NC0024406_Supplemental Permit Modification Request_20161104

(� DUKE
ENERGY
November 4, 2016
Mr. Jeff Poupart
NC Division of Water Resources
1617 Mail Service Center
Raleigh, NC 27699-1617
Subject: Duke Energy Carolinas, LLC (Duke Energy)
Belews Creek Steam Station
NPDES Permit No. NCO024406
Stokes County
Supplemental Permit Modification Request
Dear Mr. Poupart:
Harry K. Sideris
Senior Vice President
Environmental, Health & Safety
526 S. Church Streei
Mail Code: ECUP
Charlotte, NC 28202
[phone]
Lq
NOV 7 2016 t
Qlti`1S10N OF WATER
D18ECTOW� z RESOURCES
Duke Energy Carolinas LLC, (Duke Energy) requests the subject permit be modified to address
previously identified stormwater outfall SWO02 as a new NPDES outfall. This flow was referenced in
correspondence of the North Carolina Department of Environmental Quality in a letter dated September
19, 2014 (attached). At that time, Duke Energy indicated that this outfall would be removed from the
stormwater permit application and included in a subsequent amendment to the NPDES wastewater permit.
The contributing flows to this outfall are once through, non -contact chiller water and stormwater. The
stormwater drainage is approximately 3.8 acres and includes retired smokestacks in the northern portion
of the plant yard adjacent to the FGD. The entire drainage area is paved or roofed. Outfall SWO02
discharges to Belews Reservoir.
Enclosed are three copies of the completed EPA Form 1 and 2C, which have been updated to include this
outfall. Also, included are a Site Map showing the location of all Outfalls (internal and final), and a Site
Plan Stormwater locations.
Should you have ny questions regarding this submittal, please contact Joyce Dishmon at 336-623-0238.
arry Sideris
Duke Energy
Senior Vice President Environment, Health & Safety
Attachments
cc: Reginald Anderson, GM II Regulated Stations
Keeley McCormick, EHS Professional II
Joyce Dishmon, Sr. Env Specialist
Sergei Chernikov-NC DWR
1617 Mail Service Center
Raleigh, NC 27699-1617

DUKE
'ENERG
-September 19, 2014
Mr. Bradley Bennett
State of' North Carolina
Department of Environment, and Natural Resources
Division of Energy, Mineral & Land Resources
StormWater Permitting Program,
1612 Mail SerVice Center
Raleigh, NC 27699-1612,
Subject: Belews Creek Steam Station
NPDES Stormwatef Permit Application
Duke Energy Response to Additional, Information .Request
Dear Mr: Bennett;
Environmental Services
'Duke Energy.
526 South Church Street
Charlotte, NC ,28202
Mailing Address: -
Mall Code EC1 W P.O. Box 1006
Charlotte, NC 28201-1006
Duke Energy Carolinas, LLC (Duke Energy) presents the following information to the North
Carolina Department of Environment.and Natural Resources (NCDENR) — Division of Energy,
Mineral, and, Land Minerals in response to NCDENR's request for additional information dated
August 26, 2014.. The request was, submitted "following Duke Energy's August 1, 2014 submittal
of a National Pollutant Discharge Elimination System (NPDES) stormwater permit application for
the Belews' Creek Steam Station -located in Stokes County, North Carolina.
For ease of reference, NCDENR's excerpted queries appear in italics below, followed by Duke
Energy's (DE) associated response.
NCDENR Request is Analytical sampling results. were provided for stormwater discharges
from a July 15, 2014, rain event. Outfalls SW002; SWO06, and SW015
were sampled. No results for any other outfalls were provided. Dur
understanding was that Duke would follow the same format as the
Riverbend application in subsequent application submittals, including
sample results from all stormwater discharge,outfalls. We understand
only these -three were sampled in part,based on inaccessibility of some
other outfalls: However, we had discussed during an on-site- visit on July
30, .2014, an. arrangement for the sampling of additional outfalls ff
representative upstream -samples points are accessible. Please'provide
sampling results for the other accessible outfalls at this site, as well as
for outfalls, where upstream sampling points are accessible and'could
be considered nearly representative -of the full flow at that outfall.
Altematively,, please provide -a schedule for sampling of these outfalls.
Please, also identify those outfalls which are inaccessible, and for which
no reasonably representative upstream sample point is accessible.
DE Response: Additional stormwater samples were collected from Outfalls SW003, SW004,
SWO05 and SW013- on September 4, 2014 as: follows:

Samples for Outfalls SW003, SW004, and SW005 were collected from the first
accessible manholes upgradient of the outfalls. The outfalls for SW003,
SW004, and SW005 are inaccessible.
The sample for Outfall SW013 was collected from a manhole located
upgradient of an oil trap that discharges through Outfall SW013.
Samples have not been collected from the remaining stormwater outfalls at the
facility due to operational constraints. The facility will identify sampling
locations for inaccessible outfalls (SW011, SW012, SW013 and SW014), and
will continue to collect samples as qualifying rainfall events occur.
NCDENR Request 2: Please provide details (dates, locations on site, drainage areas
impacted, etc.) about the presence or any past storage and/or releases
of polychlorinated biphenyl compounds (PCBs) on site. If there were
any known releases, please discuss actions taken to remediate any
areas affected. Include information about what drainage areas might
have been impacted by PCBs.
DE Response: PCB oil -filled equipment was present at the facility in the past, however, all oils
containing PCBs have been removed. A detailed timeframe of removal actions
is not available. Stormwater runoff from most areas of the site where PCB oil -
filled equipment was formerly located drains or is pumped to the ash basin
which discharges through NPDES Outfall 003. Stormwater runoff from other
areas of the site where PCB oil -filled equipment was formerly located
discharges into oil trap tanks. There have been no known PCB impacts to
stormwater at the facility.
NCDENR Request 3: Please revise the site drainage map on these few points.
Item t: Flows from the radial stacker are now pumped to the ash
basin. Consequently, other parts of the application note that
outfall SW010 has been abandoned. Please show the location
of the abandoned outfall, SWOi0.
DE Response to Item 1: The site drainage map has been revised to indicate the location of
abandoned outfall SW010.
Item 2: Two different areas are labeled as drainage area 19, but
neither includes a corresponding outfall. Please rectify or
explain, and please provide graphic indication of the discharge
points from both areas.
DE Response to Item 2: Drainage Area 19, located in the eastern portion of the property, and
Drainage Area 22 have been combined and labeled as Drainage
Area 22 on the site drainage map.
The portion of Drainage Area 19 that is located south of the
structural fill will remain labeled as Drainage Area 19. This drainage
area is primarily grassed and undeveloped woodlands. No
2

industrial activity occurs within this drainage area. Non -contact
stormwater from this area discharges into a natural stream and is
then piped beneath the existing railroad tracks and into Belews
Lake. The site drainage map has been revised to indicate the
location of SW019. This Outfall should be removed from any
permitting- requirements.
Item 3: The narrative reports that runoff from inactive cells in the FGD
landfill will be discharged into Belews Lake. Please revise the
site plan to show the discharge point into the lake.
DE Response to Item 3: Inactive cells in the FGD landfill are directed to Drainage Area 9 and
Drainage Area 26. Both of these areas have outfalls to Belews Lake
that are indicated on the site drainage map.
NCDENR Request 4: Please provide clarification on the following aspects of the application
that are unclear to us.
Item is Outfall SW002. The narrative reports that once -through, non -
contact cooling water is discharged at this location. Please
clarify your intent for permitting that non-stormwater discharge.
DE Response to Item 1: Raw lake water is used in the chiller system to cool the "center bay'
area of the station. This once -through, non -contact cooling water is
discharged through Outfall SW002. The facility will evaluate the
discharge from this location and collect samples to characterize it.
An amended NPDES permit application will be sent to the NPDES
wastewater unit to request the permit be modified to include this
outfall as an additional wastewater discharge.
Item 2: It is not clear that Outfall SW008 drains any industrial activity,
and so may not be subject to a permit However, the site plan
indicated a long linear feature apparently originating as a
drainage feature in the area of the radial stacker and
apparently discharging in Drainage Area 8. Please clarify
whether there is industrial activity in Drainage Area 8 and
whether other flows originating elsewhere are delivered to
Drainage Area 8.
DE Response to Item 2: This drainage area discharges non -contact stormwater from an
undisturbed woodlands area with no industrial activity. This Outfall
should be removed from any permitting requirements.
Item 3.• Drainage Area 9 Is only 4.7 acres, largely undeveloped, and
described as `mostly grassy; but it discharges through what
would seem to be an overly large 54" concrete culvert. Please
clarify why such a large culvert is present at this location.
Were additional areas previously drained through this culvert?
3

