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Home My WebLink AboutWQ0034880_Monitoring - 11-2016_20161222 (2)SUBMIT FORM ON YELLOW PAPER ONLY TER QUALITY MONITORING: E REPORT FORM Name: UNC COASTAL STUDIES INSTITUTE Name (if differe Address: PO BOX 689 / 850 NC 345, MANTEO NC 27954 County DARE act Person. IRVIN W. EDWARDS, JR Telephone#. 252 305.6956 Location/Site Name UNC CSI Noof wells to be sampled: 4 L ID NUMBER (from Permit): MW -1 Depth. 15 ft. i to Water Level 82546: 6.8 ,unng Point is ft. above land surface ne of water pumped/bailed before sampling: )les for metals were collected unfiltered: ❑ YES Date sample collected 11/11/2016 Well Diameter: 2 in. Screened Interval: 4.8 ft. to 15 ft. Relative M.P. Elevation: R. 5 gallons ❑ NO and field acidified: ❑ YES 'ARTMENT OF ENVIRONMENT b NATURAL RESOURCES 1SION OF WATER RESOURCES - INFORMATION PROCESSING UNIT 7 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-907-6306 RMIT Number: Expiration Date: 12/31/2016 n -Discharge WQ0034880 UIC 'DES Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other INFILTRATION PON FIELD ANALYSES: pH oo400. 7.3 units Spec. Cond. 00094. Odor 00085 _ Appearance Date sample analyzed 11/11/2016 Laboratory Name: ENVIRONMENTAL CHEMIST PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oo615 <0.02 mg/L Pb - Lead o1o51 Coliform: MF Fecal 31616 1 /100mL Nitrate (NO3) as N 00620 <0.02 mg/L Zn - Zinc 01092 Coliform: MF Total 31504 /100mL Phosphorus. Total as P o0665 mg/L N Temp. 000lr 21 2 °C DRY at µMhos time of SLIGHT CLEAR Certification No. 94 ug/L mg/L ( ole. Use MPH mallod brhg* Wrdtl sampes) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids. Total 70300 321 mg/L Al -Aluminum 01105 mg/L AMMONIA NITROGEN: 1.2 mg/L pH (Lab) 00403 7.29 units Ba - Barium 01007 ; ug/L NITRATE+NITRITE+NITROGEN: <0.02 ma/L Grease and Oils 00552 mg/L Cu - Copper 01042 r, Ifig/L TOC oo68o 5.5 mg/L Ca - Calcium 00916 mg/L "a Chloride oo94o 32 mg/L Cd - Cadmium 01027 %ug/L Arsenic 01002 ug/L Chromium. Total o1o34 o�^ glL Grease and Oils 00552 mg/L Cu - Copper 01042 r, Ifig/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ugfL Fe - Iron 01045 101- (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 —' yg& Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia ooslo mg/L Mg - Magnesium 00927 mg/L method # (Ammonu N&Wen: NH, as N: Amaronla NN n. Total) Mn - Manganese o1o55 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs. mg/L VOC Removal% IRVIN W. EDWARDS, JR. Permittee for Authorized AOent) Name and Title - Please print or Noe GW -59 Rev. 8/2013 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT 8 NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919,074306 FACILITY INFORMATION Prease Print Clearly or Type PERMIT Number: Expiration Date: 12/31/2016 Facility Name: UNC COASTAL STUDIES INSTITUTE Non -Discharge W00034880 UIC Permit Name (if different): D-1 NPDES Other Facility Address: PO BOX 689 / 850 INC 345, MANTEO NC 27954 TYPE OF PERMITTED OPERATION BEING MONITORED County DARE ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑ Spray Field ❑ Remediation: Contact Person: IRVIN W. EDWARDS, JR Telephone#: 252.305.6956 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name UNC CSI No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: INFILTRATION POND WELL ID NUMBER (from Permit): MW -2 Well Depth: 15 ft. Depth to Water Level 825,16: 7 Measuring Point is ft. above land surface Volume of water pumped/bailed before sampling: 5 Samples for metals were collected unfiltered: ❑ YES Date sample collected: 11/11/2016 Well Diameter: 2 in. Screened Interval: 4.8 ft. to 15 ft. Relative M.P. Elevation: ft. gallons ❑ NO and field acidified: ❑ YES ❑ NO FIELD ANALYSES: pH o0400-. 7 units Temp. 000lc 'C Spec. Cond. 00094 µMhos Odor 000s5: SLIGHT Appearance GREY WAS DRY at time of sampling, check here:❑ LABORATORY INFORMATION Phenol 32730 ug/L Fe - Iron o1o4s ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 Date sample analyzed. 11/11/2016 Hg - Mercury 71900 Laboratory Name: ENVIRONMENTAL CHEMIST Certification No. 94 µMhos PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. VOC 7873 method # Total Ammonia oo610 mg/L Mg - Magnesium 00827 COD 00335 mg/L Nitrite (NO2) as N 00615 0.07 mg/L Pb - Lead oios1 ug/L method # Coliform: MF Fecal 31a16 <1 /100mL Nitrate (NO3) as N 0oe2o <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total aS P 00665 mg/L (Note: Use MPN memod for hii eeeld samples) Orthophosphate 7oso7 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 7140 mg/L AI - Aluminum o11os mg/L AMMONIA NITROGEN: 73.6 mg/L pH (Lab) oo403 7.02 units Be - Barium 01007 ug/L NITRATE+NITRITE+NITROGEN: <0.02 mg/L TOC oorin 31.5 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 