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HomeMy WebLinkAboutWQ0029169_Monitoring - 11-2016_20161222 (2)ER QUALITY MONITORING: REPORT FORM =acility Name: Town of Mount Olive oermit Name (if different): °acility Address: PO Box 939, 408 Wilkins farm Rd. Mount Olive NC act Person: Glenn Holland Location/Site Name: Field #11 Mount Olive SUBMIT FORM ON YELLOW PAPER ONLY 28365 County Wayne L ID NUMBER (from Permit): WM-1 Depth: 25.0 ft. h to Water Level 82548: 13.0 ft. below measuring point luring Point is 2.0 ft. above land surface ne of water pumped/bailed before sampling: 6.0 Telephone#: 919-658-6538 No. of wells to be sampled: 4 ION OF WATER QUALITY -INFORMATION PROCESSING UNIT MAIL SERVICE CENTER. RALEIGH. NC 27999-1617 Phone: 19191733-3221 PERMIT Number: Expiration Date: 3/31/2020 Non -Discharge W00029169 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ® Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other Date sample collected: 11-17-2016 FIELD ANALYSES: Well Diameter: 2 in. pH oo400: 6.5 units Temp. 00010: 20 °C Screened Interval: 5 ft. to 25 ft. Spec. Cond. 00094: µMhos Relative M.P. Elevation: 166.23 ft. Odor 000es: Is Appearance and field acidified: ❑ YES ❑ NO its sample analyzed: 11117/2016-11/30/2016 Laboratory Name: Mlcrobac %RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo61s mg/L Coliform: MF Fecal 31616 <1 /100ml. Nitrate (NO3) as N 00620 0.41 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 0o665 <0.05 mg/L (Note: Use MPNrrethodlorhighly tor5losamples) Orthophosphate 70507 mg/L (solved SDlids:Total70300 88.0 mg/L AI -Aluminum alms mg/L pH (Lab) 00403 units Be - Barium 01007 ug/L TOC o068o 2.12 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 3.3 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L Phenol 32730 uglL Fe- Iron oio4s ug/L Sulfate 00945 mg/L Hg - Mercury 71900 ug/L ,ecific Conductance 0009s µMhos K - Potassium 00937 mg/L Total Ammonia oo6ta <0.10 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen', NH,as N Ammonle Nitrogen, Total) Mn - Manganese aioss ug/L TKN as N 00625 mg/L Ni - Nickel oio67 ug/L For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Certification No. 37714 Y� Pb - Lead 01051 ug/L Zn - Zinc 01092 mg/L Ll L 9 Other (Specify Comp P l_Tr 9tMn,Units): OEC227nii�ItJJ 1 1 �uli� Mill a _C 1, ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ® Yes (1) ❑ No (0) VOC 78732: , method # SW82608 method # method # method # Effluent Total VOCs: mg/L VOC Removal% at Of GW -59 Rev. 2/2010 SUBMIT FORM ON YELLOW PAPER ONLY TER QUALITY MONITORING: E REPORT FORM Facility Name: Town of Mount Olive Permit Name (if different): Facility Address: PO Box 939, 408 Wilkins farm Rd. Mount Olive NC 28365 County Wayne act Person: Glenn Holland Location/Site Name: Field #11 Mount Olive L ID NUMBER (from Permit): WM-2 Depth: 25.0 ft. h to Water Level 82546: 8.0 ft. below measuring point luring Point is 2.0 ft. above land surface me of water pumped/bailed before sampling: 8.31 Telephone#: 919-658-6538 No. of wells to be sampled: 4 ION OF WATER QUALITY-MFORMATION PROCESSING UNIT MAIL SERVICE CENTER, RALEIGH, NC 27999-1917 Phone: (919) 737-3221 :RMIT Number: Expiration Dale: 3/31/2020 ,n -Discharge W00029169 UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery N Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample collected: 11-17-2016 FIELD ANALYSES: Well Diameter: 2 in. pH 00400: 5.0 units Temp. 000lo: 19 °C Screened Interval: 10 ft. to 25 ft. Spec. Cord. 00094: µMhos Relative M.P. Elevation: 161.76 ft. Odor000m: iS Appearance NO and field acidified: ❑ YES 1te sample analyzed: 11/1712016-11/3012016 Laboratory Name: Microbac \RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N goals mg/L Coliform: MF Fecal 31616 <1 /100ml. Nitrate (NO3) as N 00620 16.8 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.05 mg/L (Note: Use MPN method for Nghly turbid