DE Response to Item 3: Drainage Areas 9 and 20 previously discharged through this large
culvert as one, combined drainage area. The original culvert was
sized to convey this larger runoff.
Item 4: Drainage Area 10 currently is pumped' to the ash basin, but an
abandoned outfall SWO10 is noted in the outfall description.
Please clarify the physical circumstances related to the
abandoned outfall SWO10.
DE Response to Item 4: Outfall SWO10 was abandoned in 2007. The 36 -inch diameter
corrugated metal pipe (CMP) remains in place. The site drainage
plan has been revised to indicate the location.
Item 5. The narrative reports that the discharge in Outfall SWO15
potentially includes flows from floor drains inside the building.
Please clarify your intent for permitting any non stormwater
flows in this outfall.
DE Response to Item 5: The facility believes that the non-stormwater discharge from Outfall
SWO05 includes only condensate from an AH -7 air handling unit
(commercial air conditioning unit) located over the shop area. The
condensate is piped directly into the yard drainage system for
Outfall SWO15. We believe this discharge meets the allowable non-
stormwater discharge criteria under 15A NCAC 2H .0106 (f)(3).
Item 6. !t is not clear to us that Outfall SWO18 is a regulated
stormwater outfall'since it apparently drains to the receiving
water as part of the flow from SW018A. Please clarify your
intent for permitting SWO18.
DE Response to Item 6: Overflow from the south coal yard sumps can potentially discharge
through SW018 should the sumps malfunction. Since the Outfall
SWO18 discharges into Drainage Area 18A, potential industrial
overflow will be captured through Outfall SW018A. Outfall SW018
should be considered an internal outfall and removed from permit
consideration.
Item 7. For the narrative description of SW019, please clarify which of
two Drainage Areas 19 on the site plan are being described in
the narrative. Please clarify your intent for the permitting of
both areas labeled as Drainage Area 19 on the site plan.
DE Response to Item 7: Drainage Area 19, located in the eastern portion of the property, and
Drainage Area 22 have been combined and labeled as Drainage
Area 22. This revised Drainage Area 22 includes limestone railroad
tracks and a sewage lagoon. Limestone cars are staged there for
unloading. The remaining area is mostly covered in grass with the
exception of the large laydown space located in the central portion
of the drainage area. This area drains via sheet flow towards a
stormwater detention pond located in the northeast portion of this

drainage area. Stormwater within this pond is designed to
evaporate. Any overflow would discharge into the designed riser
and discharge into Belews Lake through outfall SW022. A
blowdown line from the municipal drinking water line is discharged
through this outfall. This water is treated with chlorine
The portion of Drainage Area 19 that is located south of the
structural fill will remain labeled as Drainage Area 19. This drainage
area is primarily grassed and undeveloped woodlands. No
industrial activity occurs within this drainage area. Non -contact
stormwater from this area discharges into a natural stream and is
then piped beneath the existing railroad tracks and into Belews
Lake. The site drainage map has been revised to indicate the
location of SW019. This Outfall should be removed from any
permitting requirements.
Item 8. The narrative reports that inactive cells in the FGD landfill will
discharge into Belews Lake (Drainage Area 20). Please clarify
your intent for permitting this stormwater discharge.
DE Response to Item 8: Stormwater runoff from inactive cells in the FGD landfill discharge
into Belews Lake through Outfalls SW009 and SW026. These two
outfalls should be permitted accordingly. Stormwater runoff from
active cells in the FGD landfill discharge is directed into the adjacent
stormwater basin. The collected water is ultimately pumped to the
ash basin.
Item 9: For Drainage Area 21: Please clarify whether the organic acid
unloading area and tank containment ultimately drain to the
ash basin.
DE Response to Item 9: Stormwater runoff from the organic acid unloading area and tank
containment is directed via a network of catch basins and
underground piping to the East and West stormwater ponds. The
collected water is ultimately pumped to the ash basin.
Item 10. Drainage Area 25 appears to drain industrial activities, but the
narrative notes that sheet flow is established from this area. Is
it your intent to report that the stormwater discharged from this
sub -drainage area is not regulated on the basis of sheet flow
rather than a point source discharge?
DE Response to Item 10: Duke Energy's intent is to report that stormwater discharged from
Drainage Area 25 is considered to be sheet flow, not a point source,
and therefore not regulated.
R

Item 11: The narrative reports that Drainage Area 26 is well vegetated.
Google Maps aerial photos do not appear to show industrial
activity in the area. Has this drainage area been the location
for past or present industrial activity? Are future industrial
activities contemplated for this area? What is your intent for
the stormwater permitting of SW026?
DE Response to Item 11: Drainage Area 26 is described in the Remaining Drainage Area
Description section of the Supplemental Information document.
This area consists of a well -vegetated series of stormwater basins
that were used as best management practices (BMPs) during the
construction of the FDG landfill. Currently, no industrial activity
occurs in this area. Outfall SW026 should be removed from any
permitting requirements.
Item 12: Google Maps aerial photos show a developed area
immediately adjacent to and south of Drainage Area 26, but
there is no discussion of it in the application. What are the
circumstances of this development? Please clarify your intent
for penniffing stormwater discharges from this area.
DE Response to Item 12: The developed area immediately adjacent to and south of Drainage
Area 26 is a staging area for the ash hauling contractor. There are
no point sources for stormwater discharged from this area.
Consequently, Duke Energy requests that this area be removed
from permitting considerations.
Item 13: The application identifies the Craig Road Ash Landfill, but
apparently does not request stormwater permit coverage for
this industrial operation. Please clarify your intent with respect
to permitting stormwater discharges originating in the area of
the landfill.
DE Response to Item 13: Stormwater runoff from active cells within the Craig Road Landfill
are collected in a stormwater detention basin. Discharges are
controlled by a valve that releases flow through an outfall into
Belews Lake. Duke recommends permitting this discharge as
Outfall SW027. The site drainage plan and supplemental
information document have been revised to include this drainage
area and outfall.
Item 14: Please clarify,the description of the Fuel Oil Unloading Area to
report the ultimate disposal of rain water trapped within the
containment area and sump.
DE Response to Item 14: Stormwater captured within the Fuel Oil Unloading Area is
discharged to the North Sump, which discharges to the Ash Basin.
G

Item 15. Please clarify where the Plant Yard Holding Sump discharges
to.
DE Response to Item 15: The Plant Yard Holding Sump discharges to the Ash Basin.
Item 16. The application reports that there are five main holding sumps
at the Belews Creek Steam Station. Do any sumps on the site
include high-level overflows that would discharge stormwater
to surface waters? If so, please provide a description of the
circumstances.
DE Response to Item 16: All five holding sumps are equipped with high-level overflow alarms.
Of these, only the Coal Conveyor Sump has the potential to
discharge stormwater to surface waters. Circumstances of this
high-level overflow discharge would include a pump failure or an
overwhelming rainfall event. Such occurrences are rare.
NCDENR Request 5. In accordance with item V of the FPA Form 2F application, please
confirm that Duke has observed all stormwater outfall conveyances on
the site, and provide a signature in Part A attesting that fact. For future
reference on other stormwater applications for this facility or for other
Duke facilities, if any outfalls either were not observed, or included non-
stormwater flows, please detail those conditions in EPA Form 2F. Also,
if any other discharges have occurred during dry periods please indicate
how those discharges are currently permitted, or will be permitted.
DE Response: All stormwater outfalls have been observed during dry periods with
no discharges noted with the exception of SW002 and SW015 as
previously addressed (reference DE Responses to NCDENR
Request 4, Items 1 and 5 above).
Please find attached the following documents:
a. Revised Stormwater Site Map,
b. Revised Supplemental Information document,
C. Revised Form 1,
d. Revised Form 2F.
Duke Energy appreciates the opportunity to respond to NCDENR's request for additional
information. Should you have any questions regarding this submittal or require additional
information, please contact Mark McGary at 980-373-7898 or email Mark.McGary@duke-
energy.com.
7

I certify, underpenalty of law, that this document and all attachments were prepared under my direction
or supervision in accordance with a system designed to assure that qualified personnel properly gather
and evaluate the information submitted. Based on my inquiry of the person or persons who manage the
system, or those persons directly responsible for gathering the information, the information submitted is,
to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment
for knowing violations.
Sincerely,
lM�
sse HuntleyGG neral Manager III
Belews Creek Steam Station
Attachments

bc: Melonie Martin — Belews Creek Steam Station
Jesse Huntley - Belews Creek Steam Station
Penny Stafford
Mark McGary
Steve Cahoon
Harry Sideris
Linda Hickok
Mike Shrader
Document Number: 8-6
Record Type Code: ENV -50-02
UPS:
0

Please print or type in the unshaded areas only
/fill -on nrcac ara ennead fnralifa fvna i a 19 rharartarc/nchl
For Approved. OMB No. 2040-0086. Approval expires 5-31-92
FORM
U.S. ENVIRONMENTAL PROTECTION AGENCY
I, EPA I.D. NUMBER
GENERAL INFORMATION
i•. �IrF
E_ �Consolidated Permits Program
S
T1A C
NCD000856591 D
GENERAL
_ (Read the "General Instructions" before -star ting.)
1
2 13 14 15
LABEL ITEMS
GENERAL INSTRUCTIONS
I. EPA I.D. NUMBER
If a preprinted label has been provided,
affix it in the designated space. Review the
III. FACILITY NAME
information carefully; if. any of it is
incorrect cross through it and enter .the
correct data in the appropriate fill-in area
below: Also, if any of the prgrinted data is
absent (the area to the left of the label
V. FACILITY PLEASE PLACE LABEL
IN THIS SPACE
Space fistappear) l the information that should
lease provideit in the proper fill -
in below. If the label is complete
MAILING LIST :
VI. FACILITY
LOCATION
area(s�
and correct you need not complete Items
I, III, V, and VI(except VI -B which must be
completed regardless). Complete all items
if no label has been proved. Refer to the
instructions for detailed item descriptions
and for the legal authorization under which
this data is collected.
II. POLLUTANT CHARACTERISTICS
INSTRUCTIONS: Complete A through J to determine whether you need to submit any permit application forms
questions, you must submit this form and the supplemental from listed in the parenthesis following the question.
the supplemental form is attached. If you answer "no" to each question, you need not submit any of these forms.
excluded from permit requirements; see Section C of the instructions. See also Section D of the instructions
to the EPA. If you answer "yes" to any
Mark "X" in the box in the third columm if'
You may answer"no" if your activity is
for definitions of bold-faced terms.
SPECIFIC QUESTIONS
MARK "X"
SPECIFIC SPECIFIC QUESTIONS
MARK "XII
YES
NO
ATTACHED
YES
NO
FORM ATTACHED
A. Is this facility a publicly owned treatment works
which results in a discharge to waters of the
U.S.? (FORM 2A)
❑
®
❑
B. Does or will this facility (either existing or
proposed) include a concentrated animal
feeding operation or aquatic animal
production facility which results in a discharge
to waters of the U.S?' (FORM 2B)
❑
®
❑
16
17
18
19
20
21
C. Is this facility which currently results in®
discharges to waters of the U.S. other than
those described in A or B above? FORM 2C)
❑
®
D. s this proposal facility other Th those describe
in A or, B above) which will result in a discharge
to waters of the U.S.? FORM 2D)
E]®
EJ
22.
23
24
25
26
27
E. Does or will this facility treat-, store, or dispose of
hazardous wastes? (FORM 3)
❑
®
❑
F. Do you or will you inject at this facility industrial or
municipal effluent below the lowermost stratum
containing, within one quarter mile of the well
❑
®
❑
bore, underground sources of drinking water?
(FORM -4)
28
29
30
31
32
33
G. Do you or will -you inject, at this facility any
produced water other fluids which are brought to
the surface in connection with conventional oil or
natural gas production, inject fluids used for
enhanced recovery of oil or natural gas, or inject
❑
®
❑
H. Do you or will you inject at this facility fluids for
special processes such as mining of sulfer by the
Frasch process, -solution mining of minerals, in
situ combustion of fossil fuel, or recovery of
geothermal energy? (FORM 4)
❑
®
❑
fluids for storage of liquid hydrocarbons?
34
35
36
37
38
39
FORM 4
'I. s this facility a proposed stationary source
which is one of the 28 industrial categories listedwhich
in the instructions and which will potentially emit
100 tons per year of any air pollutant regulated
under the Clean Air Act and mayaffect or be
located in an attainment area? FORM 5
❑ ® ❑
40 41 42
J. Is this facility a proposed stationary source
is NOT one of the 28 industrial categories ❑
listed in the instructions and which will potentially
emit 250 tons ,per year of any air pollutant
regulated under the Clean Air Act and may affect
or be located in an attainment are? FORM 5 43
®
❑
44 1 45
III. NAME OF FACILITY
C SKIP Belews Creek Steam Station
1
15 16-29 30
'69
IV. FACILITY CONTACT
A. NAME & TITLE last, first, & title
B. PHONE area code & no.
2 Keeley McCormick, EHS Professional H
336 1445 1 0204
15 1 16
45 46 48 1 49 51 1 52 55
V. FACILITY MAILING ADDRESS
A. STREET OR P.O. BOX
s 3195 Pine Hall Road
15 16
45
B. CITY OR TOWN
C. STATE D. ZIP CODE
C Bele ws Creek
NC 27009
15 1 16 40
1 41 42 47 51
VI. FACILITY LOCATION
A. STREET, ROUTE NO. OR OTHER SPECIFIC IDENTIFIER
C 3195 Pine Hall Road
15 1 16
45
B. COUNTY NAME
Stokes
46 70
C. CITY OR TOWN
D. STATE
E. ZIP CODE
F. COUNTY CODE
CBelews
Creek
NC
27009
152
034
15
16 40
41 42
47 51
54
EPA FORM 3510-1(8-90) CONTINUED ON REVERSE

