NC0021920_Annual Monitoring & Polluant Scan_20160518

,0YtlTEvjJ
<j, Terry L.Mann
Mayor
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BS I�I: I Jimmy Clarida
%iu'or Pro-Tem
��— Tim Blackmon
Council Member
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1833 City ofW/iitevitiTè Robert Leder
Council,$1enncer
Vickie Pail
Darren Currie Council Member
Cit; alunu,er Sara B. Thompson
317 S.Madison Street Council Member
PO Box 607 Harold G. Troy,Sr.
Whiteville,NC 28472 Council Member
May 18, 2016
RECEIVED/NCDEQ/DUVR
Mr. Charles H.Weaver JUN 0 3 2016
NCDEQ/DWR/NPDES
1617 Mail Service Center Water Quality
Pen-nittiny Section
Raleigh, N.C. 27699-1617
Dear Mr. Weaver:
Please find enclosed for your review,the annual Priority Pollutant Analysis for NPDES Permit NC0021920
for the Whiteville Wastewater Reclamation Facility. If you have any questions, please feel free to
contact me at 910—642-5818.
Sincerely,�
J
Newlyn McCullen
WWRF Superintendent
Enclosure: 2016 Priority Pollutant Analysis

." 100(
Annual Monitoring and Pollutant Scan
Permit No. NC0021920 Month April
Outfall 001 Year 2016
Facility Name Whiteville Wastewater Reclamation Facility ORC Newlyn McCullen
Date of sampling April 7, 2016 Phone [phone]
Analytical Laboratory Environment 1, Inc.
Sample Analytical Quantitation Sample Units of Number of
Parameter Type Method Level Result Measurement
Ammonia (as N) Composite RECEIVCDINC DE
Dissolved oxygen Grab J U N 0 3 2016
Nitrate/Nitrite Composite
y
Total Kjeldahl nitrogen Composite Wal�f Section SSection
Total Phosphorus Composite
Total dissolved solids Composite SM2540C 290 mg/L 1
Hardness Composite SM2340C 95 mg/L 1
Chlorine (total residual, TRC) Grab
Oil and grease Grab
Metals(total recoverable),cyanide and total phenols
Antimony Composite EPA200.8 <3.0 ug/L 1
Arsenic Composite SM3113B <5.0 ug/L 1
Beryllium Composite EPA200.7 <1.0 ug/L 1
Cadmium Composite SM3113B <1.0 ug/L 1
Chromium Composite EPA200.7 <5.0 ug/L 1
Copper Composite EPA200.7 <10 ug/L 1
Lead Composite SM3113B <5.0 ug/L 1
Mercury Composite EPA245.1 <0.2 ug/L 1
Nickel Composite EAP200.7 <10 ug/L 1
Selenium Composite SM3113B <10 ug/L 1
Silver Composite EPA200.7 <5.0 ug/L 1
Thallium Composite EPA200.8 <1.0 ug/L 1
Zinc Composite SM3111B 22 ug/L 1
Cyanide Grab SM4500CNE <0.005 mg/L 1
Total phenolic compounds Grab EPA420.1 <5.0 ug/L 1
Volatile organic compounds
Acrolein Grab EPA624 <100 ug/L 1
Acrylonitrile Grab EPA624 <50 ug/L 1
Benzene Grab EPA624 <5.0 ug/L 1
Bromoform Grab EPA624 <5.0 ug/L 1
Carbon tetrachloride Grab EPA624 <5.0 ug/L 1
Chlorobenzene Grab EPA624 <5.0 ug/L 1
Chlorodibromomethane Grab EPA624 <5.0 ug/L 1
Chloroethane Grab EPA624 <10 ug/L 1
2-chloroethylvinyl ether Grab EPA624 <10 ug/L 1
Chloroform Grab EPA624 <5.0 ug/L 1
Dichlorobromomethane Grab EPA624 <5.0 ug/L 1
1,1-dichloroethane Grab EPA624 <5.0 ug/L 1
1,2-dichloroethane Grab EPA624 <5.0 ug/L 1
Trans-1,2-dichloroethylene Grab EPA624 <5.0 ug/L 1
Form - DMR- PPA-1 Page 1

