NC0024911_Alternate Species Toxicity Test_20160811

Metropolitan Sewerage District
OF BUNCOMBE COUNTY, NORTH CAROLINA
FF �OOUNTY. NOPSN
Environmental Sciences Branch
Division of Water Quality
NCDENR
1621 Mail service Center
Raleigh, NC 27699-1621
Dear Ms. Moore:
August 11, 2016
AUG 16 2016
Mater Quality
Permitting Section
Enclosed are the results of the alternate species toxicity testing, Fathead Minnow Survival and
Growth testing, performed week of July 18t", 2016. This is the first of four required alternate
species toxicity test for our NPDES permit renewal. A copy of these results will be attached to
our July 2016 Discharge Monitoring Report. Additionally, a copy was sent to the permit writer,
Teresa Rodriguez.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Peter Weed, Director
Treatment and Maintenance Division
Metropolitan Sewerage District of Buncombe County
cc: Teresa Rodriguez
Protecting Our Natural Resources -
2028 RIVERSIDE DRIVE, ASHEVILLE, NORTH CAROLINA 28804 TELEPHONE: [phone] FAX: [phone] WEBSITE: www.msdbc.org

�IaceAna[Xicafo
wvnxpaiWabs.com
1
August 04, 2016
Mr. Wayne Tipton
Metropolitan Sewerage District
2028 Riverside Drive
Asheville, NC 28804
RE: Project: NC0024911 7/18
Pace Project No.: 92305439
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Dear Mr. Tipton:
Enclosed are the analytical results for sample(s) received by the laboratory on July 18, 2016. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Since ely,
c
lorri Patton
[e-mail]
Project Manager
Enclosures
cc: Ms. Shannon Bergeron, Metropolitan Sewerage District Ms. Sheila Kilby, Metropolitan Sewerage District
Mr. Roger Edwards, Metropolitan Sewerage District Mr. Monty Payne, Metropolitan Sewerage District
,, REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
6 without the written consent of Pace Analytical Services, Inc.. Page 1 of 1

P
�nb ronatere� , Ires.
P.O. I30X'IE4414, Greenvi 1e, sG zgw5
(664) 877ZQ42.4=AX [phone]
4 Craftsman Court, Gmer, 5C 26650
Fathead Minnow Survival and Growth Test
EPA -821-R-02-013 Method 1000
Client: MSD OF BUNCOMBE COUNTY
Facility: WRF EFFLUENT
NPDES #: NCO024911
Permit Renewal Second Species Testing
Test Date:
19 -Jul -16
Laboratory ID#: T47365 P PROMELAS
Test Reviewed and Approved By:
l
gi/�
Robert W. Kelley, Ph.D.
QA/QC Officer
1"'M=0001 Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept. of Health. Included results pertain only to provided samples.
Page 1 of 6
Farhad Rostampour
Laboratory Director
SCDHEC Certification #23104
NCDENR Certification # 022