3760 mg/L Cd - Cadmium oio27 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o4s ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance Goose µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia oo610 mg/L Mg - Magnesium 00827 mg/L method # (AmmoNa Nitrogen; NH,ras N; Ammonia Nitrogen, Total) Mn - Manganese o1os5 ug/L method # TKN as N W625 mg/L Ni - Nickel 01067 ug/L . method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: IRVIN W. EDWARDS, JR. 7 Permittee (or Authorized Anent) Name and Title - Please Print or tvice Sionliture of Permittee (or GW -59 Rev. 812013 VOC Removal% SUBMIT FORM ON YELLOW PAPER ONLY FIELD ANALYSES: pH oo400: 6.5 units Temp. 0001C 211 IC Spec. Cond. Doo94: µMhos Odor 00055: SLIGHT Appearance LIGHT TAN WAS DRY at time of checksamplr check here: r L • . GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENT a NATURAL RESOURCES DMSIONOFWATERRESOURCES- INFORMATIONPROCESSINGUNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 276994617 Phone: 919-9076506 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 12/31/2016 Facility Name: UNC COASTAL STUDIES INSTITUTE Non -Discharge W00034880 NPDES UIC Other Permit Name (if different): Facility Address: PO BOX 689 / 850 NC 345, MANTEO NC 27954 TYPE OF PERMITTED OPERATION ❑ Lagoon BEING MONITORED ❑ Remediation: Infiltration Gallery County DARE mg/L ❑ Spray Field ❑ Remediation: Contact Person: IRVIN W. EDWARDS, JR Telephone#: 252.305.6956 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name UNC CSI No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: INFILTRATION POND ELL ID NUMBER (from Permit): MW -3 Date sample collected: 11/11/2016 ell Depth: 15 ft. „N O 2 G 17 Well Diameter: 2 in. apth to Water Level 82546: 9.1 Screened Interval: 4.8 ft. to 15 ft. aasuring Point is ft. above land surface Relative M.P. Elevation: ft. >Iume of water pumped/bailed before sampling: 5 gallons rm les for metals were collected unfiltered: ❑ YES El NO and field acidified: El YES El NO FIELD ANALYSES: pH oo400: 6.5 units Temp. 0001C 211 IC Spec. Cond. Doo94: µMhos Odor 00055: SLIGHT Appearance LIGHT TAN WAS DRY at time of checksamplr check here: r L 1BORATORY INFORMATION ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) rte sample analyzed: 11/11/2016 mg/L Laboratory Name: ENVIRONMENTAL CHEMIST Certification No. 94 ecific Conductance 00095 \RAMETERS NOTE: Values should reflect dissolved and colloidal concentrations, mg/L VOC 7873 method # Total Ammonia ooelo mg/L COD00335 mg/L Nitrite (NO2) as N Dosis <0.02 mg/L Pb - Lead o1o51 ug/L ug/L Coliform: MF Fecal 31616 1 /100mL Nitrate (NO3) as N Doom <0.02 mg/L Zn - Zinc oio92 mg/L Coliform: MF Total 31504 /100ml- Phosphorus: Total as P Doses mg/L (Nate: Use MPN metlnd/ hipvy WdMd samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): solved Solids:Total 70300 523 mg/L Al - Aluminum o11oe mg/L AMMONIA NITROGEN: 1.7 mg/L pH (Lab) 00403 6.52 units Ba - Barium oioo7 ug/L NITRATE+NITRITE+NITROGEN: <0.02 mg/L TOC oo6eo 26.7 mg/L Ca - Calcium oo916 mg/L Chloride oo94o 23 mg/L Cd - Cadmium o1o27 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper o1o42 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron o1o45 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) ecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia ooelo mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH�as N: AmmmW NWopn, TotM Mn - Manganese moss ug/L method # TKN as N oo625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% IRVIN W. EDWARDS, JR. Permittee (or Authorized Agent) Name and Title - Please print or tvoe GW -59 Rev. 812013 SUBMIT FORM ON YELLOW PAPER ONLY WELL ID NUMBER (from Permit): MW -4 Well Depth: 15 ft. Depth to Water Level e254e: 8.7 Measuring Point is ft. above land surface Volume of water pumped/bailed before sampling: 5 Samples for metals were collected unfiltered: ElYES rn = M..DIVISION GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENT 8 NATURAL RESOURCES OF WATER RESOURCES -INFORMATION PROCESSING UNIT WAS DRY at time of samplir check here: r L � COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phoft: 9192074306 uglL FACILITY INFORMATION F%asePrint ClearyorType PERMIT Number: Expiration Date: 12/31/2016 (Specify test and method X. ATTACH LAB REPORT.) Facility Name: UNC COASTAL STUDIES INSTITUTE Non -Discharge W00034880 UIC Permit Name (if different): Laboratory Name: NPDES Other CHEMIST Certification No. 94 Facility Address: PO BOX 689 / 850 INC 345, MANTEO NC 27954 TYPE OF PERMITTED OPERATION BEING MONITORED County DARE VOC 7873 method # ❑ Lagoon ❑ Remediation: Infiltration Gallery mg/L Mg - Magnesium 00927 ❑ Spray Field ❑ Remediation: mg/L Contact Person: IRVIN W. EDWARDS, JR Telephone#: 252.305.6956 ❑ Rotary Distributor ❑ Land Application of Sludge mg/L Well Location/Site Name UNC CSI No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: INFILTRATION POND WELL ID NUMBER (from Permit): MW -4 Well Depth: 15 ft. Depth to Water Level e254e: 8.7 Measuring Point is ft. above land surface Volume of water pumped/bailed before sampling: 5 Samples for metals were collected unfiltered: ElYES Date sample collected: 11/11/2016 hN 0 5 201' Well Diameter: 2 in. Screened Interval: 4.8 ft. to 15 ft. Relative M.P. Elevation: ft. gallons ❑ NO and field acidified: ❑ YES El NO FIELD ANALYSES: pH oo400. 