Annual Monitoring and Pollutant Scan
Permit No. NC0021920 Month April
Outfall 001 Year 2016
Sample Analytical Quantitation Sample Units of Number of
Parameter Type Method Level Result Measurement samples
Volatile organic compounds (Cont.)
1,1-dichloroethylene Grab EPA624 <5.0 ug/L 1
1,2-dichloropropane Grab EPA624 <5.0 ug/L 1
1,3-dichloropropylene Grab EPA624 <5.0 ug/L 1
Ethylbenzene Grab EPA624 <5.0 ug/L 1
Methyl bromide Grab EPA624 <10 ug/L 1
Methyl chloride Grab EPA624 <10 ug/L 1
Methylene chloride Grab EPA624 <10 ug/L 1
1,1,2,2-tetrachloroethane Grab EPA624 <5.0 ug/L 1
Tetrachloroethylene Grab EPA624 <5.0 ug/L 1
Toluene Grab EPA624 <5.0 ug/L 1
1,1,1-trichloroethane Grab EPA624 <5.0 ug/L 1
1,1,2-trichloroethane Grab EPA624 <5.0 ug/L 1
Trichloroethylene Grab EPA624 <5.0 ug/L 1
Vinyl chloride Grab EPA624 <10 ug/L 1
Acid-extractable compounds
P-chloro-m-creso Grab ug/L
2-chlorophenol Grab EPA625 <10 ug/L 1
2,4-dichlorophenol Grab EPA625 <10 ug/L 1
2,4-dimethylphenol Grab EPA625 <10 ug/L 1
4,6-dinitro-o-cresol Grab EPA625 ug/L 1
2,4-dinitrophenol Grab EPA625 <50 ug/L 1
2-nitrophenol Grab EPA625 <10 ug/L 1
4-nitrophenol Grab EPA625 <50 ug/L 1
Pentachlorophenol Grab EPA625 <50 ug/L 1
Phenol Grab EPA625 <10 ug/L 1
2,4,6-trichlorophenol Grab EPA625 <10 ug/L 1
Base-neutral compounds
Acenaphthene Grab EPA625 <10 ug/L 1
Acenaphthylene Grab EPA625 <10 ug/L 1
Anthracene Grab EPA625 <10 ug/L 1
Benzidine Grab EPA625 <100 ug/L 1
Benzo(a)anthracene Grab EPA625 <10 ug/L 1
Benzo(a)pyrene Grab EPA625 <10 ug/L 1
3,4 benzofluoranthene Grab EPA625 <10 ug/L 1
Benzo(ghi)perylene Grab EPA625 <10 ug/L 1
Benzo(k)fluoranthene Grab EPA625 <10 ug/L 1
Bis (2-chloroethoxy) methane Grab EPA625 <10 ug/L 1
Bis (2-chloroethyl) ether Grab EPA625 <10 ug/L 1
Bis (2-chloroisopropyl) ether Grab EPA625 <10 ug/L 1
Bis (2-ethylhexyl) phthalate Grab EPA625 <20 ug/L 1
4-bromophenyl phenyl ether Grab EPA625 <10 ug/L 1
Butyl benzyl phthalate Grab EPA625 <10 ug/L 1
2-chloronaphthalene Grab EPA625 <10 ug/L 1
4-chlorophenyl phenyl ether Grab EPA625 <10 ug/L 1
Form - DMR- PPA-1 Page 2

r Annual Monitoring and Pollutant Scan
Permit No. N C0021920 Month April
Outfall 001 Year 2016
Sample Analytical Quantitation Sample Units of Number of
Parameter Type Method Level Result Measurement samples
Base-neutral compounds (cont.)
Chrysene Grab EPA625 <10 ug/L 1
Di-n-butyl phthalate Grab EPA625 <10 ug/L 1
Di-n-octyl phthalate Grab EPA625 <10 ug/L 1
Dibenzo(a,h)anthracene Grab EPA625 <10 ug/L 1
1,2-dichlorobenzene Grab EPA625 <10 ug/L 1
1,3-dichlorobenzene Grab EPA625 <10 ug/L 1
1,4-dichlorobenzene Grab EPA625 <10 ug/L 1
3,3-dichlorobenzidine Grab EPA625 <10 ug/L 1
Diethyl phthalate Grab EPA625 <10 ug/L 1
Dimethyl phthalate Grab EPA625 <10 ug/L 1
2,4-dinitrotoluene Grab EPA625 <10 ug/L 1
2,6-dinitrotoluene Grab EPA625 <10 ug/L 1
1,2-diphenylhydrazine Grab EPA625 <10 ug/L 1
Fluoranthene Grab EPA625 <10 ug/L 1
Fluorene Grab EPA625 <10 ug/L 1
Hexachlorobenzene Grab EPA625 <10 ug/L 1
Hexachlorobutadiene Grab EPA625 <10 ug/L 1
Hexachlorocyclo-pentadiene Grab EPA625 <10 ug/L 1
Hexachloroethane Grab EPA625 <10 ug/L 1
Indeno(1,2,3-cd)pyrene Grab EPA625 <10 ug/L 1
Isophorone Grab EPA625 <10 ug/L 1
Naphthalene Grab EPA625 <10 ug/L 1
Nitrobenzene Grab EPA625 <10 ug/L 1
N-nitrosodi-n-propylamine Grab EPA625 <10 ug/L 1
N-nitrosodimethylamine Grab EPA625 <10 ug/L 1
N-nitrosodiphenylamine Grab EPA625 <10 ug/L 1
Phenanthrene Grab EPA625 <10 ug/L 1
Pyrene Grab EPA625 <10 ug/L 1
1,2,4,-trichlorobenzene Grab EPA625 <10 ug/L 1
"I certify,under penalty of law,that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of
the person or persons who managed the system,or those persons directly responsible for gathering the information,the information
submitted is,to the best of my knowledge and belief,true, accurate,and complete. I am aware that there are significant penalties for
submitting false information, including the possibility of fines and imprisonment for knowing violations."
Authorized Representative name
Newlyn McCullen
ly`n
Signatur
'5/'/ it
Dat
Form - DMR- PPA-1 Page 3