samples) Orthophosphate 70507 mg/L ;solved Solids:Tot817030o286 mg/L AI - Aluminum of1as mg/L pH (Lab) 00403 units Be - Barium 01007 ug/L TOC 0o68a 2.95 mg/L Ca -Calcium 00916 mg/L Chloride 00940 42.7 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01o42 mg/L Phenol 32730 ug/L Fe - Iron alo4s ug/L Sulfate oo945 mg/L Hg - Mercury 71900 ug/L iecific Conductance 00095 µMhos K - Potassium 00937 mg/L Total Ammonia amilt <0.10 mg/L Mg - Magnesium 00927 mg/L (AmmoNa Narogem Nl6 as N; Ammome Mtrogen, Tom) Mn - Manganese 01055 ug/L TKN as N oo62s mg/L Ni - Nickel 01067 ug/L For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs. Pb - Lead olos1 Zn - Zinc 01092 Certification No. 37714 ug/L mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? E Yes (1) ❑ No (0) VOC 78732: , method # SW8260B method # method # method # mg/L Effluent Total VOCs. mg/L VOC Removal% Charles S. Brown, Town Manager_. r— / 17-( Permittee (or Authorized Agent) Name and Tide - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW -59 Rev. 212010 DRY at time of here: El NDWATER QUALITY MONITORING: LIANCE REPORT FORM =acility Name: Town of Mount Olive permit Name (if different): =acility Address: PO Box 939,4G8 Wilkins farm Rd. Mount Olive NC 9Ct Person: Glenn Holland Location/Site Name: Field #12 Mount Olive SUBMIT FORM ON YELLOW PAPER ONLY 28365 County Wayne L ID NUMBER (from Permit): WM-3 Depth: 25 ft. h to Water Level 92546: 8.0 ft. below measuring point luring Point is 2.0 ft. above land surface ne of water pumped/bailed before sampling: 8.31 )les for metals were collected unfiltered: ❑ YES ❑ Telephone#: 919-658-6538 No. of wells to be sampled: 4 IF WATER QUALITY -INFORMATION PROCESSING UNIT SERVICE CENTER. RALEIGH. NC 27999.1917 Phone: (9191 737-3221 :RMIT Number: Expiration Date: 3/31/2020 m -Discharge W00029169 UIC IDES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample collected: 11-17-2016 FIELD ANALYSES: Well Diameter: 2 in. pH oo400: 5.6 units Temp. 000lo: 18 OC Screened Interval: 5 ft. to 25 ft. Spec. Cord. coo94: µMhos Relative M.P. Elevation: 141.10 ft. Odor 000a5: is Appearance NO and field acidified: ❑ YES ❑ NO rte sample analyzed: 11/t7/2016-1 7/2016-110=016 Laboratory Name: Microbac 1RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 mg/L Coliform: MF Fece131616 <1 /100ml- Nitrate (NO3) as N 00620 5.58 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 <0.05 mg/L (Note: Use MPN method for highly turt,id samples) Orthophosphate 70507 mg/L ,solved Solids:Total 70300 122 mg/L AI -Aluminum III los mg/L pH (Lab) 00403 units Be - Barium 01007 ug/L TOC oo690 2.26 mglL Ca - Calcium oo916 mg/L Chloride 0094o 22.3 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L Phenol 32730 ug/L Fe - Iron 01045 ug/L Sulfate 00945 mg/L Hg -Mercury 71900 ug/L iecific Conductance onogs µMhos K - Potassium 00937 mg/L Total Ammonia collo <0.10 mg/L Mg - Magnesium 06927 mg/L (Ammonia Nitrogen; NK as N; Ammonia Nitrogen, Total) Mn - Manganese oloss ug/L TKN as N 00625 mg/L Ni- Nickel 01o67 ug/L Certification No. 37714 Pb - Lead o1o51 ug/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? ® Yes (1) ❑ No (0) VOC 79732: method # SW8260S method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs. mg/L Effluent Total VOCs: mg/L VOC Removal at Of Charles S. Brown, Town Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW -59 Rev. 2/2010 SUBMIT FORM ON YELLOW PAPER ONLY WELL ID NUMBER (from Permit): WM-4 Date sample collected: 11-17-2016 Well Depth: 25 ft. Well Diameter: 2 in. Depth to Water Level 82546:_15.0 ft. below measuring point Screened Interval: 5 ft. to 25 ft. — Measuring Point is 2.0 ft. above land surface Relative M.P. Elevation: 155.69 ft. Volume of water pumped/bailed before sampling: 5.0 gallons Samples for metals were collected unfiltered: [I YES El NO and field acidified: E3 YES [I NO FIELD ANALYSES: pH 00400: 5.7 units Temp. 