M
Eff kient Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test
Facility: Buncombe Co. MSD NPDES # NCO024911
x rte.
Signature of Operator in
x
Signature of Laboratory
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Pipe #: 001 County: Buncombe
Test Initiation Date/rime
7-19-16
/ 1400
/ 7.3
7.6
Avg WVSurv. Control 1 0.7145
Test Organisms
% Eff. Repl.
1
2
3
4
/ 7.4
=Cultured In -House
Control Surviving #
10
10
10
10
% Survival 100.0%
Q X Outside Supplier
Original #
10
10
10
10
246
1 24.8
WVoriginal (mg)
0.6010
0.7910
0.6800
0.7860
Avg Wt (mg) 0.7145
Hatch Date: 7/18-19/16
0 Surviving #
10
10
10
10
% Survival 100.0%
Hatch Time: 1600-1000
Original #
10
10
10
10
WVoriginal (mg)
0.8170
0.7540
0.8040
0.9560
Avg Wt (mg) 1 0.8328
>48.0%
© Surviving #10
10
10
10
% Survival 100.0%
684
Original #
10
10
10
10
Chiorine(mg/L)
WVoriginal (mg)
0.8260
0.8450
0.8620
0.8230
Avg Wt (mg) 0.8390
12 Surviving #
10
10
10
10
% Survival 100.0%
Original #
10
10
10
10
YVVoriginal (mg)
0.7400
0.9100
0.8060
0.6730
Avg Wt (mg) 0.7823
Dilution H2O
24 Surviving #
10
10
10
10
% Survival 100.0%
11
Original #
10
10
10
10
WVoriginal (mg)
0.7080
0.7040
0.7220
0.7270
Avg Wt (mg) 0.7153
48 Surviving#
9
9
9
10
% Survival
33.1
Original #
10
10
10
10
11
21
WVoriginal (mg)
0.6900 1
0.6960
0.7220
0.7190
Avg Wt (mg) 0.7068
18
Water Quality Data
18
Day
48
Control
0
1
2
3
4 5 6
pH (SU) InitlFin
DO (mg/L) [nit/Fin
Temp (C) InitlFin
High Concentration
pH (SU) Init/Fin
DO (mg/L) Init/Fin
Temp (C) Init/Fin
7.8
/ 7.3
7.6
/ 7.3
7.6
/ 7.3
7.6
/ 7.4
7.6
/ 7.3
7.7
/ 7.3 , 7.7
/ 7.4
8.2
/ 7.6
8.2
/ 6.6
7.9
/ 6.0
7.8
/ 7.1
7.7
/ 7.0
7.8
/ 6.8 7.9
/ 6.5
246
1 24.8
24.8
/ 250
1 25.0
1 24 8
24.7
/ 25.5
24.8
1 253
24.6
/ 25.1 245
! 24.8
0 1 2 3 4 5 6
7.8
/ 7.7
1 7.6
/ 7.6
7.7
/ 7.8
8.0
/ 7.6
7.8
/ 7.6
7.9
/ 7.4
1 7.6
/ 7.4
8.5
/ 6.8
7.5
/ 5.8
8.7
/ 5.5
7.4
/ 6.1
8.2
/ 6.4
8.1
/ 5.0
6.5
/ 5.7
25.0
/ 248
24.8
/ 250
250
/ 24.8
25.1
/ 25.5
25.2
/ 263
24.7
1 261
24.6
/ 248
Sample
1
2
3
Survival
Growth
Overall Result
Collection Start Date
7-17-16
7-19-16
7-21-16
Normal
0M] no
O 93 yes
ChV >48%
Grab
Hom. Var.
- 1.3 yes8�.
no
Composite (Duration)
24 hr
24 hr
24 hr
NOEC
48.0%
48.0%
Hardness (mg/L)
90.0
81.6
76.0
LOEC
>48.0%
>48.0%
Alkalinity (mg/l.)
148.1
152.2
155.5
ChV
>48.0%
>48.0%
Conductivity (umhos/cm)
681 1
630
684
Method
Steels
Dunnetts
Chiorine(mg/L)
<0.05 1
<0.05
1 <0.05
Temp at Receipt ( C)
0.1
1.3
1.4
Stats
Survival
Growth
Conc.
Critical
Calculated
Critical
Calculated
Dilution H2O
3
11
18
11
24
Hardness (mg/L)
46.0
6
11
18
11
26
Alkalinity (mg/L)
33.1
12
11
18
11
21
Conductivity (umhos/cm)
182
24
11
18
11
18
48
11
12
11
18
DWQ Form AT -5 (1/04)
"Page 2 of 6
i