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GREENVFLLEi N.C.27835-7085
RECEIVED/NCDEQ/DWR
ID#: 856
JUN 0 3 2016
CITY OF WHITEVILLE (PPA SCAN)
MR. NEWLYN MCCULLEN Water Quality
P.O. BOX 607 DATE COLLECTED: �4rj0 jSection
WHITEVILLE ,NC 28472 DATE REPORTED : 05/16/16
REVIEWED BY•
Effluent Analysis ilfethod
PARAMETERS Date Analyst Code
Phenol, ugh! <5 04/18/16 SEJ 420.1-78
Total Cyanide, mg/1 <0.005 04/14/16 SEJ 4500CNE-99
Total Hardness, mg/I 95 04/11/16 CMC 2340C-97
Total Dissolved Residue, mg/I 290 04/11/16 KKF 2540C-97
Antimony, ugh! <3 04/21/16 LFJ EPA200.8
Arsenic, ugh' <5.0 04/14/16 MTDI 3113B-04
Beryllium, ug/1 <1.0 04/11/16 LFJ EPA200.7
Cadmium, ug/1 <1.0 04/12/16 MTM 3113B-04
Total Chromium, ug/1 <5.004/11/16 I,FJ EPA200.7
Copper, ug/1 <10 04/11/16 LFJ EPA200.7
Lead, ug/I <5.0 04/13/16 MTM 3113B-04
Mercury, ug/1 <0.2 04/25/16 Ji1'1N 245.1 R3-94
Nickel, ug/1 <10 04/11/16 LFJ EPA200.7
Selenium, ugh! <10 04/15/16 MTM 3113B-04
Silver, ug/1 <5.0 04/11/16 LFJ EPA200.7
Thallium, ug/I <1 04/21/16 LFJ EPA200.8
Zinc, ug/I 22 04/12/16 LFJ EPA200.7

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PO.BOX 7085, 114 OAKMONT DRIVE PHONE[phone] ':
GREENVILLE.N.C.:27835-7085 EAX:[phone] 1
CLIENT: CITY OF WHITEVILLE (PPA SCAN) CLIENT ID: 856
MR. NEWLYN MCCULLEN
P.O. BOX 607 ANALYST: MAO
WHITEVILLE, NC 28472 DATE COLLECTED: 04/07/16
DATE ANALYZED: 04/15/16
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DATE REPORTED: 05/16/16
REVIEWED BY:
VOLATILE ORGANICS
EPA METHOD 624
Effluent
PARAMETERS, ug/1
1. Chloromethane <10.00
2. Vinyl Chloride <10.00
3. Bromomethane <10.00
4, Chloroethane <10.00
5. '1'richlorofluorontethane <5.00
6. 1,1-Dichloroethane <5.00
7. Methylene Chloride <10.00
8. trans-1,2-Dichloroethene <5.00
9. 1,1-Dichloroethene <5.00
10. Chloroform <5.00
11. 1,1,1-Trichloroethane <5.00
12. Carbon Tetrachloride <5.00
13. Benzene <5.00
14. 1,2-Dichloroethane <5.00
15. Trichloroethene <5.00
16. 1,2-Dichioropropane <5.00
17. Bronaodichloromethane <5.00
18. 2-Chlornethylviuyl Ether <5.00
19. cis-1,3-Dichloropropene <5.00
20. Toluene <5.00
21. trans-1,3-Dichloropropene <5.00
22. 1,1,2-Trichloroethane <5.00
23. Tetrachloroethene <5.00
24. Dibromochloromethane <5.00
25. Chlorobenzene <5.00
26. Ethylbenzene <5.00
27. Bromoform <5.00
28. 1,1,2,2-Tetrachloroethane <5.00
29. l,3-Dichlorobenzene <5.00
30. 1,4-Dichlorobenzene <5.00
3I. 1,2-Dichlorobenzene <5.00
32. Acrolehi <100.00
33. Acrylonitrile <50.00