000lo: 20 °C Spec. Cond. 000s4: µMhos Odor 000e5: Appearance DEPARTMENT OF ENVIRONMENT 6 NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY411FORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: (919)7334221 FACILITY INFORMATION Please PdniClearly OFType PERMIT Number: Expiration Date: 3/31/2020 Facility Name: Town of Mount Olive Certification No. 37714 Non -Discharge W00029169 UIC Permit Name (if different): dissolved and colloidal concentrations. NPDES Other Facility Address: PO Box 939, 408 Wilkins farm Rd. TYPE OF PERMITTED OPERATION BEING MONITORED Mount Olive NC 28365 County Wayne Nitrite (NO2) as N 00615 ❑ Lagoon ❑ Remediation: Infiltration Gallery Pb - Lead oio51 ug/L ® Spray Field ❑ Remediation: Contact Person: Glenn Holland Telephone#: 919-658-6538 Nitrate (NO3) as N 00620 5.3 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Field #12 Mount Olive No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: WELL ID NUMBER (from Permit): WM-4 Date sample collected: 11-17-2016 Well Depth: 25 ft. Well Diameter: 2 in. Depth to Water Level 82546:_15.0 ft. below measuring point Screened Interval: 5 ft. to 25 ft. — Measuring Point is 2.0 ft. above land surface Relative M.P. Elevation: 155.69 ft. Volume of water pumped/bailed before sampling: 5.0 gallons Samples for metals were collected unfiltered: [I YES El NO and field acidified: E3 YES [I NO FIELD ANALYSES: pH 00400: 5.7 units Temp. 000lo: 20 °C Spec. Cond. 000s4: µMhos Odor 000e5: Appearance WAS DRY at time of sampling, check here: ❑ LABORATORY INFORMATION Date sample analyzed: 11/17/2016-11/30/2016 Laboratory Name: Microbac Certification No. 37714 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 ri Nitrite (NO2) as N 00615 mg/L Pb - Lead oio51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 5.3 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 1100mL Phosphorus: Total as P 00665 <0.05 mg/L (Note: Use NPN method t°r highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 98 ri AI - Aluminumol ms mg/L pH (Lab) 00403 units Be - Barium 01007 ug/L TOC oo68o 2.32 mg/L Ca - Calcium oo916 mg/L Chloride 00940 16.1 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01o42 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 uglL Lab Report Attached? W Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732. , method # SW8260B Total Ammonia 00610 <0.10 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3ae N; Ammonia Nitrogen, Total) Mn - Manganese om55 ug/L , method # TKN as N 00625 ri Ni - Nickel ot067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal GW -59 Rev. 212010 Town of Mt. Olive Mr. Glen Holland Post Office Box 939 Mt. Olive NC, 28365 Result Analyzed by: Microbac Laboratories, Inc. - Chicagoland 1,1,1,2 -Tetrachloroethane <0.12 1,1,1 -Trichloroethane <0.19 1,1,2,2 -Tetrachloroethane <0.20 1,1,2 -Trichloroethane <0.39 1, l -Dichloroethane <0.16 1, 1 -Dichloroethene <0.19 1,2-Dichloroethane <0.14 1,2-Dichloropropane <0. 15 2-Butanone <0.83 2-Hexanone <0.22 4-Methyl-2-Pentanone <0.26 Acetone 5.6 Acrolein Acrylonitrile Benzene B romodichloromethane Bromoform Bromomethane Carbon Disulfide Carbon tetrachloride Chlorobenzene Chloroethane Chloroform Chloromethane cis-1,2-Dichloroethene cis-1,3-Dichloropropane D ibromochloromethane Ethylbenzene m,p-Xylene Methylene chloride Microbac Laboratories, Inc. Page 1 of 16 2592 Hope Mills Road I 'Fayetteville, NC 28306 1910.864.1920 p 1910-864.8774 f I www.microbac.com <2.1 <3.