6.4 units Temp. 000u 22.2 oC Spec. Cond. 00094 µMhos Odor Paws STRONG Appearance GREY WAS DRY at time of samplir check here: r L LABORATORY INFORMATION Phenol 32730 uglL Fe - Iron 01045 ug/L (Specify test and method X. ATTACH LAB REPORT.) Sulfate oos4s Date sample analyzed: 11/11/2016 Hg - Mercury 71900 Laboratory Name: ENVIRONMENTAL CHEMIST Certification No. 94 µMhos PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. VOC 7873 method # Total Ammonia ooelo mg/L Mg - Magnesium 00927 COD 00335 mg/L Nitrite (NO2) as N Do615 0.07 mg/L Pb - Lead o1o51 uglL method # Coliform: MF Fecal 31616 <1 /1OOmL Nitrate (NO3) as N ODS20 <0.02 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P ww5 mg/L (Nate: Um MPH metnodfor hV*kKW sampas) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Assolved Solids:Total 70300 578 mg/L AI - Aluminum o1105 mg/L AMMONIA NITROGEN: 8.8 mg/L pH (Lab) 00403 6.38 units Ba - Barium 01007 ugfL NITRATE+NITRITE+NITROGEN: <0.02 mg/L TOC Poem 30 mg/L Ca - Calcium oo916 mg/L Chloride oo94o 9 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total o1o34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 uglL Fe - Iron 01045 ug/L (Specify test and method X. ATTACH LAB REPORT.) Sulfate oos4s mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) ecific Conductance 00095 µMhos K - Potassium 00937 mgfL VOC 7873 method # Total Ammonia ooelo mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH3aa N; Ammonia Nitrogen. Tote? Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% IRVIN W. EDWARDS, JR. Pemtittee (or Authorized Agent) Name and Title - Please Print or Noe GW -59 Rev. 8/2013 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax SM. 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(alenvironmentalchemists.com East Carolina University Date of Report: Dec 01, 2016 1001 East 4th Street Manteo Report #: 16M-1956 Greenville NC 27858 Report #: 2016-16263 Attention: Patrick Sherrod Customer ID: 12110019 Project ID: UNC Coastal Studies -MW Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-39297 Site: MW -1 11/11/2016 9:00 AM Water Will Coggins Test Method Results Date Analyzed Color Color Clear 11/11/2016 Depth to water, ft. Depth to water. Ft. 6.8 feet 11/11/2016 Ammonia Nitrogen EPA 350.1 1.2 mg/L 11/15/2016 Nitrite Nitrogen EPA 353.2 <0.02 mg/L 11/23/2016 Sample analyzed outside of holding time Gallons bailed before sampling GalbnsBailed before sampling 5.0 gallons 11/11/2016 Odor Qualitative Slight 11111/2016 Total Dissolved Solids (TDS) SM2540C 321 mg/L 11/14/2016 Temperature sM2550B 21.2 C 11/11/2016 Chloride SM 4500 CIE 32 mg/L 11/17/2016 pH SM4500HB 7.29 units 11/11/2016 Total Organic Carbon (TOC) SM 5310 B 5.5 mg/L 11/15/2016 1,1,1,2 -Tetrachloroethane SM 6200C <0.50 Ng/L 11/19/2016 1,1,1 -Trichloroethane SM 6200C <0.50 yg/L 11/19/2016 1,1,2,2 -Tetrachloroethane SM 6200C <0.50 Ug/L 11119/2016 1,1,2 -Trichloroethane SM 6200C <0.50 U9/L 11/19/2016 1,1-Dichloroethane SM 6200C <0.50 Ng/L 11/19/2016 1,1-Dichloroethene SM 6200C <0.50 Ng/L 11/19/2016 1, 1 -Dichloropropene sM6200C <0.50 pg/L 11/19/2016 1,2,3-Trichlorobenzene SM 6200C <0.50 Ug/L 11/19/2016 1,2,3-Trichloropropane SM 6200C <0.50 pg/L 11/19/2016 1,2,4-Trichlorobenzene SM 6200C <0.50 Ng/L 11/19/2016 1,2,4-Trimethylbenzene SM 6200C <0.50 pg/L 11/19/2016 1,2-Dibromo-3-Chloropropane SM 6200C <0.50 pg/L 11/19/2016 1,2-Dibromoethane SM 6200C <0.50 pg/L 11/19/2016 1,2 -Dichlorobenzene SM 6200C <0.50 Ng/L 11/19/2016 1,2-Dichloroethane SM62000 <0.50 Vg/L 11/19/2016 1,2-Dichloropropane SM 6200C <0.50 Ng/L 11/19/2016 1,3,5-Trimethylbenzene SM 6200C <0.50 ug/L 11/19/2016 1,3 -Dichlorobenzene SM 6200C <0.50 Ug/L 11/19/2016 1,3-Dichloropropane SM 6200C <0.50 ug/L 11/19/2016 1,4 -Dichlorobenzene SM 6200C <0.50 Ng/L 11/19/2016 2,2-Dichloropropane SM6200c <0.50 ug/L 11/19/2016 Report #::2016-16263 Page 1 of 12 Environmental Chemists, Inc. t t B 6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM.. 