Authority check NPDES Other Facility Address: 220 Dolph Everett Rd here: ❑ TYPE OF PERMITTED OPERATION BEING MONITORED Holly Ridge 's'""' NC 28445 Coun Onslow ty Chromium: Total 01034 ■ Lagoon El Remediation: Infiltration Gallery icen lsl�t') mg/L ❑ Spray Field ❑ Remediation: Contact Person: Mark C. Young Telephone#: 910-937-7570 Phenol 32730 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Northside Field 1-A No. of wells to be sampled: 4 (Specify test and method #. ATTACH LAB REPORT.) ❑ Water Source Heat Pump ❑ Other: L ID NUMBER (from Permit): MW -4 Date sample collected: 2 Nov 16 FIELD ANALYSES: WAS Depth: 23 ft. Well Diameter: 2 in. pH 00400: 5.83 units Temp. 000lo: 20.1 eC DRY at 1 to Water Level 82646: 7'3" ft. below measuring point Screened Interval: 13 ft. to 23 ft. Spec. Cond. 00094: µMhos time sampling, luring Point is 3.0 ft. above land surface Relative M.P. Elevation: ft. Odor 0008s: check ne of water pumped/bailed before sampling: 5 gallons Appearance cloudy here: ❑ .In. fn mn4.I.'u _'M1l t.r4 unaNneud• n Vi n i and finld �nirlifiorl• n VC4 n "n Chromium: Total 01034 ugiL Its sample analyzed: 2- 7 Nov 16 Laboratory Name: ONWASA Laboratory / Envirochem Certification No. 539 / 94 UtAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. ni COD 00335 mg/L Nitrite (NO2) as N oos15 mg/L Pb - Lead olos1 ugiL Coliform: MF Fecal 31616 /100ml- Nitrate (NO3) as N 00620 <0.25 mg/L Zn - Zinc 01092 ni Coliform: MF Total 31504 <1 /100ml- Phosphorus: Total as P owns 0.11 mg/L (Note: Use Mi method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): solved Solids:Total 7030o 47 mg/L Al - Aluminum o11os ni OLE - pH (Lab) 00403 5.83 units Be - Barium 01007 ug/l. 9 2016 TOC ooss0 mg/L Ca - Calcium 00916 mg/L Vft Chloride 0094o 24 mg/L Cd - Cadmium 01027 ugiL Arsenic 01002 ugiL Chromium: Total 01034 ugiL Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ugiL Fe - Iron 01045 ugiL (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? XYes (1) ElNo (0) ecific Conductance 00095 µMhos K - Potassium 9og37 mg/L VOC 78732: , method # SM 62008 Total Ammonia orisio 40.2 ni Mg - Magnesium 66927 mg/L , method # (Ammonls Nitrogen; NHsas N; Ammonle Nitrogen, Tote) Mn - Manganese atoss ug/L , method # TKN as N 00625 mgiL Ni - Nickel atos7 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%, UW -b9 Hev. zizulu GW -59A COMPLIANCE REPORT FORM Permit # woe019907 (Submit one each monitoring period with GW -59 forms.) 1 Enter date monitoring results were due. ( Nov 2016 ► Will this monitoring report (GW -59 and GW -59A) YES NO be submitted after the established due date? X 2 Was any required information missing on the GW -59 report forms? YES NO IF the answer to question 1 or 2 is 'YES' list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YFS NO identification plate, area overgrown, etc.)? Ifthe answer is "Yes", contact the Regional Officefor guidance. X 4 Are any monitored constituents equal to or above the established standards? YES If the answer to question 4 is 'NO', skip to section 8. If the answer to question 41s "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below. 