-3 <0.18 <0.30 <0.27 1.3 <0.26 <0.16 <0.16 <0.41 <0.21 <0.33 <0.20 <0.090 <0.80 <0.15 <0.43 <0.31 I ' Fayetteville Division Certificate of Analysis Project: M/W Samples - Nov Units gg/L gg/L gg/L gg/L gg/L n/L gg/L gg/L gg/L gg/L gg/L gg/L gg/L gg/L gg/L Itg[L gg/L gP/- gg/L gg/L gg/L gg/L gg/L gg/L gg/L gg/L gg/L ggA- gg/L gg/L MW#1 K6K0818-01, 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08' 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 1 i:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 1180/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 11/30/16 11:08 jln jin jin jln jin jin jin jin jin jin jin jln jin jln jln jin jin jln jln jin jln jln jln jin jin jln jln jln jin jln Date Reported: 12/06/16 Date Received: 11/17/16 Date Sampled: 11/17/16 Sampled By: Method SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846-8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B SW -846 8260B ifier J Town of Mt. Olive Mr. Glen Holland Post Office Box 939 Mt. Olive NC, 28365 I C �§ Fayetteville Division Certificate of Analysis Project: M/W Samples - Nov MW#1 Date Reported: 12/06/16 Date Received: 11/17/16 Date Sampled: 11/17/16 Sampled By: K6K0818-01 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Chicagoland Methyl -t -Butyl Ether <0.I 1 gg/L 11/30/16 11:08 jin SW -846 8260B o -Xylene <0.23 gg/L 11/30/16 11:08 jln SW -846 8260B Styrene <0.14 gg/L 11/30/16 11:08 jin SW -846 8260B Tetrachloroethene <0.32 gg/L 11/30/16 11:08 jin SW -846 8260B Toluene <0.15 gg/L 11/30/16 11:08 jln SW -846 8260B trans-l,2-Dichloroethene <0.23 gg/L 11/30/16 11:08 jin SW -846 8260B trans-l,3-Dichloropropene <0.18 gg/L 11/30/16 11:08 jin SW -846 8260B Trichloroethene <0.29 gg/L 11/30/16 11:08 jln SW -846 8260B Trichlorofluoromethane <0.30 gg/L 11/30/16 11:08 jin SW -846 8260B Vinyl Acetate <0.20 gg/L 11/30/16 11:08 jln SW -846 8260B Vinyl chloride <0.17 gg/L 11/30/16 11:08 jin SW -846 8260B Analyzed by: Microbac Laboratories, Inc. - Fayetteville Ammonia as N <0.100 mg/L 11/18/16 08:30 DSK SM 4500 NH3 C-1997 Chloride 3.30 mg/L 11/19/16 11:59 AC EPA 300.0, Rev. 2.1 (1993) Coliform, Fecal <I.0 per 100 mL 11/17/16 16:28 JR SM 9222 D-1997 Depth of Water 25.0 feet 11/17/16 10:30 DED Field Measurement Depth to Water Surface 13.0 feet 11/17/16 10:30 DED Field Measurement Gallons purged 6.0 gallons 11/17/16 10:30 DED Field Nitrate as N 0.405 mg/L 11/19/16 11:59 AC EPA 300.0, Rev. 2.1 (1993) pH, Field Test 6.5 pH Units 11/17/16 10:30 DED SM 4500 H+B-2000 (Aqueous) Phosphorus, Total <0.050 mg/L 11/21/16 12:06 DSK SM 4500-P F-1999 Total Dissolved Solids 88.0 mg/L 11/18/16 10:21 JR SM 2540 C-1997 Temperature, field 20 °C 11/17/16 10:30 DED SM 2550 B-2000 Analyzed by: Microbac Laboratories, Inc. - Ohio Valley Total Organic Carbon 2.12 mg/L 11/29/16 22:55 EPT SM5310-C-2000 MW #2 K6K0818-02 Analyte Result Units Analyzed Analyzed By Method Qualifier Microbac Laboratories, Inc. Page 2 of 16 2592 Hope Mills Road I Fayetteville, NC 28306 1 910.864.1920 p 1910.864.8774 f I www.microbac.com R Fayetteville Division Certificate of Analysis Microbac Laboratories, Inc. Page 3 of 16 2592 Hope Mills Road I Fayetteville, PIC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com Date Reported: 12/06/16 Town of Mt. Olive Date Received: 11/17/16 Mr. Glen Holland Project: M/W Samples - Nov Date Sampled: 11/17/16 Post Office Box 939 Sampled By: Mt. Olive NC, 28365 MW #2 K6K0818-02 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Chicagoland 1,1,1,2 -Tetrachloroethane <0.12 µg/L 11/30/16 11:29 jIn SW -846 8260B 1,1,1 -Trichloroethane <0.19 ltg/L 11/30/16 11:29 jln SW -846 8260B 1,1,2,2 -Tetrachloroethane <0.20 µg/L 11/30/16 11:29 jln SW -846 8260B 1,1,2 -Trichloroethane <0.39 µg/L 11/30/16 11:29 jIn SW -846 8260B 1, 1 -Dichloroethane <0.16 gg/L 11/30/16 11:29 jIn SW -8468260B IJ-Dichloroethene <0.19 µg/L 11/30/16 11:29 jln SW -846 8260B 1,2-Dichloroethane <0.14 µg/L 11/30/16 11:29 jln SW -846 8260B 1,2-Dichloropropane <0.15 µg/L 11/30/16 11:29 jln SW -846 8260B 2-Butanone <0.83 µg/L 11/30/16 11:29 jIn SW -846 8260B 2-I-lexanone <0.22 µg/L 11/30/16 11:29 jln SW -846 8260B 4-Methyl-2-Pentanone <0.26 µg/L 11/30/16 11:29 jln SW -846 8260B Acetone 4.3 µg/L 11/30/16 11:29 jln SW -846 8260B J Acrolein <2.1 ltg/L 11/30/16 11:29 jln SW -846 8260B Acrylonitrile <3.3 ltg/L 