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoCWenvironmentalchemistscom East Carolina University Date of Report: Dec 01, 2016 1001 East 4th Street Manteo Report #: 16M-1956 Greenville NC 27858 Report #: 2016-16263 Attention: Patrick Sherrod Customer ID: 12110019 Project ID: UNC Coastal Studies -MW 2-Chlorotoluene SM 6200C <0.50 ug/L 11/19/2016 4-Chlorotoluene SM 6200C <0.50 p9/L 11/19/2016 Benzene SM 6200C <0.50 Ng/L 11/19/2016 Bromobenzene sM6200C <0.50 Vg/L 11/19/2016 Bromochloromethane SM 62000 < 0.50 ug/L 11/19/2016 Bromodichloromethane SM 6200C <0.50 Ng/L 11/19/2016 Bromoform SM 8200C <0.50 Ng/L 11/19/2016 Bromomethane SM 6200C <0.50 pg/L 11/19/2016 Carbon tetrachloride SM 6200C < 0.50 ug/L 11/19/2016 Chlorobenzene SM 6200C <0.50 Ug/L 11/19/2016 Chloroethane SM 6200C <0.50 ug/L 11/19/2016 Chloroform SM62DOC <0.50 Ng/L 11/19/2016 Chloromethane SM 6200C <0.50 pg/L 11/19/2016 cis-1,2-Dichloroethene SM 6200C <0.50 Ng/L 11/19/2016 cis-1,3-Dichloropropene SM 6200C <0.50 pg/L 11/19/2016 Dibromochloromethane SM 6200C <0.50 Ng/L 11119/2016 Dibromomethane SM 6200C <0,50 pg/L 11/19/2016 Dichlorodifluoromethane sM62000 <0.50 Ng/L 11/19/2016 Ethylbenzene SM 6200C <0.50 Ng/L 11/19/2016 Hexachlorobutadiene SM 6200C <0.50 ug/L 11/19/2016 Isopropylbenzene SM 6200C <0.50 Ng/L 11/19/2016 M+P Xylene SM 6200C < 1.00 Ng/L 11/19/2016 Methylene chloride SM 62000 < 0.50 Ng/L 11/19/2016 Naphthalene SM 6200C <0.50 pg/L 11/19/2016 n-Butylbenzene SM 6200C <0.50 Ng/L 11/19/2016 n-Propylbenzene SM 6200C <0.50 ug/L 11/19/2016 ortho-Xylene SM 6200C <0.50 Ng/L 11/19/2016 p-Isopropyltoluene SM 6200c <0.50 ug/L 11/19/2016 sec-Butylbenzene SM 6200c <0.50 ug/L 11/19/2016 Styrene SM 6200C <0.50 Ng/L 11/19/2016 tert-Butylbenzene SM 6200C <0.50 yg/L 11/19/2016 Tetrachloroethene SM 6200C <0.50 ug/L 11/19/2016 Toluene SM 6200c <0.50 Vg/L 11/19/2016 Trans-1,2-Dichloroethene SM 6200C <0.50 ug/L 11/19/2016 Trans- l,3-dichloropropene SM 6200C <0.50 Ng/L 11/19/2016 Trichloroethene SM 6200C < 0.50 Ng/L 11/19/2016 Report #::2016-16263 Page 2 of 12 Environmental Chemists, Inc. / 4 ' 1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax M 255-A Wilmington Highway, Jacksonville, NC 28540 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com East Carolina University Date of Report: Dec 01, 2016 1001 East 4th Street Manteo Report #: 16M-1956 Greenville NC 27858 Report #: 2016-16263 Attention: Patrick Sherrod Customer ID: 12110019 Project ID: UNC Coastal Studies -MW Trichlorofluoromethane SM 8200C <0.50 u9/L 11/19/2016 Vinyl chloride SM 6200C <0.50 U9/L 11/19/2016 Nitrate Nitrogen (Calc) Nitrate+Nitrite-Nitrogen EPA 353.2 <0.02 mg/L 11/14/2016 Nitrate Nitrogen SubtractenMO#M <0.02 mg/L 11/28/2016 Report #::2016-16263 Page 3 of 12 Environmental Chemists, Inc. 4 ' t - & 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax M. 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL 8 CONSULTING CHEMISTS info@environmentalchemists.com East Carolina University Date of Report: Dec 01, 2016 1001 East 4th Street Manteo Report #: 16M-1956 Greenville NC 27858 Report M 2016-16263 Attention: Patrick Sherrod Customer ID: 12110019 Project ID: UNC Coastal Studies -MW Lab ID Sample ID: Collect DateMme Matrix Sampled by 16-39298 Site: MW -2 11/11/2016 8:50 AM Water Will Coggins Test Method Results Date Analyzed Color Color Grey 11/11/2016 Depth to water, ft. Depth to water. Ft. 7.0 feet 11/11/2016 Ammonia Nitrogen EPA 350.1 73.6 mg/L 11/16/2016 Nitrite Nitrogen EPA 353.2 0.07 mg/L 11/23/2016 Sample analyzed outside of holding time Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/11/2016 Odor Qualitative Slight 11/11/2016 Total Dissolved Solids (TDS) SM2540C 7140 mg/L 11/14/2016 Temperature SM2550B 17.3 C 11/11/2016 Chloride SM 4500 CIE 3760 mg/L 11/17/2016 pH SM4500HB 7.02 units 11/11/2016 Total Organic Carbon (TOC) SM 5310 B 31.5 mg/L 11/15/2016 1,1,1,2 -Tetrachloroethane SM62000 <0.50 Ng/L 11/19/2016 1,1,1 -Trichloroethane SM62000 <0.50 pg/L 11/19/2016 1,1,2,2 -Tetrachloroethane SM 6200C <0.50 pg/L 11/19/2016 1,1,2 -Trichloroethane SM 6200C <0.50 pg/L 11/19/2016 1,1-Dichloroethane SM 8200C <0.50 Ng/L 11/19/2016 1,1-Dichloroethene SM 6200C <0.50 pg/L 11/19/2016 1,1-Dichloropropene SM 6200C <0.50 pg/L 11/19/2016 1,2,3-Trichlorobenzene SM 6200C <0.50 pg/L 11/19/2016 1,2,3-Trichloropropane SM 6200C <0.50 Ug/L 11/19/2016 1,2,4-Trichlorobenzene SM6200C <0.50 Ng/L 11/19/2016 1,2,4-Trimethylbenzene SM 6200C <0.50 pg/L 11/19/2016 1,2-Dibromo-3-Chloropropane SM 6200C <0.50 Ng/L 11/19/2016 1,2-Dibromoethane SM 8200C <0.50 pg/L 11/19/2016 1,2 -Dichlorobenzene SM620OC <0.50 pg/L 11/19/2016 1,2-Dichloroethane SM 6200C <0.50 Ng/L 11/19/2016 1,2-Dichloropropane SM 8200C <0.50 pg/L 11/19/2016 1,3,5-Trimethylbenzene SM 8200C <0.50 pg/L 11/19/2016 1,3 -Dichlorobenzene SM 6200C <0.50 pg/L 11/19/2016 1,3-Dichloropropane SM 6200C <0.50 Ng/L 11/19/2016 1,4 -Dichlorobenzene SM 6200C <0.50 pg/L 11/19/2016 2,2-Dichloropropane SM62000 <0.50 pg/L 