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HomeMy WebLinkAboutWQ0005555_Monitoring - 11-2016_20161222GW -59A COMPLIANCE REPORT FORM Permit # NA'000055.55 (Submit one each monitoring period with GW -59 forms.) GW -59A 1 Enter date monitoring results were due. (Dec. 31, 2016) Will this monitoring report (GW -59 and GW -59A) be YES NO submitted after the established due date? 2 Was any required information missing on the GW -59 report forms? YES NO IF the answer to question 1 or 2 is "YES" list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? IJthe answer is "Yes". contact the Regional Offiice jorguidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is WO", skip to section 8. If the answer to question 41s "YES "list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below. MW -5 VOC Chloroform 2.2 ug/L Per NC DWQ request, we are performing VOC tests during all routine monitoring. We will be dropping back to the Nov. annual VOC monitoring, unless notified by NC DWR to do additional sampling. For the constituents identified in question 4 above, have standards been exceeded previously for the same 5 YES NO constituent(s) in the same well(s) in the last two years? Met with Patrick Mitchell on Feb. 18, 2016 to discuss high chloroform readings. The readings for MW -5 was 1.7 ug/l. It was recommended that if the well was staying consistently at this level to go back to the annual monitoring. It was noted during our meeting to monitor Chromium Levels in the wells and if they continue to rise notify NC DWR for further instructions. If the answer to question 5 is "NO", skip to section 8. ; . /'� awing If the answer to question 5 is "YES" list in the space provided below, each well with cgq�1{tpent(s) standards, concentration(a) reported, and sample collection date for each occurrence (for M61as*01m ss). OVVR <, 6 Are the monitoring wells listed in section 5 located at or beyond the review bo NPR()CFSSINGUNIT YES NO if the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer Is "NO" monitoring wells may be Improperly located; contact the Regional Office. 7 is the permittee implementing previously approved actions required by the Division Involving this YES NO groundwater quality problem? If the answer to question 7 is "YES" describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be reguired to determine the impact the waste disposal system Is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines. and/or penalties. See Responses to #4 and #5 g The person completing this portion (GW -59A) of the monitoring report should sign below and submit this form with GW -59 forms for required wells to the address provided at the top of the current GW -59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance/e ReportGW-59A) is true andreoommplete�to the best of my knowledge. Signature of Permittee (or Authorized Agent) Date Ia1) ►6 SUBMIT FORM ON YELLOW PAPER ONLY ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM Facility Name: Weyerhaeuser NR Company Permit Name (if different): Facility Address: 524 Pdde Way Elkin NC 28621 County Suny act Person: Dennis Atkinson Telephone#: 336-526-6437 Location/Site Name: 36 Deg 15.112N / 80 Deg 47.447W No. of wells to be sampled: 9 WELL ID NUMBER (from Permit): MW 4 Well Depth: 61.17 ft. Depth to Water Level 82546: 50.9 ft. below measuring point Measuring Point is 0.8 ft. above land surface Volume of water pumped/bailed before sampling: 3.5 gall Samoles for metals were collected unfiltered: 171 YES ❑ NO PARTMENT OF ENVIRONMENT B NATURAL RESOURCES ISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 7 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733.3221 RMIT Number: W00005555 Expiration Date: 4/30/2019 n -Discharge UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑� Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample collected: 11/02/16 FIELD ANALYSES: Well Diameter: 2 in. pH 00400: 6.8 units Temp. 000lo: 18.1 °C Screened Interval: ft. to ft. Spec. Cond. 00094: 45.8 µMhos Relative M.P. Elevation: ft. Odor 000es: none s Appearance mostly Gear field acidified: ® YES ❑ NO Date sample analyzed: Beginning 11102/16 Laboratory Name: Prism Lab PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 0 mg/L Nitrite (NO2) as N 00615 mg/L Coliform: MF Fecal 31616 0 /100ml- Nitrate (NO3) as N 00620 .51 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P oo665 .14 mg/L (Note: Use MPN method for highly Nroid samples) Orthophosphate 70507 mg/L )issolved Solids:Total 70300 0 mg/L AI - Aluminum D1105_mg/L pH (Lab) 00403 5.8 units Be - Barium D1007 ug/L TOC 00680 .86 mg/L Ca - Calcium 00916 mg/L Chloride oog4o 1.1 mg/L Cd - Cadmium 01027 ug/L Arsenic olo02 ug/L Chromium: Total olo34 40 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L Phenol 32730 ug/L Fe - Iron o1 o45 ug/L Sulfate oo945 mg/L Hg - Mercury 71900 0 ug/L Specific Conductance 000fis 41 µMhos K - Potassium 00937 mg/L Total Ammonia omio 0 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen) NH°as N; Ammonia Nitrogen, Toho Mn - Manganese o1 o55 uglL TKN as N 00625 mg/L Ni - Nickel 01067 ug/L Certification No. 402 Pb - Lead oio51 ug/L Zn - Zinc 01092 mg/L Other (Specify Compounds and Concentration Units): Formaldehyde, Total 0 mg/L Di ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? K Yes (1) ❑ No (0) VOC 78732: , method # 8260B method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal at of Debbie Tadlock, Mill Manager Permittee (or Authorized Agent) Name and Title - Plea" prim or type GW -59 Rev. 212010 SUBMIT FORM ON YELLOW PAPER ONLY UNDWATER QUALITY MONITORING: PLIANCE REPORT FORM Name: Weyerhaeuser NR Company Name (if different): Address: 524 Pride Way Elkin NC 28621 County act Person: Dennis Atkinson Telephone#: 336-526-6437 Location/Site Name: 36 Deg 15.112N / 80 Deg 47.447W No. of wells to be sampled: 9 OF WATER QUALITY-INFORMA'nON PROCESSING UNIT L SERVICE CENTER. RALEIGH. NC 27699.1617 Phone: (919) 733-3221 .RMIT Number: WQ0005555 Expiration Date: 4/30/2019 m -Discharge UIC IDES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery IN Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: WELL ID NUMBER (from Permit): MW 5 Date sample collected: 11/02/16 Well Depth: 45.0 ft. Well Diameter: 2 in. Depth to Water Level 82546:40.5 ft. below measuring point Screened Interval: ft. — Measuring Point is 1.0 ft. above land surface Relative M.P. Elevation: Volume of water pumped/bailed before sampling: 2..4 gallons Samples for metals were collected unfiltered: m YES ❑ NO and field acidified: ® YES to ft. ft. ❑ NO FIELD ANALYSES: pH 00400: 5.39 units Temp. 000to: 16.4 °C Spec. Cond. 000e4: 53.8 µMhos Odor 00085: None Appearance Mostly clear WAS DRY at time of sampling, check here:❑ LABORATORY INFORMATION Date sample analyzed: Beginning 11102/16 Laboratory Name: Prism Lab Certification No. 402 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 0 mg/L Nitrite (NO2) as N oosls mg/L Pb - Lead D1051 ug/L Coliform: MF Fecal 31616 0 /100ml- Nitrate (NO3) as N 00620 0 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P oo665 .24 mg/L (Note: use MPN method for highly wrote samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 0 mg/L At -Aluminum o11os mg/L Formaldehyde, Total 0 mg/L pH (Lab) 00403 5 units Ba - Barium o1oo7 ug/L nj TOC 00680 1.5 mg/L Ca - Calcium 00915 mg/L Chloride oog4o 1 mg/L Cd - Cadmium o1o27 ug/L I 2017 Arsenic 01002 ug/L Chromium: Total o1a34 13 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 uglL (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 0 ug/L Lab Report Attached? ❑W Yes (1) ❑ No (0) pecific Conductance 000ss 0 µMhos K - Potassium 00937 mg/L VOC 78732: , method # 8260B Total Ammonia 00610 0 mg/L Mg - Magnesium 00927 mg/L , method # (Ammonia Nitrogen: N1 -136s N', Amrwnia Nivogen, Total) Mn - Manganese o1o5s ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mq/L Effluent Total VOCs: mg/L VOC Removal GW -59 Rev. 2/2010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM Elkin Name: Weyerhaeuser NR Company Name (if different): Address: 524 Pride Way NC 28621 County Suny act Person: Dennis Atkinson Telephone#: 336-526-6437 Location/Site Name: 36 Deg 15.112N / 80 Deg 47.447W No. of wells to be sampled: 9 ISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 7 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 RMIT Number: WQ0005555 Expiration Date: 4/30/2019 n -Discharge UIC ,DES Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery O Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other LID NUMBER (from Permit): MW 6 Date sample collected: 11/02/16 FIELD ANALYSES: Depth: 57.7 ft. Well Diameter: 2 in. pH 00400: 6.02 units Temp. 000lo: 18.8 eC i to Water Level 82546:47.0 ft. below measuring point Screened Interval:_ft. to _ft. Spec. Cond. 000s4: 33.6 µMhos luring Point is 1.7 ft. above land surface Relative M.P. Elevation: ft. Odor 000e5: none ne of water pumped/bailed before sampling: 5 gallons Appearance Clear 11es for metals were collected unfiltered: 1.71 YES n NO and field acidified: ® YES ❑ NO Date sample analyzed: Beginning 11/02/16 Laboratory Name: Prism Lab Certification No. 402 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 0 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead oto51 ug/L Coliform: MF Fecal 31616 0 /100mL Nitrate (NO3) as N 00620 .61 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P00665 .31 mg/L (Nota: Use MPN memod formaNy turgid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Assolved Solids:Total 70300 0 mg/L AI -Aluminum o11o5 mg/L Formaldehyde, Total 0�m 11 1ee•�� pH (Lab) 00403 5.5 units Ba - Barium D1007 ug/L TOC oo6so .87 mg/L Ca - Calcium 00916 mg/L .)A N G 6 Chloride oos4o 0 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 6 ug/L Grease and Oils 00652 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oos45 mg/L Hg - Mercury 71900 0 ug/L Lab Report Attached? X Yes (1) ❑ No (0) 3pecific Conductance 000gs 22 µMhos K - Potassium 00937 mg/L VOC 78732: , method # 82608 Total Ammonia oo610 0 mg/L Mg - Magnesium 00927 mg/L , method # (Ammonia Nitrogen: NH, as K Ammonia Nitrogen. Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal Debbie Tadlock, Mill Manager Permittee (or Authonzed Agent) Name and Ti6e - Please print or type GW -59 Rev. 2/2010 at of ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM Elkin Name: Weyerhaeuser NR Company Name (if different): Address: 524 Pride Way act Person: Dennis Atkinsor Location/Site Name: 36 Deg SUBMIT FORM ON YELLOW PAPER ONLY NC 28621 County 15.112N / 80 Dea 47.447W Telephone#: 336-526-6437 No. of wells to be sampled: 9 ISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 7 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: (919)733-322' IRMIT Number: W00005555 Expiration Date: 413012019 n -Discharge UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery K Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: LID NUMBER (from Permit): MW 7 Date sample collected: 11/02/16 FIELD ANALYSES: Depth: 60.6 ft. Well Diameter: 2 in. pH 00400:_ units Temp. 000lo: °C h to Water Level 82546: ft. below measuring point Screened Interval: —ft. to _ft. Spec. Cord. 00094: µMhos curing Point is 1.84 ft. above land surface Relative M.P. Elevation: ft. Odor 000ss: me of water pumped/bailed before sampling: gallons Appearance Dies for metals were collected unfiltered: m YES ❑ NO and field acidified: ® YES ❑ NO Date sample analyzed: Beginning Laboratory Name: Prism Lab Certification No. 402 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oasis mg/L Pb - Lead olas1 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /1OOmL Phosphorus: Total as P 00665mg/L (Note: Use MPN method for higMy tumid samples) Orthophosphate 70e07—Di— mg/L Other (Specify Compounds and Concentration Units): Assolved Solids:Total 70300 mg/L. Al -Aluminum 01105 mg/L Formaldehyde, Total D41— pH (Lab) 00403 units Be - Barium oloo7' ug/L TOC oo68o mg/L Ca - Calcium oog16 mg/L nAI n 6� ��_ Chloride 00900 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total otp34 ug/L Grease and Oils oo552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1D45 ug/L (Specify test and method A ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71 goo ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: , method # 8260B Total Ammonia oo610 mg/L Mg - Magnesium 00927 mg/L , method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese o1 os5 uglL method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: ri Effluent Total VOCs: mg/L VOC Removal Debbie Tadlock, Mill Manager Families (or Authorized Agent) Name and Title - Please pant or type GW -59 Rev. 22010 at of SUBMIT FORM ON YELLOW PAPER ONLY Debbie Tadlock, Mill Manager Nfxsl I . I 0-44,4&-Zt\� 1;2 Pennines (or ANhorized Agent) Name and Title - Please print or type Signature of Permittee (or AWhonzed Agent) (I GW -59 Rev. 2/2010 DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919)733-3221 FACILITY INFORMATION Please Pnnt Clearly or Type PERMIT Number: W00005555 Expiration Date: 4/30/2019 Facility Name: Weyerhaeuser NR Company Non -Discharge UIC NPDES Other Permit Name (if different): Facility Address: 524 Pride Way TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Elkin NC 28621 County Burry M Spray Field ❑ Remediation: Contact Person: Dennis Atkinson Telephone#: 336-526-6437 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: 36 Deg 15.11214 / 80 Deg 47.447W No. of wells to be sampled: 9 ❑ Water Source Heat Pump ❑ Other: Imm PemB SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW 8 Date sample collected: 11/02/16 FIELD ANALYSES: WAS Well Depth: 57 ft. Well Diameter: 2 in. pH 00400:_ units Temp. 000to: °C DRY at Depth to Water Level 82546: ft. below measuring point Screened Interval: ft. to ft. Spec. Cord. 00094: µMhos lime sampling, Measuring Point is 1.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: gallons Appearance here: O Samples for metals were collected unfiltered: m YES ❑ NO and field acidified: ®YES ❑ NO LABORATORY INFORMATION Date sample analyzed: Beginning Laboratory Name: Prism Lab Certification No. 402 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 /100ml- Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly tuNid samples) Orthophosphate 70507 mg/L Other (Specify Ccsirs and Concentration Units): )issolved Solids:Total 70300 mg/L Al - Aluminum o11o5 mg/L Formaldehyde, TOtaISIg/L pH (Lab) 00403 units Be - Barium 01007 ug/L TOC oo68o mg/L Ca - Calcium 00916 mg/L Chloride oos4o mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) 3pecifc Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 78732: , method # 82606 Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nieogen', NHsas N; Armenia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal Debbie Tadlock, Mill Manager Nfxsl I . I 0-44,4&-Zt\� 1;2 Pennines (or ANhorized Agent) Name and Title - Please print or type Signature of Permittee (or AWhonzed Agent) (I GW -59 Rev. 2/2010 For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mq/L Effluent Total VOCs: VOC Removal% GW -59 Rev. 212010 SUBMIT FORM ON YELLOW PAPER ONLY - DEPARTMENT OF ENVIRONMENT 8 NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM , 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: W00005555 Expiration Date: 4/30/2019 =acility Name: Weyerhaeuser NR Company Non -Discharge UIC NPDES Other permit Name (if different): =acility Address: 524 Pride Way TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Elkin NC 28621 County Burry X Spray Field ❑ Remediation: contact Person: Dennis Atkinson Telephone#: 336-526-6437 ❑ Rotary Distributor ❑ Land Application of Sludge Nell Location/Site Name: 36 Deg 15.112N 180 Deg 47.447W No. of wells to be sampled: 9 ❑ Water Source Heat Pump ❑ Other: Iron Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW 9 Date sample collected: 11/02/16 FIELD ANALYSES: WAS Well Depth: 6359 ft. Well Diameter: 2 in. pH 00400: 5.54 units Temp. 000lo: 21.3 eC DRY at Depth to Water Level 62546: 56.1 ft. below measuring point Screened Interval: — ft. to ft. Spec. Cord. 00094: 52.9 µMhos time of sampling, Measuring Point is 12 ft, above land surface Relative M.P. Elevation: ft. Odor 000m None check Volume of water pumped/bailed before sampling: 1.2 gallons Appearance Clear here:❑ Samples for metals were collected unfiltered: m YES ❑ NO and field acidified: ® YES ❑ NO LABORATORY INFORMATION Date sample analyzed: eeginmg 11/02/16 Laboratory Name: Prism Lab Certification No. 402 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 0 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead olos1 ug/L Coliform: MF Fecal 31616 0 /10GmL Nitrate (NO3) as N 00620 .41 mg/L Zn - Zinc 01092 mg/L Collform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 .093 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Nssolved Solids:Total 70300 0 mg/L At - Aluminum of im mg/L Formaldehyde, MI 0 mg/L PH (Lab) 00403 5.2 units Be - Barium 01007 ug/L TOC oo68o 1.6 mg/L Ca - Calcium 00916 mg/L 7 Chloride o094o 4.3 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 1.2 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 0 uglL Lab Report Attached? X Yes (1) ❑ No (0) Specific Conductance 00095 32 µMhos K - Potassium 00937 mg/L VOC 78732: , method # 8260B Total Ammonia oo610 0 mg/L Mg - Magnesium 00927 mg/L , method # (Ammonia Nirwen; NH3 as N. Ammons Nitrogen, Total Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mq/L Effluent Total VOCs: VOC Removal% GW -59 Rev. 212010 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: mg/L DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM Coliform: MF Fecal 31616 0 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: (919)733-3221 FACILITY INFORMATION Please Print Clearly or Type mg/L PERMIT Number: W00005555 Expiration Date: 4/30/2019 Facility Name: Weyerhaeuser NR Company mg/L Non -Discharge UIC Permit Name (if different): mg/L NPDES Other Facility Address: 524 Pride Way mg/L TYPE OF PERMITTED OPERATION BEING MONITORED Elkin NC 28621 County Su rry Be - Barium 01007 ❑ Lagoon ❑ Remediation: Infiltration Gallery mg/L Ca - Calcium 1111919 IN Spray Field ❑ Remediation: Contact Person: Dennis Atkinson Telephone#: 336-526-6437 Cd - Cadmium 01027 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: 36 Deg 15.112N 180 Deg 47.447W No. of wells to be sampled: 9 Chromium: Total 01034 12 ❑ Water Source Heat Pump ❑ Other: LID NUMBER (from Permit): MW 10 Depth: 29.4 ft. r to Water Level 02646:24.9 ft. below measuring point luring Point is 2.5 ft. above land surface ne of water pumped/bailed before sampling: 1.0 3les for metals were collected unfiltered: m YES ❑ Date sample collected: 11/02/16 Well Diameter: 2 in. Screened Interval: —ft. to ft. Relative M.P. Elevation: ft. gallons NO and field acidified: ® YES ❑ NO ate sample analyzed: Beginning 11/02116 Laboratory Name: Prism Lab IRAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 69 mg/L Nitrite (NO2) as N oos15 mg/L Coliform: MF Fecal 31616 0 /100ml- Nitrate (NO3) as N 00620 1.2 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P oos65 .66 mg/L (Note: use MPN method for highly tumid samples) Orthophosphate 70507 mg/L ,solved Solids:Total 70300 0 mg/L AI - Aluminum altos mg/L pH (Lab) 00403 5.4 units Be - Barium 01007 ug/L TOC oo66o 1.5 mg/L Ca - Calcium 1111919 mg/L Chloride costo 2.5 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 12 uglL Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L Phenol 32730 ug/L Fe - Iron 01 o4s ug/L Sulfate costs mg/L Hg - Mercury 71900 0 ug/L ecific Conductance 000ss 28 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 0 mglL Mg - Magnesium oo927 mg/L (Ammonia Nitrogen: NH3as N. Ammonia Nitrogen, TOel) Mn - Manganese 01055 ug/L TKN as N 00625 mg/L Ni - Nickel 01067 ug/L For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs Debbie Tadlock, Mill Manager Permittee (or Authorized Agent) Name and Tide - Please print or type GW -59 Rev. 22010 FIELD ANALYSES: WAS pH 00400: 6.7 units Temp. goclo: 18.2 eC DRY at Spec. Cord. 00094: 35.8 pMhos time of samplir Odor 000ss: none check Appearance Mostly clear here:r Certification No. 402 Pb - Lead oloa1 ug/L Zn - Zinc 01092 mg/L Other (Specify Com unds and Concentration Units): Formaldehyde, Tot r' mg/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method A ATTACH LAB REPORT.) Lab Report Attached? R Yes (1) ❑ No (0) VOC 78732: , method # 8260B method # method # method # mg/L Effluent Total VOCs: mg/L VOC Removal SUBMIT FORM ON YELLOW PAPER ONLY UNDWATER QUALITY MONITORING: PLIANCE REPORT FORM Name: Weyerhaeuser NR Company Name (if different): Address: 524 Pride Way Elkin - NC 28621 County act Person: Dennis Atkinson Location/Site Name: 36 Deg 15.112N / 80 47.447W Telephone#: 336-526-6437 No. of wells to be sampled: 9 pARTMENT OF ENVIRONMENT a NATURAL RESOURCES iS1ON OF WATER QUALITY -INFORMATION PROCESSING UNIT 7 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: (919)733.3221 RMIT Number: W00005555 Expiration Date: 4/30/2019 n -Discharge UIC 'DES Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery A Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other LID NUMBER (from Permit): MW 11 Date sample Collected: 11/02/2016 FIELD ANALYSES: WAS Depth: 48.2 ft. Well Diameter: 2 in. pH 00400: 6.31 units Temp. o001o: 17.7 °C DRY at i to Water Level 82546: 28.9 ft. below measuring point Screened Interval: ft. to — ft. Spec. Cond. 00094: 39.00 µMhos time of samplin ,uring Point is 1.76 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check ne of water pumped/bailed before sampling: 6 gallons Appearance Clear here: r Ass for metals were collected unfiltered: m YES El NO and field acidified: ® YES El NO mg/L L Date sample analyzed: Beginningl 11022016 Laboratory Name: Prism Lab Certification No. 402 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 0 mg/L Nitrite (NO2) as N o0615 mg/L Pb - Lead olos1 ug/L Cofrform: MF Fecal 31616 0 /100mL Nitrate (NO3) as N 00620 .30 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 006135 .26 mg/L (Note'. Use MPN method for highly tumid samples) Orthophosphate 70507 mg/L Other (Specify Com jW4s and Concentration Units): )issolved Solids:Total 70300 0 mg/L Al - Aluminum o11o5 mg/L Formaldehyde, TotalW mg/L pH (Lab) 00403 5.8 units Ba - Barium 01007 ug/L 06 28!? TOC oo6so 1 mg/L Ca - Calcium 00916 mg/L 'rtp, Chloride oog4o 2.1 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 6.1 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 0 ug/L Lab Report Attached? X Yes (1) ❑ No (0) Specific Conductance 00095 30 µMhos K - Potassium 00937 mg/L VOC 78732: , method # 826013 Total Ammonia 00610 0 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NHs as N: Ammonia Nitrogen, TOM]) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal Debbie Tadlock, Mill Manager X( /011 j -// 1" Perm GW Authorized Agent) Name and Title -Please print or type Signature of Permittee (orAWhonzed Agent) (Oat) i GW -55 9 Rev. 2!2010 Elkin SUBMIT FORM ON YELLOW PAPER ONLY TER QUALITY MONITORING: E REPORT FORM I T IIYr'VRMM i tur, - r ^^�� Name: Weyerhaeuser NR Company JAN 0 V^ CU Name (if different): Address: 524 Pride Way NC 28621 County Surry act Person: Dennis Atkinson Telephone#: 336-526-6437 Location/Site Name: 36 Deg 15.112N / 80 Deg 47.447W No. of wells to be sampled: 9 LID NUMBER (from Permit): MW 12 Depth: 50 ft. i to Water Level 82546:46.1 ft. below measuring point luring Point is 1.7 ft. above land surface ne of water pumped/bailed before sampling: 1.8 PARTMENT OF ENVIRONMENT& NATURAL RESOURCES ISION OF WATER QUALITY4NFORMATION PROCESSING UNIT 7 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 133-322 RMIT Number: W00005555 Expiration Date: 4/30/2019 n -Discharge UIC 'DES Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery K Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: Date sample collected: 11/02/2016 FIELD ANALYSES: WAS Well Diameter: 2 in. pH 00400. 7.04 units Temp. 000lo: 16.6 BC DRY at Screened interval: ft. to ft. Spec. Cond. 000.94: 66.9 µMhos time of — samplin Relative M.P. Elevation: ft. Odor 00085: none check gallons YES ❑ NO de sample analyzed: Beginning 11102/16 Laboratory Name: Prism Lab 1RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 0 mg/L Nitrite (NO2) as N Do615 mg/L Coliform: MF Fecal 31616 0 /100ml- Nitrate (NO3) as N 00620 2 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P Do665 23. mg/L (Note: Use MPN method for hlglAy turbid samples) Orthophosphate 70507 mg/L solved Solids:Total 703oo 60 mg/L Al - Aluminum 01105 mg/L PH (Lab) 00403 5.6 units Ba - Barium 01007 ug/L TOC oo6so 1.5 mg/L Ca - Calcium 00916 mg/L Chloride ogg4D 2.9 mg/L Cd - Cadmium o1o27 ug/L Arsenic 01002 ug/L Chromium: Total 01034 9.6 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L Phenol 32730 ug/L Fe - Iron 01045 ug/L Sulfate 00945 mg/L Hg - Mercury 71900 0 ug/L ecific Conductance 00095 51 µMhos K - Potassium 00937 mg/L Total Ammonia 00610 0 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; 1,11-13as N: Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L TKN as N 00625 mg/L Ni - Nickel 01967 ug/L For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Appearance Pb - Lead 01051 Zn - Zinc 01092 Clear Certification No. 402 ug/L mg/L Other (Specify Compounds and Concentration Units): Formaldehyde, Total 0 mg/L ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? 0 Yes (1) ❑ No (0) VOC 78732: , method # 8260B method # method # method # Effluent Total VOCs: mg/1- VOC Removal GW -59 Rev. 2/2010 PRISM __.tea LABOIIAIpilE4 alG Weyerhaeuser Corporation Dennis Atkinson 524 Pride Way Elkin, NC 28621 NC Certification No. 402 Full -Service Analytical 8 NC Drinking Water Cert No. 37735 Environmental Solutions SC Certification No. 99012 Project: Groundwater 2016 Lab Submittal Date: 11/02/2016 Prism Work Order: 6110040 Case Narrative 11/18/2016 This data package contains the analytical results for the project identified above and includes a Case Narrative, Sample Results and Chain of Custody. Unless otherwise noted, all samples were received in acceptable condition and processed according to the referenced methods. Data qualifiers are flagged individually on each sample. A key reference for the data qualifiers appears at the end of this case narrative. Narrative Notes: Water Levels (Feet): MW -5 40.50 MWA1 19.10 MW -12 46.10 MW -10 24.90 MW -4 50.90 MW -6 47.00 MW -9 56.10 MW -7 57.60 (DRY) MW -8 55.30 (DRY) Samples for Formaldehyde and TOC were subcontracted to NC -certified laboratory, GCAL. Please call if you have any questions relating to this analytical report. Respectfully, PRISM LABORATORIES, INC. Cara C. Rusmisell Project Manager Reviewed By Cara C. Rusmisell Project Manager This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Spdngbrook Road - P.O. Box 240643 - charlotte, NC 26224-0643 Phone: 704/6294364 -Toll Free Number. 1400/629.6364- Fax: 70415264409 Page 1 of62 Data Qualifiers Key Reference: A Filtered in the lab. HT Sample received and analyzed outside of the hold time. BRL Below Reporting Limit MDL Method Detection Limit RPD Relative Percent Difference * Results reported to the reporting limit. All other results are reported to the MDL with values between MDL and reporting limit indicated with a J. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 704/525-0409 Page 2 of 62 X71 V I I Fnn-se,wee Analytical a Envkonmantxlaotic umuiwf we Sample Receipt Summary 11/18/2016 Prism Work Order: 6110040 Client Sample ID Lab Sample ID Matrix Date Sampled Date Received MW -5 6110040-01 Water 11/02/16 11/02/16 MW -11 6110040-02 Water 11/02/16 11/02/16 MW -12 6110040-03 Water 11/02/16 11/02/16 MW -10 6110040-04 Water 11/02/16 11/02/16 MW -4 6110040-05 Water 11/02/16 11/02/16 MW -6 6110040-06 Water 11/02/16 11/02/16 MW -9 6110040-07 Water 11/02/16 11/02/16 Samples were received in good condition at 2.0 degrees C unless otherwise noted. This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Sprinabrook Road - P.O. Box 240643 - Charlotte, NC 26224-0617 Phone. 704/6294764 - Toll Free Number. 1400/6294764 - Fax: 704/6264409 Page 3 of 62 I Funn-6aMeMaua Environmenn tal Solution. &F".. Weyerhaeuser Corporation Project: Groundwater 2016 Attn: Dennis Atkinson 524 Pride Way Elkin, NC 28621 Field Data Laboratory Report 11/18/2016 Prism Work Order: 6110040 Laboratory ID Client ID Field Parameter Result 6110040-01 MW -5 pH Temperature (C) Conductivity (umho) 6110040-02 MW -11 5.39 16.40 53.80 pH 6.31 Temperature (C) 17.70 Conductivity (umho) 39.00 6110040-03 MW -12 6.80 pH 7.04 Temperature (C) 16.60 Conductivity (umho) 66.9 6110040-04 MW -10 pH 6.70 Temperature (C) 18.20 Conductivity (umho) 35.80 6110040-05 MW -4 pH 6.80 Temperature (C) 18.10 Conductivity (umho) 45.80 6110040-06 MW -6 pH 6.02 Temperature (C) 18.80 Conductivity (umho) 33.6 6110040-07 MW -9 pH 5.54 Temperature (C) 21.3 Conductivity (umho) 52.9 This report should not be reproduced, except in its entirety, vnthout the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 26224-0643 Phone:7041629-6364- Toll Free Number: l -0001629.6364 -Fax: 7041525-0409 Page 4 of 62 /{�P R I S M I Fult-Service Analytical 6 -� Environmental Solutions .. ,..on..aw. Weyerhaeuser Corporation Attn: Dennis Atkinson 524 Pride Way Elkin, NC 28621 Project: Groundwater 2016 Sample Matrix: Water Laboratory Report 11/18/2016 Client Sample ID: MW -5 Prism Sample ID: 6110040-01 Prism Work Order: 6110040 Time Collected: 11/02/16 10:30 Time Submitted: 11102/16 14:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Anions by Ion Chromatography 92% 43-140 2-Flwrobiphenyl 89% 44-119 2-Fluorophenol 51% 19-119 Nirobenzened5 Chloride 1.0 man. 1.0 0.060 1 '9066A 111311612:69 EGC PSK0122 Nitrate as N BRL mg/L 0.10 0.014 1 -9056A 11/3/16 12:59 EGC P61<0122 Nitrite as N BRL mg/L 0.10 0.021 1 -9056A 11/3/16 12:59 EGC P6K0122 Sulfate BRL mg/L 1.0 0.26 1 '9056A 11/3/16 12:59 EGC P61<0122 General Chemistry Parameters 0.27 mall. 0.10 0.010 1 '60208 11/10/16 19:18 gmart P61(0190 Chemical Oxygen Demand BRL mall. 50 14 1 -SM5220 D 11/3/16 12:30 BMS PSK0085 Oil & Grease (HEM) BRL mg/L 5.0 1.0 1 '1664B 11/11/16 8:59 TJy P61<0277 Orthophosphate as P BRLA mg/L 0.050 0.014 1 -SM4500-P E 11/3/16 10:10 BMS P6K0078 pH 6.0 HT pH Units 1.0 0.020 i -SM4500-H B 11/2116 16:07 EGC PSK0067 Phosphorus -Total 0.24 mgn. 0.060 0.0090 1 -SM4600-P E 1114/16 9:46 CLB P61(0080 Specific conductance BRL umhos/cm 10 1.0 1 'SM2510B 11/3/16 14:00 BMS P61<0089 Total Dissolved Solids BRL mg/L 50 1.4 1 'SM2540 C 11!7/16 13:30 SLS P61<0159 Total Kjeldahl Nitrogen BRL mg/L 0.50 0.13 1 '351.2 11/10/16 8:36 CDE P61<0112 Ammonia as N BRL mg/L 0.10 0.034 1 'SM4500-NH3 G 11/14/16 12:20 CUB P61<0265 Microbiological Parameters Fecal Coliforms BRL CFU/100 ml 2 1 'SM9222 D 112/16 15:15 BMS P61<0094 Serllivolatile Organic Compounds by GC/MS Phenol BRL ug/L 10 0.98 1 '8270D 11/8/16 11:29 JMV P61<0133 Surrogate Recovery Control Limits 2,4,6-Tdbromophenol 92% 43-140 2-Flwrobiphenyl 89% 44-119 2-Fluorophenol 51% 19-119 Nirobenzened5 84% 44-120 Phenol -d5 33% 1152 Terphenyl-d14 89% 50-134 Total Metals Aluminum 8.1 me& 0.060 0.00093 1 '60208 11/10/16 19:18 gmart P6K0190 Mercury BRL ug/L 0.20 0.030 1 -7470A 11/9/16 13:27 JAB PBK0194 Arsenic BRL ug/L 1.0 0.29 1 '60208 11/10/16 19:18 gmart P6K0190 Barium 70 ug/L 6.0 0.041 1 '60208 11/10/16 19:18 gmart P6K0190 Cadmium BRL ug/L 1.0 0.019 1 '6020B 11/10/16 19:18 gmart P61<0190 Calcium 0.27 mall. 0.10 0.010 1 '60208 11/10/16 19:18 gmart P61(0190 Chromium 13 ug/L 1.0 0.51 1 '60208 1111011619:18 gmart P600190 Copper 0.031 mall. 0.0060 0.00044 1 '6020B 11/1011619:18 gmart P61<0190 Iron 17000 ugA. 100 16 1 '60208 11/1011619:16 gmart P61(0190 Lead 13 ug/L 1.0 0.020 1 '60206 1111011619:18 gmart P6K0190 Magnesium 0.94 mg/L 0.10 0.00025 1 '60208 11/1011619:18 gmart P6K0190 Manganese 370 ug/L 5.0 1.2 1 '6020B 11110MG 19:18 gmart PBK0190 Nickel 4.8 ug8. 2.0 0.063 1 '60208 11110/16 19:18 gmart PSK0190 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Bos 240643 - Charlotte, NC 28224-0643 Phone: 7041629-6364 - Tog Free Number. 12001529-0364 - Fax: 7041626-0409 1 Page 5 of 62 R I S M I rmi-6.n le. Maly u. Emironmantal Soruebna WnmlpmaK Laboratory Report 11/18/2016 Weyerhaeuser Corporation Project: Groundwater 2016 Client Sample ID: MW -5 Attn: Dennis Atkinson 0.0045 Prism Sample ID: 6110040-01 524 Pride Way 11110/1619:18 Prism Work Order: 6110040 Elkin, NC 28621 Sample Matrix: Water Time Collected: 11/02/16 10:30 mg/L 0.010 Time Submitted: 11/02/16 14:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Balch gmart Limit Factor Daterrime ID Potassium 1.5 mg1L 0.10 0.0045 1 '60208 11110/1619:18 gmart PGK0190 Zinc 0.043 mg/L 0.010 0.00098 1 '60208 1111011619:18 gmart PSK0190 Volatile Organic Compounds by GC/MS 11,11 -Tetrachloroethane BRL ug/L 0.50 0.11 1 '8260B 11/12/16 6:47 KOM P6K0292 1,1,1 -Trichloroethane BRL ug/L 0.50 0.061 1 '8260B 11/12/16 6:47 KDM P6K0292 1,1,2,2 -Tetrachloroethane BRL ug/L 0.50 0.036 1 '82608 11/12/16 6:47 KDM P6KO292 11,2 -Trichloroethane BRL ug/L 0.50 0.066 1 '82808 11/12/16 647 KDM P6KO292 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 '8260B 11/12/16 6:47 KDM P6K0292 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 '82608 11/12/16 6:47 KDM P6K0292 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 '82608 11/12/16 6:47 KDM P61(0292 1,2,3-Tdchlorobenzens BRL ug/L 2.0 0.40 1 '8260B 11/12/16 6:47 KDM P6K0292 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 '8260B 11/12/16 6:47 KDM P6KO292 1,2,4-Trichkxobenzene BRL ug/L 1.0 0.13 1 '82608 11/12/16 647 KDM P6KO292 1,2,4-Trimethylbenzene BRL ug/L 0.50 0.054 1 '8260B 11/12/16 647 KDM P6K0292 1,2-Dibromo-3-chbropropane BRL ug/L 2.0 0.17 1 '8260B 11/12/16 6:47 KDM P6KO292 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 '82608 11/12/16 6:47 KDM P61<0292 1,2 -Dichlorobenzene BRL ug/L 0.50 0.076 1 '82608 11/12/16 6:47 KDM P61(0292 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 '82608 11/12/16 6:47 KDM P61(0292 12-Dichloropropane BRL ug/L 0.50 0.11 1 '8260B 11/12/16 6:47 KDM PGK0292 1,3,5-Trimethylbemene BRL ug/L 0.50 0.076 1 '82608 11/12/16 6:47 KDM P6K0292 1,3 -Dichlorobenzene BRL ug/L 0.50 0.054 1 '82608 11/12/16 6:47 KDM PSK0292 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 '82608 11/12/16 6:47 KDM P6K0292 1,4 -Dichlorobenzene BRL ug/L 0.50 0.050 1 '82608 11/12/16 6:47 KDM P61(0292 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 '8260B 11/12/16 6:47 KDM P6K0292 2-Chlorotoluene BRL ug/L 0.50 0.066 1 '82606 11/12/16 6:47 KDM PSK0292 4-Chloretoluene BRL ug/L 0.50 0.050 1 '82608 11/12/16 6:47 KDM P6K0292 4-Isopropykoluene BRL ug/L 0.50 0.089 1 '82608 11/12/16 6:47 KOM P6K0292 Acetone BRL ug/L 5.0 0.31 1 '8260B 11/12/16 647 KDM P6K0292 Acmlein BRL ug/L 20 0.20 1 '82608 11/12/16 647 KDM P6K0292 Acrylombile BRL ug/L 20 0.20 1 '82608 11/12/16 6:47 KDM P6K0292 Benzene BRL ug/L 0.50 0.048 1 '82608 11/12/16 647 KDM P61(0292 Bromobenzeoe BRL ug/L 0.50 0.057 1 '8260B 11/12/16 6:47 KDM PSK0292 Bromochloromethane BRL ug/L 0.50 0.14 1 '8260B 11/12/16 6:47 KDM P61(0292 Bromodichioromethane BRL ug/L 0.50 0.062 1 '82608 11/12/16 6:47 KDM P6K0292 Bromoform BRL ug/L 1.0 0.040 1 '8260B 11/12/16 6:47 KDM P6KO292 Bromomethane BRL ug/L 1.0 0.18 1 '82608 11/12/16 6:47 KDM P61<0292 Carbon disulfide BRL ug/L 5.0 0.075 1 '8260B 11/12/16 6:47 KDM P61(0292 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 '82606 11/12/16 647 KDM POK0292 Chlorobenzene BRL ug/L 0.50 0.062 1 '82608 11/12/16 6:47 KDM P6K0292 Chloroethane BRL ug/L 0.50 0.22 1 '8260B 11/12/16 6:47 KDM P6K0292 Chloroform 2.2 ug/L 0.60 0.076 1 '82608 11112/16 6:47 KDM P61(0292 This report should not be reproduced, except in los entirety, without the written consent of Prism Laboratories, Inc. 449 6pringbrook Road - P.O. Box 240643 - Charlotte, NC 26224-0643 Phone: 70416298364 -Toll Free Number. 