5 For the constituents Identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is NO', skip to section 8. If the answer to question 5 I "YES" list in the space provided below, each well with constituents) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer Is "YES" a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. if the answer Is "NO" monitoring wells may be Improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is 'YES", describe those actions in the space provided below. If the answer to question 7 I "NO" contact the Regional Office within 90 days, an evaluation may required to determine the Tmpact the waste disposal system is having at the review and compliance boundaries surroundlna this facility. Failure to do so may sublect the permittee to a Notice of Violation lines, andlorvenaldes. g The person completing this portion (GW -59A) of the monitoring report should sign below and submit this form with GW -59 forms for required wells to the address provided at the top of the current GW -59 form. I hereby acknowledge that the above information was evalpated and the Information submitted in this report (Compliance Report GW -59A) Is true and comp the best of my knowledge. Eddie Caron z Z� Signature of Permittee (or Authorize ate GW -59A 12/8/2003 ONWASA Laborato 0 N0,",,.'.vVte w,. ,,Av. ,,,.h., sfty A 228 Georgetownry Road Jacksonville, North Carolina 28540 lark CHAIN OF CUSTODY . . . . . . . . . . . ... . ............ ............. . ............. . . . . . . . . . . . 1645007 I P;A P:A p:,c P::B P::B 1 2 M HR Effluent Composite /4La(. 0 'qL? r C WW Page of 2 Phone: (910) 389-8511 0 1 0 COC Number Fax: (910) 455-5607 or/50 G WW Lab Work Order Number 1645007 0 1 D0 0 HRMW1 Z G GW 5 0 1 1 0 1 HRMW2 cl I C- G GW 5 0 1 1 0 1 Rush requests subject to HRMW3 qs— G GW 5 0 1 1 a. additional charge. jq,j -6 HRMW4 n/, Ir G GW 5 0 1 Rush requests Subject to lab 1 1 2 .. .... . . approval. NL standard (days) O 17: Cl EU 0 > 0 h" 0 Expedited JdaVs) as: Co. . . . . . . . . . . . ... . ............ ............. . ............. . . . . . . . . . . . R I P;A P:A p:,c P::B P::B G::A M HR Effluent Composite /4La(. 0 'qL? r C WW 3 2 0 0 1 0 0 HR Effluent Grab or/50 G WW 1 0 0 1 D0 0 HRMW1 Z G GW 5 0 1 1 0 1 HRMW2 cl I C- G GW 5 0 1 1 0 1 :2:: HRMW3 qs— G GW 5 0 1 1 0 1 jq,j -6 HRMW4 n/, Ir G GW 5 0 1 1 0 0 1 1 2 By Receive Temp: 'C PH: Z Intials abix Codes: GW=GWVV%f-JVW Presem. Codes: A=Cool 6 degC - 1:1 HCkA—Cool 6 degC,8,Cbo1 6 degC M204 tZ,(>0.0005% Na2S203 Cont. Codes G,PTFE 40 mL MW VOC,NIM sterile Na2S203,P,P 1 llw,P,P 250 mlP,P 250 mil H2SO4 Permit: WQ0019907 ORC: Mark Young Sample Collection Date: 02 -Nov -16 Facility: Holly Ridge Spray Field BOD 18.5 mg/L 02 -Nov -16 Fecal MPN 7.3 #/100ml 027Nov-16 NH3 * 1.16 'mg/L 03 -Nov -16 NO3. 1.95 mg/L , ' ` 03 -Nov -16', P 2.16 mg/L 04 -Nov -16 TDS 356 mg/L . 07 -Nov -16 TKN 3.47 mg/L 03 -Nov -16 TSS 11.4 mg/L 02-1\16v46 CI- Fecal,MPN NH3 NO3 P TDS CI - Fecal MPN NH3 NO3 P TDS SM 5210 B-2001 Colilert 9223 B-2004 EPA 351.1 Rev 2, 1993 *Qualify: TRCI = 0.14 mg/L sample dechlorinated prior to analysis EPA 353.2, Rev 2, 1993 EPA 365.2, Rev 2, 1993 SM 2540 C-1997 Hach Mtd 10242 SM 2540 D-1997 14 mg/L 03 -Nov -16 SM 4500 CI -B-1997 < 1 #/100ml 02 -Nov -16 Colilert 9223 B-2004 0.45 mg/L 03 -Nov -16 EPA 351.1 Rev 2, 1993 < 0.25 mg/L 03 -Nov -16 EPA 353.2, Rev 2, 1993 < 0.05 mg/L 04 -Nov -16 EPA 365.2, Rev 2, 1993 74_ mg/L, 02 -Nov -16 ° SM 2540 C71997 45.5 mg/L < 1 #/100mi 0.47 mg/L < 0.25 mg/L < 0.05 mg/L 81 mg/L 03 -Nov -16 SM 4500 CI -13-1997 02 -Nov -16 Colilert 9223 B-2004 03 -Nov -16 EPA 351.1 Rev 2, 1,993 03 -Nov -16 EPA 353.2, Rev 2, 1993 04 -Nov -16 EPA 365.2, Rev 2, 1993 07 -Nov -16. SM, 2540 C-1997 Certified by: r1 - di�ut Lab Manager Todd A. Roberts Page 1 of 2 Permit: WQ0019907 Sample Collection Date: 02-Nov-16 a MW 3 Amount Units ' Analysis Began Analysis IVlethod Cl- 27.5 mg/L 03-Nov-16 SM 4500 CI-13-1997 Fecal MPN < 1 #/100m[ 02-Nov-16 Colilert 9223 B-2004 NH3 < 0.2 mg/L 03-Nov-16 EPA 351.1 Rev 2, 1993 NO3 <'0.25 mg/L 03-Nov-16 EPA 353.2, Rev 2, 1993 P < 0.05 mg/L 04-Nov-16 EPA 365.2, Rev 2, 1993 TDS 98 mg/L 02-Nov-16 SM 2540 C-1997 MW 4 Amount Unjts Analysis Began Analysis Method CI- 24 mg/L 03-Nov-16 SM 4500 CI-B-1997 Fecal MPN < 1 #/100ml 02-Nov-16 Colilert 9223 B-2004 NH3 < 0.2 mg/L 03-Nov-16 EPA 351.1 Rev 2, 1993 NO3 < 0.25 mg/L 03-Nov-16 EPA 353.2, Rev 2, 1993 P 0.11 mg/L 04-Nov-16 EPA 365.2, Rev 2, 1993 TDS 47 mg/L. 07-Nov-16 SM 2540 C-1997 Certified by: l r% Lab Manager Todd A. Roberts ORC: Mark Young Facility: Holly Ridge Spray Field Page 2 of 2 ENVIRONMENTAL CHEMISTS, INC Sample Collection and Chain of Custody Client: ONWASA-Holly Ridge WWTP & Spray Field Collected By:_,i,,,il.I,f k. � /��, f�,�PORC: Mark Young Sample Type: I = Influent, E Effluent, W =Well, ST =Stream, SO =Soil, SL= Sludge Other: 6602 Windmill Way Wilmington, NC 28405 Phone: (910)-392-0223 Fax: (910)-39"24 Report No: & — ` rib Sample Identification QcaH a z Collection �, „ a .Q a` c� IOU r 0 a 0. v" e .] 3.. v PRESERVATION ANALYSIS REQUESTED z z x z x c z ° H x c DATE TIME TEMP HR MW Iil- ,1645007-03 3 � t�10'D Z - 1 u 3 v r�, g W C I, X MW VOC 11.2-16 G G HRMW211-Z-1t: 1645007-04 r l'J. Y W C P X MW VOC - 2-/L G G HRMW3 1645007-05 11- 2-1G Ki" ��� + 3 W C P X MW VOC I I' Z -1 G G HR MW 4 1645007-06 3�5 U 2� W C P X MW VOC - 2- G G C P G G G P G G G P G G Transfer Relinquished By: Date/Time #qceived By: Date/Time oil 2. Temperature iv •�1 Accepted: Rejecte Resample ReM—� qu sted: Delivered By Received By: Date: /Time: V Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab • 910.392.4424 Fax 0 710 Bowsertown Road, Manteo, NC 27954 . 252.473S702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 3 CONSULTING CHEMISTS info@environmentalchemists.com Onslow Water & Sewer Authority Date of Report: Nov 14, 2016 Post Office Box 1415 Customer PO #: SM 6200C Jacksonville NC 28541 Customer ID: 08100092 Attention: Todd Roberts Report #: 2016-15820 1,1,2 -Trichloroethane Project ID: Holly Ridge Spray Fields Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-38168 Site: MW -1 11/2/2016 8:30 AM Water Joseph Arledge Test Method Results Date Analyzed 1,1,1,2 Tetrachloroethane SM6200C < 0.50 pg/L 11/5/2016 1,1,1 Trichloroethane SM 6200C <0.50pg/L ,11/512016 1,1,2,2 -Tetrachloroethane SM 6200C < 0.50 pg/L 11/5/2016 1,1,2 -Trichloroethane SM 6200C < 0.50 pg/L 11/5/2016 1,1-Dichloroethane sM 62000, < 0.50 pg/L 11/5/2016 1,1-Dichloroethene SM 6200C < 0.50 pg/L 1115/2016 1,1-Dichloropropene SM 62ODC < 0.50 pg/L 11/5/2016 1,2,3-Trichlorobenzene SM.6200C < 0.50 pg/L 11/5/2016 1,2,3-Trichloropropane SM 62000 < 0,50pg/L 