11/19/2016 Report M, 2016.16263 Page 4 of 12 Environmental Chemists, Inc. • Y '-4", till 6602 Windmi6 Way, Wilmhigton, NC 28405 • 910.3920223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoCaenvironmentalchemismcom East Carolina University Date of Report: Dec 01, 2016 1001 East 4th Street Mantso Report #: 16M-1956 Greenville NC 27858 Report M 2016-16263 Attention: Patrick Sherrod Customer ID: 12110019 Project ID: UNC Coastal Studies -MW 2-Chlorotoluene SM62ooc <0.50 Ng/L 11/19/2016 4-Chlorotoluene SM 6200C <0.50 ug/L 11/19/2016 Benzene SM 6200C <0.50 lag/L 11/19/2016 Bromobenzene SM 6200C <0.50 ug/L 11/19/2016 Bromochloromethane SM 6200C <0.50 ug/L 11/19/2016 Bromodichloromethane SM 6200C <0.50 pg/L 11/19/2016 Bromoform SM 6200C <0.50 Ng/L 11/19/2016 Bromomethane SM 6200C <0.50 Ng/L 11/19/2016 Carbon tetrachloride SM 8200C <0.50 pg/L 11/19/2016 Chlorobenzene SM 6200C <0.50 ug/L 11/19/2016 Chloroethane SM 6200C <0.50 Ng/L 11119/2016 Chloroform SM 6200C <0.50 ug/L 11/19/2016 Chloromethane SM 6200C <0.50 Ng/L 11/19/2016 cis-1,2-Dichloroethene SM 6200C <0.50 Ng/L 11/19/2016 cis-1,3-Dichloropropene SM 6200C <0.50 pg/L 11/19/2016 Dibromochloromethane SM 5200C < 0.50 NgIL 11/19/2016 Dibromomethane SM 8200C <0.50 Ng/L 11/19/2016 Dichlorodifluoromethane SM 6200C <0.50 Ng/L 11/19/2016 Ethylbenzene SM 62000 < 0.50 Ng/L 11/19/2016 Hexachlorobutadiene SM 6200C <0.50 Ng/L 11/19/2016 Isopropylbenzene SM 6200C <0.50 Vg/L 11/19/2016 M+P Xylene SM 6200C < 1.00 Ng/L 11/19/2016 Methylene chloride SM 62000 < 0.50 Ng/L 11/19/2016 Naphthalene SM 6200C <0.50 NgIL 11/19/2016 SM 62000 < 0.50 ug/L 11/19/2016 n-Butylbenzene SM 6200C <0.50 Ng/L 11/19/2016 n-Propylbenzene SM 62000 < 0.50 ug/L 11119/2016 ortho-Xylene p-Isopropyltoluene SM 6200C <0.50 NgIL 11/19/2016 sec-Butylbenzene SM 6200C <0.50 pg/L 11/19/2016 SM 6200C <0.50 NgIL 11/19/2016 Styrene SM 6200C <0.50 ug/L 11/1912016 tert-Butylbenzene SM 6200C < 0.50 Ng/L 11/19/2016 Tetrachloroethene SM 6200C <0.50 NgIL 11/1912016 Toluene Trans-1,2-Dichloroethene SM 6200C <0.50 ug/L 11119/2016 Trans-1,3-dichloropropene SM 6200C <0.50 Ng/L 11/19/2016 Trichloroethene SM 6200C <0.50 Ng/L 11/19/2016 Page 5 of 12 Report #::2016-16263 Environmental Chemists, Inc. 4 S 1 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28,540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemists.com East Carolina University Date of Report: Dec 01, 2016 1001 East 4th Street Manteo Report #: 16M-1956 Greenville NC 27858 Report #: 2016-16263 Attention: Patrick Sherrod Customer ID: 12110019 Project ID: UNC Coastal Studies -MW Trichlorofluoromethane SM 6200C < 0.50 ug/L 11119/2016 Vinyl chloride SM 6200C < 0.50 pg/L 11/19/2016 Nitrate Nitrogen (Calc) Nitrate+Nitrite-Nitrogen EPA 353.2 <0.02 mg/L 11/14/2016 Nitrate Nitrogen Subtraction Method <0.02 mg/L 11/28/2016 Report #::2016-16263 Page 6 of 12 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL R CONSULTING CHEMISTS infoC4)environmentalchemistscom East Carolina University Date of Report: Dec 01, 2016 1001 East 4th Street Manteo Report #: 16M-1956 Greenville NC 27858 Report #: 2016-16263 Attention: Patrick Sherrod Customer ID: 12110019 Project ID: UNC Coastal Studies -MW Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-39299 Site: MW -3 11/11/2016 9:10 AM Water Will Coggins Test Method Results Date Analvzed Color Color Light Tan 11/11/2016 Depth to water, ft. Depth to Water, Ft. 9.1 feet 11/11/2016 Ammonia Nitrogen EPA 350.1 1.7 mg/L 11115/2016 Nitrite Nitrogen EPA 353.2 < 0.02 mg/L 11/23/2016 Sample analyzed outside of holding time Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/11/2016 Odor Qualitative Slight 11/11/2016 Total Dissolved Solids (TDS) SM 2540 C 523 mg/L 11/14/2016 Temperature SM 25508 21.7 C 11/11/2016 Chloride SM45o0ClE 23 mg/L 11/17/2016 pH SM4500HB 6.52 units 11/11/2016 Total Organic Carbon (TOC) SM 5310 a 26.7 mg/L 11/15/2016 1,1,1,2 -Tetrachloroethane SM 6200C <0.50 Ng/L 11/19/2016 1,1,1 -Trichloroethane SM 6200C <0.50 pg/L 11/19/2016 1,1,2,2 -Tetrachloroethane SM 6200C <0.50 pg/L 11/19/2016 1,1,2 -Trichloroethane SMe200c <0.50 Ng/L 11/19/2016 1,1-Dichloroethane SM 6200C <0.50 pg/L 11/19/2016 1,1-Dichloroethene sM6200c <0.50 pg/L 11/19/2016 1,1-Dichloropropene SM 6200C <0.50 Ug/L 11/19/2016 1,2,3-Trichlorobenzene SM 6200C <0.50 pg/L 11/19/2016 1,2,3-Trichloropropane SM 13200C <0.50 Ng/L 11/19/2016 1,2,4-Trichlorobenzene SM 6200C <0.50 Ng/L 11/19/2016 1,2,4-Trimethylbenzene SM 6200C <0.50 Ng/L 11/19/2016 1,2-Dibromo-3-Chloropropane SM 6200C <0.50 ug/L 11/19/2016 1,2-Dibromoethane SM 6200c <0.50 {lg/L 11/19/2016 1,2 -Dichlorobenzene SM 6200C <0.50 Ng/L 11/19/2016 1,2-Dichloroethane SM 6200C <0.50 Ng/L 11/19/2016 1,2-Dichloropropane SM 6200C <0.50 ug/L 11/19/2016 1,3,5-Trimethylbenzene