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Page 3 of 6
Lab#
T47365 P PROMELA
Client
MSD OF BUNCOMB
Sample ID
EFFLUENT
NPDES#
N00024911
County
0
Month
7
Start 6 fed Date
19-JUI-16
Start 6 fed Time
1400
Started R fed By
AH
Teat Organism
Pimephales promela
Neo. born date
<48 HRS
Neo. born time
ABS 7-18-16
Test Type
NCCD
Dilution Water
SSF 7-9-16 C
Units for Conc.
%
%3rd BROOD
MMMMMMMMMMM
Test vessels
400 ml
Teat volume
250 ml
Incubator#
1
Light
16It/Bdk
Initial Tenn p°C
25
MMMMMMMMMMM
1.159 2XDAY
Test method
IEPA b]1 -R- 4131000
•
©--------------_—_�
Page 3 of 6
Lab#
T47365 P PROMELA
Client
MSD OF BUNCOMB
Sample ID
EFFLUENT
NPDES#
N00024911
County
0
Month
7
Start 6 fed Date
19-JUI-16
Start 6 fed Time
1400
Started R fed By
AH
Teat Organism
Pimephales promela
Neo. born date
<48 HRS
Neo. born time
ABS 7-18-16
Test Type
NCCD
Dilution Water
SSF 7-9-16 C
Units for Conc.
%
%3rd BROOD
Test vessels
400 ml
Teat volume
250 ml
Incubator#
1
Light
16It/Bdk
Initial Tenn p°C
25
Artemis
1.159 2XDAY
Test method
IEPA b]1 -R- 4131000
Comments
All reps have 10
organisms unless noted otherwise.
CON TEMP
Initial-
24.6
DAY 1-
24.8
SSF 7-9-16D
DAY 2-
25
DAY 3-
24.7
DAY 4-
24.8
DAY 4, SSF 7-9-16E
DAY 5 -
24.6
DAY 6 -
24.5
SSF 7-14-16A

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PO Box 16414, Greenville, SC 29606-:77414
[phone], [phone] Fmc(864) 877 6938
Shipping Address: 4 Craftsman Ct, Greer, SC 29650
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CHATN 'toF CUSTODY RECORD
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COMPOSITE SAMPLIMG PROCEDURES TEMPERATURE d40MITORIArG PROCEDURES HOLD 71.41E PROCEDURES
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicih, testing the sample must first be used mithin 36 hours
Time Proportional: I sample each hour for 24 hours. Equal volui 0.0 and 6.0 °C. Samples must not be frozen. Use water ice in sealed bas. - of sample collection (completion of composite sample).
or at minimum I sample every 4 hours over 24 hours. Sample may not be used after 72 hours from sample Collection.
Plow Proportional: As per instructions in NPDES permit.

ETT
PO Box 16414, Grearnille, SC 29806-7414
[phone], [phone] Fax:[phone]
Shipping Address: 4 Craftsman Ct, Greer, SC 29650
WWV. ENVIRONMENTAI..Cct,
CHAIN -OF CUSTODY RECORD
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Date Time Relinquished By / rgani�zatiio/�nr�\
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COMPOSITE SAMPLING PROCEDURES MUPER-4TURE d90MITORIlJG PROCEDURES HOLD TINE PP.00EDUR S
Composite samples must be collected over a 24 hour period. Sample temperature during collection and transport must be between For toxicity testing The sample must first be used 1i•ithin 36 hours
Time Proportional: 1 sample each hour for 24 hours. Equal volul 0.0 and 6.0 °C. Samples most not be frozen. Use water ice in sealed bas. of sample collection (completion of composite sample).
or at minimum 1 sample every 4 hours over 24 hours. Sample may not be used after 72 hour from sample collection.
Flow Proportional: As per instructions in NPDES permit.

CHAIN G -c CUSTODY RECORD
PO Box
16414, Greenville, SC 29606-7414
[phone], [phone] Fa)c(854) 877 6938
Shipping Address: 4 Craftsman Ct. Greer, SC 29650
WWl�'CNVIQONMMN AL.r-t3M

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PO. BOX 1W4, GreOnAle, 5C 29606
(6fi4) 877.6942. FAX g864j 81.7-693B
4 Craftsman Court, Greer, 5C 29650
Fathead Minnow Survival and Growth Test
EPA -821-R-02-013 Method 1000
Client: BUNCOMBE CO MSD
Facility: EFFLUENT
NPDES #: NCO024911
Permit Renewal Second Species Testing
Test Date:
Laboratory ID#: T47223
Test Reviewed and Approved By:
414
Robert W. Kelley, Ph.D.
QA/QC Officer
Certification #E87819
Test results presented in this report conform to all requirements of
NELAC, conducted under NELAC Certification Number E87819
Florida Dept. of Health. Included results pertain only to provided samples.
Page 1 of 8
21 -Jun -16
J 4
Farbad Rostamppour
Laboratory Director
SCDHEC Certification #23104
NCDENR Certification # 022

�Effluent Toxicity Report Form -Chronic Fathead Minnow Multi -Concentration Test
Facility: Buncombe Co. MSD NPDES # NCO024911 Pipe #: 001 County: Buncombe
Laboratory: Comments
Si nature of Operator' Spon ible Ch e
x
Signature of Laboratory Supervisor
MAIL ORIGINAL TO: Environmental Sciences Branch
Division of Water Quality
NC DENR
1621 Mail Service Center
Raleigh, NC 27699-1621
Test Initiation Date/Time
21 -June -16
/ 1400
/ 7.5
7.8
Avg WUSurv. Control 1 0.7303
Test Organisms
% Eff. Repl.
1
2
3
4
7.8
=Cultured In -House
Control Surviving #
10
10
9
10
%Survival 97.5%
Q X Outside Supplier
Original #
10
10
10
10
7.4
/ 6.2
Wt/original (mg)
0.7990
0.6120
0.6580
0.7790
Avg Wt (mg) 0.7120
Hatch Date: 6/20 - 6/21
0 Surviving #
10
10
10
10
% Survival 100.0%
Hatch Time: 1600 -11000
Original #
10
10
10
10
Wt/original (mg)
0.6760
0.5780
0.7530
0.6370
Avg Wt (mg) 0.6610
© Surviving #
10
10
9
10
% Survival
Original #
10
10
10
10
Wt/original (mg)
0.6440
0.5450
0.5780
0.6710
Avg Wt (mg) 0.6095
12 Surviving #
10
10
10
10
% Survival 100.0%
Original #
10
10
10
10
WUoriginal (mg)
0.7280
0.6370
0.7230
0.6420
Avg Wt (mg) 0.6825
24 Surviving #
10
9
10
10
% Survival
Original #
10
10
10
10
WUoriginal (mg)
0.6620
0.4890
0.6090
0.6590
Avg Wt (mg) 0.6048
!- 48 Surviving #
10
10
10
10
% Survival 100%
Original #
10
10
10
10
WUoriginal (mg)
0.5730
0.6280
0.5800
0.5320
Avg Wt (mg) 0.5783
Water Quality Data
Day
Control
0
1
2
3
4 5 6
pH (SU) Init/Fin
DO (mg/L) Init/Fin
Temp (C) [nit/Fin
High Concentration
pH (SU) Init/Fin
DO (mg/L) Init/Fin
Temp (C) InitlFin
Sample
Collection Start Date
Grab
Composite (Duration)
Hardness (mg/L)
Alkalinity (mg/L)
Conductivity (umhos/cm)
Chlorine(mg/L)
Temp at Receipt,( C)
7.6
/ 7.5
7.7
/ 7.5
7.8
/ 7.6
7.7
/ 7.6
7.7
/ 7.6
7.8
/ 7.7
7.8
! 7.5
7.4
/ 8.0
7.6
/ 7.7
7.8
/ 5.6
8.0
/ 6.1
8.6
/ 6.7
7.5
/ 6.8
7.4
/ 6.2
244
I 249
24.6
/ 25.0
245
/ 25.0
25.0
/ 24.9
24 9
/ 24.0
24.8
/ 24.8
24.6
/ 25.4
0 1 2 3 4 5 6
7.3
/ 7.8
7.7
/ 7.9
7.9
/ 7.8
8.0
/ 7.8
7.9
/ 7.7
7.8
/ 7.8
7.9
/ 7.2
7.6
/ 8.1
7.8
/ 7.0
8.1
/ 5.5
7.4
/ 5.6
8.2
/ 6.8
8.0
/ 6.2
7.9
/ 5.6
25.0
I 24.9
24.6
I 25.0
24.5
1 25.0
25.0
I 24.9
25.0
1 24.0
24.8
/ 24.8
24.5
/ 25.4
1
2
3
6-19-16
6-21-16
6-23-16
188
Conductivity (umhos/cm)
0 yes
24 hr
24 hr
24 hr
44.0
52.0
52.0
157.0
162.5
135.4
580
633 1
682
0.07
<0.05
<0.05
0.2
0.0 not frozen
0.7
Dilution H2O
Survival
Hardness (mg/L)
48.0
29.10
Alkalinity (mg/L)
188
Conductivity (umhos/cm)
Stats
Conc.
3
6
12
24
48
Page 2 of 8
DWQ Form AT -5 (1/04)
Survival
Critical
In
10
10
10
10
Survival
Growth Overall Result
NormalXD
no
[::] yes ChV
Hom. Var.
7 yes
0 yes
NOEC
48%
24%
LOEC
>48%
48%
ChV
>48%
33.9%
Method
Steels
Dunnetts
Stats
Conc.
3
6
12
24
48
Page 2 of 8
DWQ Form AT -5 (1/04)
Survival
Critical
In
10
10
10
10
Growth
Calculated
Critical
Calculated
20
2.41
1.06
18
2.41
2.14
20
2.41
0.61
18
2.41
2.23
20
2.41
2.79

.- g • 1 Davi I Dav 7_ I Dav 3 I Dav 4 I Dav 5 I D-6 I Dav 7 lWelahtl Fecundity
Page 3 of 8
Lab*
T47223
Client
BUNCOMBE CO MS
Sample ID
EFFLUENT
NFDES#
NCO024911
County
0
Month
6
Start & fed Date
21 -Jun -16
Start & fed Time
1400
Started & fed By
AM
Teat Organism
Pimephales promela
Neo. born dale
<48 HRS
Neo. born time
ABS HATCH 6-20-1
Teat Type
NCCD
Dilution Water
SSF 6-15-16
Units for Cone.
%
%3rd BROOD
Test vesaela
400 ml
Testvoiume
250 ml
Incubator#
1
Light
161t/8dk
InitialTemp°C
25
Artem in
.15g 2X DAY
Teat method
EPA 821-R-02-813.1888
All reps have 1 U
organisms unless noted otherwise.
;ON TEMP
NITIAL-
24.4
MY 1 -
24.6
)AY 2 -
24.5
MY 3-
25
MY 4-
24.9
)AY5 -
24.8
MY 6 -
24.6

Chain 04 -'Custody
Buncombe Co Mo
aceAn'alydbal(D
www.pac--Iabs.com
Workorder: 92302055 Workorder Name: NC0024911 6120
Results Requested By:
7/5/2016'
. . . . . . . . . .
. wa r
M
Lord Patton
Pace Analytical Asheville P.O.--' A V 10
2225 Riverside Dr.
Asheville, NC 28804
Phone [phone]
E TT
Email: [e-mail]
State of Sample origin: NC
U70 7
Z
Z
LAB USE ONLY
PLANT EFFLUENT 6/20/2016 08:34 92302055001 Water
x
2
2aQ3 A
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LMzP.i., o'Qmii"
Transfers Release By Daterrime Reo,-�
,d Date/Time
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Cooler Temperature on Receipt O.OC Custod yj Seal Y or N Received on Ice� Y2or N
Sam ples Intaq( Y N
Monday, June 20, 2016 2:33:50 PM FMT-ALL-C-002rev.00 24March2009 Page 1 of 1

—ET A_ —
PO Box 15414, Greenville, SC 29606-7414
[phone], [phone] Fax.[phone]
Shipping Address: 4 Craftsman Ct, Greer, SC 29650
WWW-=rENV1R0NME AL.CGM
C tiF CUSTODY RECORD 16/130 , ),��
Lase of
Client: — -
Le'--
'MS—bt
Program
Containers
Presenative
Parameters
Facility:
Whole Lfilucrtt Tosicih•
—
State: r, NPDES #:' J Cj i
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