CONTINUED FROM THE FRONT
VII. 81C CODES (4 -digit, in order of riorit
A. FIRST B. SECOND
4911
(specify)
Electric Services
7
.5
(specify)
1
16 17
16 19
C. THIRD D. FOURTH
c(specify) 7 (specify)
15 16 17 1 15 1 1619
VIII. OPERATOR INFORMATION
A. NAME B. Is the name listed in Item
c Duke Energy Carolinas, LLC VIII -A also the owner?
8 [EYES ❑NO
18 1 19 55
C. STATUS OF OPERATOR Enter the appropriate letter into the answerbox; if "Other,"specify.)
D. PHONE area code & no.
F = FEDERAL i M =PUBLIC (other than federal or state)
P
(specify)
336
445
0204
S = STATE I O = OTHER (specify)
Electric Utility
A
ss
16 18
19 21
22 25
P = PRIVATE
E. STREET OR PO BOX
3195 Pine Hall Road
26 55
F. CITY OR TOWN G. STATE H. ZIP CODE
I IX. INDIAN LAND
c I Belews Creek 27009 Is the facility located on Indian lands?
B ❑ YES ® NO
"42
15 16 40 47 51
X. EXISTING ENVIRONMENTAL PERMITS I MM
A. NPDES (Discharges to Surface Water D. PSD Air Emissions from Proposed Sources
C I T I ' NCO024406 ° T 8 01983T25, Non -PSD, Air
9 1 N I 9 P
15 1 16 117 18 30 15 16 1 17 1 18 30
B. UI (Underground Injection of Fluids E. OTHER (specify)
(Specify)
Industrial Landfill
C T I '
c T B
1 9
85-03,85-04,85-05
9 1 U 1
15 1 16 1 17
1 18 30 15 16 1 17
1 18 30
C. RCRA Hazardous Wastes E. OTHER (specify) (Specify)
cR NCD000856591 c T 8 WQ0000452 Distribution of residual
15 16 [�117118 30 15 18 1 17 1 18 30 Solids
XI. MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must
show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its
hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground. Include all springs,
rivers and other surface water bodies in the map area. See instructions for precise requirements.
XII. NATURE OF BUSINESS(provide a brief description)
Coal Fired Electric Generation
XIII. CERTIFICATION (see instructions
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and
all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in
the application, I believe that the information is true, accurate and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fine and impfispnnjent
A. NAME &OFFICIAL TITLE (type or print) rZEJ
C. DATE SIGNED
Harry K. Sideris, Sr Vice President - EHS
COMMENTS FOR OFFICIAL USE ONLY
EC
15
16 55
EPA FORM 3510-1(8-90)

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"IL•S^...i•1.5 C..&.ya ewa. i..•CC) OMCHAROELOCANONMAP FIGURE
HPDEE Pemd1 No: NC0024408
.+, i�.�uro mxwcrscveasse aiu w.marem.m�ma. ..QQ
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(•,:q3 L1m yv u Yeo S-fDrE3 OWNTf, NORM QVRO_It1A

CRANArE AREA
OUTFALL DESCRIPTION
RECEMNG WATER UODY
1
24Y CUP
BELEWS LAKE
2
30'0 CMP
BELEWS LAKE
.1
21'0 CMP
INTAKE CANAL
4
in CMP
INTAKE CANAL
5
Wo CMP
INTAKE CANAL
a
10'0 CMP
INTAKE CANAL -
7
74"0 CNP
NELEWS LAKE
a
12"o NOPE
DELEWS LAKE
0
54"0 CONCRETE CULVERT
BELEWS LAKE
11
15"0 CMP
DISCHAHGL CANAL
12
12'0 CNP
DISCNARCE CANAL
I3
21'0 CUP
DISCHARGE CANN
14
17'0 CNP
DISCHARGE CANAL
15
42'0 CMP
DISCHARGE CANAL
10
30'0 CNP
HELEWS LAKE
17
30'0 Cup
DELEWS LAKE
10
24'0 CNP
BELEWS LAKE
IBA
24'0 CUP
DELEWS LANE
t00
40"0 CONCRETE CULYERT
DELCWS LAKE
22
24'0 CUP
DELEWS LAKE
24
24'0 CMP
DELEWS LAKE
25
24'0 Cup
BELEWS LAKE
PARTIAL PLAN n
SCALE: 1•- 1DO.
KEY NOTE:
O DRAINAGE Y
LEGEND.
PUMP TO 0
....e DRAIMSE I
STRUCtUR6 LEGENC
OI COAL CRUS
0 SWITCHCEAf
ps COAL UNLO
Q TRANSFER '
5� MCC IIOU51
© 5CA•IIOUSE
O7 WATER TOW
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Q NEL OIL S
10 STECLUALL
II
ELECTRICAL
12 LIMESTONE
is RAILCAR UI
to UOAI STOR
lO'.. GYPSUM IN
1G WASTE WAT
17 F,O. UIVLOJ
10 F,0, TANK
ID AMMONIA T
70 CON57RUCI
100 a
6�
SCAtf w FEE
400 [
CALSrd
SCALE IN F![
eh DU0 4 ou 4 111000 Cnollotte, Nc 202024070116
IY: •lAl
DRAWN GY:
CML
OUKDENERO
BELEWS CREE
—
DESIGNED BY:
MECNANICA4
sn
STORMWA
CHECKED BY,
ELECTRICAL
APPROVED DY:
DATE:
AS NOTED
M0. wIR AIY A4 AxN 4x. CnN .w'q LNA IIIC NL6,
1'uNLCi NWUUk Op00000W]]4f01

EPA I.D. NUMBER (copyfiomItem I of Form 1) Form Approved.
OMB No. 2040-0086.
Die— min thm nnchorloA mmnc nnlu INCDO00856591 Approval expires 3-31-98.
FORM U.S. ENVIRONMENTAL PROTECTION AGENCY
2CA APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER
EPA EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURE OPERATIONS
NPDES Consolidated Permits Program
I. OUTFALL LOCATION
For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A. OUTFALL NUMBER
(list)
B. LATITUDE C. LONGITUDE
D. RECEIVING WATER (name)
1. DEG.
2. MIN.
3. SEC. 1. DEG.
2. MIN. 3. SEC.
001
36
16
49.5 80
03 39.8
Belews Lake
003
36
18
22.0 80
04 50.7
Dan River via Effluent Channel
002
36
17
8.0 80
03 53.8
Ash Basin (Internal Outfall)
SWO02
36
17
50.31 80
3 29.66
Belews Lake
II. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units
labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations,
treatment units, and outfalls. If a water balance cannot be determined (e.g., for certain mining activities), provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each ouffall, provide a description of: (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water,
and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets if
necessary.
1. OUT-
2. OPERATION(S) CONTRIBUTING FLOW 3. TREATMENT
FALL
NO. (list)
b. AVERAGE FLOW b. LIST CODES FROM
a. OPERATION (list) (include unils) a. DESCRIPTION TABLE 2C-1
001
Once Through Cooling Water Discharge to Surface Water
4A
Miscellaneous Equipment 1275 MGD
Non -Contact Cooling Water
003
Ash Settling Pond Coagulation, Sedimentation, Neutralization,
9 MGD 2D lU
Discharge from Storm Drain ion Exchange, Surface Water Dischazrge
2K 2,7
4A
002
Flue Gas Desulfurization Wastewater 0.7 MGD Sedimentation
lU 2K
(Internal Outfall) Coagulation, Chemical Precipitation 2L
Reduction, Neutralization
3C
Belt Filtration, Landfill
SC SQ
SW002
Once Through Chiller Water Dicharge to Surface Water
4A
Stormwater
OFFICIAL USE ONLY (effluent
EPA Form 3510-2C (8-90) PAGE 1 of 4 CONTINUE ON REVERSE