11/512016 1,2,4-Trichlorobenzene SM 62000 < 0.50 pg1L 11/512016 1,2,4-Tdmethylbenzene sM6200C < 0.50 pg/L 11/5/2016 1,2-Dibromo-3-Chloropropane SM 62000 < 0.50 pg1L 11/5/2016 1,2-Dibromoethane SM 6200C < 0.50 pg1L 11/5/2016 1,2 -Dichlorobenzene sM6200C < 0.50 pg/L 11/5/2016 1,2 Dichloroethane SM 62000 < 0.50 NgIL 11/5/2016 1,2-Dichloropropane SM 6200C < 0,50 pg/L 11/5/2016 1,3,5 Trimethylbenzene SM 6200C < 0.50 pg/L 11/5/2016 1,3 -Dichlorobenzene SM 6200C < 0.50 pg/L 11/5/2016 1,3-Dichloropropane SM 6200C < 0.50 pg/L 11/5/2016 1,4 -Dichlorobenzene SM 6200C < 0.50 pg/L 11/5/2016 2,2-Dichloropropane SM 6200C < 0.50 pg/L 11/512016 2-Chlorotoluene SM 6200C < 0.50 pg/L 11/5/2016 4-Chlorotoluene SM 62000 < 0.50 pg/L 11/512016 Benzene SM 6200C < 0.50 pg/L 111512016 Bromabenzene SM 62000 < 0.50 pg/L 11/5/2016 Bromochloromethane SM6200C < 0.50 pg/L 11/5/2016 Report*: 2016-15620 Page 1 of 12 Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wiimington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Pax ® 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax M 255-A Wilmin ton Hi hwa g g y, Jacksonville; NC 28540 .910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Onslow Water & Sewer Authority Date of Report: Nov 14, 2016 Post Office Box 1415 Customer PO M. Jacksonville NC 28541 Customer ID: 08100092 Attention: Todd Roberts Report #: . 2016-15820 Project ID: Holly Ridge Spray Fields Bromodichloromethane SM 6200C < 0.50 pg/L 11/5/2016 Bromoform SM 6200C < 0.50 pg/L 11/5/2016 Bromomethane SM 6200C < 0.50 pg/L 11/5/2016 Carbon tetrachloride sM 62000 < 0.50 pg/L 11/5/2016 Chlorobenzene SM 62000 < 0.50 pg/L 11/5/2016 Chloroethane sM 62000 < 0.50 pg/L 11/5/2016 Chloroform SM 6200C < 0.50 pg/L 11/5/2016 Chloromethane SM 6200C < 0.50 pg/L 11/5/2016 cis-1,2-Dichloroethene SM s200c < 0.50 pg/L 11/5/2016 cis-1,3-Dichloropropene SM 6200C < 0.50 pg/L 11/5/2016 Dibromochloromethane SM 62MC < 0.50 pg/L 11/5/2016 Dibromomethane SM 6200C < 0.50 pg/L 11/512016 Dichlorodifluoromethane SM 6200C < 0.50 pg/L 11/5/2016 Ethylbenzene SM 6200C < 0.50 pg/L 11/5/2016 Hexachlorobutadiene SM 6200C < 0.50 pg/L 11/5/2016 Isopropylbenzene SM 620oc < 0.50 pg/L 11/5/2016 M+P Xylene SM 62000 < 1.00 pg/L 11/5/2016 Methylene chloride 6M 6200C < 0.50 pg/L 11/5/2016 Naphthalene SM 6200C < 0.50 pg/L 1115/2016 n-Butylbenzene SM 6=C < 0.50 pg/L 11/5/2016 n-Propyibenzene SM 6200C < 0.50 pg1L 11/5/2016 ortho-Xylene SM 62000 < 0.50 pg/L 11/5/2016 p-lsopropyltoluene SM 62000 < 0.50 pg/L 11/5/2016 sec-Butylbenzene SM 6200C < 0.50 pg/L 11/512016 Styrene SM 66200C < 0.50 pg/L 11/5/2016 tert Butylbenzene SM 6200C < 0.50 pg/L 11/5/2016 Tetrachloroethene . SM 6200C < 0.50 pg/L 11 /512016 Toluene SM 62000 < 0.50 pg/L 11/5/2016 Trans-1,2-Dichloroethene SM 6200C <0.50pg/L 11/5/2016 Trans-1,3-dichloropropene SM 6200C < 0.50 pg/L 11/572016 Report#:: 2016-15820 Page 2 of 12 ANALYTICAL & CONSULTING CHEMISTS Onslow Water & Sewer Authority Post Office Box 1415 Jacksonville NC 28541 Attention: Todd Roberts Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 e 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Nov 14, 2016 Customer PO #: Customer ID: 08100092 Report #: 2016-15820 Project ID: Holly Ridge Spray Fields Trichloroethene SM 6200C < 0.50 Ilg/L 11/512016 Trichlorofluoromethane SM 62000 < 0.50 pg/L 11/5/2016 Vinyl chloride sM 6200C < 0.50 lag/L 11/5/2016 Report*- 2016-15020 Page 3 of 12 -71 Environmental Chemists, Inc. nvirochem 6602 Windmill Way, Wflmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax © 71013cmertown Road, Manteo, NC 27954 . 