11/30/16 11:29 jln SW -846 8260B Benzene <0.18 µg/L 11/30/16 11:29 jIn SW -846 8260B Bromodichloromethane <0.30 µg/L 11/30/16 11:29 jIn SW -846 8260B Bromoform <0.27 µg/L 11/30/16 11:29 jIn SW -846 8260B Bromomethane 0.82 µg/L 11/30/16 11:29 jln SW -846 8260B J Carbon Disulfide <0.26 gg/L 11/30/16 11:29 jln SW -846 8260B Carbon tetrachloride <0.16 µg/L 11/30/16 11:29 jln SW -846 8260B Chlorobenzene <0.16 µg/L 11/30/16 11:29 jln SW -846 8260B Chloroethane <0.41 µg/L 11/30/16 11:29 jIn SW -846 8260B Chloroform <0.21 µg/L 11/30/16 11:29 jIn SW -846 8260B Chloromethane <0.33 µg/L 11/30/16 11:29 jln SW -846 8260B cis-1,2-Dichloroethene <0.20 gg/L 11/30/16 11:29 jln SW -846 8260B cis-1,3-Dichloropropene <0.090 µg/L 11/30/16 11:29 jln SW -846 8260B Dibromochloromethane <0.80 gg/L 11/30/16 11:29 jIn SW -846 8260B Ethylbenzene <0.15 µg/L 11/30/16 11:29 jln SW -846 8260B rn,p-Xylene <0.43 µg/L 11/30/16 11:29 jln SW -846 8260B Methylene chloride <0.31 ltg/L 11/30/16 11:29 jln SW -846 8260B Microbac Laboratories, Inc. Page 3 of 16 2592 Hope Mills Road I Fayetteville, PIC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com «: Fayetteville Division Certificate of Analysis Town of Mt. Olive Mr. Glen Holland Project: M/W Samples - Nov Post Office Box 939 Mt. Olive NC, 28365 Date Reported: 12/06/16 Date Received: 11/17/16 Date Sampled: 1 I/17/16 Sampled By: MW #2 K6K0818-02 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Chicagoland <0.100 mg/L 11/18/16 08:30 DSK SM 4500 NH3 C-1997 Methyl -t -Butyl Ether <0.I 1 n/L 11/30/16 11:29 jln SW -846 8260B o -Xylene <0.23 gg/L 11/30/16 11:29 jln SW -846 8260B Styrene <0.14 ltg/L 11/30/16 11:29 jln SW -846 8260B Tetrachloroethene <0.32 µg/L 11/30/16 11:29 jln SW -846 8260B Toluene <0.15 pg/L 11/30/16 11:29 jln SW -846 8260B trans-l,2-Dichloroethene <0.23 gg/L 11/30/16 11:29 jln SW -846 8260B trans-l,3-Dichloropropene <0.18 gg/L 11/30/16 11:29 jln SW -846 8260B Trichloroethene <0.29 µg/L 11/30/16 11:29 jln SW -846 8260B Trichlorofluoromethane <0.30 µg/L 11/30/16 11:29 jln SW -846 8260B Vinyl Acetate <0.20 ltg/L 11/30/16 11:29 jln SW -846 8260B Vinyl chloride <0.17 µg/L 11/30/16 11:29 jln SW -846 8260B Analyzed by: Microbac Laboratories, Inc. - Fayetteville Ammonia as N <0.100 mg/L 11/18/16 08:30 DSK SM 4500 NH3 C-1997 Chloride 42.7 mg/L 11/19/16 11:59 AC EPA 300.0, Rev. 2.1 (1993) Coliform, Fecal <1.0 per 100 mL 11/17/16 16:28 JR SM 9222 D-1997 Depth of Water 25.0 feet 11/17/16 10:00 DED Field Measurement Depth to Water Surface 8.00 feet 11/17/16 10:00 DED Field Measurement Gallons purged 8.3 gallons 11/17/16 10:00 DED Field Nitrate as N 16.8 mg/L 11/19/16 11:59 AC EPA 300.0, Rev. 2.1 (1993) pH, Field Test 5.0 pH Units 11/17/16 10:00 JMP SM 4500 H+B-2000 (Aqueous) Phosphorus, Total <0.050 mg/L 11/21/16 12:06 DSK SM 4500-P F-1999 Total Dissolved Solids 286 mg/L 11/18/16 10:21 JR SM 2540 C-1997 Temperature, field 19 °C 11/17/16 10:00 JMP SM 2550 B-2000 Analyzed by: Microbac Laboratories, Inc. - Ohio Valley Total Organic Carbon 2.95 mg/L 11/29/16 23:16 EPT SM5310-C-2000 MW #3 K6K0818-03 Analyte Result Units Analyzed Analyzed By Method Qualifier Microbac Laboratories, Inc. Page 4 of 16 2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com ig I ,k - Result Fayetteville Divisi6n Analyzed Certificate of Analysis Method Qualifier Town of Mt. Olive Date Reported: 12/06/16 Mr. Glen Holland Project: M/W Samples - Nov Date Received: I (/17/16 Post Office Box 939 Date Sampled: 11/17/16 Mt. Olive NC, 28365 Sampled By: M W '#3 K6K0818-A3 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories,, Inc. - Chicagoland Acrylonitrile <3.3 Rg/L 11/30/16 11:50 1,1,1,2 -Tetrachloroethane <0.12 gg/L 11/30/16 11:50 jIn SW -8468260B 1,1,1 -Trichloroethane <0.19 µg/L 11/30/16 11:50 jIn SW -8468260B 1,1,2,2 -Tetrachloroethane <0.20 µg/L 11/30/16 11:50 jIn SW -846 8260B 1,1,2 -Trichloroethane <0.39 I g/L 11/30/16 11:50 jln SW -846 8260B 1, 1 -Dichloroethane <0.16 µg/L 11/30/16 11:50 jIn SW -846 8260B 1, 1 -Dichloroethene <0.19 µg/L 11/30/16 11:50 .jIn SW -8468260B 1,2-Dichloroethane <0.14 µg/L 11/30/16 11:50 jIn SW -846 8260B 1,2-Dichloropropane <0.15 gg/L 11/30/16 11:50 jln SW -846 8260B 2-Butanone <0.83 gg/L 11/30/16 11:50 jln SW -846 8260B 2-Hexanone <0.22 µg/l- 11/30/16 11:50 jIn SW -846 8260B 4-Methyl-2-Pentanone <0.26 µg/L 11/30/16 11:50 jIn SW -846 8260B Acetone 4.3 gg/L 11/30/16 11:50 jIn SW -846 8260B J Acrolein <2.1 Rg/L 11/30/16 11:50 jln SW -846 8260B Acrylonitrile <3.3 Rg/L 11/30/16 11:50 jIn SW -846 8260B Benzene <0.18 gg/L 11/30/16 11:50 jln SW -846 8260B Bromodichloromethane <0.30 µg/L 11/30/16 11:50 jIn SW -846 8260B Bromoform <0.27 µg/L 11/30/16 11:50 jIn SW -846 8260B Bromomethane <0.37 gg/L 11/30/16 11:50 jln SW -846 8260B Carbon Disulfide <0.26 µg/L 11/30/16 11:50 jIn SW -846 8260B Carbon tetrachloride <0.16 gg/L 11/30/16 11:50 jln SW -846 8260B Chlorobenzene <0.16 µg/L 11/30/16 11:50 jln SW -846 8260B Chloroethane <0.41 µg/1.. 11/30/16 11:50 jIn SW -846 8260B Chloroform <0.21 Itg/L 11/30/16 11:50 jIn SW -846 8260B Chloromethane <0.33 µg/L 11/30/16 11:50 jIn SW -846 8260B cis-1,2-Dichloroethene <0.20 gg/L 11/30/16 11:50 jIn SW -846 8260B cis-1,3-Dichloropropene <0.090 gg/L 11/30/16 11:50 jln SW -846 8260B Dibromochloromethane <0.80- gg/L 11/30/16 11:50 jln SW -846 8260B Ethylbenzene <0.15 gg/L 11/30/16 11:50 jIn SW -846 8260B m,p-Xylene <0.43 µg/L 11/30/16 11:50 jln SW -846 8260B Methylene chloride <0.31 µg/L 11/30/16 11:50 jIn SW -846 8260B Microbac Laboratories, Inc. Page 5 of 16 2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com ,' Fayetteville Division Certificate of Analysis Town of Mt. Olive Mr. Glen Holland Project: M/W Samples - Nov Post Office Box 939 Mt. Olive NC, 28365 Date Reported: 12/06/16 Date Received: 11/17/16 Date Sampled: 11/17/16 Sampled By: MW #3 K6K0818-03 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Chicagoland Methyl -t -Butyl Ether <0.I I pg/L 11/30/16 11:50 jln SW -846 8260B o -Xylene <0.23 µg/L 11/30/16 11:50 jln SW -846 8260B Styrene <0.14 µg/L 11/30/16 11:50 jln SW -846 8260B Tetrachloroethene <0.32 gg/L 11/30/16 11:50 jln SW -846 8260B Toluene <0.15 µg/L 11/30/16 11:50 jin SW -846 8260B trans-l,2-Dichloroethene <0.23 µg/L 11/30/16 11:50 jin SW -846 8260B trans-l,3-Dichloropropene <0.18 µg/L 11/30/16 11:50 jln SW -846 8260B Trichloroethene <0.29 µg/L 11/30/16 .11:50 jln SW -846 8260B Trichlorofluoromethane <0.30 µg/L 11/30/16 11:50 jin SW -846 8260B Vinyl Acetate <0.20 pg/L 11/30/16 11:50 jln SW -846 8260B Vinyl chloride <0.17 pg/L 11/30/16 11:50 jin SW -846 8260B Analyzed by: Microbac Laboratories, Inc. - Fayetteville Ammonia as N <0.100 mg/L 11/18/16 08:30 DSK SM 4500 NH3 C-1997 Chloride 22.3 mg/L 11/19/16 11:59 AC EPA 300.0, Rev. 2.1 (1993) Coliform, Fecal <1.0 per 100 mL 11/17/16 16:28 JR SM 9222 D-1997 Depth of Water 25.0 feet 11/17/16 09:45 JMP Field Measurement Depth to Water Surface 8.00 feet 11/17/16 09:45 JMP Field Measurement Gallons purged 8.3 gallons 11/17/16 09:45 JMP Field Nitrate as N 5.58 mg/L 11/19/16 11:59 AC FPA 300.0, Rev. 2.1 (1993) pH, Field Test 5.6 pH Units 11/17/16 09:45 JMP SM 4500 H+13-2000 (Aqueous) Phosphorus, Total <0.050 mg/L 11/21/16 12:06 DSK SM 4500-P F-1999 Total Dissolved Solids 122 mg/L 11/18/16 10:21 JR SM 2540 C-1997 Temperature, field 18 °C 11/17/16 09:45 JMP SM 2550 B-2000 Analyzed by: Microbac Laboratories, Inc. - Ohio Valley Total Organic Carbon 2.26 mg/L 11/29/16 23:38 EPT SM5310-C-2000 MW #4 K6K0818-04 Analyte Result Units Analyzed Analyzed By Method Qualifier Microbac Laboratories, Inc. Page 6 of 16 2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com .R Fayetteville Division Certificate of Analysis Town of Mt. Olive Date Reported: 12/06/16 Mr. Glen Holland Project: M/W Samples - Nov Date Received: 11/17/16 Post Office Box 939, Date Sampled: 11/17/16 Mt. Olive NC, 28365 Sampled By: MW #4 K6K0818-04 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Chicagoland 1,1,1,2 -Tetrachloroethane <0.12 Itg/L 11/30/16 12:12 jln SW -846 8260B 1, 1, l -Trichloroethane <0.19 gg/L 11/30/16 12:12 jln SW -846 8260B 1,1,2,2 -Tetrachloroethane <0.20 µg/L 11/30/16 12:12 jln SW -8468260B 1,1,2 -Trichloroethane <0.39 gg/L 11/30/16 12:12 jIn SW -846 8260B I,1-Dichloroethane <0.16 gg/L 11/30/16 12:12 jIn SW -846 8260B I,1-Dichloroethene <0.19 gg/L 11/30/16 12:12 jIn SW -846 8260B 1,2-Dichloroethane <0.14 µg/L 11/30/16 12:12 jln SW -846 8260B 1,2-Dichloropropane <0.15 gg/L 11/30/16 12:12 jln SW -846 8260B 2-Butanone <0.83 n/L 11/30/16 12:12 jln SW -846 8260B 2-Hexanone <0.22 gg/L 11/30/16 12:12 jln SW -846 8260B 4-Methyl-2-Pentanone <0.26 µg/L 11/30/16 12:12 jIn SW -846 8260B Acetone 3.8 µg/L 11/30/16 12:12 jln SW -846 8260B J Acrolein <2.1 µg/L 11/30/16 12:12 jIn SW -846 8260B Acrylonitrile <3.3 µg/L 11/30/16 12:12 jIn SW -846 8260B Benzene <0.18 gg/L 11/30/16 12:12 jln SW -846 8260B Bromodichloromethane <0.30 gg/L 11/30/16 12:12 jIn SW -846 8260B Bromoform <0.27 gg/L 11/30/16 12:12 jIn SW -846 8260B Bromomethane <0.37 gg/L 11/30/16 12:12 jln SW -846 8260B Carbon Disulfide <0.26 gg/L 11/30/16 12:12 jln SW -846 8260B Carbon tetrachloride <0.16 µg/L 11/30/16 12:12 jln SW -846 8260B Chlorobenzene <0.16 µg/L 11/30/16 12:12 jIn SW -846 8260B Chloroethane <0.41 gg/L 11/30/16 12:12 j1.n SW -846 8260B Chloroform <0.21 ttg/L 11/30/16 12:12 jIn SW -846 8260B Chloromethane <0.33 gg/L 11/30/16 12:12 jIn SW -846 82608 cis-1,2-Dichloroethene <0.20 µg/L 11/30/16 12:12 jln SW -846 8260B cis-1,3-Dichloropropene <0.090 gg/L 11/30/16 12:12 jln SW -846 8260B Dibromochloromethane <0.80 gg/L 11/30/16 12:12 jIn SW -846 8260B Ethylbenzene <0.15 gg/L 11/30/16 12:12 jIn SW -846 8260B m,p-Xylene <0.43 gg/L 11/30/16.12:12 jIn SW -846 8260B Methylene chloride <0.31 I g/L 11/30/16 12:12 jIn SW -846 8260B Microbac Laboratoeies; Inc. Page 7 of 16 2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com <tDMICROBAC& Fayetteville Division Certificate of Analysis Town of Mt. Olive Mr. Glen Holland Project: M/W Samples - Nov Post Office Box 939 Mt. Olive NC, 28365 Date Reported: 12/06/16 Date Received: 11/17/16 Date Sampled: I (/17/16 Sampled By: MW #4 K6KO818-04 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Chicagoland Methyl -t -Butyl Ether <0.1 I gg/L 11/30/16 12:12 jln SW -846 8260B o -Xylene <0.23 µg/L 11/30/16 12:12 jln SW -846 8260B Styrene <0.14 µg/L 11/30/16 12:12 jln SW -846 8260B Tetrachloroethene <0.32 µg/L 11/30/16 12:12 jln SW -846'8260B Toluene <0.15 µg/L 11/30/16 12:12 jln SW -846 8260B trans-1,2-Dichloroethene <0.23 µg/L 11/30/16 12:12 jln SW -846 8260B trans-l,3-Dichloropropene <0.18 gg/L 11/30/16 12:12 jln SW -846 8260B Trichloroethene <0.29 Itg/L 11/30/16 12:12 jln SW -846 8260B Trichlorofluoromethane <0.30 µg/L 11/30/16 12:12 jln SW -846 8260B Vinyl Acetate <0.20 µg/L 11/30/16 12:12 jln SW -846 8260B Vinyl chloride <0.17 gg/L 11/30/16 12:12 jln SW -846 8260B Analyzed by: Microbac Laboratories, Inc. - Fayetteville Ammonia as N <0.100 mg/L 11/18/16 08:30 DSK SM 4500 NH3 C-1997 Chloride 16.1 mg/L 11/19/16 11:59 AC EPA 300.0, Rev. 2.1 (1993) Coliform, Fecal <1.0 per 100 mL 11/17/16 16:28 JR SM 9222 D-1997 Depth of Water 25.0 feet 11/17/16 10:15 JMP Field Measurement Depth to Water Surface 15.0 feet 11/17/16 10:15 JMP Field Measurement Gallons purged 5.0 gallons 11/17/16 10:15 JMP Field Nitrate as N 5.30 mg/L 11/19/16 11:59 AC EPA 300.0, Rev. 2.1 (1993) pH, Field Test 5.7 pH Units 11/17/16 10:15 JMP SM 4500 H+B-2000 (Aqueous) Phosphorus, Total <0.050 mg/L 11/21/16 12:06 DSK SM 4500-P F-1999 Total Dissolved Solids 98.0 mg/L 11/18/16 10:21 JR SM 2540 C-1997 Temperature, field 20 °C ' 11/17/16 10:15 JMP SM 2550 B-2000 Analyzed by: Microbac Laboratories, Inc. - Ohio