1400162%364 -Fax: 7041626-0409 Page 6 Of 62 r SSMFull Laboratory Report a nosniua E.Ironmontal Solutions 11/18/2016 vuau+aerx,xc Weyerhaeuser Corporation Project: Groundwater 2016 Client Sample ID: MW -5 Attn: Dennis Atkinson Prism Sample ID: 6110040-01 524 Pride Way Prism Work Order: 6110040 Elkin, NC 28621 Sample Matrix: Water Time Collected: 11/02/16 10:30 Time Submitted: 11/02/16 14:30 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Daterrime Batch ID Chloromethane BRL ug/L 0.50 0.079 1 '82608 11/12/16 6:47 KOM PSK0292 da1,2-Dichloroathylene BRL ug/L 0.50 0.056 1 '8260B 11/12/16 647 KDM PSK0292 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 '82608 11/12/16 6:47 KDM P61(0292 Dibromochloromethane BRL ug/L 0.50 0.081 1 '82608 11/12/16 6:47 KDM P6K0292 Dibromomethane BRL ug/L 0.50 0.065 1 '8260B 11/12/16 6:47 KDM P61(0292 Dichlorodifluoromethane BRL ug/L 1,0 0.11 1 '8260B 11/12/16 6:47 KDM P61(0292 Ethylbenzene BRL ug/L 0.50 0.061 1 '8260B 11/12/16 6:47 KDM PSK0292 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 '82608 11/12/16 6:47 KDM PBK0292 Isopropyl Ether BRL ug/L 0.50 0.050 1 -8260B 11/12/16 6:47 KDM PSK0292 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 '82608 11/12/16 6:47 KDM P6K0292 m.p-xylenes BRL ug/L 1.0 0.12 1 '82608 11/12/16 6:47 KDM P61(0292 Memyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 '82608 11/12/16 6:47 KDM P61(0292 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 -8260B 11/12/16 6:47 KDM P6K0292 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 '82608 11/12/16 6:47 KDM P61(0292 Methylene Chloride BRL ug/L 1.0 0.083 1 '8260B 11/12/16 6:47 KDM P61(0292 Methyi-tort-Butyl Ether BRL ug/L 0.50 0.042 1 '82608 11/12/16 6:47 KDM P61(0292 Naphthalene BRL ug/L 1.0 0.19 1 '82608 11/12/16 6:47 KDM P61<0292 n-Butylberizene BRL ug/L 1.0 0.076 1 '82608 11/12/16 6:47 KDM PSK0292 n-Propylbertzene BRL ug/L 0.50 0.087 1 '82608 11/12/16 6:47 KDM PBK0292 o -Xylene BRL ug/L 0.50 0.044 1 '8260B 11/12/16 647 KDM PSK0292 seaButylbenzene BRL ug/L 0.50 0.076 1 '82606 11/12/16 647 KDM PSK0292 Styrone BRL ug/L 0.50 0.047 1 '82608 11/12/16 647 KDM P61<0292 tert-Butylbenzene BRL ug/L 0.50 0.088 1 '8260B 11/12/16 6:47 KDM P61(0292 Tebachloroethylene BRL ug/L 0.50 0.098 1 '82608 11/12/16 6:47 KDM P6K0292 Toluene BRL ug/L 0.50 0.044 1 '82608 11/12/16 6:47 KDM PSK0292 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 '8260B 11/12/16 6:47 KDM PSK0292 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 '82606 11/12/16 6:47 KDM PBK0292 TritlMoroethytene BRL ug/L 0.50 0.078 1 '82608 11/12/16 6.47 KDM PSK0292 Tnchlorotluoromethane BRL ug/L 0.50 0.062 1 -82608 11/12/16 647 KDM P61<0292 Vinyl acetate BRL ug/L 2.0 0.060 1 '82608 11/12/16 6:47 KDM P61(0292 Vinyl chloride BRL ug/L 0.50 0.097 1 '82608 11/12/16 6:47 KDM P61(0292 Surrogate Recovery Control Urnits 4-Bromolluorobenzene 91% 64124 Dibromofluoromethane 101 % 75129 Toluene -de 97% 77-123 This report should not be reproduced, except In its entinety, without the written consort of Prism Laboratories, Inc. 449 6pringbrook Road - P.O. Box 240643 - Charlotte, NC 262244643 Phone: 704/629 -63" -Toll Free Number. 1.600/629-6364- Fax: 704162641409 Page 7 Df 62 ISM I v ironmental eo ui i Entons Laboratory Report 11/18/2016 Weyerhaeuser Corporation Project: Groundwater 2016 'SM9222 D 11/2/16 15:15 Client Sample ID: MW -11 Semivolatile Organic Compounds by GCIMS 44-119 Attn: Dennis Atkinson 42% Phenol BRL ug/L 10 0.98 1 '8270D 11/8/16 11:52 Prism Sample ID: 6110040-02 Phenol -05 Surrogate 524 Pride Way Control Limits 82% 50-134 Arsenic Prism Work Order: 6110040 ug/L 1.0 Elkin, NC 28621 Sample Matrix: Water '60208 11/10/16 19:29 gmart Time Collected: 11/02/16 11:00 Barium 87 uglL 6.0 0.041 1 '6020B Time Submitted: 11/02/16 14:30 POK0190 Cadmium Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch P61(0190 Calcium 1.8 Limit 0.10 Factor Date/rime 1 ID Anions by Ion Chromatography PGK0190 Chromium 6.1 ug/L 1.0 0.61 1 Chloride 2.1 mg/L 1.0 0.060 1 '9066A 1113116 13:16 EGC P6KO122 Nitrate as N 0.30 mg/L 0.10 0.014 1 '9056A 1113116 13:16 EGC P6K0122 Nitrite as BRL mg/L 0.10 0.021 1 '9056A 11/3/16 13:15 EGC PBK0122 Sulfate BRL mg/L 1.0 0.26 1 '9056A 11/3/16 13:15 EGC P6K0122 General Chemistry Parameters 0.10 0.00026 1 '6020B 11110/16 19:29 gmart PGK0190 Manganese Chemical Oxygen Demand BRL mg/L 50 14 1 'SM5220 D 11/3/16 12:30 BMS P61<0085 Oil 8 Grease (HEM) BRL mg/L 5.0 1.0 1 '16648 11/11/16 9:32 TJY PSK0277 Orthophosphate as P BRLA mg/L 0.050 0.014 1 'SM4500-P E 11/3/16 10:10 BMS P61<0078 pH 6.8 HT pH Units 1 'SM4500-H B 11/2/16 16:07 EGC PSK0067 Phosphorus -Total 0.26 mglL 0.060 0.0090 1 'SM4600-P E 1114116 9:46 CLS P6KOOSO Specific conductance 30 umhos/cm 10 1.0 1 'SM2510 B 11/3116 14:00 BMS PGK0089 Total Dissolved Solids BRL mg/L 50 1.4 1 'SM2540 C 11/7/16 13:30 SLS P61<0159 Total Keldahl Nitrogen BRL mg/L 0.50 0.13 1 '351.2 11/10/16 8:38 CDE P61<0144 Ammonia as BRL mg/L 0.10 0.034 1 'SM4500-NH3G 11/14/16 12:20 CLB P6K0265 Microbiological Parameters Fecal Coliforms BRL CFU/100 ml 2 1 'SM9222 D 11/2/16 15:15 BMS P6KO094 Semivolatile Organic Compounds by GCIMS 44-119 2-Fluorophenol 42% Phenol BRL ug/L 10 0.98 1 '8270D 11/8/16 11:52 JMV P6KO133 Phenol -05 Surrogate Recovery Control Limits 2,4,6-Tnbromophenol 84% 43-140 2-Fluorobiphenyl 80% 44-119 2-Fluorophenol 42% 19-119 Nitrobenzene -d5 89% 44-120 Phenol -05 28% 11-52 Terphenykdi4 82% 50-134 Total Metals Aluminum 3.9 mg/L 0.060 0.00093 1 '60208 11/10/16 19:29 gmart P6K0190 Mercury BRL ug/L 0.20 0.030 1 7470A 11/9/16 13:38 JAB PSK0194 Arsenic BRL ug/L 1.0 0.29 1 '60208 11/10/16 19:29 gmart P61<0190 Barium 87 uglL 6.0 0.041 1 '6020B 1111011619:29 gmart POK0190 Cadmium BRL ug/L 1.0 0.019 1 '60208 11/10/16 19:29 gmart P61(0190 Calcium 1.8 mg/L 0.10 0.010 1 '6020B 1111011619:29 gmart PGK0190 Chromium 6.1 ug/L 1.0 0.61 1 '6020B 1IM0116 19:29 gmart P6K0190 Copper 0.0095 mg/L 0.0060 0.00044 1 '60206 1111011619:29 gmart P6K0190 Iron 6000 uglL 100 16 1 '60208 11/10116 19:29 gmart PSK0190 Lead 2.3 ug/L 1.0 0.020 1 '60208 11/10/16 19:29 gmart PGK0190 Magnesium 2.8 mg/L 0.10 0.00026 1 '6020B 11110/16 19:29 gmart PGK0190 Manganese 140 uglL 6.0 1.2 1 '6020B 1111011619:29 gmart FSK0190 Nickel 2.3 ug/L 2.0 0.063 1 '60208 1111011619:29 gmart P61(0190 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 704/629-6364 - Toll Free Number: I-BOWS29-6364 - Fax: 7041626-0409 Page 8 of 62 /PFRISM I ErtAro oa myt F..H.S. mAnalelai Solutionsdo s nona �nnoa� c Laboratory Report 11/10,2016 Weyerhaeuser Corporation Project: Groundwater 2016 Client Sample ID: MW -11 Attn: Dennis Atkinson Prism Sample ID: 6110040-02 524 Pride Way Prism Work Order: 6110040 Elkin, NC 28621 Sample Matrix: Water Time Collected: 11/02/16 11:00 Time Submitted: 11/02/1614:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Potaselum 3.6 mglL 0.10 0.0045 1 '6020B 1111011619:29 gmart PBK0190 Zinc 0.022 mg/L 0.010 0.00098 1 '60208 11/1011619:29 gmart PBK0190 Volatile Organic Compounds by GCIMS 1,1,1,2 -Tetrachloroethane BRL ug/L 0.50 0.11 1 '82608 11/12/16 712 KDM PSK0292 1,1,1 -Trichloroethane BRL ug/L 0.50 0.061 1 '82608 11/12/16 712 KDM PSK0292 1,1,2,2 -Tetrachloroethane BRL ug/L 0.50 0.036 1 '82608 11/12/16 7:12 KDM P61<0292 11,2 -Trichloroethane BRL ug/L 0.50 0.066 1 '8260B 11/12/16 7:12 KDM P6K0292 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 '8260B 11/12/16 7:12 KDM P6K0292 1,1-Dichlomethylene BRL ug/L 0.50 0.083 1 '8260B 11/12/16 7:12 KDM P6K0292 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 '82608 11/12/16 7:12 KDM P6K0292 1,2,3-Trichbrobenzene BRL ug/L 2.0 0.40 1 '82608 11/12/16 7:12 KDM P61<0292 1,2,3-Tdchloropropane BRL ug/L 1.0 0.14 1 '82600 11/12/16 7:12 KDM P6K0292 1,2,4-Trichlorobemene BRL ug/L 1.0 0.13 1 '82608 11/12/16 7:12 KDM P61(0292 1,2,4-Trimethylbenzene BRL ug/L 0.50 0.054 1 '8260B 11/12/16 712 KDM P6K0292 1,2-0Ibromo-3-chloropropane BRL ug/L 2.0 0.17 1 '82608 11/12/16 7:12 KDM P61<0292 1,2-0ibronnoethane BRL ug/L 0.50 0.051 1 '82608 11/12/16 7:12 KDM P6K0292 1,2 -Dichlorobenzene BRL ug/L 0.50 0.076 1 '82608 11/12/16 712 KDM P61<0292 1,2-Dichlomethane BRL ug/L 0.50 0.066 1 '8260B 11/12/16 712 KDM PBK0292 1,2-Dichloropropene BRL ug/L 0.50 0.11 1 '82608 11/12/16 7:12 KDM PSK0292 1,3,5-Trimethylbenzene BRL ug/L 0.50 0.076 1 '8260B 11/12/16 7:12 KDM P81(0292 1,3 -Dichlorobenzene BRL ug/L 0.50 0.054 1 '82608 11/12/16 7:12 KDM PSK0292 1,3-0ichloropropane BRL ug/L 0.50 0.043 1 '8260B 11/12/16 7:12 KDM P6K0292 14 -Dichlorobenzene BRL ug/L 0.50 0.050 1 '826013 11/12/16 7:12 KDM PBK0292 2,2-Dichlompropane BRL ug/L 2.0 0.11 1 `82600 11/12/16 7:12 KDM P6K0292 2-Chlorololuene BRL ug/L 0.50 0.066 1 '8260B 11/12/16 7:12 KDM P61<0292 4-Chlorotoluem BRL ug/L 0.50 0.050 1 '826013 11172/16 7:12 KDM P61<0292 44sopropyltoluene BRL ug/L 0.50 0.089 1 '82608 11112/16 7:12 KDM P6K0292 Acetone BRL ug/L 5.0 0.31 1 '82608 11/12/16 7:12 KDM PSK0292 Acrolein BRL ug/L 20 0.20 1 '82608 11/12/16 7:12 KDM PBK0292 Acrylonitrile BRL ug/L 20 0.20 1 '82608 11/12/16 712 KDM PBK0292 Benzene BRL ug/L 0.50 0.048 1 '82608 11/12/16 7:12 KDM P6K0292 Bromobemene BRL ug/L 0.50 0.057 1 '8260B 11/12/16 712 KDM P6K0292 Brorrwchloromethane BRL ug/L 0.50 0.14 1 '82608 11/12/16 7:12 KDM POK0292 Bromodichloromethane BRL ug/L 0.50 0.062 1 '82608 11/12/16 7:12 KDM P61<0292 Bromofomm BRL ug/L 1.0 0.040 1 '8260B 11/12/16 712 KDM P6K0292 Bromometharme BRL ug/L 1.0 0.18 1 '8260B 11/12/16 7:12 KDM P61<0292 Carbon disulfide BRL ug/L 5.0 0.075 1 '8260B 11/12/16 7:12 KDM PSK0292 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 '8260B 11/12/16 7:12 KDM PSK0292 Chlorobenzene BRL ug/L 0.50 0.062 1 '82808 11/12/16 7:12 KDM PBK0292 Chloroethane BRL ug/L 0.50 0.22 1 '82608 11/12/16 7:12 KDM PSK0292 Chloroform BRL ug/L 0.50 0.076 1 '82608 11/12/16 7:12 KDM PSK0292 This report should not be reproduced, except in its entirely, without the written consent of Priam Laboratories, Inc. 449 6pringbrook Road - P.O. Box 240647 - Charlene, NC 262244M Phone: 70416294364 -Toll Free Number. 1-1001629-6364- Fel: 70//626-0409 Page 9 62 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 26224.0643 Phone: 701/629 -6364 -Toll Fran Number.1200/629-6364- Fax: 704/6254409 Page 100f 62 Laboratory Report ISMFull-Sarviw MaytlW a Environmental solutions 11/1812016 ueowvwuec Weyerhaeuser Corporation Project: Groundwater 2016 Client Sample ID: MW -11 Attn: Dennis Atkinson Prism Sample ID: 6110040-02 524 Pride Way Prism Work Order. 6110040 Elkin, NC 28621 Sample Matrix: Water Time Collected: 11/02/16 11:00 Time Submitted: 11/02/16 14:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/time 10 Chloromethane BRL ug/L 0.50 0.079 1 '8260B 11/12/16 7:12 KOM PGK0292 cis-1,2-1)ichloroethylane BRL ug/L 0.50 0.056 1 '82608 11/12/16 7:12 KOM P6K0292 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 '82608 11/12/16 7:12 KOM P61<0292 Dibromochloromethane BRL ug/L 0.50 0.081 1 '82608 11/12/16 712 KOM P6K0292 Dibromomethane BRL ug/L 0.50 0.065 1 '82608 11/12/16 7:12 KOM PSK0292 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 '82608 11/12/16 712 KOM P6K0292 Ethylbenzene BRL uglL 0.50 0.061 1 '82608 11/12/16 7:12 KOM P61<0292 Hexechlorobutadiene BRL ug/L 2.0 0.16 1 '82608 11/12/16 7:12 KOM PSK0292 Isopropyl Ether BRL ug/L 0.50 0.050 1 '82608 11/12/16 7:12 KOM P6K0292 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 '82608 11/12/16 7:12 KOM PSK0292 m,p-Xylenes BRL ug/L 1.0 0.12 1 '8260B 11/12/16 7:12 KOM P61<0292 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 '82606 11/12/16 7:12 KOM PSK0292 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 '8260B 11/12/16 7:12 KOM P61(0292 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 '8260B 11/12/16 7:12 KOM P61<0292 Methylene Chloride BRL ug/L 1.0 0.083 1 '8260B 11/12/16 7:12 KOM P6K0292 Methyl-lert-Butyl Ether BRL ug/L 0.50 0.042 1 '8260B 11/12/16 7:12 KOM P6K0292 Naphthalene BRL ug/L 1.0 0.19 1 '82608 11/12/16 7:12 KOM P61<0292 n-Butylbenzene BRL ug/L 1.0 0.076 1 '8260B 11/12/16 712 KOM P6K0292 n-Propylbenzene BRL ug/L 0.50 0.087 1 '82608 11/12/16 712 KOM P61<0292 c -Xylene BRL ug/L 0.50 0.044 1 '8260B 11/12/16 7:12 KOM P61(0292 s Butylbenzene BRL ug/L 0.50 0.076 1 '8260B 11/12/16 7:12 KOM P61<0292 Styrene BRL ug/L 0.50 0.047 1 '82608 11/12/16 7:12 KOM PSK0292 tert-Butylbenzene BRL ug/L 0.50 0.088 1 '82608 11/12/16 7:12 KOM P61<0292 Tetrechlorcethylene BRL ug/L 0.50 0.098 1 '82608 11/12/16 7:12 KOM P6K0292 Toluene BRL ug/L 0.50 0.044 1 '82608 11/12/16 7:12 KOM P61<0292 trans-11,2-Dichloroethylene BRL ug/L 0.50 0.094 1 '82609 11/12/16 7:12 KOM P6K0292 trans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 '82608 11/12/16 712 KOM P6K0292 Trichloroethylene BRL ug/L 0.50 0.078 1 '8260B 11/12/16 712 KOM P61(0292 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 '82608 11/12/16 7:12 KOM PSK0292 Vinyl acetate BRL ug/L 2.0 0.060 1 '82608 11/12/16 7:12 KOM P61<0292 Vinyl chloride BRL ug/L 0.50 0.097 1 '8260B 11/12/16 7:12 KOM P61(0292 Surrogate Recovery Control Limits 4-Bromofluorobenzene 92 % 80-124 Dibromoeuoromethane 98 % 75-129 Toluene -de 100% 77-123 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 26224.0643 Phone: 701/629 -6364 -Toll Fran Number.1200/629-6364- Fax: 704/6254409 Page 100f 62 R I S M I fullueS.M.. Analytical 6 Ell nmmxntal Solutions t4MNMtl41NC Weyerhaeuser Corporation Attn: Dennis Atkinson 524 Pride Way Elkin, NC 28621 Project: Groundwater 2016 Sample Matrix: Water Laboratory Report 11/18/2016 Client Sample ID: MW -12 Prism Sample ID: 6110040-03 Prism Work Order: 6110040 Time Collected: 11/02/16 11:15 Time Submitted: 11/02/16 14:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Anions by ton Chromatography 86% 4&140 2-Fluorobiphenyl 79% 44-119 2-Fluorophenol 49% 19-119 Nitrobenzene -d5 Chloride 2.9 mg/L 1.0 0.060 1 '9066A 111111613:31 EGC PSK0122 Nitrate as N 2.0 mg/L 0.10 0.014 4 '9056A 1113116 13:31 EGC PSK0122 Ndrde as N BRL mg/L 0.10 0.021 1 '9056A 11/3/16 13:31 EGC P61(0122 Sulfate BRL mg/L 1.0 0.26 1 '9056A 11/3/16 13:31 EGC PSK0122 General Chemistry Parameters 4.6 mg/L 0.10 0.010 1 '6020B 11/1011619:33 gmart P61<0190 Chemical Oxygen Demand BRL mg/L 50 14 1 'SM5220 D 11/3/16 12:30 BMS P6KO085 Oil b Grease (HEM) BRL mg/L 5.0 1.0 1 '16648 11/11/16 9:32 TJY P6KO277 Orthophosphate as P BRLA mg/L 0.050 0.014 1 'SM4500-P E 11/3/16 10:10 BMS P61<0078 PH 6.6 HT pH Units 1.0 0.020 1 -SM45004t B 1112116 16:07 EGC P61(0067 Phosphorus -Total 0.23 mg1L 0.050 0.0090 1 -SM4600-P E 1114116 9:46 CLB PGKOOSO Specific conductance 61 umhoslcm 10 1.0 1 'SM26108 111311614:00 BMS PSK0089 Total Dissolved Solids 60 mg/L 50 1.4 1 'SM2640 C 1117/16 14:52 SLS P6K0159 Total K4eldahl Nitrogen BRL mg/L 0.50 0.13 1 '351.2 11/10/16 8:38 COE P61<0144 Ammonia as N BRL mg/L 0.10 0.034 1 'SM4500-NH3 G 11/14/16 12:20 CLB P6K0265 Microbiological Parameters Fecal Coliforms BRL CFU/100 ml 2 1 'SM9222 D 11/2/16 15:15 BMS P6KO094 Semivolatile Organic Compounds by GC/MS Phenol BRL ug/L 10 0.98 1 '8270D 11/8/16 12:15 JMV P61<0133 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 86% 4&140 2-Fluorobiphenyl 79% 44-119 2-Fluorophenol 49% 19-119 Nitrobenzene -d5 72% 44-120 Phenol -d5 32% 11-52 Terphenyl-d14 84% 50-134 Total Metals Aluminum 7.3 mg/L 0.060 0.00093 1 '60208 1111011619:33 gmart P6KO190 Mercury BRL ug/L 0.20 0.030 1 '7470A 11/9/16 1342 JAB PSK0194 Arsenic BRL ug/L 1.0 0.29 1 '6020B 11/10/16 19:33 gmart P61<0190 Barium 130 ug/L 6.0 0.041 1 '60208 11110/16 19:33 gmart P6KO190 Cadmium BRL ug/L 1.0 0.019 1 '60208 11/10/16 19:33 limen P61<0190 Calcium 4.6 mg/L 0.10 0.010 1 '6020B 11/1011619:33 gmart P61<0190 Chromium 9.6 ugll. 1.0 0.61 1 '60208 1111011619:33 gmart P6K0190 Copper 0.011 mg/L 0.0060 0.00044 1 '60208 1111011619:33 gmart PBK0190 Iron 10000 ug/L 100 16 1 '602013 1111011619:33 gmart P61(0190 Lead 6A ug& 1.0 0.020 1 '60208 1111011619:33 gmart POK0190 Magnesium 6.2 mg/L 0.10 0.00025 1 '60206 1111011619:33 gman P6100190 Manganese 250 uglL 6.0 1.2 1 '60208 1111011619:13 gmart P61(0190 Nickel 4.9 ug/L 2.0 0.063 1 '60208 11/10/16 19:33 gmart P6KO190 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 4,19 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0543 Phone: 7041529.8364 -Tall Free Number../ -8001529.6364 -Fax: 7041525-0409 Page 11 of 62 Potassium Report Full-Sarvlce Analytical a SSMLaboratory 0.10 Environmental Solutions uo�mwu oc 11/18/2016 Weyerhaeuser Corporation Project: Groundwater 2016 Client Sample ID: MW -12 Attn: Dennis Atkinson Prism Sample ID: 6110040-03 524 Pride Way Prism Work Order: 6110040 Elkin, INC 28621 Sample Matrix: Water Time Collected: 11/02/16 11:15 0.00098 Time Submitted: 11/02/16 14:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daterrime ID Potassium 3.6 mg/l- 0.10 0.0046 1 '60208 1111011619:33 gmart PSK0190 Zinc 0.036 mg/L 0.010 0.00098 1 •60206 11/10/16 19:33 smart PSK0190 Volatile Organic Compounds by GCIMS 1,1,1,2 -Tetrachloroethane BRL ug/L 0.50 0.11 1 '82608 11/12/16 7:38 KDM P61<0292 1,1,1 -Trichloroethane BRL ug/L 0.50 0.061 1 '82608 11/12/16 7:38 KDM P61<0292 1,1,2,2 -Tetrachloroethane BRL ug/L 0.50 0.036 1 '82608 11/12/16 7:38 KDM P61(0292 11,2 -Trichloroethane BRL ug/L 0.50 0.066 1 '82608 11/12/16 738 KDM P6K0292 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 '8260B 11/12/16 738 KDM P61<0292 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 '82606 11/12/18 7:38 KDM P61<0292 1,1-Dichioropropylene BRL ug/L 0.50 0.051 1 '8260B 11/12/16 738 KDM P61<0292 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 '82608 11/12/16 7:38 KDM P6K0292 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 '8260B 11/12/16 7:38 KDM P61(0292 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 '8260B 11/12/16 738 KDM P61<0292 1,2,4-Trimethylbenzene BRL ug/L 0.50 0.054 1 '82608 11/12/16 738 KDM P61<0292 1,2-Dibroml-3-chloropropane BRL ug/L 2.0 0.17 1 '8260B 11/12/16 738 KDM P61<0292 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 '82606 11/12/16 7:38 KDM P61<0292 1,2 -Dichlorobenzene BRL ug/L 0.50 0.076 1 '82606 11/12/16 738 KDM P61<0292 1.2-Dichloroethane BRL ug/L 0.50 0.066 1 '8260B 11/12/16 7:38 KDM P61<0292 1,2-Dichlampropane BRL ug/L 0.50 0.11 1 '8260B 11/12/16 738 KDM P61<0292 1,3,5-Trimalhylbenzene BRL ug/L 0.50 0.076 1 '82608 11/12/16 7:38 KDM P61<0292 1,21 -Dichlorobenzene BRL ug/L 0.50 0.054 1 '8260B 11/12/16 7:38 KDM P61(0292 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 '8260B 11/12/16 7:38 KDM PSK0292 1,4-11ichlorobenzene BRL ug/L 0.50 0.050 1 '82608 11/12/16 7:38 KDM P61<0292 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 '8260B 11/12/16 738 KDM P6K0292 2-Chlorotoluene BRL ug/L 0.50 0.066 1 '82608 11/12/16 738 KDM P61<0292 4-Chlorotoluene BRL ug/L 0.50 0.050 1 '8260B 11/12/16 7:38 KDM P61(0292 4-Isopropyttoluene BRL ug/L 0.50 0.089 1 '82608 11/12/16 7:38 KDM P61<0292 Acetone BRL ug/L 5.0 0.31 1 '82608 11/12/16 7:38 KDM POK0292 Acrolem BRL ug/L 20 0.20 1 '82608 11/12/16 7:38 KDM PSK0292 AcryloniMle BRL ug/L 20 0.20 1 '8260B 11/12/16 7:38 KDM P61<0292 Benzene BRL ug/L 0.50 0.048 1 '82608 11/12/16 7:38 KDM P61<0292 Bronmbenzene BRL ug/L 0.50 0.057 1 '8260B 11/12/16 738 KDM P61<0292 Bromochlommethane BRL ug/L 0.50 0.14 1 '82608 11/12/16 738 KDM PSK0292 Bromodichloromethane BRL ug/L 0.50 0.062 1 '8260B 11/12/16 7:38 KDM P61(0292 Bromoform BRL ug/L 1.0 0.040 1 '82608 11/12/16 738 KDM P61(0292 Bromomethane BRL ug/L 1.0 0.18 1 '82608 11/12/16 7:38 KDM PSK0292 Carbon disulfide BRL ug/L 5.0 0.075 1 '82608 11/12/16 7:38 KDM P6K0292 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 '8260B 11/12/16 7:38 KDM P61<0292 Chlorobenzene BRL ug/L 0.50 0.062 1 '8260B 11/12/16 7:38 KDM P61(0292 Chloroethane BRL ug/L 0.50 0.22 1 '82608 11/12/16 7:38 KDM PBK0292 Chloroform BRL ug/L 0.50 0.076 1 '8260B 11/12/16 736 KDM P61(0292 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224-0643 Phone: 704/529-6364- Toll Frac Number. l -000/629 -6364 -Fax: 704/626409 Page 1-2 -of 62 PRISM I Funninics Analy6Cal EAronmnt nvieal SOIWIone 4eaumerR ac Weyerhaeuser Corporation Attn: Dennis Atkinson 524 Pride Way Elkin, NC 28621 Project: Groundwater 2016 Sample Matrix: Water Laboratory Report 11/18/2016 Client Sample ID: MW -10 Prism Sample ID: 6110040-04 Prism Work Order: 6110040 Time Collected: 11/02/16 11:30 Time Submitted: 11/02/16 14:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daternme ID Anions by Ion Chromatography 69% 43-140 2-Fluorobiphenyl 67% 44-119 2-Fluorophenol 39% 19-119 Nitrobenzen"5 Chloride 2.6 mg/L 1.0 0.060 1 '9066A 111311613:47 EGC P6K0122 Nitrate as N 1.2 mg/L 0.10 0.014 1 '9066A 1113/16 13:47 EGC P61(0122 Nitrite as N BRL mg/L 0.10 0.021 1 '9056A 11/3/16 13:47 EGC P61<0122 SuBate BRL mg/L 1.0 0.26 1 '9056A 11/3/16 13:47 EGC P61<0122 General Chemistry Parameters 2.0 mg/L 0.10 0.010 1 '6020B 1111011619:36 gmart P6K0190 Chemical Oxygen Demand 69 mg/L 60 14 1 'SM6220 D 11/3116 12:30 BMS P6"086 Oil & Grease (HEM) BRL mg/L 5.0 1.0 1 '16646 11/11/16 9:32 TJY P61<0277 Orthophosphate es P BRLA mg/L 0.050 0.014 1 'SM4500-P E 11/3/16 10:10 BMS P6K0078 pH 6.4 HT pH Units 1.0 0.020 1 'SM460041 B 11/2116 16:07 EGC P6K0067 Phosphon s -Total 0.66 mglL 0.060 0.0090 1 -SM4600-P E 1114116 9:45 CLB P6K0080 Specific conductance 28 umhos/cm 10 1.0 1 'SM26110 B 11/3/16 14:00 BMS P6K0089 Total Dissolved Solids BRL mg/L 50 1.4 1 'SM2540 C 1177/16 14:52 SLS P61<0159 Total Neldahl Nitrogen BRL mg/L 0.50 0.13 1 '351.2 11/10/16 8:38 CDE P61<0144 Ammonia as N BRL mg/L 0.10 0.034 1 'SM4500.NH3 G 11/14/16 12:20 CLS PBK0265 Microbiological Parameters Fecal Coliforms BRL CFU/100 ml 2 1 'SM9222 D 11/2/16 15:15 BMS PSK0094 Semivolatile Organic Compounds by GC/MS Phenol BRL ug/L 10 0.98 1 '8270D 11/8/16 12:38 JMV PSK0133 Surrogate Recovery Control Limits 2,4,6-Tribri nophenol 69% 43-140 2-Fluorobiphenyl 67% 44-119 2-Fluorophenol 39% 19-119 Nitrobenzen"5 59% 44-120 Phenol -d5 25% 11-52 Terphenyl-d14 71% 50-134 Total Metals Aluminum 9.1 mg/L 0.060 0.00093 1 •60206 11110116 19:36 gmart P6100190 Mercury BRL ug/L 0.20 0.030 1 '7470A 11/9/16 13:46 JAB P6K0194 Arsenic BRL ug/L 1.0 0.29 1 '60208 11/10/16 19:36 gmart PSK0190 Barium 160 uglL 5.0 0.041 1 '6020B 1111011619:36 gmart PBK0190 Cadmium BRL ug/L 1.0 0.019 1 '6020B 11/10/16 19:36 gmart P61<0190 Calcium 2.0 mg/L 0.10 0.010 1 '6020B 1111011619:36 gmart P6K0190 Chromium 12 ug/L 1.0 0.51 1 '6020B 1111011619:36 smart PBK0190 Copper 0.020 mg/L 0.0060 0.00044 1 '60208 11/1011619:36 smart P8K0190 Iron 21000 ug/L 100 16 1 '60208 11110116 19:16 gmart PSK0190 Lead 10 ug/L 1.0 0.020 1 '60206 11110M619:36 gmart P6K0190 Magnesium 1.9 11111911. 0.10 0.00026 1 '60206 1111011619:36 gmart P6100190 Manganese 440 ug/L 5.0 1.2 1 '60208 1111011619:36 gmart P6K0190 Nickel 14 ug/L 2.0 0.053 1 '6020B 11/10/1619:16 gmart P6K0190 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springhrock Road - P.O. Box 240643 - Charlotte, KC 28224-0543 Phone: 704/6298364- Toll Free Number. 1200/629 -0364 -Fax: 7041526-0409 1 Page 14 of 62 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Chadofb, NC 26224.0643 Phone: 70W629-6364 - Tall Free Number: 1-000/629-6364 - Fax: 704f626-0409 J Page 13 of 62 Laboratory Report Full-Sarvles Ms1y11W a SSM Environmental Solutions urwiaeu ec 11/18/2016 Weyerhaeuser Corporation Project: Groundwater 2016 Client Sample ID: MW -12 Attn: Dennis Atkinson Prism Sample ID: 6110040-03 524 Pride Way Prism Work Order: 6110040 Elkin, NC 28621 Sample Matrix: Water Time Collected: 11/02/16 11:15 Time Submitted: 11/02/16 14:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daternme ID Chloromethane BRL ug/L 0.50 0.079 1 '82608 11/12/16 7:38 KOM P6K0292 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 •82608 11/12/16 7:38 KOM P61<0292 ds-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 '82608 11/12/16 738 KOM P6K0292 Dibromoohloromethane BRL ug/L 0.50 0.081 1 '8260B 11/12/16 738 KOM P6K0292 Dibromomethane BRL ug/L 0.50 0.065 1 '82608 11/12/16 738 KOM P61<0292 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 '82608 11/12/16 7:38 KOM P6K0292 Ethylbenzene BRL ug/L 0.50 0.061 1 '82608 11/12116 7:38 KOM P6K0292 Hexachlorobutediene BRL ug/L 2.0 0.16 1 '82608 11/12/16 7:38 KOM P6K0292 Isopropyl Ether BRL ug/L 0.50 0.050 1 '8260B 11/12/16 7:38 KOM P6K0292 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 '82608 11/12/16 7:38 KOM P61<0292 m,p-Xylenes BRL ug/L 1.0 0.12 1 '82608 11/12/16 7:38 KOM P61<0292 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 '82606 11/12/16 7:38 KOM P6K0292 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 '82608 11/12/16 7:38 KOM P6K0292 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 '82608 11/12/16 7:38 KOM P61<0292 Methylene Chloride BRL ug/L 1.0 0.083 1 '8260B 11/12/16 7:38 KOM P61<0292 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 '82608 11/12/16 7:38 KOM P61<0292 Naphthalene BRL ug/L 1.0 0.19 1 -82606 11/12/16 738 KOM P61<0292 n-Butylbenzene BRL ug/L 1.0 0.076 1 '82608 11/12/16 7:38 KOM P61<0292 n-Propylbenzene BRL ug/L 0.50 0.087 1 '82608 11/12/16 7:38 KOM P61<0292 o -Xylene BRL ug/L 0.50 0.044 1 '82608 11/12/16 7:38 KOM PSK0292 s Butylbenzene BRL ug/L 0.50 0.076 1 '82608 11/12/16 7:38 KOM P61<0292 Styrene BRL ug/L 0.50 0.047 1 '82608 11/12/16 738 KOM P61<0292 tart-Butylbenzene BRL ug/L 0.50 0.088 1 '8260B 11/12/16 7:38 KOM P6K0292 Tetrachloroethylene BRL ug/L 0.50 0.098 1 '82608 11/12/16 738 KOM P6K0292 Toluene BRL ug/L 0.50 0.044 1 '82608 11/12/16 7:38 KOM P61<0292 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 '8260B 11/12/16 7:38 KOM P6K0292 trans-1,3Dichloropropylene BRL ug/L 0.50 0.070 1 '82608 11/12/16 7:38 KOM P6K0292 Trichloroethylene BRL ug/L 0.50 0.078 1 '82606 11/12/16 7:38 KOM P61<0292 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 '82608 11/12/16 738 KOM P61<0292 Vinyl acetate BRL ug/L 2.0 0.060 1 '82608 11/12/16 7:38 KOM P61<0292 Vinyl chloride BRL ug/L 0.50 0.097 1 '8260B 11/12/16 7:38 KOM P6K0292 Surrogate Recovery Control Limits 4-Bromofluorobenzene 92% 80-124 Dibromofluoromethane 99% 75-129 Toluene -de 104% 77-123 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Chadofb, NC 26224.0643 Phone: 70W629-6364 - Tall Free Number: 1-000/629-6364 - Fax: 704f626-0409 J Page 13 of 62 ZP r�IAIli-Seric* MN ludo s �r'�_ M EnWnanmental Solutions umunfeq Mc Weyerhaeuser Corporation Attn: Dennis Atkinson 524 Pride Way Elkin, NC 28621 Project: Groundwater 2016 Sample Matrix: Water Laboratory Report 11/16/2016 Client Sample ID: MW -10 Prism Sample ID: 6110040-04 Prism Work Order: 6110040 Time Collected: 11/02/1611:30 Time Submitted: 11/02/16 14:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Potassium 2.4 mglL 0.10 0.0046 1 '60208 11/1011619:36 gmart P6K0190 Zinc 0.093 mg/L 0.010 0.00098 1 '602013 1111011619:36 gman PGK0190 Volatile Organic Compounds by OCIMS 1,1,1,2 -Tetrachloroethane BRL ug/L 0.50 0.11 1 '8260B 11/12/16 8:04 KOM P6K0292 1,11 -Trichloroethane BRL ug/L 0.50 0.061 1 '82608 11/12/16 804 KDM P6K0292 1,1,2,2 -Tetrachloroethane BRL ug/L 0.50 0.036 1 '82606 11/12/16 804 KDM P61<0292 1,1,2 -Trichloroethane BRL ug/L 0.50 0.066 1 -82608 11/12/16 804 KDM P6K0292 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 '82608 11/12/16 804 KDM P6K0292 1,1-Dichioroethylene BRL ug/L 0.50 0.083 1 '82608 11/12/16 8:04 KDM P61<0292 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 '826013 11/12/16 804 KDM P6K0292 12,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 '826013 11/12/16 804 KDM PSK0292 1,2,3-Trichloropmpane BRL ug/L 1.0 0.14 1 '82608 11/12/16 8:04 KDM P61(0292 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 '82606 11/12/16 804 KDM POK0292 1,2,4-Trimethylbenzene BRL ug/L 0.50 0.054 1 '82608 11/12/16 8:04 KOM POK0292 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 '82608 11/12/16 6:04 KDM P61<0292 12-Dibromoethane BRL ug/L 0.50 0.051 1 '8260B 11/12/16 804 KDM PSK0292 12 -Dichlorobenzene BRL ug/L 0.50 0.076 1 '82608 11/12/16 804 KDM P6K0292 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 '82608 11/12/16 8:04 KDM P61<0292 1,2-Dichlompmpane BRL ug/L 0.50 0.11 1 '82600 11/12/16 8:04 KDM P61<0292 1,3,5-Trimethylbenzene BRL ug/L 0.50 0.076 1 '8260B 11/12/16 8:04 KOM P6K0292 1,3-Dichlombenzene BRL ug/L 0.50 0.054 1 '82608 11/12/16 804 KDM PSK0292 1,3-0ichlompropane BRL ug/L 0.50 0.043 1 '826013 11/12/16 804 KDM P61(0292 1,4 -Dichlorobenzene BRL ug/L 0.50 0.050 1 '82606 11/12/16 8:04 KDM PSK0292 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 '82608 11/12/16 804 KDM P61(0292 2-Chlorotoluene BRL ug/L 0.50 0.066 1 '82608 11/12/16 8:04 KDM POK0292 4-Chlorotoluene BRL ug/L 0.50 0.050 1 '82608 11/12/16 8:04 KDM P6K0292 4-Isopropy8eluene BRL ug/L 0.50 0.089 1 '82608 11/12/16 8:04 KDM P61(0292 Acetone BRL ug/L 5.0 0.31 1 -82608 11/12/16 8:04 KDM POK0292 Arxolein BRL ug/L 20 0.20 1 -82608 11/12/16 8:04 KDM POK0292 Acrylonitrile BRL ug/L 20 0.20 1 '82608 11/12/16 804 KDM POK0292 Benzene BRL ug/L 0.50 0.048 1 '82608 11/12/16 8:04 KDM P6K0292 Bromcbenzene BRL ug/L 0.50 0.057 1 '8260B 11/12/16 804 KDM POK0292 Bromochloromethene BRL ug/L 0.50 0.14 1 '82606 11/12/16 8:04 KDM P61<0292 Bromodlollloromethane BRL ug/L 0.50 0.062 1 '82608 11/12/16 8:04 KDM P61<0292 Bromoroml BRL ug/L 1.0 0.040 1 '8260B 11/12/16 804 KDM POK0292 Bromomethane BRL ug/L 1.0 0.18 1 '82608 11112/16 8:04 KDM P81<0292 Carbon disulfide BRL ug/L 5.0 0.075 1 '826013 11/12/16 8:04 KDM P61<0292 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 '826013 11/12/16 804 KDM P6K0292 Chlorobenzene BRL ug/L 0.50 0.062 1 '826013 11/12/16 804 KDM P6K0292 Chloroethane BRL ug/L 0.50 0.22 1 '82608 11/12/16 8:04 KDM POK0292 Chloroform BRL ug/L 0.50 0.076 1 '82608 11/12/16 8:04 KDM P6K0292 This report should not be reproduced, except in hs entirety, without the written consent of Prism Laboratories, Inc. 449 Bprirlgbrook Road - P.O. Box 240643 - Chadolb, NC 28224-0643 Phone: 704/6294364- Toll Free Number. l -00016294364 -Fax: 7041626.0409 Page 15 of 62 RISM Laboratory Report Fun -serve. sl Solutions a EmlronmenW 9orutlone 11118/2016 uen,eeera uc Weyerhaeuser Corporation Project: Groundwater 2016 Client Sample ID: MW -10 Attn: Dennis Atkinson Prism Sample ID: 6110040-04 524 Pride Way Prism Work Order: 6110040 Elkin, NC 28621 Sample Matrix: Water Time Collected: 11/02/16 11:30 Time Submitted: 11/02/16 14:30 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst DateTm , Batch ID Chloromethane BRL ug/L 0.50 0.079 1 '82608 11/12/16 8:04 KDM P6K0292 cis-1,2-1)ichloroethylene BRL ug/L 0.50 0.056 1 '82608 11/12/16 804 KDM P61<0292 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 '82608 11/12/16 8:04 KDM PSK0292 Dibromochloromethane BRL ug/L 0.50 0.081 1 '82608 11/12/16 804 KDM P6K0292 Dibromomethane BRL ug/L 0.50 0.065 1 '8260B 11/12/16 8:04 KDM P61<0292 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 '8260B 11/12/16 804 KDM P61(0292 Ethylbemene BRL ug/L 0.50 0.061 1 '82608 11/12/16 8:04 KDM P61<0292 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 '82608 11/12/16 804 KDM P6K0292 Isopropyl Ether BRL ug/L 0.50 0.050 1 '8260B 11/12/16 804 KDM P6K0292 Isopropylbenzene (Cumene) BRL ug/L 0.50 0.054 1 '82606 11/12/16 804 KDM P6K0292 m,p-Xylenes BRL ug/L 1.0 0.12 1 '82608 11/12/16 804 KDM P6K0292 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 '82608 11/12/16 8:04 KDM P6K0292 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 '82608 11/12/16 8:04 KDM P61<0292 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 '82608 11/12/16 8:04 KDM P61(0292 Methylene Chloride BRL ug/L 1.0 0.083 1 '82608 11/12/16 8:04 KDM P6K0292 Methyl-tert-Butyl Ether BRL ug/L 0.50 0.042 1 '82608 11/12/16 804 KDM P6K0292 Naphthalene BRL ug/L 1.0 0.19 1 '82608 11/12/16 8:04 KDM P6K0292 n-Buylbenzene BRL ug/L 1.0 0.076 1 '82608 11/12/16 804 KDM P6K0292 n-Propylbenzene BRL ug/L 0.50 0.087 1 '82608 11/12/16 804 KDM P6K0292 o -Xylene BRL ug/L 0.50 0.044 1 '82608 11/12/16 8:04 KDM P61<0292 sec-Butylbenzene BRL ug/L 0.50 0.076 1 '8260B 11/12/16 804 KDM P6K0292 Styrene BRL ug/L 0.50 0.047 1 '82608 11/12/16 8:04 KDM P6K0292 tert-Buylbenzene BRL ug/L 0.50 0.088 1 '82608 11/12/16 8:04 KDM P6K0292 Tetrachloroethylene BRL ug/L 0.50 0.098 1 '82608 11/12/16 8:04 KDM P6K0292 Toluene BRL ug/L 0.50 0.044 1 '8260B 11/12/16 804 KDM P61<0292 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 '82608 11/12/16 8:04 KDM PSK0292 bans-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 '82608 11/12/16 8:04 KDM PSK0292 Trichloroethylene BRL ug/L 0.50 0.078 1 '82608 11/12/16 804 KDM PBK0292 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 '82608 11/12/16 804 KDM PSK0292 Vinyl acetate BRL ug/L 2.0 0.060 1 '82608 11/12/16 8:04 KDM P61<0292 Vinyl chlonde BRL ug/L 0.50 0.097 1 '82608 11/12/16 804 KDM P61<0292 Surrogate Recovery Control Limits 4-Bromofluorobenzene 98 % 80-124 Dibromofluoromethane 99% 75729 Toluene -de 92% 77-123 This report should not be reproduced, except in its entirety, vathout the written consent of Prism Laboratories, Inc. 449 8prirlgbrook Road - P.O. Box 240643 - Charlotte, NC 29214-0843 Phone: 704/5294394 -Toll Free NumMr.12001629-63"-Fax: 7041526409 Page 16 0f 62 Fun4 Anelyt ARISM I Erwimninental solutions - 'ueosacwu „c Weyerhaeuser Corporation Attn: Dennis Atkinson 524 Pride Way Elkin, NC 28621 Project: Groundwater 2016 Sample Matrix: Water Laboratory Report 11/18/2016 Client Sample ID: MW -4 Prism Sample ID: 6110040-05 Prism Work Order: 6110040 Time Collected: 11/02/16 12:00 Time Submitted: 11/02/16 14:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Anions by Ion Chromatography 80% 43140 2-Flucrobiphenyl 75% 44-119 2-Fluorophenol 40% 19-119 Nitroben2en"5 Chloride 1.1 mg/L 1.0 0.060 1 '9056A 11/311614:02 EGC P6K0122 Nitrate as N 0.61 mall. 0.10 0.014 1 '9066A 1113116 14:02 EGC P6K0122 Nitrite as BRL mg/L 0.10 0.021 1 '9056A 11/3/1614:02 EGC P61(0122 Sulfate BRL mg/L 1.0 0.26 1 '9056A 11/3/16 14:02 EGC P6K0122 General Chemistry Parameters 3.6 mg/L 0.10 0.010 1 '602013 11/16M6 18:43 bgm P6K0190 Chemical Oxygen Demand BRL mg/L 50 14 1 'SM5220 D 1113116 12:30 BMS PSK0085 Oil 8 Grease (HEM) BRL mg/L 5.0 1.0 1 -16646 11/11/16 10:07 TJV PSK0277 Orthophosphate as P BRLA mg/L 0.050 0.014 1 'SM4500-P E 11/3/16 10.10 BMS P6K0078 pN 6.8 KT pH Unita 1.0 0.020 1 'SM460041 B 11/2116 16:07 EGC P61(0067 Phosphorus -Total 0.14 mg/L 0.060 0.0090 1 'SM4600-P E 11/4116 9:45 CLS P6K0080 Specific conductance 41 umhos/cm 10 1.0 1 'SM2510 B 11/3116 14:00 BMS P6K0089 Total Dissolved Solids BRL mg/L 50 1.4 1 'SM2540 C 11/7/16 14:52 SLS P6K0159 Total Keldahl Nitrogen BRL mg/L 0.50 0.13 1 '351.2 11/10/16 8:38 CDE P6K0144 Ammonia as N BRL mg/L 0.10 0.034 1 'SM4500-NH3 G 11/14/16 12:20 CLB P6K0265 Microbiological Parameters Fecal Coliforms BRL CFU/100 ml 2 1 'SM9222 D 11/2/16 15:15 BMS P6K0094 Semivolatile Organic Compounds by GC/MS Phenol BRL ug/L 10 0.98 1 '8270D 11/8/16 13:01 JMV P61<0133 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 80% 43140 2-Flucrobiphenyl 75% 44-119 2-Fluorophenol 40% 19-119 Nitroben2en"5 63% 44-120 PhenoW5 26% 11-52 TerphenyF<114 75% 54134 Total Metals Aluminum 8.6 mg/L 0.060 0.00093 1 '60208 11/15/1618:43 barn P6K0190 Mercury BRL ug/L 0.20 0.030 1 '7470A 11/9/16 13:49 JAB P6K0194 Arsenic BRL ug/L 1.0 0.29 1 '6020B 11/15/16 18:43 bgm PSK0190 Badum 97 uglL 5.0 0.041 1 '602013 1111611618:43 bgm PGK0190 Cadmium BRL ug/L 1.0 0.019 1 '6020B 11/15/16 18:43 bgm P6K0190 Calcium 3.6 mg/L 0.10 0.010 1 '602013 11/16M6 18:43 bgm P6K0190 Chromium 40 ug1L 1.0 0.51 1 '60208 11/1511618:43 bgm P6K0190 Copper 0.010 mg/L 0.0050 0.00044 1 '60208 1111611618:43 ham Ps"190 Iron 12000 ugJL 100 16 1 '60208 11/1611618:43 ham FSK0190 Lead 4.1 ug1L 1.0 0.020 1 '60208 1111611618:41 bgm PBK0190 Magnesium 8.2 mall. 0.10 0.00026 1 '60208 1111611616:43 bgm P6K0190 Manganese 220 ug1L 5.0 1.2 1 '6020B 1111611618:41 ham P6K0190 Nickel 16 ug/L 2.0 0.061 1 '60208 11115/1618:43 ham PSK0190 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Spdngl rook Road - P.O. Boa 240643 - Charlotte, NC 28224.0643 Phone: 70415294364- Toll Free Number: 14100/6294394 -Fax: 7041526-0409 Page 17 of 62 Laboratory Report Fall-aamlaa Analytical a Environmental Solatlona 11118/2016 aaonaaw•aac Weyerhaeuser Corporation Project: Groundwater 2016 Client Sample ID: MW -4 Attn: Dennis Atkinson Prism Sample ID: 6110040-05 524 Pride Way Prism Work Order: 6110040 Elkin, NC 28621 Sample Matrix: Water Time Collected: 11/02/16 12:00 Time Submitted: 11/02/16 14:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DatelTime ID Potassium 4.2 mg/L 0.10 0.0045 1 '60206 11/16116 18:43 bgm PGK0190 Zinc 0.043 mg/L 0.010 0.00098 1 '60206 11/16116 18:43 bgm P6K0190 Volatile Organic Compounds by GCIMS 1,1,1,2-Tetrachloroathene BRL ug/L 0.50 0.11 1 '82608 11/12/16 8:30 KDM P61(0292 1,1,1 -Trichloroethane BRL ug/L 0.50 0.061 1 '8260B 11/12/16 8:30 KDM P61<0292 1,1,2,2-Tebachloroethane BRL ug/L 0.50 0.036 1 '8260B 11/12/16 8:30 KDM P61<0292 1,1,2 -Trichloroethane BRL ug/L 0.50 0.066 1 '8260B 11/12/16 8:30 KDM PSK0292 1,1-Dichlormthane BRL ug/L 0.50 0.083 1 '82608 11/12/16 830 KDM P61<0292 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 '82608 11/12/16 8:30 KDM P61(0292 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 '826013 11/12/16 8:30 KDM PSK0292 1,2,3-Trichlorobenzene BRL ug/L 2.0 0.40 1 '82608 11/12/16 830 KDM P61<0292 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 '82608 11/12/16 830 KDM P61(0292 1,2,4-Trichlorobemene BRL ug/L 1.0 0.13 1 '82608 11/12/16 830 KDM P6K0292 1,2,4-Trimethylbomene BRL ug/L 0.50 0.054 1 '8260B 11/12/16 830 KDM P61<0292 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 '8260B 11/12/16 8:30 KDM P61<0292 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 '8260B 11/12/16 8:30 KDM PBK0292 1,2 -Dichlorobenzene BRL ug/L 0.50 0.076 1 '8260B 11/12/16 8:30 KDM P61(0292 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 '8260B 11/12/16 830 KDM PSK0292 1,2-Dichloropropane BRL ug/L 0.50 0.11 1 '8260B 11/12/16 830 KDM P6K0292 1,3,5-Trimethylbenzene BRL ug/L 0.50 0.076 1 '8260B 11/12/16 8.30 KDM P61<0292 1,3 -Dichlorobenzene BRL ug/L 0.50 0.054 1 '8260B 11/12/16 830 KDM P6K0292 1,3-Dichloropropam BRL ug/L 0.50 0.043 1 '82608 11/12/16 830 KDM P61(0292 1,4 -Dichlorobenzene BRL ug/L 0.50 0.050 1 '82608 11/12/16 8:30 KDM P61<0292 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 '8260B 11/12/16 830 KDM P61<0292 2-Chloromluene BRL ug/L 0.50 0.066 1 '8260B 11/12/16 830 KDM P61<0292 4-Chlorotoluene BRL ug/L 0.50 0.050 1 '82608 11/12/16 8:30 KDM PSK0292 4-Isopropyholuene BRL ug/L 0.50 0.089 1 '8260B 11/12/16 8:30 KDM PSK0292 Acetone BRL ug/L 5.0 0.31 1 '8260B 11/12/16 8:30 KDM PSK0292 Acrolein BRL ug/L 20 0.20 1 '82608 11/12/16 830 KDM P61<0292 Acrylonitnle BRL ug/L 20 0.20 1 '82608 11/12/16 8:30 KDM PGK0292 Benzene BRL ug/L 0.50 0.048 1 '82608 11/12/16 6:30 KDM P61<0292 Bromobenzene BRL ug/L 0.50 0.057 1 '82608 11/12/16 830 KDM P6K0292 Bromochloromethane BRL ug/L 0.50 0.14 1 '82608 11/12/16 8:30 KDM P61<0292 Bromodichloromethane BRL ug/L 0.50 0.062 1 '8260B 11/12/16 8:30 KDM P61<0292 Bromoform BRL ug/L 1.0 0.040 1 '8260B 11/12/16 830 KDM P6K0292 Bromomethane BRL ug/L 1.0 0.18 1 '82608 11/12/16 6:30 KDM P6K0292 Carbon disulfide BRL ug/L 5.0 0.075 1 '82608 11/12/16 8:30 KDM P61<0292 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 '82608 11/12/16 8:30 KDM P61(0292 Chlorobenzene BRL ug/L 0.50 0.062 1 '82608 11/12/16 8:30 KDM P61<0292 Chloroethane BRL ug/L 0.50 0.22 1 '82608 11/12/16 830 KDM P61<0292 Chloroform BRL ug/L 0.50 0.076 1 '82608 11/12/16 8:30 KDM P61(0292 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0643 Phone: 70W62%361-TopFreeFs Number: 1.80016291364 - Fax: 7041626-0 Page 18 of 62 409 Full-SaMce Analytical 8PRWISMIEnvionmental Solution. Weyerhaeuser Corporation Attn: Dennis Atkinson 524 Pride Way Elkin, NC 28621 Project: Groundwater 2016 Sample Matrix: Water Laboratory Report 11/18/2016 Client Sample ID: MW -6 Prism Sample ID: 6110040-06 Prism Work Order: 6110040 Time Collected: 11/02/16 12:15 Time Submitted: 11/02/16 14:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Daternme ID Anions by Ion Chromatography 70% 43-140 2-Fluorobiphenyl 70% 44-119 2-Fluorophenol 37% 19-119 Nitrobenzene -d5 Chloride BRL mg/L 1.0 0.060 1 '9056A 11/3/16 14:34 EGC P6K0122 Nitrate as N 0.61 mg/L 0.10 0.014 1 '9066A 11/3116 14:34 EGC PI K0122 Nitrite as BRL mg/L 0.10 0.021 1 '9056A 11/3/16 14:34 EGC P61<0122 Sulfate BRL mg/L 1.0 0.26 1 '9056A 11/3/16 14:34 EGC P61<0122 General Chemistry Parameters 1.6 melt 0.10 0.010 1 '60208 1111611618:47 bgm PBK0190 Chemical Oxygen Demand BRL mg/L 50 14 1 'SM5220 D 11/3/16 12:30 BMS P61<0085 Oil B Grease (HEM) BRL mg/L 5.0 1.0 1 '16648 11/11/16 10:07 TJY PSK0277 Orthophosphate as P BRLA mg/L 0.050 0.014 1 'SM4500-P E 11/3/16 10:10 BMS P61<0078 pH 6.5 HT pH Units 1.0 0.020 1 -SM4500-H B 1112116 16:07 EGC P61<0067 Phosphorus -Total 0.31 mill 0.060 0.0090 1 'SM4500-P E 11/4/16 9:45 CLB PGK0080 Specific conductance 22 umhoslcm 10 1.0 1 'SM2610 B 11/3116 14:00 BMS P6K0089 Total Dissolved Solids BRL mg/L 50 1.4 1 'SM2540 C 11/7/16 1452 SLS P61<0159 Total Neldahl Nitrogen BRL mg/L 0.50 0.13 1 '351.2 11/10/16 8:38 CDE P61<0144 Ammonia as N BRL mg/L 0.10 0.034 1 'SM4500-NH3 G 11/14/16 12:20 CLB P61<0265 Microbiological Parameters Fecal Coliforms BRL CFU/100 ml 2 1 'SM9222 D 11/2/16 15:15 BMS P61(0094 Semivolatile Organic Compounds by GCIMS Phenol BRL ug/L 10 0.98 1 '8270D 11/8/16 13:23 JMV P61<0133 Surrogate Recovery Control Limits 2,4,6-Tribromophenol 70% 43-140 2-Fluorobiphenyl 70% 44-119 2-Fluorophenol 37% 19-119 Nitrobenzene -d5 59% 44-120 Phenol-dS 24% 11-52 Terphenyl-d14 71% 50-134 Total Metals Aluminum 3.5 mill. 0.060 0.00093 1 '60208 11/1611618:47 him PBK0190 Mercury BRL ug/L 0.20 0.030 1 '7470A 11/9/16 13:53 JAB P6K0194 Arsenic BRL ug/L 1.0 0.29 1 '6020B 11/15/16 18:47 bgm PBK0190 Barium 61 ugfL 6.0 0.041 1 '60208 11116116 18:47 him P6K0190 Cadmium BRL ug/L 1.0 0.019 1 '60208 11/15/16 18:47 bgm P61<0190 Calcium 1.6 melt 0.10 0.010 1 '60208 1111611618:47 bgm PBK0190 Chromium 6.0 ug/L 1.0 0.61 1 '602013 11115/1618:47 bgm P6K0190 Copper 0.0085 mg/L 0.0050 0.00044 1 '6020B 1111611618:47 bgm PIK0190 Iron 6800 uglL 100 1s 1 '6020B 11/16116 18:47 bgm PBK0190 Lead 3.1 ug1L 1.0 0.020 1 '60206 11/1611618:47 bgm PSK0190 Magnesium 1.6 mg/L 0.10 0.00026 1 '60208 11116116 18:47 bgm PI K0190 Manganese 100 ug/L 6.0 1.2 1 '60208 1111611618:47 bgm P6140190 Nickel 6.1 ug1L 2.0 0.063 1 '6020B 11/15/1618:47 bgm PBK0190 This report should not be reproduced, except in its entirely, without the written consent of Pnsm Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 28224.0643 Phone: 704/529 -6364 -Toll Free Number. l -000/629 -6364 -Fax: 704/625-0409 1 Page 20 of 62 RISM Laboratory Report P. FuII-Sarvlu Malyllul a , Envimnmentel Solon... 11/18/2016 uuo.oane. we Weyerhaeuser Corporation Project: Groundwater 2016 Client Sample ID: MW -4 Attn: Dennis Atkinson Prism Sample ID: 6110040-05 524 Pride Way Prism Work Order: 6110040 Elkin, NC 28621 Sample Matrix: Water Time Collected: 11/02/16 12:00 Time Submitted: 11/02/16 14:30 Parameter Result Units Report Limit MDL Dilution Factor Method Anatysis Analyst Daterrime Batch ID Chloromethane BRL ug/L 0.50 0.079 1 '82608 11/12/16 830 KDM P61<0292 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 '8260B 11/12/16 830 KDM PSK0292 cis11,3-Dichloropropylene BRL ug/L 0.50 0.079 1 '8260B 11/12/16 830 KDM P61<0292 Dibromochloromethane BRL ug/L 0.50 0.081 1 '82608 11/12/16 8:30 KDM P6K0292 Dibromomethane BRL ug/L 0.50 0.065 1 '82608 11/12/16 830 KDM P61<0292 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 '82608 11/12/16 830 KDM P6K0292 Ethylbenzene BRL ug/L 0.50 0.061 1 '82608 11/12/16 830 KDM P61<0292 Hexachlorobutadiene BRL ug/L 2.0 0.16 1 '8260B 11/12/16 8:30 KDM P61<0292 Isopropyl Ether BRL ug/L 0.50 0.050 1 '82608 11/12/16 830 KDM P8K0292 Isopropylbenzene(Cumene) BRL ug/L 0.50 0.054 1 '82608 11/12/16 8:30 KDM P61<0292 m,p-Xylenes BRL ug/L 1.0 0.12 1 '82608 11/12/16 830 KDM P6K0292 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 '8260B 11/12/16 8:30 KDM P61<0292 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 '82608 11/12/16 8:30 KDM P6K0292 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 '8260B 11/12/16 830 KDM P61<0292 Methylene chloride BRL ug/L 1.0 0.083 1 '8260B 11/12/16 830 KDM P61(0292 Methyl -ten -Butyl Ether BRL ug/L 0.50 0.042 1 '82608 11/12/16 890 KDM P6K0292 Naphthalene BRL ug/L 1.0 0.19 1 '82608 11/12/16 8:30 KDM P61<0292 n-BuMbenzene BRL ug/L 1.0 0.076 1 '82608 11/12/16 8:30 KDM P61<0292 n-Propylbenzene BRL ug/L 0.50 0.087 1 '82608 11/12/16 8:30 KDM P6K0292 o -Xylene BRL ug/L 0.50 0.044 1 '82608 11/12/16 830 KDM P61<0292 seo-Butylbenzene BRL ug/L 0.50 0.076 1 '82608 11/12/16 8.30 KDM P61<0292 Styrene BRL ug/L 0.50 0.047 1 '82606 11/12/16 8.30 KDM P61<0292 tert-Butylbenzene BRL ug/L 0.50 0.088 1 '82608 11/12/16 8:30 KDM P6K0292 Tetrachloroethylene BRL ug/L 0.50 0.098 1 '82608 11/12/16 830 KDM P6K0292 Toluene BRL ug/L 0.50 0.044 1 '82606 11/12/16 830 KDM P61<0292 trans-1,2-Dichlcroethylene BRL ug/L 0.50 0.094 1 '82606 11/12/16 8:30 KDM P61<0292 bans1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 '82606 11/12/16 8:30 KDM P6K0292 Trichloroethylene BRL ug/L 0.50 0.078 1 '82608 11/12/16 8:30 KDM P6K0292 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 '82608 11/12/16 830 KDM P6K0292 Vinyl acetate BRL ug/L 2.0 0.060 1 '82608 11/12/16 830 KDM P61<0292 Vinyl chloride BRL ug/L 0.50 0.097 1 '82606 11/12/16 830 KDM P61<0292 Surrogate Recovery Control Limits 4-Bromofluorobenzene 97% 80-124 Dibromofluoromethane 100% 75-129 Toluene -d8 96 % 77-123 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratones, Inc. 449 Springbrook Road - P.O. Box 240643 - charlotte, NC 26224-0643 Phone: 704f629-0364 - Toll Free Number: 1.9001629.6364 - Fax: 704/626-0409 ZPRRISM Laboratory Report Full-Sarvlaa Mtlplwl a Envininmontal aeluMor. 11/18/2016 Weyerhaeuser Corporation Project: Groundwater 2016 Client Sample ID: MW -6 Attn: Dennis Atkinson Prism Sample ID: 6110040-06 524 Pride Way Prism Work Order: 6110040 Elkin, NC 28621 Sample Matrix: Water Time Collected: 11/02/16 12:15 Time Submitted: 11/02/16 14:30 Parameter Result Units Report Limit MDL Dilution Factor Method Analysis Analyst Date/time Batch ID Potassium 1.9 fnvL 0.10 0.0045 1 '60208 11/1511618:47 bgm P6100190 Zinc 0.023 mg/L 0.010 0.00098 1 '60208 11/1511618:47 bgm P61(0190 Volatile Organic Compounds by GCIMS 1,1,1,2 -Tetrachloroethane BRL ug/L 0.50 0.11 1 '8260B 11/12/16 8:55 KDM PBK0292 1,1,1 -Trichloroethane BRL ug/L 0.50 0.061 1 -82608 11/12/16 8:55 KDM P61<0292 11,2,2 -Tetrachloroethane BRL ug/L 0.50 0.036 1 '82608 11/12/16 855 KDM P61<0292 1,1,2 -Trichloroethane BRL ug/L 0.50 0.066 1 -82608 11/12/16 8:55 KDM P6K0292 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 -82608 11/12/16 8:55 KDM P6K0292 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 '82608 11/12/16 8:55 KDM P6K0292 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 '82608 11/12/16 8:55 KDM P6K0292 1,2,3-Trichlorobemzene BRL ug/L 2.0 0.40 1 -82608 11/12/16 8:55 KDM P61<0292 1,2,3-Trichloropropane BRL ug/L 1.0 0.14 1 '8260B 11/12/16 8:55 KDM P61(0292 1,24-Trichlorobemem BRL ug/L 1.0 0.13 1 '82608 11/12/16 8:55 KDM P61<0292 1,2,4-Trimethylbomens BRL ug/L 0.50 0.054 1 '82606 11/12/16 8:55 KDM P6K0292 1,2-Dibromc-3chlompropane BRL ug/L 2.0 0.17 1 '82608 11/12/16 855 KDM P61<0292 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 '82608 11/12/16 8:55 KDM POK0292 1,2 -Dichlorobenzene BRL ug/L 0.50 0.076 1 '82608 11/12/16 855 KDM PSK0292 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 '82608 11/12/16 8:55 KDM P6KO292 1,2-Dichlompmpane BRL ug/L 0.50 0.11 1 '82608 11112/16 855 KDM P6K0292 1,3,5-Trimethylbenzene BRL ug/L 0.50 0.076 1 '82608 11/12/16 8:55 KDM P61<0292 1,3 -Dichlorobenzene BRL ug/L 0.50 0.054 1 '82608 11/12/16 855 KDM P6K0292 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 '82608 11/12/16 8:55 KDM P6K0292 1,4 -Dichlorobenzene BRL ug/L 0.50 0.050 1 '82608 11/12/16 8:55 KDM P61<0292 2,2-Dichloropropane BRL ug/L 2.0 0.11 1 '62608 11/12/16 855 KDM P6KO292 2Chlorotoluene BRL ug/L 0.50 0.066 1 '82608 11/12/16 8:55 KDM PSK0292 4Chloratoluene BRL ug/L 0.50 0.050 1 '8260B 11/12/16 8:55 KDM P61<0292 4- Isopropyltoluene BRL ug/L 0.50 0.089 1 '82608 11/12/16 855 KDM P6K0292 Acetone BRL ug/L 5.0 0.31 1 '82606 11/12/16 855 KDM PBK0292 Acrolein BRL ug/L 20 0.20 1 -82608 11/12/16 8:55 KDM P61<0292 Acrylonitrile BRL ug/L 20 0.20 1 '82606 11/12/16 8:55 KDM P6K0292 Benzene BRL ug/L 0.50 0.048 1 -82608 11/12/16 8:55 KDM P6K0292 Bromobamene BRL ug/L 0.50 0.057 1 '82608 11/12/16 8:55 KDM P6K0292 Bromochloromethane BRL ug/L 0.50 0.14 1 '82608 11/12/16 8:55 KDM P61<0292 Bromodichloromethane BRL ug/L 0.50 0.062 1 '8260B 11/12/16 855 KDM P61<0292 Bromoform BRL ug/L 1.0 0.040 1 '82608 11/12/16 8:55 KDM P61<0292 Bromomethane BRL ug/L 1.0 0.18 1 '82608 11/12/16 8:55 KDM P61<0292 Carbon disulfide BRL ug/L 5.0 0.075 1 '82608 11/12/16 8:55 KDM PSK0292 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 '82608 11/12/18 855 KDM PSK0292 Chlorobenzeme BRL ug/L 0.50 0.062 1 '8260B 11/12/16 8:55 KDM P6K0292 Chloroethane BRL ug/L 0.50 0.22 1 '8260B 11/12/16 8:55 KDM P6K0292 Chloroform BRL ug/L 0.50 0.076 1 '82608 11/12/16 8:55 KDM P61(0292 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 6pringbrook Road - P.O. Box 240613 - Chadone, NC 282240643 Phona: 7046294364 - Toll Free Number. 