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CLIENT: CITY OF WHITEVILLE (PPA SCAN) CLIENT ID: 856
MR. NEWLYN MCCULLEN
P.O. BOX 607 ANALYST: CHS
WHITEVILLE, NC 28472 DATE COLLECTED: 04/07/16 Page: 1
DATE EXTRACTED: 04/08/16
DATE ANALYZED: 04/24/16
REVIEWED BY: DATE REPORTED: 05/16/16
SEMIVOLATILE ORGANICS
EPA METHOD 625
Effluent
PARAMETERS, ugh'
1. N-Nitrosodunethylamine <10.00
2. Phenol <10.00
3. Bis(2-Chloroet1yl) Ether <10.00
4. 2-Chlorophenol <10.00
5. 1,3-Dichlorobenzene <10.00
6. 1,4-Dichlorobenzene <10.00
7. 1,2-Dichlorobenzene <10.00
8. Bis(2-Chloroisopropyl) Ether <10.00
9. Hexachloroethane <10.00
10. N-Nitrasodi-N-Propylamine <10.00
11. Nitrobenzene <10.00
12. Isophorone <10.00
13. 2-Nitrophenol <10.00
14. 2,4-Dimethylphenol <10.00
15. Bis(2-Chloroethoxy) Methane <10.00
16. 2,4-Dichlorophenol <10.00
17. 1,2,4-Trichlorobenzene <10.00
18. Naphthalene <10.00
19. Hexachlorobutadiene <10.00
20. 4-Chloro-3-Methylphenol <20.00
21. Hexachlorocyclopeutadiene <10.00
22. 2,4,6-Trichlorophenol <10.00
23. 2-Chloronaphthalene <10.00
24. Acenaphthylene <10.00
25. Dimethylphthalate <10.00
26. 2,6-Dinitrotoulene <10.00
27. Acenaphthene <10.00
28. 2,4-Dinitrophenol <50.00
29. 4-Nitrophenol <50.00
30. 2,4-Dinitrotoluene <10.00
31. Fhiorene <10.00
32. Diethylphthalate <10.00
33. 4-Chlorophenyl Phenyl Ether <10.00
34. 4,6-Diinitro-2-Methylphenol <50.00
35. N-Nitrosodiphenylamh:e <10.00
36. 4-Broniophenyl Phenyl Ether <10.00
37. Hexachlorobenzene <10.00
38. Pentachlorophenol <50.00
39. Phenanthrene <10.00
40. Anthracene <10.00
41. Di-N-Butylphthalate <10.00
42. Fiuoranthene <10.00
43. Benzidine <100.00
44. Pyretic <10.00
45. Bntylbenzylphthlate <10.00
46. Benzo[a]authracene <10.00
47. 3,3-Dichlorobenzadine <10.00
48. Chrysene <10.00

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'GREENVILLE, N.0 27835-7085 FAX[phone]
CLIENT: CITY OF WHITEVILLE (PPA SCAN) CLIENT IDs 856
MR. NEWLYN MCCULLEN
P.O. BOX 607 ANALYST: CHS
WHITEVILLE, NC 28472 DATE COLLECTED: 04/07/16 Paget 2
DATE EXTRACTED: 04/08/16
DATE ANALYZED: 04/24/16
REVIEWED BYs DATE REPORTED: 05/16/16
SEMIVOLATILE ORGANICS
EPA METHOD 625
Effluent
PARAMETERS, ug/l
49. Bis(2-Ethyihexyl)phthalate <20.00
50. Di-N-Octylphthalate <10.00
51. Benzo[b]f uoranthene <10.00
52. Benzo[k]iluoranthene <10.00
53. Benzo[a]pyrene <10.00
54. Indeno(1,2,3-C,d)pyrene <10.00
55. Dibenzo[a,h]anthracene <10.00
56. Benzo[g,h,t]perylene <10.00
57. 1,2-Diphenylhydrazine <10.00

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