SM 6200C <0.50 Ng/L 11/19/2016 1,3 -Dichlorobenzene SM 6200C <0.50 pg/L 11/19/2016 1,3-Dichloropropane SM 6200C <0.50 U9/L 11/19/2016 1,4 -Dichlorobenzene SM 6200C <0.50 Ng/L 11/19/2016 2,2-Dichloropropane SM 6200C <0.50 pg/L 11/19/2016 Report #::2016-16263 Page 7 of 12 Environmental Chemists, Inc. 9e7mA 6602 Windmill Way, Wilmington, NC 28405 • 910.3920223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Mantra, NC 27954 • 252.473.5702 Lab/Fax s" 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(ritenvironmentalchemists.com East Carolina University Date of Report: Dec 01, 2016 1001 East 4th Street Manteo Report #: 16M-1956 Greenville NC 27858 Report #: 2016-16263 Attention: Patrick Sherrod Customer ID: 12110019 Project ID: UNC Coastal Studies -MW 2-Chlorotoluene sM6200C <0.50 pg/t. 11/19/2016 4-Chlorotoluene SM 6200C <0.50 N9/L 11/19/2016 Benzene SM 6200C <0.50 Ng/L 11/19/2016 Bromobenzene SM 6200C <0.50 ug/L 11/19/2016 Bromochloromethane SM8200c <0.50I1g/L 11/19/2016 Bromodichloromethane SM 6200C <0.50 Ng/L 11/19/2016 Bromoform SM 6200C <0.50 Ng/L 11/19/2016 Bromomethane SM 6200C <0.50 ug/L 11/19/2016 Carbon tetrachloride SM 62000 < 0.50 Ng/L 11/19/2016 Chlorobenzene SM 6200C <0.50 NgIL 11/19/2016 Chloroethane SM 6200C <0.50 Ng/L 11/19/2016 Chloroform SM 6200C <0.50 Vg/L 11/19/2016 Chloromethane SM620DC <0.50 Ng/L 11/19/2016 cis- 1, 2-Dichloroethene SM 6200C <0.50 yg/L 11/19/2016 cis-1,3-Dichloropropene SM 6200C <0.50 pg/L 11/19/2016 Dibromochloromethane SM 6200C <0.50 Ng/L 11/19/2016 Dibromomethane SM 6200C <0.50 Ng/L 11/19/2016 Dichlorodifluoromethane SM62DOC <0.50 Vg/L 11/19/2016 Ethylbenzene SM62MC <0.50 pg/L 11/19/2016 Hexachlorobutadiene SM 6200C <0.50 pg/L 11/19/2016 Isopropylbenzene SM 6200C <0.50 NgIL 11/19/2016 M+P Xylene SM 6200C < 1.00 NgIL 11/19/2016 Methylene chloride SM 62000 < 0.50 ug/L 11/19/2016 Naphthalene SM 62000 < 0.50 pg/L 11119/2016 n-Butylbenzene SM 62000 < 0.50 ug/L 11/19/2016 n-Propylbenzene SM6200C <0.50 NgIL 11/19/2016 Ortho -Xylene SM 6200C < 0.50 pg/L 11/19/2016 p-Isopropyltoluene SM82ODC <0.50 Ug/L 11/19/2016 sec-Butylbenzene SM 6200C <0.50 u9/L 11/19/2016 Styrene SM 6200C <0.50 Ng/L 11/19/2016 tert-Butylbenzene SM6200C <0.50 Ng/L 11/19/2016 Tetrachloroethene SM 62000 < 0.50 ug/L 11119/2016 Toluene SM 6200C < 0.50 pg/L 11/19/2016 Trans-1,2-Dichloroethene SM 6200C <0.50 pg/L 11/19/2016 Trans-1,3-dichloropropene SM62WC <0.50 Ng/L 11/19/2016 Trichloroethene SM 62000 < 0.50 ug/L 11/19/2016 Report # 2016-16263 Page 8 of 12 Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(aenvironmentalchemists.com East Carolina University Date of Report: Dec 01, 2016 1001 East 4th Street Manteo Report #: 16M-1956 Greenville NC 27858 Report M 2016-16263 Attention: Patrick Sherrod Customer ID: 12110019 Project ID: UNC Coastal Studies -MW Trichlorofluoromethane SM 52000 < 0.50 u9/L 11/19/2016 Vinyl chloride SM 6200C 4 0.50 Ng/L 11/19/2016 Nitrate Nitrogen (Calc) Nitrate+Nitrite-Nitrogen EPA 3532 <0.02 mg/L 11/14/2016 Nitrate Nitrogen Subtraction Method 40.02 mg/L 11/28/2016 Report #::2016-16263 Page 9 of 12 Environmental Chemists, Inc. 01 0A I oigftjv:-�4116602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 8owsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax SM 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS infoCatienvironmentalchemists.com East Carolina University Date of Report: Dec 01, 2016 1001 East 4th Street Manteo Report #: 16M-1956 Greenville NC 27858 Report M 2016-16263 Attention: Patrick Sherrod Customer ID: 12110019 Project ID: UNC Coastal Studies -MW Lab ID Sample ID: Collect Date/Time Matrix Sampled by 16-39300 Site: MW -4 11/11/2016 9:20 AM Water Will Coggins Test Method Results Date Analyzed Color Depth to water, ft. Ammonia Nitrogen Nitrite Nitrogen Sample analyzed outside of holding time Gallons bailed before sampling Odor Total Dissolved Solids (TDS) Temperature Chloride pH Total Organic Carbon (TOC) 1,1,1,2 -Tetrachloroethane 1,1,1 -Trichloroethane 1,1,2,2 -Tetrachloroethane 1,1,2 -Trichloroethane 1,1-Dich loroethane 1,1-Dichioroethene 1,1-Dichloropropene 1, 2, 3-Trichlorobenzene 1,2, 3-Trichloropropane 1,2,4-Trichlorobenzene 1,2,4-Trimethylbenzene 1,2-Dibromo-3-Chloropropane 1,2-Dibromoethane 1,2 -Dichlorobenzene 1, 2-Dichloroethane 1,2-Dichloropropane 1, 3,5-Trimethylbenzene 1,3 -Dichlorobenzene 1,3-Dichloropropane 1,4 -Dichlorobenzene 2,2-Dichloropropane Color Depth to water, Ft. EPA 350,1 EPA 353.2 Gallons Bailed before sampling Qualitative SM 2540 C SM 2550 8 SM 4500 CI E SM 4500 H 8 SM 5310 8 SM 6200C SM 62000 SM 6200C SM 6200C SM 62000 SM 62000 SM 62000 SM 6200C SM 6200C SM 6200C SM 62000 SM 62000 SM 6200C SM 6200C SM 6200C SM 6200C SM 62000 SM 6200C SM 6200C SM 6200C SM 62000 Grey 8.7 feet 8.8 