252.4735702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Onslow Water &. Sewer Authority Post Office Box 1415 Jacksonville NC 28541 Attention: Todd Roberts Date of Report: Nov 14, 2016 Customer PO #: Customer ID: 08100092 Report #: 2016-15820 Project ID: Holly Ridge Spray Fields Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-38170 Site: MW -2 11/2/2016 9:15 AM Water Joseph Arledge Test Method Results Date Analyzed 1,1,1,2 -Tetrachloroethane SM 6200c < 0.50 pg1L 11/5/2016 1,1,1 Trichloroethane sM 62ooc < 0.50 pg/L 11/512016 1,1,2,2 -Tetrachloroethane SM 62000 < 0.50 pg/L 11/5/2016 1,1,2 -Trichloroethane SM 62000 < 0.50 pg/L 11/5/2016 1,1-Dichloroethane SM 6200C < 0.50 pg1L 11/5/2016 1,1-Dichloroethene sM 6200c < 0.50 pg1L 11/5/2016 1,1-Dichloropropene sM 8200C < 0.50 pg/L 11/512016 1,2,3 Trichlorobenzene SM 6200c < 0.50 pg/L 11/5/2016 1,2,3-Trichloropropane SM 62MG < 0.50 pg/L 11/5/201 e 1,2,4-Trichlorobenzene SM 6260C < 0.50 pg/L 11/5/2016 1,2,4 Trimethylbenzene SM 6200c < 0.50 pg/L 11/5/2016 1,2-Dibromo-3-Chloropropane SM 6200c < 0.50 pg/L 11/5/2016 1,2-Dibromoethene SM 62ooc < 0.50 pg/L 1115/2016 1,2 -Dichlorobenzene SM 62000 < 0.50 pg/L 11/5/2016 1,2-Dichloroethane SM 62000 < 0.50 pg/L 11/5/2016 1,2-Dichloropropane SM 6200c < 0.50 pg/L 11/5/2016 1,3,5-T rimethylbenzene SM 6200c < 0.50 pg/L 11/512016 1,3 -Dichlorobenzene SM 62ooc < 0.50 pg/L 11/5/2016 1,3-Dichloropropane SM 6280c < 0.50 pg/L 11/5/2016 1,4 -Dichlorobenzene sM 6200c < 0.50 pg/L 11/5/2016 2,2-Dichloropropane sM 6200c < 0.50 pg1L 11/5/2016 2-Chlorotoluene sM enoc < 0,50 pg/L 11/5/2016 4-Chlorotoluene SM 6200C < 0,50 pg1L 11/5/2016 Benzene SM 6200C < 0.50 pg/L 11/5/2016 Bromobenzene SM 62000 < 0.50 pg/L 11/5/2016 Bromochloromethane SM 62ooc < 0.50 pg/L 11/5/2016 Repodtk: 2016-15820 Page 4 of 12 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392A424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax info@environmentalchemists.com Onslow Water & Sewer Authority Date of Report: Nov 14, 2016 Post Office Box 1415 Customer PO #: Jacksonville NC 28541 Customer ID: 08100092 Attention: Tadd Roberts Report #: 2016-15820 Project ID: Holly Ridge Spray Fields Bromodichloromethane SM 6200C < 0.50 pg/L 11/5/2016 Bromoform SM 62000 < 0.50 pg/L 11/512016 Bromomethane SM 6200c < 0.50 pg/L 11/5/2016 Carbon tetrachloride SM 62000 < 0.50 pg/L 11/5/2016 Chlorobenzene SM 6200c < 0.50 pg/L 11/6/2016 Chloroethane SM 6200C < 0.50 pg/L 11/512016 Chloroform SM 62000 < 0.50 pg/L 11/5/2016 Chloromethane SM 62MC < 0.50 pg/L 11/5/2016 cis-1,2-Dichloroethene SM 6200C < 0.50 pg/L 11/6/2016 cis-1,3-Dichloropropene sM 6200C < 0.50 pg/L 11/5/2016 Dibromochloromethane SM 6200c < 0.50 pg/L 11/5/2016 Dbromomethane SM 6200C < 0.50 pg/L 1115/2016 Dichlorodifluoromethane SM 6200c < 0.50 pg/L 11/5/2016 Ethylbenzene SM 6200c < 0.50 pg/L 1115/2016 Hexachlorobutadiene sM 6200c < 0.50 pg/L 11/5/2016 lsopropylbenzene SM 62ooc < 0.50 pg/L 11 /512016 M+P Xylene SM 6200C < 1.00 