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HomeMy WebLinkAboutWQ0007026_Monitoring - 09-2016_20161024 (4)Description: MW -1 Matrix: Ground Water Project: Groundwater Mcinitoring(Sep) ANALYTICAL RESULTS Lab Sample ID:CZ11268-01 Sampled: 09/13/16 09:40 Sampled By: Randall 3arrell Received: 09/13/16 13:15 Work Order: CZ11268 (Volatile Organic Compounds by GCMS ^ - ENCO(3ry ceitified anatyte (NC 5911 Analyte FCAS Numbed Results Flan units DF MDL POL Batch Method Analyzed _By Notes 1,1,1,2 -Tetrachloroethane [630-20-6]^ < 0.091 ug/L 1 0.091 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ 1,1,1 -Trichloroethane [71-55-61^ < 0.15 ug/L 1 0.15 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ 1,1,2,2 -Tetrachloroethane [79-34-5]^ < 0,085 ug/L 1 0.085 0.50 6I13021 EPA 8260B16230D 09/13/16 16:16 MSZ 1,1,2 -Trichloroethane (79-00-5]^ < 0.068 ug/L 1 0.068 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ 1,1-Dichloroethane [75-34-3]^ < 0.050 ug/L 1 0.050 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ 1,1-Dichloroethene [75-35-4]^ < 0.15 ug/L 1 0.15 0.50 6I13021 EPA 8260B16230D 09/13/16 16:16 MSZ 1,1-Dichloropropene [563-58-6]^ < 0.063 ug/L 1 0.063 0.50 6I13021 EPA 82606/62301) 09/13/16 16:16 MSZ 1,2,3-Trichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0.25 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ 1,2,3-Trichloropropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.50 6I13021 EPA 82606/6230D 09/13/16 16:16 MSZ 1,2,4-Trichlorobenzene [120-82-1]^ < 0.097 ug/L 1 0.097 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ 1,2,4-Trimethylbenzene [95-63-61^ < 0.067 ug/L 1 0.067 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ 1,2-Dibromo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ 1,2-Dibromoethane [106-93-4]^ < 0.27 ug/L 1 0,27 0.50 6113021 EPA 8260B/6230D 09/13/16 16:16 MSZ 1,2 -Dichlorobenzene [95-50-1]^ < 0.062 ug/L 1 0.062 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ 1,2-Dichloroethane [107-06-21^ < 0.082 ug/L 1 0.082 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ 1,2-Dichloropropane [78-87-S]^ < 0.098 ug/L 1 0.098 0.50 6113021 EPA 8260B/6230D 09/13/16 16:16 MSZ 1,3,5-Trimethylbenzene [108-67-8]^ < 0.10 ug/L 1 0.10 0.50 6I13021 EPA 82608/62301) 09/13/16 16:16 MSZ 1,3 -Dichlorobenzene [541-73-1]^ < 0.092 ug/L 1 0.092 0.50 6I13021 EPA 82608/6230D 09/13/16 16:16 MSZ 1,3-Dichloropropane [142-28-9]^ < 0.15 ug/L 1 0.15 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ 1,4 -Dichlorobenzene [106-46-7]^ < 0.10 ug/L 1 0.10 0.50 6I13021 EPA 82606/6230D 09/13/16 16:16 MSZ 2,2-Dichloropropane [594-20-7]^ < 0.12 ug/L 1 0.12 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ 2-Chlorotoluene [95-49-8]^ < 0.10 ug/L 1 0.10 0.50 6113021 EPA 8260B/6230D 09/13/16 16:16 MSZ 4-Chlorotoluene [106-43-4]^ < 0.10 ug/L 1 0.10 0.50 6I13021 EPA 82606/6230D 09/13/16 16:16 MSZ 4-Isopropyltoluene [99-87-6]^ < 0.066 ug/L 1 0.066 0.50 6I13021 EPA 82608/62301) 09/13/16 16:16 MSZ Benzene [71-43-2)A < 0.050 ug/L 1 0.050 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Bromobenzene [108-86-1]^ < 0.13 ug/L 1 0.13 0.50 6I13021 EPA 8260B/6230D 03/13/16 16:16 MSZ Bromochloromethane [74-97-5]^ < 0.11 ug/L 1 0.11 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Bromodichloromethane [75-27-4]^ < 0.010 ug/L 1 0.010 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Bromoform [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 M5Z Bromomethane [74-83-9]^ < 0.28 ug/L 1 0.28 0.5o 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Carbon Tetrachloride [56-23-5]^ < 0.082 ug/L 1 0.082 