1400/629-9364 - Fax: 704/626-0409 Page21 0 62 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240642 - charlotte, NC 26224-0643 Phone: 7041529 -6764 -Toll Free Number: 1.8001629 -0364 -Fee: 7041626-0409 Page 22 of 62 Report Full-8erviw Analytical t &RISMLaboratory Enol o mal 9ol�tlone 11/18/2016 Weyerhaeuser Corporation Project: Groundwater 2016 Client Sample ID: MW-6 Attn: Dennis Atkinson Prism Sample ID: 6110040-06 524 Pride Way Prism Work Order: 6110040 Elkin, NC 28621 Sample Matrix: Water Time Collected: 11/02/16 12:15 Time Submitted: 11/02/1614:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor DateTme ID Chloromethane BRL ug/L 0.50 0.079 1 '8260B 11/12/16 855 KDM PSK0292 cis-1,2-Dichloroethylene BRL ug/L 0.50 0.056 1 '82608 11/12/16 8:55 KDM PSK0292 cis-1,3-Dichloropropyiene BRL ug/L 0.50 0.079 1 '82608 11/12/16 8:55 KDM P6K0292 Dibromochloromethane BRL ug/L 0.50 0.081 1 '8260B 11/12/16 855 KDM P61(0292 Dibromomethane BRL ug/L 0.50 0.065 1 '82608 11/12/16 855 KDM P61<0292 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 '8260B 11/12/16 8:55 KDM P6K0292 Ethylbenzene BRL ug/L 0.50 0.061 1 '82608 11/12/16 8:55 KDM PBK0292 Hexachlorobutediene BRL ug/L 2.0 0.16 1 '8260B 11/12/16 855 KDM P6K0292 Isopropyl Ether BRL ug/L 0.50 0.050 1 '8260B 11/12/16 8:55 KDM P6K0292 Isopropylbenzene(Cumene) BRL ug/L 0.50 0.054 1 '82608 11/12/16 855 KDM PSK0292 m,p-Xylenes BRL ug/L 1.0 0.12 1 '82608 11/12/16 8:55 KDM P61<0292 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 '82608 11/12/16 855 KDM P6K0292 Methyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 '8260B 11/12/16 8:55 KDM P61<0292 Methyl Isobutyl Ketone BRL ug/L 5.0 0.078 1 '82606 11/12/16 8:55 KDM P61<0292 Methylene Chloride BRL ug/L 1.0 0.083 1 '82608 11/12/16 855 KDM P61<0292 Methy4tert-Butyl Ether BRL ug/L 0.50 0.042 1 '82608 11/12/16 8:55 KDM P6K0292 Naphthalene BRL ug/L 1.0 0.19 1 '82608 11/12/16 8:55 KDM P61<0292 n-Butylbenzene BRL ug/L 1.0 0.076 1 '82608 11/12/16 855 KDM P6K0292 n-Propylbenzene BRL ug/L 0.50 0.087 1 '82608 11/12/16 8:55 KDM P61<0292 o-Xylene BRL ug/L 0.50 0.044 1 '8260B 11/12/16 8:55 KDM PBK0292 sec-Buylbenzene BRL ug/L 0.50 0.076 1 '82608 11/12/16 6:55 KDM P61<0292 Styrene BRL ug/L 0.50 0.047 1 '82608 11/12/16 8:55 KDM P6K0292 tart-Buyibemene BRL ug/L 0.50 0.088 1 '82608 11/12/16 8:55 KDM P61<0292 Tetrachloroethylene BRL ug/L 0.50 0.098 1 '82608 11/12/16 8:55 KDM P61<0292 Toluene BRL ug/L 0.50 0.044 1 '8260B 11/12/16 8:55 KDM P6K0292 trans-1,2-Dichloroethylene BRL ug/L 0.50 0.094 1 `8260B 11/12/16 8:55 KDM P61<0292 bens-1,3-Dichloropropylene BRL ug/L 0.50 0.070 1 '82608 11/12/16 855 KDM P6K0292 Trichloroethylene BRL ug/L 0.50 0.078 1 '82608 11/12/16 855 KDM P6K0292 Trichlorofluoromethane BRL ug/L 0.50 0.062 1 '8260B 11/12/16 8:55 KDM P61<0292 Vinyl acetate BRL ug/L 2.0 0.060 1 '82608 11/12/16 8:55 KDM P6K0292 Vinyl chloride BRL ug/L 0.50 0.097 1 '82608 11/12/16 8:55 KDM PSK0292 Surrogate Recovery Control Limits 4-Bromofluorobenzene 89% 80-124 Dibromofluoromethane 99% 75-129 Tolusne-dtl 100% 77-123 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240642 - charlotte, NC 26224-0643 Phone: 7041529 -6764 -Toll Free Number: 1.8001629 -0364 -Fee: 7041626-0409 Page 22 of 62 Full LE R I S M IEnvironmental ANyutio s rviea AnSolutions ,.amnawea rec Weyerhaeuser Corporation Attn: Dennis Atkinson 524 Pride Way Elkin, NC 28621 Project: Groundwater 2016 Sample Matrix: Water Laboratory Report 11/18/2016 Client Sample ID: MW -9 Prism Sample ID: 6110040-07 Prism Work Order: 6110040 Time Collected: 11/02/16 13:00 Time Submitted: 11/02/16 14:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Anions by Ion Chromatography 79% 43-140 2-Fluorobiphenyl 77% 44-119 2-Fluorophenol 39% 19-119 Nitrobenzene -d5 Chloride 4.3 mglL 1.0 0.060 1 '9066A 1113/16 14:18 EGC PSK0122 Nkrate as N 0.41 mg/L 0.10 0.014 1 '9066A 1113/16 14:18 EGC P6K0122 Nitrite as BRL mg/L 0.10 0.021 1 '9056A 11/3/16 14:18 EGC PBK0122 Sulfate BRL mg/L 1.0 0.26 1 '9056A 11/3/16 14:18 EGC P61<0122 General Chemistry Parameters '60208 11/10/16 19:46 gmart P6K0190 Chromium 1.2 ug/L 1.0 0.61 1 Chemical Oxygen Demand BRL mg/L 50 14 1 'SM5220 D 11/3/16 12:30 BMS P61<0085 Oil B Grease (HEM) BRL mg/L 5.0 1.0 1 `16648 11/11/16 10:07 TJY P61<0277 Orthophosphate as P BRLA mg/L 0.050 0.014 1 'SM4500-P E 11/3/16 10:10 BMS P61<0078 PH 5.2 HT PH Units 0.10 0.00026 1 'SM4600-H B 1112116 16:07 EGC PSK0057 Phosphoms-Total 0.093 mg/L 0.050 0.0090 1 -SM4500-P E 11/4/16 9:46 CLE P6K0080 Specific conductance 32 umhos/cm 10 1.0 1 'SM2610 B 1113/16 14:00 BMS P6K0089 Total Dissolved Solids BRL mg/L 50 1.4 1 'SM2540 C 11(//16 14:52 SLS P61<0159 Total Kieldahl Nitrogen BRL mg/L 0.50 0.13 1 '351.2 11/10/16 8:38 CDE PBK0144 Ammonia as N BRL mg/L 0.10 0.034 1 'SM4500-NH3 G 11/14/16 12:20 CLB PBK0265 Microbiological Parameters Fecal Coliforms BRL CFU/100 ml 2 1 'SM9222 D 11/2/16 15:15 BMS P6K0094 Semivolatile Organic Compounds by GC/MS Phenol BRL ug/L 10 0.98 1 '8270D 11/8/16 13:46 JMV P61<0133 Surrogate Recovery Control Limits 2,4,&Tdbromophenol 79% 43-140 2-Fluorobiphenyl 77% 44-119 2-Fluorophenol 39% 19-119 Nitrobenzene -d5 60% 44-120 Phenol -d5 28% 11-52 Terphenyl-d14 79% 50-134 Total Metals Aluminum 0.41 mg/L 0.050 0.00093 1 '60208 11/1011619:46 gmart PSK0190 Mercury BRL ug/L 0.20 0.030 1 '7470A 11/9/16 13:57 JAB P61<0194 Arsenic BRL ug/L 1.0 0.29 1 '60208 11/10/16 19:46 gmart POK0190 Barium 67 ug/L 6.0 0.041 1 '6020B 11110/16 19:46 gmart PBK0190 Cadmium BRL ug/L 1.0 0.019 1 '60208 11/10/16 19:46 gmart P61<0190 Calcium 0.79 mg/L 0.10 0.010 1 '60208 11/10/16 19:46 gmart P6K0190 Chromium 1.2 ug/L 1.0 0.61 1 '6020B 11/1011619:46 gmart PSK0190 Copper BRL mg/L 0.0050 0.00044 1 '60208 11/10/16 19:46 gmart P61<0190 Iron 700 ugA. 100 16 1 '6020B 1111011619:46 gmart PS"190 Lead BRL ug/L 1.0 0.020 1 '6020B 11/10/16 19:46 gmart P6K0190 Magnesium 1.1 mg/L 0.10 0.00026 1 '6020B 11110116 19:46 gmart P6K0190 Manganese 20 ug/L 6.0 1.2 1 '60208 11/1011619:46 gmart P6K0190 Nickel BRL ug/L 2.0 0.053 1 '6020B 11/10/16 19:46 gmart P61<0190 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 - Charlotte, NC 29224-0543 Phone: 704/629.6364- Toll Free Number. 1-800/629.6364- Fax: 704/525.0409 I Page 23 of 62 Fan Analytic8RISM I Baatmnunanat Solutions >ueoMmwa c Weyerhaeuser Corporation Attn: Dennis Atkinson 524 Pride Way Elkin, NC 28621 Project: Groundwater 2016 Sample Matrix: Water Laboratory Report 11/18/2016 Client Sample ID: MW -9 Prism Sample ID: 6110040-07 Prism Work Order: 6110040 Time Collected: 11/02/16 13:00 Time Submitted: 11/02/16 14:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Datefrime ID Potassium 2.2 mg/L 0.10 0.0045 1 '60208 11/10/16 19:46 gmart PGK0190 Zinc 0.016 m9/t. 0.010 0.00098 1 '60208 11/10/16 19:46 gmart P6K0190 Volatile Organic Compounds by GC/MS 1,1,1,2 -Tetrachloroethane BRL ug/L 0.50 0.11 1 '82608 11/12/16 9:21 KOM P61<0292 1,1,1 -Trichloroethane BRL ug/L 0.50 0.061 1 '8260B 11/12/16 9:21 KOM P6K0292 1,12,2 -Tetrachloroethane BRL ug/L 0.50 0.036 1 '8260B 11/12/16 9:21 KOM P61<0292 1,12 -Trichloroethane BRL ug/L 0.50 0.066 1 '82608 11/12/16 9:21 KOM P61<0292 1,1-Dichloroethane BRL ug/L 0.50 0.083 1 '82608 11/12/16 921 KOM P6K0292 1,1-Dichloroethylene BRL ug/L 0.50 0.083 1 '82608 11/12/16 921 KOM P61<0292 1,1-Dichloropropylene BRL ug/L 0.50 0.051 1 '82608 11/12/16 921 KOM P61<0292 1,2,3-Tdchlorobenzene BRL ug/L 2.0 0.40 1 '8260B 11/12/16 9:21 KOM PSK0292 1,2,3-Trichloropmpane BRL ug/L 1.0 0.14 1 '82608 11/12/16 9:21 KOM P6K0292 1,2,4-Trichlorobenzene BRL ug/L 1.0 0.13 1 '8260B 11/12/16 9:21 KOM P61<0292 1,2,4-Thmethylbemene BRL ug/L 0.50 0.054 1 '82608 11/12/16 9:21 KOM P61<0292 1,2-Dibromo-3-chloropropane BRL ug/L 2.0 0.17 1 '8260B 11/12/16 921 KOM PSK0292 1,2-Dibromoethane BRL ug/L 0.50 0.051 1 '82608 11/12/16 921 KOM P6K0292 1,2 -Dichlorobenzene BRL ug/L 0.50 0.076 1 '8260B 11/12/16 9:21 KOM P61<0292 1,2-Dichloroethane BRL ug/L 0.50 0.066 1 '8260B 11/12/16 921 KOM P61<0292 1,2-Dichloropropans BRL ug/L 0.50 0.11 1 '8260B 11/12/16 921 KOM PSK0292 1,3,5-Thmethylbamene BRL ug/L 0.50 0.076 1 '82608 11/12/16 921 KOM P61<0292 1,3 -Dichlorobenzene BRL ug/L 0.50 0.054 1 '82608 11/12/16 921 KOM P6K0292 1,3-Dichloropropane BRL ug/L 0.50 0.043 1 '82608 11/12/16 9:21 KOM P6K0292 1,4 -Dichlorobenzene BRL ug/L 0.50 0.050 1 '82608 11/12/16 9:21 KOM P61<0292 2,2-Dichioropropane BRL ug/L 2.0 0.11 1 '8260B 11/12/16 921 KOM P61<0292 2-Chlarotoluene BRL ug/L 0.50 0.066 1 '82606 11/12/16 9:21 KOM P6K0292 4-Chlorotoluene BRL ug/L 0.50 0.050 1 '82608 11/12/16 921 KOM P61<0292 4-Isopropyholuene BRL ug/L 0.50 0.089 1 '82608 11/12/16 9:21 KOM P6K0292 Acetone BRL ug/L 5.0 0.31 1 '8260B 11/12/16 9:21 KOM P61<0292 Acrolein BRL ug/L 20 0.20 1 '82600 11/12/16 921 KOM P61<0292 Acrylonitrile BRL ug/L 20 0.20 1 '8260B 11/12/16 921 KOM P61<0292 Benzene BRL ug/L 0.50 0.048 1 '8260B 11/12/16 921 KOM P61<0292 Bromobenzene BRL ug/L 0.50 0.057 1 '8260B 11/12/16 9:21 KOM P61<0292 Bromochloromethane BRL ug/L 0.50 0.14 1 '8260B 11/12/16 921 KOM P61<0292 Bromodichloromethane BRL ug/L 0.50 0.062 1 '8260B 11/12/16 9:21 KOM P61<0292 Bromolonn BRL ug/L 1.0 0.040 1 '82608 11/12/16 9:21 KOM P61<0292 Bromimethane BRL 119/1. 1.0 0.18 1 '826013 11/12/16 9:21 KOM P6K0292 Carbon disulfide BRL ug/L 5.0 0.075 1 '8260B 11/12/16 9:21 KOM P6K0292 Carbon Tetrachloride BRL ug/L 0.50 0.11 1 '8260B 11/12/16 9:21 KOM PGK0292 Chlorobenzene BRL ug/L 0.50 0.062 1 '826013 11/12/16 921 KOM P61<0292 Chloroethane BRL ug/L 0.50 0.22 1 '82608 11/12/16 921 KOM P6K0292 Chloroform BRL ug/L 0.50 0.076 1 '82608 11/12/16 9:21 KOM P61<0292 This report should not be reproduced, except in its entirely, without the written consent of Prism Laboratories, Inc. 449 Springl rook Road - P.O. Boz 240643 - Charlotte, NC 28224-0643 Phone: 704/529-6364- Toll Free Number. l-600/529-6364- Fax: 704/6254409 Page 24 of 62 &R I S M I Fullironmea Meyutio s Full-S nmaatel Solutions umumera we Laboratory Report 11/16/2016 Weyerhaeuser Corporation Project: Groundwater 2016 Client Sample ID: MW -9 Attn: Dennis Atkinson Prism Sample ID: 6110040-07 524 Pride Way Prism Work Order: 6110040 Elkin, NC 28621 Sample Matrix: Water Time Collected: 11/02/16 13:00 Time Submitted: 11/02/16 14:30 Parameter Result Units Report MDL Dilution Method Analysis Analyst Batch Limit Factor Date/Time ID Chioremethane BRL ug/L 0.50 0.079 1 '82608 11/12/16 9:21 KDM P6K0292 cis-1,2-Dichlomel1hytene BRL ug/L 0.50 0.056 1 '8260B 11/12/16 921 KDM P61(0292 cis-1,3-Dichloropropylene BRL ug/L 0.50 0.079 1 '82608 11/12/16 9:21 KDM P6K0292 Dibromochloromethane BRL ug/L 0.50 0.081 1 '8260B 11/12/16 9:21 KDM PSK0292 Dibranomethane BRL ug/L 0.50 0.065 1 '8260B 11/12/16 9:21 KOM P6K0292 Dichlorodifluoromethane BRL ug/L 1.0 0.11 1 '82608 11/12/16 9:21 KDM P6K0292 Ethylbenzene BRL ug/L 0.50 0.061 1 '82608 11/12/16 921 KDM P6K0292 Hexachlombutadiene BRL ug/L 2.0 0.18 1 '82608 11/12/16 921 KDM P61(0292 Isopropyl Ether BRL ug/L 0.50 0.050 1 '82608 11/12/16 9:21 KDM P6K0292 Isopropylbenzene(Cumene) BRL ug/L 0.50 0.054 1 -82608 11/12118 9:21 KDM P6K0292 m,p-Xylenes BRL ug/L 1.0 0.12 1 '82606 11/12/16 9:21 KDM P6K0292 Methyl Butyl Ketone (2-Hexanone) BRL ug/L 5.0 0.065 1 '8260B 11/12/16 9:21 KDM PBK0292 Mathyl Ethyl Ketone (2-Butanone) BRL ug/L 5.0 0.24 1 '8260B 11/12/16 9:21 KDM PSK0292 Methyl Isobuyl Ketone BRL ug/L 5.0 0.078 1 -82608 11/12/16 9:21 KDM PSK0292 Methylene Chloride BRL ug/L 1.0 0.083 1 -82608 11/12/16 9:21 KDM P6K0292 Mallryl-tart-Butyl Ether BRL ug/L 0.50 0.042 1 '82608 11/12/16 9:21 KDM P6K0292 Naphttiskone BRL ug/L 1.0 0.19 1 -82608 11/12/16 9:21 KDM PSK0292 n-Buylhenzene BRL ug/L 1.0 0.076 1 -82608 11112116 9:21 KDM POK0292 n-Propylbemene BRL ug/L 0.50 0.087 1 '8260B 11/12/16 921 KDM P61(0292 o -Xylene BRL ug/L 0.50 0.044 1 '82608 11/12/16 921 KDM P61(0292 s Butylbsnzene BRL ug/L 0.50 0.076 1 '8260B 11/12/16 9:21 KDM PSK0292 Styrene BRL ug/L 0.50 0.047 1 '8260B 11/12/16 921 KDM PSK0292 tat-Bulylbenzene BRL ug/L 0.50 0.088 1 '82608 11/12/16 9:21 KDM P6K0292 Tetrachloroethylene BRL ug/L 0.50 0.098 1 '82608 11/12/16 921 KDM P6K0292 Toluene BRL ug/L 0.50 0.044 1 '8260B 11/12/16 9:21 KDM PBK0292 trans-1,2-Dichloroe0rybne BRL ug/L 0.50 0.094 1 '8260B 11/12/16 9:21 KDM P6K0292 trans-11,3-Dichloropropylene BRL ug/L 0.50 0.070 1 '8260B 11/12/16 9:21 KDM P6K0292 Trichlorcemylene BRL ug/L 0.50 0.078 1 '8260B 11/12/16 9:21 KDM PSK0292 TrictIorolluoromelhane BRL ug/L 0.50 0.062 1 '82608 11/12/16 921 KDM PBK0292 Yuryl soviets BRL ug/L 2.0 0.060 1 '8260B 11/12/16 921 KDM P6K0292 Kmyl chloride BRL ug/L 0.50 0.097 1 '8260B 11/12/16 9:21 KDM P6K0292 Surrogate Recovery Control Limits 4-Bromofluorobenzene 90% 80-124 Dibromofluoromethane 97% 75729 TolueneA8 104% 77-123 This report should not be reproduced, except in its enerey, without the written consent of Priam Laboratories, Inc. 449 Springbrook Road - P.O. Boz 240643 - Charlotte, NC 28224-0643 Phone: 70M6294364- Toll Free Number, 1400/6294364-Fas: 704/6264M Page25062 Sample Extraction Data Prep Method: 351.2 Lab Number Batch Initial Final Date/Time 6110040-01 P6K0112 25 mL 25 mL 11/04/16 10:20 6110040-02 P6K0144 25 mL 25 mL 11/07/16 10:00 6110040-03 P61<0144 25 mL 25 mL 11/07/16 10:00 6110040-04 P6K0144 25 mL 25 mL 11/07/16 10:00 6110040-05 P61<0144 25 mL 25 mL 11/07/16 10:00 6110040-06 P61<0144 25 mL 25 mL 11/07/16 10:00 6110040-07 P61<0144 25 mL 25 mL 11/07/16 10:00 Prep Method: SM4600-PBS Lab Number Batch Initial Final Daterrime 6110040-01 P61<0080 50 mL 50 mL 11/03/16 10:45 6110040-02 P61<0080 50 mL 50 mL 11/03/16 10:45 6110040-03 P61<0080 50 mL 50 mL 11/03/16 10:45 6110040-04 P61<0080 50 mL 50 mL 11/03/16 10:45 6110040-05 P6K0080 50 mL 50 mL 11/03/16 10:45 6110040-06 P6K0080 50 mL 50 mL 11/03/16 10:45 6110040-07 P61<0080 50 mL 50 mL 11/03/16 10:45 Prep Method: 3510C MS Lab Number Batch Initial Final Date/Time 6110040-01 P6K0133 1000 mL 1 mL 11/07/16 9:20 6110040-02 P61<0133 1000 mL 1 mL 11/07/16 9:20 6110040-03 P61<0133 1000 mL 1 mL 11/07/16 9:20 6110040-04 P61<0133 1000 mL 1 mL 11/07/16 9:20 6110040-05 P6K0133 1000 mL 1 mL 11/07/16 9:20 6110040-06 P61<0133 1000 mL 1 mL 11/07/16 9:20 6110040-07 P61<0133 1000 mL 1 mL 11/07/16 9:20 Prep Method: 3005A Lab Number Batch Initial Final Date/Time 6110040-01 P61<0190 50 mL 50 mL 11/09/16 7:55 6110040-02 P61<0190 50 mL 50 mL 11/09/16 7:55 6110040-03 P6K0190 50 mL 50 mL 11/09/16 7:55 6110040-04 P61<0190 50 mL 50 mL 11/09/16 7:55 6110040-05 P61<0190 50 mL 50 mL 11/09/16 7:55 6110040-06 P61<0190 50 mL 50 mL 11/09/16 7:55 6110040-07 P61<0190 50 mL 50 mL 11/09/16 7:55 Prep Method: 7470A Lab Number Batch Initial Final Daternme 6110040-01 P61<0194 20 mL 30 mL 11/09/16 8:30 6110040-02 P61<0194 20 mL 30 mL 11/09/16 8:30 6110040-03 P61<0194 20 mL 30 mL 11/09/16 8:30 6110040-04 P61<0194 20 mL 30 mL 11/09/16 8:30 6110040-05 P61<0194 20 mL 30 mL 11/09/16 8:30 6110040-06 P61<0194 20 mL 30 mL 11/09/16 8:30 6110040-07 P61<0194 20 mL 30 mL 11/09/16 8:30 Prep Method: 6030B Lab Number Batch Initial Final Daternme 6110040-01 P61<0292 10 mL 10 mL 11/11/16 15:10 6110040-02 P61<0292 10 mL 10 mL 11/11/16 15:10 6110040-03 P61<0292 10 mL 10 mL 11/11/16 15:10 This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240643 -Charlotte, NC 28224-0543 Phone: 7041529-6364 - Toll Free Number: 1-8001529-6364 - Fax: 7041525-0409 Page 26 of 62 Prep Method: 5030B Lab Number Batch Sample Extraction Data Initial Final Date/Time 6110040-04 P61<0292 10 mL 10 mL 11/11/16 15:10 6110040-05 P6K0292 10 mL 10 mL 11/11/16 15:10 6110040-06 P61<0292 10 mL 10 mL 11/11/16 15:10 6110040-07 PSK0292 10 mL 10 mL 11/11/16 15:10 6110040-07 Formaldehyde(Sub) 6110040-07 TOC (Sub) Subcontracted Analyses The following analyses were subcontracted to Gulf Coast Analytical Labs, Inc. Lab Number Analysis 6110040-01 Fonnaldehyde(Sub) 6110040-01 TOC (Sub) 6110040-02 Formaldehyde (Sub) 6110040-02 TOC (Sub) 6110040-03 Formaldehyde (Sub) 6110040-03 TOC (Sub) 6110040-04 Fonualdehyde(Sub) 6110040-04 TOC (Sub) 6110040-05 Fonnaldehyde(Sub) 6110040-05 TOC (Sub) 6110040-06 Formaldehyde (Sub) 6110040-06 TOC (Sub) 6110040-07 Formaldehyde(Sub) 6110040-07 TOC (Sub) This report should not be reproduced, except in its entirety, without the written consent of Prism Laboratories, Inc. 449 Springbrook Road - P.O. Box 240543 - Charlotte, NC 28224-0543 Phone: 704/529-6364 - Toll Free Number: 1-800/529-6364 - Fax: 704/525-0409 Page 27 of 62 CHAON OF CUSTODY RECORD 1 N FUll-Service Analytical & YES NO NIA m � ` Environmental Solutions PAGE- OF quoaE # To ENSURE PR®PEagt(,saLLING: St�mpv p LABORATORIES, INC.V�vy �.� Project Name: �� 00 RG'CelVed ON WET IG ? •� '� , CNI 44s Springbrook Road • Charlotte. 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Gort:d °C Phone: Fax (Yes) (No): Purchase Order No./Billing Reference TO BE FILLED IN BY CLIENTISAMPLING PERSONN Email Address: Requested Due Date ❑ 1 Day ❑ 22Ds ❑ 3 Days ❑ 4 Days ❑ 5 Days Certification: NELAC DOD FL NC EDD Type: PDF Excel ` Other "Working Days" ❑ 6-9 Days Standard 10 days ❑ Rush re h Work Must Be SC OTHER NIA Site Location Name: Samples received after 14:00 will be.processed next business day. ,��'�� ✓ time is based business days, excluding weekends and holidays!\' Water Chlorinated: PIES_ NO_ i ,� Turnaround on Site Location Physic dress: r (SEE REVERSE FOR TERMS & CONDITIONS REGARDING SERVICES ..� Sample Iced Upon Collection: YES_ NO_ RENDERED BY PRISM LABORATORIES, INC. TO CLIENT) ° LJ TIME MATRIX SAMPLE CONTAINER NALYSIS REQUESTED cam- a ,� PRISM CLIENT DATE COLLECTED (SOIL, PRESERVA- TIVES v a n > i MARK L4 LAB SAMPLE DESCRIPTION COLLECTED MILITARY WATER OR *TYPE NO. SIDE �r ` HOURS SLUDGE) SEE BELOW y'• i0 fyb g /� ID NO. \ -�!- 1� L�`•r�il I I I � SJ C p � i 'I� lam•, �j�, �l 1 i Sampler's Signature Sampled By (Print Name) Affiliation Upon relinquishing, this Chain of Custody is your authorization for Prism to proceed with the analyses as requested above. Any changes must be e submitted in writing to the Prism Project Manager. There will be charges for any changes after analyses have been initialized. Relinquished By: (Signature) Received By: (Signature Date MillterylHours Additional Comments bite Arr(Val Tlme r Relinquished By: (Signature)\ Received By: (Signature) Date %Site Departure Tirpe Relinquished By: (Signature) } Received F ri�ln Laho aFies B Dale w '•' �.Fleld Tech Feb rrnn n .;�' l ­EO Method of Shipment: NOT ALL SAMPLT OLERS SHOULD BE TAPE SHUT W(y ,CUSTODY SEALS FOR TRANSPORTATION TO THE LABORATORY. UG No. SAMPLES ARE NOCEPTED AND VERIFIED AGAINST G..6d UNTIL RECEIVED AT THE LABORATORY. yI N i 1. 1J L' {3 ❑ Fed Ex ❑ UPS ❑ Hand-deliveredrism Field Service ❑ Other NPDES. UST: GROUNDWATER: DRINKING WATER: SOLID WASTE: RC : CERCLA LANDFILL SEE REVERSE OTHER: TERMS & O, RN ❑NC❑SCI ❑NC ❑SC ❑NC ❑SC UNC ❑$C ®NC CSC I ONC❑SC LNC ❑SC ONC LSC O❑NC LSC t i�31G11 -RA i��^, NAL *CONTAINER TYPE CODES: A = Amber C = Clear G= Glass P = Plastic; TL = Teflon -Lined Cap VOA = Volatile Urganlcs Hnalysls (4ero mead zapace) PRYLY-B -O. --]1 H0 -R -AX'S FIELD INFORMATION LOG _1 Facility: Location: Sample Matrix: PURGE INFORMATION: Sample Point ID:. Field Representative: Lab Sample #: Method of Well Purge: �.-�`.\0 Dedicated: Y .1 N _Date / Time Initiated: �` 0\ One.