mg/L 0.07 mg/L 5.0 gallons Strong 578 mg/L 22.2 C 9 mg/L 6.38 units 30.0 mg/L < 0.50 Ng/L < 0.50 ug/L < 0.50 Ng/L < 0.50 Ng/L < 0.50 pg/L < 0.50 Ng/L < 0.50 Ng/L < 0.50 pg/L < 0.50 pg/L < 0.50 pg/L < 0.50 pg/L * 0.50 pg/L 0.50 ug/L < 0.50 Ng/L < 0.50 pg/L < 0.50 pg/L < 0.50 pg/L < 0.50 ug/L a 0.50 ug/L < 0.50 ug/L < 0.50 ug/L 11/11/2016 11/11/2016 11/16/2016 11/23/2016 11/11/2016 11/11/2016 11/14/2016 11/11/2016 11/17/2016 11/11/2016 11/15/2016 11/19/2016 11/19/2016 11/19/2016 11/19/2016 11/19/2016 11/19/2016 11/19/2016 11/19/2016 11/19/2016 11/19/2016 11/19/2016 11/19/2016 11/19/2016 11/19/2016 11/19/2016 11119/2016 11/19/2016 11/19/2016 11/19/2016 11/19/2016 11/19/2016 Report #::2016-16263 Page 10 of 12 Environmental Chemists, Inc. W' gam' 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 'm 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347 5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info(l)environmentalchemists,com East Carolina University Date of Report: Dec 01, 2016 1001 East 4th Street Manteo Report #: 16M-1956 Greenville NC 27858 Report M 2016-16263 Attention: Patrick Sherrod Customer ID: 12110019 Project ID: UNC Coastal Studies -MW 2-Chlorotoluene sM62000 <0.50 pg/L 11/19/2016 4-Chlorotoluene SM 6200C <0.50 pg/L 11/19/2016 Benzene SM6200C <0.50 pg/L 11/19/2016 Bromobenzene SM 6200C <0.50 p9/L 11/19/2016 Bromochloromethane SM 6200C <0.50 pg/L 11/19/2016 Bromodichloromethane SM 8200C <0.50 pg/L 11/19/2016 Bromoform SM 6200C <0.50 pg/L 11/19/2016 Bromomethane SM62DOC <0.50 pg/L 11/19/2016 Carbon tetrachloride SM620DC <0.50 pg/L 11/19/2016 Chlorobenzene SM 6200C <0.50 pg/L 11/19/2016 Chloroethane SM6200C <0.50 pg/L 11/19/2016 Chloroform SM620DC <0.50 pg/L 11/19/2016 Chloromethane SM62000 <0.50 pg/L 11/19/2016 cis-1,2-Dichloroethene SM 6200C <0.50 pg/L 11/19/2016 cis-1,3-Dichloropropene SM 6200C <0.50 pg/L 11/19/2016 Dibromochloromethane SM 6200C <0.50 pg/L 11/19/2016 Dibromomethane SM 6200C <0.50 pg/L 11/19/2016 Dichlorodifluoromethane SM 6200C <0.50 pg/L 11119/2016 Ethylbenzene SM620DC <0.50 pg/L 11/19/2016 Hexachlorobutadiene SM 6200C <0.50 pg/L 1111912016 Isopropylbenzene sM6200C < 0.50 pg/L 11/19/2016 M+P Xylene SM 6200C < 1.00 pg/L 11/19/2016 Methylene chloride SM 6200C <0.50 pg/L 11/19/2016 Naphthalene SM 6200C <0.50 pglL 11/19/2016 n-Butylbenzene SM620DC <0.50 pg/L 11/19/2016 n-Propylbenzene SM620DC <0.50 pg/L 11/19/2016 ortho-Xylene SM 62000 < 0.50 pg/L 11/19/2016 p-Isopropyltoluene SM 6200C <0.50 pg/L 11/19/2016 sec-Butylbenzene SM 6200C <0.50 pg/L 11/19/2016 Styrene SM 62000 < 0.50 pg/L 11119/2016 tert-Butylbenzene SM 02000 < 0.50 pg/L 11119/2016 Tetrachloroethene SM62000 <0.50 pg/L 11/19/2016 Toluene SM 6200C <0.50 pg/L 11/19/2016 Trans-1,2-Dichloroethene SM 6200C <0.50 pg/L 11/19/2016 Trans-1,3-dichloropropene SM 6200C <0.50 pg/L 11/19/2016 Trichloroethene SM 6200C <0.50 pg/L 11/19/2016 Report #':2016-16263 Page 11 of 12 IEnvironmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 26405 • 910.392.U223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS inro(ryenvironmentalchemists.com East Carolina University Date of Report: Dec 01, 2016 Matrix 1001 East 4th Street Manteo Report #: 16M-1956 11/11/2016 9:00 AM Greenville NC 27858 Report #: 2016-16263 Test Attention: Patrick Sherrod Customer ID: 12110019 Results Date Analyzed Fecal Coliform Project ID: UNC Coastal Studies -MW Trichlorofluoromethane SM 8200C <0.50 Ng/L 11/19/2016 Vinyl chloride SM 6200C < 0.50 u9/L 11/19/2016 Nitrate Nitrogen (Cale) 11/11/20168:50AM Water Nitrate+Nitrite-Nitrogen EPA 353.2 <0.02 mg/L 11/14/2016 Nitrate Nitrogen SubbachonMethod <0.02 mg/L 11/28/2016 Lab ID Sample ID: M-3829 Collect DatelTime Matrix Sampled by 16-39301 Site: MW -1 11/11/2016 9:00 AM Water Will Coggins Test Method Results Date Analyzed Fecal Coliform SM9222DMF 1 Colonies/100mL 11/11/2016 Lab ID Sample ID: M-3830 Collect Date/Time Matrix Sampled by 16-39302 Site: MW -2 11/11/20168:50AM Water Will Coggins Test Method Results Date Analyzed Fecal Coliform SM9222DMF <1 Colonies/tOOmL 11/11/2016 Lab ID Sample ID: M-3831 Collect DatelTime Matrix Sampled by 16-39303 Site: MW -3 11/11/2016 9:10 AM Water Will Coggins Test Method Results Date Analyzed Fecal Coliform SM9222DMF 1 Colonies/1O0mL 11/11/2016 Lab ID Sample ID: M-3832 Collect DaterTime Matrix Sampled by 16-39304 Site: MW -4 11/11/2016 9:20 AM Water Will Coggins Test Method Results Date Analyzed Fecal Coliform SM9222DMF <1 Colonies/1OOmL 11/11/2016 Comment: Reviewed by Report #::2016-16263 Page 12 of 12 Analylh:ul a Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION 6 94 NCDHHS: DLS CERTIFICATION X 37729 COLLECTION AND CHAIN OF CUSTODY 6602 Windmill Way Wllmin9ton, NC 26a OFFICE: 910-392.0223 FAX 9110492.44: i nfo@envimmnemalche