r:ONTINI IFn FROM THF FRONT
C. Except for storm runoff, leaks, or spills, are any of the discharges described in Items II -A or B intermittent or seasonal?
❑ YES (complete the following table) 91 NO (go to Section III)
3. FREQUENCY
4 FLOW
a. DAYS PER
B. TOTAL VOLUME
2. OPERATION(s)
WEEK
b. MONTHS
a. FLOW RATE (inmgd)
(speafywilh units)
1. LONG TERM
2 MAXIMUM
1. LONG TERM
2. MAXIMUM
1 OUTFALL
CONTRIBUTING FLOW
(specify
PER YEAR
C. DURATION
NUMBER (list)
(fist)
average)
(speciifi'--age)
AVERAGE
DAILY
AVERAGE
DAILY
tin days)
III. PRODUCTION
A. Does an effluent guideline limitation promulgated by EPA under Section
304 of the
Clean Water
Act apply to your
facility?
® YES (complete Item III -B)
❑
NO (go to Section
In
B. Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure of operation)?
❑ YES (complete Item III -C) W1 NO (go to Section If)
C. If you answered "yes" to Item III -B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used in the
applicable effluent guideline, and indicate the affected outfalls.
1. AVERAGE DAILY PRODUCTION
2. AFFECTED OUTFALLS
(list outfall numbers)
a. QUANTITY PER DAY
b. UNITS OF MEASURE
c. OPERATION, PRODUCT, MATERIAL, ETC.
(specify)
IV. IMPROVEMENTS
A. Are you now required
by any Federal, State or local
authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or
practices or any other environmental
programs which may affect the discharges described in this application? This includes, but is not limited to,
permit conditions, administrative
or enforcement orders,
enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions.
® YES (complete
the following table)
❑ NO (go to Item IT' B)
1. IDENTIFICATION OF CONDITION,
2. AFFECTED OUTFALLS
3. BRIEF DESCRIPTION OF PROJECT
4. FINAL COMPLIANCE DATE
AGREEMENT, ETC.
a. NO.
b. SOURCE OF DISCHARGE
a REQUIRED
b. PROJECTED
North Carolina Coal Ash
003
Ash Sluice
The act requires closure of ash basin.
5/17/23
5/17/23
Management Act of 2014
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned, and indicate your actual or planned schedules for
construction.
❑ MARK "X" IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C (8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA Form 3510-2C (8-90) PAGE 3 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
VII. BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
© YES (idents the test(s) and describe their purposes below) ❑ NO (go to Section VIII)
Toxicity testing is performed as required by the station's current NPDES permit. The acute toxicity test is
conducted and reported quarterly for the ash basin discharge (Outfall 003).
VIII. CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
® YES (list the name, address, and telephone number of, andpollutams analyzed by, ❑ NO (go to Section LX)
each such laboratory or firm below)
C. TELEPHONE
D. POLLUTANTS ANALYZED
A. NAME
B. ADDRESS
(area code & no.)
(list)
Duke Energy Analytical Lab
13339 Hagers Ferry Road
980-875-5245
Metasls, COD, TKN,
NC# 248
Huntersville, NC 28078
Nitrate -nitrite, TP, Oil &
Grease, TSS, TOC, Bromide,
Sulfate, Flouride
Shealy Lab
106 Vantage Point Dirve
803-791-9700
BOD, Fecal ColiformColor,
NC# 329
West Columbia, SC 29172
Sulifide, Sulfite,
Surfactants, Cyanide,
Phenol, Volatiles,
Semi -volatiles Acid
compounds, PCBs, Mercury
GEL, Inc.
2040 Savage Road
843-556-8171
Radiology
NC# 233
Charleston, SC 29417
Pace Analytical
9800 Kincey Avenue, Suite 100
704-875-9092
Ammonia Nitrogen
NC# 633
Huntersville, NC 28078
Dioxins and Furans
Cape Fear Analytical
3306 Kitty Hawk Road, Suite 120
910-795-0421
an affiliate of The GEL Group
Wilmington, NC 28405
NC# 065-1519-1
IX. CERTIFICATION
1 certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there
are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.
A. NAME & OFFICIAL TITLE (type orprtnt)
B. PHONE NO. (area code & no.)
Harry K. Sideris - Sr Vice President, EHS
[phone]
C. SIG
61,
D. DATE SIGNED
ul ( L
l0
EPA,P'o',m 35=C,�8-g0) PAGE 4 of 4

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information EPA I. D. NUMBER (copy from Item 1 of Form 1)
on separate sheets (use the same format) instead of completing these pages. NCD000856591
SEE INSTRUCTIONS.
OUTFALL NO.
V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C)
sw002
PART A —You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
3. UNITS
4. INTAKE
2. EFFLUENT
(sped if blank)
(optionab
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONGTERM
a. MAXIMUM DAILY VALUE
(Ifavailable)
(ifavailable)
AVERAGE VALUE
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
1. POLLUTANT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
(1) CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
a. Biochemical Oxygen
Demand (BOD)
b. Chemical Oxygen
<20
1
mg/1
Demand (COD)
c. Total Organic Carbon
(TOC)
d. Total Suspended
<5
1
mg/l
Solids (TSS)
e. Ammonia (as A)
VALUE
VALUE
VALUE
VALUE
f. Flow
2.59 MGD*
*Max. Design Flow
g. Temperature
VALUE
VALUE
VALUE
°C
VALUE
(winter)
h. Temperature
VALUE
VALUE
VALUE
°C
VALUE
(summer)
27.9
MINIMUM
MAXIMUM
MINIMUM
MAXIMUM
L pH
7.21
STANDARD UNITS
PART B — Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either
directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide
quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements.
2. MARK "X°
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG. VALUE
a. LONG TERM AVERAGE
AND
a.
b.
a. MAXIMUM DAILY VALUE
(ifavailable)
(ifavailable)
VALUE
CAS NO.
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
a. Bromide
(24959-67-9)
b. Chlorine, Total
Residual
c. Color
d. Fecal Coliform
\X
X
/�`
e. Fluoride
(16984-48-8)
f. Nitrate -Nitrite
v
(as M
EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE

ITEM V -B CONTINUED FROM FRONT
EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (opdona4
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG. VALUE
a. LONG TERM
AND
a
b,
a MAXIMUM DAILY VALUE
(ifavailable)
(1favailable)
AVERAGE VALUE
CAS NO.
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
g. Nitrogen,
Total Organic (as
\ /
A)
/X\
h. Oil and
<5
1
mg/1
Grease
i. Phosphorus
`
(as P), Total
X
(7723-14-0)
j. Radioactivity
(1) Alpha, Total
(2) Beta, Total
\X
X
,�`
(3) Radium,
Total
(4) Radium 226,
Total
k. Sulfate
(-SO,)
15
1
mg/ 1
(14808-79-8)
I. Sulfide
�/
(as 5)
x
m. Sulfite
(as SO,)
X
(14265-45-3)
n. Surfactants
x
o. Aluminum,
Total
0.153
1
mg/1
(7429-90-5)
p. Barium, Total
(7440-39-3)
x
0.021
1
Mg/1
q. Boron, Total
(7440-42-8)
(7
/\ x
0.077
1
mg/1
r. Cobalt, Total
(7440-48-4)
s. Iron, Total
0.184
1
mg/1
(7439-89-6)
t. Magnesium,
Total.
67
1
mg/1
(7439-95-4)
u. Molybdenum,
Total
1.7
1
ug/1
(7439-98-7)
v. Manganese,
Total
0.016
1
mg/1
(7439-96-5)
w. Tin, Total
\/
(7440-31-5)
x
x. Titanium,
Tota
(7440-32-6)
EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C NCD000856591 SWO02
PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and nonrequired GC/MS
fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must
provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2 -methyl -4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (a// 7 pages) for each outfall. See instructions for
additional details and requirements.
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a,
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. N0. OF
a. CONCEN-
b. NO OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
METALS, CYANIDE, AND TOTAL PHENOLS
1M.Antimony, Total�/
X
<1
1
Ug/1
(7440-36-0)
2M. Arsenic, Total
<1
1
Ug/1
(7440-38-2)
3M. Beryllium, Total
v
(7440-41-7)
4M Cadmium, Total
<1
1
Ug/1
(7440-43-9)
5M. Chromium,�/
X
<1
1
Ug/1
Total (7440-47-3)
6M. Copper, Total
<1
1
M9/1
(7440-50.8)
7M. Lead, Total
<1
1
Ug/1
(7439-92.1)
8M. Mercury, Total
<50
1
ng/1
(7439-97-6)
9M. Nickel, Total
<1
1
Ug/1
(7440-02-0)
10M. Selenium,
<1
1
Ug/1
Total (7782.49-2)
11 M. Silver, Total
(7440-22-4)
12M. Thallium,
<0.02
1
Ug/1
Total (7440-28-0)
13M. Zinc, Total
0.008
1
Mg/1
(7440-66-6)
14M. Cyanide,
Total (57-12-5)
0.011
1
tn9/1
15M. Phenols,
Total
DIOXIN
2,3,7,8 -Tetra-
DESCRIBE RESULTS
chlorodibenzo-P-
Dioxin (1764-01-6)
EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE

r`nr,1T1r,1 17n FDMA THE FRONT
EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V-5
2. MARK "X"
3. EFFLUENT 4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavaVable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
Ofavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —VOLATILE COMPOUNDS
1V. Accrolein
x(107-02-8)
2V. Acrylonitrile
x(107-13-1)
3V. Benzene
�/
(71-43-2)
x
4V. Bis (Chloro-
\ /
methyl) Ether
(542-88-1)
/X\
5V. Bromoform
(75-25-2)
6V. Carbon
Tetrachloride
'
X
(56.23-5)
7V. Chlorobenzene
x(108-90-7)
BV. Chlorodi-
bromomethane
(124-48-1)
/X\
9V. Chloroethane
x(75-00-3)
ethylvinyl Ether
X
(110-75-8)
11 V. Chloroform
(67-66-3)
12V. Dichloro-
bromomethane
X
(75-27-4)
13V. Dichloro-
difluoromethane
X
(75-71-8)
14V.1,1-Dichloro-
ethane (75-34-3)
15V.1,2-Dichloro-
x\/
ethane (107-06-2)
16V.1,1-Dichloro-
ethylene (75-35-4)
17V.1,2-Dichloro-
xpropane
(78-87-5)
18V.1,3-Dichloro-
\ /
propylene
(542-75-6)
/X\
19V. Ethylbenzene
\/
x
(100-41-4)
20V. Methyl
Bromide (74-83-9)
21V. Methyl
Chloride (74-87.3)
EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V-5