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Chlorobenzene(108-90-7]^ < 0.069 ug/L 1 0.069 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Chloroethane [75-00-3]^ < 0.18 ug/L 1 0.18 0.50 6113021 EPA 8260B/6230D 09/13/16 16:16 MSZ Chloroform [67-66-3]^ < 0.083 ug/L 1 0.083 0.50 6113021 EPA 8260B/6230D 09/13/16 16:16 MSZ Chloromethane [74-87-31^ < 0.050 ug/L 1 0.050 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ cis-1,2-Dichloroethene [156-59-2]^ < 0.075 ug/L 1 0.075 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ cis-1,3-Dichloropropene [10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Dibromochloromethane [124-48-1]^ < 0.067 ug/L 1 0.067 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Dibromomethane [74-95-3]^ < 0.13 ug/L 1 0.13 0.50 6113021 EPA 8260B/6230D 09/13/16 16:16 MSZ Dichlorodifluoromethane [75-71-8]^ < 0.091 ug/L 1 0.091 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Ethylbenzene[100-41-4]^ < 0.10 ug/L 1 0.10 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Hexachlorobutadlene [87-68-3]^ < 0.15 ug/L 1 0.15 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Isopropyl Ether (108-20-3]^ < 0.20 ug/L 1 0.20 0.50 6I13021 EPA 82608/6230D 09/13/16 16:16 MSZ Isopropylbenzene [98-82-8]^ < 0.13 ug/L 1 0.13 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ m,p-Xylenes [108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Methylene Chloride [75-09-2]1 < 0.070 ug/L 1 0.070 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Methyl-tert-Butyl Ether [1634-04-4]A < 0.12 ug/L 1 0.12 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 4 Of ZO FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 5 Of 2O www.encolabs.com ANALYTICAL RESULTS Description: MW-1 Lab Sample ID:CZ11268-01 Received: 09/13/16 13:15 Matrix: Ground Water Sampled: 09/13/16 09:40 Work Order: CZ11268 Project: Groundwater Monitoring(Sep) Sampled By: Randall Jarrell Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flag Units DF MDL POL Batch Method Analyzed ly Notes Naphthalene [91-20-3]^ < 0.086 ug/L 1 0.086 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ n-Butyl Benzene [104-51-8]^ < 0.074 ug/L 1 0.074 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ n-Propyl Benzene [103-65-1]^ < 0.073 ug/L 1 0.073 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ o-Xylene[95-47-6]^ < 0.088 ug/L 1 0.088 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ sec-Butylbenzene [135-98-8]^ < 0.053 ug/L 1 0.053 0.50 6I13021 EPA 8260B16230D 09/13/16 16:16 MSZ Styrene [100-42-5)^ < 0.082 ug/L 1 0.082 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ tert-Butylbenzene [98-06-6]^ < 0.094 ug/L 1 0.094 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Tetrachloroethene [127-18-4]^ < 0.099 ug/L 1 0.099 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Toluene [108-88-3]^ < 0.053 ug/L 1 0.053 0.50 6I13021 EPA 8260B/62300 09/13/16 16:16 MSZ trans-1,2-Dichloroethene [156-60-51^ < 0.11 ug/L 1 0.11 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ trans-1,3-Dichloropropene [10061-02-61^ < 0.080 ug/L 1 0.080 0.50 6I13021 EPA 826013/6230D 09/13/16 16:16 MSZ Trichloroethene [79-01-6]^ < 0.13 ug/L 1 0.13 0.50 6I13021 EPA 8260B/6230D 09/13/16 16:16 MSZ Trichlorofluoromethane [75-69-4]^ < 0.15 ug/L 1 0.15 0.50 6113021 EPA 8260B/6230D 09/13/16 16:16 MSZ Vinyl chloride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 6113021 EPA 8260B/6230D 09/13/16 16:16 MSZ Xylenes (Total) [1330-20-7]A < 0.22 ug/L 1 0.22 0.50 6113021 EPA 82606/6230D 09/13/16 16:16 MSZ Surrogates Resu/ts DF Saike Lv/ % Rec % Rigg Limits Batch Method Ana/vzed _By Notes 4-Bromofluorobenzene 56 1 50.0 117 % 53-136 