(1). Casing Volume, Gal: tJ c y ((�� 4 Initial Water Level, Feet: `�/ Total Volume Purged, Gal:—c� Ground Water Elevation, MSL': s Was Well Purged To Dryness: Well Total Depth, Feet: i C Casing Diameter, Inches: ,, PURIaE DATA: Water Level After Purge, Feet: Date /Time Completed: PAGE 1 OF 2 Page 29 of 62 pH (std units) Conduct. Wmhos/cm) Turb. (NTU) Other (_) Time Purge Rate (gpmlhtz) Cumulative Volume Temp. (°C) I i I1 I I ' . i► � II PAGE 1 OF 2 Page 29 of 62 FIELD INFORMATION LOG (continued) I SAMPLING INFORMATION: Sample Point ID: Method of Sampling: \ � ( Z�0: r Dedicated: Y / N Water Level @ Sampling, Feet: Well Collection Sequence Number: - Parameters: Annual () Semi -Annual () Quarterly () Monthly () Other SAMPLING DATA: INSTRUMENT CHECK DATA: �� �, s � Turbidity Serial #: NTU szd. = NTU NTU std. = NTU p.H Serial #: Conductivity Serial K: GENERAL INFORMATION: 4.0 std. = 7.0 std. = umhos;cm = Weather Condiiions @ time of sampling: St j n (L4 Sample Characterisitics: 10.0 std. = umhos,cm = ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: EFTS AND OBSERVATIONS: I certify that sampling procedures were in accordance with all applicable EPA, State and Cllerr protocols. s IDate: A () By: Company: - �- PAGE 2OF2 Page 30 of 62 4 '%i ' Other Temp. pH Conduct. Turb, DateMme- Sample Rate (°C) (Std. Units) (ymhos/cm) (NTU) ( ) VOA , Other INSTRUMENT CHECK DATA: �� �, s � Turbidity Serial #: NTU szd. = NTU NTU std. = NTU p.H Serial #: Conductivity Serial K: GENERAL INFORMATION: 4.0 std. = 7.0 std. = umhos;cm = Weather Condiiions @ time of sampling: St j n (L4 Sample Characterisitics: 10.0 std. = umhos,cm = ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: EFTS AND OBSERVATIONS: I certify that sampling procedures were in accordance with all applicable EPA, State and Cllerr protocols. s IDate: A () By: Company: - �- PAGE 2OF2 Page 30 of 62 4 '%i FIELD E"4FORMATION LOG Facility:Sample Point ID: Location:e�LField Representative: Sample Matrix: Lab Sample !#: PURGE INFORMATION: Method of Well Purge: �\�� �" Dedicated: .1 NLA ,10 . _Date / Time Initiated: - V' One (1) Casing Volume, Gal: Initial Water Level, Feet: ,c1 Total Volume Purged, Gal: F �� Ground Water E:evation, MSL': ``/ Was Well Purged To Dryness:�'�--- Well Total Depth, Feet: DO Water Level After Purge. Feet: c C •� Casing Diameter, Inches: Date /Time Completed: PURGE DATA: Time Purge Rate (gpmlhtz) Cumulative Volume Temp. (°C) pH (std units) Conduct. (Nmhoslcm) Turb. (NTU) Other — .! (_) I I� I I �► PAGE 1 OF 2 Page 31 of 62 C:y FIELD INFORMATION LOG (continued) SAMPLING INF0RMATION: Sample Point ID: /\ W — V Method of Sampling: AIXrll,� \C; Dedicated: �J0J l N Water Level @ Sampling, Feet: Well Collection Sequence Number: _ r� Parameters: Annual {) Semi -Annual () Quarterly () Monthly () Other SAMPLING DATA: INSTRUMENT CHECK DATA: Turbidity Serial #: pH Serial #: Conductivity Serial n: GENERAL INF0RMATION: N i U szd. = NTU 4.0 std. _ umhos;c:n = 7.0 std. _ NTU std. = NTU 10.0 std. _ umhos/cm = Weather Conditions @ time of sampling: S� n � Sample Characterisitics: ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: . OMMENTS AND OBSERVATIONS: certify that sampling procedures were in accordance with all applicable EPA, State and clier."r protocols. Date: �/� By: Company: PAGE 2 OF 2 Page 32 of 62 Other Temp. pH Conduct. Turb. DateMme Sample Rate (°C1 (Std. Units) Wrrihoslcm) (NTU) ( ) VOA Other INSTRUMENT CHECK DATA: Turbidity Serial #: pH Serial #: Conductivity Serial n: GENERAL INF0RMATION: N i U szd. = NTU 4.0 std. _ umhos;c:n = 7.0 std. _ NTU std. = NTU 10.0 std. _ umhos/cm = Weather Conditions @ time of sampling: S� n � Sample Characterisitics: ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: . OMMENTS AND OBSERVATIONS: certify that sampling procedures were in accordance with all applicable EPA, State and clier."r protocols. Date: �/� By: Company: PAGE 2 OF 2 Page 32 of 62 FIELD INFORMATION LOG Facility: e ' ay� e � S' Sample Point ID: . Location:Field Representative: Sample Matrix: Lab Sample tf: PURGE INFORMATION: Method of Welf Purge: A a Dedicated:./ N _Date / Time Initiated: � i 1 LA'S One (1) Casing Volume, Gal:' 0 9 (00 i Initial Water Level, Feet: •�► �10 Total Volume Purged, Gal: � %y Ground Water Elevation, MSL':y Wa-s Well Purged To Dryness: Well Total Depth, Feet: U Water Level After Purge, Feet: f. Casing Diameter, Inches: L� Date /Time Completed: PURGE DATA: Time Purge Rate (gpmlhtz) Cumulative Volume Temp. (°C) pH (std units) Conduct. (pmhoslcm) Turb. (NTU) Other 3 (_} I I I ii II I 11 PAGE 1 OF 2 Page 33 of 62 FIELD INFORMATION LOG (continued) SAMPLING INFORMATION: Sample Point ID: Method of Sampling: � � \ —' .\ 0 Dedicated: P 9 @/ N Water Level @ Sampling, Feet: , Well Collection Sequence Number: `3 Parameters: Annual 4) Semi -Annual () Quarterly () Monthly () Other �'�I:�C = • v SAMPLING DATA: INSTRUMENT CHECK DATA: Turbidity Serial #: p.H Serial #: NTU szd. = NTU NTU std. = NTU 4.0 std. = 7.0 std. = 10.0 std. _ Conductivity Serial #: umhos;cm = umhos/cm = GENERAL INFORMATION: Weather Conditions @ time of sampling: Sy [\ C\ L4 wzzx rrx Sample Characterisitics: ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: j COMMENTS AND OBSERVATIONS: 1" c i o n es p 0A, OR` t I certify that sampling procedures were in accordance with all applicable EPA, State and Client protocols. Date: �a/% By: Company: PAGE 2 OF 2 Page 34 of 62 Other Temp. pH Conduct. Turb. DateMme Sample Rate (°C) (Std. Units) Ujmhoslcm) (NTU) WA VOA Other ! INSTRUMENT CHECK DATA: Turbidity Serial #: p.H Serial #: NTU szd. = NTU NTU std. = NTU 4.0 std. = 7.0 std. = 10.0 std. _ Conductivity Serial #: umhos;cm = umhos/cm = GENERAL INFORMATION: Weather Conditions @ time of sampling: Sy [\ C\ L4 wzzx rrx Sample Characterisitics: ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: j COMMENTS AND OBSERVATIONS: 1" c i o n es p 0A, OR` t I certify that sampling procedures were in accordance with all applicable EPA, State and Client protocols. Date: �a/% By: Company: PAGE 2 OF 2 Page 34 of 62 h_S LAD-0-`TOIES9 FIELD INFORMATION LOG Facility:�� Location: Sample Matrix: PURGE INFORMATION: Sample Point ID:.`�v Field Representative: . Lab Sample #: Method of Well Purge: wit, M1L_'1r Y Dedicated: Y / N _Date / Time Initiated: �'l� -�� One (1) Casing Volume, Gal:* Cr t� Initial Water Level, Feet: < < L Total Volume Purged, Gal: Ground Water Elevation, MSL. 1� Wa-s Well Purged To Dryness: Well Total Depth, Feet: 0"%100 Water Level After Purge. Feet: A ` Casing Diameter, Inches: Date/ Time Completed: -0 `� U '��`,D PURGE DATA: Time Purge Rate (gpmfhtz) Cumulative Volume Temp. (°C) pH (std units) Conduct. (umhos/cm) Turb. (NTU) Other t — (_) I I ►i , it i I iI I II PAGE 1 OF 2 Page 35 of 62 ,I FIELD INFORMATION LOG (continued) SAMPLING INFORMATION: Sample Point ID: Method of Sampling: ��ti \�; Dedicated: Q1 N Water Level @ Sampling, Feet: Well Collection Sequence Number: LA Parameters: Annual () Semi -Annual () Quarterly () Monthly () Other I J , at' , SAMPLING DATA: INSTRUMENT CHECK DATAklk Turbidity Serial #: p.H Serial #: Conductivity Serial #: _ GENERAL INFORMATION: NTU s:d. = NTU 4.0 std. _ umhos;cm = 7.0 std. _ NTU std. = NTU 10.0 std. _ umhos;cm = Weather Conditions @ time of sampling: SCJ r. Sample Characterisitics: ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: ` ONIM)EIVTS " \ Q AND OBSERVATIONS: > v��,,. n OLS e I certify that sampling procedures were in accordance with all applicable EPA, State and cner.r protocols. Date:1611% By:o Company: i PAGE 2 OF 2 Page 36 of 62 i Other Temp. pH Conduct. Turb. DateMme Sample Rate (°C) (Std. Units) (1.rmhoslcm) (NTU) (_) � , 50 W VOA Other INSTRUMENT CHECK DATAklk Turbidity Serial #: p.H Serial #: Conductivity Serial #: _ GENERAL INFORMATION: NTU s:d. = NTU 4.0 std. _ umhos;cm = 7.0 std. _ NTU std. = NTU 10.0 std. _ umhos;cm = Weather Conditions @ time of sampling: SCJ r. Sample Characterisitics: ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: ` ONIM)EIVTS " \ Q AND OBSERVATIONS: > v��,,. n OLS e I certify that sampling procedures were in accordance with all applicable EPA, State and cner.r protocols. Date:1611% By:o Company: i PAGE 2 OF 2 Page 36 of 62 i PPJS LXB0�A-T -0-R1E�� FI]EILD INFORMATION LOG Facility: Location:���-� Sample Matrix: PURGE INFORMATION: Sample Point ID:. J rA Field Representative: Lab Sample 9: Method of Well Purger �-fDedicated: @.l N _Date / Time Initiated: w One (1) Casing Volume, Gal: Initial Water Level, Feet:. - � Total Volume Purged, Gal: So eo Ground Water E:evation, MSL': s l0 Was Well Purged To Dryness: k�'. Well Total Depth, Feet: '`�, , 0 Water Level After Purge, Fest: Casing Diameter, Inches: �—i� Date /Time Completed: PURI3E DATA: Time Purge Rate (gpm/htz) Cumulative Volume Temp. (°C) pH (std units) Conduct. Wmhoslcm) Turb. (INTU) Other t fl PAGE 1 OF 2 Page 37 of 62 FIELD INFORMATION LOG (continued) SAMPLING INFORMATION: Sample Point ID: )-\ W m Method of Sampling: Tc�n�.� �+\oma Dedicated: / N 3 Water Level @ Sampling, Feet: Well Collection Sequence Number: - Parameters: Annual () Semi -Annual () Quarterly () Monthly () Other SAMPLING DATA: INSTRUMENT CHECK DATA Turbidity Serial: NTU std. = NTU NTU std. = NTU p.H Serial #: 4.0 std. = 7.0 std. = 10.0 std. _ Conductivity Serial r : umhes;cm = umhcs;cm = GENERAL INFORMATION: Weather Conditions @ time of sampling: Sample Characterisitics: ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: COMMENTS AND OBSERVATIONS: ��o 11n ��i ��� �r�ID t certify that sampling procedures were in accordance with all applicable EPA, State and cnar"r protocols. Date: By: Company: PAGE 2 OF 2 Page 38 of 62 Other Temp. pH Conduct. Turb. Date/Time Sample Rate (°C) (Std. Units) Cpmhos/cm) (NTU) ( ) �� _ � %SOA ,� Other iLA - v : 040 s INSTRUMENT CHECK DATA Turbidity Serial: NTU std. = NTU NTU std. = NTU p.H Serial #: 4.0 std. = 7.0 std. = 10.0 std. _ Conductivity Serial r : umhes;cm = umhcs;cm = GENERAL INFORMATION: Weather Conditions @ time of sampling: Sample Characterisitics: ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: COMMENTS AND OBSERVATIONS: ��o 11n ��i ��� �r�ID t certify that sampling procedures were in accordance with all applicable EPA, State and cnar"r protocols. Date: By: Company: PAGE 2 OF 2 Page 38 of 62 L Facility: Location: Sample Matrix: PURGE INFORMATION: Sample Point ID:. Field Representative: Lab Sample ff: Method of Well Purge: V -,,I Dedicated: UY .! N r _Date / Time Initiated: 0\_I�•�5-0,0 One (1) Casing Volume, Gal:- 60 Initial Water Level, Feet: �� tO'1, Total Volume Purged, Gal: 5 r0 i,) Ground Water Elevation, MSL': D,Pc? Wa-s Well Purged To Dryness: 0 Well Total Depth, Feet: , V Casing Diameter, Inches: PURQE DATA: Water Level Ater Purge, Feet: e Date /Time Completed: Time Purge Rate (gpmlhtz) Cumulative Volume Temp. (°C) pH (std units) Conduct. (imhoslcm) Turb. (NTU) � II PAGE 1 OF 2 J Page 39 of 62 1 Eg? i FIELD INFORMATION LOG (continued) SAMPLING INFORMATION: Sample Point ID: j,-) G r . \J Method of Sampling: '�.y,rP �1-�,. � r Dedicated: y / N Water Level @ Sampling, Feet: Well Collection Sequence Number: Parameters: Annual () Semi -Annual () Quarterly () Monthly () Other - l SAMPLING DATA: INSTRUMENT CHECK DATA: Turbidity Serial #: p.H Serial #: Conductivity Serial M: GENERAL INFORMATION: NTU srd. = NTU 4.0 std. = 7.0 std. _ umhos;cm = NTU std. = NTU 10.0 std. = umhos/cm = Weather Conditions @ time of sampling: SQ r\ Sample Characterisitics: ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: COMMENTS AND OBSERVATIONS: I certify that sampling procedures were in accordance with all applicable EPA, State and Client protocols. Date: /� By: Company: PAGE 2 OF 2 Page 40 of 62 Other Temp. pH Conduct. Turb. Date/Time Sample Rate (°C) (Std. Units) (umhos/cm) (NTU) (_) VOA a Other i, INSTRUMENT CHECK DATA: Turbidity Serial #: p.H Serial #: Conductivity Serial M: GENERAL INFORMATION: NTU srd. = NTU 4.0 std. = 7.0 std. _ umhos;cm = NTU std. = NTU 10.0 std. = umhos/cm = Weather Conditions @ time of sampling: SQ r\ Sample Characterisitics: ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: COMMENTS AND OBSERVATIONS: I certify that sampling procedures were in accordance with all applicable EPA, State and Client protocols. Date: /� By: Company: PAGE 2 OF 2 Page 40 of 62 PIRT -M-L-AB-0-T0IES- —. FIELD INFORMATION LOG Facility: �Z? Location: i .��r\ Sample Matrix: PURGE INFORMATION: Sample Point ID::�~� Field Representative: Lab Sample #: Method of Well Purge: �s�: ��Dedicated: Y N - r F� � _Date /Time Initiated: ��"�``" ,`� `� One (1) Casing Volume, Gal: 0 "So • l Initial Water Level, Feet: r' '�J Total Volume Purged, Gal: C� To Dryness' 4' Ground Water E:evation, MSL': Wa-s Well Pur � g� � - Well Total Depth, Feet: S I T)0 Water Level After Purge, Feet: Casing Diameter, Inches:�l Date /Time Completed: v PURRE DATA: Time Purge Rate (gpmlhtz) Cumulative Volume Temp. (°C) pH (std units) Conduct. Wmhos/cm) Turb. (NTU) Other i — 'I (� , i� . c i I it i Il PAGE 1 OF 2 Page 41 of 62 ==i FIELD INFORMATION LOG (continued) 17-4 SAMPLING INFORMATION: Sample Point !D: �,jo Method of Sampling: ��\l``yC Dedicated: ! N Water Level @ Sampling, Feet: Well Collection Sequence Number: l Parameters: Annual () Semi -Annual () Quarterly (} Monthly {) Other ( b SAMPLING DATA.: INSTRUMENT CHECK DATA: Turbidity Serial #: p1H Serial #: NTUSd. = 4.0 std. = Conductivity Serial #: umhos;cm = GENERAL INFORMATION: NTU 7.0 std. = NTU std. = NTU 10.0 std. = umhos/cm = - Weather Conditions @ time of sampling: SQ C' (_- cl Sample Characterisitics: ANALYTE: COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: COMMENTS AND OBSERVATIONS: 1 certify that sampling procedures were in accordance with all applicable EPA, State and Clier."r protocols. Date: �/�� By: Company: nom - PAGE 2 OF 2 Page 42 of 62 Other Temp. pH Conduct. Turb. DateMme Sample Rate (°C) (Std. Units) (pmhos/cm) (NTU) ( ] VOA ` <; A Other a;90 INSTRUMENT CHECK DATA: Turbidity Serial #: p1H Serial #: NTUSd. = 4.0 std. = Conductivity Serial #: umhos;cm = GENERAL INFORMATION: NTU 7.0 std. = NTU std. = NTU 10.0 std. = umhos/cm = - Weather Conditions @ time of sampling: SQ C' (_- cl Sample Characterisitics: ANALYTE: COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: COMMENTS AND OBSERVATIONS: 1 certify that sampling procedures were in accordance with all applicable EPA, State and Clier."r protocols. Date: �/�� By: Company: nom - PAGE 2 OF 2 Page 42 of 62 FIELD INFORMATION LOG Facility: Location: r" Sample Matrix: PURGE INFORMATION: Sample Point ID:. Field Representative: Lab Sample #: Method of Well Purge: �� .\t7t� Dedicated: ;�Y ./ N � —Date/ Time Initiated: t' �'�� One (1) Casing Volume, Gal:* o Initial Water Level, Feet: i . Total Volume Purged, Gal: ! Ground Water Elevation, MSL-: I'LA ci Well Total Depth, Feet:D` •�� Casing Diameter, Inches: PURQE DATA: Wa-s Well Purged To Dryness: Water Level After Purge. Feet: C \V CK - �J-j Date /Time Completed: Time Purge Rate (gpmlhtz) Cumulative Volume Temp. (°C) pH (std units) Conduct. (.umhos/cm) Turb. (NTU) Other �t PAGE 1 OF 2 Page 43 of 62 r FIELD INFORMATION LOG (continued) SAMPLING INFORMATION: Method of Sampling: Water Level @ Sampling, Feet: Parameters: Annual () Semi -Annual ( ) SAMPLING DATA: Sample Point ID: Mij "� Dedicated: Well Collection Sequence Number - Quarterly () Monthly () Other (v( f INSTRUMENT CHECK DATA: Turbidity Serial #: p.H Serial #: Conductivity Serial #: GENERAL INFORMATION: NTU std. = NTU 4.0 std. = 7.0 std. umhosrc:n = NTU std. = NTU 10.0 std. _ umhos/cm = Weather Conditions @ time of sampling: S(j n (I,- W Sample Characterisitics: ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: COMMENTS AND 0BSERVATIONS: I certify that sampling procedures were in accordance with all applicable EPA, State and clieriT protocols. Date:v lalU� 6 y: Company: PAGE 2 OF 2 Page 44 of 62 Other Temp. pH Conduct.. Turb. Date/Time Sample Rate PC) (Std. Units) (Jumhos/cm) (NTU) ( ) VOA Other i INSTRUMENT CHECK DATA: Turbidity Serial #: p.H Serial #: Conductivity Serial #: GENERAL INFORMATION: NTU std. = NTU 4.0 std. = 7.0 std. umhosrc:n = NTU std. = NTU 10.0 std. _ umhos/cm = Weather Conditions @ time of sampling: S(j n (I,- W Sample Characterisitics: ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: COMMENTS AND 0BSERVATIONS: I certify that sampling procedures were in accordance with all applicable EPA, State and clieriT protocols. Date:v lalU� 6 y: Company: PAGE 2 OF 2 Page 44 of 62 g ,5m_ LAB- 0 1ESy-i?��-�.' FIELD INFORMATION LOG t Facility: Sample Point ID:.�_ Location:Field Representative: ` Sample Matrix: Lab Sample 9: PURGE INFORMATION: Method of Well Purge: j ` ��`� Dedicated: Y ( N k� j� -( l ��_Date /Time Initiated: i��' � � •.� - - One (1) Casing Volume, Gal:- � ' � 0 AO Initial Water Level, Feet: J� V Total Volume Purged, Gal: J r c 1 Ground Water E:evation, MSL:: y ��u Was Well Purged To Dryness:P Well Total Depth, Feet: Water Level After Purge, Feet: �•a t 1 Casing Diameter, Inches: Date /Time Completed:V PURI -E DATA: PAGE 1 OF 2 Page 45 of 62 Temp. (°C) pH (std units) Conduct.QT�) (pmhoslcm)(__--J Other i 1 Time Purge Rate (gpmlhtz) Cumulative Volume I !{{I I 1! I - I l :I PAGE 1 OF 2 Page 45 of 62 - I= FIELD INFORMATION LOG (continued) SAMPLING INFORMATION: Method of Sampling: Water Level @ Sampling, Feet: Parameters: Annual (1 Semi -Annual ( ) SAMPLING DATA: Sample Point ID: Dedicated: Y/ N Well Collection Sequence Number: _ Quarterly () Monthly () Other � 4l ,IL INSTRUMENT CHECK DATA: Turbidity Serial #: p.H Serial #: Conductivity Serial #: GENERAL INFORMATION: NTU std. _ 4.0 std. _ umhos;cm = _ NTU NTU std. = NTU 7.0 std. = 10.0 std. _ umhos; cm = Weather Conditions @ time of sampling: SQ r\ (_- Sample Characterisitics: ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: COMMENTSAND OBSERVATIONS: I certify that sampling procedures were in accordance with all applicable EPA, State and Cllenr protocols. Date:`\ lam-"/� By: Company: PAGE 20F2 Page 46 of 62 Other Temp. pH Conduct. Turb. DateMme Sample Rate (°C) (Std. Units) Vmhas/cm) (NTU1 ( ] VOA I Other t INSTRUMENT CHECK DATA: Turbidity Serial #: p.H Serial #: Conductivity Serial #: GENERAL INFORMATION: NTU std. _ 4.0 std. _ umhos;cm = _ NTU NTU std. = NTU 7.0 std. = 10.0 std. _ umhos; cm = Weather Conditions @ time of sampling: SQ r\ (_- Sample Characterisitics: ANALYTE COLLECTION ORDER, CONTAINERS, PRESERVATIVES AND TESTS PERFORMED: COMMENTSAND OBSERVATIONS: I certify that sampling procedures were in accordance with all applicable EPA, State and Cllenr protocols. Date:`\ lam-"/� By: Company: PAGE 20F2 Page 46 of 62 ACCESS ANALYTICAL, INC. ANALYTICAL. REPORT CLIENT Prism Laboratories, Inc. PO BOX 240543 Charlotte, NC 28224 ATTENTION Cara Rusmisell PROJECTID 6110040 LABORATORY REPORT NUMBER 216110366 DATE 11/11/2016 Primary Data Review By I Robyn Mlgues/Dirof ata !' r l�- Authorize Signatu/rV'e PLEASE NOTE: Secondary Data Review By Ashley B. Amick Project Manager, Access Analytical, Inc. aamick@accessanalyticalinc.com - Unless otherwise noted, all analysis on this report performed at Gulf Coast Analytical Labs (GCAL), 7979 Innovation Park Dr., Baton Rouge, LA 70820. - GCAL is SCDHEC certified laboratory # 73006, NCDENR certified lab # 618, GA certified lab # LA -01955, NELAP certified laboratory # 01955 Local support services for this project are provided by Access Analytical, Inc.. Access Analytical is a representative of GCAL serving clients in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll free at 888.315.4243. Lab Report#: 216110366 Revision 1Pace 1 of 16 Page 47 of 62 NELAP CERTIFICATE NUMBER: 01955 DOD ELAP CERTIFICATE NUMBER: L14-243 PERFORMED BY GCAL, LLC 7979 Innovation Park Dr. Baton Rouge, LA 70820 Report ®ate 11/11/2016 IIVIAIVIIII�IIIIIIIOIIIIIIIIa91�l1 Project 6110040 Deliver To Additional Recipients Cara Rusmisell NONE Prism Laboratories, Inc. PO BOX 240543 Charlotte, NC 28224 706-529-6364 / I S C0011 17025 P3V Testing DaD EIAF Lab Report#: 216110366 Revision 1 Page 48 of 62 l Report#: 216110366 AL A td ALY T IIC AtOR1'es. uc Project IDS 6110040 Laboratory Endorsement Report Date: 11/11/2016 Sample analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized agencies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this retention period the samples will be disposed in accordance with GCAL's Standard Operating Procedures. Common Abbreviations that may be Utilized in this Report ND Indicates the result was Not Detected at the specified reporting limit NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030 DO Indicates the result was Diluted Out MI Indicates the result was subject to Matrix Interference TNTC Indicates the result was Too Numerous To Count SUBC Indicates the analysis was Sub -Contracted FLD Indicates the analysis was performed in the Field DL Detection Limit DL Diluted analysis —when appended to Client Sample ID LOD Limit of Detection LOQ Limit of Quantitation RE Re -analysis CF HPLC or GC Confirmation 00:01 Reported as atime equivalent to 12:00 AM Reporting Flags that may be Utilized in this Report J or I Indicates the result is between the MDL and LOQ J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria U Indicates the compound was analyzed for but not detected B or V Indicates the analyte was detected in the associated Method Blank Q Indicates a non-compliant QC Result (See Q Flag Application Report) * Indicates a non-compliant or not applicable QC recovery or RPD —see narrative E The result is estimated because it exceeded the instrument calibration range E Metals - % diference for the serial dilution is > 10% P RPD between primary and confirmation result is greater than 40 Sample receipt at GCAL is documented through the attached chain of custody. In accordance with NELAC, this report shall be reproduced only in full and with the written permission of GCAL. The results contained within this report relate only to the samples reported. The documented results are presented within this report. This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited. I certify that this data package is in compliance with The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee, as verified by the following signature. Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if applicable. 4 Robyn MigueslDir of Data Dei i Authorized Signature GCAL Report 216110366 Lab Report#: 216110366 Revision 1 Page 49 of 62 e� g;i 3aiH. -+� sg,5nur sG .�3�3�.h. 'f•E£,p5=. Report#: 216110366 Project ID: 6110040 Certifications Report Date: 11/11/2016 Certification Certification Number DOD ELAP L14-243 Alabama 01955 Arkansas 12-060-0 Colorado 01955 Delaware 01955 Florida E87854 Georgia 01955 Hawaii 01955 Idaho 01955 Illinois 200048 Indiana 01955 Kansas E-10354 Kentucky -95 Louisiana 01955 Maryland 01955 Massachusetts 01955 Michigan 01955 Mississippi 01955 Missouri 01955 Montana N/A Nebraska 01955 New Mexico 01955 North Carolina 618 North Dakota R-195 Oklahoma 9403 South Carolina 73006001 South Dakota 01955 Tennessee 01955 Texas T104704178 Vermont 01955 Virginia 460215 USDA Soil Permit P330-10-00117 Lab Report#: 216110366 Revision 7 Page 50 of 62 Report#: 216110366 gtLA LY TICLOFAIGPI=S: LLC Project ID: 6110040 Report Date: 11/11/2016 Case Narrative Client: Access Analytical Report: 216110366 Gulf Coast Analytical Laboratories received and analyzed the sample(s) listed on the Report Sample Summary page of this report. Receipt of the sample(s) is documented by the attached chain of custody. This applies only to the sample(s) listed in this report. No sample integrity or quality control exceptions were identified unless noted bblow. This report was revised 11/11/16 to exclude a sample that required a separate report. GENERAL CHEMISTRY In the SM 5310 B-2011 analysis, a chemical or physical interference necessitated a dilution for all samples.This is reflected in elevated detection limits. Lab Report#: 216110366 Revision 1PAge 5 of 16 Page 51 of 62 Report#: 216110366 Project ID: 6110040 Sample Summary Report Date: 11/11/2016 GCAL ID Client ID Matrix Collect Date/Time Receive Date/Time 21611036601 MW -5 Water 11102/201610:30 11/03/201610:00 21611036602 MW -11 Water 11/02/201611:00 11/03/201610:00 21611036603 MW -12 Water 11102/201611:15 11/03/201610:00 21611036604 MW -10 Water 11/02/201611:30 11/03/201610:00 21611036606 MW -4 Water 11/02/201612:00 11103/201610:00 21611036607 MW -6 Water 11/021201612:15 11/031201610:00 21611036608 MW -9 Water 11/02/201613:00 11/03/201610:00 Lab Report#: 216110366 Revision 1 Pa e 6 of 16 Page 52 of 62 J�9 Report#: 216110366 Project ID: 6110040 Report Date: 11/11/2016 Summary of Compounds Detected Collect Date •11/021201611:00 GCAL ID 21611036602 Mw -I I Receive Date 11103/201610:00Water Matrix SM 5310 B-2011 CAS# Parameter Result DL LOQ Units C-012 Total Organic Carbon 1.01 0.60 4.0 mg/L Collect Date 11/02/2016 12:00 GCAL ID -21 611036606 MW -4'; Receive Date 11103/201.6 10:0.0 Matrix. Water SM 5310 B-2011 CAS# Parameter Result DL LOQ Units C-012 Total Organic Carbon 0.861 0.60 4.0 mg/L Collect Date 11/02/2016 12:15 GCAL Jl) 21611.036607 MW' 6 Receive Date 11103!2016.10:00 Matrix: Water SM 5310 B-2011 CAS# Parameter Result DL LOQ Units C-012 Total Organic Carbon 0.87J 0.60 4.0 mg/L Collect Date .11102/2016 13:00 GCAL ID 21611036608 Receive Date 11103/2016 10:00 'Matrix Water SM 5310 B-2011 CAS# Parameter C-012 Total Organic Carbon Result DL LOQ Units 1.61 1.5 10.0 mg/L Lab Report#: 216110366 Revision 1 Pacie 7 of 16 1 Page 53 of 62 k= i Report#: 216110366 ;_• AfIn LY TILAL L:1 f!Ofl ATO RIES, LLC Project ID: 6110040 Report Date: 11/11/2016 F � Sample Results 1= Collect Date 11!0.2/2016 10:30 GOAL ID 21611036601 Mw -5 Receive Date 11!03/2016.10:00 Matrix Water 5310 B-2011 Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch NA NA NA 5 11/071201613:34 JEM 598338 CAS# Parameter Result DL LOQ Units C-012 Total Organic Carbon 1.5U 1.5 10.0 mg/L EPA 8315A Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch 11105/2016 12:00 598256 EPA 8315A 1 11105/2016 20:39 CLH 598348 CAS# Parameter 50-00-0 Formaldehyde Result DL LOQ 226U 226 500 Collect Date 11/0272016 11:00 GCAL ID 21611036602 mw -*1'f Receive Date 11/03/2016 10:00 Matrix Water 5310 B-2011 Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch NA NA NA 2 11/07/201613:59 JEM 598338 CAS# Parameter Result DL LOQ Units C-012 Total Organic Carbon 1.01 0.60 4.0 mg/L SPA Rg1RA Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch 11/05/2016 12:00 598256 EPA 8315A 1 11/05/2016 20:56 CLH 598348 CAS# Parameter Result DL LOQ Units 50-00-0 Formaldehyde 22.61-1 22.6 50.0 ug/L Lab Report#: 216110366 Kevision Page 54 of 62 Sample Results Collect Date 11/02/2016 11:15 GCAL ID 21611036603 MW -12 Receive Date 11/03/2016 16:00 Matrix.: Water D B-2011 Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch NA NA NA 5 11/07/201614:16 JEM 598338 CAS# Parameter Result DL LOQ Units C-012 Total Organic Carbon 1.51-1 1.5 10.0 mg/L. EPA 8315A Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch 11/05/201612:00 598256 EPA 8315A 1 11/05/2016 21:13 CLH 598348 CAS# Parameter 50-00-0 Formaldehyde Result DL LOQ 22.6U 22.6 50.0 Collect Date, 11/02/2016 11:30 ..GCAL ID 2161,1036604 MW -10 Receive Date 11/03/2016 10:00 Matrix Water SP ) B-2011 Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch NA NA NA 5 11/07/201614:33 JEM 598338 CAS# Parameter Result DL LOQ Units C-012 Total Organic Carbon 1.51-1 1.5 10.0 mg/L EPA 8315A Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch 11/05/201612:00 598256 EPA 8315A 1 11/05/2016 21:30 CLH 598348 CAS# Parameter 50-00-0 Formaldehyde Lab Report#: 216110366 Result DL LOQ Units 22.6U 22.6 50.0 ug/L evision 1 Page 55 of 62 t=' SI GCA&LReport#: 216110366 AtfALYTICAL LACOFAMRIES. L1. Project .ID: 6110040 Report Date: 11/11/2016 Sample Results Collect Date 11/02/2016 12:00 GCAL ID 21611036606 Receive Date 11/03/2016 10:00 ' Matrix Water 10 B-2011 Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch NA NA NA 2 11/07/201615:10 JEM 598338 CAS# Parameter Result DL LOQ Units C-012 Total Organic Carbon 0.86J 0.60 4.0 mg/L EPA 8315A Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch 11/05/2016 12:00 598256 EPA 8315A 1 11/05/2016 22:03 CLH 598348 CAS# Parameter 50-00-0 Formaldehyde Result DL LOQ Units 22.6U 22.6 50.0 ug/L Collect Date 11/02/2016 12:15 GCAL ID ` 21611036607; MW -6 Receive Date 11!03!2016 10:00 Matrix Water 10 B-2011 Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch NA NA NA 2 11/07/201615:27 JEM 598338 CAS# Parameter Result DL LOQ Units C-012 Total Organic Carbon 0.87J 0.60 4.0 mg/L EPA 8315A Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch 11/05/2016 12:00 598256 EPA 8315A 1 11/05/2016 22:20 CLH 598348 CAS# Parameter Result DL LOQ Units 50-00-0 Formaldehyde 22.6U 22.6 50.0 ug/L Lab Report#: 216110366 Revision 1 Parip 10 of 16 Page 56 of 62 --- ----- - --- - Reportk 216110366 Project I D: 6110040 Sample Results Report Date: 11/11/2016 Collect Date 11102/2016 13:00 G.CAL ID 2161103.6608 Mw -9 Receive Date 11/03/2016 10:00 Matrix Water Sf U B-2011 Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch NA NA NA 5 11/07/201615:44 JEM 598338 1 GAS# C-012 EPA 8315A Parameter Result Total Organic Carbon 1.61 DL LOQ Units 1.5 10.0 mg/L Prep Date Prep Batch Prep Method Dilution Analysis Date By Analytical Batch 11/05/201612:00 598256 EPA 8315A 1 11/05/2016 22:36 CLH 598348 CAS# Parameter Result 50-00-0 Formaldehyde 22.6U DL LOQ Units 22.6 50.0 ug/L Lab Report#: 216110366 Revision 1 Pane 11 of 16 - I Page 57 of 62 ASKiff Report#: 21611066 %3 1 CAL Project ID: 6110040 Report Date: 11/11/2016 ANALYT CAL LAF09AIDRIPS. LLC General Chemistry QC Summary 5 16269 598339; GOAL ID 1626 162691 6 LOS Sample Type MB LCSD. Prep Date NA; NA NA Analysis Date 11107/2016 08:48 ll./97/2016 08:06 11/07/2016 2:10 ater Matrix W Water: Water r9l Spik Result %R RPD SM 5310 B�20 1 Result DL Added 6hiits%R , Added Limit Total Organic Carbon I C-012 1 0,3011 0.301 50.01 45.01901 90-110 1 50.01 4601921 2 1 20 1 Analytical Batch' Client ID. Ave C (003) -.TOC- 16251357MS 1625957 216ilO33901 1626917 16269 8 598338 '66AL I Di mpleType SA Prep Date 'NA N NA A nillys'isb6te 11107/2016 10:18 /07/26id* 0.36'-.'. 11/07/2016 10:51 matrix Water Water wl:-:.: Water rng�!- Spike Spike RPD Unit Cqntrol I s DLI Added Limits%. R- Added Result I Total Organic Carbon I C-012 1 5.21 0.301 50.01 52.91 951 80-120 1 50.01 52.9 96 1 0 1 20 Analytical Batch Client ID MW -9 IM0861VIS 1626086MSD �98338 GOAL ID 21611036608 1626920 a Sam pie Type SAMPLE MSD 'Prep.Date NA NA NA 11 /0712616 17':20 Matrix Water. Water Water SM 5310 B-2011 Spike I Resu t RRD Total Organic Carbon I C-012 1 1.61 1.51 2501 2241 891 80-120 1 2501 223188 1 0 1 20 1 Lab Report#: 216110366 Revision 1 Pnot, 12 of 16 1 Page 58 of 62 Report#: Project ID: 216110366 6110040 General Chromatography QC Summary Report Date; 11/11/2016 AnaJlytica I Batch Client ID MB598256 - LCS598256 LCSD598256 ' 598348 Gr -AL. ID 1626492 1626493 1626464 Prep Patch Sample Type MB LCS LCSD 598256Prep Date 11/05/2016 12:00 11/05/2016 12:00 1.110512016 1.2:00 alysis Da .1 t . e Prep Method Analysis 11/05120 . 16 19:16 11/05/2016 19:32 1-1/05/2016 19:49 EPA 8315A Matrix Water Water Water . PPA $315A. Units ug/L S ke p! KR6�s�**ull %R I Control I Spike 16, RPb DI RPD I - -.:.. . p. .. 1. .. I 1 1, Result DL ,Added Added L:imits%R I Added 1 , ed �16 Limit Formaldehyde 1 50-00-0 1 22.6U 1 22.61 2501 26311051 2501 29-168 1 2501 247199 29 -168 1 2501 1 30 Analytical Batch - 1 Client ID MW -9..: 1626086MS 1626086MSD 598348 G6AL'ID 21611036608 1626498 1626499 Prep Batch Sarnple Type SAMPLE MS MSD 598256 Prep Date 11/05/2016 12:00 11/05/2016 12:0.0.1. 11/0512016 12:00 Prep Method Analysis Date 11/05/2016 22:36 11/05/2016 22:53 11/05/2616 23:10 EPA 8315A' Matrix waier:-,;,.— Water Water EP A 8315A Units Spike t Result I" "Spike =Add( s Result 1 RPD RPD - - Result DL Added �- I Limit. -/.R , ed Limit, Formaldehyde 1 56-00-5 1 9.671 22.61 2501 274 11061 29 -168 1 2501 27211051 1 1 30 1 pnrl., III nf 1 A Lab Report#: 216110366 Revision 1 1 Page 59 r m Cr X '0 0 0 C', M Fvmica Analytical R- ISM IEnvironmental Solutionss �Apos&=Rlss' on SUBCONTRACT ORDER Certification:' NELAC_ USACE Prism Laboratories, Inc. NC� SC_ Other i I 6110040 SENDING LABOIL4TORY: RECER'ING LABORATORY: Prism Laboratories; Inc. Gulf Coast Analytical Labs, Inc. R O. Box 240543 7979 Innovation Park Drive Charlotte, NC 28224-0543 Bator. Rouge, LA 70820 Phone: 800-529-6364 Phone :(225) 769-4900 Fax: 704-525-0409 Fax: (225) 767-5717 PTojecth4anager_ Cara C. Rusmisell 1113011611:15 Analysis Due Expires Laboratory ID Comments Sample 1D: 6110040-01 TOC (Sub) Formaldehyde (Sub) Containers Supplied.• Water Sampled:11/02/1610:30 11/30/1610:36 11/05/16 10:30 Sample 1D: 6110040-02 Water Sampled:11/02/1611:00 (p TOC (sub) C Formaldehyde (Sub) Containers Supplied: O Sample ID: 6110040 Formaldehyde (Sub) TOC (Sub) [Containers Supplied: Sample ID: 6110040 TOC (Sub) Formaldehyde (Sub) '_-ontainers Supplied.• Released By Date Received By Date 1 Released By Date Received By Date Pane I of 2 T 0 CC <D .11 0 rn Page 60 of 62 11/30/16 11:00 11/05/16 11:00 3 Water Sampled:]1/02/1611:15 11105/1611'.15 1113011611:15 4 Water Sampled:11/02116 11:30 1 113 0/16 11:30 11/0511611:30 ate,. Released By Date Received By Date 1 Released By Date Received By Date Pane I of 2 T 0 CC <D .11 0 rn Page 60 of 62 00 rr X CD '0 0 ik N W O rn CD U) 0 0w SUBCONTRACT ORDER Certification: NELAC USACE Prism Laboratories, Inc- NC— SC— Other 6110040 rN!A Analysis Due Expires Laboratory ID Comments Sample ]D- 6110040-05 Water Sampled:11/02116 12:00 TOC (Sub) 11/3011612:00 Formaldehyde (Sub) 11105!1612:00 .ontainers Supplied. Sample ID: 6110040-06 Water Sampled:11/02116 12,15 TOC (Sub) 11/30116 12:15 Formaldehyde (Sub) 11/05/16 12:15 Containers Supplied. Sample ED: 6110040-07 Water Sampled:11/02/16 13:00 -:7 TOC (Sub) 1113011613:00 Formaldehyde (Sub) 11103116 13:00 Containers Supplied: BReleased By Date Received By Date RReleased By Date Received By Date Page2 of2 I Page 61 of 62 (VOTES Revision 1.5 Page 1 of 1 Lab Report#: 216110366 Revision 1 Page 16 of 16 cu SAMPLE RC •-,` _". '1 NG CHECKLIST !i'�'��111911�11�111�11>lll�l{W11111 SAMPLE DELIVERY GROUP 226110366 CHECKLIST YES NO NA Client PM SAB3 Transport Method Samples received with proper thermal and chemical preservation? oll -------- ® ® ❑ ❑ ❑ 4565 -Access Analytical 4566 FEDEX Radioactivity is <7600 corp? If no, record crop value in nates section. Custody seals present and intact? _®, ; ._❑,.•-„ _❑_, is (including sample IDs, collect dalesltimes, and sampler name)? COC relingwshed and coni .. ___—_..___........ ... ..colo._.—._-.-..,..---._....... ® ❑ . Profile Number Receival By ..__ . _.... ples received? Short holds RUSH samples Short __. 80251 McCune, Dodie N. .colo __ _... _..........__ ... _.: ...... Alt containers received in good condition and within hold time? _-® ❑ _❑_ All sample labels and containers received match the chain of custody? ❑ Receive Date(s) _:_.. __. .. -._.. loll Preservation checked at receipt? Exce tions: VOC, Coliform, TOC, Oil and Grease. DOC +� Line Item(s) 34 - Waler-TOC/ 11/03/16 Preservative added to any containers? .. . ❑ ❑ MEE /Formaldehyde/8082 VO containers received with headspace < 6mm? VO _ _ .water ,.... _....... __.......--- loll- .... ...... ... Received filtered sample volume for dissolved analysis? ❑ ❑ Trip blank present in all coolers containing VOC waters? ❑ ❑ _ . _ll Samples collected in containers provided by GCAL? ❑ 0 ❑ DISCREPANCIES LAB PRESERVATIONS COOLERS Airbill Thermometer IQ: E25 Temp(°C) None None 777622636568 1.5 (VOTES Revision 1.5 Page 1 of 1 Lab Report#: 216110366 Revision 1 Page 16 of 16