Valley Total Organic Carbon 2.32 mg/L 11/29/16 23:59 EPT SM5310-C-2000 Trip Blank K6KO818-05 Analyte Result Units Analyzed Analyzed By Method Qualifier 1 Microbac Laboratories, Inc. Page 8 of 7 2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com ,k VMICROBAC Fayetteville Division Certificate of Analysis Town of Mt. Olive Date Reported: 12/06/16 Mr. Glen Holland Project: M/W Samples - Nov Date Received: 11/17/1.6 Post Office Box 939 Date Sampled: I (/17/16 Mt. Olive NC, 28365 Sampled By: Trip Blank K6K0818-05 Analyzed by: Microbac Laboratories, Inc. - Chicagoland 1,.1,1,2 -Tetrachloroethane <0.12 gg/L 11/30/16 10:47 jIn SW -846 8260B 1,1,1 -Trichloroethane <0.19 µg/L 11/30/16 10:47 jIn SW -8468260B 1,1,2,2 -Tetrachloroethane <0.20 n/L. 11/30/16 10:47 jln SW -846 8260B 1,1,2 -Trichloroethane <0.39 n/L 11/30/16 10:47 jln SW -846 8260B 1, 1 -Dichloroethane <0.16 µg/L 11/30/16 10:47 jln SW -846 8260B 1, 1 -Dichloroethene <0,19 gg/L 11/30/16 10:47 jln SW -8468260B 1,2-Dichloroethane <0.14 gg/L 11/30/16 10:47 j1n SW -846 8260B 1,2-Dichloropropane <0.15 µg/L 11/30/16 10:47 jln SW -846 8260B 2-Butanone <0.83 µg/L 11/30/16 10:47 jln SW -846 8260B 2-Hexanone <0.22 gg/L 11/30/16 10:47 jln SW -846 8260B 4-Methyl-2-Pentanone <0.26 gg/L 11/30/16 10:47 jln SW -846 8260B Acetone 3.1 gg/L 11/30/16 10:47 jIn SW -846 8260B Acrolein <2.1 µg/L 11/30/16 10:47 jln SW -846 8260B Acrylonitrile <3.3 ltg/L 11/30/16 10:47 jln SW -846 8260B Benzene <0.18 gg/L _ 11/30/16 10:47 jIn SW -846 8260B Bromodichloromethane <0.30 m/L 11/30/16 10:47 jln SW -846 8260B Bromoform <0.27 gg/L 11/30/16 10:47 jin SW -846 8260B Brotnomethane <0.37 µg/L 11/30/16 10:47 jln SW -846 8260B Carbon Disulfide <0.26 µg/L 11/30/16 10:47 jln SW -846 8260B Carbon tetrachloride <0.16 µg/L 11/30/16 10:47 jln SW -846 8260B Chlorobenzene <0.16 µg/L 11/30/16 10:47 j1n SW -846 8260B Chloroethane <0.41 n/L 11/30/16 10:47 jln SW -846 8260B Chloroform 0.95 gg/L 11/30/16 10:47 jln SW -846 8260B Chloromethane <0.33 gg/L 11/30/16 10:47 jln SW -846 8260B cis-1,2-Dichloroethene <0.20 µg/L 11/30/16 10:47 jln SW -846 8260B cis-1,3-Dichloropropene <0.090 µg/L 11/30/16 10:47 jln SW -846 8260B Dibromochloromethane <0.80 µg/L 11/30/16 10:47 jln SW -846 8260B Ethylbenzene. <0.15 µg/L 11/30/16 10:47 jln SW -846 8260B m,p-Xylene <0.43 µg/L _ 11/30/16 10:47 jIn SW -846 8260B Methylene chloride 1.7 µg/L, 11/30/16 10:47 jIn SW -846 8260B J J J Microbac Laboratories, Inc. Page 9 of 16 2592 Hope Mills Road I Fayetteville, NC 28306 1 910.864.1920 p 1910.864.8774 f I www.microbac.com ICS . Fayetteville Division Certificate of Analysis Town of Mt. Olive Mr. Glen Holland Project: M/W Samples - Nov Post Office Box 939 Mt. Olive NC, 28365 Date Reported: 12/06/16 Date Received: 11 / 17/16 Date Sampled: 11/17/16 Sampled By: Trip Blank K6K0818-05 Analyte Result Units Analyzed Analyzed By Method Qualifier Analyzed by: Microbac Laboratories, Inc. - Chicagoland Methyl -t -Butyl Ether <0.I I µg/L 11/30/16 10:47 jln SW -846 8260B o -Xylene <0.23 µg/L 11/30/16 10:47 jln SW -846 8260B Styrene <0.14 µg/L 11/30/16 10:47 jln SW -846 8260B Tetrachloroethene <0.32 µg/L 11/30/16 10:47 jln SW -846 8260B Toluene <0.15 µg/L 11/30/16 10:47 jln SW -846 8260B trans-l,2-Dichloroethene <0.23 gg/L 11/30/16 10:47 jln SW -846 8260B trans-l,3-Dichloropropene <0.18 µg/L 11/30/16 10:47 jln SW -846 8260B Trichloroethene <0.29 µg/L 11/30/16 10:47 jln SW -846 8260B Trichlorofluoromethane <0.30 µg/L 11/30/16 10:47 jln SW -846 8260B Vinyl Acetate <0.20 gg/L 11/30/16 10:47 jln SW -846 8260B Vinyl chloride <0.17 µg/L 11/30/16 10:47 jln SW -846 8260B Notes and Definitions U Not detected at or above adjusted sample detection limit i The analyte was positively identified, but the quantitation was below the RL Microbac Laboratories, Inc. •I Page 10 of 16 2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 19,10.864.8774 f I www.microbac.com