raiste.Com Client: East Carolina University PROJECT NAME: UNC Coastal Studies Institute REPORT NO: XO rlr ADDRESS: 1001 East 4th Street CONTACT NAME: Monitoring Wells Dare Count Site Patrick: 252.328.4045 or 252.916.4494 Greenville, NC 27858 REPORT TO: Patrick Sherrod, Facilities Services PHONE (Junior); 252.305.6956 Tam COPY TO: Junior Edwards, Atlantic qqdtEig2und JOBX emall: sherrodp@ecu.edu Sampled 6v: ✓I I 110 0 4d7l C SAMPLE TYPE: I e Influent. E = Effluent. W = Well, ST = Stream, 50 = Soil, SL = Sludge, Other: Sample Identification Collection �1 F �Y k _ fi 3 6 u u _ 9 ] PRESERVATION ANALYSIS REQUESTED Date Time Tam �w r Well: 1 22' C P X Chloride, NO2 TDS —I 1 V G G �1 Depth to water: t� C P X NO3 NH3 G G Gallons Bailed: C P X Fecal Coliform G G H (field): U C P X TOC G G �Ihl� field odor/color: 1' C P G G V / C P X VOC's November only) G 1 G C P G G G P G G C P G G Total of 4 welt to be collected In a6rdl, July, November. Well sit on HWy 34S Wenctwse, NC. Transfer Relinquished By: Dato/Time Received BY: DatelTimo 2. Temperature when IlMil Delivered By: Received Analytical t: Comullinc Chemists ENVIRONMENTAL CHEMISTS, INC NCDF.NR' DWQ CERTIFICATION 094 NCDHHS: DLS CERTIFICATION 0 37729 COLLECTION AND CHAIN OF CUSTODY 0002 Windmill Way Wilmington, NC 2041 OFFICE: 910392-0223 FAX 910.392-44: InfollIlenvlronmenteichemists.co n Client: East Carolina University PROJECT NAME: UNC Coastal Studies Institute REPORT NO: 16 /), / �l Sl ADDRESS: 1001 East 4th Street CONTACT NAME: Monitoring Wells Dare Count Site Patrick: 252.328.4046 or 252.916.4494 Greenville, NC 27658 REPORT TO: Patrick Sherrod, Facilities Services PHONE (Junior): 252.305.6956 ANALYSIS REQUESTED COPY TO: Junior Edwards Atlantic Underground OBX email: shaffodp@ecu.edu Sampled Bv: V1 1 11 *IS SAMPLE TYPE: I - Influent. E = Effluent, W = Well, ST = Stream, SO = Sall, SL = Sludge, Other: Sample Identification Collection r g E 5 s `o i c o s PRESERVATION ANALYSIS REQUESTED Date Time Tem r x y Well: ZI rd�N X Chloride NO2. Ms TFl a G G f 1/ Depth to water: (� C P �y n� ' X L NO3 NH3 G G Gallons Balled: C P X Fecal Coliform G G H field le C P X TOC G G field odor/color: /1411 C P G G 1 / y{ C P X VOCs November only) G G C P G G C P G G C P G G Taal of 4 wNk to be collected In Mvoh, duly, November. Well Site an Hwy 315 WancheOE N0. Trander Relin wished B : Dale(Time Received By: DatefTime a if Cc 2. Temperature when i Delivered By. Received Analytical d Consulting Chemists ENVIRONMENTAL CHEMISTS, INC NCDENR: DWO CERTIFICATION N 04 NCDHHS: DLS CERTIFICATION • 37729 rM 1 09 -Thal Aaln CHAIN nF CUSTODY 6602 Wlndmid Way Wltndngton, NC 2841 OFFICE: 910-392-0223 FAX 910.392-447 Info@enyironmentalchemistb.carn Client: East Carolina University PROJECT NAME: UNC Coastal Studies Institute REPORT NO: ADDRESS: 1001 East 4th Street CONTACT NAME: Monitoring Wells Dare County Sit2L Patrick: 262.328.4046 or 252.916.4494 Greenville, NC 27858 REPORT TO: Patrick Sherrod, Facilities Services PHONE (Junior): 252.305.6956 Tem COPY TO: Junior Edwards, Atlantic Under round OBX email: sherrod ecu.edu ev — es.e.... en s: nmi sL = smaoe. Omer: Sampled By: W . .if Sample Identification 2anmr" Collection , . r&. J! , - .,... �.,.. - ...__... ..-•.• - - PRE . , . SERVATION ANALYSIS REQUESTED Data Time Tem Well: -2, ,I C] �' 07 X Chloride NO2, TDS G G De th to water. l� X NO3, NH3 G G Gallons Bailed: C P X Fecal Coliform G G H (field): t% C P X TOC G G C P field odor/color: 5I1'111� G G y C P X VOC's November ont G G C P G G C P G G C P G G Tetel of 4 W els to be wllected M NOrch, July, November. W W site on Nwy 34/ Wam:hsss, NC. Transfer Relinquished By: DaterrimsRec ved By: Daterrime 2' n,. ..lo On c�4ur1• Temperature when Received: LS • I Acceprea: Inal 14169Y. -•••r •- • -' Delivered By: Received By T t2 ��-� Dater �1O I o r tun Time: ENVIRONMENTAL CHEMISTS, INC NCDENR: DWQ CERTIFICATION 0 91 NCDHHS: CLS CERTIFICATION Y 37729 Analytical $ Consulang ChCMISts COLLECTION AND CHAIN OF CUSTODY 1001 NC 27858 Junior 6602 Windmill Way Wilmington, NC 2811 OFFICE: 910.392.0223 FAX 010.30241: Infa@envifonmsntatchemlata.com _., �_ co... sn = snit SL = Sludoe. Other: I B tification i% Collection 5ArAl'1-t a € 'i C I Tre: s P I -a mmmm, ! e c — o m ° g �.,. PRESERVATION — •--" —' -- ANALYSIS REQUESTED Ch do, NO2, TOS NO3. NH3 Fecal , NI -1 nn w $ X a XC � s X o; Date Time Tem ? 1" t V G GG G P 2 gjCP r. 4 : ")G 0.- G X TOC (� / C P 4 fieldodoricolor; field G G VOCs Novemtleron MG Total at ♦ Weds to be colleatod In M Ch. Adyl Nowmber. Wen ua on Hwy 344 Wanohesq No. Rees ed By: DaleRlme Transfer Reh wished FIX: DatelThne 1. 2• o .e I. Resamole Requested: Temperature when Receive(]: 1 ^UU VjJ.W..• c Delivered By: Received By:J Z 0 rn 0 W 00 W M 4-1