r.ONTINI IFIL FRC)M PAC;F V-4
EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG,
a. LONGTERM
AND
a,
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —VOLATILE COMPOUNDS (continued)
22V. Methylene
Chloride (75-09-2)
Tetrachloroethane
X
-
79-34-5
24V. Tetrachloro-
ethylene (127-18-4)
25V. Toluene
(108-88-3)
26V.1,2 -Trans-
` ,
Dichloroethylene
X
(156-60-5)
27V.1,1,1 -Trichloro-
ethane (71-55-6)
28V.1,1,2 -Trichloro-
ethane (79-00-5)
29V Trichloro-
ethylene (79-01.6)
30V. Trichloro-
fluoromethane
75-69-4
/X\
31V. Vinyl Chloride
�/
x
(75-01-4)
GC/MS FRACTION — ACID COMPOUNDS
1A.2 -Chlorophenol
�/
x
(95-57-8)
2A. 2,4-Dichloro-
�/
x
phenol (120-83-2)
3A. 2,4 -Dimethyl-
phenol (105-67-9)
4A.4,6-Dinitro-0-
�/
x
Cresol (534-52-1)
5A.2,4-Dinitro-
�/
x
phenol (51-28-5)
6A.2-Nitrophenol
(88-75-5)
7A.4-Nitrophenol
�/
x
(100-02-7)
8A. P -Chloro -M -
Cresol (59-50-7)
9A. Pentachloro-
phenol (87-86-5)
10A. Phenol
x(108-95-2)
111 A.
1
ll (88.05-2)
EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7
2. MARK "X"
3. EFFLUENT
4. UNITS 5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a,
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
(1)
b. NO. OF
(1)
(1)
(1)
Ofavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS CONCENTRATION (2) MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS
1 B. Acenaphthene
x(83-32-9)
2B. Acenaphtylene
x(208-96-8)
3B. Anthracene
�/
(120-12-7)
x
4B. Benzidine
�/
(92-87-5)
x
5B. Benzo (a)
Anthracene
(56-55-3)
6B. Benzo (a)
�/
x
Pyrene (50-32-8)
76
rant-Benzo-
fluoranthene
(205-99-2)
8B. Benzo (glu)
�/
x
Perylene (191-24-2)
9B. Benzo (k)
Fluoranthene
(207-08-9)
10B. Bis (2-Chloro-
eUio* Methane
(111-91-1)
11 B. Bis (2-CIVoro-
e1hyq Ether
�/
x
(111-44-4)
12B. Bis (2-
ChloroisopropyQ
Ether (102-80-1)
13B. Bis (2-Ethyl-
1jexyl) Phthalate
(117-81-7)
14B. 4-Bromophenyl
Phenyl Ether
(101-55-3)
15B. Butyl Benzyl
�/
x
Phthalate (85-68-7)
16B. 2 -Chloro -
naphthalene
(91-58-7)
17B. 4 -Chloro -
phenyl Phenyl Ether
x(7005-72-3)
18B. Chrysene
�/
x
(218-01-9)
19B. Dibenzo (ah)
Anthracene
(53-70-3)
20B.1,2-Dichloro-
xbenzene
(95-50-1)
216.1,3 -Di -chloro-
�/
benzene (541-73-1)
EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE
2. MARK "X"
3. EFFLUENT
4. UNITS 5. INTAKE (optionA
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE I
(ifavailable)
VALUE (ifavallable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
(1)
b. NO. OF
(1)(1)
(1)
Ofavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS CONCENTRATION (2) MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (condnued)
22B.1,4 -Dichloro-
benzene (106-46-7)
238.3,3-Dichloro-
benzidine (91-94-1)
24B. Diethyl
Phthalate (84.66-2)
Dimethyl
Phthalate
(131-11-3)
26B. Di -N -Butyl
Phthalate (84-74-2)
27B.2,4-Dinitro-
toluene (121-14-2)
28B.2,6-Dinitro-
toluene (606-20-2)
29B. Di-N-Octyl
Phthalate (117-84-0)
30B. 1,2 -Diphenyl -
hydrazine (as Azo-
benzene)(122-66-7)
31B. Fluoranthene
(206-44-0)
32B. Fluorene
(86-73-7)
33B. Hexachloro-
benzene (118-74-1)
34B. Hexachloro-
butadiene (87-68-3)
35B. Hexachloro-
cyclopentadiene
X
(77-47-4)
36B Hexachloro-
ethane (67-72-1)
37B.3 o
-Cd)
(7,2,3 -cd) Pyrene
'
X
(193-39-5)
38B.Isophorone
(78-59-1)
39B. Naphthalene
(91-20-3)
40B. Nitrobenzene
(98-95-3)
416. -
sodimethylaethylamine
X
(62-75-9)
42B. N-Nitrosodi-
N-Propylamine
(621-64-7)
EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE

r'r1AITIKII p7n FRr)rA TNF FRr1NT
EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9
2. MARK -X-
3. EFFLUENT
4. UNITS
5. INTAKE (optiona4
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable) I
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
Ofavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (continued)
43B. N-Nitro-
sodiphenylamine
(86-30-6)
44B. Phenanthrene
x(85-01-8)
45B. Pyrene
(129-00.0)
46B. 1,2,4-Tri-
chlorobenzene
x(120-82-1)
GC/MS FRACTION — PESTICIDES
1 P. Aldrin
(309-00-2)
2P. a -BHC
(319-84-6)
3P. P -BHC
(319-85-7)
4P. y -BHC
(58-89-9)
5P. 8 -BHC
(319-86-8)
6P. Chlordane
(57-74-9)
7P. 4,4' -DDT
(50-29-3)
8P. 4,4' -DDE
(72-55-9)
9P. 4,4' -DDD
(72-54-8)
1OP. Dieldrin
(60-57-1)
11 P. a-Enosulfan
(115-29-7)
12P. ji-Endosulfan
(115-29-7)
13P. Endosulfan
Sulfate
(1031-07-8)
14P. Endrin
(72-20-8)
15P. Endrin
Aldehyde
(7421-93-4)
16P. Heptachlor
(76-44-8)
EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9

EPA I. D. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-8 NCD000856591 SWO02
EPA Form 3510-2C (8-90) PAGE V-9
2. MARK"X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG.
a. LONGTERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(ifavallable)
VALUE (Ifavailabie)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. 140. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
Ofavallable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — PESTICIDES (continued)
17P. Heptachlor
Epoxide
(1024-57-3)
18P. PCB -1242
(53469-21-9)
19P. PCB -1254
\/
x
(11097-69-1)
20P. PCB -1221
\/
(11104-28-2)
x
21 P. PCB -1232
\�
(11141-16-5)
x
22P. PCB -1248
(12672-29-6)
23P. PCB -1260
\�
(11096-82-5)
x
24P. PCB -1016
(12674-11-2)
25P. Toxaphene
(8001-35.2)
EPA Form 3510-2C (8-90) PAGE V-9

.DUKE Analytical Laboratory
E ER 0a
13339 Hagers Ferry Road
Huntersville, NC 28078-7929
McGuire Nuclear Complex - MG03A2
Phone: [phone] Fax: [phone]
Order Summary Report
Order Number: J14070330
Project Name: NPDES Seep/SW
Customer Name(s): Melonie Martin, Allen Stowe,Josh Quinn
Customer Address: 3195 Pine Hall Rd
Mailcode: Belews Steam Station
Belews Creek, NC 28012
Lab Contact: Mary Ann Ogle Phone: [phone]
Report Authorized By: Date:
(Signature)
Mary Ann Ogle
Program Comments:
Please contact the Program Manager (Mary Ann Ogle) with any questions regarding this report.
Data Flags & Calculations:
7/22/2014
Page 1 of 22
Any analytical tests or individual analytes within a test flagged with a Qualifier indicate a deviation from the method quality
system or quality control requirement. The qualifier description is found at the end of the Certificate of Analysis (sample results)
under the qualifiers heading. All results are reported on a dry weight basis unless otherwise noted. Subcontracted data
included on the Duke Certificate of Analysis is to be used as information only. Certified vendor results can be found in the
subcontracted lab final report. Duke Energy Analytical Laboratory subcontracts analyses to other vendor laboratories that have
been qualified by Duke Energy to perform these analyses except where noted.
Data Package:
This data package includes analytical results that are applicable only to the samples described in this narrative. An estimation of
the uncertainty of measurement for the results in the report is available upon request. This report shall not be reproduced, except
in full, without the written consent of the Analytical Laboratory. Please contact the Analytical laboratory with any questions. The
order of individual sections within this report is as follows:
Job Summary Report, Sample Identification, Technical Validation of Data Package, Analytical Laboratory Certificate of Analysis,
Analytical Laboratory QC Reports, Sub -contracted Laboratory Results, Customer Specific Data Sheets, Reports &
Documentation, Customer Database Entries, Test Case Narratives, Chain of Custody (COC)
Certification:
The Analytical Laboratory holds the following State Certifications : North Carolina (DENR) Certificate #248, South Carolina
(DHEC) Laboratory ID # 99005. Contact the Analytical Laboratory for definitive information about the certification status of
specific methods.

Sample ID's & Descriptions:
Page 2 of 22
Sample ID
Plant/Station
Collection
Date and Time
Collected By
Sample Description
2014020714
BELEWS
15 -Jul -14 3:28 PM
MELONIE MARTIN
S-7
2014020715
BELEWS
15 -Jul -14 5:40 PM
MELONIE MARTIN
SW 006
2014020716
BELEWS
15 -Jul -14 5:58 PM
MELONIE MARTIN
SW 015
2014020717
BELEWS
15 -Jul -14 6:10 PM
MELONIE MARTIN
SW 002
4 Total Samples

Technical Validation Review
Checklist:
COC and .pdf report are in agreement with sample totals 0 Yes ❑ No
and analyses (compliance programs and procedures).
All Results are less than the laboratory reporting limits. ❑ Yes Fv� No
All laboratory QA/QC requirements are acceptable. F./� Yes ❑ No
Report Sections Included:
❑d Job Summary Report
❑d Sample Identification
0 Technical Validation of Data Package
Analytical Laboratory Certificate of Analysis
❑ Analytical Laboratory QC Report
Page 3 of 22
❑d Sub -contracted Laboratory Results
❑ Customer Specific Data Sheets, Reports, & Documentation
❑ Customer Database Entries
❑ Chain of Custody
❑ Electronic Data Deliverable (EDD) Sent Separately
Reviewed By: DBA Account Date: 7/22/2014

Certificate of Laboratory Analysis Page 4 of 22
This report shall not be reproduced, except in full.
Order # J14070330
Site: S-7 Sample #: 2014020714
Collection Date: 15 -Jul -14 3:28 PM Matrix: NPDES
Analyte Result Units Qualifiers RDL DF Method
OIL AND GREASE IN WATER - SOLID PHASE EXTRACTION - (Analvsis Performed by Pace Laboratories
Vendor Parameter
Complete
< 1
N1
10.6
Cadmium (Cd)
Vendor Method
CHEMICAL OXYGEN DEMAND
< 1
Copper (Cu)
13.9
Lead (Pb)
< 1
Molybdenum (Mo)
COD
< 20
mg/L
N1
20
1
HACH 8000
INORGANIC IONS BY IC
07/21/2014 09:37
TDS
34
TOTAL SUSPENDED SOLIDS
1
TSS
Chloride
4.2
mg/L
1
1
10
EPA 300.0
Fluoride
< 1
mg/L
1
1
10
EPA 300.0
Sulfate
1.5
mg/L
N1
1
10
EPA 300.0
MERCURY (COLD VAPOR) IN WATER
1
EPA 200.8
07/18/2014 12:11
JAHERMA
ug/L
Mercury (Hg)
< 0.05
ug/L
07/18/2014 12:11
0.05
1
EPA 245.1
TOTAL RECOVERABLE METALS BY ICP
EPA 200.8
07/18/2014 12:11
JAHERMA
ug/L
1
Aluminum (AI)
0.103
mg/L
JAHERMA
0.005
1
EPA 200.7
Barium (Ba)
0.055
mg/L
ug/L
0.005
1
EPA 200.7
Boron (B)
< 0.05
mg/L
N1 25
0.05
1
EPA 200.7
Calcium (Ca)
1.61
mg/L
B1
0.01
1
EPA 200.7
Hardness
9.31
mg/L
0.19
1
EPA 200.7
Iron (Fe) 13.3
Magnesium (Mg) 1.28
Manganese (Mn) 0.604
Zinc (Zn) < 0.005
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
Arsenic (As)
10.6
Cadmium (Cd)
< 1
Chromium (Cr)
< 1
Copper (Cu)
13.9
Lead (Pb)
< 1
Molybdenum (Mo)
< 1
Nickel (Ni)
< 1
Selenium (Se)
< 1
Thallium (TI) Low Level
< 0.2
TOTAL DISSOLVED SOLIDS
07/21/2014 09:37
TDS
34
TOTAL SUSPENDED SOLIDS
1
TSS
37
(CaCO3)
Analysis Date/Time Analyst
V_PACE
07/22/201410:50 TJA7067
07/16/2014 22:20
BGN9034
07/16/2014 22:20
BGN9034
07/16/2014 22:20
BGN9034
07/20/201410:20 JRF7131
07/21/2014 09:37
MHH7131
07/21/2014 09:37
MHH7131
07/21/2014 09:37
MHH7131
07/21/2014 09:37
MHH7131
07/21/2014 09:37
MHH7131
mg/L
0.01
1
EPA 200.7
07/21/2014 09:37
MHH7131
mg/L
0.005
1
EPA 200.7
07/21/2014 09:37
MHH7131
mg/L
0.005
1
EPA 200.7
07/21/2014 09:37
MHH7131
mg/L
0.005
1
EPA 200.7
07/21/2014 09:37
MHH7131
ug/L
1
1
EPA 200.8
07/18/2014 12:11
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:11
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:11
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:11
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:11
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:11
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:11
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:11
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:11
JAHERMA
ug/L
0.2
1
EPA 200.8
07/18/2014 12:11
JAHERMA
mg/L
N1 25
1
SM2540C
07/21/201414:52
DSBAKEI
mg/L
N1 23
1
SM2540D
07/17/201411:45
DSBAKE1

Certificate of Laboratory Analysis Page 5 of 22
This report shall not be reproduced, except in full.
Order # J14070330
Site: SW 006 Sample #: 2014020715
Collection Date: 15 -Jul -14 5:40 PM Matrix: NPDES
Analyte Result Units Qualifiers RDL DF Method
OIL AND GREASE IN WATER - SOLID PHASE EXTRACTION - (Analvsis_Performed bV Pace Laboratories
Vendor Parameter Complete
Antimony (Sb)
N1
Arsenic (As)
4.32
Vendor Method
< 1
Chromium (Cr)
25.0
Copper(Cu)
20.5
Lead (Pb)
CHEMICAL OXYGEN DEMAND
Molybdenum (Mo)
1.86
Nickel (Ni)
14.8
Selenium (Se)
COD 25
mg/L
N1
20
1
HACH 8000
INORGANIC IONS BY IC
TOTAL SUSPENDED SOLIDS
1
TSS
320
MHH7131
Chloride < 1
mg/L
1
1
10
EPA 300.0
Fluoride < 1
mg/L
1
1
10
EPA 300.0
Sulfate 770
mg/L
N1
10
100
EPA 300.0
MERCURY (COLD VAPOR) IN WATER
1
1
EPA 200.8
07/18/2014 12:16
JAHERMA
Mercury (Hg) 0.18
ug/L
1
0.05
1
EPA 245.1
TOTAL RECOVERABLE METALS BY ICP
1
1
EPA 200.8
07/18/2014 12:16
JAHERMA
Aluminum (AI) 12.3
mg/L
1
0.005
1
EPA 200.7
Barium (Be) 0.160
mg/L
1
0.005
1
EPA 200.7
Boron (B) < 0.05
mg/L
1
0.05
1
EPA 200.7
Calcium (Ca) 181
mg/L
B1
0.1
10
EPA 200.7
Hardness 480
mg/L
1
0.19
1
EPA 200.7
Iron (Fe) 19.9
Magnesium (Mg) 6.76
Manganese (Mn) 0.355
Zinc (Zn) 0.664
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
Arsenic (As)
4.32
Cadmium (Cd)
< 1
Chromium (Cr)
25.0
Copper(Cu)
20.5
Lead (Pb)
10.5
Molybdenum (Mo)
1.86
Nickel (Ni)
14.8
Selenium (Se)
4.89
Thallium (TI) Low Level
0.326
TOTAL DISSOLVED SOLIDS
07/21/2014 09:50
TDS
690
TOTAL SUSPENDED SOLIDS
1
TSS
320
Analysis Date/Time Analyst
V_PACE
07/22/201410:50 TJA7067
07/16/2014 22:38 BGN9034
07/16/2014 22:38 BGN9034
07/16/2014 22:38 BGN9034
07/20/201410:23 JRF7131
07/21/2014 09:50 MHH7131
07/21/2014 09:50 MHH7131
07/21/2014 09:50 MHH7131
07/21/2014 09:50 MHH7131
07/21/2014 09:50 MHH7131
(CaCO3)
mg/L
0.01
1
EPA 200.7
07/21/2014 09:50
MHH7131
mg/L
0.005
1
EPA 200.7
07/21/2014 09:50
MHH7131
mg/L
0.005
1
EPA 200.7
07/21/2014 09:50
MHH7131
mg/L
0.005
1
EPA 200.7
07/21/2014 09:50
MHH7131
ug/L
1
1
EPA 200.8
07/18/2014 12:16
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:16
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:16
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:16
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:16
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:16
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:16
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:16
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:16
JAHERMA
ug/L
0.2
1
EPA 200.8
07/18/2014 12:16
JAHERMA
mg/L N1
25
1
SM2540C
07/21/201414:52
DSBAKE1
mg/L N1
25
1
SM2540D
07/17/201411:45
DSBAKE1

Certificate of Laboratory Analysis Page 6 of 22
This report shall not be reproduced, except in full.
Order # J14070330
Site: SW 015 Sample #: 2014020716
Collection Date: 15 -Jul -14 5:58 PM Matrix: NPDES
Analyte Result Units Qualifiers RDL DF Method
OIL AND GREASE IN WATER - SOLID PHASE EXTRACTION - (Analysis Performed by Pace Laboratories
Vendor Parameter Complete
Antimony (Sb)
N1
Arsenic (As)
Vendor Method
CHEMICAL OXYGEN DEMAND
< 1
Chromium (Cr)
5.87
Copper (Cu)
COD 24
mg/L
N1 20
1
HACH 8000
INORGANIC IONS BY IC
8.39
Selenium (Se)
5.54
Thallium (TI) Low Level
Chloride 4.5
mg/L
1
10
EPA 300.0
Fluoride < 1
mg/L
1
10
EPA 300.0
Sulfate 39
mg/L
N1 1
10
EPA 300.0
MERCURY (COLD VAPOR) IN WATER
ug/L
1
1
EPA 200.8
Mercury (Hg) < 0.05
ug/L
0.05
1
EPA 245.1
TOTAL RECOVERABLE METALS BY ICP
07/18/2014 12:20
JAHERMA
ug/L
1
Aluminum (Al) 2.27
mg/L
0.005
1
EPA 200.7
Barium (Ba) 0.030
mg/L
0.005
1
EPA 200.7
Boron (B) < 0.05
mg/L
0.05
1
EPA 200.7
Calcium (Ca) 13.8
mg/L
0.01
1
EPA 200.7
Hardness 46.1
mg/L
0.19
1
EPA 200.7
Iron (Fe) 2.72
Magnesium (Mg) 2.82
Manganese (Mn) 0.255
Zinc (Zn) 0.468
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
Arsenic (As)
5.70
Cadmium (Cd)
< 1
Chromium (Cr)
5.87
Copper (Cu)
12.2
Lead (Pb)
4.91
Molybdenum (Mo)
1.97
Nickel (Ni)
8.39
Selenium (Se)
5.54
Thallium (TI) Low Level
0.351
TOTAL DISSOLVED SOLIDS
07/21/2014 09:45
TDS
100
TOTAL SUSPENDED SOLIDS
1
TSS
76
Analysis Date/Time Analyst
V_PACE
07/22/201410:50 TJA7067
07/16/201419:52
BGN9034
07/16/201419:52
BGN9034
07/16/201419:52
BGN9034
07/20/201410:25 JRF7131
07/21/2014 09:45
MHH7131
07/21/2014 09:45
MHH7131
07/21/2014 09:45
MHH7131
07/21/2014 09:45
MHH7131
07/21/2014 09:45
MHH7131
(CaCO3)
mg/L
0.01
1
EPA 200.7
07/21/2014 09:45
MHH7131
mg/L
0.005
1
EPA 200.7
07/21/2014 09:45
MHH7131
mg/L
0.005
1
EPA 200.7
07/21/2014 09:45
MHH7131
mg/L
0.005
1
EPA 200.7
07/21/2014 09:45
MHH7131
ug/L
1
1
EPA 200.8
07/18/2014 12:20
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:20
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:20
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:20
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:20
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:20
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:20
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:20
JAHERMA
ug/L
1
1
EPA 200.8
07/18/2014 12:20
JAHERMA
ug/L
0.2
1
EPA 200.8
07/18/2014 12:20
JAHERMA
mg/L N1
25
1
SM2540C
07/21/201414:52
DSBAKE1
mg/L N1
8.33
1
SM2540D
07/17/201411:45
DSBAKE1

Certificate of Laboratory Analysis
This report shall not be reproduced, except in full.
Order # J14070330
Site: SW 002 Sample #: 2014020717
Collection Date: 15 -Jul -14 6:10 PM Matrix: NPDES
Analyte Result Units Qualifiers RDL DF Method
OIL AND GREASE IN WATER - SOLID PHASE EXTRACTION - (Analysis Performed by Pace Laboratories
Vendor Parameter
Complete
07/21/2014 09:41
N1
07/21/2014 09:41
MHH7131
Vendor Method
CHEMICAL OXYGEN DEMAND
07/21/2014 09:41
MHH7131
07/21/2014 09:41
MHH7131
07/21/2014 09:41
MHH7131
COD
< 20
mg/L
N1
20
1
HACH 8000
INORGANIC IONS BY IC
Chloride
7.9
mg/L
1
10
EPA 300.0
Fluoride
< 1
mg/L
1
10
EPA 300.0
Sulfate
15
mg/L
N1
1
10
EPA 300.0
MERCURY (COLD VAPOR) IN WATER
Mercury (Hg)
< 0.05
ug/L
0.05
1
EPA 245.1
TOTAL RECOVERABLE METALS BY ICP
Aluminum (AI)
0.153
mg/L
0.005
1
EPA 200.7
Barium (Ba)
0.021
mg/L
0.005
1
EPA 200.7
Boron (B)
0.077
mg/L
0.05
1
EPA 200.7
Calcium (Ca)
10.4
mg/L
B1
0.01
1
EPA 200.7
Hardness
41.0
mg/L
0.19
1
EPA 200.7
(CaCO3)
Iron (Fe)
0.184
mg/L
0.01
1
EPA 200.7
Magnesium (Mg)
3.67
mg/L
0.005
1
EPA 200.7
Manganese (Mn)
0.016
mg/L
0.005
1
EPA 200.7
Zinc (Zn)
0.011
mg/L
0.005
1
EPA 200.7
TOTAL RECOVERABLE METALS BY ICP -MS
Antimony (Sb)
< 1
ug/L
1
1
EPA 200.8
Arsenic (As)
< 1
ug/L
1
1
EPA 200.8
Cadmium (Cd)
< 1
ug/L
1
1
EPA 200.8
Chromium (Cr)
< 1
ug/L
1
1
EPA 200.8
Copper (Cu)
5.91
ug/L
1
1
EPA 200.8
Lead (Pb)
< 1
ug/L
1
1
EPA 200.8
Molybdenum (Mo)
1.70
ug/L
1
1
EPA 200.8
Nickel (Ni)
<1
ug/L
1
1
EPA 200.8
Selenium (Se)
< 1
ug/L
1
1
EPA 200.8
Thallium (TI) Low Level
< 0.2
ug/L
0.2
1
EPA 200.8
TOTAL DISSOLVED SOLIDS
TDS
89
mg/L
N1
25
1
SM2540C
TOTAL SUSPENDED SOLIDS
TSS
< 6
mg/L
N1
5
1
SM2540D
Page 7 of 22
Analysis Date/Time Analyst
V_PACE
07/22/201410:50 TJA7067
07/16/2014 22:57 BGN9034
07/16/2014 22:57 BGN9034
07/16/2014 22:57 BGN9034
07/20/201410:13 JRF7131
07/21/2014 09:41
MHH7131
07/21/2014 09:41
MHH7131
07/21/2014 09:41
MHH7131
07/21/2014 09:41
MHH7131
07/21/2014 09:41
MHH7131
07/21/2014 09:41
MHH7131
07/21/2014 09:41
MHH7131
07/21/2014 09:41
MHH7131
07/21/2014 09:41
MHH7131
07/18/201412:24
JAHERMA
07/18/201412:24
JAHERMA
07/18/201412:24
JAHERMA
07/18/201412:24
JAHERMA
07/18/201412:24
JAHERMA
07/18/201412:24
JAHERMA
07/18/201412:24
JAHERMA
07/18/201412:24
JAHERMA
07/18/201412:24
JAHERMA
07/18/201412:24
JAHERMA
07/21/201414:52 DSBAKEI
07/17/201411:45 DSBAKE1

Certificate of Laboratory Analysis Page 8 of 22
This report shall not be reproduced, except in full.
Order # J14070330
Qualifiers:
B1 Target analyte detected in method blank at or above the reporting limit. Target analyte concentration in
sample was greater than 1 OX the concentration of the target analyte detected in the method blank. Analyte
concentration in sample is not affected by contamination.
N1 See additional information listed below.
- Additional Information --
The samples were received at 7.9 C which is does not meet preservation requirements for TSS, TDS, Sulfate, Oil
and Grease, COD.

aceAnalytical
www.pacelabs.com
July 17, 2014
Program Manager
Duke Energy
13339 Hagers Ferry Road
Bldg. 7405 MG30A2
Huntersville, NC 28078
RE: Project: J14070330
Pace Project No.: 92209584
Pace Analytical Services, Inc.
VR�RcW Ye. Suite 100
Huntersville, NC 28078
[phone]
Dear Program Manager:
Enclosed are the analytical results for sample(s) received by the laboratory on July 16, 2014. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
HORIZON Database Administrator
Enclosures
cc: Program Manager, Duke Energy
Rodney Wike, Duke Energy
9e0 p't�Q`
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 13

,�acmnalytical"
www.pacelabs.com
Project: J14070330
Pace Project No.: 92209584
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Virginia/VELAP Certification #: 460221
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
op8aKiec8y2hp. Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 13

REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 13
Pace Analytical Services, Inc.
®
• aceAnalXical
�gBgfliRcef�e. Suite 100
99 HuntersNlle, NC 28078
vimpacelabs.com
[phone]
SAMPLE ANALYTE COUNT
Project: J14070330
Pace Project No.: 92209584
Analytes
Lab ID Sample ID
Method
Analysts
Reported Laboratory
92209584001 2014020714
EPA 1664B
CLW
1 PASI-C
92209584002 2014020715
EPA 16648
CLW
1 PASI-C
92209584003 2014020716
EPA 1664B
CLW
1 PASI-C
92209584004 2014020717
EPA1664B
CLW
1 PASI-C
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 13

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
0e8a Iilnyle. Suite 100
y Huntersville, NC 28078
[phone]
PROJECT NARRATIVE
Project: J14070330
Pace Project No.: 92209584
Method: EPA 1664B
Description: HEM, Oil and Grease
Client: Duke Energy
Date: July 17, 2014
General Information:
4 samples were analyzed for EPA 1664B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Surrogates:
All surrogates were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 4 of 13

�acleAnalj&a!
www.pacelabs.com
ANALYTICAL RESULTS
Project: J14070330
Pace Project No.: 92209584
Pace Analytical Services, Inc.
j
0g8a gSye. Suite 100
Huntersville, NC 28078
[phone]
Sample: 2014020714 Lab ID: 92209584001 Collected: 07/15/14 15:28 Received: 07/16/14 16:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 07/17/14 16:30
Date: 07/17/2014 07:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 13

�-aceAnalyfica(
wwwpacelabs.com
ANALYTICAL RESULTS
Project: J14070330
Pace Project No.: 92209584
Pace Analytical Services, Inc.
� $9 Kl V2"� a- Suite 100
y Hunterswlle, NC 28078
[phone]
Sample: 2014020715 Lab ID: 92209584002 Collected: 07/15/14 17:40 Received: 07/16/14 16:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 16648
Oil and Grease ND mg/L 5.0 1 07/17/14 16:31
Date: 07/17/2014 07:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 13

Pace Analytical Services, Inc.
® oqg Kligcff�e. Suite 100
' aceAnalyt oal Huntersville, NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: J14070330
Pace Project No.: 92209584
Sample: 2014020716 Lab ID: 92209584003 Collected: 07/15/14 17:58 Received: 07/16/14 16:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
HEM, Oil and Grease Analytical Method: EPA 1664B
Oil and Grease ND mg/L 5.0 1 07/17/14 16:31
Date: 07/17/2014 07:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 7 of 13