pg/L 11/5/2016 Methylene chloride SM 6200c < 0.50 pg/L 11/5/2016 Naphthalene SM 62000 < 0.50 pg/L 11/5/2016 n-Butylbenzene SM 6200C < 0.50 pg/L 11/512016 n-Propylbenzene SM62o0C < 0.50 pg/L 11/5/2016 ortho-Xylene SM 6200c < 0.50 pg/L 1115/2016 p-Isopropyltoluene SM 6200C < 0.50 pg/L 11/5/2016 sec-Butyibenzene SM 6200C < 0.50 pg/L 11/5/2016 Styrene sM6200C < 0.50 pg/L 11/5/2016 tert Butylbenzene sM6200C < 0.50 pg/L 11/5/2016 Tetrachloroethene SM 62000 < 0.50 pg/L 11/512016 Toluene SM 6200C < 0.50 pg/L 11/5/2016 Trans-l,2-Dichloroethene SM 6200c < 0.50 pg/L 11/5/2016 Trans-1,3-dichloropropene SM 6200C < 0.50 pg/L 11/5/2016 P,eport#:: 2016-15820 Page 5 of 12 :(�311vi ochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax info@environmentalchemists.com Onslow Water & Sewer Authority Date of Report: Nov 14, 2016 Post Office Box 1415 Customer PO #: Jacksonville NC 28541 Customer ID: 08100092 Attention: Todd Roberts Report #: 2016-15820 Project ID: Holly Ridge Spray Fields Trichloroethene SM 6200C < 0.50 pg/L 11/5/2016 Trichlorofluoromethane SM 6200C < 0.50 pg/L 11/5/2016 Vinyl chloride SM 6200C < 0.50 pg/L 11/5/2016 Report #:: 2016-15820 Page 6 or 12 envirochem ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax info@environmentalchemists.com Onslow Water & Sewer Authority Date of Report: Nov 14, 2016 Post Office Box 1415 Customer PO #: Jacksonville NC 28541 Customer 1D: 08100092 Attention: Todd Roberts Report #: 2016-15820 Project ID: Holly Ridge Spray Fields Lab ID ;Sample' -1D`= Collect Date/Time Matrix Sampled by �T6=3817n1 Slte;MW=3; 11/2/2016 9:45 AM Water Joseph Arledge -Test; Method Results Date Analyzed 1,1,1,2 -Tetrachloroethane SM 6200C <0.50pg/L 11/6/2016 1,1,1 -Trichloroethane SM 62000 < 0.50 pg/L 11/6/2016 1,1,2,2 -Tetrachloroethane sM62000 < 0.50 pg/L 11/6/2016 1,1,2 -Trichloroethane SM 6200C < 0.50 pg/L 11/6/2016 1,1-Dichloroethane SM 6200C < 0.50 pg/L 11/6/2016 1,1-Dichloroethene SM 62000 < 0.50 pg/L 11/6/2016 1,1-Dichloropropene SM 6200C < 0.50 pg/L 11/6/2016 1,2,3-Trichlorobenzene SM Mac < 0.50 pg/L 11/6/2016 1,2,3-Tdchloropropane SM 62000 < 0.50 pg/L 11/6/2016 1,2,4-Trichlorobenzene SM 62000 < 0.50 pg/L 11/6/2016 1,2,4 Trimethylbenzene SM 6200C <0.50pg/L 11/6/2016 1,2-Dibromo-3-Chloropropane SM 62000 < 0.50 pg/L 11/6/2016 1,2-Dibromoethane SM 6200C < 0.50 pg/L 11/6/2016 1,2 -Dichlorobenzene SM 6200C < 0.50 pg/L 11/6/2016 1,2-Dichloroethane SM 6200C < 0.50 pg/L 11/6/2016 1,2-Dichloropropane SM 62000 < 0.50 pg/L 11/6/2016 1,3,5-Trimethylbenzene SM 5200C < 0.50 pg/L 11/6/2016 1,3 -Dichlorobenzene SM62UDC < 0.50 pg/L 11/6/2016 1,3-Dichloropropane SM 6200C < 0.50 pg/L 11/6/2016 1,4 -Dichlorobenzene SM 62aoc < 0.50 pg/L 11/6/2016 2,2-Dichloropropane SM 6200C < 0.50 pg/L 11/6/2016 2-Chlorotoluene SM 6200C < 0.50 pg/L 11/6/2016 4-Chlorotoluene SM 62ooC < 0.50 pg/L 11/6/2016 Benzene SM 6200C < 0.50 pg/L 11/6/2016 Bromobenzene SM 6200C < 0.50 pg/L 111612016 Bromochloromethane SM 6200C < 0.50 pg/L 1116/2016 Report M: 2016-15620 Page 7 of 12 -:"Oqql F"Op, -- - I Environmental Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax ©710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax M 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Onslow Water & Sewer Authority Date of Report: Nov 