6113021 EPA 82608162300 09/13/16 16:16 MSZ Dibromofluoromethane 53 1 50.0 105 % 67-129 6113021 EPA 826OB16230C 09/13/1616:16 MSZ Toluene-d8 45 1 50.0 89% 59-134 6113021 EPA 826OB16230C 09/13/16 16:16 MSZ Classical Chemistry Parameters ^ - ENCO Cary certiried analyte [NC 591] Analyte rCAS Number] Results Flaa Units DF MDL POL Batch Method Analyzed By Notes Ammonia as N [7664-41-71^ < 0.045 mg/L 1 0.045 0.10 6114003 EPA 350.1 09/14/16 11:06 JLJ Chloride [16887-00-6]^ 8.5 mg/L 1 1.9 5.0 6I19013 SM 45000 E-1997 09/19/16 12:50 JLI Nitrate as N [14797-55-81^ 3.2 mg/L 1 0.025 0.10 6I19003 EPA 353.2 09/19/16 08:52 JLJ Nitrate/Nitrite as N^ 3.2 D mg/L 5 0.20 0.50 6I16003 EPA 353.2 09/16/16 11:12 JLJ Nitrite as N [14797-65-0]^ < 0.017 mg/L 1 0.017 0.10 6I13002 EPA 353.2 09/13/16 14:35 JLJ Microbiological Parameters ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flao Units DF POIL Batch Method Analyzed fly Notes Coliform, Fecal^ 28 MPN/100 1 1.0 6I19027 Colilert 18 09/14/16 09:30 RAY ml- LClassical ClassicalChemistry Parameters ^ - ENCO Orlando certfried analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed Notes Total Organic Carbon^ 15 mg/L 1 0.34 1.0 6I21029 SM 53108-2000 09/21/16 15:50 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 5 Of 2O M-1-1-11-11 XA #w c www.encolabs.com ANALYTICAL RESULTS Description: MWA Lab Sample ID:CZ11268-02 Received: 09/13/16 13:15 Matrix: Ground Water Sampled: 09/13/16 08:35 Work Order: CZ11268 Project: Groundwater Monitoring(Sep) Sampled By: Randall Jarrell lVolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte (NC 5911 Analyte fCAS Number l Results Flag Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2 -Tetrachloroethane [630-20-6]^ < 0.091 ug/L 1 0.091 0.50 6I14035 EPA 82603/6230D 09/14/16 16:38 M5Z 1,1,1 -Trichloroethane [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 1,1,2,2 -Tetrachloroethane [79-34-5]^ < 0.085 ug/L 1 0.085 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 1,1,2 -Trichloroethane [79-00-5]^ < 0.068 ug/L 1 0.068 0.50 6114035 EPA 8260B/6230D 09/14/16 16:38 MSZ 1,1-Dichloroethane [75-34-3]^ < 0.050 ug/L 1 0.050 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 1,1-Dichloroethene [75-35-4]^ < 0.15 ug/L 1 0.15 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 M5Z 1,1-Dichloropropene [563-58-6]^ < 0.063 ug/L 1 0.063 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 1,2,3-Trichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0.25 0.50 6I14035 EPA 8260B/62301) 09/14/16 16:38 MSZ 1,2,3-Trichloropropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.50 6I14035 EPA 8260B16230D 09/14/16 16:38 M5Z 1,2,4-Trichlorobenzene [120-82-1]^ < 0.097 ug/L 1 0.097 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 1,2,4-Trimethylben2ene [9S-63-61^ < 0.067 ug/L 1 0.067 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 1,2-Dibromo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 1,2-Dibromoethane [106-93-4]^ < 0.27 ug/L 1 0.27 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 1,2 -Dichlorobenzene [95-50-1]^ < 0,062 ug/L 1 0.062 0.50 6I14035 EPA 826OB/6230D 09/14/16 16:38 MSZ 1,2-Dichloroethane [107-06-2]^ < 0.082 ug/L 1 0.082 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 1,2-Dichloropropane [78-87-5]^ < 0.098 ug/L 1 0.098 0.50 6I14035 EPA 82608/62301) 09/14/16 16:38 MSZ 1,3,5-Trimethylbenzene [108-67-B]^ < 0.10 ug/L 1 0.10 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 1,3 -Dichlorobenzene [541-73-1]^ < 0.092 ug/L 1 0.092 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 1,3-Dichloropropane [142-28-9]^ < 0.15 ug/L 1 0.15 0.50 6114035 EPA 8260B/6230D 09/14/16 16:38 MSZ 1,4 -Dichlorobenzene [106-46-7]^ < 0.10 ug/L 1 0.10 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 2,2-Dichloropropane [594-20-7]^ < 0.12 ug/L 1 0.12 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 2-Chlorotoluene [95-49-8]^ < 0.10 ug/L 1 0.10 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 4-Chlorotoluene [106-43-4]^ < 0.10 ug/L 1 0.10 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ 4-Isopropyltoluene [99-87-6]^ < 0.066 ug/L 1 0.066 0.50 GI14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Benzene [71-43-2]A < 0.050 ug/L 1 0.050 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Bromobenzene [108-86-1]^ < 0.13 ug/L 1 0.13 0.50 6][14035 EPA 8260B16230D 09/14/16 16:38 MSZ Bromochloromethane [74-97-51^ < 0.11 ug/L 1 0.11 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Bromodichloromethane [75-27-4]^ < 0.010 ug/L 1 0.010 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Bromoform [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Bromomethane [74-83-9]^ < 0.28 ug/L 1 0.28 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Carbon Tetrachloride [56-23-5]^ < 0.082 ug/L 1 0.082 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Chlorobenzene [108-90-7]^ < 0.069 ug/L 1 0.069 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Chloroethane [75-00-3]^ < 0.18 ug/L 1 0.18 0.50 6I14035 EPA 626OB/6230D 09/14/16 16:38 MSZ Chloroform [67-66-3]^ < 0.083 ug/L 1 0.083 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Chloromethane [74-87-3]A < 0.050 ug/L 1 0.050 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ cis-1,2-Dichloroethene [156-59-2]^ < 0.075 ug/L 1 0.075 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ cis-1,3-Dichloropropene [10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Dibromochloromethane [124-48-1]^ < 0.067 ug/L 1 0.067 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Dibromomethane [74-95-3]^ < 0.13 ug/L 1 0.13 0.50 6][14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Dichlorodifluoromethane [75-71-8]^ < 0.091 ug/L 1 0.091 0.50 6I14035 EPA 8260B/62301) 09/14/16 16:38 MSZ Ethylbenzene [100-41-4]^ < 0.10 ug/L 1 0.10 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 M5Z Hexachlorobutadiene [87-68-3]^ < 0.15 ug/L 1 0.15 0.50 6I14035 EPA 8260B16230D 09/14/16 16:38 MSZ Isopropyl Ether [108-20-3]A < 0.20 ug/L 1 0.20 0.50 6I14035 EPA 826OB/6230D 09/14/16 16:38 MSZ Isopropylbenzene [98-82-8]^ < 0.13 ug/L 1 0.13 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ m,p-Xylenes [108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Methylene Chloride [75-09-2]^ < 0.070 ug/L 1 O.D70 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Methyl-tert-Butyl Ether [1634-04-4]A < 0.12 ug/L 1 0.12 0.50 6I14035 EPA 826OB/6230D 09/14/16 16:38 MSZ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. L Page 6 Of 20 r ANALYTICAL RESULTS Description: MW -4 Lab Sample ID:CZ11268-02 Received: 09/13/16 13:15 Matrix: Ground Water Sampled: 09/13/16 08:35 Work Order: CZ11268 Project: Groundwater Monitoring(Sep) Sampled By: Randall Jarrell (Volatile Organic Compounds by GCMS ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL Q Batch Method Analyzed By Notes Naphthalene [91-20-3]A < 0.086 ug/L 1 0.086 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ n -Butyl Benzene [104-51-8]^ < 0.074 ug/L 1 0.074 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ n -Propyl Benzene [103-65-1]^ < 0.073 ug/L 1 0.073 0.50 6114035 EPA 8260B/6230D 09/14/16 16:38 MSZ o-Xylene[95-47-6]^ < 0.088 ug/L 1 0.088 0.50 6114035 EPA 8260B/6230D 09/14/16 16:38 MSZ sec-Butylbenzene[135-98-8]^ < 0.053 ug/L 1 0.053 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Styrene [100-42-51A < 0.082 ug/L 1 0.082 0.50 6114035 EPA 8260B/6230D 09/14/16 16:38 MSZ tert-Butylbenzene [98-06-6]^ < 0.094 ug/L 1 0.094 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Tetrachloroethene[127-18-4]^ < 0.099 ug/L 1 0.099 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Toluene [108-88-3]A < 0.053 ug/L 1 0.053 0.50 6114035 EPA 8260B/6230D 09/14/16 16:38 MSZ trans-1,2-Dichloroethene [156-60-5]^ < 0.11 ug/L 1 0.11 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ trans-l,3-Dichloropropene [10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Trichloroethene [79-01-6]1 < 0.13 ug/L 1 0.13 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Trichlorofluoromethane [75-69-4]^ < 0.15 ug/L 1 0.15 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Vinyl chloride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 6I14035 EPA 8260B/6230D 09/14/16 16:38 MSZ Xylenes(Total)[1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 6114035 EPA 8260B/6230D 09/14/16 16:38 MSZ Surrogates Results DF Spike Lv/ % Re c 1/a Rec Limits Batc Method Ana/vzed By Notes 4-Bromoflucrobenzene 59 1 50.0 117 % 53-136 6114035 EPA 626OB16230C 09/14/16 16:38 MSZ D/bromofluoromethane 57 1 50.0 114% 67-129 6114035 EPA 826OB16230L 09/14/1616.•38 MSZ Toluene -d8 44 1 50.0 88% 59-134 6114035 EPA 82608162300 09/14/16 16.38 M5Z Classical Chemistry Parameters ^ - ENCO Cary certified ana/yte [NC 591J Analyte rCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes Ammonia as N [7664-41-7]^ 0.061 J mg/L 1 0.045 0.10 6I14003 EPA 350.1 09/14/16 11:08 JU Chloride [16887-00-6]^ 25 mg/L 1 1.9 5.0 6I19013 SM 45o0Cl E-1997 09/19/16 12:57 JU Nitrate as N [14797-55-8]^ 0.076 J mg/L 1 0.025 0.10 6119003 EPA 353.2 09/19/16 08:52 JU Nitrate/Nitrite as N^ 0.076 J mg/L 1 0.041 0.10 6I16003 EPA 353.2 09/16/16 11:14 JU Nitrite as N [14797-65-0]^ < 0.017 mg/L 1 0.017 0.10 6113002 EPA 353.2 09/13/16 14:36 JU Microbiological Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF SL Batch Method Analyzed Ay Notes Coliform, Fecal^ < 10 MPN/100 10 10 6119027 Colilert 18 09/14/16 09:30 RAY mL �SslcalChemistry PmOndo certified analyre [NC 424J Analyte [CAS Numberl Results Flag Units DF MDL POL Batch Method Analyzed fly Notes Total Organic Carbon^ 0.49 J mg/L 1 0.34 1.0 6121029 SM 531OB-2000 09/21/16 15:50 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full, Page 7 Of 20 www.encolabs.com ANALYTICAL RESULTS Description: MW -5 Lab Sample ID: CZ11268-03 Received: 09/13/16 13:15 Matrix: Ground Water Sampled: 09/13/16 09:10 Work Order: CZ11268 Project: Groundwater Monitoring(Sep) Sampled By: Randall Jarrell (Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flag Units DF MDL POL Batch Method Analyzed By Notes 1,1,1,2 -Tetrachloroethane [630-20-6]^ < 0.091 ug/L 1 0.091 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ 1,1,1 -Trichloroethane [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ 1,1,2,2 -Tetrachloroethane [79-34-5]^ < 0.085 ug/L 1 0.085 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ 1,1,2 -Trichloroethane [79-00-5]^ < 0.068 ug/L 1 0.066 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ 1,1-Dichloroethane [75-34-3]^ < 0.050 ug/L 1 0.050 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ 1,1-Dichloroethene [75-35-4]^ < 0.15 ug/L 1 0.15 0.50 6I14035 EPA 8260B/62301) 09/14/16 17:07 MSZ 1,1-Dichloropropene [563-58-6]^ < 0.063 ug/L 1 0.063 0.50 6I14035 EPA 8260B/62301) 09/14/16 17:07 MSZ 1,2,3-Trichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0.25 0.50 6I14035 EPA 8260B16230D 09/14/16 17:07 MSZ 1,2,3-Trichloropropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ 1,2,4-Trichlorobenzene [120-82-1]^ < 0.097 ug/L 1 0.097 0.50 6I14035 EPA 8260B/6230D 03/14/16 17:07 MSZ 1,2,4-Trimethylbenzene [95-63-6]^ < 0.067 ug/L 1 0.067 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ 1,2-Dibromo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ 1,2-Dibromoethane [106-93-4]^ < 0.27 ug/L 1 0.27 0.50 6114035 EPA 8260B/6230D 09/14/16 17:07 MSZ 1,2 -Dichlorobenzene [95-50-1]^ < 0.062 ug/L 1 0.062 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ 1,2-Dichloroethane [107-06-2]^ < 0.082 ug/L 1 0.082 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ 1,2-Dichloropropane [78-87-5]^ < 0.098 ug/L 1 0.098 0.50 6I14035 EPA 8260B/62301) 09/14/16 17:07 MSZ 1,3,5-Trimethylbenzene [108-67-8]^ < 0.10 ug/L 1 0.10 0.50 6I14035 EPA 82606/62301) 09/14/16 17:07 MSZ 1,3 -Dichlorobenzene [541-73-1]^ < 0.092 ug/L 1 0.092 0.50 6114035 EPA 82606/62301) 09/14/16 17:07 MSZ 1,3-Dichloropropane [142-28-9]^ < 0.15 ug/L 1 0.15 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ 1,4 -Dichlorobenzene [106-46-7]^ < 0.10 ug/L 1 0.10 0.50 6I14035 EPA 8260B/62301) 09/14/16 17:07 MSZ 2,2-Dichloropropane [594-20-7]^ < 0.12 ug/L 1 0.12 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ 2-Chlorotoluene [95-49-8]^ < 0.10 ug/L 1 0.10 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ 4-Chlorotoluene [106-43-4]^ < 0.10 ug/L 1 0.10 0.50 6I14035 EPA 8260B/62301) 09/14/16 17:07 MSZ 4-Isopropyltoluene [99-87-6]^ < 0.066 ug/L 1 0.066 0.50 6I14035 EPA 8260B/62301) 09/14/16 17:07 MSZ Benzene [71-43-2]^ < 0.050 ug/L 1 0.050 0.5D 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Bromobenzene [108-86-1]^ < 0.13 ug/L 1 0.13 0.50 6114035 EPA 8260B/6230D 09/14/16 17:07 MSZ Bromochloromethane [74-97-5]^ < 0.11 ug/L 1 0.11 0.50 6114035 EPA 8260B/6230D 09/14/16 17:07 MSZ Bromodichloromethane [75-27-4]^ < 0.010 ug/L 1 0.010 0.50 6I14035 EPA 8260B/62301) 09/14/16 17:07 MSZ Bromoform [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Bromomethane [74-83-9]^ < 0.28 ug/L 1 0.28 0.50 6I14035 EPA 82606/6230D 09/14/16 17:07 MSZ Carbon Tetrachloride [56-23-5]^ < 0.082 ug/L 1 0.082 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Chlorobenzene[108-90-7]^ < 0.069 ug/L 1 0.069 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Chloroethane [75-00-3]A <'0.18 ug/L 1 0.18 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Chloroform [67-66-3]^ < 0.083 ug/L 1 0.083 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Chloromethane [74-87-3]A < 0.050 ug/L 1 0.050 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ cis-1,2-Dichloroethene [156-59-2]^ < 0.075 ug/L 1 0.075 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ cis-1,3-Dichloropropene [10061-01-5]^ < 0,073 ug/L 1 0.073 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Dibromachloromethane [124-48-1]^ < 0.067 ug/L 1 0.067 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Dibromomethane [74-95-3]^ < 0.13 ug/L 1 0.13 0.50 6114035 EPA 8260B/6230D 09/14/16 17:07 MSZ Dichlorodifluoromethane [75-71-B]^ < 0.091 ug/L 1 0.091 0.50 6114035 EPA 8260B/6230D 09/14/16 17:07 MSZ Ethylbenzene [100-41-4]^ < 0.10 ug/L 1 0.10 0.50 6114035 EPA 82606/6230D 09/14/16 17:07 MSZ Hexachlorobutadiene [87-68-3]^ < 0.15 ug/L 1 0.15 0.50 6I14035 EPA 8260B/62301) 09/14/16 17:07 MSZ Isopropyl Ether [108-20-3]A < 0.20 ug/L 1 0.20 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Isopropylbenzene [98-82-8]^ < 0.13 ug/L 1 0.13 0.50 6114035 EPA 8260B/6230D 09/14/16 17:07 MSZ m,p-Xylenes [108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Methylene Chloride [75-09-2]^ < 0.070 ug/L 1 0.070 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Methyl -tent -Butyl Ether [1634-04-4]^ < 0.12 ug/L 1 0.12 0.50 6I14035 EPA 8260B/62301) 09/14/16 17:07 MSZ FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 8 of 2O sopa pilo � tlflnr www.encolabs.com ANALYTICAL RESULTS Description: MW -5 Lab Sample ID:CZ11268-03 Received: 09/13/16 13:15 Matrix: Ground Water Sampled: 09/13/16 09:10 Work Order: CZ11268 Project: Groundwater Monitoring(Sep) Sampled By: Randall Jarrell (Volatile Organic Compounds by GCMS Analyte rCAS Numberl ^ - ENCO Cary rertifred analyte [NC 5911 Flaa Units DF MDL Q Batch Method Analyzed -By Notes Ammonia as N [7664-41-7]^ < 0.045 Analyte rCAS Numbed Results Flan Units DF MDL JQL Batch Method Analyzed Notes Naphthalene (91-20-3]^ < 0.086 5.0 ug/L 1 0.086 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ n -Butyl Benzene [104-51-81^ < 0.074 6I19003 ug/L 1 0.074 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ n -Propyl Benzene [103-65-1]^ < 0.073 EPA 353.2 ug/L 1 0.073 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ o -Xylene [95-47-6]^ < 0.088 09/13/16 14:37 ug/L 1 0.088 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ sec-Butylbenzene [135-98-8]^ < 0.053 ug/L 1 0.053 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Styrene[100-42-5]^ < 0.082 ug/L 1 0.082 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ tert-Butylbenzene [98-06-6]^ < 0.094 Coliform, Fecal^ ug/L 1 0.094 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Tetrachloroethene [127-18-4]^ < 0.099 ug/L 1 0.099 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Toluene [108-88-3]A < 0.053 ug/L 1 0.053 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ trans-1,2-Dichloroethene [156-60-5]^ < 0.11 ug/L 1 0.11 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ trans-1,3-Dichloropropene [10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Trichloroethene [79-01-6]^ < 0.13 ug/L 1 0.13 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Trichlorofluoromethane [75-69-41^ < 0.15 ug/L 1 0.15 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Vinyl chloride [75-01-4]A < 0.083 ug/L 1 0.083 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Xylenes (Total)[1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 6I14035 EPA 8260B/6230D 09/14/16 17:07 MSZ Surrogates Results DF Spike L v/ % Rec % Rec Limits Batch Method Ana/Vied By Notes 4-Bromofluorobenzene 61 1 50.0 122 56 53-136 6114035 EPA 82608162300 09/14/16 17.07 M5Z Dibromofluoromethane 55 1 50.0 111 % 67-129 6714035 EPA 8260B16230L 09/14/1617.•07 MSZ Toluene -d8 47 1 50.0 94% 59-134 6114035 EPA 8260816230L 09/14/16 17.•07 MSZ Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed -By Notes Ammonia as N [7664-41-7]^ < 0.045 mg/L 1 0.045 0.10 6I14003 EPA 350.1 09/14/16 11:10 JU Chloride [16887-00-6]^ 40 mg/L 1 1.9 5.0 6I19013 SM 4500CI E-1997 09/19/16 12:57 JU Nitrate as N [14797-55-8]^ 0.11 mg/L 1 0.025 0.10 6I19003 EPA 353.2 09/19/16 08:52 JU Nitrate/Nitrite as N^ 0.11 mg/L 1 0.041 0.10 6I16003 EPA 353.2 09/16/16 11:16 JU Nitrite as N [14797-65-0]^ < 0.017 mg/L 1 0.017 0.10 6I13002 EPA 353.2 09/13/16 14:37 JU Microbiological Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF PSL Batch Method Analyzed By Notes Coliform, Fecal^ < 10 MPN/100 10 10 6119027 Colilert 18 09/14/16 09:30 RAY mL (Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 4241 Analyte (CAS Numberl Results Flag Units DF MDL . PSL Batch Method Analyzed By Notes Total Organic Carbon^ 0.66 J mg/L 1 0.34 1.0 6][21029 SM 53106-2000 09/21/16 15:50 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 20