�AoeAnalydoal"
www.pacelabs.com
ANALYTICAL RESULTS
Project: J14070330
Pace Project No.: 92209584
Pace Analytical Services, Inc.
papKli wke. Suite 100
Huntersville, NC 28078
[phone]
Sample: 2014020717 Lab ID: 92209584004 Collected: 07/15/14 18:10 Received: 07/16/14 16:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM, Oil and Grease Analytical Method: EPA 16646
Oil and Grease ND mg/L 5.0 1 07/17/14 16:31
Date: 07/17/2014 07:38 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 13

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: J14070330
Pace Project No.: 92209584
QC Batch: GCSV/18263 Analysis Method: EPA 16648
QC Batch Method: EPA 1664B Analysis Description: 1664 HEM, Oil and Grease
Associated Lab Samples: 92209584001, 92209584002, 92209584003, 92209584004
METHOD BLANK: 1244255 Matrix: Water
Associated Lab Samples: 92209584001, 92209584002, 92209584003, 92209584004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 07/17/14 16:26
Pace Analytical Services, Inc.
098 Ki�cfr�e. Suite 100
a Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
1244256
Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 37.6
94
78-114
MATRIX SPIKE SAMPLE:
1244257
92209020001 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
ND 40
36.6
90
78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/17/2014 07:38 PM without the written consent of Pace Analytical Services, Inc..
Page 9 of 13

aceAnalytical
wmpacelab&com
QUALIFIERS
Project: J14070330
Pace Project No.: 92209584
DEFINITIONS
Pace Analytical Services, Inc.
0$6a li'ny;g�ye. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-C Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/17/2014 07:38 PM without the written consent of Pace Analytical Services, Inc.. Page 10 of 13

�-'aceAnalyfical"
www.pacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: J14070330
Pace Project No.: 92209584
Lab ID Sample ID QC Batch Method
92209584001
2014020714
EPA1664B
92209584002
2014020715
EPA1664B
92209584003
2014020716
EPA1664B
92209584004
2014020717
EPA1664B
Pace Analytical Services, Inc.
of0gKi§cff�e. Suite 100
99 Huntersville, NC 28078
[phone]
QC Batch Analytical Method
GCSW18263
GCSV/18263
GCSW18263
GCSW18263
REPORT OF LABORATORY ANALYSIS
Analytical
Batch
This report shall not be reproduced, except in full,
Date: 07/17/2014 07:38 PM without the written consent of Pace Analytical Services, Inc.. Page 11 of 13

1'7P540Alkrlyticul Sample Condition Upon Receipt S
• ! Document Number:
( F-CHR-CS-003-rev.14
Client Name:d)44 �bck/ - ?X-lewS C r2.Q-K
1 of 2
issuing Authoph& 20 of 22
Pace Huntersville Quality Office
Courier:Fed Ex [IUPS❑ USPS❑ Client❑ Commercial❑ Pace Other
Custody /(Seal on Cooler/Box Present: ❑ yes P no Seals intact: ❑ yes ❑ no
Packing Material: ❑ Bubble Wrap Bubble Bags ❑ None ❑ Other '���
Thermometer Used: IR Gun T1102 T1401 ' Type of Ice: Wets Blue None LQf�amples on ice, cooling process has begun
,r--. rl--,...as..-, 0...4— T•i4n7• Aln i'nrrcnfinn TV41114• Aln r r%rronfinn
Temp.: oC
Corrected Cooler Tem
g. Date and Initials of U xa ini g
Biological Tissue is Frozen: Yes N N/A '7 �(0 c�
contents •
Temp should be above freezing to 6°C
Comments:
Chain of Custody Present:
s ❑No
❑N/A 1.
Chain of Custody Filled Out:
Layes []No
❑NIA
2.
Chain of Custody Relinquished:
%Z%s ❑No
❑NIA
3.
Sampler• Name & Signature on COC:
Wes ❑No
❑NIA
4.
Samples Arrived within Hold Time:
'des DNo
❑N/A
5.
Short Hold Time Analysis (<72hr):
❑Yes 142
❑N/A
6.
Rush Turn Around Time Requested:
Wes ❑No
❑N/A
7.
Sufficient Volume:
�es ❑No
❑N/A
8.
Correct Containers Used:
7 []Yes []No
El NIA
9, a C -O A �d1 t
0'%)lTC-�C'
SLY C
-Pace Containers Used:
❑Yes Zo
❑NIA
a ,l1CY
Y ' Y/
Containers Intact:
s ❑No
❑N/A
10.
Filtered volume received for Dissolved tests
❑Yes []No
W
11.
Sample Labels match COC:
V ess
❑NIA
12.
�❑No
-includes date/time/ID/Analysis Matrix: (J3aA-C/'r
All containers needing preservation have been checked.
[]Yes []No
1�1/A
13.
All containers needing preservation are found to be in
❑Yes ❑NotI/A
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, W -DRO (water)
?es ONO
Samples checked for dechlorination:
❑Yes ❑No
/A
14.
•
Headspace in VOA Vials (>6mm):
❑Yes ❑No
/A
15.
Trip Blank Present:
❑Yes ❑No
\YZA
16.
Trip Blank Custody Seals Present
❑Yes ❑No
�1/A
1
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution: Field Data Required? Y / N
Person Contacted:
Comments/ Resolution:
Date/Time:
SCURF Review: Date: bVV&
SRF Review: 22
Date: 7 /'7 I
Note: Whenever the a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp,
incorrect containers)
Place label here
zZGnS I OR
Handwrite project number
(if no label available)
Page 12 of 13

N
N
O
N
N
0)
m
a
s
CHAIN OF CUSTODY RECORD AND ANALYSIS REQUEST FORM (�
r - - _--
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Mao Coa. meoaAs iaataieg 7�os) :Order # y Matrix NPDES NC— Page _t _ of _7
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Chain of Custody 3 rweenrWr,, N. c xaora ) Logg.d By Date a rime ORIGINAL to LAB. COPY to CLIENT
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Sample Log (70a)a7537a3 A� , SAMPLE PROGRAM
Pet
_
._ _._...�. _ _Far 0� a75L07! DO Ground Water NPDES
�- - —
,Pr4er,iM
r Vendor q
Bale" Creek 1P11ooe No: i Drinking Water _ LIST—
i �. 1 W,rto
RCRA
Soap Sampling
Client Josh Quinn, Melonia MartiFax No:n, ggD-875so32 �
Allen Stowe , I PACE S um) Unfiltered b
Business Unit: Poo,rar. SENVrlr IRnp. P -W To: -
votive leo •we. leo ,csa
Pmj.aroi s54t— ac TYrD: 11
aacoon: PO# 6537197�L,rO MGD3A3 t(ml) 20110 1000 300 25D FIELD MEASUREMENTS
aMrDOdy: Statbn: _t
Container Type PET Glass PET HDPE HOPE
a CE c
v U E U N
Sample Description or ID --
P P Cusrorrrer to eompiery all appropriate a U. to o a ci a C to c
aon�horded a -a:% y N
V V
_
.......... Collection Information y tj N O G UI'o N tj1 U Z~ 9 ro
GPS LocationE a y p = e vM uri .: ti m w o
Date Timo Signature $ 0 1- O U U a 1, in x Q U 2 to x t-
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716 -•el �6?1 �
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y 9
o
•14 Days
7Days
-_Age
Dat in a (Accepted By. DateMme
RSo3W-.=0ck*d
By Da[clTtttue Ope By Daterrima
�SealedlLock
3
• 48 Hr
•Other_ASAP
�ama�
ELEMENTS by ICP -MS (Digested-TRM): As, Cd, Cr, Cu, 161o, Ni, Pb, a (CRC Metbod) TI (low levoq Hy by 245.1
ELEMENTS by ICP (Digested TRM): Al, Be, B, Fe, Mn, ran Please copy Tim Hunsucker on extol EDD results
.=1
'Add. Cost Will ADoly
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IS
Z
04
(5 Dom_
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7,
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2
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0
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0
0
0
0
0
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0
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0
TOTAL
Retinqui*ed By
■ DatefTinw
AW^/D?
Accepted By.
/ Daterrime
2
Requested Turnaround
WNW-
I57 19
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e
Roffn-qu I I batemme
Accepted By Datemaiii
/
716 -•el �6?1 �
� �
y 9
o
•14 Days
7Days
-_Age
Dat in a (Accepted By. DateMme
RSo3W-.=0ck*d
By Da[clTtttue Ope By Daterrima
�SealedlLock
3
• 48 Hr
•Other_ASAP
�ama�
ELEMENTS by ICP -MS (Digested-TRM): As, Cd, Cr, Cu, 161o, Ni, Pb, a (CRC Metbod) TI (low levoq Hy by 245.1
ELEMENTS by ICP (Digested TRM): Al, Be, B, Fe, Mn, ran Please copy Tim Hunsucker on extol EDD results
.=1
'Add. Cost Will ADoly
Total Fs]
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M
0
co
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c
m
0-
k/D I U- PRK614 IA
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___.____ __ _ _ _._s�. ' '-' Analytical Laboratory Use only �i Page 22 of 22
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Analytical Laboratory typett.grn Forty Rd } 1(1 T_V1DO I
} Chain of Custody & tt mmnwm. N.C. 79078 i 'Logoea ey Date & Tune ORIGINAL to LAB, COPY to CLIENT
Sample Log poa)87ss7e5 ' ��o /_' : �O SAMPLE PROGRAM t
' I lY Ground Water_ NPDES_
Vendor�' Q Dmkiny wale( UST
Prolog Nam. Belews Creek IPnO"'nO' I I RCRAwaste_ ' COC REV DAT 4128l201A
Seep Sampling ._
- -- _
Client Josh Quinn, Melonia Martin,
YI _ __ -_ 900 8765032 , +- PACE S um)l Unfiltered
Relinquished By Date/Ttme IAccepted
ReI afsho ~i7_1�) ,N•"A�/ ato�hima ZJ
Rmtttr� y Dat into �]Accept
By. DatelTime�
Acee od By: Datemme
IAceep d By: DatefTime
Requested Turnaround
•14 Days -
7 Days V
'48 Hr
'Other ASAP
'Add. Cost Will APPIY
SoalfLocked ByDatcfrlme
ScalodlLack Opc d By Dntcmo
� rTl�
tA9Yi3®p1 6iQ1icyJ u &W 309.4
Total
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