14, 2016 Post Office Box 1415 Customer PO #: Jacksonville NC 28541 Customer lD: 08100092 Attention: Todd Roberts Report #: 2016-15820 Project ID: Holly Ridge Spray Fields Bromodichloromethane SM 6200C < 0.50 pg/L 11/6/2016 Bromoform SM 6200C < 0.50 pg/L 11/6/2016 Bromomethane SM 62000 < 0.50 pg/L 111612016 Carbon tetrachloride SM 6200C < 0.50 pg/L 11/6/2016 Chlorobenzene SM 6200C < 0.50 pg/L 11/6/2016 Chloroethane SM 62000 < 0.50 pg/L 11/6/2016 Chloroform SM 62000 < 0.50 pg/L 11/6/2016 Chloromethane SM 6200C < 0.50 pg/L 11/6/2016 cis-1,2-Dichloroethene SM 6200C < 0.50 pg/L 11/6/2016 cis-1,3-Dichloropropene SM 6200C < 0.50 pg/L 11/6/2016 Dibromochloromethane SM 6200C < 0.50 pg/L 11/6/2016 Dibromomethane SM 62000 < 0.50 pg/L 11/6/2016 Dichlorodifluoromethane SM 62000 < 0.50 pg/L 11/6/2016 Ethylbenzene SM 65200C < 0.50 pg/L 11/6/2016 Hexachlorobutadiene SM 62000 < 0.50 pg/L 11/612016 lsopropylbenzene SM 6200C < 0.50 pg/L 11/6/2016 M+P Xylene sM 62000 < 1.00 pg/L 11/612016 Methylene ehlorule SM s2o0c 1 28Ug/L 11/6/2016 Naphthalene SM 6200C < 0.50 pg/L 11/6/2016 n-Butylbenzene SM 6200C < 0.50 pg/L 11/6/2016 n-Propylbenzene SM 6200C < 0.50 pg/L 11/6/2016 ortho-Xylene SM 6200C < 0.50 pg/L 11/612016 p-Isopropyltoluene SM 6200C < 0.50 pg1L 11/6/2016 sec-Butylbenzene SM 6200C < 0.50 pg/L 11/6/2016 Styrene SM 6200C < 0.50 pg/L 11/6/2016 tert Butylbenzene SM 62000 < 0.50 pg/L 11/6/2016 Tetrachloroethene SM 62000 < 0.50 pg/L 11/6/2016 Toluene SM 62000 27 5 Ug1L' 11/6/2016 Trans-1,2-Dichloroethene SM 62000 < 0.50 pg/L 11/6/2016 Trans-1,3-dichloropropene SM 6200C < 0.50 pg/L 11/6/2016 Report#:: 2016-15820 Page 8 of 12 envirochem ANALYTICAL & CONSULTING CHEMISTS Onslow Water & Sewer Authority Post Office Box 1415 Jacksonville NC 28541 Attention:. Todd Roberts Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Nov 14, 2016 Customer PO M Customer ID: 08100092 Report #: 2016-15820 Project ID: Holly Ridge Spray Fields Trichloroethene SM 6200C < 0.50 pg/L 1116/2016 Trichlorofluoromethane SM 6200C < 0.50 pg/L 11/6/2016 Vinyl chloride SM 6200C < 0.50 pg/L 11/6/2016 Report#:: 2016-16820 Page 9 of 12 LL enviroehe,1�71 ANALYTICAL & CONSULTING CHEMISTS pp - Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax info@environmentalchemists.com Onslow Water & Sewer Authority Date of Report: Nov 14, 2016 Post Office Box 1415 Customer PO #: sM 62000 Jacksonville NC 28541 Customer 1D: 08100092 Aftention: Todd Roberts Report #: 2016-15820 1,1,2 -Trichloroethane Project ID: Holly Ridge Spray Fields Lab ID Sample ID: Collect Date/Time Matrix Sampledb� y 16-38172 Site: MW -4 11/2/2016 10:15 AM Water Joseph Arledge Test Method Results Date Analyzed 1,1,1,2 -Tetrachloroethane SM 6200C <0.50pg1L 11/6/2016 1,1,1 Trichloroethane sM 62000 < 0,50 pg/L 11/6/2016 1,1,2,2 -Tetrachloroethane SM6200C <0.50pg/L 11/6/2016 1,1,2 -Trichloroethane SM 6200C < 0.50 pg/L 11/6/2016 1,1-Dichloroethane SM 62000 < 0.50 pg/L 11/6/2016 1,1-Dichloroethene SM 6200C < 0.50 pg/L 11/6/2016 1,1-Dichloropropene SM 6200C < 0.50 pg/L 11/6/2016 1,2,3 Trichlorobenzene SM 6200C < 0.50 pg/L 11/6/2016 1,2,3-Trichloropropane SM 62000 < 0.50 pg/L 11/6/2016 1,2,4-Trichlorobenzene SM 6200C < 0.50 pg/L 11/6/2016 1,2,4-Trimethylbenzene SM 6200C < 0.50 pg/L 11/6/2016 1,2-Dibromo-3-Chloropropane