WQ0033589_Monitoring - 09-2016_20161027 (3)

Environmental Chemists, Inc.
enviroche, 1 7i 6602 Wmdmili Way, Wilmington, NC 28405 ° 910.392.0223 Lab u 910.392.4424 Fax
® 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Atlantic Coast Underground Date of Report: Oct 20, 2016
5115 Pine Hill Lane Manteo Report #: 16M-1806
Kitty Hawk NC 27949 Report #: 2016-14504
Attention: Irvin Edwards Jr. Customer ID: 09070020
Project ID: Jennetts Pier/ NC Aquarium
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
16-35157 Site: Effluent 1 54 6. 101 l __ Water I.W. Edwards Jr.
Test Method Results Date Analyzed
Ammonia Nitrogen
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
Nitrate+Nitrite-Nitrogen
Total Nitrogen
EPA 350.1 < 0.2 mg/L 10111/2016
EPA 351.2 < 0.5 mg/L 10/1412016
EPA 353.2 4.91 mg/L 10/12/2016
Total Nitrogen 4.9 mg/L 10/18/2016
Lab ID Sample ID: M-3503 Collect Date/Time Matrix Sampled by
16-35158 Site: Effluent 10/6/2016 12:15 PM Water I.W. Edwards Jr.
Test Method results Date Analyzed
Residue Suspended (TSS) SM 2540 D <2.6 mg/L 10/06/2016
BOD SM 5210 B <2 mg/L 10/06/2016
Fecal Coliform SM 92= MF <1 Colonies/100ml- 10/0612016
Comment:
Reviewed by: XJ=
Report #n 2016-14504 Page 1 of 1

[enviroehe]m
ANALYTICAL & CONSULTING CHEMISTS
Atlantic Coast Underground
5115 Pine Hill Lane
Kitty Hawk . NC
Attention: Junior Edwards
Lab ID Sample ID:
16-30421 Site: Effluent
Environmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ° 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Sep 19, 2016
Manteo Report #: 16M-1587
27949 Report 0: 2016-12514
Customer ID: 09070020
Project ID: Jennetts Pier/ NC Aquarium
Collect Date/Time Matrix Sampled by
9/1/2016 11:30 AM Water I.W. Edwards Jr.
Test
Method
Results
Date Analyzed
Ammonia Nitrogen
EPA 350.1
< 0.2 mg/L
09/05/2016
Total Phosphorus
SM 4500 P F
5.59 mg/L
09/12/2016
Total Nitrogen (Cale)
Total Kjeldahi Nitrogen (TKN)
EPA 351.2
0.8 mg/L
09/10/2016
Nitrate+Nitrite-Nitrogen
EPA 363.2
0.62 mg/L
09/07/2016
Total Nitrogen
Total Nitrogen
1.4 mg/L
09/12/2016
Lab ID Sample ID: W062 Collect DatelTime Matrix Sampled by
16-30422 Site: Effluent 9/1/2016 11:30 AM Water I.W. Edwards Jr.
Test Method Results Date Analyzed
Residue Suspended (TSS) SM 2540 D <2.6 mg/L 09101/2016
BOD SM 521013 <2 mg/L 09/02/2016
Sample estimated. Did not meet quality control requirements. CGA above acceptable limits of 167.5-228.5mg/L
Fecal Coliform SM8222DMF <1 Colonies/100ml- 09/01/2016
Comment:
t
Reviewed by: &LWQX
Report* 2016-12514 Page 1 of 1

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G6+9R�aWiad�dill�'�ay
Wihnington, NC 28405
Phone: [phone]
Fax: [phone]
NCDENC, DWQ Certificate 094
ENVMONNIEINTAL
Outer Bartle
INC.
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sample Tvne: Y = in'ftfia+n+_ ' s T.�iivt►nt• W —well Cm ..�.G14.......... an 6-12
71.0 Bowsertown Road
Manteo, NC 27954
Phone: [phone]
Far: [phone]
NCDENC, DWQ Certificate #628
Report No: 1(p M ! 5A
Sample Identifications
A
Collection
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Nom_ DI;CHLORi1�ATION : Samples for Ammonia, TjKN, Cyanide, Pfi ol, and IIacteria must be decldorin ted (t1.2 ppm or less) in the field at
the time of collection. See reverse side for instructions.
Transfer Relinquished B : Date/Time0 Received By: Date/Time
SIN TV
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Temperature when Received., . 1 Arran+nri.
Delivered By:. ti . ; - - -- ' �""-� i 1SrgP1 LAAO
COI1lfnentS:
(, Received By: _roQ,`jj�

Environmental Chemists, Inc.
7envirochem 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax
® 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax
ANALYTICAL & CONSULTING CHEMISTS [e-mail]
Atlantic Coast Underground
Date of Report: Sep 21, 2016
5115 Pine Hill Lane
Manteo Report #: 16M-1596
Kitty Hawk NC 27949
Report #: 2016-12640
Attention: Junior Edwards
Customer ID: 09070020
Project ID: Jennetts Pier/ NC Aquarium
Lab ID Sample 1D:
Collect Date/Time Matrix Sampled by
16-30717 Site: Effluent
9/6/2016
10:00 AM Water I.W. Edwards Jr.
Test
Method
Results Date Analyzed
Ammonia Nitrogen
EPA 350.9
0.2 mg/L 09/08/2016
Total Phosphorus
SM 4500 P F
3.77 mg/L 09/15/2016
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 361.2
1.0 mg/L 09/14/2016
Nitrate+Nitrite-Nitrogen
EPA 353.2
0.51 mg/L 09/08/2016
Total Nitrogen
TWO NlbWen
1.5 mg/L 09/21/2016
Lab lD Sample ID: M-3082
Collect DatelTime Matrix Sampled by
16-30718 Site: Effluent
9/6/2016
10:00 AM Water I.W. Edwards Jr.
Test
Method
Results Date Analyzed
Residue Suspended (TSS)
SM 2540 D
<2.6 mglL 09/08/2016
BOD
SM 5210 a
<2 mg/L 09/07/2016
Fecal Coliform
SM 9222D MF
<1 Colonies/100ml- 09/06/2016
Comment
Reviewed by:
Report#: 2016-12640 Page 1 of 1

6mWind1iiilFway
Wilmington, NC 2.8405
Phone: [phone]
Fax: [phone]
NCDENC, DWQ Certificate #94
ENVMONMENTAL CHEMISTS, INC.
Outer Banksbivision
Samule Collection -and! Chain of Custody
a.wiec�eq is • .� • w. k : w a. Sri,•.
tSaninli! Tvnw Y a TJJflnant_. i1'_ = T_Pilnnra+ vu ccxr..11 o•r_nJ• --- nn _,2_H rtr — m --J_- AL1_ - --
710 Bowsertown Road
Manteo, NC 27954
Phone: [phone]
P'ax: [phone]
NCDENC, DWQ Certiricate 0628
Sample Identification
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Collection
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PRESERVATION
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DATE TIMI
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NOTICE — DLCHI .QRINATION : Samples for Ammonia, TKN, Cyanide, Phe ol, and Bacterix ifiust be dechlorinated (0.2 ppm or less) in the field at
the time of collection. See reverse aide for instructions.
Transfer
Relenquished By:
Date/Time i
Received By:
Date/Time
1.�
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Unnerature when
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Delivered By. �� ` Received By.� � ,,gate; q •� ime;
Comments: