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WQ0001861_Monitoring - 09-2016_20161007
*ESC ANALYTICAL REPORT myE L•A-B S•C•1•E•N•C•E•S September 29, 2016 f e• Soil & Env. Consultants - Raleigh, NC Sample Delivery Group: L861403 Samples Received: 09/23/2016 Project Number: GW -1 1061-200 Description: Groundwater Job #1061 Report To: Mr. Don Wells 8412 Falls of Neuse Road, Suite 104 Raleigh, NC 27615-3543 Entire Report Reviewed By: Terrie Fudge Technical Service Representative Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 060304. 4° , i TABLE OF CONTENTS ONE LAB. NATIONWIDE. 'Cp: Cover Page 2Tc: Table of Contents 3Ss: Sample Summary 4Cn: Case Narrative 5Sr: Sample Results MW -2A L861403-01 MW -3 L861403-02 MW -4A L861403-03 TRIP BLANK L861403-04 60c: Quality Control Summary Gravimetric Analysis by Method 2540 C-2011 Wet Chemistry by Method 4500P E-2011 Wet Chemistry by Method 5540 C-2011 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 7GI: Glossary of Terms 8 A Accreditations & Locations 9Sc: Chain of Custody ACCOUNT: PROJECT: SDG: DATE/TIME: Soil & Env. Consultants - Raleigh, NC GW -11061-200 L861403 09/29/1617:12 1 2 3 4 5 5 7 9 11 13 13 14 15 16 22 23 24 PAGE: 2of25 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, INC GW -1 1061-200 L861403 09/29/1617:12 3 of 25 SAMPLE SUMMARY ONE LAB. NATIONWIDE. e Collected by Collected date/time Received date/time MW-2A L861403-01 GW Don Wells 09/22/1611:55 09/23/1609:00 FIP Method Batch Dilution Preparation Analysis Analyst date/time date/time ITC] Gravimetric Analysis by Method 2540 C-2011 WG911816 1 09/28/16 04:10 09/28/16 05:04 JM Volatile Organic Compounds (GC/MS) by Method 62008-1997 WG911119 1 09/26/1617:10 09/26/1617:10 LRL Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG911119 1 09/28/16 03:57 09/28/16 03:57 DWR Wet Chemistry by Method 4500P E-2011 WG910672 1 09/23/1613:30 09/23/1613:30 JJL Wet Chemistry by Method 5540 C-2011 WG910670 1 09/23/1613:19 09/23/1614:37 JJL Fn] Collected by Collected date/time Received date/time s MW-3 L861403-02 GW Don Wells 09/22/1611:20 ,09/23/1609:00 Sr Method Batch Dilution Preparation Analysis Analyst date/time date/time rQC1 Gravimetric Analysis by Method 2540 C-2011 WG911816 1 09/28/16 04:10 09/28/16 05:04 JM Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG911119 1 09/26/1617:31 09/26/1617:31 LRL GI Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG911119 1 09/28/16 04:53 09/28/16 04:53 DWR Wet Chemistry by Method 4500P E-2011 WG910672 1 09/23/1613:31 09/23/1613:31 JJL FAI Wet Chemistry by Method 5540 C-2011 WG910670 1 09/23/1613:19 09/23/1614:37 JJL Collected by Collected date/time Received date/time 9 SC MW-4A L861403-03 GW Don Wells 09/22/1612:25 09/23/16 09:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Gravimetric Analysis by Method 2540 C-2011 WG911816 -� 1 09/28/16 04:10 09/28/16 05:04 JM Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG911119 1 09/28/1610:44 09/28/1610:44 JHH Volatile Organic Compounds (GC/MS) by Method 620OB-1997 WG911119 1 09/29/1612:35 09/29/1612:35 BMB Wet Chemistry by Method 4500P E-2011 WG910672 1 09/23/1613:32 09/23/1613:32 JJL Wet Chemistry by Method 5540 C-2011 WG910670 1 09/23/1613:19 09/23/1614:37 JJL Collected by Collected date/time Received date/time TRIP BLANK L861403-04 GW Don Wells 09/22/1600:00 09/23/1609:00 Method Batch Dilution Preparation Analysis Analyst date/time date/time Volatile Organic Compounds (GC/MS) by Method 62008-1997 WG911119 _ 1 09/26/16 08:52 09/26/16 08:52 LRL ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, INC GW -1 1061-200 L861403 09/29/1617:12 3 of 25 1 i CASE NARRATIVE ONE LAB. NATIONWIDE. All sample aliquots were received at the correct temperature, in the proper containers, with the F-P] appropriate preservatives, and within method specified holding times. All MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the r7c analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the r Ss laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. s Sr 6 . QC 7G1 Terrie Fudge rAl] Technical Service Representative 9 Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants Raleigh, NC GW -1 1061-200 L861403 09/29/1617:12 4 of 25 l � MW -2A SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 09/22/16 11:55 L861403 Gravimetric Analysis by Method 2540 C-2011 , Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Dissolved Solids 102000 10000 1 09/28/2016 05:04 WG911816 Wet Chemistry by Method 4500P E-2011 Result Qualifier Analyte ug/I Phosphate,OrthoND Wet Chemistry by Method 5540 C-2011 RDL Dilution ug/I 25.0 1 Analysis date / time 09/23/201613:30 Batch WG910672 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I _ date / time MBAS ND 100 1 09/23/201614:37 WG910670 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time J - Acetone ND 50.0 1 09/26/201617:10 WG911119 Acrolein ND 50.0 1 09/26/201617:10 WG911119 Acrylonitrile ND 10.0 1 09/26/201617:10 WG911119 Benzene ND 1.00 1 09/26/201617:10 WG911119 Bromobenzene ND 1.00 1 09/26/201617:10 WG911119 Bromodichloromethane ND 1.00 1 09/26/201617:10 WG911119 Bromoform ND 1.00 1 09/26/201617:10 WG911119 Bromomethane ND 5.00 1 09/26/201617:10 WG911119 n-Butylbenzene ND 1.00 1 09/26/201617:10 WG911119 sec-Butylbenzene ND 1.00 1 09/26/201617:10 WG911119 tert-Butylbenzene ND 1.00 1 09/26/201617:10 WG911119 Carbon tetrachloride ND 1.00 1 09/26/201617:10 WG911119 Chlorobenzene ND 1.00 1 09/26/201617:10 WG911119 `Chlorodibromomethane ND 1.00 1 09/26/201617:10 WG911119 Chloroethane ND 5.00 1 09/26/201617:10 WG911119 Chloroform ND 5.00 1 09/26/201617:10 WG911119 Chloromethane ND 2.50 1 09/26/201617:10 WG911119 2-Chlorotoluene ND 1.00 1 09/26/201617:10 WG911119 4-Chlorotoluene ND 1.00 1 09/26/201617:10 WG911119 1,2-Dibromo-3-Chloropropane ND 5.00 1 09/26/201617:10 WG911119 1,2-Dibromoethane ND 1.00 1 09/26/201617:10 WG911119 'Dibromomethane ND 1.00 1 09/26/201617:10 WG911119 1,2 -Dichlorobenzene ND 1.00 1 09/26/201617:10 WG911119 1,3 -Dichlorobenzene ND 1.00 1 09/26/201617:10 WG911119 1,4 -Dichlorobenzene ND 1.00 1 09/26/201617:10 WG911119 Dichlorodifluoromethane ND 5.00 1 09/26/201617:10 WG911119 1,1-Dichloroethane ND 1.00 1 09/26/201617:10 WG911119 1,2-Dichloroethane ND 1.00 1 09/26/201617:10 WG911119 1,1-Dichloroethene ND 1.00 1 09/26/201617:10 WG911119 cis-1,2-Dichloroethene ND 1.00 1 09/26/201617:10 WG911119 trans-1,2-Dichloroethene ND 1.00 1 09/26/201617:10 WG911119 1,2-Dichloropropane ND 1.00 1 09/26/201617:10 WG911119 1,1-Dichloropropene ND 1.00 1 09/26/201617:10 WG911119 1,3-Dichloropropane ND J4 1.00 1 09/26/201617:10 WG911119 2,2-Dichloropropane ND 1.00 1 09/26/201617:10 WG911119 Di -isopropyl ether ND 1.00 1 09/26/201617:10 WG911119 Ethylbenzene ND 1.00 1 09/26/201617:10 WG911119 Hexachloro-1,3-butadiene ND 1.00 1 09/26/201617:10 WG911119 Isopropylbenzene ND 1.00 1 09/26/201617:10 WG911119 ACCOUNT: PROJECT: SDG: Soil & Env. Consultants - Raleigh, NC GW -1 1061-200 L861403 DATE/TIME: PAGE: 09/29/1617:12 5 of 25 t MW -2A SAMPLE RESULTS - 01 ONE LAB. NATIONWIDE. Collected date/time: 09/22/16 11:55 1-861403 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW -1 1061-200 L861403 09/29/1617:12 6 of 25 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time p-Isopropyltoluene ND 1.00 1 09/26/201617:10 WG911119 2-Butanone (MEK) ND 10.0 1 09/26/201617:10 WG911119 Methylene Chloride ND 5.00 1 09/26/201617:10 WG911119 4-Methyl-2-pentanone (MIBK) ND 10.0 1 09/26/201617:10 WG911119 Methyl tert-butyl ether ND 1.00 1 09/26/201617:10 WG911119 Naphthalene ND 5.00 1 09/28/201603:57 WG911119 n-Propylbenzene ND 1.00 1 09/26/201617:10 WG911119 Styrene ND 1.00 1 09/26/201617:10 WG911119 1,1,1,2 -Tetrachloroethane ND 1.00 1 09/26/201617:10 WG911119 1,1,2,2 -Tetrachloroethane ND 1.00 1 09/26/201617:10 WG911119 Tetrachloroethene ND 1.00 1 09/26/201617:10 WG911119 Toluene ND 5.00 1 09/26/201617:10 WG911119 1,2,3-Trichlorobenzene ND 1.00 1 09/26/201617:10 WG911119 1,2,4-Trichlorobenzene ND 1.00 1 09/26/201617:10 WG911119 1,1,1 -Trichloroethane ND 1.00 1 09/26/201617:10 WG911119 1,1,2 -Trichloroethane ND 1.00 1 09/26/201617:10 WG911119 Trichloroethene ND 1.00 1 09/26/201617:10 WG911119 Trichlorofluoromethane ND 5.00 1 09/26/201617:10 WG911119 1,2,3-Trichloropropane ND 2.50 1 09/26/201617:10 WG911119 1,2,4-Trimethylbenzene ND 1.00 1 09/26/201617:10 WG911119 1,3,5-Trimethylbenzene ND 1.00 1 09/26/201617:10 WG911119 Vinyl chloride ND 1.00 1 09/26/201617:10 WG911119 o -Xylene ND 1.00 1 09/26/201617:10 WG911119 m&p-Xylenes ND 2.00 1 09/26/201617:10 WG911119 (S) Toluene -d8 100 90.0-115 09/26/201617.70 WG911119 (S) Toluene -d8 98.6 90.0-115 09/28/2016 03:57 WG911119 (S) Dibromofluoromethane 88.0 79.0-121 09/28/2016 03:57 WG911119 (S) Dibromofluoromethane 89.8 79.0-121 09/26/201617.70 WG911119 (S)a,a,a-Trifluorotoluene 99.8 90.4-116 09/26/201617.70 WG911119 (S) a, a, o-Trifluorotoluene 100 90.4-116 09/28/201603:57 WG911119 (S)4-Bromofluorobenzene 35.5 J2 80.1-120 09/28/201603:57 WG911119 (S) 4-Bromofluorobenzene 106 80.1-120 09/26/201617.70 WG911119 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW -1 1061-200 L861403 09/29/1617:12 6 of 25 4 MW -3 SAMPLE RESULTS.- 02 ONE LAB. NATIONWIDE. Collected date/time: 09/22/16 11:20 L861403 Gravimetric Analysis by Method 2540 C-2011 , C Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Dissolved Solids 138000~^ ,�.„....�._..__-10000 1 � Y 09/28/2016 05:04~ � WG911816 ______._..,_._..-�._.� -��✓ Wet Chemistry by Method 4500P E-2011 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time Phosphate,Ortho ND~ 25.0 11 09/23/201613:31 WG910672 Wet Chemistry by Method 5540 C-2011 ACCOUNT: PROJECT: SDG: Soil & Env. Consultants - Raleigh, NC GW -1 1061-200 L861403 Batch WG910670 Batch WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 DATE/TIME: 09/29/1617:12 PAGE: 7of25 Result Qualifier RDL Dilution Analysis Analyte ug/I u ugh date / time MBAS ND 100 1 09/23/201614:37 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Qualifier RDL Dilution Analysis Analyte ug/I �- ug/I Y date/time Acetone ND 50.0 1 09/26/201617:31 Acrolein ND 50.0 1 09/26/201617:31 Acrylonitrile ND 10.0 1 09/26/201617:31 Benzene ND 1.00 1 09/26/201617:31 Bromobenzene ND 1.00 1 09/26/201617:31 Bromodichloromethane ND 1.00 1 09/26/201617:31 Bromoform ND 1.00 1 09/26/201617:31 Bromomethane ND 5.00 1 09/26/201617:31 n-Butylbenzene ND 1.00 1 09/26/201617:31 sec -Butyl benzene ND 1.00 1 09/26/201617:31 tert-Butylbenzene ND 1.00 1 09/26/201617:31 :Carbon tetrachloride ND 1.00 1 09/26/201617:31 Chlorobenzene ND 1.00 1 09/26/201617:31 -Chlorodibromomethane ND 1.00 1 09/26/201617:31 Chloroethane ND 5.00 1 09/26/201617:31 Chloroform ND 5.00 1 09/26/201617:31 Chloromethane ND 2.50 1 09/26/201617:31 2-Chlorotoluene ND 1.00 1 09/26/201617:31 4 -Chloro toluene ND 1.00 1 09/26/201617:31 1,2-Dibromo-3-Chloropropane ND 5.00 1 09/26/201617:31 1,2-Dibromoethane ND 1.00 1 09/26/201617:31 Dibromomethane ND 1.00 1 09/26/201617:31 1,2 -Dichlorobenzene ND 1.00 1 09/26/201617:31 1,3 -Dichlorobenzene ND 1.00 1 09/26/201617:31 1,4 -Dichlorobenzene ND 1.00 1 09/26/201617:31 Dichlorodifluoromethane ND 5.00 1 09/26/201617:31 1,1-Dichloroethane ND 1.00 1 09/26/201617:31 1,2-Dichloroethane ND 1.00 1 09/26/201617:31 1,1-Dichloroethene ND 1.00 1 09/26/201617:31 cis-1,2-Dichloroethene ND 1.00 1 09/26/201617:31 trans-1,2-Dichloroethene ND 1.00 1 09/26/201617:31 1,2-Dichloropropane ND 1.00 1 09/26/201617:31 1,1-Dichloropropene ND 1.00 1 09/26/201617:31 ,1,3-Dichloropropane ND J4 1.00 1 09/26/201617:31 2,2-Dichloropropane ND 1.00 1 09/26/201617:31 Di -isopropyl ether ND 1.00 1 09/26/201617:31 Ethylbenzene ND 1.00 1 09/26/201617:31 -Hexachloro-1,3-butadiene ND 1.00 1 09/26/201617:31 Isopropylbenzene ND 1.00 1 09/26/201617:31 ACCOUNT: PROJECT: SDG: Soil & Env. Consultants - Raleigh, NC GW -1 1061-200 L861403 Batch WG910670 Batch WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 DATE/TIME: 09/29/1617:12 PAGE: 7of25 MW -3 SAMPLE RESULTS - 02 Collected date/time: 09/22116 11:20 L861403 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 ONE LAB. NATIONWIDE. * ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW -1 1061-200 L861403 09/29/1617:12 8 of 25 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date / time p-Isopropyltoluene ND 1.00 1 09/26/201617:31 WG911119 2-Butanone (MEK) ND 10.0 1 09/26/201617:31 WG911119 Methylene Chloride ND 5.00 1 09/26/201617:31 WG911119 4-Methyl-2-pemanone (MIBK) ND 10.0 1 09/26/201617:31 WG911119 Methyl tert-butyl ether ND 1.00 1 09/26/201617:31 WG911119 Naphthalene ND 5.00 1 09/28/201604:53 WG911119 n-Propylbenzene ND 1.00 1 09/26/201617:31 WG911119 Styrene ND 1.00 1 09/26/201617:31 WG911119 1,1,1,2 -Tetrachloroethane ND 1.00 1 09/26/201617:31 WG911119 1,1,2,2 -Tetrachloroethane ND 1.00 1 09/26/201617:31 WG911119 Tetrachloroethene ND 1.00 1 09/26/201617:31 WG911119 Toluene ND 5.00 1 09/26/201617:31 WG911119 1,2,3-Trichlorobenzene ND 1.00 1 09/26/201617:31 WG911119 1,2,4-Trichlo robe nzene ND 1.00 1 09/26/201617:31 WG911119 1,1,1 -Trichloroethane ND 1.00 1 09/26/201617:31 WG911119 1,1,2 -Trichloroethane ND 1.00 1 09/26/201617:31 WG911119 Trichloroethene ND 1.00 1 09/26/201617:31 WG911119 Trichlorofluoromethane ND 5.00 1 09/26/201617:31 WG911119 1,2,3-Trichloropropane ND 2.50 1 09/26/201617:31 WG911119 1,2,4-Trimethylbenzene ND 1.00 1 09/26/201617:31 WG911119 1,3,5-Trimethylbenzene ND 1.00 1 09/26/201617:31 WG911119 Vinyl chloride ND 1.00 1 09/26/201617:31 WG911119 o -Xylene ND 1.00 1 09/26/201617:31 WG911119 m&p-Xylenes ND 2.00 1 09/26/201617:31 WG911119 (S) Toluene -d8 101 90.0-115 09/26/201617.31 WG911119 (S)Toluene-d8 100 90.0-115 09/28/201604:53 WG911119 (S) Dibromofluoromethane 88.6 79.0-121 09/28/2016 04:53 WG911119 (S) Dibromofluoromethane 88.2 79.0-121 09/26/201617:31 WG911119 (S) a, a,a-Trifluorotoluene 99.4 90.4-116 09/26/201617.31 WG911119 (S)a,a,a-Trifluorotoluene 99.3 90.4-116 09/28/201604:53 WG911119 (S)4-Bromofluorobenzene 123 11 80.1-120 09/28/201604:53 WG911119 (S) 4-Bromofluorobenzene 104 80.1-120 09/26/201617.•31 WG911119 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW -1 1061-200 L861403 09/29/1617:12 8 of 25 MW -4A SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE. Collected date/time: 09/22/16 12:25 L861403 Gravimetric Analysis by Method 2540 C-2011 Result Qualifier RDL Dilution Analysis Batch u Analyte ug/I Dissolved Solids 192000 ug/I 10000 1 date / time 09/28/2016 05:04 WG911816 FTC] Wet Chemistry by Method 4500P E-2011 ND Bromobenzene ND FSSResult Qualifier RDL Dilution Analysis Batch ND Analyte ug/I ug/I date / time ND rCn] Phosphate,Ortho ND 25.0 1 09/23/201613:32 WG910672 ND Wet Chemistry by Method 5540 C-2011 ND Chloroethane ND 0 Result Qualifier Analyte ug/I RDL Dilution ug/I Analysis date / time Batch s QC MBAS ND 100 1 09/23/201614:37 WG910670 1,2-Dibromoethane by Method 620OB-1997 ,Dibromomethane ND AGI Volatile Organic Compounds (GC/MS) 1,3 -Dichlorobenzene ND 1,4 -Dichlorobenzene ND Qualifier RDL Dilution Result Analyte- ug/l Acetone ND Acrolein ND Acrylonitrile ND Benzene ND Bromobenzene ND Bromodichloromethane ND Bromoform ND Bromomethane ND n-Butylbenzene ND sec-Butylbenzene ND tert-Butylbenzene ND Carbon tetrachloride ND Chlorobenzene ND Chlorodibromomethane ND Chloroethane ND Chloroform ND Chloromethane ND 2-Chlorotoluene ND 4-Chlorotoluene ND 1,2-Dibromo-3-Chloropropane ND 1,2-Dibromoethane ND ,Dibromomethane ND 1,2 -Dichlorobenzene ND 1,3 -Dichlorobenzene ND 1,4 -Dichlorobenzene ND Dichlorodifluoromethane ND L1-Dichloroethane ND 1,2-Dichloroethane ND 1,1-Dichloroethene ND cis-1,2-Dichloroethene ND trans-1,2-Dichloroethene ND 1,2-Dichloropropane ND 1,1-Dichloropropene ND 1,3-Dichloropropane ND 2,2-Dichloropropane ND Di -isopropyl ether ND Ethylbenzene ND Hexachloro-1,3-butadiene ND Isopropylbenzene ND ACCOUNT: SDG: Soil & Env. Consultants - Raleigh, NC Qualifier RDL Dilution Analysis ug//I.___date/time__ 9 50.0 1 09/28/201610:44 50.0 1 09/28/201610:44 10.0 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 5.00 1 09/29/2016 12:35 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 5.00 1 09/28/201610:44 5.00 1 09/28/201610:44 2.50 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 5.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 5.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09128/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 J4 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 1.00 1 09/28/201610:44 PROJECT: SDG: GW -1 1061-200 L861403 Batch WG91 SAI WG911119 9 WG911119 1119 SC WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 WG911119 DATE/TIME: 09/29/1617:12 PAGE: 9of25 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW -11061-200 L861403 09/29/1617:12 10 of 25 MW -4A SAMPLE RESULTS - 03 ONE LAB. NATIONWIDE. Collected date/time: 09/22/16 12:25 L861403 , Volatile Organic Compounds (GC/MS) by Method 620OB-1997 Result Qualifier RDL Dilution Analysis Batch FP1 Analyte ug/I ug/I date / time p-IsOpropyIto 1uene ND 1.00 1 09/28/201610:44 WG911119 ITC 2-Butanone (MEK) ND 10.0 1 09/28/201610:44 WG911119 Methylene Chloride ND 5.00 1 09/28/201610:44 WG911119 3 4-Methyl-2-pentanone (MIBK) ND 10.0 1 09/28/201610:44 WG911119 SS ;Methyl tert-butyl ether ND 1.00 1 09/28/201610:44 WG911119 Naphthalene ND 5.00 1 09/28/2016 10:44 WG911119 Fn] n-Propylbe zene ND 1.00 1 09/28/201610:44 WG911119 Styrene ND 1.00 1 09/28/201610:44 WG911119 1,1,1,2 -Tetrachloroethane ND 1.00 1 09/28/201610:44 WG911119 1,1,2,2 -Tetrachloroethane ND 1.00 1 09/28/201610:44 WG911119 Tetra chloroethene ND 1.00 1 09/28/201610:44 WG911119 - - 6 QC Toluene ND 5.00 1 09/28/201610:44 WG911119 !1,2,3-Trichlorobenzene ND 1.00 1 09/28/201610:44 WG911119 7G1 1,2,4-Trichlorobenzene ND 1.00 1 09/28/201610:44 WG911119 '1,1,1 -Trichloroethane ND 1.00 1 09/28/201610:44 WG911119 1,1,2 -Trichloroethane ND 1.00 1 09/28/201610:44 WG911119 FA Trichloroethene ND 1.00 1 09/28/201610:44 WG911119 Trichlorofluoromethane ND 5.00 1 09/28/201610:44 WG911119 9 1 2 3 Trichloropropane ND 2.50 1 09/28/201610:44 WG911119 SCI 1,2,4-Trimethylbenzene ND 1.00 1 09/28/201610:44 WG911119 1,3,5-Trimethylbenzene ND 1.00 1 09/28/201610:44 WG911119 Vinyl chloride ND 1.00 1 09/28/201610:44 WG911119 o -Xylene ND 1.00 1 09/28/201610:44 WG911119 m&p-Xylenes ND 2.00 1 09/28/201610:44 WG911119 (S) Toluene -d8 102 90.0-115 09/28/201610:44 WG911119 (S) Toluene -d8 101 90.0-115 09/29/201612:35 WG911119 (S) Dibromofluoromethane 97.8 79.0-121 09/29/201612.35 WG911119 (S) Dibromofluoromethane 95.8 79.0-121 09/28/201610:44 WG911119 (S) a,a,a-Trifluorotoluene 97.5 90.4-116 09/28/201610:44 WG911119 (S) a,a,a-Trifluorotoluene 94.5 90.4-116 09/29/201612:35 WG911119 (S) 4-Bromofluorobenzene 101 80.1-120 09/29/201612:35 WG911119 (S) 4-Bromofluorobenzene 99.5 80.1-120 09/28/201610:44 WG911119 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW -11061-200 L861403 09/29/1617:12 10 of 25 'TRIP BLANK SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE. Collected date/time: 09/22/16 00:00 L861403 Volatile Organic Compounds (GC/MS) by Method 620OB-1997 DATE/TIME: 09/29/1617:12 PAGE: 11 of 25 Result Qualifier RDL Dilution Analysis Batch Analyte ug/I ug/I date /time Acetone ND 50.0 1 09/26/2016 08:52 WG911119 Acrolein ND 50.0 1 09/26/2016 08:52 WG911119 Acrylonitrile ND 10.0 1 09/26/2016 08:52 WG911119 Benzene ND 1.00 1 09/26/2016 08:52 WG911119 Bromobenzene ND 1.00 1 09/26/2016 08:52 WG911119 Bromodichloromethane ND 1.00 1 09/26/2016 08:52 WG911119 Bromoform ND 1.00 1 09/26/2016 08:52 WG911119 Bromomethane ND 5.00 1 09/26/2016 08:52 WG911119 n-Butylbenzene ND 1.00 1 09/26/2016 08:52 WG911119 sec -Butyl benzene ND 1.00 1 09/26/2016 08:52 WG911119 tert-Butylbenzene ND 1.00 1 09/26/2016 08:52 WG911119 Carbon tetrachloride ND 1.00 1 09/26/2016 08:52 WG911119 Chlorobenzene ND 1.00 1 09/26/2016 08:52 WG911119 Chlorodibromomethane ND 1.00 1 09/26/2016 08:52 WG911119 Chloroethane ND 5.00 1 09/26/2016 08:52 WG911119 Chloroform ND 5.00 1 09/26/2016 08:52 WG911119 Chloromethane ND 2.50 1 09/26/2016 08:52 WG911119 2-Chlorotoluene ND 1.00 1 09/26/2016 08:52 WG911119 4-Chlorotoluene ND 1.00 1 09/26/2016 08:52 WG911119 1,2-Dibromo-3-Chloropropane ND 5.00 1 09/26/201608:52 WG911119 1,2-Dibromoethane ND 1.00 1 09/26/2016 08:52 WG911119 Dibromomethane ND 1.00 1 09/26/201608:52 WG911119 1,2 -Dichlorobenzene ND 1.00 1 09/26/201608:52 WG911119 1,3 -Dichlorobenzene ND 1.00 1 09/26/2016 08:52 WG911119 1,4 -Dichlorobenzene ND 1.00 1 09/26/2016 08:52 WG911119 Dichlorodifluoromethane ND 5.00 1 09/26/2016 08:52 WG911119 1,1-Dichloroethane ND 1.00 1 09/26/2016 08:52 WG911119 1,2-Dichloroethane ND 1.00 1 09/26/2016 08:52 WG911119 1,1-Dichloroethene ND 1.00 1 09/26/2016 08:52 WG911119 cis-1,2-Dichloroethene ND 1.00 1 09/26/201608:52 WG911119 trans-1,2-Dichloroethene ND 1.00 1 09/26/201608:52 WG911119 1,2-Dichloropropane ND 1.00 1 09/26/201608:52 WG911119 1,1-Dichloropropene ND 1.00 1 09/26/201608:52 WG911119 1,3-Dichloropropane ND J4 1.00 1 09/26/201608:52 WG911119 2,2-Dichloropropane ND 1.00 1 09/26/201608:52 WG911119 Di -isopropyl ether ND 1.00 1 09/26/2016 08:52 WG911119 Ethylbenzene ND 1.00 1 09/26/201608:52 WG911119 Hexachloro-1,3-butadiene ND 1.00 1 09/26/2016 08:52 WG911119 Isopropylbenzene ND 1.00 1 09/26/2016 08:52 WG911119 p-Isopropyltoluene ND 1.00 1 09/26/2016 08:52 WG911119 2-Butanone (MEK) ND 10.0 1 09/26/2016 08:52 WG911119 Methylene Chloride ND 5.00 1 09/26/2016 08:52 WG911119 4-Methyl-2-pentanone (MIBK) ND 10.0 1 09/26/2016 08:52 WG911119 Methyl tert-butyl ether ND 1.00 1 09/26/2016 08:52 WG911119 Naphthalene ND 5.00 1 09/26/2016 08:52 WG911119 n-Propylbenzene ND 1.00 1 09/26/201608:52 WG911119 Styrene ND 1.00 1 09/26/201608:52 WG911119 1,1,1,2 -Tetrachloroethane ND 1.00 1 09/26/2016 08:52 WG911119 1,1,2,2 -Tetrachloroethane ND 1.00 1 09/26/2016 08:52 WG911119 Tetrachloroethene ND 1.00 1 09/26/2016 08:52 WG911119 Toluene ND 5.00 1 09/26/201608:52 WG911119 1,2,3-Trichlorobenzene ND 1.00 1 09/26/201608:52 WG911119 1,2,4-Trichlorobenzene ND 1.00 1 09/26/201608:52 WG911119 1,1,1 -Trichloroethane ND 1.00 1 09/26/2016 08:52 WG911119 1,1,2 -Trichloroethane ND 1.00 1 09/26/2016 08:52 WG911119 Trichloroethene ND 1.00 1 09/26/2016 08:52 WG911119 ACCOUNT: PROJECT: SDG: Soil & Env. Consultants - Raleigh, NC GW -1 1061-200 L861403 DATE/TIME: 09/29/1617:12 PAGE: 11 of 25 ACCOUNT:. PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants -Raleigh, NC 7RIP BLANK L861403 SAMPLE RESULTS - 04 ONE LAB. NATIONWIDE. I Collected date/time: 09/22/16 00:00 L861403 Volatile Organic Compounds (GC/MS) by Method 62008-1997 Result Qualifier RDL Dilution Analysis Batch Cp Analyte ug/I ug/I date / time Trichlorofluoromethane ND 5.00 1 09/26/2016 08:52 WG911119 C 12,3-Trichloropropane ND" 2.50 1 09126/201608:52 WG911119 1,2,4 Trimethylbenzene ND 1.00 1 09/26/2016 08:52 WG911119 :1,3,5-Trimethylbenzene ND 1.00 1- 09/26/2016'08:52 WG911119 SS Vinyl chloride ND 1.00 1 09/26/2016 08:52 WG911119 �o-Xylene ND 1.001 09/26/2016 08:52 WG911119 rqn m&p-Xylenes ND 2.00 1 09/26/2016 08:52 WG911119 (S) Toluene& 100 90.0-115 09/26/2016 08:52 WG911119 (S) Dibromofluoromethone 924 790-121 09/26/201608:52 WG911119 a tol ,a, (S)a,,o-Trifluototoluene 98.2 90.4-116 09/26/201608:52 WG911119 - --- (S) 4-Bromofluorobenzene 102 80.1-120 09/2612016 08:52 WG911119 rQcl AGI FAI 9 Sc ACCOUNT:. PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants -Raleigh, NC GW -1 1061-200 L861403 09/29/16'17:12 12 of 25 - WG911816 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Gravimetric Analysis by Method 2540-C-2011_ L861403-01,02.03 - - - Method Blank (MB) C (MB) R3166859-1 09/28/16 05:04 MB Result MB Qualifier MB MDL MB RDL Analyte Ug/I ug/I ugn FTC] Dissolved Solids U 2820 10000 3S-9 L861343-01 Original Sample (OS) • Duplicate (DUP) 4Cn (OS) L861343-01 09/28/16 05:04 • (DUP) R3166859-4 09/28/16 05:04 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits s Analyte ugh ug/I % _ % - w� Sr Dissolved Solids 1600000 1560000 1 2.38 5 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) 2GI (I -CS) R3166859-2 09/28/16 05:04 • (LCSD) R3166859-3 09/28/16 05:04 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I ug/I % % % % % Dissolved Solids 8800000 8290000 8620000 94.2 98.0 85.0-115 3.90 5 9Sc ACCOUNT: PROJECT: SDG: DATE/TIME: Soil & Env. Consultants - Raleigh, NC GW -1 1061-200 L861403 09/29/1617:12 PAGE: 13 of 25 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: 1 Soil & Env. Consultants - Raleigh, NC GW -1 10 61-2 00 L861403 09/2911617:12 14 of 25 WG910672 QUALITY CONTROL SUMMARY ONE LAB, NATIONWIDE. � j Wei Chemistry by Method-450,OP E-2011 _ _ L861403-01,02,03, Method Blank (MB) 1 (MB) R3165708-1 09/23/1613:29 Cp MB Result MB Qualifier MB MDL MB RDL Analyte ugA ug/I ug/I 2 TC Phosphate,Ortho U 9.00 25.0 3Ss L861452-06 Original Sample (OS) • Duplicate (DUP) 4 (OS) L861452-06 09/23/1613:34 • (DUP) R3165708-4 09/23/1613:35 Cin Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte ug/I ugh % %_ s Phosphate,Ortho U ND 1 0.000 20 ' Laboratory Control Sample (LCS) •Laboratory Control Sample Duplicate (LCSD) 7 (LCS) R3165708-2 09/23/16 13:29 • (LCSD) R3165708-3 09/23/16 13:29 GI Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits ' Analyte ugA ug/I ugA % % % % % aAl Phosphate,Ortho 750 767 778 102 104 85.0-115 1.00 20 FSCL861452-06 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L861452-06 09/23/1613:34 • (MS) R3165708-5 09/23/16 13:35 • (MSD) R3165708-6 09/23/16 13:35 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ugA ug/I ugA ugA % % % % % Phosphate,Ortho 500 U 509 500 102 100 1 80.0-120 2.00 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: 1 Soil & Env. Consultants - Raleigh, NC GW -1 10 61-2 00 L861403 09/2911617:12 14 of 25 I WG910670 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Wet Chemistry by Method_ 5540 C-2011 - -„ L861403-01,02,03 Method Blank (MB) 1C (MB) R3165748-1 09/23/16 14:33 p MB Result MB Qualifier MB MDL MB RDL 2TC Analyte ugA ug/I ug/I MBAS U 19.0 100 ®® 3S5 L8614O3-03 Original Sample (OS) • Duplicate (DUP) 4Cn (OS) L861403-03 09/23/1614:37 • (DUP) R3165748-4 09/23/1614:52 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte ugA ug/I % % s Sr F MBAS ND ND 1 0.000 20 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) 7GI (LCS) R3165748-2 09/23/1614:34 • (LCSD) R3165748-3 09/23/1614:34 Spike Amount LCS Result LCSD Result LCS Ret. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug/I ug/I ugA % % % % % 8Al MBAS 1000 1050 1080 105 108 90.0-110 3.00 20 —11 9Sc L8614O3-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L861403-03 09/23/1614:37 • (MS) R3165748-5 09/23/1614:53 • (MSD) R3165748-6 09/23/1614:55 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte ugA ug/I ugA ugA % % % % ' % MBAS 1000 ND 1120 1120 103 103 1 90.0-110 0.000 20 ACCOUNT: PROJECT: SDG: DATEMME: PAGE: Soil & Env. Consultants - Raleigh, NC GW -1 1061-200 L861403 09/29/16 17:12 15 of 25 WG911119 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 62008-1997 L861403-01,02,03,04 Method Blank (MB) (MB) R3166468-3 09/26/16 08:03 MB Result MB Qualifier MB MDL MB RDL Analyte ug/I ug/I ugh Acetone U 10.0 50.0 Acrolein U 8.87 50.0 Acrylonitrile U 1.87 10.0 Benzene U 0.331 1.00 Bromobenzene U 0.352 1.00 Bromodichloromethane U 0.380 1.00 Bromoform \ U ) 0.469 1.00 Bromomethane U 0.866 5.00 n-Butylbenzene U 0.361 1.00 sec-Butylbenzene U 0.365 1.00 tert-Butylbenzene U 0.399 1.00 Carbon tetrachloride U 0.379 1.00 Chlorobenzene U 0.348 1.00 Chlorodibromomethane U 0.327 1.00 Chloroethane U 0.453 5.00 Chloroform U 0.324 5.00 Chloromethane U 0.276 2.50 2-Chlorotoluene U 0.375 1.00 4-Chlorotoluene U 0.351 1.00 1,2-Dibromo-3-Chloropropane U 1.33 5.00 1,2-Dibromoethane U 0.381 1.00 Dibromomethane U 0.346 1.00 1,2 -Dichlorobenzene U 0.349 1.00 1,3 -Dichlorobenzene U 0.220 1.00 1,4 -Dichlorobenzene U 0.274 1.00 ,Dlchlorodifluoromethane U 0.551 5.00 1,1-Dichloroethane U 0.259 1.00 1,2-Dichloroethane U 0.361 1.00 1,1-Dichloroethene U 0.398 1.00 cis4,2-Dichloroethene U 0.260 1.00 trans-1,2-Dichloroethene U 0.396 1.00 1,2-Dlchloropropane U 0.306 1.00 1,1-Dlchloropropene U 0.352 1.00 1,3-Dichloropropane U 0.366 1.00 2,2-Dichloropropane U 0.321 1.00 DI -isopropyl ether U 0.320 1.00 Ethylbenzene U 0.384 1.00 Hexachloro-1,3-butadiene U 0.256 1.00 Isopropylbenzene U 0.326 1.00 p-Isopropyltoluene U 0.350 1.00 ACCOUNT: PROJECT: Soil & Env. Consultants- Raleigh, NC GW -1 1061-200 SDG: DATE/TIME L661403 09/29/16 17:12 ONE LAB. NATIONWIDE. * PAGE: 16 of 25 WG911119 QUALITY CONTROL SUMMARY ONE LAB.. NATIONWIDE. i.' Volatile Organic,Compounds (GC/MS) by Method 62008-1997 L861403-01,02,03,04 Rec. Limits Method Blank (MB) Analyte ug/I ug/I ugh % - % C % (MB) R3166468-3 09/26/16 08:03 129 110 104 p 6.11 Analyte MB Result ug/I MB Qualifier MB MDL 44 MB RDL ug/I 2 2-Butanone (MEK) U 3.93 10.0 113 ;Methylene Chloride IJ 1.00 5:00 FSS 4 Methyl-2-pentanone (MIBK) U 2.14 10.0 ' _ 26.2 IMeihyl tert-butyl ether Naphthalene ..0 U 0.367 .. 1.00 1.00 - ....5.00 _.. 4 Cn :n Propylbenzene L1 0.349 1.00 2.46 Tetrachioroethene U _ 0.372 1.00 Sr Styrene U 01.307 _ . 1.00. GW -11061-200 1,112 Tetrachloroethane Toluene U U 0.385 0.780 1.00 5.00 1,1,2,2 Tetrachloroethane U 0.130 1.00 1,11 Trichloroethane U 0.319 1.00 7GI 1,2,3 Trichlorobenzene U 0.230 1.00 ;Trichloroethene 1,24Trichlorobenzene _ U U 0 398 0.355 9.00 1.00 - AI ,1,1 2 Trichloroethane U 0 383 1.00. Trichlorofluoromethane U 120 5.00 SC 9,23Trichloropropane U 0.807 2.50 1,2,4-Trimethylbenzene U 0.373 1.00 1,3,5-Trimethylbenzene U 0.387 1.00 Vinyl chloride U 0.259 1.00 'c -Xylene U 0.341 1.00 m&p-Xylenes U 0.719 2.00 (SJ Toluene -d8 99.5 90.0-115 (S) Dibromolluoromethone 91.9 79.0-111 j (5)o,a,o-1'rifluorotoluene 974 90.4-116 (S)4-Bromotluorobenzene 104 80.1-110 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3166468-1 09/26/16 06:36 • (LCSD) R3166468-2 09/26/16 06:58 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD Analyte ug/I ug/I ugh % - % % % Acetone 125 138 129 110 104 28.7-175 6.11 ,Acrolein - 125 92.9 97.6 _ 74.3 78.1 40.4-172. 4.88 Acrylonitrile 125 140 141 112 113 58.2-145 0.480 'Benzene 25.0 27.3_ 26.3 109 105 730-122 3.82 Bromobenzene 25.0 26.5 _ 26.2 106 105 81.5-115 _ 1.23 Bromodichlorometh ane 25.0 26.2 25.5 105 102 75:5-121 2.46 ACCOUNT: - PROJECT: SDG: Soil &Env. Consultants -Raleigh, NC GW -11061-200 L861403 RPD Limits % 20.9 20 . 20 20 20 20- - - - DATE/TIME: PAGE: 09/29/16 17.12 17 of 25 WG911119 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE, Volatile Organic Compounds (GC/MS) by Method 620OB-1997 L861403-01,02,03,04 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3166468-1 09/26/16 06:36 • (LCSD) R3166468-2 09/26/16 06:58 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte ug71 ug/I ug/I % % % % % Bromoform 25.0 26.0 26.3 104 105 71.5-131 1.12 20 Bromomethane 25.0 26.9 25.7 108 103 22.4-187 4.80 20 n-Butylbenzene 25.0 23.0 21.9 92.1 87.6 75.9-134 5.00 20 sec-Butylbenzene 25.0 24.2 23.6 96.8 94.2 80.6-126 2.69 20 tert-Butylbenzene 25.0 25.5 24.9 102 99.6 79.3-127 2.47 20 'Carbon tetrachloride 25.0 24.0 22.9 96.0 91.5 70.9-129 4.82 20 Chlorobenzene 25.0 28.3 27.8 113 111 79.7-122 1.67 20 Chlorodibromomethane 25.0 27.9 27.6 112 110 78.2-124 1.16 20 Chloroethane 25.0 28.5 25.8 114 103 41.2-153 9.73 20 Chloroform 25.0 26.5. 25.5 106 102 73.2-125 3.66 20 Chloromethane 25.0 26.6 25.1 106 101 55.8-134 5.57 20 2-Chlorotoluene 25.0 25.9 25.6 104 102 76.4-125 1.34 20 4-Chlorotoluene 25.0 26.9 26.4 108 106 81.5-121 1.74 20 1,2-Dibromo-3-Chloropropane 25.0 26.9 27.5 107 110 64.8-131 2.37 20 1,2-Dibromoethane 25.0 30.1 30.4 120 121 79.8-122 1.05 20 Dibromomethane 25.0 28.4 28.1 114 112 79.5-118 1.22 20 1,2 -Dichlorobenzene 25.0 26.4 25.4 106 102 84.7-118 3.88 20 1,3 -Dichlorobenzene 25.0 26.0 25.6 104 103 77.6-127 1.25 20 1,4 -Dichlorobenzene 25.0 26.0 24.7 104 99.0 82.2-114 4.99 20 Dichlorodifluoromethane 25.0 28.5 27A 114 110 56.0-134 3.78 20 1,1-Dichloroethane 25.0 27.0 25.8 108 103 71.7-127 4.41 20 1,2-Dichloroethane 25.0 27.4 27.1 110 108. 65.3-126 1.42 20 1,1-Dichloroethene 25.0 26.5 25.7 106 103 59.9-137 3.22 20 cis-1,2-Dichloroethene 25.0 27.7 26.8 111 107 77.3-122 3.49 20 trans-1,2-Dichloroethene 25.0 27.7 26.9 111 107 72.6-125 3.13 20 1,2-Dichloropropane 25.0 26.8 26.1 107 104 77.4-125 2.79 20 1,1-Dichloropropene 25.0 28.2 26.6 113 106 72.5-127 5.72 20 1,3-Dichloropropane 25.0 29.5 29.9 118 120 80.6-115 J4 34 1.40 20 2,2-Dichloropropane 25.0 29.0 25.5 116 102 61.3-134 12.9 20 Di -isopropyl ether 25.0 24.3 23.7 97.1 94.8 65.1-135 2.32 20 Ethylbenzene 25.0 27.6 26.9 110 108 80.9-121 2.37 20 Hekachloro-1,3-butadiene 25.0 20.4 19.6 81.5 78.5 73.7-133 3.80 20 Isopropylbenzene 25.0 25.9 25.2 103 101 81.6-124 2.49 20 p-Isopropyltoluene 25.0 25.4 24.7 101 98.6 77.6-129 2.82 20 2-Butanone (MEK) 125 128 125 103 100 46.4-155 2.65 20 Methylene Chloride 25.0 27.4 26.8 109 107 69.5-120 2.18 20 4-Methyl-2-pentanone (MIBK) 125 127 127 102 102 63.3-138 0.0100 20 Methyl tert-butyl ether 25.0 19.5 19.2 77.9 76.7 70.1-125 1.53 20 Naphthalene 25.0 27.4 27.1 110 108 69.7-134 1.16 20 n-Propylbenzene 25.0 26.1 25.3 104 101 81.9-122 3.02 20 ACCOUNT: PROJECT: SDG: DATE/TIME: Soil & Env. Consultants - Raleigh, NC GW -1 1061-200 L861403 09/29/16 17:12 PAGE: 18 of 25 WG911119 Spike Amount ug/I Original Result MS Result ug/I ug/I MSD Result ug/I MS Rec. % QUALITY CONTROL SUMMARY Dilution Rec. Limits % MS Qualifier ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 62008-1997 L861403-01,02,03,04 ND ND 0.000 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) J6 0.000 C (LCS) R3166468-1 09/26/16 06:36 • (LCSD) R3166468-2 09/26/16 06:58 125 U 46.4 ND 37.1 p 1 34.0-194 STC Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits 200 21.5 Analyte ug/I ug/I ug/I % % % 1 55.9-161 J6 J3 J6 123 20 Styrene--- - 25.0 26.2 27.8 113 ` 111 79.9-124 1.38 20 E V 1,1,1.2 -Tetrachloroethane 25.0 26.2 26.0 105 104 78.5-125 0.670 20 a SS 1,1,2,2 -Tetrachloroethane 25.0 29.2 28.9 117 116 79.3-123 0.950 20 52.7 Tetra chloroethene 25.0 26.8 26.1 107 104 73.5-130 2.58 20 4 Toluene 25.0 27.6 26.8 110 107 77.9-116 2.84 20 Cn 1,2,3-Trichlorobenzene 25.0 26.4 26.1 106 104 75.7-134 1.19 20 20.5 1,1,1 -Trichloroethane 25.0 26.1 24.8 104 99.3 71.1-129 4.83 20 6 Sr . 1,2,4-Trichlorobenzene 25.0 26.6 25.8 107 103 76.1-136 3.21 20 1 66.8-139 1,1,2 -Trichloroethane 25.0 28.8 28.7 115 115 81.6-120 0.190 20 51.5 Trichloroethene 25.0 26.1 25.4 104 102 79.5-121 2.68 20 11.7 Trichlorofluoromethane 25.0 25.9 24.5 104 98.1 49.1-157 5.50 20 ACCOUNT: 1,2,3-Trichloropropane 25.0 29.0 29.4 116 118 74.9-124 1.68 20 7G1 1,2,4-Trimethyibenzene 25.0 26.1 25.6 104 102 79.0-122 2.07 20 09/29/1617:12 1,3,5-Trimethylbenzene 25.0 25.5 25.1 102 100 81.0-123 1.51 20 e Vinyl chloride 25.0 27.1 25.5 109 102 61.5-134 6.27 20 A o -Xylene 25.0 27.2 26.5 109 106 79.1-123 2.26 20 m&p-Xylenes 50.0 54.7 53.2 109 106 78.5-122 2.72 20 SC (S) Toluene -d8 100 101 90.0-115 (S) Dibromofluoromethane 92.9 92.8 79.0-121 (S)a,a,a-Tntluorotoluene 99.4 99.5 90.4-116 (S) 4-Bromolluorobenzene 98.9 100 80.1-120 L860928-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L860928-02 09/26/1612:07 • (MS) R3166468-4 09/26/1612:29 • (MSD) R3166468-5 09/26/1612:51 Analyte Spike Amount ug/I Original Result MS Result ug/I ug/I MSD Result ug/I MS Rec. % MSD Rec. % Dilution Rec. Limits % MS Qualifier MSD Qualifier RPD % RPD Limits % Acetone 125 U ND ND 0.000 0.000 1 25.0-156 J6 J6 0.000 21.5 Acroleln 125 U 46.4 ND 37.1 0.000 1 34.0-194 J3 J6 200 21.5 Acrylonitrile 125 U 59.4 14.1 47.5 11.3 1 55.9-161 J6 J3 J6 123 20 Benzene 25.0 464 471 462 25.9 0.000 1 58.6-133 E V E V 1.86 20 Bromobenzene 25.0 U 14.4 4.88 57.5 19.5 1 70.6-125 J6 J3 J6 98.7 20 Bromodichloromethane 25.0 U 13.2 3.63 52.7 14.5 1 69.2-127 J6 J3 J6 114 20 Bromoform 25.0 U 12.9 3.46 51.5 13.8 1 66.3-140 J6 J3 J6 115 20 Bromomethane 25.0 U 11.7 3.31 46.8 13.2 1 16.6-183 J3 J6 112 20.5 n-Butylbenzene 25.0 U 12.1 4.37 48.4 17.5 1 64.8-145 J6 J3 J6 94.0 20 sec-Butylbenzene 25.0 U 11.4 3.75 45.6 15.0 1 66.8-139 J6 J3 J6 101 20 tert-Butylbenzene 25.0 U 12.9 4.38 51.5 17.5 1 67.1-138 J6 J3 J6 98.5 20 Carbon tetrachloride 25.0 U 11.7 3.23 46.8 12.9 1 60.6-139 J6 J3 J6 113 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW -1 1061-200 L861403 09/29/1617:12 19 of 25 WG911119 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 62006-1997 L861403-01,02,03,04 L86O928-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L860928-02 09/26/1612:07 • (MS) R3166468-4 09/26/1612:29 • (MSD) R3166468-5 09/26/1612:51 MS Qualifier MSD Qualifier RPD Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution 1 Analyte ug/I ug/I ug/I ug/I % �N % L6 J6 Chlorobenzene 25.0 U 11.2 3.41 44.7 13.6 1� Chlorodibromomethane 25.0 U 14.0 4.04 55.9 16.1 1 Chloroethane 25.0 U 12.9 3.71 51.6 14.8 1 Chloroform 25.0 U 14.1 4.13 56.5 16.5 1. Chloromethane 25.0 U 11.2 3.39 44.9 13.6 1 '2-Chlorotoluene 25.0 U 20.5 12.1 81.9 48.5 1 4-Chlorotoluene 25.0 U 13.2 3.86 52.8 15.4 1 1,2-Dibromo-3-Chloropropane 25.0 U 3.82 ND 15.3. 0.000 1 1,2-Dlbromoethane 25.0 U 15.5 4.63 61.9 18.5 1 Dibromomethane 25.0 U 13.5 3.87 53.9 15.5 1 1,2 -Dichlorobenzene 25.0 U 13.8 3.83 55.1 15.3 1 1,3 -Dichlorobenzene 25.0 U 12.6 3.52 50.4 14.1 1 1,4 -Dichlorobenzene 25.0 U 13.7 3.89 54.6 15.6 1 'Dichlorodifluoromethane 25.0 U 16.5 4.21 65.9 16.8 1 1,1-Dichloroethane 25.0 U 14.0 4.11 56.2 16.4 1 1,2-1)ichloroethane 25.0 U 14.6 4.35 58.5 17.4 9 1,1-Dichloroethene 25.0 U 12.1 3.41 48.3 13.6 1 'cis-1,2-Dichloroethene 25.0 U 14.0 4.32 56.2 17.3 1 trans-1,2-Dlchlo�roethene 25.0 U 12.2 3.60 48.6 14.4 1 1,2-Dichloropropane 25.0 U 13.6 3.78 54.3 15.1 1 1,1-Dichloropropene 25.0 U 12.7 3.68 50.7 14.7 1 1,3-Dichloropropane 2510 U 15.2 4.54 60.8 18.2 1 2,2-Dichloropropane .25.0 U 15.9 4.33 63.5 17.3 1 DI -Isopropyl ether 25.0 U 12.4 3.27 49.7 13.1 1 Ethylbenzene 25.0 932 937 994 17.8 246 1 Hexachloro-1,3-butadiene 25.0 U 1.46 0.470 5.82 1.88 1 Isopropylbenzene 25.0 57.5 68.5 60.3 44.3 11.2 1 p-Isopropyltoluene 25.0 7.85 20.2 16.8 49.2 35.8 1 2-Butanone (MEK) 125 U 36.0 6.67 28.8 5.33 1 Methylene Chloride 25.0 U 13.0 3.91 51.9 15.6 1 4-Methyl-2-pentanone (MIBK) 125 U 61.4 14.5 49.1 11.6 1 Methyl tert-butyl ether 25.0 U 9.64 2.50 38.5 10.0 1 Naphthalene 25.0 494 371 365 0.000 0.000 1 n-Propylbenzene 25.0 15.0 27.3 18.7 49.2 15.0 1 Styrene 25.0 92.5 105 80.7 50.7 0.000 1 1,1,1,2 -Tetrachloroethane 25.0 U 12.7 3.61 50.9 14.4 1 1,1,2,2 -Tetrachloroethane 25.0 U 15.2 4.15 60.8 16.6 1 Tetra chloroethene 25.0 U 13.2 4.01 52.8 16.1 1 Toluene 25.0 563 575 566 48.3 13.4 1 1,2,3-Trichlorobenzene 25.0 U ND ND 0.000 0.000 1 ACCOUNT: PROJECT: Soil &. Env. Consultants - Raleigh, NC GW -1 1061-200 ONE LAB. NATIONWIDE. * Rec. Limits �- MS Qualifier MSD Qualifier RPD RPD Limits 70.1-130 JG J3 J6 _--106 ®--�-� 2071.6-132 L6 J6 J3 J6 110 20 33.3-155 J3 J6 111 20 66.1-133 J6 J3 J6 109 20 40.7-139 J3 J6 107 20 66.9-134 J3 J6 51.3 20 66.8-134 J6 J3 J6 110 20 63.9-142 J6 J3 J6 200 20.2 73.8-131 J6 J3 J6 108 20 72.8-127 J6 J3 J6 111 20 77.4-127 J6 J3 J6 113 20 67.9-136 J6 J3 J6 113 20 74.4-123 J6 J3 J6 111 20 42.2-146 J3 J6 119 20 64.0-134 J6 J3 J6 109 20 60.7-132 J6 J3 J6 108 20 48.8-144 J6 J3 J6 112 20 60.6-136 J6 J3 J6 106 20 61.0-132 J6 J3 J6 109 20 69.7-130 J6 J3 J6 113 20 61.5-136 J6 J3 J6 110 20 74.3-123 J6 J3 J6 108 20 54.9-142 J3 J6 114 20 59.9-140 J6 J3 J6 117 20 62.7-136 E V E V 5.92 20 61.1-144 J6 J3 J6 102 20.1 67.4-136 J6 J6 12.9 20 62.8-143 J6 J6 18.2 20 45.0-156 J6 J3 J6 138 20.8 61.5-125 J6 J3 J6 107 20 60.7-150 J6 J3 J6 124 20 61.4-136 J6 J3 J6 118 20 61.8-143 E V E V 1.74 20 63.2-139 J6 J3 J6 37.2. 20 68.2-133 J6 J3 J6 26.3 20 70.5-132 J6 J3 J6 112 20 64.9-145 J6 J3 J6 114 20 57.4-141 J6 J3 J6 107 20 67.8-124 E V E V 1.53 20 65.7-143 J6 J6 0.000 20 SDG: DATE/TIME: PAGE: L861403 09/29/16 17:12 20 of 25 WG911119 QUALITY CONTROL SUMMARY ONE LAB. NATIONWIDE. Volatile Organic Compounds (GC/MS) by Method 6 2 0 0 8-1997 L861403-01,02,03,04 - L860928-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) C (OS) L860928-02 09/26/16 12:07 • (MS) R3166468-4 09/26/16 12:29 • (MSD) R3166468-5 09/26/1612:51 p Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 2 Analyte UQ4 ug/I ug/I ug/I % % % % % TC 1,1,1 -Trichloroethane 25.0 U 13.4 3.63 53.6 14.5 1 58.7-134 J6 J3 J6 115 20 .1,2.4-Trichlorobenzene 25.0 U 0.716 ND 2.86 0.000 1 67.0-146 J6 J3 J6 200 20 a SS 1,1,2 -Trichloroethane 25.0 U 15.7 4.62 62.6 18.5 1 74.1-130 J6 J3 J6 109 20 Trichloroethene 25.0 U 12.1 3.49 48.3 14.0 1 48.9-148 J6 J3 J6 110 20 4Cn Trichlorofluoromethane 25.0 U 11.9 2.95 47.7 _ 11.8 1 39.9-165 J3 J6 121 20 1,2,3-Trichloropropane 25.0 U 14.4 4.39 57.4 17.5 1 71.5-134 J6 J3 J6 106 20 1,2,4-Trimethylbenzene 25.0 292 302 299 40.3 28.5 1 60.5-137 E V E V 0.980 20 SSr 1,3,5-Trimethylbenzene 25.0 82.9 93.2 86.4 41.0 14.1 1 67.9-134 J6 J6 7.49 20 Vinyl chloride 25.0 U 12.6 3.83 50.6 15.3 1 44.3-143 J3 J6 107 20 'o -Xylene 25.0 585 571 590 0.000 1 67.1433 E V E V 2.32 20 m&p-Xylenes 50.0 813 822 861 18.4 _21.1 96.1 1 64.1-133 E V E 4.61 20 (S) Toluene -d8 96.1 94.3 90.0-115 (S) Dibromofluoromethone 94.4 91.7 79.0-121 (S) o,o.o-Trifluorotoluene _ 96.5 96.0 _ 90.4-116 e (S)4-Bromoflucrohenzene 96.9 97.7 80.1-120 AI ACCOUNT: PROJECT: SDG: Soil $ Env. Consultants - Raleigh, NC GW -1 1061-200 L861403 DATE/TIME: 09/29/1617:12 PAGE: 21 of 25 9Sc y GLOSSARY OF TERMS ONE LAB. NATIONWIDE. Abbreviations and Definitions SDG Sample Delivery Group. ;MDL Method Detection Limit. RDL Reported Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). U Not detected at the Reporting Limit (_or MDL_ where applicable). RPD Relative Percent Difference. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. (S) Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery_ Surrogates are not expected to be detected in all environmental media. Rec. Recovery. Qualifier Description E The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial calibration (ICAL). J1 Surrogate recovery Limits have been exceeded; values are outside upper control limits. J2 Surrogate recovery limits have been exceeded; values are outside lower control limits. J3 The associated batch QC was outside the established quality control range for precision. J4 The associated batch QC was outside the established quality control range for accuracy. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low. V The sample concentration is too high to evaluate accurate spike recoveries. ACCOUNT: PROJECT: SDG: DATE/TIME: Soil & Env. Consultants - Raleigh, NC GW -11061-200 L861403 09/29/1617:12 PAGE: 22 of 25 ACCREDITATIONS & LOCATIONS ONE LAB. NATIONWIDE. ESC Lab Sciences is the only environmental laboratory accredited/certified to support your work nationwide from one location. One phone call, one point of contact, one laboratory. No other lab is as accessible or prepared to handle your needs throughout the country. Our capacity and capability from our single location laboratory is comparable to the collective totals of the network laboratories in our industry. The most significant benefit to our "one location" design is the design of our laboratory campus. The model is conducive to accelerated productivity, CP decreasing turn -around time, and preventing cross contamination, thus protecting sample integrity. Our focus on premium quality and prompt service allows us to be YOUR LAB OF CHOICE. Not all certifications held by the laboratory are applicable to the results reported in the attached report. 1-9 State Accreditations Alabama 40660 Nevada TN -03-2002-34 s Alaska UST 080 New Hampshire 2975 SSI Arizona AZ0612 New Jersey—NELAP TN002 Arkansas 88-0469 New Mexico TN00003 Cn California _ 01157CA New York _11742 Colorado TN00003 North Carolina Erl Conneticut PH -0197 North CarolinaDW21704 s r Florida E87487 North Carolina Georgia — NELAP North Dakota R-140 Georgia' 923 Ohio VAP CL0069 QC Idaho TN00003 Oklahoma 9915 Illinois 200008 Oregon TN200002 Indiana C -TN -01 Pennsylvania 68-02979 7Gi Iowa 364 Rhode Island 221 Kansas E-10277 South Carolina _ 84004 Kentucky' 90010 South Dakota — n/a a Kentucky2 16 Tennessee'" 2006 Louisiana AI30792 Texas _ _ T104704245 -07 -TX 9 Maine TN0002 Texas 5 LABO152 SC Maryland 324 Utah — _ _ _6157585858 Massachusetts M-TNO03 Vermont _ _ _ —_ - VT2006 Michigan 9958Virginia 109 Minnesota 047-999-395 Washington _ . C1915 _ -------------------------------- -- Mississippi TN00003 West Virginia 233— Missouri 340 Wisconsin __9980939910 Montana CERT0086 Wyoming A2LA Nebraska NE -OS -15-05 Third Party & Federal Accreditations A2LA — ISO 17025 1461.01 AIHA 100789 QLA— ISO 170255 1461.02 DOD 1461.01 Canada 1461.01 USDA S-67674 EPACrypto--TN00003 ' Drinking Water ' Underground Storage Tanks ' Aquatic Toxicity' Chemical/Microbiological '-Mold "a Accreditation not applicable Our Locations ESC Lab Sciences has sixty-four client support centers that provide sample pickup and/or the delivery of sampling supplies. Ifyou would like assistance from one of our support offices, please contact our main office. ESC Lab Sciences performs all testing at our central laboratory. L.A �y ME MT ND �p OR �q rAN 7 T ID SD v✓1 NY VJY 1A Q ----`� T rA NV q NE T 7 `1 T 1 r,� UT T T A �O VVV T CA KS FAT. KY T ,� ♦ * 'N f--� AZ Nryl OK AF� e a ® T 5C MS A GC, + • i AK � ® FL ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: Soil & Env. Consultants - Raleigh, NC GW -1 1061-200 L861403 09/29/1617:12 23 of 25 y x� Billing information: Analysis'/.Container/Preservative - Chalnof Custody ' Page of Soil &Env. Consultants -Raleigh, NC attn: Don Wells 8412 'FaI 26 ; Is of Neuse Road *ESC 8412 Falls of Neuse Road, Suite 104 Suite lq4 Raleigh, NC 27615-3543 g � Raleigh, NC 27615-3543 L•A'e 5•C•f-EaN•C•E•5 Ross I.A.—Rd Reportto: ErttailTo.dwells@sandec.com Mr. Don Wells - Lb ID� - Peobeau47sassse7 ft—: 600.767-5859 Fac 615.788-5859 Project City/State CI State - Description: Groundwater Job#1061 Collected: tiz Phone; 919-846-5900 Client Project # Lab Project # Fax: 919-846-9467 GW -1 1061 200 SOILENV-J081061 a ro`" - Collected by(print): nn Slte/Faality.ID# P.O. -'�- - - Acctnum:SOILENV � w a., CL 0. J Q f -T4885 Prelogin P 56687 ge Collected by (signature): Imo• CtJQ�% - Rush? (tab MUST Be Notified) Same Day........... 200% DateResults Needed . , ,... - it c--�•" �" V % dam„ _ _ Next Day............ 100% Email?_No X Vey - ' s'_ p �=- TSR: 064 Immediately Packed on Ice N _ Y ��. _Iwo Day ......:......... ...-........50% _ Three Day.............................25% No FAX? _No _Yes Of H. �; O� Q ;o: d• 0 o G. - PBa S 'Date ntrs Shipped wa:FedEXGround Sample ID Comp/Grab Matrix" Depth - Time A` t0 .• >. SO .1-.:: '. --. '-- :---;:':� RemJConwminant SampleM llab only)' MW-2AGW 4 1 Xv . X X'" MW -3 GW %^12-% G :Za 4 X X X MW -4A GW y,'22-1 4 X X s X, TRIP BLANK GW �ti,zy ZZ. I: 1 _ X � I i - Matrix: SS - Soil GW - Groundwater WW -Wastewater DW- Drinking Water OT - Other Bntarks: �� pH Temp Flow Other Hold if Re nquis d by (Signas>ure _ Date: Time: Received by (Signa uree) Samples returned via: 17 UPS Condition: - (lab use only) L /7Jil2YA:; -Z146.,'. C �Z,: J ): ❑FedEx ❑Courier ❑_ .p�IL. _ ---^ Relinquished by (Sig�neture) "' - Date: Timer -. - Received by: (Signa ute)' Temp: - °C =Bottles Received; COC Seal Intact: _Y'I N_NA Relinquished by (Signature): ,�', Date: Time: Recelved for lab_ by: (Signature) Date:.. e: pH Checked: NCF:: ' ., _ . #04 L -A-6 S-C-I-E-N-C-E.s 'Co-oler Receipt Form Client: SDG# So ZUNI% Cooler Received/Opened On: Temperature Upon Receipt: 'c Received By: Michael Witherspoon Signature: Receipt Check List Yes No N/A Were custody seals on outside of cooler and intact? �'c'65to r6ijdrlv'filled '60 dy. apers"pi L a Did all bottles arrive in good condition? Were correct bottles used for the a'naly'ses requested? - Was sufficient amount of sample sent in each bottle? Were all applicablesample containers correctly preserved and' checked for preservation? (Any not in accepted range noted on COQ If applicable, was an observable VOA headspace present? Non conformance -Generated.. (if yes see attached NCF)