SM 6200C < 0.50 pg/L 11/6/2016 1,2-Dibromoethane SM 62000 < 0.50 pg/L 1116/2016 1,2 -Dichlorobenzene SM 6200C < 0.50pg/L 11/612016 1,2-Dichloroethane SM 62000 < 0.50 pg/L 11/6/2016 1,2-Dichloropropane SM 6200C < 0.50 pg/L 11/6/2016 1,3,5-Trimethyibenzene SM 62MC < 0.50 pg/L 11/6/2016 1,3 -Dichlorobenzene SIA 6200C < 0.50 pg/L 11/6/2016 1,3-Dichloropropane SM 6200C < 0.50 pg/L 11/6/2016 1,4 -Dichlorobenzene SM 6200C < 0.50 pg/L 11/6/2016 2,2-Dichloropropane SM 62000 < 0.50 pg/L 11/6/2016 2-Chlorotoluene SM 62000 < 0.50 pg/L 11/6/2016 4-Chlorotoluene sM 62000 < 0.50 pg/L 11/612016 Benzene SM 62000 < 0.50 pg/L 11/6/2016 Bromobenzene SM 6200C < 0.50 pg/L 11/6/2016 Bromochloromethane sM 6200C < 0.50 pg/L 1116/2016 Report*.: 2016-16820 Page 10 of 12 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax sM 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Onslow Water & Sewer Authority Date of Report: Nov 14, 2016 Post Office Box 1415 Customer PO #: Jacksonville NC 28541 Customer ID: 08100092 Attention: Todd Roberts Report #: 2016-15820 Project ID: Holly Ridge Spray Fields Bromodichloromethane SM 62000 < 0.50 pg/L 11/6/2016 Bromoform SM 6200C < 0.50 pg/L 11/6/2016 Bromomethane SM 6200C < 0.50 pg/L 11/6/2016 Carbon tetrachloride SM 62000 < 0.50 pg/L 11/6/2016 Chlorobenzene SM 62ooc < 0.50 pg/L 11/6/2016 Chloroethane SM 6200c < 0.50 pg/L 111612016 Chloroform SM 6200C < 0.50 pg/L 11/6/2016 Chloromethane SM 62000 < 0.50 pg/L 11/6/2016 cis-1,2-Dichloroethene SM 6200C < 0.50 pg/L 11/6/2016 cis-1,3-Dichloropropene SM 6200C < 0.50 pg/L 11/6/2016 Dibromochloromethane SM 6200c < 0.50 pg/L 11/6/2016 Dibromomethane SM 62000 < 0.50 pg/L 11/6/2016 Dichlorodifluoromethane SM 6200C' < 0.50 pg/L 11/6/2016 Ethylbenzene SM 6200C < 0.50 pg/L 11/612016 Hexachlorobutadiene SM 6200C < 0.50 pg/L 11/6/2016 Isopropylbenzene SM 6200C < 0.50 pg1L 11/6/2016 M+P Xylene SM 62000 < 1.00 pg/L 111612016 Methylene chloride SM 6200C < 0.50 pg/L 11/6/2016 Naphthalene SM 6200c < 0.50 pg/L 11/6/2016 n-Butylbenzene SM 62ooc < 0.50 pg/L 11/6/2016 n-Propylbehzene sM 6200C < 0.50 pg/L 1116/2016 ortho-Xylene SM6200C < 0.50 pg/L 11/6/2016 p-Isopropyltoluene SM 6200c < 0.50 pg/L 11/6/2016 sec-Butylbenzene SM 62000 < 0.50 pg/L 11/6/2016 Styrene SM 6200c < 0.50 pg/L 11/6/2016 tert Butylbenzene SM 6200c < 0.50 pg/L 11/6/2016 Tetrachloroethene SM 62000 < 0.50 pg/L 11/6/2016 Toluene sM62000 < 0.50 pg/L 11/612016 Trans-1,2-Dichloroethene SM 6200c < 0.50 pg/L 11/6/2016 Trans-1,3-dichloropropene SM 6200c < 0.50 pg/L 11/6/2016 Reportk 2016-15820 Page 11 of 12 --71 Environmental Chemists, Inc. envirochem6602 Windmill Way, Wilmington, NC 28405 . 910.392.0223 Lab . 910.392.4424 Fax sM 710 Bowsertown Road, Manteo, NC 27954 . 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 . 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com Onslow Water & Sewer Authority Date of Report: Nov 14, 2016 Post Office Box 1415 Customer PO #- Jacksonville NC 28541 Customer ID: 08100092 Attention: Todd Roberts Report #: 2016-15820 Project ID: Holly Ridge Spray Fields Trichloroethene SM 6200c < 0.50 pg/L 11/6/2016 Trichlorofluoromethane SM 6200C < 0.50 pg/L 11/612016 Vinyl chloride SM 6200C < 0.50 pg/L 111612016 Comment: Reviewed by: Report#.': 2016-15820 Page 12 of 12